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ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000 <g/ml) ML Lab File ID: A89152JJ37.RES Level: (lou/med) LOW Date Received: 05/25/89 X Moisture: not dec dec. Date Extracted: 05/30/89 Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 06/01/89 GPC Cleanup: (Y/N) N pH: 6.6 Dilution Factor: 1.0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L CAS NO. COMPOUND ————— I 319-84-6—————alpha-BHC I 319-85-7—————beta-BHC_ 319-86-8—————delta-BHC 58-89-9—————gamma-BHC (Lindane). 76-44-8——————Heptachlor_______ 309-00-2—————Aldrin__________ 1024-57-3————Heptachlor epoxide_ 959-98-8—————Endosulfan I_____ 60-57-1—————Dieldrin________ 72-55-9—————4,4'-DDE________ 72-20-8—————Endrin__________ 33213-65-9———Endosulfan II____ 72-54-8——————4,4'-ODD________ 1031-07-8————Endosulfan sulfate. 50-29-3——————4,4'-DOT___________ 72-43-5—————Methoxychlor____ 53494-70-5———Endrin ketone____ 5103-71-9————alpha-Chlordane__ 5103-74-2————gamma-Chlordane___ 8001-35-2————Toxaphene__________ 12674-11-2———Aroclor-1016____ 11104-28-2———Aroclor-1221____ 11141-16-5———Aroclor-1232_____ 53469-21-9———Aroclor-1242_____ 12672-29-6———Aroclor-1248_____ 11097-69-1———Aroclor-1254_____ 11096-82-5———Aroclor-1260_____ 1. .05 ,05 .05 ,05 .05 ,05 .05 .05 .1 ,1 .1 .1 .1 .1 .1 .5 .1 ,5 .5 i .5 .5 .5 .5 .5 1. 1. U U U U U U U U U U U U U U U U U U U U U U U U U U U FORM I PEST 1/87 Rev. I I Lab Name: LANCASTER LABS Contract: I hTHBLK I ——————————————— ———————— I ________________ I ab Code: LANCAS Case No: SAS No: SDG No: Matrix (soil/water) UATER Lab Sample ID: 1393518 AR3G3675

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Page 1: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ID EPA SAMPLE NO.PESTICIDE ORGAN I CS ANALYSIS DATA SHEET

Sample wt/vol: 1000 <g/ml) ML Lab File ID: A89152JJ37.RES

Level: (lou/med) LOW Date Received: 05/25/89

X Moisture: not dec dec. Date Extracted: 05/30/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 06/01/89

GPC Cleanup: (Y/N) N pH: 6.6 Dilution Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NO. COMPOUND —————

I 319-84-6—————alpha-BHCI 319-85-7—————beta-BHC_319-86-8—————delta-BHC58-89-9—————gamma-BHC (Lindane).76-44-8——————Heptachlor_______309-00-2—————Aldrin__________1024-57-3————Heptachlor epoxide_959-98-8—————Endosulfan I_____60-57-1—————Dieldrin________72-55-9—————4,4'-DDE________72-20-8—————Endrin__________33213-65-9———Endosulfan II____72-54-8——————4,4'-ODD________1031-07-8————Endosulfan sulfate.50-29-3——————4,4'-DOT___________72-43-5—————Methoxychlor____53494-70-5———Endrin ketone____5103-71-9————alpha-Chlordane__5103-74-2————gamma-Chlordane___8001-35-2————Toxaphene__________12674-11-2———Aroclor-1016____11104-28-2———Aroclor-1221____11141-16-5———Aroclor-1232_____53469-21-9———Aroclor-1242_____12672-29-6———Aroclor-1248_____11097-69-1———Aroclor-1254_____11096-82-5———Aroclor-1260_____

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FORM I PEST 1/87 Rev.

I ILab Name: LANCASTER LABS Contract: I hTHBLK I

——————————————— ———————— I ________________ I

ab Code: LANCAS Case No: SAS No: SDG No:

Matrix (soil/water) UATER Lab Sample ID: 1393518

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Page 21: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

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HR303695

Page 22: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

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Page 23: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

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27AR303697

Page 24: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

SDG-5

MAY 1989

Rl-BAN

SR303698

Page 25: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1ft EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET __________

! MW-9ALab Nam»: LANCASTER LABS__________ Contract: __________ !______

Lab Cod«: LANCQ5 Ca«« No.s 220970 SAS No.: ______ SDQ No.s

Matrix: (soil/wat.r) UATER Lab Samplt. ID: C1393590U

Sampl* wt/vol: 5.0 <g/mL) Ml,_ L*b Fil« ID> C1393590W

L«v»l: <low/rm-d> LOU Dat» R»c»iv»di 05/36/89

X Moiatur*: not d»e. ___ Data Analyzed: 06/01/89

Column: (pack/cap) PACK Dilution Factor: l.OO

CONCENTRATION UNITSICAS NO. COMPOUND (ug/L or ug/Kg> UB/L Q

! IJ 74-87-3———————Chlorom«than«______________S 1O !U! 74-83-9———————Bromom»than«______________S 1O iU\ 75-O1-4———————Vinyl Chloridw____________» 10 !U! 75-OO-3———————Chloro«than«_.______________ \ 10 IU! 75-O9-2———————M»thyl«n« Chlorid*_________! 5 !U

10 !U5 !U45 !4 !J28 !5 !Us :u10 !U97 !15 !U10 !U5 !U5 !U5 !U

! 67-S4-1 ————————Ac»t on»_______! 75-15-0———————Carbon Di»ulfid«___________! 75-35-4————————1, 1 -D ich 1 oro«t h«n»_________! 75-34-3———————— 1. 1 -D i ch 1 or o«t h an*____;_____J 540-59-O———————1. 2-Dichloro«th«n« (total) __! 67-6S-3———————Chloroform___ __________107-OS-2—————— 1. 2-D i ch 1 or o»t han».

! 78-93-3———————2-Butanon«_! 71-55-6———————1, 1, 1-TrichloroBthan-.! 56-23-5———————Carbon T«trachlorid«_,! 108-05-4——————Vinyl Ac«tat»______! 75-27-4————————Bromod i ch 1 orom«t han«.i 78-87-5———————1. 2-D i ch 1 or opro pan*___! 1O061-01-5—————ci»-l, 3-Dichloroprop«n«..79-01 -6———-———Tr i ch 1 oro«t h»n«________124-48— 1 ——-—•—D i br omoeh 1 or om«t han« __..._.79-OO-5———————lf 1, 2-Trichloro«than»__.71-43-2———————•B*nz«n«.10061 -02-6—————Tr an»-1, 3-D i ch 1 oroprop«n»_,

j 75—25-2——————Bromoform—.,5 108-10-1 ———————4-M»t hy 1 -2-P«nt anon»_.! 591 -78-6———————2-H«x anon«__________J 127-18-4———————Tetrach loro«th«n«___.79-34-5————————1, 1, 2, 2-T«trachloro«than«___108-88—3——————To! u»n»________________,_

5 108-9O-7———————Chlorob«nz«n«

88 1s :us :u5 :u5 5U5 !U10 !U10 !U5 !U5 !U5 !Us :u

I 1OO-41-4———————Ethylb«nz»n»______________! 51 100-42-5———————Styr«n»___________________5 S! 1330-20-7——————Xyl»n» (total)_____________S S

6R303699

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J6Y1A ' EPA SAMPLE NO.

VOLATILE ORBANICS ANALYSIS DATA SHEET ______

! MW-9Bab Name: LANCASTER LABS - Contract: !___

Lab Code: LANCAS Case No. : 220970 SAS No. : SDG No. :

Matrix: (soi1/water) WATER Lab Sample ID: C1393591W

Sample wt/vol: 5.0 <g/mL) ML Lab Fila ID: C1393591W

Level: (low/med) LOW Date Received: 05/2S/89

% Moisture: not dec. Data Analyzed: 06/01/89

Column: (pack/cap) PACK Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3 ———————— Chloromethane _ ____74-83-9 ———————— Bromomethane _ _ ________ _75-O1-4 ———————— Vinyl Chloride ____________75— OO— 3 ———————— Chloroethane __, ^ _.-._TCT _*iQ •_& iu.__i.iWk-l •_.--•_• f i— . 1 A w» < »4 _•

67- 64-1 ———————— Acetone ' _ _ _75- 1S-O ———— ' ——— Carbon D i »ul f i da ___________75-35-4 ——————— 1, l-Dichloro»th»ne ________75-34-3 ——————— 1, l-Diehloro«thane _540-59-0 ——————— 1 , 2-D i ch 1 oroet h one (total) __£7-66-3 ——————— Ch 1 oro form _____ \ _____1 07-06-2 —————— 1 , 2-D i ch 1 or o«t h ane _________

71-55-6 ———————— 1, 1, 1-Trichloroe thane _ ____56-23-5 ———————— Carbon Tetrachloride _1 08-05-4 ——————— V i ny 1 Acet at e ______________75-27-4 ——————— Sromod i ch 1 oromet hane _"78-87-5 ———— ; ——— 1, 2-Diehloropropane _

79-01-6 ——————— Trichloroethene ^124-48-1 —————— Dibromochloromethane ___ __79-00-5 ——————— 1, 1,2-Trichloroethane ... __71-43-2 ——————— Benzene ___ _______10061 -02-6 ———— --Tr an»- 1 , 3-D i ch 1 oropropene ___75-25-2 —————— v-Bromoform ____1 08- 10-1 —————— -4-Met hy 1 -2-Pent anone591-78-6 ——————— 2-<-Hex anone _ _ _____1 27- 1 8-4 —————— Tet r ach 1 oroet h ene __________79-34-5 ——————— 1, 1, 2, 2-T»trachloro»than»_ ...108-88-3 —————— Toluene _____1 08-90-7 —————— Ch 1 orob»n zene ______ . _100-41-4 —————— Ethyl benzene _ _________100-42-5 —————— Styrene _ _________1330-20-7 —————— Xylen-t (total) ____________

10101010710576555510600510555

16OO5555•510105515555

___

11

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8R3037QQ-OM T UHQ ^ « « w w v / f u u 1/87 Rev

Page 27: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

370

ift EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET (—————————————

i! MW-9BDL

Lab Name: LANCASTER LABS_________ Contract: __________ !—_——————————

Lab Code: LANCAS^ Case No. : £20970 SAS No. : ______ SDG No. s —————

Matrix: (soil/water) WATER Lab Sample ID: Cl393591WD

Sample wt/vol: 5.0 (g/mL) ML__ Lab Fil« ID» C1393591WD

Level: (low/med) LOW Date Received: 05/26/89

% Moisture: not dec. ___ Date Analyzed: O6/O1/S?

Column: (pack/cap) PACK Dilution Factor: 1O._0———

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

11

! 74-87-3 ——————— Ch 1 or omet h ane ______________\ 74-83—9 ——————— Bromomethane _ __._ __ m ______ „ __! 75-01-4 ———————— Vinyl Chloride ___________ __! 75-00-3 ——————— Ch 1 or oet hane ______________! 75-O9-2 ——————— Methylene Chloride _________8 67-64-1 ——————— Acetone_ _____ ________! 75-15-0 ——————— Carbon Dimulfide _____ . _____j 75-35-4 ——————— 1, 1-Dichloroethene _________! 75-34-3 ———————— 1 , 1 -D i ch 1 oroet h ane __! 54O-59-O —————— 1,2-Dichloroethene (total) __* 67-66-3 ——— • — — — Chloroform _ ,__._,,- ,_.-__ ___,.-„, -_-..—! 107-06-2 —————— 1,2-Dichloroethane _ ______! 7S-93-3 ———— - ——— 2-But anone _______ __ __ ^ .„! 71-55-6 ——————— 1, 1, 1-Trich lor oet hane _______5 Bfi-23-5 ———————— Carbon Tetraehloride _______ ,_,! 108-05-4 —————— Vinyl Acetate.. __! 75-27- 4 ——————— Bromod i ch 1 or omet h ane ________! 78-87-5 ———————— 1 . 2-Dichloroprop*ne _________S 1OO61-01-5 ————— ei»-l, 3-Dichloropropene _____! 79-0 1 -6 ——————— Tr i ch 1 oroet hene ____________5 1 24-48- 1 —————— D i bromoch 1 oromet h ane ________! 79-OO-5-: —————— 1,1, 2-Tr i ch 1 oroet h *ne _______i 71-43-2 ——————— Benzene ____________5 10061-02-6 ———— -Trar.»- 1, 3-Dichloropropene ___! 75-25-2 ————— • —— Bromofortn _ _ _______ _..__ _____! 108-10-1 —————— 4-Methyl-2-Pent anone _ _____', 591-78-6 ——————— 2-Hexanone _, ^ _ _ ra^! 127-18-4 —————— Tetrachl oroet hene ______ _! 79-34-5 ——————— 1,1,2, 2-Tet rach 1 oroet h ane ___1 ! oa-88-3 ——————— Tol uene ____________________S 108-90-7 ——— -- — Chlorobenzene __,„-., _'. 1 00-4 1 -4 —————— Et hy 1 benzene _____________i 100-42-5 ——————— Styrene _. __ ^ __ „„._5 1330-20-7 ————— Xylene (total) ____________

100100100100111005065505050501003705O1005050509305O50SO505010010050SO505050

S 50J 50! _ ___

1

!U1UID: u!DJ:u:u:D:u;u:u:u:u!D:uIU:u!UIUID:u:uIU1 UiU:u:u1 U!U:u!UiUiU:u!

AR30370It VOO M H O U O / U I 1/87 Re«_>e

Page 28: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

Ifl EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET i ~" ——

! EQB-lLab Name: LANCASTER LABS__________ Contract: __________ !

Lab Code: LANCAS Case No. : 220970 SOS No. : ______ SDG No.:

Matrix: (soil/water) WATER Lab Sample ID: C1393S92W

Sample wt/vol: 5.0 (g/mL) Ml,__ Lab File IDi C1393S9gW

Level: (low/med) LOW Date Receivedi 05/26/89

% Moisture: not dec. ___ Date Analyzed: 06/01/89

Column: (pack/cap) PACK Dilution Factor: 1.00__________

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) U6/L Q

174-87-3 ———————— Ch loromet hane ______________ 8

75-O1 -4 ——————— Vinyl Chloride _ ____ _ 875-OO-3 ——————— Ch 1 oroet hane ______________ 875-09-2 ——————— Methylene Chloride _ _ _867-64-1 ——————— Acetone _. .. _____ _ 875-15-0 ———————— Carbon Disul fide ___________ 875-35-4 ——————— 1 , 1 -D i ch 1 oroet hene _ ... 875-34-3 ——————— 1, 1-Dich lor oet hane ^ _8540-59-O ———— - —— 1 , 2-D ichl oroet hene (total ) __ 867-66—3 ———————— Ch 1 or o form 8107-06-2 —————— 1 , 2-D ichl oroet hane _________ 878-93-3 ——— • ——— —2— But anone ________________ . 871-55-6 ——————— -1, 1, 1-Tr ichl oroet hane _._._.. ____ !

108-05-4 —————— Vinyl Acetate __ ____ ___ 8

78-67-5 ——— - ——— •!, 2— Dichloropropane _ _.____,__ _ .'1 006 1-01 -5 ————— c i s- 1 , 3-D i ch 1 or opropene _____ 879-O1-6 ———————— Trichloroethene _ ____ _81 24-48- 1 —— —— — D i bromoch 1 oromet h ane 879-OO-5 ——————— 1, 1, 2-Tr ichl or oet hane _______ 871-43-2 ——————— Benzene ___ 81 006 1 -02-6——— — -Trans— 1 , 3-D ichl or opropene_._..__._. 875-25-2 ——————— Bromoform _ _ __ ?1 08- 10-1 —————— 4-Met hy 1 -2-Pent anone _______ !Va 4 ^ . - J » *•% • I 1w_fi — /o— o—— — — —— s— nex anone _. •.••.•_•_•_-_•_»•127-18-4 ——————— Tetrach 1 oroet hene _ . _ . _ . __ , __ 8

108-68-3 ——————— Toluene ... _ _ _ __________ 8108—90-7 —— -— — —— Chlorobenzene I10O-41-4 —————— Ethy lbenzene_ ____________ 8100-42-5 ——————— Styrene _ ___________ 81330-2O-7 ————— Xylene (total) ... . . «__ ____ . ... _ 5 ___ .

101010105105555551O55105555555551010555555S

11

IU:u:u:u!U!U!UIU:u:u!U:u:u:u!U8U:u:u:u;u:u:u;u:u:u:u:u:u:u:u:u:u:u;ui

SR303702

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•1A • EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _____________

II

i TRIP_BLKLab Name: LANCASTER LASS_________ Contract: _________ '•_____________

Lab Code: LANCA5 Case No.: 220970 SAS No. : ______ SDG No. :

Matrix: (soil/water) WATER Lab Sample ID: C1395593W

Sample wt/vol: S. 0 (g/mL) Ml._ Lab File ID: C1393593W

Level: (low/med) LOW Date Received: 05/26/89

% Moisture: not dec. ___ Date Analyzed: 06/01/89

Column: (pack/cap) PACK Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

i i5 74-87-3————————Chloromethane______________8 10 5 U8 74-83-9————————Bromoraethane_______________8 10 5 U8 75-O1-4———————Vinyl Chloride____________! 10 !U8 75-OO-3———————Chloroethane______________8 1O !U8 75-09-2———————Methylene Chloride_________8 5 !U5 67-64-1————————Acetone___________________! -10 !U8 75-15-0———————Carbon Disulfide___________8 5 8U8 75-35-4———————1,1 -D i ch 1 oroet hene_________ 8 5 ! U8 75-34-3——————— 1, 1 -D i ch 1 oroet h ane_________ 8 5 ! U! 540-59-0———————1, 2-D ichl oroet hene (total)__8 5 !U8 67-66-3————————Chloroform_________________8 5 !U5 1O7-O6-2———————1,2-D ichl oroet hane_________8 5 !U8 78-93-3———————2-But anone________________! 1O "->8 71-55-6———————1,1,1-Tr ichl oroet hane______5 5 JU8 56-23-5———————Carbon Tetrachloride_______8 5 !U8 108-05-4——————Vinyl Acetate_____________8 10 !U8 75-27-4———————BrotnodiChloromethane_______8 5 !U8 78-87-5———————1,2-Dichloropropane________8 5 !U8 10061-O1-5—————cis-1, 3-Dichloropropene_____8 5 !U8 79-O1-6———————Tr ichl or oet hene____________8 3 !U8 124-48-1—————Dibromochloromethane_______8 5 5U8 79-OO-5———————1,1,2-Tr ichl oroet hane______8 5 !U8 71-43-2————'•———Benzene__________________8 5 iU8 10061-O2-6—————Trans-1, 3-D i ch 1 oropropene___ 8 S ! Uj 75-25-2———————Bromoform______________„__8 S !U8 108-10-1———————4-Methyl-i-Pentanone__I_____18 10 !U8 591-78-6———————2-Hexanone________________8 10 !U5 127-18-4——————Tetrachl oroet hene__________ 5 5 !U8 79-34-5——————— 1, 1, 2, 2-Tet rach 1 oroet hane___ 8 5 8 U8 108-88-3———————Toluene___________________.8 5 !UI 108-90-7——————Chlorobenzene_____________! 5 !U8 10O-41-4——————Ethylbenzene______________» S !U8 100-42-5——————Styrene_________________8 5 !UI 1330-2O-7——————Xylene (total)_____________8 5 SU

flR303703

Page 30: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPfl SAMPLE NO.SEfllUOLftTILE QRGflNICS ANALYSIS DATA SHEET _____________

I| MU-9A

ab Names LANCASTER LABS -Contract' RI2ZO ASSO |_____________

Lab Code' LflNCfiS Case No.: ____. SAS No.' ____. SDG No.:

Hatrix: (soil/water) WATER Lab Sample ID: 1393590

Sample ut/uol* iOOO (g/mL) ML Lab File IDs >D8351

Leuels (lou/med) LOU Date Received' 05/26/89

'/. Moistures not dec. ____. dec. ____. Date Extracted* 05/28/8?

