icp test report certification packet2014/04/23 · issue date: april 23, 2014 it is hereby...
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1
ICP Test Report Certification Packet
Company name : Littelfuse, Inc. Product Series: 5x20 Cartridge Product #: 213xxxXEP Series Issue Date: April 23, 2014
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.
Issued by: [Global EHS Engineer]
(1) Parts, sub-materials and unit parts This document covers the 5x20 Cartridge RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used
Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1
Remarks:
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2
Table 1: List of Raw Materials covered by this report
ICP ID Raw Material Part Number Raw Material Description Page(s) ICP-052 910-555 Cap – Base & plating 3-10 ICP-053 C909543 Soda Lime Glass Tubes 11-15 ICP-054 C909542 Borosilicate Glass Body 16-20
ICP-0294 082xxx-001 Element - 99% Sn Plated Cu 21-24 ICP-056 687xxx-001 Element – Ag-Cu Sn Plated 25-30 ICP-080 934-077 (C030208) Overcap – Cap & Lead (Base & plating) 31-34 ICP-061 648115 Yarn 35-40 ICP-060 648150 Yarn 41-46 ICP-0118 692535-005 Solder Wire 47-52
Form 585-047 Rev. A 2/21/06
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Durch die DAkkS nach DIN EN ISO/IEC 17025 akkreditiertes Prüflaboratorium Die Akkreditierung gilt für die in der Urkunde aufgeführten Prüfverfahren.
Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] USt-IdNr. DE169317871 Jan-Jörg Müller-Seiler
Intertek Consumer Goods GmbH · Würzburger Straße 152 · 90766 Fürth · Germany
Polyfil AG Gina Gregorio Oberallmendstrasse 20A
6300 Zug / Switzerland Fürth, 2013-12-17
Test report No. FUHLP2013-3898
Testing of a material sample according to the RoHS directive 2011/65/EC
Sample description: Cu99.9MSn
Arrival in lab: 2013-12-02; Period of analysis: 2013-12-04 – 2013-12-13 Head of Inorganic Lab: Claudia List
Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item. This report consists of 6 page(s). The test methods signed with * are not listed in the attachment of the accreditation certificate.
Conclusion based on tested item
Test order Status testing according to the RoHS directive 2011/65/EC pass°
° Please see overview of test results
- Test results see next pages -
Littelfuse Philippines Inc.Arsenio M. Cesista Jr.LIMA Technology Center, SEZ
4233 Malvar / Batangas
Littelfuse Philippines Inc. Arsenio M. Cesista Jr. LIMA Technology Center, SEZ 4233 Malvar / Batangas
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Sample description: Cu99.9MSn
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Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Jan-Jörg Müller-Seiler
nM = non Metal M = Metal cM = composite Material
List of component parts:
Sample No. Part No. Material Description
334031 1 M Tinned copper wire
Photo: �
Sample No. 334031
Part No. 1
Analysis of metals by ICP-MS, results in mg/kg Method: Pb, Cd, Cr: DIN EN ISO 17294-2** Digestion: with conc. HNO3 + HCl** Detection limit: Pb 5.0 mg/kg, Cd 1.0 mg/kg, Cr 10 mg/kg, Hg: 0.5 mg/kg
Sample No. Part No. Pb Hg Cd Crtotal Status
334031 1 50 <0.5 <1.0 <10 pass
Comment: Elements RoHS-limit valueLead (Pb) 1000 mg/kg Mercury (Hg) 1000 mg/kg Cadmium (Cd) 100 mg/kg Chromium VI (Cr VI) 1000 mg/kg Polybrominated Biphenyle (PBBs) 1000 mg/kg Polybrominated Diphenyl ether (PBDEs) 1000 mg/kg
- Flow charts see next page(s) -
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Test Report Number: 140100488SHA-002 ����
Intertek Testing Services Ltd., Shanghai Page 1 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
��������� ���
