icp test report certification packet/media/electronics... · 1/8/2013 · chemic€l test direcror...

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: 5x20 Cartridge Fuse Product #: 217P Series Issue Date: January 8, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the 5x20 Fuse Rohs-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 C910541 Cap 3-6 2 C910510 Cap 3-6 3 C909543 Body – Soda Lime Glass 7-11 4 082xxx Element - Ag Plated Wires 12-21 5 687xxx Element – Copper Cladded Wires 22-31 6 YTW206 (692529) Solder 32-36 7 YTW102 (692535-002) Solder 37-41

8 3M-3779-PG (087244) HMA (RoHS & Halogens) 42-48

9 EP608 (087335) Glue (RoHS & Halogens) 49-60

10 030204 Overcap (Cap base & plating)

Overcap (Cap wire base & plating) 61-64

11 934-077 (C030208) Overcap (Cap base & plating)

Overcap (Cap wire base & plating) 61-64

12 C030210 Overcap (Cap base & plating)

Overcap (Cap wire base & plating) 61-64 13 425901 Ink - Red 65-75 14 425902 Ink - Black 76-86 15 425903 Ink - Yellow 87-97 16 425904 Ink - Blue 98-108 17 425906 Ink - Brown 109-119 18 425907 Ink - Green 120-130 19 425909 Ink - Grey 131-141 20 425913 Ink - Pale Blue 142-152

Customer: Suzhou FuHong Electronjc InduslrialCo., Lld.

Addres!: NO.89 WEIDU ROAD, WANGTINGTOWN, XIANGCHENG DlsTRlCT, SUZHOU, CHINA

Report on ths submitred s.mplesald to be

S.mple name: CoppeJ,shell

Mod€h/

Item/LoiNo.:/

Metar lal : / ,

Buyer: / ,

Suppli€r: /

Samplo recaivsd d.te: Ocl. 08. 2012

Testins period: Ffom oct os, 20!€ 1o'O4r'10, 2012 . . ,,' \ l '

E9S!.s-Ecs!ed9!f

NO.: 4002R12100802+1 R02

As specified by dient, to determine ihe Lead, cadmlun,

accordance with Dircctive 2002/95/EC {RoHS).

AOV"BPFS,U

LiTingting, Maggie

Chemic€l Test Direcror

TEST REPORTDare: ocr.10, 2012

Mercury & Hexavalent Chrcmium content in the submitled sample in

Ylan Qi, lrickey

Ec!!!s-ee$9!.:Testing ltem Measunng instrumeni I\4QL

Lead (Pb) IEC 62321: 2008, s€ction 9 ICP€ES 2-'nglkg

Cadmium (cd) |EC62321: 2008, seclion I ICP-OES 2 mg/kg

[4ercury (Hg) lEc 62321 2008, seclron 7 tcP-oEs 2 mg/kg

Chromum (Cr\rl) IEC 62321 2008 Annex B 0.02m9/k9'

Ieqr 0.02 mg/kg reE|s to the MQL ofsample extfaction liquid

SsElcge!:-when tesled as speci{i€d the submitted sample complied with the requirements of commission Decision ol 18 Aug 2005

amending Directjve 2002/95/Ec noiilied under document 2005/618/Ec

ILS, PLEASE REFER TOTHE FOLLOWNG PAGE(S)***

signed lor and on behalfof

Shenzhen AOV Tesling Technology Co., Ltd, Kunshan Brcncn

caeateaaer: /blfil **n*"oor, We-r k] n ooo,',*or44.

SI tEN2HEN AOV Tf S I ING T€CHNOI ,O6Y CO. , I "TO.KUNSNAN BRANCTI /// \ Noll ne, J a,t 7tt) 9€'t'o

AOV'*F#S,[

NO.: 4002R121008024-1 R02

TEST REPORTOate :Od.10,2012

Content i|retb.r sulit€le). \ .

Cooling the vess€|, nlter;washed and

Rlled 10 the mark with distill€d wat€r.

The sample is digested in the

microwave oven following a specific

decomposrlon program

Test the sample solution and lhe 0.02

ng/kg standard solltion by uv-vls.F;;1.-

SH€NZH€N AOV TESTITIG lCCINOLOGY CO.,LTD.KUNSIIAN BSANCH( :

H o t l r n e'tL)0 700 8600

1. To Determiney'.ead, C€dmium Contenli (Metal subslrate)

I*redby (y'a04*

Add ihe digestion solulioni the

vessel is heated unlil the sampleWeigh ihe sample into

Add HrOruntilthe sample is clear

To Dete

Weigh ihe sample

Cooling the vessel, tiltei washed and

filled lothe maiK wilh dislilled water.Tested by lcP-oES

Chromium Contenl (boiling- wat€F €xtlaclion): ([4etal Eubstrate)

Remove lhe sample, and cool

the beak€r to room temperature,

and do the color reaction

Take the (50i5) cm,

sample in the beaker.Heat 50 mL of Olwater in

the be6ker to boiling for 1o

nov'Bpf,F,il

NO.: 4002R121008024-1R02

5. To oetemine Hexavalenl Chromium Contonl in_ .. -i\

: va'hu't'

TEST REPORTDaie: Ocl.10, 2012

colorless and colored chromate coating on metats: iPtating)

5.2 Boiling-wateF enradion

lfthe lest result is positive,

the sample is considered to

have hexavalent chmmium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extraotionprocedu€ shall be used to

lflhee is interference or it is hard to decide

whetherlhe sample have lhe hexavalent

Remove the sample, and coolthe beaker lo room temperalure,and do lhe color reaction

sample in the beaker.Heat 50 mlof Dlwaier in the

beaker to boiling for 10 min

Test tne sample solution and lhe 0.02mg/kg standad solulion by UV-VIS.

Sample Delcriptlon:

Code Sample Descndion

1-1 Substrate

Plating

Te3t R63ulb:

Unit RoHS Limit

Lead (Pb) msfts 1000 N.D. 1 0

Cadmium (Cd) mg/K9 100 N.D. N.O.Merorry (Hg) ms/Kg 1000 N.D, N.D.

Chromium {Crl,ll) m9/kg 1000 Negative Negative

s8€NZh€N AOV T€SrtNG TECHNOlOSY CO,,tTD,TUNSHAI!ARANCH H ot l in e.100 700 B6a0

,.r

nov'F"Ff"qn

No.: A002R1210o602:L1 R02

neoatve.,-"The te8t is bas€d on lhe followins d!!{mplifi:

maybe cannot stand lor the physical lrdh 6t s€r

TEST REPORT

Coppershell

-The new RoHS dircclive 2011/6tEU, on Jul. 21, 2011 come into forc€, on Jan. 03, 2013lhe formal implementation, Direclive

2002r'95/EC ahall be repealed simultaneously.

Sp€cimens, which r€Slested lo detemine Lead, Cadmium and Mercury Content, have been dissolved completely,-mg/kg=ppm ,-N.D.=not

i",, ,,,,( The iested sample result is uncertain or

SH€NZII AOVTIST|n|G TECHNOIOCV CO.,ITD.KUNSHAN AFANCH H ot l in e400 /00 8600

Test Report No. CANEC1207912201 Date: 26 Jun 2012 Page '1 of 5

XIAMEN LICHUN ELECTRONIC ELEIVENT CO''LTD

42_2XINGLIN WEST RD.,361O22,JIMEI DISTRICT,XIAI\,IEN''FUJIAN,P.R'C

The followjng sample(s) was/were submitted and identified on b€half of the ctiens as: SODA LIME GLASS

SGS Job No. :

Date of Sample Received :

Testing Peiod :

Test Requested :

Test Method :

Test Results :

C,onclusion :

xrvtl390111gEC - Xl\,1'18 Jun 2012

18 Jun 2012 - 26 Jun 2012

Selected test(s) as requested by client

Please refer to next Page(s).

Please refer to next Page(s)

Based on the performed tests on submitted samples, thg results of Lead'

I\rercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB)' -PolybrominateO diphenyl ethers (PBDE) comply with the limits as set by RoHS

Direc{ive 2011/65/EU Annex ll; rec€sting 200295/EC

Signed fof and on behalf ofscs-csrc Ltd.

Approved Signatory

:ffitili":;r,:1"'),i:;'"""ft1u1!'irlil"l'.:".-".:"^:;-:*;r::r"';',:""*i:::l;l,l:iiiiirii$ii:iii:l+*tij'"$:ff.+#.,;1]:ii::T;.^.Ji{,*isi"iilj:ilii:{fiIj,^,ti{+:i':'i!*it**

isGs96s9f 0a9o@ s t&rq L4'or!ixdatgro 510'63

4t.rii Ettt*eB*+tl&*C1e3! ml:\'0633i rs6-20ier56666 lls-20)@075r13 @'i sqeco6

| {6-201s?it55ss rie20ls2075rl3 ' lgsdm@t{sd

Mombo.olth€SGS Group (SGS SA)

Test Report No. oANEC1207912201 Date: 26 Jun 2012 Page 2 of 5

Test Results :

Test Part Descriotion :

Sp€dmon No. SGS Samplo lD D€sc.l$ion1 CAN12'079122.001 Transparentglasstube

Remarl..s :(1) 1 mg/kg= 1 PPm =00001%

(2) MDL = Method Detection Limat

(3) ND = Not Detected ( < MDL )(4) "-" = Po1 P"n''"t"d

RoHS Oit€dhe 201 1,/66/EU

Test lvethod: with reference to IEC 62321:2008(1) Determination ofCadmium bv ICP"OES(2) Determination of Lead by ICP-OES.(3) Determination of l\rercury by ICP'OES'(4) Determination of Hexavalent Chromium by Colorjmetric Method using IJV-Vis'

(5) Determination of PBBS / PBDES content by GC-I\'S

Test ltem(s)

Cadmium (Cd)

Lead (Pb)

Mercury (Hg)

Hexavalent Chromium (CrVl)

Sum of PBBSMonobrcmobiPhenylDibromobiPhenylTnbromobiphenylTetrabromobiPhenYlPentabromobiPhenYlHexabromobiphenylHeptabromobiPhenylOctabromobiPhenylNonabromobiphenyl

DecabromobiPhenYlSum of PBDESMonobromodiphenyl ether

;ili,ii' !n'i*-"i,i;r i*i.p. -t, -r, td rh. sncr'(3)r63Ed

001N D229N DNDNDN DNONONDNDNDNDNDNDN DNDND

1 6&m)SZ1555.€ 1 136-20)32075113 twcn'.qs@

l i36-e)s21s5566 iistr0)lco791s e l{schit@{3s

Memb€roilhe sGS GouP (s6SSA)

t!!i!100

1,0001,0001,0001,000

Unit MO!mg/kg 2mg/kg 2mg/kg 2mg/kg 2

mgKgmg/kg 5mg/kg 5mdkg 5mg/kg 5

mg/kg 5mS^(S 5mg/kg 5mg/kg 5mS-ftS 5

mgikg 5mg/KgmS/kg 5

1,000

ii":-iit#$:1ft +iifr fi.'q*rii';l*l'#ilriilrrryiili.iii',fi ,'i;lill"':i:istii;,,*$:,:l+3i+i*+ul+:l**-{+-;ft1fi::ilffi}ii.lq'f."'.",r'",:,l;!i"Trtritirtlm';i:i:trieifi"i#i:T#jih';#}##',*;b#;ii:ix""d..;";rl'Hri'::::r'r$";*r n1?:1:r'i''rr:irl

rs16!ltod,*tdrrllolrdutlmrTdridqt06!r{s'ro.n0tdooitr 510663

+8. , - f l € ' . t1 (+&Ef lS f lS4 t1$q '6 |6 :s10€63

Test Report

Test ltem(s)

Dibromodiphenyl etherTribromodiphenyl ethetTetrabromodiphenyl etherPentabromodiphenYl etherHexabromodiphenyl ether

HeptabromodiPhenyl elher

OctabromodiPhenyl ether

Nonabromodiphenyl ether

DecabromodiPhenyl ether

Notes :

No. CAN EC 120791220'l

titri!