Extractions (SepF/Cont/Sonc) SEPF Date Analyzed* 05/31/89

GPC Cleanups (Y/N) N pH« 6.8 . ... Dilution Factor* 1.000

CONCENTRATION UNITSs.CflS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

108-95-2- ————— Phenol______________111-44-4-—————bis(2-Chloroethyl)ether.95-57-8 ——————— 2-Chlorophenol_______541-73-1--------1,3-0ichlorobenzene.106-46-7--------1,4-Dichlorobenzene.100-51-6-—-----Benzyl alcohol_____95-50-1-—------i,2-Dichlorobenzene,95-48-7 ——— -- — -2-Methyl phenol.108-60-1---——--bi*(2-ChloroisopropylJether_106-44-5———--—4-Methylphenol621-64-7-----—-N-Nitroso-di-n-propylamine_67-72-l---------Hexach1 oroethane__________98-95-3———————Nitrobenzene_____________78-59-1 ——— - —— -Isophorone88-75-5 ——————— 2-Nitrophenol____105-67-9 —— - ——— 2,4-0 i methyl phenol.65-85-0---------Benzoic acid_____111-91-1——----bi«(2-Chloroethoxy)methane_120-83-2 ——————— 2,4-Dich lorophenol_________120-82-1 — —— ---1,2,4-Tr ich1orobenzene91-20-3———————Naphthalene.106-47-8----———4-Chloroani1ine___87-68-3 —— - ———— Hexachlorobutadiene.59-50-7--—————4-Ch 1 or o-3-methy 1 phenol.91-57-6-- — ——— 2-flethyl naphthalene.77-47-4---------Hexach1orocyc1 opentad iene.88-06-2 ——————— 2,4,6-Tr i chloropheno 1___95-95-4 —————— --2,4, 5-Trich lorophenol____91-58-7-—-—---2-Chloronaphthalene_____88-74-4————————2-Nitroani 1 ine__________131-11-3 —————— -D i met hylph thai ate_______208-96-8 ———— - — flcenaphthy lene.606-20-2 —————— 2,6-D initrotoluene.

101010101010101010101010101010105010101010101010101010501050101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

Page 31: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1C EPA SAMPLE NO.SEfllUOLATILE QRGANICS ANALYSIS DATA SHEET _____________

| MU-9ALab Names LANCASTER LABS Contract: RIZZO ASSO |________

Lab Code: LAISCAS Case No.: ____. SAS No.: ____. SDG No.:

Matrix: (soil/water) WATER Lab Sample IDs 1393590

Sample ut/uol» 1000 Cg/rnL) ML Lab File ID: >D8351

Levels (lou/med) LOW Date Received: 05/26/89

y. Moistures not dec. ____. dec. ____. Date Extracted: 05/28/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed* 05/31/89

GPC Cleanups (Y/N) N pH* 6.8 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND ('jg/L or ug/Kg) UG/L Q

99-09-2 —— ————— 3-Nitroani 1 i ne_83-32-9---------Acenaphthene__51-28-5- ————— -2,4-Dinitrophenol_100-02-7——————4-Nitrophenol____132-64- 9--—————Dibenzofuran121-14-2----———2,4-0initrotoluene.84-66-2 ——————— Diethy Iph thai ate,,7005-72-3-—-——4-Chloropheny1-phenylether_86-73-7----——--Fluorene__________________100-01-6--------4-Nitroani1ine____________534-52-1———————4,6-Dinitro-2-methylphenol__86-30-6-- — - — --N-Nitrosodiphenylamine (1)_101-55-3----- — -4-Bromopheny1-pheny1 ether__118-74-1-—-----Hexachlorobenzene_________87-86-5-————--Pentachlorophenol_________85-01-8---—-——Phenanthrene_____________120-12-7 —————— Anthracene________________84-74-2- — ------Di-n-butyIphthai ate.206-44-0——————Fluor an thene______129-00-0 —————— Pyrene.85-68-7————————Butyl benzy Iph thai ate.91-94-1———————3,3'Dichlorobenzidin<56-55-3--——--—Benzo.a.anthracene218-01-9 —————— Chrysene.117-81-7——————bis(2-Ethylhexyl)phthalate_117-84-0 — —— —— Di-n-octyIphthai ate_______205-99-2——————Benzo (b)fluo ran thene_______207-08-9 —————— Ben zo(k)f luo ran thene_______50-32-8———————Benzo(a)pyrene_193-39-5———-——Indeno(l,2,3-cd)pyrene.53-7"0-3 ——————— D ibenz( a, h) anthracene_191-24-2-—-----Benzo(g,h,i.perulene

5010505010101010105050101010501010101010102010107210101010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

(1) - Cannot be seperated from Diphenylamine

FORM i su-2 flR303705 1/87 Re'-I

Page 32: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB • EPA SAMPLE NOSEfllUOLATILE ORGANICS ANALYSIS DATA SHEET _______

I MU-9ARE iLab Names LANCASTER LABS Contract: RIZZO flSSOC.L_____________|

Lab Code* 'LANCAS Case No.' ____. SAS No.: ____. SDG No.: ____.

Matrix* (soil/water) UATER Lab Sample ID: 1393590RE

Sample ut/uol: 500 (g/mL) ML Lab File IDs >D8401

Level: (lou/med) LOW Date Received: 05/26/89

X Moistures not dec. ____. dec. ____. Date Extracted* 05/30/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed' 06/01/89

GPC Cleanups (Y/N) N pH* 6.8 D i l u t i o n Factor* 1.000

CONCENTRATION UNITSsCAS NO. COMPOUND ('jg/L or ug/Kg) UG/L Q

108-95-2 —————— Phenol_____________111-44-4 —————— bis(2-Chloroethyl )ether.95-57-8 ————— --2-Ch lorophenol_______541-73-1--------1.3-0 ichlorobenzene.106-46-7--------1,4-D ichlorobenzene.100-51-6--------Benzy1 alcohol_____95-50-1---------1,2-D ichlorobenzene.95-43-7- ——— ----2-Methyl phenol.108-60-l--------bis(2-Chloroisopropyl)ether_106-44-5 —— -----4-Methy1 phenol621-64-7--------N-Nitroso-di-n-propylarni ne_67-72-l---------Hexachloroethane__________98-95-3---------Ni trobenzene_____________78-59-l---------Isophorone.88-75-5-----—--2-Nitropheno?____105-67-9 —— --- — 2,4-Dimethy1 phenol.65-85-0---------Benzoic acid______lll-91-l--------bis(2-Chloroethoxy)methane_120-83-2 ———— —— 2,4-Dich lorophenol_________120-82-1 —— r----l,2,4-Trichlorobenzene.9 1-20-3-- —— —— -Naphthalene.106-47-8-—-----4-Chloroani1ine___87-68-3---------Hexach1 orobutadiene.59-50-7---------4-Ch1oro-3-methy1pheno1.91-57-6---——---2-Methylnaphthalene.77-47-4---------Hexachlorocyc1open tad iene.88-06-2- — —— — -2,4,6-Trichlorophenol____95-95-4- —— --- — 2,4,5-Tr ich1oropheno1____91-58-7- ——————— 2-Chloronaphthalene_____88-74-4 ——————— 2-Nitroani 1 ine__________131-11-3- ——— ---DimethyIphthai ate_______208-96-8 —— --- — Acenaphthylene.606-20-2—---——2.6-Oinitrotoluene

20202020202020202020202020202020

1002020202020202020202010020100202020

03706

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuU'u

- Jt *C\

Page 33: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

376 I1C EPA SAMPLE NO.

SEHIUOLATILE ORGANICS ANALYSIS DATA SHEET _______________

| MU-9ARELab Name: LANCASTER LABS Contract: RIZZO ASSOC.I__________

Lab Code: LANCAS Case No.:-____. SAS No.: ____. SDG No.:

natrixs (soil/water) UATER Lab Sample IDs 1393590RE

Sample ut/vol: 500 (g/mL) HL Lab File ID: >D8401

Levels (lou/med) LOU Date Received: 05/26/89

'/. Moistures not dec. ____. dec. ____. Date Extracted* 05/30/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 06/01/89

GPC Cleanups (Y/N) N pH* 6.8 D i l u t i o n Factor* 1.000

CONCENTRATION UNITS*CAS NO. COHPOUNO (ug/L or ug/Kg) UG/L Q

99-09-2- — - — — -3-Nitroani1 inc.83-32-9---------Acenaphthene__51-28-5-- —— — --2,4-Din itrophenol.100-02-7———————4-N itrophenol____132-64-9--------Dibenzofuran____121-14-2 ——— - —— 2,4-Oinitrotoluen«84-66-2 ——————— Diethy Iph thai ate.7005-72-3 — —— —4-Ch1 orophenyl-pheny1 ether_86-73-7-- ————— Fluorene_________________100-01-6———--—4-Nitroani1ine____________534-52-1- — ———— 4,6-Dinitro-2-methy1 phenol_86-30-6- — ------N-Ni trosod iphenylamine (1)_101-55~3--------4-Bromopheny1-pheny1 ether__118-74-1--------Hexach1orobenzene_________87-86-5----—---Pentachlorophenol_________85-01-8---———-Phenanthrene______________120-12-7-- — —"—Anthracene_______________84-74-2- ———— - — Oi-n-butyIphthai ate.206-44-0--——---Fluoranthene______129-00-0 ——— —— Pyrene.85-68-7 ——————— But ylbenzy Iph thai ate_________91-94-1 ———— ——— 3,3'Dichlorobenzidine_____56-55-3---------Benzo(a)anthracene________218-01-9 —— — —— Chrysene__________________117-81-7-- ————— bis(2-Ethylhexy1)phthai ate_117-84-0 —— - —— -Oi-n-octyIphthai ate________205-99-2 ——— - —— Benzo(b)f luo ran thene_______207-08-9——————Ben zo(k)f luo ran thene______50-32-8----—---Benzo(a)pyrene___________193-39-5 —————— Ine!eno(l,2 ,3-cd)pyrene_____53-70-3 ——————— D ibenz(a,h) anthracene_____191-24-2——————Benzo(g,h, i ) per y Iene_______

10020

10010020202020201001002020201002020202020204020202020202020202020

UUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

(1) - Cannot be aeperated from 0iphenylamine

FORM I SU-2 &R3037Q7 1/87

Page 34: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______

| MU-98Name* LANCASTER LABS Contract: RIZZO ASSOC.I

Lab Code' LANCAS Case No.: ____. . SAS No.: ____. SDG No.:

Matrix: (soil/water) UATER Lab Sample ID: 1393591

Sample wt/vol* 1000 (g/mL) ML Lab File ID: >D8352

Level: (lou/med) LOW Date Received: 05/26/89

'/. Moisture* not dec. ____. dec. ____. Date Extracted* 05/28/89

Extractions (SepF/Cont/Sonc) SEPF Date Analyzed* 05/31/89

GPC Cleanup* (Y/N) N - pH* 7.4 Dilution Factor* 1.000

CONCENTRATION UNITS*CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

108-95-2 ——————— Phenol______________111-44-4 — — ———bis(2-Chloroethyl Jet her.95-57-8 — ——— —— 2-Ch lorophenol_______541-73-1 ——————— I, 3-D ichl orobenzene.106-46-7----——-1,4-Dichlorobenzene.100-51-6 — — --—Benzyl alcohol______95-50-1---——---1,2-Dichlorobenzene95-48-7 ——————— 2-Methyl phenol.108-60-1-----—-bis(2-Chloroisopropyl)ether_106-44-5——--—-4-Methylphenol___________621-64-7-—-----N-Nitroso-di-n-propylamine.67-72-l---------Hexachloroethane_________98-95-3- —— -———Nitrobenzene____________78-59-1---------Isopho rone______,_________88-75-5 — - ————— 2-N itrophenol_____________105-67-9——————2,4-0 i methyl phenol_________65-85-0-- —— -- — Benzoic acid_______________111-9l-l--------bis(2-Chloroethoxy)methane_120-83-2 —————— 2,4-0 ich lorophenol________120-82-1 ——— - —— 1,2,4-Trich1orobenzene_____91-20-3———————Naphthalene______________106-47-8——————4-Chloroani 1 ine___________87-68-3 ——————— Hexachlorobutadiene________59-50-7--- — ----4-Chloro-3-methy1 phenol.91-57-6---------2-Methy1 naphthaIene_____77-47-4---------Hexachlorocyclopentad iene.88-06-2---------2,4,6-Tr ich1 oropheno1____95-95-4———————2,4, 5-Tr ich lorophenol____91-58-7-—--——2-Chloronaphthalene_____88-74-4———————2-Nitroani 1 ine_________131-11-3——————D i met hy Iph thai ate_______208-96-8 —— ———— Acenaphthy Iene__________606-20-2-——--—2,6-Din.trotoluene.

101010101010101010101010101010

101010501050101010

uuuuuuuuuuuuuuu

10 i U50 I U10 ! U10 I U10 I U10 I U10 ! U10 I U10 I U

uuuuuuuuu

FORM T SV..AR303708 1/37

Page 35: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1C EPA SAMPLE NO.SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET _______-._______

| MU-9BLab Names LANCASTER LABS Contract* RIZZO ASSOC.I________

Lab Code* LANCAS Case No.* ____• SAS No.* ____. SDG No.*

Matrix* (soil/water) WATER Lab Sample ID* 1393591

Sample ut/vol* 1000 (g/mL) ML Lab File IDs >D8352

Level* (lou/med) LOU Date Received* 05/26/89

'/. Moisture* not dec. ____. dec. ____. Date Extracted* 05/28/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed* 05/31/39

GPC Cleanups (Y/N) N pH* 7.4 Dilution Factor* 1.000

CONCENTRATION UNITS*CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

99-09-2 ——————— 3-Ni troani 1 inc.83-32-9--——-—Acenaphthene.51-28-5 ————— — -2,4-Dinitrophenol__100-02-7- — ————4-N itrophenol____132-64-9--——---Dibenzofuran_____121-14-2 —— ———— 2,4-Dinitrotoluene.84-66-2 ———————— D \ ethyl ph thai at.7005-72-3-------4-Chloropheny1-phenylether_86-73-7-- —— - — -Fluorene_____________;_______100-01-6 — -————4-N i troani 1 ine____________534-52-1--------4,6-Dinitro-2-methyIphenol_86-30-6---- — ---N-Nitro-sodi pheny lam ine (1)_101-55-3--------4-Bromophenyl-pheny1ether__118-74-1----——Hexachlorobenzene_________87-86-5--———--Pentachlorophenol_________85-01-8--———---Phenanthrene_____________120-12-7- — - ——— flnthracene_______________84-74-2 — —————— Di-n-buty Iph thai ate.206-44-0----- — -Fluoranthene_______129-00-0- —————— Pyrene____________85-68-7- — - — ---Buty1 benzylphthai ate_____91-94-1 ——————— 3,3'Dichlorobenzidine____56-55-3-—-———Benzo(a)anthracene_______218-01-9——————Chrysene_______________117-81-7 —————— bis(2-Ethylhexyl )phthalate.117-84-0 — — - —— Oi-n-octyIphthai ate______205-99-2---——--Benzo(b)fluoranthene_____207-08-9——---—BenzoCkJfluoranthene_____50-32-8----—-—Benzo(a)pyrene.193-39-5-——----Indeno(1,2,3-cd)pyrene.53-70-3---------0 ibenz(a,h)anthracene_191-24-2—————-Benzo(g,h,i.perulene

50105050101010101050501010105010102101010201010510101010101010

Uuuuuuuuuuuuuuuuuuuuuuuu

uuuuuuu

(1) - Cannot be seperated from 0ipheny1 amine

FORM i su-2 AR303709 1/87 Reu

Page 36: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

18 EPA SAMPLE NO.SEMIvOLATILE ORGANICS ANALYSIS DATA SHEET

I| EQB-1

rab Name-' LANCASTER LABS Contract* RIZZO ASSOC.I_____________

Lab Codes LANCAS Case No.* ____. SAS No.: ____. SDG No.:

Matrix: (-so i 1/water ) WATER Lab Sample ID* 1393592

Sample wt/vols 1000 (g/mL) ML Lab File ID* >D8353

Levels (low/med) LOU Date Received* 05/26/39

'/. Moisture* not. dec. ____. dec. ____. Date Extracted* 05/28/89

Extraction* (SepF/Cont/Sonc) SEPF Date Analyzed* 05/31/89

GPC Cleanup* (Y/N) N pH* 6.0 Dilution Factor* 1.000

CONCENTRATION UNITS*CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

108-95-2 ——————— Phenol______________111-44-4 —————— bis(2-Chloroethyl )ether.95-57-8 ——————— 2-Ch lorophenol_______541-73-1--- —— —1,3-0ichlorobenzene.106-46-7-—-----i,4-0ichlorobenzene.100-51-6-——---Benzyl alcohol95-50-1-—--——-1,2-Dichlorobenzene.95-48-7 ——————— 2-Methyl phenol.108-60-1-—-——-bis(2-Ch1oroisopropylJether.106-44-5 —— ---—4-Methy 1 phenol.621-64-7--------N-Nitroso-di-n-propylamine_67-72-i---------Hexach1 oroethane__________98-95-3----————Nitrobenzene______________78-59-1------—-Isophorone88-75-5--- ————— 2-N itrophenol____105-47-9 — - — —— 2,4-0 i methyl phenol.65-85-0--————-Benzoic acid_____111-91-1 ———— --bis(2-Chloroethoxy)methane_120-83-2 ——————— 2,4-D ich lorophenol_________120-82-1- ——— ---l,2,4-Tr ich1 orobenzene.91-20-3 ——————— Naphthalene.106-47-8--------4-Chloroani1ine____87-68-3---- — ---Hexachlorobutad iene.59-50-7-- —— --—4-Chl or o-3-methyl phenol.91-57-6—-———2-Methylnaphthalene.77-47-4---------Hexach1orocyc1 opentad iene.88-06-2 ——————— 2 ,4, 6-Tr ich lorophenol____95-95-4 ——————— 2,4, 5-Tr ich lorophenol___91-58-7- ———— —— 2-Chloronaphthalene_____88-74-4——— ———— 2-Nitroani 1 ine__________131-11-3 ————— — D i met hy Iph thai ate;_______208-96-8 ———— —— Acenaphthy Iene.606-20-2—*———— -2,6-Dinitrotoluene.