������801 �������B ��200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Applicant: ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU GMBH Date: Jan. 21, 2014 GEWERBESTRASSE 87, D-98669, VEILSDORF,
GERMANY
Sample Description: One (1) submitted sample said to be: Item Name : Wires with plating Item No. : 101--23-.----tin plated silver copper alloy wire – AgCu, Sn--% Country of Origin : GERMANY
***************************************************************************************************************************************************** Tests conducted:
As requested by the applicant, for details refer to attached page(s). ***************************************************************************************************************************************************** Conclusion:
Tested sample Standard ResultTested components of submitted sample
Restriction of the use of certain hazardous substance in electrical and electronic equipment (RoHS Directive 2011/65/EU)
See Test Conducted
***************************************************************************************************************************************************** To be continued
Prepared and check by:For Intertek Testing Services Ltd., Shanghai
Authorized by:For Intertek testing services Ltd., Shanghai
Joy Zhou Jonny Jing Manager
Applicant: Littelfuse Philippines Inc. Date: Jan. 21, 2014LIMA Technology Center, Lipa City,Malvar, Batangas
Applicant: Littelfuse Philippines Inc. Date: Jan. 21, 2014 LIMA Technology Center, Lipa City, Malvar, Batangas
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Test Report Number: 140100488SHA-002 ����
Intertek Testing Services Ltd., Shanghai Page 2 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
��������� ���
������801 �������B ��200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
(A) Test result of RoHS Directive:
Testing itemResult
(1)
Cadmium (Cd) content (mg/kg) /plating ND
Lead (Pb) content (mg/kg) /plating 17
Mercury (Hg) content (mg/kg) /plating ND
Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) /plating
ND
Testing itemResult
(2)
Cadmium (Cd) content (mg/kg) ND
Lead (Pb) content (mg/kg) ND
Mercury (Hg) content (mg/kg) ND
Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2)
ND
Remark� mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter
ND = not detected
Tested components: (1) Silver color metal wire plating (2) Silver color metal wire substrate
(B) RoHS Requirement:
Restricted substances Limits Cadmium (Cd) 0.01% (100 mg/kg) Lead (Pb) 0.1% (1000 mg/kg) Mercury (Hg) 0.1% (1000 mg/kg) Chromium (VI) (Cr6+) 0.1% (1000 mg/kg) Polybrominated biphenyls (PBBs) 0.1% (1000 mg/kg) Polybrominated diphenyl ethers (PBDEs) 0.1% (1000 mg/kg)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material. ***********************************************************************************************************************************************
To be continued
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Test Report Number: 140100488SHA-002 ����
Intertek Testing Services Ltd., Shanghai Page 3 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
��������� ���
������801 �������B ��200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
(C) Test method:
Testing item Testing method Reporting limit
Cadmium (Cd) content With reference to IEC 62321-5 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Lead (Pb) content With reference to IEC 62321-5 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Mercury (Hg) content With reference to IEC 62321-4 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 mg/kg
Chromium (VI) (Cr6+) content(for metal)
With reference to IEC 62321 Edition 1.0: 2008, by boiling water extraction and determined by UV-VIS Spectrophotometer.