Date: 26 Jun 2012

MDL 0915 N D5 N D

Page 3 of 5

5555555

'!rM ed,ed %c4g,tslEl kdEqt0'6d!ikdcqr9(Cx" 5 10663

+E.r f i .4#6n+Etsqe4i q* t$c an 51$Rj

NDN DNDN DNONDND

r r€6 2olers5ai5 I136+0J32!7t13I isHls2lSsss I €6-20)s20/5113 o tssdlBe3s'gM

MenbBf olthe sGs Group (sGs sA)

udtmg/Kg

ms,ksmg/Kg

mg/Kg

mg/Kg

mg/kg

mg/Kg

mgK9

mg/Kg

(1) The maximum permissible limit is quoted from the directive 2011/65/Eu' Annex ll

igi,i#*iffi*f:iffi iiilttll$jf*:nii.l,irJg'fr*fiiq*ts**efti#*fi*,}Iiifl,ii:le;i:,;liir,';i;i#li::li:"j#'i:rir:;*':11"""::;"'T;;;";;;:;';'::::"";:r111x11:::"r':;:'r:

Test Report

ATTACHMENTS

'1) Name of the person who madetesting: Bella Wang / Cutey Yu2t Name of the berson in charge of testing: Adams Yu / Ryan Yangii in."" Lroriti

"tt" dissolfu totally by pre-conditioning method according to below flow chaft

(cf' and PbBs/PBDEs test method excluded)

Pb/Cd/Hg PBBS/PBDE8

Positive

vrb,e,10,ico'd.uon'trNorsd!,:ilJlll"#rl:i1!':i[#.$.:.::;,,,-;!U,";q" i!il;iii:.il*.*df'#m:tilsrillil':l;:tHT:"1!}i6ii:;::i:",,xr.1"Hi:'Hl;ixlfi';i'"r:;::;*lui;1";iq;'i;,"."xii:dr;#i;lffi:1.ffi"c;i:;ifi"j|.r*;in-'i#:'-*il4!:1:i{:riii".liiliiji"i.#i::;:f.::i:r;iii;li*'*'.*:;*?:;;r::';r:r;*'

Page 4 of5

i ts6 rts21566i,5 I i36_20)3S75113 M43!5oh

' i*-mietlass r (!6eo420751'g d 4s'1i*€{3s

Momberor$e SGS GrcuP (SGS sA)

No. CANEC12O7S12201 Date:26 Jun 2012

RoHS T€sting Flow Chart

Sample PreParation

Sample Measurement

Acid digestion withrnicrowave/ hotplate

Conc€ntration/Dilution of extraction

solution

1) Alkali Fusion /Dry Ashing

2) Acid todissolve

Filtration andpH adjustment

Adding 1,5-diphenylcarbazidefor colordevelopment

Adding '1,$

diphenyloarbazidefor @lordevelopment

A red colorindicates thepresence of CF*I n€cessary,confirm with

'416rNdld$'|rotl@o tdurrbqroit{oltr0do'tgs rtu 51066J

cE.r 6 .*ts *rtEf+Eflel1e8t |!F: 110633

T€st Report

Sample photo:

No. CANEC1207912201 Datet 26 Jun 2012 Page 5 of 5

ses authenticate the photo on original report only

ri* End of Repod rd

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L(s-ers2155556 1 (s5 20)3205113 { 3$dmo3osm

Membeiollhe sGS G'ouP (SOs sA)

,fl.d,+E+Test Report f i , S ( N " . ) , c E / 2 0 1 2 / ] 0 8 3 5

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|l] t|| fl m

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(The fo l loe ins saDples ra . / rc re s rbe i t tcd and

SILIER PIATED & PURE SILVM $'IRES',tr+*sR (PLEASE REFER To PAGE s)

{EE (GERI4A\"Y)

2012/0t /04

2 0 1 2 / 0 t / 0 4 ' f o 2 a t 2 / a t / t l

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,fla,+E+Test Report

! t45(No. ) : cE/20I2 l lodJs

ELSCHUKOM ELU(TRqSCHUTZXOMPONENTENMU GVBHGENERBESTI{ASSE 87, D-98669'IIEIISDORF, CE!.T{Ar\Y

I t** (T.st Re6ul ts)

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]||lt[ttl||||fiml|!

ie;qma&ein& (6{t,r) (Jt6t ) (MTXED ALL mLoR tltErAr Nrm( INCLUDING TIiE PLATINC LA\'ER) (6 TYPES) )

pelsr reded rhE bd rcpod Enid bec o n o a . y t r r , : 1 r 1 , r ! _ i ' , r r l - J i j i r n : : l , ] . r : . a i i . ; ; r t i ] 1 , . r , r j r , ! * .

iy $qd ro b cene6 cdidroc d s

onlysndwibinlh.imlsoic€nls'ns

r|iiit E +lt( U r i t )

*ittri ttt.ttrlEtl{N(rDL)

s*(Resq l t )

N o , 1,fr / cadniun (cd) +arEc 623zLt 2oo8r; i , 4&,S*{

6€*.F+&4t*.*d,h;Fl. / q'i threfe.ence to IFC 62327t 2008 anlperforfted 6y ICP-AFS.

S / Lead (Pb) ++IEc 6232rt 2008ti1, rr t$A*t+t*fr+**i*,;*d&;il. / {i ih.e fe rence to IEC 62321: 2008 and

ter fo raed by ICP- , ES.

*- / vercury (Hs) ++ lEx. 62321 : 2008t&,'r€E*4+€ {/F + **t rt ;* d, *birl . / $i r1're fe rence to IEC 62321: ?008 andper fo rned by tCP- r {XS,

, i . f lJ ' / Heaav, lent chroni !n c . (v I ) ++ \F : 62321. 2OO8li*, t)a.,fr *+Rl iAt l l . / wi th fefe.€n€e ro IEc62321. 2 iAB and per formed byB o i I i n s s a t e r e x t . a c t i o n M € t h o d . #

} f r .+B** / Perrruo.oocranesu l fonates (PF!S-Ac id . Ueta l sa l t

nglka t+us EPA 3540C: 1996t i i , ' l i liE,9*f 1[-r*&}f,4 an+,t,4*69'/ t r i th reference to us EPA 3540c1996 n€thod for PFoS Co. le. l .Analys is was per lorned by tClMS.

I O

an+6.(J+) / PFoA (cAs No.: 335 6?r )

++US EPA 3540c: l996tt ! , ,Xt l&Eif 1{r*{,*fl an+d(n) }f/ wi th refetenc€ to US EPA 3540C1996 eethod for PFOA Content .Analys is was per fofned by rc /MS.

l 0

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lll l ]tl| ]t

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,{fi,t*( Ie thod)

,illt,rlEIE{I(IDL)

r**( R e s u 1 t )

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*trEc 623211 zoo$iiF, ,tfu|aE+8dl f : *d,&j r l . / $ i th rererencero IEC 62321: ?008 and per fornedby rc/MS.

:14#* / uonobronobiphenyt: i *#f ' / Dib.onobip l tenyl: ;Ad* / Tr ibronobi phenylqA#tr i / Tet rabr6nob L ohenvlI *#X i / Pentabronob r ohen! I

?!4$it / Hexabronobi phenyl 5+iASf / Heprab.onobi phe.y1 5^i t r f i A / o . rabronobipheDyl 54)qS* / Nonabromobipheryt 5+;ASf / Decabronobi phenyt 5t*AS.t&t" / suo of PBDES- ;ASf ! { / Monobronod i Dhehv l e ther 5=-r [#*e / Dibronodi phenyl ether 5: ; A # + a { / ' l r i b r o d o d i p } e n v l e r h e . 5B,*S iFa* / Te t ra6 .onod i phe.v l e rher 5i ;*Sxad / Pe.rabromodi Dh€"v l ether 5' r*S*a* / Heaabronodi phervt erher 5-k ;A#Xa{ / Heptabromodi Dh€nv l e ther 5, \ ; *SXa{ / ocrabronodi Dhe.v l e ther 5,L ; i#*e i Nonabromodi Dhenv l e t le r 5+&#i i4 / D€cabronodiDhenvl ether

a* / s"l.s."6* ( f r . ) / Halogen-Floo. ine (F) (c{sN o . : 1 4 ? 6 ? _ 9 4 - 8 )

ng/18

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6* (5. ) / Haloeen-chlo. ine (c l ) (cAs

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&* (* ) / Haloren-Bronine (Br) (cAS

l { o . : 1 0 0 9 7 - 3 2 - 2 )5 0

6fr (dU / Halocen-lodine (I) (cASN o . : 1 4 3 6 2 - 4 4 - 8 )

5 0

hrr.(s) rssbd rh s resr €pon ennd bc o n F i v ; " r 1 l l u . , [ r ' r , l : i / i r r . r I i . t l l t ! , l r ' i i q l L r L t [ ] ! .

o y g l b r e d b b 6 a i . ' a l c o n d l o i s d s

3 p d J b ' t } 6 l o b c € d a ^ d h s d o c u

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aBlJzr.) . 20L2/ot/71 Ftk(pare) : 1 of r0

[]tl||t][]tI| l

f i i i ( N . t . ) :

l . m g l k g : p p m ; 0 . | w t % = l o o o p p n2 _ n _ d . = N o r D e t e c t e d ( * . t A r r )

3- MDL : Met lod Detect ion L i r i i ( r l t lA; { ts1816)

4. ' - = Not R"sulated (Sl i ,+&.6)

5 . r ' = Q u a t i t a t i v e a n a L y s i s ( N o u n i t ) _ € , B r ) * f ( * + & )6 . # : a . P o s i t i v e b e a ! s t l e p . e s e n c e o f C r V t o n t h e r € s t e d a r e a s

(po s i t i ve *,F rq,l it E q.tF jq r{ ,r{l rS)b. Negat ive neans the absence of CiVI on rh€ rested a.eas

( Nesa t i ve i nr::tl *, E 4 t.tA ).14 'r1l1g )T h e d e t e c t e d c o h c e n r r a t i o n i n b o i l ] n a - e a r € r - e x r r a c t i o n s o l u t i o n i s50 cn: tested ar .a" . / l i6 ; i {XA>0.02 nslka * i ih 50 cm, ( tested

z. tte.i,tlS{r.'Af ;F./.**isArxl:{, , *E+ titi,sA,tt:ri}: +.Tftt 4 +1Erll+-ttlt aiAE.(The sanp les sas /were ana lyzed on beha l f o f the a t f r i can t as mix ing sanpre in one resr ine . The above! e s u l t s w a s / w e r e o n l y g i v e n a s r t e i n f o . n a t i t y v a l u e , )

PFos++*d,(R"f " ' .o"€

Inf or lat ion) ' !A+ 2oo6t rzztEa (Di rect iae 2006/t2ztw)(1 ) riitrrf rTfi.'|tsld.&n,r+r+4rrf, d.Ee,Ed,rlE*tla+,i6d.n,+0. 005%.