101010101010101010101010101010105010101010101010101010501050101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

flR3037IOcu-1 n i.wwv/ iv 1/87 Re-

Page 37: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1C EPA SAMPLE NO.SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET _____________

I| EUB-1

Lab Name: LANCASTER LABS Contract* RIZZO ASSOC.|_____________

Lab Code: LANCAS Case No.* ____• SAS No.* ____. SDG No.*

Matrix: (soil/uater) WATER Lab Sample ID: 1393592

Sample ut/vol* 1000 (g/rnL) ML Lab File ID* >D8353

Level* (lou/med) LOW Date Received* 05/26/89

7. Moisture* not dec. ____. dec. ____. Date Extracted* 05/28/89

Extraction* (SepF/Cont/Sonc) SEPF Date Analyzed* 05/31/39

GPC Cleanup* (Y/N) N pH* 6.0 . Dilution Factor* 1.000

CONCENTRATION UNITS*CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

99-09-2--————-3-Nitroani1in«83-32-9--—-----Acenaphthene.51-28-5-- — ———— 2,4-Dinitrophenol.100-02-7 ————— -4-N itrophenol___132-64-9—-———Dibenzofuran____121-14-2 ———— -—2,4-Dinitrotoluen«84-66r2-- ————— Diethy 1 phthalate.7005-72-3-------4-Ch1 orophenyl-pheny1 ether_86-73-7-----——-Fluorene________________100-01-6——————4-N i troani 1 ine____________534-52-1 —————— -4,6-Dinitro-2-methylphenol_86-30-6—————-—N-Nitroaodiphenylamine (1)_101-55-3--------4-Bromopheny1-phenylether__118-74-1-——----Hexachlorobenzene_________87-86-5---—----Pentachlorophenol_________85-01-8- — — — --Phenanthrene______;______120-12-7 ——— —— Anthracene_______________84-74-2-------—Oi-n-butyIphthai ate.206-44-0————-Fluoranthene ____129-00-0——————Pyrene___________85-68-7 —————— -Butyl benzyl phthalate_91-94-1 ———————— 3,3'Oichlorobenzidine.56-55-3---------Benzo(a)anthracene___218^01-9 —————— Chry-iene___________117-81-7 —————— bis(2-Ethylhexyl )phthalate_117-84-0——-———Oi-n-octy1phthalate__2Q5-99-2——————Benzo (b)fluoranthene.207-08-9——————Benzo(k)fluoranthene.50-32-8———————Benzo (a) pyrene.193-39-5——————Indeno (1,2,3-cd) pyrene.53-70-3 ——————— Dibenz(a,h)anthracene_191-24-2 —————— Benzo(g,h, i ) pery lene__

5010505010101010105050101010501010101010102010101010101010101010

(1) - Cannot be seperated from Diphenylamine

FORM I SU-2 flR3037ll

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

Page 38: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS Contract: I MU-9A

Lab Code: LANCAS Case No: SAS No: SDG No:

Matrix (soil/water) WATER . Lab Sample ID: 1393590

Sample ut/vol: 1000 (g/ml) ML Lab File ID: A89150_041.RES

Level: (lou/med) LOU Date Received: 05/26/89

\ Moisture: not dec dec. Date Extracted: 05/30/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/31/89

GPC Cleanup: (Y/N) N pH: 6.9 Dilution Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NO. COMPOUND ——————— Q

I 319-84-6—————alpha-BHC_' 319-85-7—————beta-8HC_319-86-8—————de I ta-8HC_58-89-9—————gamma-BHC (Lindane).76-44-8—————Heptachlor______

I 309-00-2—————Aldrin.____________I 1024-57-3————Heptachlor epoxide.I 959-98-8—————Endosulfan I_____I 60-57-1——————Dieldrin________I 72-55-9——————4,4'-DOE________I 72-20-8——————Endrin__________I 33213-65-9———Endosulfan II____I 72-54-8—————4,4'-ODD________I 1031-07-8————Endosulfan sulfate50-29-3—————4,4'-ODT.72-43-5—————Methoxych lor__53494-70-5———Endrin ketons_5103-71-9————alph*-Chlordan«_5103-74-2————g»mraa-Chlordane_8001-35-2————Toxaohane12674-11-2———Aroclor-1016__11104-28-2———Aroclor-1221__11141-16-5———Aroclor-1232__53469-21-9———Aroclor-1242__12672-29-6———Aroclor-1248__11097-69-1———Aroclor-1254__11096-82-5———Aroclor-1260__

1.

.05

.05

.05

.05

.05

.05

.05

.05

.1

.1

.1

.1

.1

.1

.1

.5

.1,5.5•

.5

.5

.5

.5

.51.1.

I UUUUUUUUUUUUuuu

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FORM I PEST 1/87 Rev.

flR3037!2

Page 39: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

. ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _____________

.ab Name: LANCASTER LABS • Contract: I MU-9B

Lab Code: LANCAS Case No: SAS No: SD6 No:

Matrix (soil/water) WATER Lab Sample ID: 1393591

Sample wt/vol: . 1000 (g/ml) ML Lab File ID: A89150JJ43.RES

Level: (low/mod) LOUI Date Received: 05/26/89

\ Moisture: not dec dec. Date Extracted: 05/30/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 06/01/89

GPC Cleanup: (Y/N) N - pH: 7.4 Dilution Factor: l.Q

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NO. COMPOUND ——————— Q

319-84-6—————alpha-BHC_______319-85-7—————beta-BHC________319-86-8—————delta-BHC_______58-89-9—————gamma-BHC (Lindane).76-44-8——————Heptachlor_______'309-00-2—————Aldrin__________1024-57-3————Heptachlor epoxide959-98-8—————Endosulfan I_____60-57-1—————Dieldrin_______72-55-9—————4,4'-DDE________72-20-8—————Endr in_________33213-65-9———Endosulfan II____72-54-8—————4,4'-ODD_______1031-07-8————Endosulfan sulfate.50-29-3—————4,4'-DOT_______72-43-5—————Methoxych lor_____53494-70-5———Endrin ketons____5103-71-9————«lph«-Chlordane__5103-74-2————gatMM-Chlordane__8001-35-2————Toxaphens_______12674-11-2———Aroclor-1016____11104-28-2———Aroclor-1221____11141-16-5———Aroclor-1232_____53469-21-9———Aroclor-1242_____12672-29-6———Aroclor-1248_____11097-69-1———Aroclor-1254____11096-82-5———Aroclor-1260______

I

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.05

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.05

.05

.05

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FORM I PEST 1/87 Rev.

flR3037!3 269

Page 40: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

; ID EPA SAMPLE NO.PESTICIDE ORGAN ICS ANALYSIS DATA SHEET _____________

•b Name: LANCASTER LABS Contract: I EQ8-1

Lab Code: LANCAS Case No: SAS No: SDG No:.»»_.. — ,_.»_•.» •» •• «• w .• — — — •• »•«-« — «•-_.•• »«

Matrix (soil/water) WATER Lab Sample ID: 1393592

Sample wt/vol: 1000 (g/ml) ML Lab File ID: AS9150_044.RES

Level: (low/med) LOU Data Received: 05/26/89

* Moisture: not dec dec. Date Extracted: 05/30/89

Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 06/01/89

GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NO. COMPOUND —————

319-84-6—————a Ipha-BHC_______319-85-7—————beta-BHC________319-86-8—————de I ta-BHC_______58-89-9-—————gamma-BHC (Lindane).76-44-8——————Heptach lor_______309-00-2—————Aldrin__________1024-57-3———-Heptachlor epoxide_959-98-8—————Endosulfan I_____60-57-1—————Oieldrin________72-55-9—————4,4' -ODE________.,72-2Q-8—————Endr in__________33213-65-9———Endosulfan II____72-54-8—————4,4' -ODD________1031-07-8————Endosulfan sulfate_50-29-3——————4,4'-DOT____'72-43-5——————Methoxychlor_____53494-70-5———Endrin ketone____

I 5103-71-9————alpha-Chlordane.I 5103-74-2———--gamma-Chlordane.8001-35-2————Toxaphene12674-11-2———Aroclor-1016.11104-28-2———Aroclor-1221.11141-16-5———Aroclor-1232.53469-21-9———Aroclor-1242,12672-29-6———Aroclor-1248,11097-69-1———Aroclor-1254.11096-82-5———Aroclor-1260

I

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FORM I PEST 1/87 Rev.

flR3037IU

Page 41: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

38T

U.S. EF'A - CLPEPA SAMPLE

1INORGANIC ANALYSIS DATA SHEET I

I MW—9?Lab Name: Lancaster Laboratories Contract: I

Lab Codes Case No.: SAS No.: SDS No.: MU-t

Matrix (soil/water): WATER Lab Sample ID: 13935e?0

Level (low/med): LOW Date Received: 05/E6/E1

'/. Solids: 0.0

Concentration Units (ug/L or rug/kg dry weight): UG/L

I1C AS No.11 7459-90-5I 7440-36-O1 7440-38-21 7440-39-317440-4 1-7| 7440-43-9| 744O-70-2| 7440-47-3| 7440-49-41 7440-50-817439-89-617439-92-117439-95-417 39-96-51 7439-97-6I 7440-OS-O| 7440-09-71 7782-49-2| 7440-22-41 7440-23-51 7440-28-01 744O-62-21 7440-66-61 __________1

11 Analyte11 Aluminum1 Ant imony1 Arsenic1 Bar iufn1 Beryl 1 iu.m1 Cadmium1 C a 1 c i urn1 Chromium1 Cobalt1 CoE2er1 Iron(Lead1 MagnesiumI Manaanese1 Mercury(Nickel1 PotassiumI Selenium1 S i 1 ver1 SodiumIThal 1 iu.m1 VanadiumISinc1 Cy am de _1

Co nc en t r a. t i o n

681014.61.8

_2030 . 500 . 95268004.54. 1

_ ____ il._a________ 1600_

2.52350087.10. 165.043700 . 802.9

1 860O2.010.534.4_ 2_.5_

1 1I CI1 t1 1I U IIUI1 i£IUIIUI1 1IUIIBI1 11 1'Il__1 11 1I B IIBI1 1MJIIUI1 1IUII B I1 1IUI1 l"

1 !a in .1

1 1IP 1IP 1IF 1IP 1IP-IPIP-IPIPIPIPIFIPIPICVIPIPIFIPIPIFIP-IP

___ J.ASl"

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM i - IN AR3037I5

Page 42: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA '- CLPEPA SAMPLE t

1INORGANIC ANALYSIS DATA SHEET |—————

I MW—98Lab Name: Lancaster Laboratories Contract: I

Lab Code: Case No.: SAS No.: SDG No.: MW—

Matrix (soi1/water): WATER Lab Sample ID: 1393391

Level (low/med): LOW Date Received: 05/26/89

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): US/L

1ICAS No.11 7429-90-51 7440-36-0| 744O-38-2| 7440-39-3| 7440-4 1 -7| 7440-4.3-9| 7440-70-2| 7440-47-3I 7440-48-4(7440-50-81 7439-89-6 'I7439-.J2-11 7439-95-41 7439-96-31 7439-97-6| 74 0-02-0I 7440-00-71 7782-49-21 7440-22-41 7440-23-51 7440-28-01 7440-62-217440-66-61 ____________1

11 Analyte11 Aluminum1 Antimony1 Arsenic1 Bar iu.m1 Bervl 1 ium1 Cadmium1 Calcium1 Chromium(Cobalt1 Cogger1 Iron1 Lead(Magnesium(Manganese1 Mercury(Nickel(Potassium1 SeleniumISi Iver1 Sodium1 Thai 1 ium1 Vanadium(Zinc1 Cyanide _1

Concentration

50 . 614.65. 154.60 . 50

_ ___ 4j.I_362004.52... 3-

_____ 3.0_______ 23.8

2.41O3001 0 . 0

_ _ Oj.124.2967

______ 1*2-_____ __2.i_L

12100- — S.O

4.027.8

___ 2.5

1 IICI G1 1IB!IUIIBIWIBIEIUIf (1 1IUIIUI _____IUIIBIIUI1 11 1IBIIUIIB!IBIIUI1 IIUIIBI1 l1 LM ______i~T

1IM1IPIPIFIPIP-IPIPIPIPIPIPIFIPIPICVIPIP-IPIP 1IP 1IF 1IP 1IP 1J.ASI1 ~l

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comment's:

FORM I - IN

8flR3037!6

Page 43: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLP

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract: _______

Lab Code: Case No.: SAS No.: SDG No.: M.-J--l

Matrix (soi1/water): WATER Lab Sample ID: 139259E

Level (low/med): LOW Date Received: 05/E6/E?

'/, Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

1ICAS No.11 7429-90-51.7440-36-01 7440-38-21 7440-39-317440-41-71 7440-43-9| 7440-70-21 7440-47-3| 7440-48-4| 7440-50-817439-89-617439-92-11 74.39-95-417439-96-517439-97-61 7440-02-01 7440-09-71 7782-49-2I 7440-22-41 7440-23-51 7440-28-0| 7440-62-2| 7440-66-611

11 Analyte11 Aluminum1 AntimonyI Arsenic1 Bar ium1 Beryl 1 ium1 Cadmium1 Calcium1 ChromiumICoba.lt1 Cogger1 Iron •ILgad__ _1 Magnesium1 Manaanese1 Mercurv1 Nickel1 Potags ium1 SeleniumISilver1 Sodium1 Thai 1 ium1 Vanad i urnIZinc1 Cvanide1

Concentration

29.614.61 .81.50 . 500 . 9588 . 04.52.33.0

16.82.423.0

_______ §^2_0 . 1 04.254.50 . 80

________ §_,?_1712.0

______ i^_4.82.5

1 1ICI Q1 1I UIIUIIUIIB IEI U II U IIBIIUIIUIIUII B IIUIIBIIU IIUIIUII U IIUIIUIIBIIUIIU IIBIIUI1 1

1IM1IP-IPIFIF'IP-IPIP-IPIPIPIPIFIP-IPICVIP-IPIFIP-IPIFIPIPIAS1

Color Before: Clarity Before: Texture:

Color After: , Clarity After: Artifacts:

Comments:

FORM I -5 0 l 7I / Rev, IFB ftf-e-.-_r.--.«-

Page 44: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

. • "•••;•-- • - -

PHASE II

ANALYTICAL RESULTS BYSAMPLE DELIVERY GROUP

Rl-BAN

RR3037I8

Page 45: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

SDG-WST8

rl.ban - . , - - - - . . . ... L,.,- ;:7,7

*"-»---- .." " , r " -: " ,_"•. .i'

fi3031fi

Page 46: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS • Contract:SW06H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587952

Sample wt/vol: ' 5.0 (g/mL) ML Lab File ID: A1587952

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3——————Chloromethane_74-83-9——————Bromomethane_75-01-4——————vinyl Chloride,75-00-3———————Chloroethane__75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide_____________75-35-4———————1,1-Dichloroethene________75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3——————Chloroform__________107-06-2—————l,2-Dichloroethane_78-93-3——————2-Butanone_________________71-55-6———————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate _____75-27-4—————--Bromodichloromethane____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43 -2 ——————Benzene______________10061-02-6————trans-l,3-Dichloropropene_75-25-2———————Bromoform108-10-1——————4-Methyl-2-Pentanone_591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane.108-88-3—•———Toluene______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene______•100-42-5—————Styrene1330-20-7—————Xylene (total).

1010101051355555510551055555555510105555555

UUUuuBUUUuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I VOA flR303l7a^ORev.

Page 47: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SW07H

- 7

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587953

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587953

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO.. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3——————Chloromethane_74-83-9———————Bromomethane__75-01-4——————Vinyl Chloride,75-00-3——————Chloroethane_75-09-2———————Methylene Chloride,67-64-1———————Acetone________________75-15-0——————-Carbon Disulfide________75-35-4——'—•———1,1-Dichloroethene_______75-34-3 ——————— 1,1-Dichloroetharie_______540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform____________\107-06-2—————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5——•———Carbon Tetrachloride108-05-4—————Vinyl Acetate____________75-27-4———————Bromodichloromethane___,_78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-I,3-Dichloropropene__79-01-6——————-Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2--—————Benzene______________10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene_______7 9-34-5———————1,1,2,2 -Tetrachloroethane,108-88-3——————Toluene______________108-90-7——————Chlorobenzene_________100-41-4—————Ethylbenzene_________100-42-5——————Styrene_______________1330-20-7—————Xylene (total)________

10•10810516555

31055105510555

3605555510105555555

UUJUuBUUUEUuuuuuuuuEUUuuuuuuuuuuuu

FORM I VC^R 3 Q 3 7 2 | 1/87 Rev .