Positive/Negative (Threshold of
0.02mg/kg with 50cm2)
Date sample received: Jan. 13, 2014 Testing period: Jan. 13, 2014 To Jan. 16, 2014
***************************************************************************************************************************************************** To be continued
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Test Report Number: 140100488SHA-002 ����
Intertek Testing Services Ltd., Shanghai Page 4 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
��������� ���
������801 �������B ��200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
(D) Measurement flowchart�
Test for Cd/Pb/Hg/Cr (VI) contents Reference standard�IEC 62321 Edition 1.0�2008&2013
Remarks�
*1�list of appropriate acid�Material Acid added for digestion Polymers HNO3,HCl,HF,H2O2,H3BO3
Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2�If the result of spot test is positive, Chromium VI would be determined as detected. ****************************************************************************************************************************************************
To be continued
No
Yes
Sampling/grinding or cutting
Weigh sample and for different material, digest
the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add diphenyl-carbazide
solution
Cr6+
Analyzed by UV-VIS
Spot test
Get 50cm2
samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved Cool and filter the
extract
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Test Report Number: 140100488SHA-002 ����
Intertek Testing Services Ltd., Shanghai Page 5 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
��������� ���
������801 �������B ��200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
**************************************************************************************************************************************************** To be continued
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Test Report Number: 140100488SHA-002 ����
Intertek Testing Services Ltd., Shanghai Page 6 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
��������� ���
������801 �������B ��200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
****************************************************************************************************************************************************
End of report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
![Page 31: ICP Test Report Certification Packet2014/04/23 · Issue Date: April 23, 2014 It is hereby certified by Littelfuse, Inc. that there is neither (EU Directive RoHS 2002/95/EC, 2011/65/EU)-restricted](https://reader030.vdocument.in/reader030/viewer/2022040920/5e9827ace62e730b6a7c89a4/html5/thumbnails/31.jpg)
TEST REPORT
NO.: A002R131010052-2R02 Date: Oct. 12, 2013 Page 1 of 4
Customer: Suzhou Fuhong Electronic Industrial Co., Ltd.
Address: NO.89 WEI DU ROAD. WANGTING TOWN XIANGCHENG DISTRICT SUZHOU. CHINA
Report on the submitted sample said to be
Sample name: Lead copper shell
Model: /
Item/Lot No.: /
Material: /
Buyer: /
Supplier: /
Manufacturer: /
Sample received date: Oct. 10, 2013
Testing period: From Oct. 10, 2013 to Oct. 12, 2013
Testing Requested
As specified by client, to determine the Lead, Cadmium, Mercury, Hexavalent Chromium content in the submitted sample in
accordance with Directive 2011/65/EU (RoHS).
Testing method:
Testing Item Pretreatment method Measuring instrument MQL
Lead (Pb) IEC 62321: 2008, section 9 ICP-OES 2mg/kg
Cadmium (Cd) IEC 62321: 2008, section 9 ICP-OES 2 mg/kg
Mercury (Hg) IEC 62321: 2008, section 7 ICP-OES 2 mg/kg
Chromium (Cr Ⅵ) IEC 62321: 2008, Annex B UV-VIS 0.02mg/kg*
Note: -* 0.02 mg/kg refers to the MQL of sample extraction liquid.
Conclusion: When tested as specified, the submitted sample complied with the requirements of Directive 2011/65/EU (RoHS).
******FOR FURTHER DETAILS, PLEASE REFER TO THE FOLLOWING PAGE(S)******
Signed for and on behalf of
Shenzhen AOV Testing Technology Co., Ltd, Kunshan Branch
Project Leader:
Reviewed by:
Approved by:
Li Tingting, Maggie Wang Wexin, Weikin Yuan Qi, Mickey
Chemical Test Director Technical Director Lab Manager
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TEST REPORT
NO.: A002R131010052-2R02 Date: Oct. 12, 2013 Page 2 of 4
Test Flow: 1. To Determine Lead, Cadmium Content: (Metal parent metal )
Tested by:
2. To Determine Mercury Content: (Metal parent metal )
Tested by:
3. To Determine Hexavalent Chromium Content (boiling- water- extraction): (Metal parent metal )
Tested by:
4. To Determine Lead, Cadmium and Mercury Content: (Plating)
Tested by:
Weigh the sample
into a vessel.
Add the digestion solution, close
the microwave vessel.
Cooling the vessel, filter; washed and
filled to the mark with distilled water. Report Tested by ICP-OES
The sample is digested in the
microwave oven following a specific
decomposition program.
Weigh the sample into
a vessel.
Add the digestion solution; the
vessel is heated until the sample
has been dissolved
Cooling the vessel, filter; washed and
filled to the mark with distilled water. Report Tested by ICP-OES
Add H2O2 until the sample is clear
Heat 50 mL of DI water in the
beaker to boiling for 10 min
Take the (50±5) cm2
sample in the beaker.