(May no t be p laced on the marke t o . used as a sDbstance o . consr i tuent o f p reparar rons€ q u a l i o o r n i g h € r t h a n 0 . 0 0 5 % b y n a s s . )

(2rtit{ttX4n&*fi&}.ei+d."%d.6s{.*{r1+;1!i*€1+}aX*Jt+ApFosi.4t?J*fi}.e.t&r€t6€};l4pFosEE,i.&+,i!d.i, i fo.r%,6*r&€d.4{tt i.4rf. {,RprrsaAt*f + 6E*;Ad.Ji;Aruc/.,.( M a y n o t b e p l a c e d o n i h e n a . k € t i n s e n i - l i n i s n e d p r o d o c t s o r a r t i c l e s , o r p a . t s r h e r e o f , i f u r ec o n c e n t . a t i o n o f P F O S i s e q u a t r o o r h i g h e . t h a n 0 . 1 % b y n a s s c a l c ! l a t e d s i t h r e f e r e n c e t o t l e n a s s o fs t . u c t u r a l i y o . f r i c . o s t r u c r u r a l l y d i s r i n . r p a r r s t ! a i c o n t a i n P F o . s o r , f o . r e x r i t e s o r o t h e . c o a r e dnater ia ls , i f thc anoun! o f PFOS is equa l to o . h iahcr than Ug/nr o f thc coated na ter ia t . )

c o m p a i y t r : ; r , r ; : i r l , , ; - f i t . r l J r . n i r r , . r , , t i i L t l t t r 1 i . , r " . l , r ! / , ) !

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f t ,q(No. ) : cE/20r2lr0835

EI-SCHIXOi,I ELEKTRO€CHUIZKNTPONENTENMU CVBHGEIIERBESTInSSE 87, D 98669 IEIT,SDORF. GERILUY

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p sG) rssr€d rh s€d Gpon€ind ecoDoanv t l r I t ! . , r - N ' | , r " l : l , i l l l i : . ! 1 1 : ; ! 1 , 1 \ ! r l l l r i l l r l .

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t ttt*/t rtt+4+f *,aE / PBB/PBDE anatyticat FLOW CHARTa }l{,/\l I a_i9*, / Name ofthe person who made measuremenl: Roman Wonqr,$Ji( fr t ^ : &+le / Nam€ of the person In charge of measurement Trcy Cha;gn^ ld,ElF / First lestry proce.s ------------f€*,E&*€F / OptionalscE€n prccess ....,---.*{.€,S / Confimation orccess -. -,t

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pslsl bdad h€rad cpod€nnorb3c o m D a n ! + " , I r i r r , , : i ; r . l J : ? . l r i a 1 . : - ! i - j ! , A l r I i . , . - l : r 3 1 1 . !

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rF{-d,+E+Test ReportEI.SCHUI(OM ELEI{TROSCHUTZ(OMA)NENTENB,{U GVBIiGE9ERBESTTASSE 87, D 98669 \,'EIT-SDoRF. GEf,Vl}IY

f t 1 4 ( N o . ) , C E / 2 0 r 2 l 1 0 8 3 5E S ( D a r . ) , 2 o l 2 l l ] t / t t F & { p r s e )

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it+&fiAn / Analyticalflow chart of halogen content

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*+E &t&.'sl' IAnalysis wE6 perfomed by lC

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i t4(No. ) : cE/2012l10835

E-SCHUKOM EI-E(TROSCHUTZKO]\IIONENTEN&{U GMBHGEFERBESTRASSE 87, D-98669 VEIISDORF, CERMA]\ry

AS(Dare) : 201210r/ tr F*.(pase) : 9 of lo

tI|fll|t][taf, l

*Ji+n+fin€n /Analytical flow chart ofSoxhtet extraction (LC/MS) procedure

r i A/-F : ij!9*y / Name ofthe person who made meesuement Rcman Wongr t4j :{, q i,\ : tF'.*4 / Name of the person in charge of measurement: Troy Chang

( rd8,{ a : Afi.+n*.n/Afi.+rt(*) , **.:4i{bA4, /Test ltems: PFOS/PFOA . Benzotriazole )

*{* / Datia

p 3G)r8sbd rh s rsd ,epon €inor ecmpany r:i r , tr 'ri_ ll i ,r'"'ll:l ill+ r. r i rtirril: . -. '.- it!,1 .

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f i6(N". ) , c-E/2072/10a35 Es(Date) : 2tr2/ar/r1 E*@aEe) : r0 of t0

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c d h p , i i n r . i ' , r , " r i l ' i , , i : . j : r . i | , . t l l i t t : I ' . . . ! , r : L ! .rhsdoarudE 3s!sdbyhe.omp,^yeqedb G6erydcodromor s

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t(Ttjd,&sfi &*r,t&, -eA fP +*trE*P **iTi d e ! t i f i e d b y / o ! b e h a l f o I t h e c l i e ! t a s ) :

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PrsG) bi€d rh s €d €Pod ennd ecomoanv + j l 1 / n r l , r r , f ' | ,1 , i :1 f i l r , r . I l t r i { : : - _ ' ,1 r ! t ! , . ! '

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2

,5 / Lead ( Pb) +*rDt 6232L' 2oo8ttA, ,r(&,6FA{*AA44I{*&A:.1. r

"i,nrefer€nc€ to IEC 6232r: 2008 andperforf,ed by ICP-nnS.

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2

7i ' l l r& / nexavalent chroniun cr(v I ) ++tgc 6232r. 2oo9fit, r/)k,Y"44. i * l t ;F l . / r i th ref€rence to IEc62321: ?008 and per for0€d byBoi I inE water ext ract ion Merhod,#

An+R&* / Perr luoroocta.esu l fonat€s (PFOS-Ac id , Mera l Sa l t

4+us EPA 35.10C, 1996ti4, 'Xr{h.t 44 f, ;*A,if :rl Afl.*R tt&+E./ I i l h re fe ren .e 16 us EPA 3540C:

1996 ne thod fo r PFoS Content .

Ana lys is sas per fo rned by LCINS,

i f t+d.(14) / PFoA (cAs No.: 33s-6?-1 )

4+US EPA 35a0c: l996tii, ,)(t{iEa fi J{:*.t*,tairl 4fr.+c( J*) n&/ s i th reference to US EPA 35.{0c1996 nethod for PFOA Content .Analys is vas per forned by tClMS.

l 0

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lE*r (No-) : CE/2012/108s6 E S ( D a r e ) : 2 0 1 2 1 0 1 / 1 1 F & ( p a s e )

I|lt|||||N ||[l tELSCHUKOI ELEKTROGCHUTZLOVPoNU,ITINtsAU G[tsHGEWERBESTMSSE 8?, D-98669 VEIISDoRF, CERMANry

jnd,{ E +'fs(Uni t )

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++r!x 6232t, zoo9tit, ,\^lBE*f&,/lf *A.Axl. / x,ith r€r€.€n€eto IEC 62321. 2008 a,d p€. lorhedby GC/MS.

- iAl f i ;F / Morobronobi phenyl 5: iA l f t * / Di bronobi rhenyr 5

: A S * / T r i b r o n o b r p h c n y l 5

€;ESX / Tetrabronobiphenyl 5

t ;9#E / P€ntab!omobi Dhenv I 5

' i ;A#*. / Hexab!omobipheny L 5-L i l l$ * / Heptabronob i pheny l 5^tA#f / octabromobi phenyl 5

, , ,LAS * ' / Nonabronob iphenyl 5

iA$t / Decabromobiphenyl 5

t ttfltlltrfr / suo of PBDES-_A#Xi4 / Monobronodi phenyl ether 5: A S 8 d / D i b r o m o d i p h e n y L € ( h € . 5

: i *d86d / T r ib ronod i ohenv I e rher 5q A d S E t / T e r r a b r o n o d , p h € n y l e t h € r 5A;&l$r i6{ / PentabronodiDnerv l € th€r^ ;& IS l iAC / Hexabronod i obenv l e ther 5t ,F l f i ; .a* / Heo lab .oood i lh€nv l e the . 5^*lSX.6t / octab.onod 5,L*SXAt / Nodabfonod 5**#XEn / o"catronoa 5air / Halo..n6* ( f l . ) / Ha lose !_F luor i .e (F) (cAs

N o . : 1 4 7 6 2 - 9 4 - 8 )

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5 0

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! o . : 2 2 5 3 7 - 1 5 - 1 )50

&l ( ; i ) / Halos€.-Bronine (Br) (cAs

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6* (4t ) / Halogen- lodin€ ( l ) (cAs

N o . : 1 4 3 6 2 - 4 4 - 8 )5 0

c o m D a n v ; " , r 1 r i | l , f _ a { l , r . r r , , J t n i j l r : r ] . 2 j i i i ! . f l i , r . 1 r r r r l J L l .

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,t. ' : Nor Resulated (**ei'.ii.)

5 . . .= Qual i ta i ive analys is (No u. i r ) € , I4r) t t ( *+dn)6 , # = a . P o s j l i v e E e a i s t h e F r e s e n c e o f C r V I o n r h e t e s t e d a r e a s

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50 cm, tes ted areas . / l i i ) * i { , i ,8=0.02 malks s i th 50 cm, ( tes ted areas)

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i n f o r n a l i l y v a l u € . )

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€ q u , l i o o r ! i g h e r l h a n 0 . 0 0 5 % b y n a s s . )

(2,t hY4q&*fr*rii+d.sd.fi"%4.*#r{+r 1kr5e+rExfirt 4ApFosltti€,*+6-La&.rElt€_LitSPFlsg&i.lA+,Ad.ri^0.1%, d,1 && A,t+!-&6,*,9, t'*Isos.arts't f + Al+Ad.d,Arus/".( M a y . o t b e p l a c e d o n t h € n a r k e ! i n s e n i f i n i s h e d p r o d u c t s o r a . t i c l e s , o r p a r i s r h € r e o f , i f t h e

c o n c e n t r a t i o n o f P I O S i s e q u a l t o o r h i a b € r t h a n 0 . 1 % b y n a s s c a l c u l a t e d * i t h r € f e r e n c e t o t h e n a s s o f

s t r u c t u . a l l y o . n i c r o s t r u c t u r a 1 L y d i s t i n c t p a r r s r h a t c o n t a i n P F 0 6 o r , f o ! t € x t i l e s o r o t h e . c o a t e d

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( c - 9 ) r 0 1 . 0 1 5 7 . 0 -