Page 48: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS Contract:SW07HDL

- 7

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587953D2

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587953D2

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 2.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83-9——————Bromomethane_75-01-4——————Vinyl Chloride,75-00-3——————Chloroethane75-09-2——————Methylene Chloride,67-64-1———————Acetone_________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0—————'-1,2-Dichloroethene (total)67-66-3——————Chloroform__________'107-06-2—————1,2-Dichloroethane,78-9 3-3 ——————2 -Butanone_______~_71-55-6——————1,1, l-Trichloroethane_56-23-5———————Carbon Tetrachloride_108-05-4——————Vinyl Acetate_75-27-4———————Bromodichloromethane,78-87-5———————l,2-Dichloropropane_10061-01-5————cis-l,3-Dichloropropene_79-01-6———————Trichloroethene______124-48-1——————Dibromochloromethane_79-00-5——————1,1,2-Trichloroethane,71-43-2——————Benzene10061-02-6————trans-l,3-Dichloropropene_75-25-2———————Bromofonn _____108-10-1——————4-Methyl-2-Pentanone.591-78-6——————2-Hexanone________127-18-4——————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene108-90-7——•——Chlorobenzene_100-41-4—————Ethylbenzene_100-42-5—————styrene_____1330-20-7—————Xylene (total)

20208201029101010

2801010201010201010103101010101010202010101010101010

UuDJUUBDUUUDUUUUUUUUUDUUUUUUUUUUUUUu

FORM I VOAH30 1/87 ReV'

Page 49: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A . EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SW10H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587950

Sample wt/vol: . 5.0 (g/mL) ML Lab File ID: A1587950

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3 ——————— -74-83-9 ——————— -75-01-4 ——————— -75-00-3 ——————— -

67-64-1 ——————— -75-15-0 ——————— -75-35-4 ——————— -75-34-3 ——————— -540-59-0 —————— -

107-06-2 —————— -

71-55-6 ——————— •

108-05-4 —————— •75-27-4 ——————— •/o O/ O10061-01-5 ———— •

124-48-1 —————— •

/ .1- ^ — ' £+

10061-02-6 —— ' — •* ._* «• ~* _i108-10-1 —————— •591-78-6 —————— -127-18-4 —————— •79-34-5 ——————— •

108-90-7 —————— •100-41-4 —————— •100-42-5 —————— •1330-20-7 ————— •

•Chloromethane•Bromomethane-Vinvl Chloride•Chloroethane-Methvlene Chloride•Acetone•Carbon Disulfide-1 , 1-Dichloroethene•1, 1-Dichloroethane•1,2-Dichloroethene (total) __•Chloroform-1 , 2-Dichloroethane•2-Butanone-1,1, l-Trichloroethane-Carbon Tetrachloride-Vinyl Acetate- Br omod ichl o r omethane-1,2-Dichloropropane-cis-1, 3-Dichloropropene-Trichloroethene-Dibromochloromethane-1, 1, 2-Trichloroethane-Benzene-trans-1, 3-Dichloropropene ___-Bromoform-4 -Methyl -2 -Pentanone

£16XuIiOri6is uju awnxo_L oe unene-1,1,2,2 -Tetrachloroethane ___

JU WX l_L«Si IvS

-Chlorobenzene-Ethylbenzene-Styrene-Xylene (total)

101010458552535551065510555175555510105555555

UUUJUBJU

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FORM i voA 1/87 Rev>

Page 50: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS Contract:SW10D

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587951

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587951

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane____74-83-9——————Bromomethane75-01-4——————Vinyl Chloride___75-00-3——————Chloroethane_____75-09-2——————Methylene Chloride,67-64-1———————Acetone_____________~75-15-0———————Carbon Disulfide__75-35-4———————l,l-Dichloroethene_75-34-3———————1,1-Dichloroethane"540-59-0——————1,2-Dichloroethene (total)__67-66-3——————Chloroform107-06-2——————1,2-Dichloroethane__78-93-3——————2-Butanone________71-55-6——————1,1,1-Trichloroethane,56-23-5——————Carbon Tetrachloride_108-05-4——————Vinyl Acetate75-27-4——————Bromodichloromethane_78-87-5———————l,2-Dichloropropane_10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1——————Dibroraochlorome thane____79-00-5——————1,1,2-Trichloroethane___71-4 3-2 ——————Benzene_________________10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform108-10-1——————4-Methyl-2-Pentanone591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene___________79-34-5———————1, l,2,2-Tetrachloroethane_108-88-3——————Toluene__________________~_108-90-7——————Chlorobenzene______________100-41-4—————Ethylbenzene_________100-42-5—————Styrene_____________1330-20-7—————Xylene (total)________

1010105rs56

2940551076510555205555510105555555

UUUJJBJU

FORM I VO - 1/87 Rev.O|R 3 Q g -, g

Page 51: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _______

Lab Name: LANCASTER LABS Contract:SW14H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587949

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587949

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/9.0

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. "COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83 -9 ———————Bromomethane_75-01-4———————Vinyl Chloride.75-00-3———————Chloroethane75-09-2———————Methylene Chloride67-64-1———————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3———————Chloroform ____________107-06-2——————1,2-Dichloroethane__78-93-3——'•————2-Butanone_________71-55-6———————1,1,1-Trichloroethane,56-23-5———————Carbon Tetrachloride_108-05-4—————Vinyl Acetate,75-27-4——————Bromodichloromethane__78-87-5——————1,2-Dichloropropane___10061-01-5————cis-l,3-Dichloropropene_79-01-6——————Trichloroethene124-48 -1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———————Benzene________________10061-02-6————trans-l,3-Dichloropropene_75-25-2———————Bromoform____________________108-10-1——-——4-Methyl-2-Pentanone,591-78-6——————2-Hexanone • __"127-18-4—————Tetrachloroethene______79-34-5——————1/1,2,2-Tetrachloroethane_108-88-3——————Toluene______________108-90-7——————Chlorobenzene_________'_100-41-4——————Ethylbenzene__________100-42-5——————styrene______________1330-20-7—————Xylene (total)________

101010105955555510551055555555510105555555

UUUuuBJUUUUUUUUuuuuuuuuuuuuuuuuuuuu

FORM I VOA 1/87 Rev.

Page 52: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA 'SHEET

,ab Name: LANCASTER LABS Contract:SW17H•JT/.J-/7

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587944

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587944

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3 —————

75-01-4 —————75-00-3 —————/ _/ w y ft67-64-1 —————75-15-0 — - ——75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————/ O . 7 J J"T *. P? E £ - -

c ez *.» i c

108-05-4 ————~i & f\ *^ j

10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————•".- t .* ••* *•»71-43-2 —— • — --10061-02-6 ——75-25-2 —— ——108-10-1 ————

127-18-4 — ——79-34-5 —————

100-41-4 ————100-42-5 ————1330-20-7 ———

—— Chloromethane—— Bromomethane—— Vinyl Chloride—— Chloroethane—— Methylene Chloride

Acetone— —Carbon Disulfide—— 1 , 1-Dichloroethene—— 1, 1-Dichloroethane—— 1,2-Dichloroethene (total)—— Chloroform—— 1 , 2-Dichloroethane—— 2-Butanone—— 1,1, 1-Trichloroethane—— Carbon Tetrachloride—— Vinyl Acetate—— Bromodichloromethane—— 1 . 2-Dichloropropane—— cis-1 , 3 -Dichioropropene—— Trichloroethene—— Dibromochloromethane—— 1,1,2-Trichloroethane—— Benzene—— trans-l, 3-Dichloropropene ___—— Bromoform—— 4-Methyl-2-Pentanone—— 2 -Hexanone—— Tetrachloroethene—— 1 ,1,2, 2-Tetrachloroethane ___—— Toluene—— Chlorobenzene— — Ethylbenzene—— Styrene—— Xvlene (total)

101010105655555510751055525555510105555555

UUuuuBJUUUJUUU

UuuuuJuuuuuuuuuuuuuu

FORM I VC&R 303726 V87 Rev. 63

Page 53: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO,VOLATILE ORGANICS ANALYSIS DATA SHEET ___

Lab Name: LANCASTER LABS Contract:SW18H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587942

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587942

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83 -9 ———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride,67-64-1———————Acetone_______________75-15-0——————--Carbon Disulfide________75-35-4———————1,1-Dichloroethene________75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3———————Chloroform107-06-2——————1, 2-Dichloroethane__78-93-3———————2-Butanone____________71-55-6———:———1,1,1-Trichloroethane.56-23-5———————Carbon Tetrachloride_108-05-4——————Vinyl Acetate,75-2 7-4 ——————Bromodichlororaethane____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene79-01-6——————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6————trans-l,3-Dichloropropene_75-25-2———————Bromoform_______________108-10-1——————4-Methyl-2-Pentanone____591-7-8-6——————2-Hexanone127-18-4——————Tetrachloroethene______79-34-5——————1, l,2,2-Tetrachloroethane_108-88-3——————Toluene______________~108-90-7——————Chlorobenzene__________100-41-4—————Ethylbenzene__________100-42-5——————Styrene___________________1330-20-7—————Xylene (total)__________

10101010510555555105510555555555 .10105555555

UUuuuBJUUUUUUuuuuuuuuuuuuuuuuuuuuuu

FORM I VOAftR3Q3727 1/87 Rev.

Page 54: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS Contract:SW18D

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587943

Sample wt/vol: 5.0 (g/mL) ML . Lab File ID: A1587943

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: i.o

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83-9 ———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3——————Chloroethane75-09-2———————Methylene Chloride________67-64-1——————Acetone______________________75-15-0——————Carbon Disulfide_____________75-35-4——————1,1-Dichloroethene________75-34-3——————1,1-Dichlor.oethane_________540-59-0—————1,2-Dichloroethene (total)__67-66-3——————Chloroform_______________________107-06-2 —————— 1,2-Dichloroethane____________78-93-3————————2-Butanone_____________________71-55-6———————1,1,1-Trichloroethane______56-23-5———————Carbon Tetrachloride_______108-05-4—-———vinyl Acetate________________75-27-4——-———Bromodichloromethane______78-87-5——————1,2-Dichloropropane_________10061-01-5————cis-l, 3-Dichloropropene_______79-01-6——————Trichloroethene__________124-48-1——————Dibromochloromethane_______79-00-5———————1,1,2-Trichloroethane______71-43-2———————Benzene_________________10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform____________"108-10-1——————4-Methyl-2-Pentanone591-7-8-6——————2-Hexanone127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene___________________________108-90-7——————Chlorobenzene_________100-41-4——————Ethylbenzene__________________100-42-5——————Styrene________________________1330-20-7—————Xylene (total)__________

101010105755555510551055555555510105555555

UUUuuBJUUUuuuuuuuuuuuuuuuuuuuuuuuuu

FORM i WH303728 1/87 Rev-

Page 55: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

SW19HLab Name: LANCASTER LABS Contract:

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587948

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587948

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK .Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83 -9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride______67-64-1——————Acetone______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene________75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform107-06-2————;—1,2-Dichloroethane____78-93-3———————2-Butanone___________71-55-6-——————1,1,1-Trichloroethane__56-23-5———————Carbon Tetrachloride__108-05-4——————Vinyl Acetate________75-27-4——————Bromodichloromethane__78-87-5——————1,2-Dichloropropane___10061-01-5————cis-1,3-Dichloropropene,79-01-6———————Trichloroethene______124-48-1——————Dibromochlorome thane__79-00-5———————1,1,2-Trichloroethane__71-4 3-2 ———————Benzene10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform108-10-1——————4-Methyl-2-Pentanone_591-78-6——————2-Hexanone127-18-4—————-Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene__________100-42-5——————Styrene1330-20-7—————Xylene (total).

101010105855555510551055555555510105555555

UUUuuBJUUUUUUUUuuuuuuuuuuuuuuuuuuuu o

FORM i vo 1/87 Rev- 93

Page 56: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A ' EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Name: LANCASTER LABS Contract:SW20H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587945

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587945

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/22/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. 'COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4——————Vinyl Chloride,75-00-3——————Chloroethane75-09-2——————Methylene Chloride,67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3 ——————— 1,1-Dichloroethane_______540-59-0——————1,2-Dichloroethene (total).67-66-3———————Chloroform_____________107-06-2—————1,2-Dichloroethane__78-93-3——————2-Butanone________71-55-6———•——1,1, l-Trichloroethane_56-23-5——————Carbon Tetrachloride_^108-05-4——————Vinyl Acetate,75-27-4———————Bromodichloromethane____78-87-5———————1,2-Dichloropropane_____10061-01-5——:—cis-1,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene______________10061-02-6————trans-1,3-Dichloropropene,75-25-2——————Bromoform108-10-1——————4-Methyl-2-Pentanone591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3—————Toluene_____________"108-90-7——————Chlorobenzene__________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Xylene (total)____

1010101052054555510851055555555510105555555

UUuuuBUJUUUUU

Uuuuuuuuuuuuuuuuuuuu

FORM I TO303730 1/87 Rev

Page 57: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _________

Lab Name: LANCASTER LABS Contract:SW21H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587941

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587941

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane__75-09-2———————Methylene Chloride__________67-64-1———————Acetone__________75-15-0——————-Carbon Disulfide________75-35-4——•————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3——————Chloroform107-06-2——————1,2-Dichloroethane________78-93-3———————2-Butanone____________________71-55-6———————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane78-87-5———————1,2-Dichloropropane________10061-01-5————cis-1,3-Dichloropropene_79-01-6——————Trichloroethene_______124 -48-1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane___71-43-2—•—————Benzene_______________10061-02-6————trans-1,3-Dichloropropene,75-25-2———————Bromoform108-10-1——————4-Methyl-2-Pentanone_591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7——————Chlorobenzene________________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_________________________1330-20-7—————Xylene (total) ______

101010105

2355555510551055555555510105555555

__ i

FORM I VO 1/87 Rev. 39

Page 58: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO'.VOLATILE ORGANICS ANALYSIS DATA SHEET ___

b Name: LANCASTER LABS Contract:SW22H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587939

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587939

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3 — —— -74-83-9 —— — —75-01-4 —— ——75-00-3 —————

67-64-1 —————75-15-0 —— ——75-35-4 —————75-34-3 —— ——540-59-0 ————67-66-3 —— ——107-06-2 ————/ O — ' _> J71-55-6 —— ——56-23-5 —— ——108-05-4 ————75-27-4 —————T O O — / . ?

10061-01-5 ——

124-48-1 ————79-00-5 —————71-43-2 —— ——10061-02-6 ——75-25-2 —— ——108-10-1 ————

127-18-4 ————79-34-5 —————

100-41-4 ————100-42-5 ————1330-20-7 ———

—— Chloromethane—— Bromomethane—— Vinvl Chloride—— Chloroethane—— Methylene Chloride

AC @ *— O Ii VS

—— Carbon Disulfide—— 1, 1-Dichloroethene—— 1 , 1-Dichloroethane—— 1,2-Dichloroethene (total) __—— Chloroform—— 1 , 2-Dichloroethane—— 2-Butanone—— 1, 1, 1-Trichloroethane—— Carbon Tetrachloride—— Vinyl Acetate—— Bromodichloromethane—— 1 , 2-Dichloropropane—— cis-1 , 3 -Dichloropropene—— Trichloroethene—— Dibromochloromethane—— l ,1,2 -Trichloroethane—— Benzene—— trans-l, 3-Dichloropropene ___—— Bromoform—— 4 -Methyl-2 -Pentanone—— 2-Hexanone—— Tetrachloroethene—— 1,1 , 2 , 2-Tetrachloroethane ___—— Toluene—— Chlorobenzene—— Ethylbenzene—— Styrene—— Xvlene (total)

101010105

2255555510551055555555510105555555

UUUuuBUUUUUuuuuuuuuuuuuuuuuuuuuuuu

FORM I VOA $R3Q3732 V87 Rev.

Page 59: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _____________

Lab Name: LANCASTER LABS Contract:SW23H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587940

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587940

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane__74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane__75-09-2———————Methylene Chloride.67-64-1———————Acetone________________75-15-0———————Carbon Disulfide__________75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform____________'107-06-2—————1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6——————1,1,1-Trichloroethane___56-23-5———-———Carbon Tetrachloride______108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6—————-Trichloroethene________124-48 -1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane___71-43-2———————Benzene_____________'10061-02-6——;——trans-1,3-Dichloropropene,75-25-2———————Bromoform______________~108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_________________127-18-4——————Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________~108-90-7—————Chlorobenzene_______________100-41-4——————Ethylbenzene__________100-42-5——————styrene______________1330-20-7—————Xylene (total)_________

101010105

2355555510551055555555510105555555

UUUuuBUUUUUUUuuuuuuuuuuuuuuuuuuuuu

FORM IVO£R3Q3733 1/87 Rev. 31

Page 60: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ___

Name: LANCASTER LABS Contract:SW25H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER ' Lab Sample ID: A1587957

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587957

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK • Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride_75-00-3 ———————Chloroethane__75-09-2———————Methylene Chloride_______67-64-1——————Acetone____________________75-15-0—:————Carbon Disulfide_______75-35-4-'—————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform____________'107-06-2——————1,2-Dichloroethane____78-93-3———————2-Butanone___________71-55-6——————1,1,1-Trichloroethane_56-23-5———————Carbon Tetrachloride__108-05-4——————Vinyl Acetate________75-27-4——————Bromodichloromethane__78-87-5——————1,2-Dichloropropane___10061-01-5————cis-l,3-Dichloropropene_79-01-6——————Trichloroethene_______124-48-1——————Dibromochloromethane__79-00-5———————1,1,2-Trichloroethane__71-43-2—r—————Benzene_____________________10061-02-6————trans-1,3-Dichloropropene,75-25-2——————Bromoform____________"108-10-1——————4-Methyl-2-Pentanone591-78-6——————2-Hexanone_______ "127-18-4——————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3——————Toluene______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene__________________100-42-5——————Styrene1330-20-7—————Xylene (total).

101010105

2655555510551055555555510105555555

UUUuuBUuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I V O A R l 1/87 ReV'

Page 61: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SW26H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587959

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587959

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. ' COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————/ O J -> -S — — «•-•—•^ 1 C? K f

c e__ *} o .___. e

108-05-4 ————75-27-4 —————/ O O / ;j»~» — » —

10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——•7 C •- C O

108-10-1 ————

127-18-4 ————79-34-5 —————

100-41-4 ————100-42-5 ————1330-20-7 ———

—— Chloromethane—— Bromomethane—— Vinvl Chloride—— Chloroethane—— Methvlene Chloride

«_WC3 U-Wilt.5

—— Carbon Disulfide—— 1. 1-Dichloroethene—— 1, 1-Dichloroethane—— 1,2-Dichloroethene (total) __—— Chloroform—— 1 , 2-Dichloroethane—— 2-Butanone—— 1 , 1 , 1-Trichloroethane—— Carbon Tetrachloride—— Vinyl Acetate—— Bromodichloromethane—— 1, 2-Dichloropropane—— cis-1, 3-Dichloropropene—— Trichloroethene—— Dibromochloromethane—— 1 , 1 , 2-Trichloroethane—— Benzene—— trans-1, 3-Dichloropropene ___—— Bromoform—— 4-Methyl-2-Pentanone—— 2-Hexanone—— Tetrachloroethene—— 1 ,1,2,2 -Tetrachloroethane ___

jLoxusne—— Chlofobenzene—— Ethylbenzene

ot*y.ut5iie—— Xylene (total)

101010105955555510551055555555510105555555

UUUuuBJUUUUUUUUuuuuuuuuuuuuuuuuuuuu

popI VOA V87 Rev.