Test the sample solution and the 0.02
mg/kg standard solution by UV-VIS.
Remove the sample, and cool
the beaker to room temperature,
and do the color reaction
Report
Cooling, filter; washed and filled
to the mark with DI water. Report
Tested by
Instrument
Weigh the plating-out
sample
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TEST REPORT
NO.: A002R131010052-2R02 Date: Oct. 12, 2013 Page 3 of 4
5. To Determine Hexavalent Chromium Content in colorless and colored chromate coating on metals: (Plating)
Tested by:
5.1 Spot-test
5.2 Boiling- water- extraction
Test Results:
Item Unit RoHS
Limit
Results
Lead substrate Lead Plating**Copper shell
substrate
Copper shell
Plating**
Lead (Pb) mg/kg 1000 N.D. 3 N.D. N.D.
Cadmium (Cd) mg/kg 100 N.D. N.D. N.D. N.D.
Mercury (Hg) mg/kg 1000 N.D. N.D. N.D. N.D.
Chromium (CrⅥ) mg/kg 1000 Negative 阴性 阴性 阴性
If the test result is positive,
the sample is considered to
have hexavalent chromium
If there is interference or it is hard to decide whether
the sample have the hexavalent chromium
If the test result
is negative
Place 1-5
drops of test
solution on
the sample
Report
Boiling- water- extraction
procedure shall be used to
verify the result
Compare the
sample solution
and the 0.02 mg/kg
standard solution
Heat 50 ml of DI water in the
beaker to boiling for 10 min
Take the (50±5) cm2
sample in the beaker.
Test the sample solution and the 0.02
mg/kg standard solution by UV-VIS.
Remove the sample, and cool
the beaker to room temperature,
and do the color reaction
Report
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TEST REPORT
NO.: A002R131010052-2R02 Date: Oct. 12, 2013 Page 4 of 4
Note: -N.D.=not detected(<MQL)
-MQL=Method Quantitation Limit
-Negative=Absence of Cr (Ⅵ) coating;
Positive=Presence of Cr (Ⅵ) coating;
Uncertain= can not verify whether the sample have Hexavalent Chromium by spot-test.
(The tested sample should be further verified by boiling-water-extraction method if the spot test result is uncertain or
negative.)
-**Testing part-- Plating
The test is based on the following assumption: The sample plating is a single layer and each part is uniform. The test result
maybe cannot stand for the physical truth of sample plating.
-Photo is included
Photograph of Sample
Lead copper shell
***End of Report***
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Test Report Number: 140100201SHA-004
Intertek Testing Services Ltd., Shanghai Page 1 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Applicant: LITTELFUSE, INC. Date: Jan. 15, 2014 800 E. NORTHWEST HWY
DES PLAINES, IL 60016 ATTN: J. CABILAN / A. CESISTA JR
Sample Description: One (1) submitted sample said to be: White yarn Part Description : YARN Part Number : 648115
***************************************************************************************************************************************************** Tests conducted:
As requested by the applicant, for details refer to attached page(s). ***************************************************************************************************************************************************** Conclusion:
Tested sample Standard Result Submitted sample Restriction of the use of certain hazardous substance in electrical
and electronic equipment (RoHS Directive 2011/65/EU) Pass
**************************************************************************************************************************************************** To be continued
Prepared and check by: For Intertek Testing Services Ltd., Shanghai
Authorized by: For Intertek testing services Ltd., Shanghai
Joy Zhou Jonny Jing Manager
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Test Report Number: 140100201SHA-004
Intertek Testing Services Ltd., Shanghai Page 2 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (I) Test Result Summary:
Testing Item Result (ppm) Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND
Remarks:ppm = parts per million = mg/kg
ND = not detected Responsibility of Chemist:John Zeng / Leaf Liu Date sample received: Jan. 07, 2014 Testing period: Jan. 07, 2014 To Jan. 09, 2014
***************************************************************************************************************************************************** To be continued
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Test Report Number: 140100201SHA-004
Intertek Testing Services Ltd., Shanghai Page 3 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (II) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(III) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content With reference to IEC 62321-5 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 ppm
Lead (Pb) content With reference to IEC 62321-5 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 ppm
Mercury (Hg) content With reference to IEC 62321-4 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-VIS Spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by Ion Chromatography
50 ppm
Remark:Reporting limit = Quantitation Limit of Analyze in Sample
***************************************************************************************************************************************************** To be continued
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Test Report Number: 140100201SHA-004
Intertek Testing Services Ltd., Shanghai Page 4 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (IV) Measurement Flowchart:
Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs Contents Reference Standard: IEC 62321 Edition 1.0:2008 & 2013
Remarks:
*1: List of appropriate acid:
MATERIAL ACID ADDED FOR DIGESTION Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4
*2: If the result of spot test is positive, Chromium (VI) would be determined as detected.