( c - 1 0 ) 1 0 1 . 0 1 3 6 . - -

( c - 1 1 ) 1 0 1 - - 0 6 4 . -( c - r 2 ) 1 0 1 . 0 1 6 6 . - -( c - 1 3 ) 1 0 1 . 0 1 s 8 . - -( c - 1 4 ) 1 0 1 . 0 1 6 1 . - -( c - 1 5 ) 1 0 1 . 0 1 5 5 . O( c - 1 6 ) 1 0 1 . 0 1 2 8 . 0 -

c o p p e r t i n a l l o y w i r e C u S n 6

c o p p e r c L a d { i r e - E l c o n 3 0

c o p p c r c L a d s t e e l w i r e - E l c o n F

c o p p e r c l a d i r o n - n i c k € l - a l l o y s i . e - E l c o n D

s i l v e . c o p p e r a l l o y w i r e - A g C ! 5 0s i l v e r c o p p e r a l L o y w i . e - A g c u g o

. o p p e r v i r e - C u 9 9 . 9 %

s i l v e r c o p p e r a l l o y w i r e - A g 7 2 C u 2 8

c o p p e r - z i n c - a l l o y w i r e - C u 8 0 Z n 2 0. i l ' e r c o p n e r a l l o / r i - F - A g 4 5 C L 5 5 ( A g a L 5 5 )

- c o p p e r p l a r e d , b r a s s p l a r e d s p . i n g - s t e e l w i r e - F S T , C u - %

s i l v e r c o p p e r a l l o y s i r e - A 8 c u 7 0 ( E l c u 7 0 )

s i l v € r c o p p e . a l l o y v i r e - A N u 8 0 ( E l c u 8 o )

oxyaenf r€€ copper v i re - OF Cu- c o p p e r - , i n . - a l l o y v i . e - C ! 7 0 Z n 3 0 ( V s 7 0 )- t u n g s t e n F u r i r y u i r e - l V

c d p a i y : 1 1 l t r - l l i , , r i ; . l l i l r ' i 1 ! . I 1 1 1 i r . . l : : r . , . , , r i f t , y .DyabPd lob6e la | co fu l d i 3b i s

i 4 r i i i ; , x {1 i . r ! , ) , r16 .^En - : , r r : r : * ! t . . : i1+s60, r , ,e r r t

scs,n{-d,*E+Test ReportDI-SCHLTI(OI\4 ELEKTRO6CHUTZI<OIIR}NENTEI{BAU OVBHGEWE&BESTRASSE 87. D 98669 VEII^SDoRF, CEL\IAI\ry

r)

! t r6(No.) : cE/2012l108s6 E S ( D a t e ) : 2 0 1 2 l 0 1 / 1 1 q r & . ( P a s e ) : 6 o f 1 0

||l| [ttn]t |l!r

2)3)

*{itrTil,i{!Ezi*?+ ' fsEe}:tsfl.( trliJ$)}lilttilArl. ) / TtEse samde reedissolv€d lotally by pE{onditioning melhod according !o below iow chan. ( cP bst method excluded )jd :l\',,.I : t} 4.L / N6me or the person who made measuremsntr Climbg€at Yang,Ilit I t ^ . t[4* / Nam€ of the person in chaqe of measuRent Trry Chans

a|!g+€d4+41#t*& / rcP-AES

p 6(s) resred rh s led epod eiid *comeany l i l , 1 / l l r i r ! - t i ' i , r r , . ' i , ! i ! . i i r r i i ) . ? r l ; r i n 4n L r i t l r l .

ont 3id w u'n rh6 h{s or c iads nshldLois iany rhaConFntssoe6s

tri{ ' {I*i*.s /Cutins. Pl€ aBlion

idnt*stl / Sample Measu€menl

f.f,1. Fl *e $tl f ,6,x,af 6l riG lifi lt (:{'T,i.ti) /Acid digstion by suilable acid depeded ondireren! ssmde maiedal (as below lable)

4i CJ{ Ct/l.f!&trr&,tfi rL /Micro'i/ave digeslion wilh HNOy'HCUHF

,!ll4,6f [A4tiifrit,+*. / Heal to apprcpdate

lftA|+ / HCl lo di$ol',€ filier digestate lhough liller

,"^*ailxa /add

'tX,l/.-q t +,k).ltr'tjrii{srg{a 540 nm 6t4

.b60rbance at :40 nm by

{,%+tJ / SamPle Material irlLAitllt / oiqeslion Acd

q€el. coo!€i. aluminun. soltler.t,t, diaa, taa, &,*.at, ,tl"t /&@ Esia. HNO3, HCl, Hl H,o,{ft,1Rli / HNOyI-IF

Gdld datirum Mlladium erami.

{.d, !ln+, 4&, Ec / H,so., Ho,, HNo! Hcl,! \1t1T.{4: ?,:|6tl / Any acrd to total dig€€tion

rfla#+f t t6(No. ) : cE/2012l10836

Test ReportET,SCIIUKOM ELEK'|RGSCHUTZKOMPONENTENMU GMBq

GEWERBESTTSSE 87. D-98669 \,'EII-SDOXF. GERV,q\Y

E S ( D u t " ) , 2 o l 2 l 0 1 / 1 1 F * . ( p a s e ) : z o r r 0

tl| tI || flttt]l

t*t*/ t i**tl,*+&fiaf / PBB/PBDE anaryticat FLOW CHART. ,|l:{,,i.F I 44ry / Name olthe person $ho made measurement Roman Wong. t'l*i F 1,,- : 'f,+q / Name of lhe p€rcon in cnaee of measufement T'oy Changt\,ilil{rr / FiFl tsiing prccess ----------.f*f.E&&44 / Oplionalscrcen prcc€ss ...----.4t{AF /Cmfimalion Dro.ess - . -.>

. r r r r r t r r r r r r r r r . . rScre€n analysis / tSriif

Filter / +S.i{€,8

Analysis by Gc/lvfs / RleE&f.'*&.+&

Sample exlraolion +l&+S.lSoxhlet merhod i *.+tdi*

Concentral€/Dalute Enracled solulion+Rn,ilB/ri#

*+r**

pe{3)€jed rh s r€d GFn €i.or becompany d r l i , l , l L i ' ! , . ' r . l : l i r i l i r : . r r r . . r l i t i . r r . r ! l ! ! ! .

,41'd,*E+Test ReportEISCIIUKOM ELEKTROGCHUTZI{OIIPONENTENB,{U GMBHGEtrERBESTRASSE 8?. D-98669 WII.SDORF. CXRMANry

f i ,6(r" .) , CE/2012/1aa36 E r q ( D a r e , : 2 0 1 2 / 0 r / r r F i H . t p a B e ) : 8 o r t 0

trffLntI| Ilrtfll

f f'+fit€f, / Analyticalflou, chart of halogen content

,!13t,\F : ttg* / Name ofthe person who made meesurement: Rita Chentr! 3t, € l,\ : 'Fr$4 / Name of the person in charge of measu€ment: Troy Chang

*a & frFr}+tr IAnalysis was performed by lC

prsG) rared rh s€dr4o^6.^d *c o m p a i r : i i r i t t ! j ! - l l ' i l r l i | i , i t r r . i . . l i i i l } ! . r i . i . r r . r . | r l l i -

spoisbtV €roGc Bdandh6 de!

l l + *6O" rex r r+$6o rn ,e r r Nws {oD

tI

rFl-d,+E+Test ReportET-SCHUI{OM ELEI{TROSCHUTZ(OMPONENTENMU GI!BIiGEWE&BESTMSSE 87. D 98669 VEILSDORF. GE&\!AIY

€i6(No. ) : CE/20t2 l r0836 A S ( D a t e ) : 2 0 1 2 l 0 1 / l l F l R ( P a s e ) i e o f t o

rtl |lll ![ltrt]t

*{+F}frfi4cf /Analytical flow chart of So)drlet extraction (LC/MS) procedure

r ic|l:{ -F: Ai4# / Name of the percon who made measurement Roman WongI tll*,Atl.: tiBF / Name of the person in charge of measurement:Trcy Chang

( ls'{ E: AE+H,*.t/An+*(s)' *it:4i{E6& /Te6t ltems: PFOS/PFOA ' Benzotriazolo )

Itfr i Data

prsG) rar6d rh s led @od 6ind *company. r . r1 , l1 l L r i : , r l ,11 : i | r r l . . t i l t { . r l ! t , . r . r r t r l .

sponsb q sbrsc 3d.ndh,sdru

,F{-d,*E+lEq(No.) : CE/2012l10836 E s ( D a t e ) , 2 0 1 2 l 0 1 / 1 1 F { ( p a g e ) : 1 o o f l o

l||tllttt][ |l t

Test ReportET-SCHUI<OI.T ELq(TRqSCHIIIZ(OMPONENTENMU GIIBHGEWERBESTMSSE 87, D-98669 VEIISDORF. GERVINY

t RH fst*fi*+ ' ,,1*.ft&t*i*x'ti-&.s/fiti. .(The tes t€d sa&p le / la r t i s na lLed by ao ar ro r i f i r , s shoen o ! th€ phoro . )

. . #** :E(E d of Report ) ++

pelst€dad ihs r€d Gpd €nior bec o m p a n y ; : r _ r r r : , 1 . r _ l r r r i : i : i l , : . r . : . r i i . l t l r 1 r . . , . : t 1 r \ a .

Lr i t : . 1 t i , i i r

r0836

10836

T€st Report No. SHAEC1216714738 Date: 25 Sep 201 2 Page 1 ol5

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTD

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CIry' ZHEJIANG, PROVINCE' CHINA

The following 6ample(s) was/were submitted and identified on behalf of the clients as : LEAD-FREE SoLDER

WIRE

SGS Job No. :

Part No. (PN) :

Compositlon :

Date of Sampl€ Received :

Testing Period :

Test R€quested :

Test Method :

T€st Resulb :

Condusion :

Signed for and on b€half ofscs-csTc Ltd.

sP12-028285 - SH

YTW2O6

sno.3Ag0.7ouce

21 Sep 2012

21 s,ep 2012 - 25 SeP 2012

Selected test(s) as requested by client

Please refer to next Page(s)

Please refer to next Page(s).Baa€d on the perfomed tests on submitted samples' the results of Lead'I\rercury, Cadmium, Hexavalent chomium, Polybrorninated biphenyls (PBB)'

Polybrominated diphenyl ethe6 (PBDE) comply with the limits as set by RoHS

Di.ective 201 1/65/EU Annex ll; recasting 200295/EC

/Qv''Fan Jingiie, JJApproved Signatory

.n#ffiffiirmr r* u-ra -td *vot rmrr.t.t t*

tirtDafi$EE|ihtltrorr zxtaoil.t.|.*f,Ertr€€.lt$l ll@3

tErEl@llitldt6!E{ti"clt06t'9 ffior*ofrxr.c+rti el Kr(,-tt)Eaffi 1j!ltor-

iLnlirotllt SOS Otbt4 (aGS 8A)

T€6t Report

Test Results :

Test Pert De€criotion ;

S@rn6n No, SGS Sampl€ lD D6ctiptioi1 SHA12-167147.035 Silvery wire

Rgmarks :(1) 1 mg/kg= I PPm=00001%(2) MDL = Method Deteclion Limit

(3) ND = Not D€teded ( < lrDL )(4) '-' = Not Regulated

RoHS DllBdivs 201 l/85/EU

Test Llethod

No. SHAEC1216714734 Date: 25 Sep 2012 Page 2 o15

with reference to lEc 6232 1 :2008(1) Determination of cadmium by ICP-oEs.(2) Dete.mination of Lead by ICP-oEs(3) Determination of Mercrlry by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colorimetric l\,ethod using UV-Vis(5) Detemination of PBBS i PBoES by GC-[IS.