Page 62: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLEZNQ.VOLATILE ORGANICS ANALYSIS DATA SHEET '''''

b Name: LANCASTER LABS Contract:SW27H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587958

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A158795S

Level: (low/med) LOW • Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3——————Chloromethane_74-83-9——————Bromomethane_75-01-4——————Vinyl Chloride,75-00-3——————Chloroethane75-09-2———————Methylene Chloride,67-64-1———————Acetone________________75-15-0———————'Carbon Disulfide________75-35-4———;—'——1,1-Dichloroethene_______75-34-3———————1,1-Dichloroethane______•540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform___________________107-06-2—————1,2-Dichloroethane______78-93-3——————2-Butanone_________________71-55-6——————1,1,1-Trichloroethane___56-23-5———•———Carbon Tetrachloride_____108-05-4—————Vinyl Acetate__________75-27-4———————Bromodichloromethane78-87-5———————l,2-Dichloropropane________10061-01-5————cis-1,3-Dichloropropene__79-01-6——————Trichloroethene___________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene______________10061-02-6——;——trans-l,3-Dichloropropene_75-25-2———————Bromoform108-10-1——————4-Methyl-2-Pentanone_591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane,108-88-3—————Toluene_____________~108-90-7—————Chlorobenzene____________100-41-4—————Ethylbenzene__________100-42-5—————Styrene______________1330-20-7—————Xylene (total)______________

101010105755555510551055555555510105555555

UUuuuBJUUUUuuuuuuuuuuuuuuuuuuuuuuuu

FORM I VOA . nonOTJC 1/87 Rev.flR3037361/87

Page 63: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:REF1H

Lab Code: LANCAS Case No.-: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587956

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: A1587956

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3——————Chloromethane_74-83-9——————Bromomethane_75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride,67-64-1———————Acetone_____75-15-0———————Carbon Disulfide________75-35-4--—————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride108-05-4——————Vinyl Acetate__________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane____10061-01-5——.——cis-1,3-Dichloropropene_79-01-6——————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6————trans-1,3-Dichloropropene,75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene79-34-5——————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene_____________~108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene__________100-42-5——————styrene______________1330-20-7—————Xylene (total) _____

101010105

2455555510551055555555510105555555

FORM I VOA, Q n Q -, Q 7 1/87 Rev. 20'^303737

Page 64: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS Contract:HA02H

Lab Code: LANCAS Case No.: 276702 SAS No.: SDG No.: WST8

Matrix: (soil/water) WATER Lab Sample ID: A1587955

Sample wt/vol: 5.0 (g/mL) ML . Lab File ID: A1587955

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. Date Analyzed: 10/23/90

Column: (pack/cap) PACK Dilution Factor: i.o

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4——————Vinyl Chloride,75-00-3——————Chloroethane75-09-2——————Methylene Chloride,67-64-1———————Acetone______________________75-15-0——-——Carbon Disulfide_______75-35-4——-———1,1-Dichloroethene__________75-34-3-——————1,1-Dichloroethane__________540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________________107-06-2——————1,2-Dichloroethane__78-93-3——————2-Butanone_____________71-55-6——————1,1, l-Trichloroethane_56-23-5——————Carbon Tetrachloride_I108-05-4—————vinyl Acetate,75-27-4——————Bromodichloromethane,78-87-5——————1,2-Dichloropropane,10061-01-5———'—cis-1,3-Dichloropropene79-01-6———————Trichloroethene_______________124-48 -1——————Dibromochloromethane____79-00-5———————1,1, 2-Trichloroethane___71-43-2——————Benzene______________10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform____________________108-10-1—————4-Methyl-2-Pentanone_591-78-6—————2-Hexanone127-18-4—————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene_____________________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene____________________100-42-5—————Styrene____________________1330-20-7—————Xylene (total)_______________

101010105

2055555510551055555555510105555-555

UUuuuBUuuuuuu.uuuuuuuuuuuuuuuuuuuuu

199FORM/fjf3i33738 1/87 Rev<

Page 65: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW06H

Lab Code: Case No.: SAS No.: SDG No.: WST8-I

Matrix (soil/water): WATER Lab Sample ID: 1587952

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercury^NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

2.2

4.0

8.6

3.9

56.6

1.4

119

C

U

B

U

B

U

Q

W

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/33

BR3Q3739

Page 66: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 ___INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW07HI

Lab Code: Case No.: SAS No.: SDG No.: WST8-I

Matrix (soil/water): WATER Lab Sample ID: 1587953

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercury^NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

5.2

38.7

31.0

230

1.4

85.8

C

U

U

U

Q M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/83

AR3037i»0

Page 67: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW10HI

Lab Code: Case No.: SAS No.: SDG No.: WST8-I

Matrix (soil/water): WATER Lab Sample ID: 1587950

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-4.8-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMaqnes iumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

7.2

22.3

35.8

108

1.4

43.6

C

U

U

u

Q M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/88

ftR3Q37M 18

Page 68: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 ' ___________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW10DI

Lab Code: Case No.: SAS No.: SDG No.: WST3-I

Matrix (soil/water): WATER Lab Sample ID: 1587951

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0 .

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromium.CobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

15.9

35.6

77.0

241

1.4

59.2

C

U

U

u

Q M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/8317

Page 69: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 ' __________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW14HI

Lab Code: Case No.: SAS No.: SD.G No.: WST3-I

Matrix (soil/water): WATER Lab Sample ID: 1587949

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

12.9

3.4

42.7

1.4

16.7

C

U

U

U

u

Q

W

M

NRPNRNRNR1PNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/33

AR3037^3 19

Page 70: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 ______INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW17HI

Lab Code: Case No.: SAS No.: SDG No.: WSTS-I

Matrix (soil/water): WATER Lab Sample ID: 1587944

Level (low/raed): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

6.7

13.4

7.1

269

1.4

326

C

U

U

U

Q

w

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/83

flR3037i.ii ^°

Page 71: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 __________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW18HI

Lab Code: Case No.: SAS No.: SDG No.: WST8-I

Matrix (soil/water): WATER Lab Sample ID: 1587942

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

10.2

2.3

243

1.4

60.9

C

U

U

U

B

B

U

Q

w

M

NRPNRNRNR-PNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/83

22flR3037t.5

Page 72: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 ____INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW18DI

Lab Code: Case No.: SAS No.: SDG No.: WSTS-I

Matrix (soil/water): WATER Lab Sample ID: 1537943

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimony:ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

7.5

1.2

207

1.4

50.4

C

U

U

U

B

B

U

Q

W

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN ' 7/33

23.HR3Q371.6

Page 73: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW19H

Lab Code: Case No.: SAS No.: SDG No.: WST3-I

Matrix (soil/water): WATER Lab Sample ID: 1587948

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-4 .7439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobalt •CopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

15.6

44.5

6.3

206

1.4

64.5

C

U

u

u

Q M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN . 7/88

AR3Q37U7

Page 74: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW20HI |

Lab Code: Case No.: SAS No.: SDG No.: WST8-I

Matrix (soil/water): WATER Lab Sample ID: 1587945

Level (low/med): LOW . Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

13.7

1.3

135

1.4

26.8

,C

U

U

u

B

U

Q

w

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/33

AR303748 24

Page 75: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 __________INORGANIC ANALYSIS DATA SHEET _I

SW21HILab Name: Lancaster Laboratories Contract:

Lab Code: Case No.: SAS No.: SDG No.: WST8-I

Matrix (soil/water): WATER Lab Sample ID: 1587941

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumcobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

8.3

2.0

2610

1.4

20.5

C

U

U

uB

B

U

Q

w

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/33<j r—

Page 76: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - .CLPEPA SAMPLE NO.

1 ______INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW224I

Lab Code: Case No.: SAS No.: SDG No.: WSTS-I

Matrix (soil/water): WATER Lab Sample ID: 1587939

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

7.6

0.70

561

1.4

7.7

C

U

U

uB

B

U

B

Q

w

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

•Comments:

FORM I - IN . 7/38

26SR303750

Page 77: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW23HI

Lab Code: Case No.: SAS No.: SDG No.: WST3-

Matrix (soil/water): WATER Lab Sample ID: 1587940

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

8.5

0.70

423

1.4

12.5

C

U

U

uB

U

U

Q

w

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/83

flR30375l Z7

Page 78: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 _______INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW25HI \\

Lab Code: Case No.: SAS No.: SDG No.: WSTS-I

Matrix (soil/water): WATER Lab Sample ID: 1587957

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439^95-4"7439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

9.9

0.70

56.8

1.4

18.6

C

U

U

uB

U

U

Q

w

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/85

AR303752 *8

Page 79: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 ' ___.INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW26HI

Lab Code: Case No.: SAS No.: SDG No.: WST8-I

Matrix (soil/water): WATER Lab Sample ID: 1587959

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

6.0

14.9

1.8

521

1.4

21.6

C

U

U

B

U

Q

W

w

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/88

8R303753

Page 80: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 _________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SW27HI

Lab Code: Case No.: SAS No.: SDG No.: WST8-:

Matrix (soil/water): WATER Lab Sample ID: 1587958

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

_ _,.,.

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

8.7

0.70

74.3

1.4

10.8

C

U

U

uB

U

U

Q

W

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts;

Comments:

FORM I - IN 7/38

flR30375if 30

Page 81: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 __________IINORGANIC ANALYSIS DATA SHEET

REF1HILab Name: Lancaster Laboratories Contract:

Lab Code: Case No.: SAS No.: SDG No.: WST3-I

Matrix (soil/water): WATER Lab Sample ID: 1587956

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

7.9

0.70

98.1

1.4

11.1

C

U

U

uB

B

U

Q

W

M

NRPNRNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/83

BR303755 14

Page 82: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLP - .EPA SAMPLE NO.

INORGANIC ANALYSIS DATA SHEETHA02HI

Lab Name: Lancaster Laboratories Contract:

Lab Code: Case No.: SAS No.: SDG No.: WST8-I

Matrix (soil/water): WATER Lab Sample ID: 1587955

Level (low/med): LOW Date Received: 10/17/90

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-0 .7440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercury-NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

9.0

1.7

4.0

8.8

0.90

39.9

1.4

8.7

C

U

U

uB

B

U

B

Q

W

M

NRPNRNRNR'PNRPNRPNRFNRPNRNRNRFNRNRNRNRPNR

Color Before: Clarity Before: Texture:

Color After: Clarity After: Artifacts:

Comments:

FORM I - IN 7/88

HR3Q3756

Page 83: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

SDG-WST9

\.

rl.bu

8R303757

Page 84: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _______.

b Name: LANCASTER LABS___________ Contract:SD06H

Lab Code: LANCAS Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1587986

Sample wt/vol: 5.0 (g/mL) G__ . Lab File ID: B1587986

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 29 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3———————Chloromethane_74-83-9——————Bromomethane_75-01-4——————Vinyl Chloride,75-00-3——————Chloroethane75-09-2———————Methylene Chloride______67-64-1———————Acetone________________75-15-0———————Carbon Disulfide_____________75-35-4 ——————— 1,1-Dichloroethene________75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichlorpethene (total)67-66-3——————Chloroform____________________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6——————1,1,1-Trichloroethane___56-23-5—————Carbon Tetrachloride108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_______78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1, 2-Trichloroethane___71-43-2——————Benzene____________________10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform____________~108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane,108-88-3———————Toluene________________108-90-7——————Chlorobenzene__________100-41-4—————-Ethylbenzene__________100-42-5——————Styrene_______________________1330-20-7—————Xylene (total)_____________

141414147

1377777714771477777777714147777777

FORM I VOA AR303fl*8

UUUUUJUuuuuuuuuuuuuuuuuuuuuuuuuuuu

234

Page 85: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SD06H

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587986

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0358

Level: (low/med) LOW Date Received: 10/17/90% Moisture: not dec. 29 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/25/90

GPC Cleanup: (Y/N) N pH: 6.7 Dilution Factor: 1.000CONCENTRATION UNITS:

CA'S. NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

—— bis (2-Ethylhexyl) phthalate _ 47 J

FORM I SV-1 1/87

534AR303759

Page 86: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Name: LANCASTER LABS___________ Contract:SD07H

Lab Code: LANCAS __ Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1587987

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587987

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 52 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3——————Chloromethane_74-83-9——————Bromomethane_75-01-4——————vinyl Chloride,75-00-3———————Chloroethane__75-09-2———————Methylene Chloride_________67-64-1———————Acetone_________________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane________540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform________________107-06-2——————1,2-Dichloroethane__78-93-3——————2-Butanone_______71-55-6——————1,1,1-Trichloroethane,56-23-5——————Carbon Tetrachloride_J108-05-4——————Vinyl Acetate,7 5-27-4 ———————Bromodichloromethane_78-87-5———————1,2-Dichloropropane,10061-01-5———"—cis-l,3-Dichloropropene_79-01-6———————Trichloroethene_________124-48-1—————Dibromochloromethane__79-00-5——————1,1,2-Trichloroethane_71-43-2——————Benzene10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform108-10-1——————4-Methyl-2-Pentanone_591-78-6——————2-Hexanone__________________127-18-4——————Tetrachloroethene______79-34-5———————1, lr 2,2-Tetrachloroethane_108-88-3——————Toluene_____________~108-90-7——————Chlorobenzene_________100-41-4—————Ethylbenzene_________100-42-5—————Styrene______________1330-20-7—————Xylene (total)________

2121962188410101013010101810102110101042101010101021211010310210

UuuJuuuuuJuuuuuuuuuuuuuuuJuJu

FORM I VOAAR303760 1/87 Rev.

29

242

Page 87: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SD07H

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ____

Matrix: (soil/water) SOIL Lab Sample ID: 1587987

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0359

Level: (low/med) LOW Date Received: 10/17/90% Moisture: not dec. 52 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 10/25/90

GPC Cleanup: (Y/N) N pH: 6.3 Dilution Factor: 1.000CONCENTRATION UNITS:

CAS. NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

—— bis(2-Ethylhexyl) phthalate _ 430 J

FORM I SV-1 1/87 Rev.

flR30376l

Page 88: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SD07HRE

Lab Code: LANCAS Case No.: . SAS No.: . SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587987RE

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0360

Level: (low/med) LOW ' Date Received: 10/17/90% Moisture: not dec. 52 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/25/90

GPC Cleanup: (Y/N) N pH: 6.3 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ——— —— bis( 2 -Ethy Ihexyl ) phthalate _ 490 J

FORM I SV-1 1/87 Rev

AR303762

Page 89: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA .SHEET ____________

Lab Name: LANCASTER LABS__________ Contract:SD08H

Lab Code: LANCAS Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1597985

Sample wt/vol: , 5.0 (g/mL) G__ Lab File ID: B1587985

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 23 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3 —————74-83-9 —————75-01-4 —— ——75-00-3 —————75-09-2 —— ——67-64-1 —————75-15-0 —— ——75-35-4 —————75-34-3 —————540-59-0 — ——67-66-3 —————107-06-2 ————

«7 i c c _ a

F; f o T* P

108-05-4 ————75-27-4 —————/ O O / —3——————

10061-01-5 ——79-01-6 —————J_ f-i ~T T W -W

79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————i no — Q Q— "5 _____i no — Q n — ~7 ___— _100-41-4 ————100-42-5 ————1330-20-7 ———

—— Chloromethane—— Bromomethane—— Vinyl Chloride—— Chloroethane—— Methylene Chloride—— Acetone—— Carbon Disulfide—— 1, l-Dichloroethene—— 1, l-Dichloroethane—— 1,2-Dichloroethene (total) __—— Chloroform—— 1 , 2-Dichloroethane—— 2-Butanone—— 1 , 1 , l-Trichloroethane—— Carbon Tetrachloride—— Vinyl Acetate—— Bromodichloromethane—— 1,2-Dichloropropane—— cis-1 , 3-Dichloropropene—— Trichloroethene—— Dibromochloromethane—— 1 , 1 , 2 -Trichloroethane—— Benzene—— trans-1, 3-Dichloropropene ___—— Bromoform—— 4-Methyl-2-Pentanone—— 2-Hexanone

X t3 l_>_. dwllJ. wl. WC k»* 1C I LCS

—— 1 ,1,2, 2-Tetrachloroethane ___—— Toluene—— Chlorobenzene—— Ethylbenzene—— Styrene—— Xylene (total)

131313136

136662066

1366136661866666

13136666666

UUUuJuuuuuuuuuuuuuuuuuuuuuuuuuuu •

AR303763FORM I VOA 1/87 Rev.