*****************************************************************************************************************************************************
To be continued
No
Yes
Sampling/grinding or cutting
Weigh sample and for different material, digest
the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add diphenyl-carbazide
solution
Cr6+
Weigh sample and add organic
solvent
Soxhlet extraction or
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved Cool and filter the extract
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Test Report Number: 140100201SHA-004
Intertek Testing Services Ltd., Shanghai Page 5 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (V) Measurement flowchart:
Test or Halogen content Reference standard: EN 14582
*****************************************************************************************************************************************************
To be continued
Add absorbent in a combustion
flask & place weighted sample
in equipment
Fill the combustion flask with Oxygen
Ignite then leave the flask at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by Ion Chromatography
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Test Report Number: 140100201SHA-004
Intertek Testing Services Ltd., Shanghai Page 6 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
****************************************************************************************************************************************************
End of report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to
the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of
our gross negligence or wilful misconduct.
![Page 41: ICP Test Report Certification Packet2014/04/23 · Issue Date: April 23, 2014 It is hereby certified by Littelfuse, Inc. that there is neither (EU Directive RoHS 2002/95/EC, 2011/65/EU)-restricted](https://reader030.vdocument.in/reader030/viewer/2022040920/5e9827ace62e730b6a7c89a4/html5/thumbnails/41.jpg)
Test Report Number: 140100201SHA-002
Intertek Testing Services Ltd., Shanghai Page 1 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Applicant: LITTELFUSE, INC. Date: Jan. 15, 2014 800 E. NORTHWEST HWY
DES PLAINES, IL 60016 ATTN: J. CABILAN / A. CESISTA JR
Sample Description: One (1) submitted sample said to be: White yarn Part Description : GLASS YARN Part Number : 648150
***************************************************************************************************************************************************** Tests conducted:
As requested by the applicant, for details refer to attached page(s). ***************************************************************************************************************************************************** Conclusion:
Tested sample Standard Result Submitted sample Restriction of the use of certain hazardous substance in electrical
and electronic equipment (RoHS Directive 2011/65/EU) Pass
**************************************************************************************************************************************************** To be continued
Prepared and check by: For Intertek Testing Services Ltd., Shanghai
Authorized by: For Intertek testing services Ltd., Shanghai
Joy Zhou Jonny Jing Manager
![Page 42: ICP Test Report Certification Packet2014/04/23 · Issue Date: April 23, 2014 It is hereby certified by Littelfuse, Inc. that there is neither (EU Directive RoHS 2002/95/EC, 2011/65/EU)-restricted](https://reader030.vdocument.in/reader030/viewer/2022040920/5e9827ace62e730b6a7c89a4/html5/thumbnails/42.jpg)
Test Report Number: 140100201SHA-002
Intertek Testing Services Ltd., Shanghai Page 2 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (I) Test Result Summary:
Testing Item Result (ppm) Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND Halogen Content Fluorine (F) 1100 Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND
Remarks:ppm = parts per million = mg/kg
ND = not detected Responsibility of Chemist:John Zeng / Leaf Liu Date sample received: Jan. 07, 2014 Testing period: Jan. 07, 2014 To Jan. 09, 2014
***************************************************************************************************************************************************** To be continued
![Page 43: ICP Test Report Certification Packet2014/04/23 · Issue Date: April 23, 2014 It is hereby certified by Littelfuse, Inc. that there is neither (EU Directive RoHS 2002/95/EC, 2011/65/EU)-restricted](https://reader030.vdocument.in/reader030/viewer/2022040920/5e9827ace62e730b6a7c89a4/html5/thumbnails/43.jpg)