Test ltem{s)

Cadmium (Cd)

Lead (Pb)

Mercury fig)Hexavalent Chromium (Ci(VD)

Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiph€nylTetrabrornobiphenylPentabromobiPhenYlHe/€bromobiphenylHeptabromobiPhenylOctabromobiphenylNonabromobiPhenylDecabromobiPhenYlSum oI PBDESMonobromodiphenyl ether

Limit UlE l\rDL

100 mdkg 2

1000 ms/kg 2

1000 ms/kS 2o

1000 mS.ftS- mS/kS 5- mdkg 5- mdkS s- mSikS 5- mdks 5- ms/kg 5- mg/kg 5- mdkS 5- msikg 5- mdks 5

1m0 mgftS- mg/KS 5

Ij*tffib D.r. na co{d6 *r I ffi*,Hffi !#,g;"EHT* ###f g"fff ffi Stift Ufiffiffi:ffi

Sffi *ff rffi #ffi*,rx*$'#'ffi *lvl*sm.1m*ts""nr*

ND50ND

N€gativeNDNDNDNDNDNDNDNDNDNDNDNDND

;;bii*hEni-.6fr d tbtk r6tr.{.)r-H

tt-ErrlFYasft.cxd|lt.9|dlcrn zfrlr3 rd€6+1)6r.@ tElEF{lF6tlHit!-2l164@raa it{&aFl@+l -l|.*tr[lt|fte||6+l lr:2@

lr.nD.t o1$.8Gg OrouP (8cgs )

Tes{ Report

Test ltem(s)Dibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl etherPentabromodiphenyl elherHexabromodiphenyl etherHeptabromodiphenyl etherOc-tabromodiphenyl etherNonabro.nodiphenyl etherD€cabromodiphenyl ether

thi!

t'ilt,b.aYrbto drchrbrd,Swaon !e3a+1

No. SHAEC1216714738 Date: 25 Sep 2012

UdT MDt @mdkS 5 NDmdkS 5 NDmdkS 5 NDmdkg 5 NOmS/kg 5 NDmSikS 5 NDmg/kg 5 NDmS/kS 5 NDmgkg 5 ND

I ErE {O-Zr)OtrOO*FA)ala@!.a

Page 3 of 5

raEFaFffiTl|{j{l.?J)6r@

Notes :(1) The maximum permissible limit is quoted from diredive 2011/65/EU, Annex ll(2) ospot{est:

Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;CIhe tested sample should be fudher verifed by boiling-waterextraction method if the spot test resultis Negative or cannot be confirmed.)oBoiling-wateFextraction:Negative = Ahsence of Cr(Vl) coatingPositive = Pesence of Cr(Vl) coating; the detected concentration in boiling-water-ext€ction solution isequal or greater than 0.02 mgl(q with 50 cm'z sample surtace area.For corrosion protection coatings on metals: Information on storage conditions and produclion date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status of lhe sample at the timeof testing.

M.m!.rorh.scsGtuc(acgs )

Test Report No. SHAEC1216714734 Date: 25 S€p 2012 Page 4 of 5

' l ' ;-;Ltidbd$rffi '-d6.h*lhE.,nrdri*6

ATTACHMENTS

RoHS Te€ting Flow Chart

1) Name of the person who madetesting: Jan Shi/Yoyo Wang/Allen Xiao/Gary xu2i Name of the berson in charge of testing: Jeff Zhang/George Xu/ Linda Liiiiii,"i !!rir!!,i. aissoried totarry 6'y pre-condit-roningherhod accorcting to berowflow chart. (Cf '

and PBBdPBDES test method excluded)

tr

Sample Prcparation

Sample Measurement

Acid digestion withmicrow€ve/ hotplate

Concentration/Dilution of extraclion

solution

'1) Alkali Fusion /DryAshing

2) Acid to dissolve

Adding 1,sdiphenylcarbazide

for colordevelopment

A red colorindicatesthe

presence of cP'.neceas€ry,confirm with

Pbrcd,Hg PB86fPBDE8

tilairl$gYb.rto dErloat4ltrtracnr 20(43fl..tjt.*Iqldl|6els+l a|lM

rEtE Fzr)0tac53l+{a-a)dlqaa

rE&&4lrsartjF.?1)6@

$6nb.fol th.ao6 GlDlD {8oas )

Test Report

Sample photo:

No. SHAECl2'16714738 Date: 25 Sep 201 2 Page 5 of 5

sHA12-167147.035

SGS authenticato the photo on original report only'* End of Report ""

(d-l!r. .Dor d6.ccil-iibhihr.ldcn.h,

' | l ! !a|i!!{ l |ddbd',td.lwb|||d4ded

tLlliDl! Bftfiufition 2dEs rElE[6-eDdag6l lElfF2l!ffia *6r*.&rr{&a1}ara@a ttF+lFN .,9d'rt.l.-tr.tl.*tr6l||,|rF|6r+l ll: @3

l|.fiDcrolm. SOS Gtu,D |SOSS ]

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING I.iIATERIAL CO., LTD

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE, CHINA

Test Report

SGS Job No. :

Part No. (P/N) :

Composition :

Date of Sample Received :

Testing Period I

Test Requested I

Test l\relhod :

T€st Results :

Condusion :

No. SHAEC1216714749 Date: 25 Sep 2012 Page 1of 5

sP12-028285 - SH

YTW'102 (692535-002)

Sn2.ocuRE21 Sep 2012

21 Sep 2012 - 25 Sep 2012

Selecled test(s) as requested by client.

Please refer to next page(s).

Pleas€ refer to next page(s).

Based on the performed tesb on submitted s€mples, th€ results of Lead,Meroiry, Cadmium, Hexavalent cfi romium, Polybrominated biphenyls (PBB),Polybrominated diphenylethers (PBDE) comply with the limits as set by RoHSDirective 2011/65/EtJ Annex ll; rec€sting 200295/EC.

The following sample(s) was/were submitted and identified on behalf of the clients as : LEAD-FREE SOLDERWIRE

Signed for and on bohalf ofSGgCSTC Ltd.

.,/1,-

,rt*{'""^Fan Jinqjie, JJApproved Signatory

t.Uiltrar|$&r,lrnllq,gldicti! @*l '.tf. *ir8l'lraast3rtll ar:M

tEl€(S{1)t1{q60 l6lE(E-llF{S't9 M6t{rmHljfi.2l)614&r04 rl!(s-n)$5d83''q9dmFdl

',E l.db&o-d cdd|{d. or swI6

H, frqiiffi*#r"r#H'ffil'ft1#l'l'Id*i,ffi

Momlarol th. SGsGloup (SGssA)

Tast Report No. SHAECl216714749 Date: 25 Sep 201 2 Page 2 of 5

Test Resulb :

Test Part Descriotion :

Sp6dr|on No. SGS Samplo lD Dgcriptio.l1 SHA12-167147.042 Silvery wire

Rema*s :(1) 1 mg/ks= 1 PPm=0.0001%(2) lrDL = Llethod Deteclion Limit(3) ND = Not Detected ( < IVDL )(4) '-" = 1o1 q*r,","d

RoHS DlrB.dv€ 201 1/55iEU

Test Method : With reference to IEC 62321:2008(1) Determination of Cadmium by ICP-OES.(2) Determination of Lead by ICP-OES.(3) Determin€tion of l\rercury by ICP-OES.(4) Detemination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis.(5) Detemination of PBBS / PBDES by GC-[IS.

Test ltem(s)Cadmium (Cd)

Lead (Pb)Merd.iry (Hg)Hexavalent Chromium (C(Vl))

Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPenlabromobiphenylHexabmmobiphenylHeptabromobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl ether

Limit unit100 msfts1000 mdkg,o:o *1*1000 mdlQ

- ms,/KS_ mg/Kg- mg/Kg- mgxs- mg/Kg- ms/Kg- msfts- mg/Kg- mgKg- mgKg

1000 mg/kgmg/Kg

MDt @22 N D2 1 n2 N Do Negative- N D

5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D- N D

5 N D

rh!dcll ld|rb.4.' lhirdd,''q1..!'*fut

-rd.dcr{rt h&!tu, riE.Ir.c@-tr rh dr$fitv t F ht c r.d ndtu @mr.6 i.r ffirna.!rdb. rd, firhr.drd [email protected] doffid sd b E Md d-tr h Mr'. md Fr {nl!...li;c-;ii;di;d; rr;'iirrd it(rn;i;. nia &diii, sd b E 6,tu0.. d-pt n Mr'. md Fd

blB thbrdrr.tth.4s' *.ry6brhrr.olr..bd

tr.ldnlBrrsto d&nrdri4srtrcrh [email protected]|.*f:At[lls8eB3et l* 2@3

lElEteeld.0e$! IElE&al6OSt9 *.i..4..06ru{s-2r)61r&9r rLo-aFas! ..$drro.}6

lilrmDor or th€ SOS Glou! (scs s )

Test ReportT6st ltem(s)

Dibromodiphenyl etherTribrcmodiphenyl elherTetrabromodiphenyl etherPentabohodiphenyl etherHexabrcmodiphenyl etherHeptabromodiphenyl etherOclabromodiphenyl etherNonabromodiphenyl etherDecabromodiphenyl ether

No. SHAECl2'16714749 Date: 25 Sep 201 2

thi! g2NDNDNDNDNDNDNDNDND

Page 3 of 5

llil MDtmg/kS 5mg/kg 5mSikS 5mg/kg 5mg/kg 5mg/kg 5mg/kg 5mg/kS 5mg/kg 5

Notes :(1) The maximum permissible limit is quoted from diroclive 2011/65/EU, Annex ll(2)

"spot-test:Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coatingi(The tested sample should be further verified by boiling-wateFextraction method if the spot test resultis Negative or cannot be confirmed.)oBoiling-wateFext€c{on:Negative = Abs€nc€ of Cr(Vl) coatingPositive = Presence of Cr(Vl) coalingt the detected concentration an boiling-water-extraction solution isequal or gre€ter than 0.02 mg/kg wilh 50 cm': sample surface area,For corosion protection coatings on melals: Information on storage conditions and production date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the timeof testing.

.Md b r&d br rh cmtsry !!Fr b r. o.€llc.ndr6o, !.n14 pid-.shd, Nr.Db d rqu.l e xdrd!|. d !!e44a, {r 6'!4qtil.dr6r&iid d.dniatL4n l.ft.na cor,|n6

l E!E$-A)6!1G53 lElEl{E AF6!r9 r*.64*MHr{an}6J4G04 fr(6-A)do63 .!d..dire.t-6

ri.t'rl.ddbrl h.t!dn, nri rh.C@!/. ro,.r-M.e$r hblt [email protected]'I|dhmcot&.rb.frrst rE.d'{t E4dd.rarr h tu[,*r6d rd'd

brstddoidoxbm'd.el4dbdold.lbofu|irrbih.rnD.(.)bbc

t: I I rtallt&lb.r'idErilb!{tllrlto.r 2!@

Mombd ol rh. sqs cloup (8qs sA)

+r.tl.*tr

T€€t Report No. SHAEC121671474S Date: 25 Sep 2012

rr b tu rhrr.(,) brh .