Page 90: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SD08H

Lab Code: LANCAS Case No.: . SAS No.: . SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587985

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0304

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 23 dec. ____. Date Extracted: 10/21/90Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/24/90

GPC Cleanup: (Y/N) N pH: 6.8 Dilution Factor: i.ooo

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ——— —— bis(2-Ethylhexyl) phthalate _ 430 U

FORM I SV-1 1/87 Rev

53 iAR30376J*

Page 91: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS_________ Contract:SD09H

Lab Code: LANCAS Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL___ Lab Sample ID: B1587984

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587984

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 26 Date Analyzed: 10/26/90

Column: (pack/cap) PACK__ Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —— ——75-15-0 —— ——/ *j ~J — / "

75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 — ——/ o ^ - J J*7 1 C C £

C £ *. O C

108-05-4 ————75-27-4 —————

10061-01-5 ——79-01-6 —————124-48-1 —— —79-00-5 —————71-43-2 —————10061-02-6 ——•7K — TK_ "i — — —

108-10-1 ————591-78-6 — ——127-18-4 — —— -79-34-5 —————i no —a Q-.'J _____

100-41-4 -----100-42-5 -----1330-20-7 ———

—— Chloromethane—— Bromomethane—— Vinyl Chloride—— Chloroethane—— Methylene Chloride

—— Carbon Disulfide—— 1 , 1-Dichloroethene—— 1, 1-Dichloroethane—— 1,2-Dichloroetherie (total) __—— Chloroform—— 1 , 2-Dichloroethane—— 2 -Butanone—— 1, 1, 1-Trichloroethane—— Carbon Tetrachloride

V ...Aijr _» AWCS Ivd _><S

—— Bromodichloromethane—— 1, 2-Dichloropropane—— cis-1, 3-Dichloropropene—— Trichloroethene—— Dibromochloromethane—— 1, 1, 2-Trichloroethane—— Benzene—— trans-1, 3-Dichloropropene ___—— Bromoform—— 4 -Methyl-2 -Pentanone—— 2-Hexanone—— Tetrachloroethene—— 1 ,1,2, 2-Tetrachloroethane ___—— Toluene—— Chlorobenzene—— Ethylbenzene—— Styrene—— Xylene (total)

14141414121477737714771477737777714147777777

UUUU

UUUUJUuuuuuuuuJuuuuuuuuuuuuuu

2 OrAR303765FORM I VOA M 1 1 W V J V 1/87 Rev.

Page 92: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB . EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _____________

Lab Name: LANCASTER LABS Contract:SD09H

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: _____

Matrix: (soil/water) SOIL Lab Sample ID: 1587984

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0356

Level: (low/med) LOW Date Received: 10/17/90% Moisture: not dec. 26 dec. ______. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/25/90

GPC Cleanup: (Y/N) N pH: 6.7 Dilution Factor: 1.000CONCENTRATION UNITS:

CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

'117-81-7 ——— I™ -1 J—l--- bis(2-Ethylhexyl)phthalate _ 57 J

FORM I SV-1 1/87 Rev.

flR303766

Page 93: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LASS___________ Contract:SD10H

Lab Code: LANCAS Case No.: 276703 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1587981

Sample wt/vol: , 5.0 (g/mL) G__ Lab File ID: B1587981

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 38 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: l._o_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3———————Chloromethane_74-8 3-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene_________75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3———————Chloroform107-06-2 —————— 1,2-Dichloroethane,78-93-3———————2-Butanone71-55-6———————1,1, l-Trichloroethane_56-23-5———————Carbon Tetrachloride_^108-05-4——————Vinyl Acetate75-27-4——————Bromodichloromethane.,78-87-5————.——1,2-Dichloropropane_10061-01-5————cis-l,3-Dichloropropene_79-01-6——————Trichloroethene_______124-48-1——————Dibromochloromethane__79-00-5———————1,1,2-Trichloroethane__71-43-2——————Benzene10061-02-6————trans-l,3-Dichloropropene_75-25-2———————Bromoform_______108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene108-90-7——————Chlorobenzene100-41-4—————Ethylbenzene_100-42-5——————Styrene_______1330-20-7—————Xylene (total)

161616165248812158816581688838838816168888888

&R3Q3767

UUUJuuuuuJuuuuuuuuuuuuuu

FORM i VOA 1/87 Rev>

Page 94: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _________________ '

ab Name: LANCASTER LABS Contract:SD10H

Lab Code: LANCAS Case No.: ____. SAS No.: _____,. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: -1587981

Sample wt/vol: 30.0(g/mL) G . Lab File ID: >G0353

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 38 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/25/90 •

GPC Cleanup: (Y/N) N pH: 6.4 Dilution Factor: 1.000CONCENTRATION UNITS:

CAS-NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ——— —— bis(2--Ethylhexyl)phthalate _ J. o U J

FORM I SV-1 1/87 Rev.

AR303768

Page 95: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _______________

Lab Name: LANCASTER LABS__________ Contract:SD11H

Lab Code: LANCAS _ Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1537982

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587982

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 42 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride,67-64-1———————Acetone_________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform____________'107-06-2——————1, 2-Dichloroethane__78-93-3———————2-Butanone_________71-55-6———————1,1, l-Trichloroethane_56-23-5———————Carbon Tetrachloride_108-05-4——————Vinyl Acetate,75-27-4——————Bromodichloromethane____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene_79-01-6——————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6————trans-l,3-Dichloropropene_75-25-2———————Bromoform________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone___________127-18-4——————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene______________~108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100.-42-5——————Styrene______________1330-20-7—————Xylene (total)_________

17171717.9489912219910491799939999917179999999

UUUuuuu

uuJJuuuuuJuuuuuuuuuuuuuu

SR3Q3769 172FORM I VOA HIIUUU/O3 1/37 Rev.

Page 96: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS . Contract:SD11H

Lab Code: LANCAS Case No.: ____. SAS No.: . SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587982

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0354

Level: (low/med) LOW Date Received: 10/17/90% Moisture: not dec. 42 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 10/25/90

GPC Cleanup: (Y/N) N pH: 6.1 Dilution Factor: 1.000CONCENTRATION UNITS:

CAS- NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ——— —— bis(2-Ethylhexyl)phthalate _ 490 J

FORM I SV-1 1/87 Rev.

SR303770

Page 97: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS__________ Contract:SD11D

Lab Code: LANCAS Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL ' Lab Sample ID: B1587983

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587983

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 55 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4——————Vinyl Chloride,75-00-3——————Chloroethane75-09-2——————Methylene Chloride,67-64-1———————Acetone____________75-15-0——.————Carbon Disulfide________75-35-4————'———1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6——————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride108-05-4——————Vinyl Acetate_________75-2 7-4 ——————Bromodichloromethane j_______78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————-Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2-——————Benzene_______________10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane.108-88-3——————Toluene108-90-7——————Chlorobenzene_100-41-4——————Ethylbenzene_100-42-5——————Styrene_____1330-20-7—————Xylene (total)

2222222211271111791111224112211111131111111111222211111111111111

UUJJUuuJuuuuuJuuuuuuuuuuuuuu

FORM Ift 1 80 37 7 I 1/87 Rev,

Page 98: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Naroe: LANCASTER LABS Contract:SD11D

Lab Codes LANCAS Case No.: ____. SAS No.: ________. SDG No.: __Matrix: (soil/water) SOIL Lab Sample ID: 1587983Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0355

Level: (low/meet) LOW Data Received: 10/17/90% Moisture: not dec. 55 dec. . Date Extracted: 10/21/90Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 10/25/90

GPC Cleanup: (Y/N) N pH: 6.1 Dilution Factor: 1.000CONCENTRATION UNITS:

CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ————— bis (2-Ethylhexyl) phthalate _ 2900

FORM I SV-1 1/87 Rev.

520SR303772

Page 99: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA "SHEET ___

Lab Name: LANCASTER LABS__________ Contract:SD12H

-/a.Lab Code: LANCAS._. Case No.: 276708 SAS No.: _______ SDG No.: WST9

Matrix: (soil/water) SOIL . Lab Sample ID: Bl587980

Sample wt/vol: , 5.0 (g/mL) G__ Lab File ID: B1587980

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 53 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane__75-09-2———————Methylene Chloride______67-64-1———————Acetone_________________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3———————Chloroform_____________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6——————1, l, 1-Trichloroethane___56-23-5———————Carbon Tetrachloride108-05-4——————Vinyl Acetate___________75-27-4———————Bromodichloromethane____78-87-5———————1,2-Dichlorop-ropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——————Dibromochloromethane______79-00-5——————1,1,2-Trichloroethane___71-43-2———————Benzene_____________________10061-02-6——•——trans-l,3-Dichloropropene_75-25-2———————Bromoform108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane,108-88-3—————Toluene____________________~_108-90-7——————Chlorobenzene______'100-41-4—————Ethylbenzene_________100-42-5—————Styrene______________1330-20-7—————Xylene (total)_________

212121211125111142111121111121111111111111111111212111111111111111

UUUuuuuJJuuuuuuuuuuuuuuuuuuuuuuuu

FORM I VOA$R3Q3773 1/87 Rev.

Page 100: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Name: LANCASTER LABS Contract:SD12H '

rab Code: LANCAS Case No.: ______. SAS No.: ____. SDG No.: ___

Matrix: (soil/water) SOIL Lab Sample ID: 1587980

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0352

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 53 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/25/90

GPC'Cleanup: (Y/N) N pH: 5.9 Dilution Factor: 1.000CONCENTRATION UNITS:

CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

»

117-81-7 ——— —— bis(2-Ethylhexyl)phthalate _ 230 J

FORM I SV-1 1/87 Rev.

Page 101: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _______

Name: LANCASTER LABS Contract:SD13H

Lab Code: LANCAS Case No.': 276708 SAS No.: SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1537979

Sample wt/vol: 5.0 (g/mL) G Lab File ID: B1587979

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 58 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

74-87-3——————Chloromethane_74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride_________67-64-1———————Acetone_____________________75-15-0———————Carbon Disulfide________75-35-4—————-1,1-Dichloroethene______75-34-3 ——————— 1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform__________________107-06-2 —————— 1,2-Dichloroethane______78-93-3——————2-Butanone __ __71-55-6———————1,1, l-Trichloroethane_56-23-5———————Carbon Tetrachloride__108-05-4——————Vinyl Acetate,75-27-4———————Bromodichloromethane____78-87-5————-—1,2-Dichloropropane_______10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene____________124-48 -1 ———,——Dibromochloromethane____79-00-5————'——1,1,2-Trichloroethane___71-43-2——————Benzene___________________10061-02-6————trans-1,3-Dichloropropene,75-25-2——————Bromoform___________~108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2, 2-Tetrachloroethane_108-88-3——————Toluene_____;_________~108-90-7——————Chlorobenzene_____________100-41-4——————Ethylbenzene______________100-42-5——————Styrene_______________1330-20-7—————Xylene (total)________

242424242

881212127121219121224121212121212121212242412123

"12121212 124

FORM I VOA flR30u/7b i/87 Rev.

Page 102: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract: ____.

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587979

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0351Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 58 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/25/90GPC,Cleanup: (Y/N) N pH: 6,2 , Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or Ug/Kg) UG/KG Q

•-1_ • ,_— — bis(2-Ethylhexyl)phthalate _ 360 J

FORM I SV-1

AR303776

Page 103: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET ___

b Name: LANCASTER LABS_________ Contract:SD14H

Lab Code: LANCAS Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1587978

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587978

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 24 Date Analyzed: 10/26/90

Column: (pack/cap) PACK Dilution Factor: 1.0___

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride______67-64-1——————Acetone___________________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1, 2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2——————1,2-Dichloroethane_________78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane____56-23-5——•———Carbon Tetrachloride______108-05-4——————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene_79-01-6———————Trichloroethene_____________124-48-1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane___71-43-2———————Benzene________________10061-02-6————trans-l,3-Dichloropropene_75-25-2———————Bromoform______________________"_108-10-1——————4-Methyl-2-Pentanone_____591-78-6——————2-Hexanone___________127-18-4——————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene_____________________108-90-7——————Chlorobenzene_____________100-41-4—————Ethylbenzene__________100-42-5——————Styrene________________________1330-20-7—————Xylene (total)_____________

1313131361077777713771377777777713137777777

UUUUJJUUUUUUUUUUUUUUUuuuuU'uuuuuuuu

FORM I \&B303777 1/87 Rev.

Page 104: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SD14H

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587978Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0350

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 24 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/25/90

GPC Cleanup: (Y/N) N pH: 6.8 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

—— bis (2-Ethylhexyl) phthalate _ 54 J

FORM I SV-1

RR303778

Page 105: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET

rab Name: LANCASTER LABS__________ Contract:SD17H

Lab Code: LANCAS Case No.: 276703 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1587973

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: • B1587973

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 31 Date Analyzed: 10/24/90

Column: (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. ' COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3 — -—————Chloromethane_7 4-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane__75-09-2——————Methylene Chloride_________67-64-1——————Acetone______________75-15-0——————Carbon Disulfide___________75-35-4——————1,1-Dichloroethene________75-34-3———————1,1-Dichloroethane______540-59-0——————1, 2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2 —————— 1,2-Dichloroethane_______78-93-3——————2-Butanone ____71-55-6——•-----1,l,l-Trichloroethane_56-23-5——————Carbon Tetrachloride__108-05-4——————Vinyl Acetate________75-27-4 ——————Bromodichloromethane__78-87-5——————1,2-Dichloropropane___10061-01-5————cis-l,3-Dichloropropene,79-01-6———————Trichloroethene______124-48-1—•————Dibromochloromethane__79-00-5-:——————1,1,2-Trichloroethane__71-43-2———————Benzene10061-02-6————trans-1,3-Dichloropropene,75-25-2———————Bromoform108-iO-l——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene_____;______________108-90-7—————Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Xylene (total)____________

141414145777777714271477777777714147777777

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flR303779 -FORM I VOA 1/87 Rev.

Page 106: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DA'TA SHEET ______ >

Lab Name: LANCASTER LABS Contract:SD17H

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587973

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0305

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 31 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 10/24/90

GPC Cleanup: (Y/N) N pH: 6.9 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS. NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ——— —— bis (2-Ethylhexyl) phthalate _ 790

FORM I SV-1

6R303780

Page 107: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS_____________ Contract:SD18H

Lab Code: LANCAS._ Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1537972

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587972

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 48 Date Analyzed: 10/24/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

*

74-87-3 — — —74-83-9 — —— -75-01-4 —————75-00-3 —————/ O U;?— -"~ — "• — «••

67-64-1 —————75-15-0 —— ——75-35-4 ———— -75-34-3 —— ——540-59-0 -----67-66-3 —— ——107-06-2 ————

•-» -i er c? /r __

e? _- O T f

108-05-4 — ~-75-27-4 —————*7 O O *7 R — .

10061-01-5 ——79-01-6 —— ——124-48-1 —— ~79-00-5 —————71-43-2 —— ——10061-02-6 ——/ •_• f. _.»108-10-1 ————591-78-6 -----127-18-4 —— —79-34-5 —————1 nQ_Qa_ •)_—_—_

100-41-4 ————100-42-5 ————1330-20-7 ———

—— Chloromethane—— Bromomethane—— vinyl Chloride—— Chloroethane—— Methylene Chloride—— Acetone—— Carbon Disulfide-—— 1, 1-Dichloroethene—— 1, 1-Dichloroethane—— 1,2-Dichloroethene (total)—— Chloroform—— 1 , 2-Dichloroethane—— 2 -Butanone—— 1, 1, 1-Trichloroethane—— Carbon Tetrachloride

vinyj. Aceuctue—— Bromodichloromethane—— 1, 2-Dichloropropane—— cis-l,3-Dichl.oropropene

ii i_>nxOiastuene—— Dibromochloromethane—— 1 , 1 , 2-Trichloroethane—— Benzene—— trans-1 , 3 -Dichloropropene ___—— Bromoform—— 4 -Methyl-2 -Pentanone—— 2 -Hexanone—— Tetrachloroethene—— 1, 1,2,2-Tetrachloroethane ___—— Toluene—— Chlorobenzene—— Ethylbenzene

w w y die—— Xylene (total)

19191919316101010 '10101019101019101010101010101010191910101010101010

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FORM I VOA 1/8?

Page 108: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ____________._____

Lab Name: LANCASTER LABS Contract:SD18H

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.: ___

Matrix: (soil/water) SOIL Lab Sample ID: 1587972

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0308

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 48 dec. _____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 10/24/90

GPC Cleanup: (Y/N) N pH: 6.4 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7————— bis(2-Ethylhexyl)phthalate. 910

;7 Re^

flR303782

FORM I SV-1 1/87 Rev41 +—• f •4 /o

Page 109: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS____________ Contract:SD19H

Lab Code: LANCAS Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1587977

Sample wt/vol: 5.0 (g/mL) G__ ' Lab File ID: B1587977

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 30 Date Analyzed: 10/24/90

Column: (pack/cap) PACK Dilution Factor: 1.0____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane__75-09-2———————Methylene Chloride______67-64-1———————Acetone________________________75-15-0——————Carbon Disulfide___________75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform_______________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone_____________________71-55-6——————1,1,1-Trichloroethane______56-23-5———————Carbon Tetrachloride_____108-05-4—————Vinyl Acetate_____________75-27-4———————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene_79-01-6——————Trichloroethene________12 4-48-1—————Dibromochloromethane____79-00-5——————l, 1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform____________,108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_________________127-18-4——————Tetrachloroethene______79-34-5———————1/1/2,2-Tetrachloroethane_108-88-3——————Toluene______________ios-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene_______________100-42-5——————Styrene_______________1330-20-7—————Xylene (total)__________

1414141472477777714771477777777714147777777

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106,8_f?303783FORM I vOA'u u <-" u 1/87 Rev.