Test Report Number: 140100201SHA-002
Intertek Testing Services Ltd., Shanghai Page 3 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (II) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(III) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content With reference to IEC 62321-5 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 ppm
Lead (Pb) content With reference to IEC 62321-5 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 ppm
Mercury (Hg) content With reference to IEC 62321-4 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-VIS Spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by Ion Chromatography
50 ppm
Remark:Reporting limit = Quantitation Limit of Analyze in Sample
***************************************************************************************************************************************************** To be continued
![Page 44: ICP Test Report Certification Packet2014/04/23 · Issue Date: April 23, 2014 It is hereby certified by Littelfuse, Inc. that there is neither (EU Directive RoHS 2002/95/EC, 2011/65/EU)-restricted](https://reader030.vdocument.in/reader030/viewer/2022040920/5e9827ace62e730b6a7c89a4/html5/thumbnails/44.jpg)
Test Report Number: 140100201SHA-002
Intertek Testing Services Ltd., Shanghai Page 4 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (IV) Measurement Flowchart:
Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs Contents Reference Standard: IEC 62321 Edition 1.0:2008 & 2013
Remarks:
*1: List of appropriate acid:
MATERIAL ACID ADDED FOR DIGESTION Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4
*2: If the result of spot test is positive, Chromium (VI) would be determined as detected.
*****************************************************************************************************************************************************
To be continued
No
Yes
Sampling/grinding or cutting
Weigh sample and for different material, digest
the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add diphenyl-carbazide
solution
Cr6+
Weigh sample and add organic
solvent
Soxhlet extraction or
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved Cool and filter the extract
![Page 45: ICP Test Report Certification Packet2014/04/23 · Issue Date: April 23, 2014 It is hereby certified by Littelfuse, Inc. that there is neither (EU Directive RoHS 2002/95/EC, 2011/65/EU)-restricted](https://reader030.vdocument.in/reader030/viewer/2022040920/5e9827ace62e730b6a7c89a4/html5/thumbnails/45.jpg)
Test Report Number: 140100201SHA-002
Intertek Testing Services Ltd., Shanghai Page 5 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted (V) Measurement flowchart:
Test or Halogen content Reference standard: EN 14582
*****************************************************************************************************************************************************
To be continued
Add absorbent in a combustion
flask & place weighted sample
in equipment
Fill the combustion flask with Oxygen
Ignite then leave the flask at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by Ion Chromatography
![Page 46: ICP Test Report Certification Packet2014/04/23 · Issue Date: April 23, 2014 It is hereby certified by Littelfuse, Inc. that there is neither (EU Directive RoHS 2002/95/EC, 2011/65/EU)-restricted](https://reader030.vdocument.in/reader030/viewer/2022040920/5e9827ace62e730b6a7c89a4/html5/thumbnails/46.jpg)
Test Report Number: 140100201SHA-002
Intertek Testing Services Ltd., Shanghai Page 6 of 6 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233
上海天祥質量技術服務有限公司
上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Tests Conducted
****************************************************************************************************************************************************
End of report
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to
the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of
our gross negligence or wilful misconduct.
![Page 47: ICP Test Report Certification Packet2014/04/23 · Issue Date: April 23, 2014 It is hereby certified by Littelfuse, Inc. that there is neither (EU Directive RoHS 2002/95/EC, 2011/65/EU)-restricted](https://reader030.vdocument.in/reader030/viewer/2022040920/5e9827ace62e730b6a7c89a4/html5/thumbnails/47.jpg)
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