Page 4 of 5

ATTACHMENTS

RoHS Testing Flow Chart

1 ) Name of the person who made testing: Jan Shi/Yoyo Wangy'A en Xiaor'cary Xu2) Name of the person in charge of testing: Jeff ZhangJceorge Xd Linda Li3) These samples were da66olved totally by preconditioning method according to betow flow chad. (Cf'

and PBBS,/PBDES test method excluded)

Pb/CdrHg PBB8/PBDEs

Sample I\reasurement

Nonmetallicmateial

Concentration/Dilution of extraction

solution

1) Alkali Fusion /DryAshing

2) Acjd to dissolve Adding 1,5-diphenylcarbalde


Adding 1,5-diphenylcabazide


A red colorindicates the

presence of Cr6'.necessary,confirm with

htr @dd I sud br rh 6l!|q eq.d b L o,nrc.dd*..r 3.e tsdr os&t,.nbr. m q{, d |d'D. r! ib:lffi E.ffin !!m rlld .!!'!rc!rl

r-{!rtRt&. d lud'& h,.otod tulr ^ry Fr.r.,dr @id h dld hriiGd$-EAE ia6ffEft ccqdrr rEir .'hbdd tlslfii,-dlli!$in|ltr. hr d q$t| hd6noE. r mr n 6o.bvr ,r. i@dr'ny i b rn crr.d $itFltc*larrfimhnrddl{.rrd.uic..UihB.dbdddnts.r rrh@ddflior!.|@d,{d.,F rInlull,rhtu4tsrdr!.t/d@o,Ed .,..fle.,6l!" d

s't-E't e Ylu tod&trl|tr.€E torr 2@Sl,I|.ftE8l'!ft3e+3*l ll:2@

rEEis-el)il{@! IEtEFA)64Agn *6Ia..mH!(6-41)61{@l fNrl*-a)Aaa63 ..g5d.qb.@

M6mbq ol the AGS Oroqp (SqS SA)

Test Repori

Sample photo:

No. SHAEC1216714749 Date: 25 Sep 20 1 2 Page 5 of 5

sHAl2-167147.042

SGS authenticate the photo on original repod only'"' End of Reporl "*

..no|x*rg&.lidp'hr'rg.4ldii'i i.;i'' r-m* r-io a"-;.N eq- b r.n. d (dh.n bi Eb.n'

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BEIJING HYSTIC NEW MATERIALS CO,, LTD.

5 SHUANGYUAN ROAD, BADACHU HIGH.TECH ZONE,BEIJING,100041, cHtNA

Test Report

l\rodel No. :

Date of Sample Received :Testing Period :Test Requested :

Test Method :

Test Results :

Conclusion i

O\ N6'(

The following sample(s) was^^/ere submitted and identified on behalf of the ctients as : EpOXy ADHESTVE

SGS Job No. : TP12-004950 - TJ

EP6O8

3l Mat 2012

31 Mat 2012 - 09 Apt 2012Selecled test(s) as requested by client.



Based on the perfomed tesb on submitted samples, the resutts of Lead,Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyts (PBB),Polybrominated diphenyl ethers (PBDE) comply with the limits as set by RoHSDirective 2011/65/EU Annex ll; recasting 2002/95/EC.

Signed for and on behalf ofscs-csTc Ltd.

No. TSNEC1200272601 Date: 09 Apr 2012 Page 1 of I

r 13t2?66233000 I l|t2ri5e95?52 {r*cr !$.ohr 136 266233000 r 136-?a2546?52 e s!.c\ia@6!3@

Aimy WangApproved Signatory

rh!do.!n'lt6!.d5ylh.con!.iy

' id ! ' .drdoi r. i,.; dsr..d 't.,.h r Nift_a'rni ;iir..d h!'F''fl *

I i is do.,m;iclnndis ro'odutad

scsMans'6i.N6.41Th. srf Avenue rloA,Ti.nj n china 3ol4s74 E .*tlisftfi{*€6tt*S4l es6s*l Srl 300457

Memberol rh. SGSGolp{SGS SAI

Te€t Report No. TSNEC1200272601 Date: 09 Apr 20 1 2 Page 2 ol8

Test Results :

Test Part Description :

Sp€d.n€n No. SGS Ssmple lD D€6criplion1 TSN12-002726.001 ivory-white paste

Remarks :(1) 1mg/kg= 1 ppm = 0.0001%(2) IIDL = Method Detection Limit(3) ND = Not Deteded ( < MDL )(4) "-' = 1o1 q"nu,","o

RoHS Dirodive 201 t/66/EU

Test Method : With reference to |EC62321:2008(1) Determination ofCadmium by tCP-OES.(2) Determination of Lead by ICP-OES.(3) Detemination of l,rercury by ICP-OES.(4) Determination of Hexavalent Chrcmium by Colo metric Method using UV-Vis(5) Detemination of PBBS / PBDES content by GC-MS.

Test ltem(s)Cadmium (Cd)Lead (Pb)lllercury (Hg)Hexavalent Chromium (Cr(Vl))Sum of PBBSIvlonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOclabromobiphenylNonabromobiphenyl

DecabromobiphenylSum of PBDESMonobromodiphenyl ether

tinit Ud!100 mg/kg1000 mS/kS1000 mS/KS1000 mS/kS1000 mdks

- mg/Kg- mg/Kg- mg/Kg- mg-fts' mgKg- mgKS- ms/Ks- mg/kg- mgKg- m9x9

1000 ms/ksmg/Kg

sG s Madsioi Nc.41 .Tho slh Avenue T EoA,llan in, chiM 1l}a57s F . *lriE*fitrtte8lit641Cscs*l ffll: 300457

MDt 0p12 N O2 N D2 N D2 N D- N D

5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D

ND5 N D

;trvdGhFo&de,sr,E^rh.;d.i@br.^ {1d".'db.tr' bt6$n;tonl!N{h'i rh rnir t r rd r . 6i1rir h 6 do.vnld d.di'ci't6rr.nE i DaDbh" -d d e

h,q!aoit" rc'rdn dr s.iod.d'

I 136 2aBA80CC | 0G42529s29 f,nqc'i!9s@rI {3f2r66?8806 l1e2?26&12 s sss.f'[email protected]

Membero, rbe SGS Group (SGS SA)

Test Report

Tost ltem(s)Dibromodiphenyl elherTdbromodiphenyl elherTelrab.omodiphenyl etherPentabromodiphenyl elh€rHexabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl etherDecabromodiphenyl elher

Notes :

No. TSNEC1200272601 Date: 09 Apr 2012 Page 3 of 8

trd!

(1) The maximum permissibte limit is quoted from directive 2011/65/EU. Annex lt.

Horebrpmocrrdododecane THBCDD)

Test lvlethod : With reference to IEC 62321:2008, anatysis was p€rfomed by GC-N4S.

udtms/Kgmg/KgmS/kSms/Ksmg/kgmg/Kgm9KSmgKsmgKs

UlitmgKg

MDt555555555

@1N DN DNDNDNDNDNDNDND

pp1N D

T€st ltem(s)Hexabromocyclododecane (HBCDD)

Notes :

Test ltem(s)Dibutyl Phthalate (DBP)B€nzylbutyl Phthalate (BBP)Bis (2-elhylhexyD Phthalale (DEHP)

Notes :

!d! MDt 0p1% (w4,,/) 0.003 ND% (ww) 0.003 ND% (Ww) 0.003 ND

MDI1 0

(1) Reference Information: Diredive 201 1/6S/EU recasting RoHS directive 200?J9S/EC:Hexabromocydododec€ne (HBCDD) is considered as a priority for riskevaluation and substancerestriclion.

Phthalatss

Test l\Iethod: With reference to EN14372:2004, anatysis was performed by co-tvts.

(1) Reference Infomation: Directive 2011/65/EU recasting RoHS directive 200295/EC:Bis (2-ethylhexyl) phthaiate (DEHP), Butyl benzyt phthatate (BBP) and oibutyt phthatate (DBp) areconsidered as a pdority for riskevaluation and subslance restiction.

l 6 y h . c o f r ' m ' s b ] k l ] o t 6 . n ' d

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M,mber o l rhe SGSG,orp tSGS SAI

Test ReportResult shown is

No. TSNEC1200272601

of the total weight of wet sample

Date: 09 Apr 201 2 Page 4 of I

r i . coh r . i y t ' oh , . . po iN rV r t

y rubt.cr 'o {. o.i.'.r coid [oi. or s.rdrtrr @Mr,idrJ.d 'o rdnt rd

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1 )

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Test ReDort No. TSNEC1200272601 Date: 09 Apr 2012 Page 5 of 8

ATTACHMENTS

cd/Pb/Hg/Cf'lPBB5&PBOES Flow Chart

Name of lhe person who made tesl ing: Aer0n Wang/Jason Li /Angel l Yao

Name ofthe percon in charge oftest ing: Cindy Yin/Rel ZhuThsse samples wsrs dissolved tolal ly by pre-condi l ioning melhod according to

below l low chari . (C16* and PBBS/PBDES test melhod excluded)

ill;l,ffi;i;lii'#:;' i;;;;i'-,iiiliir ii'iiii;'";l;;n *a ro 1t:.,.trere1"l:,11e191191':ll1"l:11*:::::L:11.,1:1:":i:YlTi."ii i i; ;ii; ;'. ti;;:'ii.c"npi'ivt or..p*rurv "tid."di^, ; rn! dod@dca'mri . '#li*lr,:*r";*iitikl.*ri:ni*l:"ll*t:iim::,ttiil:r:r.""i?i"::::'ii,llii:::lligiirliii:?';"'tiiii'i:il*"'

scsManeion.No 41,Ti6 5U Av€rueTEOA.Ianjri ChiM 3COa57

+F.*Ffislit$*x&8tEt! 1qscs*! itia:3m45rI waa'52tflt( I t*r425294244r lst-Pr65a&[0 I]36-24?52S52t e s{sch$@s!s'm

Sample Preparation

Sample lVeasuremenl

Acid digest ion wi lhmicrcwave/ holplale

Sample solvent Adding digest ion reagent

Heating io 9tF95'C forextractionConcentral ion/

Di lut ion ofextract ions0iuIt0n

ResiduBSolution Fi l t ral ion and pHadjustmenl

1) Akali Fusion IDry Ashin g2) Acid todissolve

Adding 1 ,5'diphenylcarbazide fo!

coloi development

Fb/Cd/Hg PEB'PEDE5

Membero , lne SCS Group (SGS SA)

Test Report

ATTACHMENTS

' l ) Name ofthe percon

2) Nams of lhe person

No. TSNEC1200272601 Date: 09 Apr 2012 Page 6 ofB

HECDD Tosting Flow Chaft

who made test ing: Marine Sunin charge oftest ingr Rex Zhu

h'iii d*,n'n.&ij'd b i.rrs

Liliiiiiidin'ii riirul6d t'.ry. tbi"6p.^,! -h..ts*,', t'uf,.dr rh* eon..r ei@' bo 'Jed

scs M.Giai.No 41 ft. &n A64rEDAri.nJh,chi.a 3&457+E *afiE lE*tla lritr! | i scs*l ilfl.3045,