Page 110: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:Lab Code: LANCAS Case'No.: ____. SAS No.: ____. SDG No.: ___

Matrix: (soil/water) SOIL Lab Sample ID: 1587977

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0300

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 30 dec. ___. Date Extracted: 10/21/90Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 10/24/90

GPC Cleanup: (Y/N) N pH: 6.8 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ——— —— bis(2-Ethylhexyl)phthalate _ 470 U

FORM I SV-1 l/8 v

431AR3Q37814

Page 111: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

,ab Name: LANCASTER LABS__________ Contract:SD20H

Lab Code: LANCAS Case No..: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1587976RR

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587976RR

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 21 Date Analyzed: 10/25/90

Column: (pack/cap) PACK Dilution Factor: 1.0

. , CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

74-87-3———————Chloromethane_74-83-9———————Bromomethane__75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride____________67-64-1————————Acetone______________________________75-15-0———————Carbon Disulfide__________75-35-4———————1,1-Dichloroethene________75-34-3——————1,1-Dichloroethane_________540-59-0——————1,2-Dichloroethene (total)__67-66-3———————Chloroform_______107-06-2——————1, 2-Dichloroethane________78-93-3———————2-Butanone71-55-6———————1,1,1-Trichloroethane,56-23-5———•———Carbon Tetrachloride_108-05-4——————Vinyl Acetate,75-27-4———————Bromodichloromethane____78-87-5———————1,2-Dichloropropane_____10061-01-5—-——cis-1,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene______________10061-02-6————trans-1,3-Dichloropropene,75-25-2———————Bromoform_____________~108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone__________________127-18-4——————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene108-90-7——————Chlorobenzene_100-41-4—————Ethylbenzene_100-42-5—————Styrene_____1330-20-7—————Xylene (total)

1313131365666666

1366

13666666666

13136666-666

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~- 9SFORM o 1/87 Rev-

Page 112: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SD20H

Lab Code: LANCAS Case No.: . SAS No.: ___. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587976

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0307

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 21 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/24/90

GPC Cleanup: (Y/N) N pH: 6.8 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ——— —— bis (2-Ethylhexyl) phthalate _ 79 J

FORM I SV-1

4866R303786

Page 113: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

ib Name: LANCASTER LABS_________ Contract:SD21H

Lab Code: LANCAS Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: S1587971

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587971

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 24 Date Analyzed: 10/24/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3——————Chloromethane_74-83-9——————Bromomethane_75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2———————Methylene Chloride,67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4 ——————— 1,1-Dichloroethene_______75-34-3 ——————— 1,1-Dichloroethane_______540-59-0—————1,2-Dichloroethene (total).67-66-3———————Chloroform__________•107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone_________________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride108-05-4——————Vinyl Acetate______________75-27-4———————Bromodichloromethane____78-87-5———————1, 2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene______________10061-02-6————trans-l,3-Dichloropropene_75-25-2——————Bromoform____________________~_108-10-1——————4-Methyl-2-Pentanone_591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene______79-34-5 ——————— 1,1,2,2-Tetrachloroethane,108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene__________100-42-5——————Styrene_________________________1330-20-7—————Xylene (total)________

131313132

207777 .77

1377

1377777777713137777777

UUUUJ

UUUUUUUUUUUUUUUUUuuuuuuuuuuu

FORM i VOA QR3Q3787 1/87 Rev<

Page 114: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _________ ____

Lab Name: LANCASTER LABS Contract:SD21H

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587971

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0302

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 24 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/24/90

GPC Cleanup: (Y/N) N pH: 5.8 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7————— bis(2-Ethylhexyl)phthalate_ 69

FORM I SV-1 1/87 Rev

flR303788 47

Page 115: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS__________ Contract:SD22H

Lab Code: LANCAS Case No.: 276703 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: S1587968

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587968

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 38 pate Analyzed: 10/24/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3 —— ——74-83-9 —— ——75-01-4 —————75-00-3 —————

75-15-0 — — —75-35-4 —— ——75-34-3 —— ——540-59-0 —— ~67-66-3 —— ——107-06-2 ————

71-55-6 —— ——56-23-5 —————108-05-4 — ——75-27-4 —————"7 Q Q"7_K — — —

10061-01-5 ——79-01-6 —— ——124-48-1 —— —79-00-5 —— ——71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 — ——591-78-6 -----127-18-4 — ——79-34-5 —————

i n Q _ Q n_ *7 — — — — _100-41-4 -----100-42-5 -----1330-20-7 ———

—— Chloromethane—— Bromomethane—— Vinyl Chloride—— Chloroethane—— Methylene Chloride—— Acetone—— Carbon Disulfide—— 1, 1-Dichloroethene—— 1, 1-Dichloroethane—— 1,2-Dichloroethene (total) __—— Chloroform—— 1, 2-Dichloroethane—— 2 -Butanone—— 1, 1, 1-Trichloroethane—— Carbon Tetrachloride—— Vinyl Acetate—— Bromodichloromethane .—— 1,2-Dichloropropane—— cis-1, 3-Dichloropropene—— Trichloroethene—— Dibromochloromethane—— 1 , 1 , 2-Trichloroethane

Benzene—— trans-1 , 3-Dichloropropene ___— — • Br omo f o rm—— 4 -Methy 1 -2 -Pentanone—— 2 -Hexanone—— Tetrachloroethene—— 1 ,1,2, 2-Tetrachloroethane ___—— Toluene—— Chlorobenzene—— Ethylbenzene—— Styrene—— Xylene (total)

161616164

43888888168816888888888161688888BB

UUUuJuuuuuuuuuuuuuuuuuuuuuuuuuuuu

38FORM I VOA SR303789 1/37 Rev.

Page 116: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:

Lab Code: LANCAS Case No.: ____. SAS No.: ____. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587968

Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0253

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 38 dec. ____. Date Extracted: 10/21/90

Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 10/24/90GPC Cleanup: (Y/N) N pH: 6.3 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117- O J..-7 ——— —— bis(2--Ethylhexyl) phthalate _ 540 U

FORM I SV-1 1/87

43:AR303790

Page 117: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NO.•VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER .LABS___________ Contract:SD22D

Lab Code: LANCAS Case No.: 276708 SAS No.: ______ SDG No.: W5T9

Matrix: (soil/water) SOIL Lab Sample ID: B1587969

Sample wt/vol: 5.0 (g/mL) G__ Lab File ID: B1587969

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 30 Date Analyzed: 1.0/24/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3——————Chlororaethane__74-83 -9 ——————Bromomethane_75-01-4———————Vinyl Chloride,75-00-3——————Chloroethane75-09-2———————Methylene Chloride__________67-64-1———————Acetone________________________75-15-0———————Carbon Disulfide____________75-3 5-4 ---:—————1,1-Dichloroethene___________75-34-3———————1, 1-Dichloroethane^________540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform____________107-06-2——————1,2-Dichloroethane _____78-93-3——————2-Butanone_________________71-55-6——————1,1,1-Trichloroethane_____56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate_____________75-27-4———————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane,10061-01-5————cis-1,3-Dichloropropene79-01-6———————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene_____________10061-02-6————trans-l,3-Dichloropropene_75-25-2————•——Bromoform________________~_108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone127-18-4——————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane,108-88-3——————Toluene______;_________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene__________________100-42-5——————Styrene_____________________1330-20-7—————Xylene (total)________

141414147

37,77777714771477777777714147777777

UUUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

~~ 45FORM I VOAQR3Q379 I 1/87 Rev.

Page 118: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract:SD22D

Lab Code: LANCAS Case No.: _____• SAS No.: ____. SDG No.:

Matrix: (soil/water) SOIL Lab Sample ID: 1587969

Sample wt/vol: 30.0(g/mL) G . Lab File ID: >G0254

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 30 dec. ____. Date Extracted: 10/21/90Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 10/24/90

GPC Cleanup: (Y/N) N pH: 6.3 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS.NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

—— bis(2-Ethylhexyl)phthalate _ 180 J

7 Rev,FORM I SV-1 1/87

AR303792 4BJ

Page 119: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS_________ Contract:SD23H

Lab Code: LANCAS^ Case No.: 276708 SAS No.: ______ SDG No.: WST9

Matrix: (soil/water) SOIL Lab Sample ID: B1587970

Sample wt/vol: , 5.0 (g/mL) G__ ' Lab File ID: B1537970

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 33 Date Analyzed: 10/24/90

Column: (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG

74-87-3——————Chloromethane_74-83-9——————Bromomethane_75-01-4———————Vinyl Chloride,75-00-3———————Chloroethane75-09-2——————Methylene Chloride,67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide____________75-35-4———————1,1-Dichloroethene__________75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform___________________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone________________71-55-6——————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride____ios-05-4——————Vinyl Acetate75-27-4———————Bromodichloromethane____78-87-5 ——————— 1, 2-Dichloropropane______10061-01-5————cis-1,3-Dichloropropene__79-01-6——————Trichloroethene____________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene______________10061-02-6——>—trans-l,3-Dichloropropene_75-25-2——————Bromoform_____________________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene__________79-34-5———————1,1,2, 2-Tetrachloroethane_108-88-3——————Toluene___________ ___108-90-7——————Chlorobenzene_100-41-4—————Ethylbenzene_100-42-5—————Styrene_______1330-20-7—————Xylene (total)

15151515451677777715771577777777715157777777

UUUUUUUUUUUuuuuuuuuuuuuuuuuU'

SR303793 1/87Rev

Page 120: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: LANCASTER LABS Contract: ___ .Lab Code: LANCAS Case No.: ______. SAS No.: ____. SDG No.: ___

Matrix: (soil/water) SOIL Lab Sample ID: 1587970Sample wt/vol: 30.0(g/mL) G Lab File ID: >G0303

Level: (low/med) LOW Date Received: 10/17/90

% Moisture: not dec. 33 dec. ____. Date Extracted: 10/21/90Extraction: (SepF/Cont/Sonc) SONG Date Analyzed: 10/24/90

GPC Cleanup: (Y/N) N pH: 6.2 Dilution Factor: 1.000

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

117-81-7 ——— —— bis (2-Ethylhexyl) phthalate _ 140 J

FORM I SV-1 1/8Ot ' * f4ot

Page 121: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

INORGANIC ANALYSIS DATA SHEETSD06H1

Lab Name: Lancaster Laboratories Contract:

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587986

Level (low/med): LOW Date Received: 10/17/90

% Solids: 71.0

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440 23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.64.4

0.73

39.1

13.3

6.0

1440

0.30

94.00.16

C

UB

B

U

Q

NN

N*

N*

*

*

N

E

M -

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before,: GROWN Clarity Before: Texture: COARSE

Color After: GREEN Clarity After: Artifacts: YES

Comments:-

flR303795 7/33

Page 122: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLP p.,;*""•' EPA SAMPLE NO

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD07HI

- 7

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587987

Level (low/med): LOW Date Received: 10/17/90

% Solids: 48.3

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMa ernes iumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

5.51.8

0.46

994

426

.4300

395

0.57

2370.25

C

BB

U

B

U

Q

NN

N*

N*

*

*

N

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BLACK Clarity Before: Texture: COARSE

Color After: GREEN Clarity After: Artifacts: YESComments:

14

Page 123: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLP /ip.,.,7(L'E'ft& SAMPLE NO

1 /'*#INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD08HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1537985

Level (low/med): LOW Date Received: 10/17/90

% Solids: 76.8

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-4''7440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.56.9

0.28

50.4

32.9

341

1060

0.45

1030.16

C

U

u

B

U

Q

NN

N*

N*

*

*

NS

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: MEDIUM

Color After: YELLOW Clarity After: Artifacts: YES

Comments:

15FORM I - IN " 7/83

AR303797

Page 124: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE MC

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD09HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587984

Level (low/med): LOW Date Received: 10/17/90

% Solids: 73.9

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMacrnesiumMancraneseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.61.2

0.30

45.3

52.2

128

335

0.28•

84.30.17

C

UB

U

B

U

Q

NN

N*

N*

*

*

NW

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: GRAY Clarity Before: Texture: FINE

Color After: GREEN Clarity After: Artifacts: YES

Comments:

FORM I - IK r, O n O 1 Q Q 7/3C8R303798

Page 125: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NC

1 ___________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD10HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-

Matrix (soil/water): SOIL Lab Sample ID: 1587981

Level (low/med): LOW Date Received: 10/17/90

% Solids: 61.9

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

2.73.5

0.66

200

259

987

1300

0.19•

2970.20

C

BB

B•

U

Q

NN

N*

N*

*

*

N

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: COASE

Color After: GREEN Clarity After: Artifacts: YES

Comments:

FORHI-1^303799 " 7/3i

Page 126: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLP /7V.

1 '••-INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD11HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587982

Level (low/med): LOW Date Received: 10/17/90

% Solids: 58.5

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

4.35.0

0.60

191

326

999

657

0.34

2390.21

C

BB

B

U

Q

NN

N*

N*

*

*

N

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: MEDIUM

Color After: GREEN Clarity After: Artifacts: YES

Comments:

PORMI-IlIaR303800.: 13 7/3£

Page 127: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO,

1 _________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD11DI

-//£>Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587933

Level (low/med): LOW Date Received: 10/17/90

% Solids: 45.0

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercury-NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

4.49.7

0.49

291

373

1150

984

0.63

*

3670.28

C

B

U

B

U

Q

NN

N*

N*

*

*

MN

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: MEDIUM

Color After: GREEN Clarity After: Artifacts: YES

Comments:

FORM I - IN A^««rtT- 7/33flR30380l

Page 128: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NC

1 __________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD12HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587980

Level (low/med): LOW Date Received: 10/17/90

% Solids: 46.8

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

3.53.2

0.64

282

307

1520

506

0.65

3270.26

C

BB

B

B

U

Q

NN

N*

N*

*

*

N

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: MEDIUM

Color After: GREEN Clarity After: Artifacts: YES

Comments:

FORH '' * 7/3S

Page 129: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NC

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD13HI

Lab Code: Case No.: SAS No..: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587979

Level (low/med)': LOW Date Received: 10/17/90

% Solids: 41.9

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

2.82.9

0.54

168

292

146

1340

0.63

4090.28

C

UB

U

B

U

Q

NN

N*

N*

*

*

NS

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: GRAY Clarity Before: Texture: MEDIUM

Color After: GREEN Clarity After: Artifacts: YES

Comments:

217/83

Page 130: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NC

1 __________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD14HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587973

Level (low/med): LOW Date Received: 10/17/90

% Solids: 75.6

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManqaneseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.54.3

0.62

27.0

65.2

91.6

2290

0.16

3830.16

C

U

B

U

Q

NN

N*

N*

*

*

N

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: COARSE

Color After: GREEN Clarity After: Artifacts: YES

Comments:

22FORM I - IN '_«, 7/83&R30380U

Page 131: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NC

1 __________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD17HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1537973

Level (low/med): LOW Date Received: 10/17/90

% Solids: 68.6

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimony^ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.75.9

0.32

22.4

38.2

87.8

925

0.50

2940.19

C

U

U

U

Q

NN

N*

N*

*

*

NS

E

M

NRPFNR-NRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: FINE

Color After: GREEN Clarity After: Artifacts: YES

Comments:

; 23FORM I - IN nnnnnr. 7/83AR303805

Page 132: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NC

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD18HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587972

Level (low/med): LOW Date Received: 10/17/90

% Solids: 51.8

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

2.25.6

0.68

14.6

34.7

92.2

809

0.53

3230.23

C

UB

B

Q

NN

N*

N*

*

*

MN

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: FINE

Color After: GREEN Clarity After: Artifacts: YES

Comments:

FORM i - : 7 / 3 8

Page 133: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NC

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD19HI

Lab Code: - .Case No.: SAS No.: SDG No.: WST3-:

Matrix (soil/water): SOIL Lab Sample ID: 1587977

Level (low/med): LOW Date Received: 10/17/90

% Solids: 70.3

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.72.5

0.32

34.9

80.3

16.8

211

1.1

41.80.16

C

UU

u

u

Q

NNW

N*

N*

*

*

NS

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: MEDIUM

Color After: GREEN Clarity After: Artifacts: YES

Comments:

FOSM1-INAR303807 ,~ 25

Page 134: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO

1INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD20HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-

Matrix (soil/water): SOIL Lab Sample ID: 1587976

Level (low/med): LOW Date Received: 10/17/90

% Solids: 78.9

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimony^ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.56.3

0.23

23.6

34.2

26.9

704

0.36•

79.50.16

C

U

U

B

U

Q

NN

N*

N*

*

*

MN

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: COARSE

Color After: YELLOW Clarity After: Artifacts: YES

Comments:

26FORM I - IN flR3Q3808 " 7/88

Page 135: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

\

U.S. EPA - CLPEPA SAMPLE NO

1 _________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD21HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1537971

Level (low/med): LOW Date Received: 10/17/90

% Solids: 75.7

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManqaneseMercury-NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.68.2

0.52

22.2

13.0

16.2

2820

0.52*

81.10.20

C

UB

U

Q

NN

N*

N*

W*

*

N

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: COARSE

Color After: YELLOW Clarity After: Artifacts: YES

Comments:

;,. 27FORM I - IN flR3Q3809

Page 136: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO

1 __INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD22HI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587963

Level (low/med): LOW Date Received: 10/17/90

% Solids: 61.7

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-1.7439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMaqnesiumManqaneseMercuryNickelPotassiumSeleniumSilverSodiumThallium •VanadiumZincCyanide

Concentration

1.93.4

0.36

32.2

10.2

9.5

518

0.22

57.00.20

C

UB

U

B

U

Q

NN

N*

N*

*

*

N

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: GRAY Clarity Before: Texture: FINE

Color After: GREEN Clarity After: Artifacts: YES

Comments:

23FORM I - IN -" 7/33

AR303810

Page 137: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NO.

1 __________INORGANIC ANALYSIS DATA SHEET

Lab Name: Lancaster Laboratories Contract:SD22DI

Lab Code: Case No.: SAS No.: SDG No.: WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1587969

Level (low/med): LOW Date Received: 10/17/90

% Solids: 69.6

Concentration Units (ug/L or mq/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMaqnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.75.5

0.32

30.3

12.3

21.2

542

0.32

51.20.17

C

U

U

B

U

Q

NN

N*

N*

*

*

N

E

M

NRPFNRNRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: COARSE

Color After: GREEN Clarity After: Artifacts: YES

Comments:

28FOEMI-INflR3038ll 7/83

Page 138: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

U.S. EPA - CLPEPA SAMPLE NC

1 __________INORGANIC ANALYSIS DATA SHEET

SD23HILab Name: Lancaster Laboratories Contract:

Lab Code: Case No.: SAS No.: SDG No.: .WST9-:

Matrix (soil/water): SOIL Lab Sample ID: 1537970

Level (low/med): LOW Date Received: 10/17/90

% Solids: 66.9

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManqaneseMercury-NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

1.78.1

0.33

20.5

13.0

11.4

2080

0.47

91.10.17

C

U

U

B

Q

NN

N*

N*

*

*

N

E

M

NRPFN3NRPNRPNRPNRFNRPNRNRNRFNRNRNRNRPAS

Color Before: BROWN Clarity Before: Texture: COARSE

Color After: YELLOW Clarity After: Artifacts: YESComments:

FORM I - IN .30 7/33flR303812

Page 139: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

Lancaster Laboratories,,ttl-ftlUfaiaRh-.i-3.icaaiHr.rai 17601-599* 1717)656-2301

LLI Saaple No. SV 1587968Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-22 Grab Soil Sample Time Collected 0830Hunterstovn Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OP

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 5,900. mg/kg 50. 013807500Cyanide, Total • <0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 5.9 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture , 38.3 Z by vt. 0.1 135301200pH " 6.34 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.The pH of the method blank for samples 1587968-1587973 vas 6.68.

Antimony < 5. mg/kg 5. 164401400"-•dmium < 0.5 mg/kg 0.5 164901400

20. mg/kg 1. 165101400per 6. mg/kg 2. 165301400ganese 319. mg/kg 1. 165801400

Zinc 35. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

W»*M .* IAU4

«oniiuEQperganes

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 < Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation T.mnrhv <? nrxst-Hvk R A ""~~Of Symbols And Abbreviations And limotny b. UOStdyk, B.A.__ Our Standard Terms And Conditions Manager GC/MS

,ler,ber Ar-errcar Ccutx:,, _f ^ "' fl R 3 0 3 8 i 3noeoeraert Lacoratones. ire ^^. . _ . H l « v / v - « w ^ » * i > - '

Page 140: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

SIS REPORT

Lancaster Laboratories m» „,»,„LLI Sample No. SW 1587968

Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-22 Grab Soil Sample Time Collected 0830Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 9,600. mg/kg 80. 013840000Cyanide, Total ' < 0.2 mg/kg 0.2 023740000Arsenic (furnace method) < 8. mg/kg 8. 114540000Lead (furnace method) 9.5 mg/kg 0.8 115540000Selenium (furnace method) < 0.8 mg/kg : 0.8 116440000TCL Volatiles (Soil) attached 117840000Moisture *AS RECEIVED* 38.3 % by wt. 0.1 135340000Antimony < 8. mg/kg 8. 164440000Cadmium . < 0.8 mg/kg 0.8 164940000Chromium 32. mg/kg 2. 165140000'Copper 10. mg/kg 3. 165340000Manganese 518. mg/kg 2. '165840000Zinc 57. mg/kg 3. 167240000

•5(2-ethylhexyl)phthalate < 530. ug/kg 530. ' 900140000

i COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

>rx Questions? Contact Environmental Respecrfullv Submittedr.rnerra, Client Services at (717) 656-2301 . Lanca- .ooratories, Inc.