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Mebberol rh6 scs Grouo (SGS SAI

Sample cutt ing/preparation

Sample measurement

Solvenl exhaction

ConcBntral iodDilut ion

Test Report

ATTACHMENTS

Phthalde Testng Floli, chaft

1) Nams of lhe pelson who made lest ingi Maina Sun

2) Name ofthe person in charge oftesl ing: Rsx Zhu

i,ffi{{ftf#,fii#jja!:i;'}'.f:rir"" lirid+s6s Ma nsion, No 41 ,Th. 5lh Av.n u. T EDA,llr.jl., ChlM 3Xr457 I l€6 2?)65:4q10 r 1!t2)25295252 slcir93@tr

+F.iitejtfr*teEfEt64lcscs^! tl:300457 lls6'4)652$ffi I [t42529525? t sqsd'ha@'ssom

Mbfrberoilh6 SGs 6roup {SGs 5A)

No. TSNEC1200272601 Date: 09 Apr 2012 Page 7 of I

Solvenl exhacl ion

Conc entralion/Dil ution

Fihralion

Test Report

Sample photo:

TSN12-002726.001

SGS authenticate the photo on original repoionly

'*. End of Report '-

$:l:S,e*',#l+-*I*fiini,iil'*t";l*l'";*i#;fi l#;tr$#,Ii.1i;;iffi ri[l,iL"r't*xf"i,f,itii5rffii:Iitrfl{'iflrif.t*n,lf*jli;i+Ui*l'11;':r"-ff:"{'iili"iir,:,,i1ifi;'ilt-:;;t;;iJ; -;;";,'.; - "- "op-:. 91,.":9:t!"^"

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Mehboror $€ scs GbuP (SGS SA)

No. TSNEC1200272601 Date: 09 Apr 20 1 2 Page 8 of 8

scs Malior.No 4l,rno 5h aleFJ. rEDA qan 'n chrB 3m'5'

+!.xt6e;r*iteEtt16llCscs*! {|:30q9l

Test Report

BEIJING HYSTIC NEW IVATERIALS CO,, LTD,

5 SHUANGYUAN ROAD, BADACHU HIGH.TECH ZONE,BEIJING.100041, cHtNA


The following sample(6) wasirere submitted and identified on behalfof the clients as : EPOXY ADHESIVE

SGS Job No. :

lvodel No. :

Date of Sample Received

Testing Pedod :

Test Requested :

Test lvlethod :

Test Results :

TP12-004950 - TJ

EP6O8

31 Mat 2012

31 Mat 2012 - 0g Apt 2012

Selecled test(s) as requested by client.



Signed for and on behalf ofscs-csTc Ltd.

o*) N-(Aimy WangApproved Signatory

fi:id;:ifillll'.i.i ;i;i;l 6iililiii'"iriiiriirn;o*i'-r.;:i ;;i;;:;;;;";;;;; i;rhdd-"nh.e-i."he'.ao'ti1Y"ll'a-:l:1*-*::::::|jl:11'"::::il*lilii:i"il;Ii:lii"";

- i i n . " " . s " knnF i . 6 . * y

Avonu.TEDA,n.dh.Chl,E3OO{57 1 (3aJ?r65233CrI I l&_21252!529

+8.*t6*tt6i*tattt64rqscs^! oi:300457 r(86 2 i,528e0J I i6 el?5?e5252 | srsdit@sssM

M€mb€rol ths sGS G.ooP (scs sA)

Test RemrtTest Results :

Test Part Descdption :

Spodm€i No.1

Remarks :

No. TSNEC1200272602 Date: 09 Apr 20'l 2 Page 2 of 4

SGS Sample lD D€6criptionTSN12-002726.002 ivorv-whiteDaste

0 )(2)(3)(4)

1 m g / k g = 1 p p m = 0 . 0 0 0 1 %

[,lDL = lllethod Detection Limit

ND = Not Detected ( < IVIDL )'!" = Not Regulated

Halogen

Test Method : With reference to EN 14582:

Test ltem(s)Fluorine (F)Chlorine (Cl)Bromine (Br)lodine (l)

2007, analysiswas performed by lon Chromatograph (lC).

u!j!mg/(9mgKsmg/Kgmg/kg

MDt O@50 5750 755750 ND50 NO

Result shown is of the total weight of wet sample

i#Hi i ; ; ] t i : ; - ; , ; ; ; ; ; l i , . ; ; ' i ; ; . ; ;D; ' ' " ; ;+- 'dt ,"

h.5ampr.L6)i.( 'd

scs Ma nsioi. No 4 1 ,Th€ An Av.nu. TEDA11lniin, ChiM 3C0457 l ls 2)6?M10 i i8cgll252$252 srcisgsotr

. +!,^tiistf&*ft6lii${lgs6s*! 6ili 3aor57 l16a)65?880r)c i 1FzJ52$?52 4 eotd'ft@3$@

Metob6ro| lhe sGs Gro!D (sGs sA)

Test Report

ATTACHMENTS

1) Name ofthe percon2) Name ofthe psrson

No. TSNEC1200272602 Dater09Apr2012 Page 3 of 4

Halogen Testing Flow Chad

who made tesl ing: Angell Yaoin charge oflesl ing: Rsx Zhu

;L"iliiliiii'i]'i;;fi" ;;,;4";;i;-; d rbdio tuL'cB^^t'o'd.'d' roo. _'

" '_";d'ia ioniro1rc"! dha'o !k a

' I -" ,- -'ory ' -" -viii'u'!'v tb b cl sr sd s B do;'""d 6s Tl "f9"-"-'19qi:lll11"l;"::'::i"r'irni" iictn ' ..*.u-. no trc.n@ryr iqF rsd

A!on-. lo\Tirr.r Chrtu 10045/

4! . r !6*rd iFEat I*&4 i lscs* ! i !n :3e. ,r {!fn|65?33001 l1s-212i29529 *k di s96 @mr€6'2a66a!0of l1&22J5.'96?t e sss 'ntu€'q6 mn

Menberor lhe sGSOro!P lSGS sA)

Sample cutt ing/preparat ion

Sample measuremsnl

Combusl ion in oxygen bomb

Dissolv€d in an absorption

Analyzed by ionchromatography. Do!ble

conlim by other inslruments, ifnacessaty

Test Report

Sample photo:


TSN l2-002726.002

'";';;;; ;; ;.,'ai.;:';;i ;, ;ei5"t -:j-1.1 l?:.-:-.-9: ::li:l?::*"":

SGS authenticate the photo on odginal report only

'*" End of Report ""'

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" ' r " t " . 0 . , - t - ' . . , * " " q ,

" " a

scsManst$.No41,ri.5$ Av.nueTEOA riaiih chiM 3&457 | w22tt{wx/', t i*?a252*)e *wi^.'g! @m

cE.iiie;f^;&srta6r'c.".*! a!l:3m457 1(s6-2?6624s$ 11sr242s2e5!t e isrdiu6'$M

Momb€rot lho sGs Goup (sGS SAI

Cuslomer: Suzhou FuHong Electronic IndustriatCo., 16.

Addr6s: NO.89 \/ElDU ROAD, WANGTING TOVIN, XTANGCHENG DISTR|CI SUZHOU. CHINARepod on the submltted samrl€ said to be

sample name: Lead wife coppershell

Modol:/

Itefi/Lot Io.: /Matonal:/Buyen/ :S u p p l i e r : / ,

l i lanufacturE:/- . _ - i

- fSample recelved date: Gq _08, 2012 :t*,tn o"n.o, t.. o".;;,,013

"."r.-,.,,613, 1 ,]

&glirs-Bgsccsgq i

As specifed by dienl, to determine the L€ad, Cadrium, l,tercury & tiexayabntChrcmium conle in the 6ubmitted sampte inaccodance with Directive 2OO2I95/EC {RoHS). j

l\OV'BF.F.q,A

TEST REPORTNO.: 4002R121008024-2R02 Oate: Oct.1 0, 2012

Testing ltem Measufing instrument ,MQL

Lead (Pb) IEC 62321:2008. section I rcP-oEs a!gagcadmium (Cd) IEC 62321:2008, s€ction 9 tcP-oEs 2 mg/kg

[,lercury (Hg) IEC 62321r2008, s€ction 7 rcP-oEs 2 mg/kg

Chromium (CrM) IEC 62321: 2008, Annex B 0.02mg/kg*

Testino method:

lsqj 0.02 mg/tg rcturs to the MQL olsample exlraction liquid.

Conclu3ion:-\ryhen tested as specified lhe submilied sample compried with th€ requircments of commission D€cision of 18 Aug 2005

amending Dircctive 2002/95/EC notilied under docum€nt 2005/618/EC.

LiTingting, Maggie

Chemical Test Direclor

Yuan Qi, l,lickey

LabManager

Sign€d ior and on behallol

Shenzhen AOV Testing Technology Co., Ltd, Kunshan 8ran6h

ea"arc"a"r, A?1 W a l b n OrO."*0r44

."*FOR FURTHER DETAILS, PLEASE REFERTOT

Technical Di€clor

STIENZIIEN AOVTE$Tl'{G I€CHI!OLOGY CO,.I.TD,KUNSHAN BRANCI]

(,10",'ll,,u*

l\ov"BF,?sn

NO.: A0O2R12100802+2R02

T63l Flow:

Cooling the vessel, fiitei washed and

fllled lo the mafK with distilled waler.

Add the digestion solulionj thevess€l is heated until the sample

TEST REPORTDate Oci .10,2012

L To Detemine/lead, Cldmium Content (Metal substrale)lestedbY

L7.^otq,

-*".irl,"*J "r,to,"t|,

Add lhe digestion soluUon, closelhe microwave vessel.

f---- -].-

(Plating)

The sample is digested in the

micrcwave oven tollowing a specinc

deoomposilion progrcm.

Test the sample solulion and ihe 0.02

mg/kg slandard solution by uv-vls.

' H o t l r n e40a 700 8600

Cooling the vessel, frller;washed and

filled to the maft wilh dislilled waler.

Remove lhe sample, and cool

the beak€r lo room temperature,

and do the color reaclion

______-l "*rn nrte,.washedand l_____*p;-r, f;;-1

I rilled lo$e mark with Dlwaler I

ShENZH€N AOV I6STII {G T 'C NOIOGY CO.. ITD.XUNSHAN OEANCH

/\OV"BF#,HN

NO.i A002R121008024-2R02

Sample Doscripilon:

TEST REPORTOate :Oc l10 2012

5. To Deiermine Hexavalent Chromium Content in colorless and colorcd chromate coaling on metals: (Plating)

r e s t e d b v : l ) ^ ,' L/A^U,4.

5.1 Spotlesl (

f l;"')l;**SN€$ZHEN AOVI :STING T€C NOIOGY CO' ' ITD.XUNSI lAN BBANCI I

lf the lest result is posiiive,

ihe sample is considered lo

have hexavalenl chromium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extracton

procedurc shall be us€d tolf the test reslrlt

lltherc is intederence or it is had to decide

whetherlhe sample have the hexavalent

5.2 Boilin9- water- enractronRemove the sample, and cool

the beaker to rcom temperalu€,

and do the color rcaolion

Take the (50i5)cm2

sample in the beaker.Heat 50 ml ol Dl waler in the

beak€r to boiling lof 10 min

Code Sample Desc{iplion Code

copper shell subslfate

Lead wire Plating 24 Copper shell Platng

Unit RoHS Limit Result

2-3

Lead {Pb) mg/l(g 1000 N.D. N.D. N.D. N.O

Cadmium (Cd) mg/k9 100 N.D. N.D. N.D, N.D.

Meroury (Hg) mg/kg 1000 N.D. N.D. N.D, N D .

Chromum (Crl'I) mg/K9 1000 Negalive Negalrve Negaliv€ Negative

TEST REPORToare: oct.10,2012

-:fh€ new RoHS di€ctive 2011/65/EU, on Jul. 21,2011 come inlo force, on Jan. 03, 2013 ths formal implementation, Direcliv€

200295/EC ahall be repeal€d simultaneously-

Sp€cimens, which ggqeted to d€temine Lead, Cadmium and Mercury conient have been dissolved completelv.

NO.: A0O2R12100802+2R02

-mg/Kg=ppm

--The iest is bas€d on the following

ce of C_rl\,I)lif"veiry/y6hetp ttef.limere sr{.q!.be/rurTr v ii'iffyiT-''

*'q:*lhe spot test result is uncertain or

each pad is unifom. The tesl rcsult

maybe cannot stand for the physical truth-Photo is included

Lead wir€ copper shell

"'End of Repod""

sHEI\tZH:ir AOVrlsrr'tc IECNl'lO!OeY CO.,ITD KUNSHAN SRANCIi

r.r i35.1J:55i0eo0o Fd.3F1t?55roEr$ hrr ,w.d{.di' Fodrdo 1r.r00/ , Hot l rne

I , 400 700 8600

TEST REPORT NUMBER: SH AH00346635

AUTHORIZED BY： FOR INTERTEK TESTING SERVICES LTD., SHANGHAI

JACOB LIN GENERAL MANAGER

PAGE 1 OF 11 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

APPLICANT: LITTELFUSE,INC. DATE: OCT 29, 2012 800 E. NORTHWEST HWY ATT N: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE RED INK. PART DESCRIPTION : INK-RED. PART NUMBER : 425901. DATE SAMPLE RECEIVED : OCTOBER.19, 2012. DATE TEST STARTED : OCTOBER.19, 2012.

***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED





1 ( Ⅰ) Test Result Summary :

Testing Item Result (ppm) Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

(Ⅲ) Test Method:

Testing Item T esting Method R eporting Limit

Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





(Ⅳ) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO 3,HCl,HF Electronics H NO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

************************************************************************************************************************************************** TO BE CONTINUED

sampling/grinding or cutting

weigh sample and for different

material, digest the sample with

make up with deionized water

Cd/Pb/Hg

analyzed by ICP-OES

weigh sample and add alkaline solution

definite temp.

make up with deionized water and add diphenyl-

carbazide solution

Cr6+

weigh sample and add organic

soxhlet extraction or

solvent extraction

concentrate the extract and make up with organic

PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples

boiling water extraction

metalpolymers / electronics

negative*2

confirm the tested samples are totally

dissolved No

cool and filter the extract


TESTS CONDUCTED





2 ( ) Ⅰ Test Result Summary :

Testing Item Result (ppm) Halogen Content

Fluorine (F) ND Chlorine (Cl) 1000 Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million = mg/kg ND = Not detected

Responsibility Of Chemist : Leaf Liu

(Ⅲ) Test Method:


Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






Test For Halogen Content Reference Standard： EN 14582

**************************************************************************************************************************************************

TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask



analyzed by ion chromatography


TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY:

TESTING ITEM R ESULT(ppm) HBCD (HEXABROMOCYCLODODECANE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED (B) TEST METHOD :

TESTING ITEM TE STING METHOD REPORTING LIMIT

HBCD (HEXABROMOCYCLODODECANE) WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS

10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART:

TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT

************************************************************************************************************************************************** TO BE CONTINUED

WEIGH SAMPLE AND PLACE INTO A THIMBLE

SOXHLET EXTRACTION WITH ORGANIC SOLVENT

CONCENTRATE THE EXTRACT

ANALYZE BY GC-MSD

MAKE UP WITH ORGANIC SOLVENT

TRANSFER THE EXTRACT INTO A VOLUMETRIC FLASK


TESTS CONDUCTED





4 PHT HALATE CONTENT TEST

WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W) (MAX.)

DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND --- SUM OF THREE PHTHALATES ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH

REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.

DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED


WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W)

(MAX.) DI-BUTYL PHTHALATE (DBP) ND 0.1 DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND 0.1 BENZYL BUTYL PHTHALATE (BBP) ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY

IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.


DATE SAMPLE RECEIVED : OCT.19, 2012 TESTING PERIOD : OCT.19, 2012 TO OCT.23, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (EN14372)

************************************************************************************************************************************************** TO BE CONTINUED

WEIGH SAMPLE AND PLACE IN A THIMBLE

EXTRACTED BY SOXHLET EXTRACTION WITH ORGANIC SOLVENT


ANALYZE BY GC-MSD


Transfer the extract into a volumetric flask


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)

************************************************************************************************************************************************** TO BE CONTINUED


EXTRACTED WITH ORGANIC SOLVENT BY ULTRASONIC WATER BATH

ANALYZE BY GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************

END OF REPORT This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.









SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE BLACK INK. PART DESCRIPTION : INK-BLACK. PART NUMBER : 425902. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.

************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS:




************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED










(Ⅲ) Test Method:




************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED







REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED

(B) TEST METHOD :



10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED









REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.









DATE SAMPLE RECEIVED: OCT.15, 2012 TESTING PERIOD : OCT.15, 2012 TO OCT.18, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED

Weigh sample and place in a tube

Extracted with organic solvent by ultrasonic water bath

Analyze by GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************









APPLICANT: LITTELFUSE,INC. DATE: OCT 26, 2012 800 E. NORTHWEST HWY AT TN: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE YELLOW INK. PART DESCRIPTION : INK-YELLOW. PART NUMBER : 425903. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS:




************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED








Remarks: ppm = Parts per million = mg/kg N D = Not detected


(Ⅲ) Test Method:




************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED








(B) TEST METHOD :

TESTING ITEM T ESTING METHOD REPORTING LIMIT


10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED





4 PHTHALATE CONTENT TEST


LIMIT(%,W/W) TESTED COMPOUND RESULT (%,W/W) (MAX.)


REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.




LIMIT(%,W/W) TESTED COMPOUND RESULT (%,W/W)





DATE SAMPLE RECEIVED: OCT.15, 2012 TESTING PERIOD : OCT.15, 2012 TO OCT.19, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED


Extracted with bath organic solvent by w\trasonic water

Analyze by GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************










SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE BLUE INK. PART DESCRIPTION : INK-BLUE. PART NUMBER : 425904. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012. ******************************************************************************************************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

****************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample ******************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED







REMARKS:



*2: If the result of spot test is positive, Chromium VI would be determined as detected. ************************************************************************************************************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED










(Ⅲ) Test Method:




************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY: TESTING ITEM R ESULT(ppm)

HBCD (HEXABROMOCYCLODODECANE) ND


(B) TEST METHOD :


HBCD (HEXABROMOCYCLODODECANE) WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS 10 ppm

************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT ************************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED

















IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.


************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (EN14372) ************************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3) ************************************************************************************************************************************************************

TO BE CONTINUED

WEIGH SAMPLE AND PLACE IN A TUBE

EXTRACTED WITH ORGANIC SOLVENT BY ULTRASONIC WATER

BATH

ANALYZE BY GC-MSD


TESTS CONDUCTED





************************************************************************************************************************************************************

END OF REPORT

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.









SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE BROWN INK. PART DESCRIPTION : INK-BROWN. PART NUMBER : 425906. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.

***************************************************************************************************************************************************** TESTS CONDUCTED:

AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED





1 ( Ⅰ) Test Result Summary : Testing Item Result (ppm)

Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND



(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS: *1: List of appropriate acid：

Material Acid added for digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO 3,HCl,HF Electronics H NO3,HCl,H2O2,HBF4


***************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED






Result (ppm) Testing Item

Halogen Content




(Ⅲ) Test Method:




***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







*****************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED






TESTING ITEM R ESULT(ppm)



(B) TEST METHOD :



10 ppm

***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT *****************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED








DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND ---

SUM OF THREE PHTHALATES ND 0.1

REMARK： THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 (FORMERLY KNOWN AS DIRECTIVE 2005/84/EC) FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.






REMARK： THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY

IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES. DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED

DATE SAMPLE RECEIVED：OCT.15, 2012 TESTING PERIOD：OCT.15, 2012 TO OCT.23, 2012

***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






*****************************************************************************************************************************************************

TO BE CONTINUED

Weigh sample and place in a thimble

Extracted by Soxhlet extraction with organic solvent

Concentrate the extract

Analyze by GC-MSD

Make up with organic solvent



TESTS CONDUCTED






*****************************************************************************************************************************************************

TO BE CONTINUED



Analyze by GC-MSD


TESTS CONDUCTED





*****************************************************************************************************************************************************

END OF REPORT










SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE GREEN INK. PART DESCRIPTION : INK-GREEN. PART NUMBER : 425907. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS:




************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED





2 ( ) Test Result Summary :Ⅰ


Fluorine (F) 200 Chlorine (Cl) 650 Bromine (Br) ND Iodine (I) ND



(Ⅲ) Test Method:




************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED










10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED




















************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED


EXTRACTED BY SOXHLETEXTRACTION WITH ORGANIC SOLVENT


ANALYZE BY GC-MSD

MAKE UP WITH ORGANICSOLVENT



TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED



Analyze by GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************










SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE:GREY INK. PART DESCRIPTION : INK-GREY. PART NUMBER : 425909. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012. ******************************************************************************************************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

****************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample ******************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED







REMARKS:



*2: If the result of spot test is positive, Chromium VI would be determined as detected. ************************************************************************************************************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED







Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg N D = Not detected

Responsibility Of Chemist : Ken He

(Ⅲ) Test Method:




************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY: TESTING ITEM R ESULT(ppm)



(B) TEST METHOD :


HBCD (HEXABROMOCYCLODODECANE) WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS 10 ppm

************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT ************************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED

















IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.


************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (EN14372) ************************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3) ************************************************************************************************************************************************************

TO BE CONTINUED

WEIGH SAMPLE AND PLACE IN A TUBE

EXTRACTED WITH ORGANIC SOLVENT BY ULTRASONIC WATER

BATH

ANALYZE BY GC-MSD


TESTS CONDUCTED





************************************************************************************************************************************************************

END OF REPORT










SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE PALE BLUE INK. PART DESCRIPTION : INK-PALE BLUE. PART NUMBER : 425913. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS:




************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED







Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND



(Ⅲ) Test Method:




************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED










10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED




















************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED



Analyze by GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************


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