:es<ir*_~ ~ ~ Revii .d Approved by:

See Reverse Side For Explanation Timoti Oo«?tdvk B AOf Symbols And Abbreviations And limoUi, ... UOStayK, B.A. -.-Our Standard Terms And Conditions Manager GC/MS ^O

Merger Arnencar Council of>oecercept Ljboratcr «?s 'nc RR3038U

Page 141: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

/: f\_______' _^ ANALYSIS REPORT

Lancaster Laboratories m,m1717)656-2301

LLI Sample No. SV 1587969Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90'Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-22D Grab Soil Sample Time Collected 0830Hunterstovn Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 4,300. mg/kg 50. 013807500Cyanide, Total ' <0.1 mg/kg 0.1 023704000Arsenic (furnace method) 4. mg/kg 1. 114504000Lead (furnace method) 14.7 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture . 30.4 % by wt. 0.1 135301200pH 6.31 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400•romium 21. mg/kg 1. 165101400^ per 9. mg/kg 2. 165301400WBganese 377. mg/kg 1. 165801400.Zinc . 36. mg/kg 2. 167201400

Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timothv S Oo«.tdvl. R AOf Symbols And Abbreviations And limotny b. UOStayK, B.A.___ Our Standard Terms And Conditions Manager #W Wp O Q I C

Vtemcer American CCUTOI 3f ' _§ST' . ' HltOUwOlV'indecenaent Latxiraiones. inc

Page 142: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster Laboratories,_raLLI Sample No. SU 1587969

Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-22D Grab Soil Sample Time Collected 0830Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 6,100. mg/kg 70. 013840000Cyanide, Total < 0.1 mg/kg 0.1 023740000Arsenic (furnace method) 5. mg/kg 1. 114540000Lead (furnace method) 21.2 mg/kg 0.7 115540000Selenium (furnace method) , < 0.7 mg/kg 0.7 116440000TCL Volatiles'(Soil) attached 117840000Moisture *AS RECEIVED* 30.4 % by wt. 0.1 135340000Antimony < 7. mg/kg 7. 164440000Cadmium < 0.7 mg/kg 0.7 . 164940000Chromium . 30. mg/kg 1. 165140000Copper 12. mg/kg 3. 165340000Manganese 542. mg/kg 1. 165840000•"tic 51. .mg/kg 3. 167240000

(2-ethylhexyl)phthalate < 470. ' ug/kg 470. 900140000

1 COPY TO Paul C. Rizzo Associates - ATTN: Mr. Ken Bird1 COPY TO Data Package Group

.r=ar Associate-or Questions? Contact Environmental Respectfully Submittedjo-.4cs-wt.Mr Client Services at (717) 656-2301 Lancaster Laboratories, Inc.

i 3.cic_i_ai A Ervirormeriai _ . .:_stip_ Reviewed and Approved by:

Memeer Ar-vcar Councilindependent .-sooratcres sn

See Reverse Side For Explanation Timothv S Oostdvk B AOf Symbols And Abbreviations And limotny b. UOStdyK, B.A.Our Standard Terms And Conditions Manager GC/HSp O n Q Q I C

Page 143: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

+12LANALYSIS REPORT

Lancaster"Laboratories'«»«„«.mm !•*••! flili. I ii inlrr PIT 1TT-1T ITIf .717} 8»-23ft1

III Saaple No. SV 1587970Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-23 Grab Soil Sample Time Collected 0840Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 7,400. mg/kg 50. 013807500Cyanide, Total < 0.1 mg/kg 0.1 023704000Arsenic (furnace method) 5. rag/kg 1. 114504000Lead (furnace method) 7.6 mg/kg 0.5 115504000Selenium (furnace method) . < 0.5 mg/kg 0.5 116404000TCL Volatiles°{Soil) attached 117827000Moisture 33.1 %bywt. 0.1 135301200pH 6.21 0.01 144101000

Note:The pH was performed on a 1:1 .slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400< 0.5 mg/kg 0.5 '16490140014. mg/kg 1. 1651014009. mg/kg 2. 165301400

ganese - 1,390. mg/kg 1. 165801400Zinc ' 61. mg/kg 2. 167201400Bi's(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Memoer American Council _lirdeswoenj Lacoratcc'es. Ire

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Tlmothv <? f)o<-:r..vk R AOf Symbols And Abbreviations And iimotny b. UOStdyk, B.A. -><iOur Standard Terms And Conditions Manager GC/MSft D "^ H 3 ft j 7

Page 144: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster Laboratories Kamma.Hi,li<i iilPtm.Lancprter.F* l76Ot-Saate ffTT>n»llHI

LLI Sa»ple Mo. SW 1587970Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-23 Grab Soil Sample Time Collected 0840Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 11,000. mg/kg 70. 013840000Cyanide, Total < 0.1 mg/kg 0.1 023740000Arsenic (furnace method) 8. mg/kg 1. 114540000Lead (furnace method) 11.4 mg/kg 0.7 115540000Selenium (furnace method) < 0.7 mg/kg 0.7 116440000TCL Volatiles (Soil) attached 117840000Moisture *AS RECEIVED* 33.1 % by wt. 0.1' 135340000Antimony < 7. mg/kg 7. 164440000Cadmium < 0.7 mg/kg 0.7 164940000Chromium 20. mg/kg 1. 165140000Copper 13. mg/kg 3. 165340000Manganese 2,080. mg/kg 1. 165840000?inc 91. mg/kg 3. 167240000

;(2-ethylhexyl)phthalate < 490. ug/kg 490. 900140000

1 COPY TO ' Paul C. Rizzo Associates • ATTN: Mr. Ken Bird1 COPY TO Data Package Group

:,..Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.

e«:s.",si,p. Reviewed and Approved by:See Reverse Side For Explanation _. , ., _ , . _ AOf Symbols And Abbreviations And Timothy S. Oostdyk, B.A.

Amercar Cct.ncii o'Dorarcnes ;nc

Our Standard Terms And Conditions Manager GC/M^ Q 3 8 O 30

Page 145: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

Lancaster Laboratories2423r*n»HbtendRke,Lancaster.FK 17601-5984 (717)656-2301

LLI Sample No. SW 1587971Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-21 Grab Soil Sample Time Collected 0925Hunterstown Road Site . P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 6,000. mg/kg 50. 013807500Cyanide, Total 0.2 mg/kg 0.1 023704000Arsenic (furnace method) < 10. mg/kg 10. 114504000Lead (furnace method) 12.2 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture ' 24.3 X b y v t . 0.1 135301200pfl 5.77 • 0.01 144101000

Note:The pH was performed on a 1:1 .slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400Chromium 17. mg/kg 1. 165101400

>per 10. mg/kg 2. ' 1653014002,130. mg/kg . 1. 165801400

61. mg/kg . 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ' ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation iMm/.t-.v., c nnc-t-AM], n AOf Symbols And Abbreviations And Timothy S. Oostdyk, B.A. ^Our Standard Terms And Conditions Manager GC/MS *-*-*•

Vte-"b_f American Council ofinoeoenaent uaooratones !nc flR3038!9

Page 146: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

'*.e-ANALYSIS REPORT

LancasterLabomto,Tvnes-(7t7)fl66-23Q1

LLI Sample No. SW 1587971Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 • Discard Date 11/23/90

Collected 10/16/90 by CVSD-21 Grab Soil Sample Time Collected 0925Hunterstown Road Site P.O. ' ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 8,000. mg/kg 70. 013840000Cyanide, Total 0.3 mg/kg 0.1 023740000Arsenic (furnace method) < 10. mg/kg 10. 114540000Lead (furnace method) 16.2 mg/kg 0.7 115540000Selenium (furnace method) < 0.7 mg/kg 0,7 116440000TCL Volatiles (Soil) attached 117840000Moisture *AS RECEIVED* 24.3 % by wt. 0.1 135340000Antimony . < 7. mg/kg 7. 164440000Cadmium < 0.7 mg/kg 0.7 164940000Chromium 22. mg/kg 1. 165140000Copper 13. mg/kg 3. 165340000Manganese 2,820. mg/kg 1. 165840000Zinc 81. mg/kg 3. 167240000's(2-ethylhexyl)phthalate < 440. ug/kg 440. 900140000

j. COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

..arAssoc.awr.cr Questions? Contact Environmental Respectfully Submittedclient Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved by:

See Reverse Side For Explanation IMmnrhv •? rincrHvlr R AOf Symbols And Abbreviations And Timothy S. Oostdyk, B.A.Our Standard Terms And Conditions Manager GC/MS

pcecencenr

Page 147: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYS

Lancaster Laboratories K,m(7t7>668-2301

LLI Sample No. SV 1587972Paul C. Rizzo Associates-.PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-18 Grab Soil Sample • Time Collected 1000Hunterstown Road Site . P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 14,000. mg/kg 50. 013807500Cyanide, Total 0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 47.7 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture 48.2 % by wt. 0.1 135301200pfl 6.39 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gins, of sample and 50 ml.

• of deionized water) after being tumbled for one hour.Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400

-omium 8. • mg/kg 1. 165101400«er ' • 18. mg/kg 2. 165301400

anese 419. • mg/kg 1. 165801400• . 167. mg/kg 2. 167201400

Bis(2-ethylhexyl)phthalate 470. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

Member American Council ofindeoendent Laooratones. tnc.

See Reverse Side For Explanation Timofhv <. nn-srHvl^ R AOf Symbols And Abbreviations And iimotny S>. UOStdytC, B.A.Our Standard Terms And Conditions Manager GC/MS 33

AR30382I

Page 148: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

.NALYSIS REPORT

Lancaster'Laboratories,....,.,,.,|Zt7) 66 2301

LLI Sample No. SW 1587972Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-18 Grab Soil Sample Time Collected 1000Hunterstown Road Site ' P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 27,000. mg/kg , 100. 013840000Cyanide, Total 0.2 mg/kg 0.2 023740000Arsenic (furnace method) < 10. mg/kg 10. 114540000Lead (furnace method) 92.2 mg/kg 1.0 115540000Selenium (furnace method) < 1.0 mg/kg 1.0 116440000TCL Volatiles (Soil) attached 117840000Moisture *AS-RECEIVED* 48.2 % by wt. 0.1 135340000Antimony " < 10. mg/kg 10. 164440000Cadmium < 1.0 mg/kg 1.0 164940000Chromium 15. mg/kg 2. 165140000Copper 35. mg/kg 4. 165340000Manganese 809. mg/kg 2. 165840000Zinc 323. mg/kg 4. 167240000"<s(2-ethylhexyl)phthalate 910. ug/kg 640. 900140000

. COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group •

. . . - c * Questions? Contact Environmental Respectfully Submitted*c:-Mtat,or Client Services at (717) 656-2301 Lancaster Laboratories, Inc.

~ " '•sws:t:*.i.rg Reviewed and Approved by:

See Reverse Side For Explanation Timothv S Oostdvk B AOf Symbols And Abbreviations And limotny b. UOStayK., B.A.Our Standard Terms Arid Conditions Manager GC/MS

•/e-cer Ar ar r-. ,,.,•r»c«ro«ri LMoratflf.es ire

Page 149: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

____ IS REPORT

ancasterLaboratories, ^Np.iliaiidPiie.LancaatBr.Rrl 17601-599* .7t7)«58-a3_k* .

LLI Sample No. SV 1587973Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-17 Unspiked Grab Soil Sample . Time Collected 1015Bunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 11,000. mg/kg 50. 013807500Cyanide, Total 0.1 mg/kg 0.1 023704000Arsenic (furnace method) 4. mg/kg 1. 114504000Lead (furnace method) 60.3 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture - 31.4 % by wt. 0.1 135301.200pH 6.85 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400

15. mg/kg 1. 16510140026. mg/kg 2. 165301400634. mg/kg 1. 165801400

Zinc 201. mg/kg 2. 167201400Bis('2-ethylhexyl)phthalate 550. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timnthv S Onsrrlvk R AOf Symbols And Abbreviations And iimotny b. UOS tayK, B.A.___ Our Standard Terms And Conditions Manager GC/MS flP3Q3823

American Council -' ' ^"" H I Yincecenaent LaDoraiones i

Page 150: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

iNALYSIS REPORT

Lancaster Laboratories ^.IBM !!•••• i ri.. t in 1111,11 rn mm nni ffTOfiee-asn

LLI Saaple No. SW 1587973Paul C. Rizzo Associates-PA ' Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/-16/90 by CVSD-17 Unspiked Grab Soil Sample Time Collected 1015Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 16,000. mg/kg 70. 013840000Cyanide, Total ' 0.1 mg/kg 0.1 023740000Arsenic (furnace method) 6. mg/kg 1. 114540000Lead (furnace method) 87.8 mg/kg 0.7 115540000Selenium (furnace method) < 0.7 mg/kg 0.7 116440000TCL Volatiles (Soil) attached 117840000Moisture *AS RECEIVED* 31.4 % by wt. 0.1 135340000Antimony < 7. mg/kg 7. 164440000Cadmium < 0.7 mg/kg 0.7 164940000Chromium 22. mg/kg 1. 165140000'Copper 38. mg/kg 3. 165340000Manganese 925. mg/kg 1. '165840000Zinc 294. mg/kg 3. 167240000•5(2-ethylhexyl)phthalate 800. ug/kg 480. • 900140000

i COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.<-rti .,cai Bicioc.K.31 i Erwcrirental ' , .>«eias of testing Reviewed and Approved by:

See Reverse Side For Explanation IMmothv S Ooqtrlvk R AOf Symbols And Abbreviations And iimotny b. UOStayK, B.A._ _ ^ Our Standard Terms And Conditions Manager GC/MS

Member Amer-can Ccc-nc1' 3f.pcjeoencent Laboratcr es inc

Page 151: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

ncasterLaboratories ,„,„,«,.IJIif.HM-.iii,> P** Lancaster, E* 17G01-59fl» (717) 6SB-23Bt

LLI Sample No. SV 1587976Paul C. Rizzo Associates-PA ' Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-20 Grab Soil Sample Time Collected 1150Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic-Carbon 5,000. mg/kg 50. 013807500Cyanide, Total < 0.1 mg/kg 0.1 023704000Arsenic (furnace method) 5. mg/kg 1. 114504000Lead (furnace method) 21.2 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture 21.1 £byw t . 0.1 135301200pH 6.81 0.01 144101000

Note:The pfl was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400

romiujn 19. mg/kg 1. 165101400per 27. mg/kg 2. 165301400ganese 556. mg/kg 1. 165801400

Zinc 63. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Memcer American Council of'.raecenaen Uooratones ine

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation T.mnrhv «. nnorrlvl.- U iOf Symbols And Abbreviations And iimotny b. UOStdyfc, B.A.Our Standard Terms And Conditions Manager GC/HS D <J f\ Q g 9 5

Page 152: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

Lancaster LaboratoriesINUiriPOHArE.D

LLI Sample No. SU 1587976Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 . Discard Date 11/23/90

Collected 10/16/90 by CVSD-20 Grab Soil Sample Time Collected 1150Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY UT. BASIS QUANTITATION LAB CODETotal Organic Carbon 6,400. mg/kg 60. 013840000Cyanide, Total < 0.1 mg/kg 0.1 023740000Arsenic (furnace method) 7. mg/kg 1. 114501500Lead (furnace method) 26.9 mg/kg 0.6 115501500Selenium (furnace method) < 0.6 mg/kg 0.6 116401500TCL Volatiles (Soil) . attached ' 117827000Moisture *AS RECEIVED* 21.1 % by wt. • 0.1 135327000Antimony < 6. mg/kg 6. 164427000Cadmium < 0.6 mg/kg 0.6 164927000Chromium 24. mg/kg 1. 165127000'Copper . 34. mg/kg 3. 165327000Manganese 704. mg/kg 1. 165827000Zinc 80. mg/kg 3. 167227000T»is(2-ethylhexyl)phthalate < 420. . ug/kg 420. 900140000

. COPY TO ' Paul C. Rizzo Associates ATTN: .Mr. Ken Bird1 COPY TO Data Package Group

S'er-ce*' Arrencar Courcn ofnoecencent Ucoratores !nc

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved by:

See Reverse Side For Explanation Timothy S. Oostdyk, B.A. « -Of Symbols And Abbreviations And u-„-.,-.. rr/uc «4-jLOur Standard Terms And Conditions Manager bU/M5> ,,__,_,,..

AR303826

Page 153: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

•ancasteraoratoriesHpfcndPg-a,l.-u mtu^PH 176O1-599* (717) 6GO-23Q1

LLI Sample No. SV 1587977Paul C. Rizzo Associ?.tas-PA Date Reported 11/15/90300 Oxford Drive . Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-19 Grab Soil Sample Time Collected 1200Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 1,800. mg/kg 50. 013807500Cyanide, Total <0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 10. mg/kg 10. 114504000Lead (furnace method) 11.8 mg/kg 0.5 115504000Selenium (furnace method) . 0.8 mg/kg 0.5 116404000TCL Volatiles' (Soil) attached 117827000Moisture 29.7 X by wt. 0.1 135301200pH 6.75 0.01 144101000

Note:The pH was performed on a 1:1 .slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400r.admium . < 0.5 mg/kg 0.5 164901400

romium 25. mg/kg 1. 165101400per ' 56. mg/kg 2. 165301400ganese . 148. . 'mg/kg 1. 165801400

Zinc ' 29. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully c KmittedClient Services at (717) 656-2301 Lancaster Lr ;ries, Inc.270 04757 250.00 126100 Reviewed ar oved by:

Menoer American Council 3f

See Reverse Side For Explanation Timothy S -lyk B.A. t\Of Symbols And Abbreviations And _.„ _ ,,, -rsr»'/^AA/\-. «4-<UOur Standard Terms And Conditions Manager Gu"--^ft303827

Page 154: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

caster Laboratories ,iar

LLI Sample No. SW 1587977Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA -15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-19 Grab Soil Sample Time Collected 1200Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY VT. BASIS QUANTITATION LAB CODETotal Organic Carbon 2,600. mg/kg 70. 013840000Cyanide, Total <0.1 mg/kg 0.1 023740000Arsenic (furnace method) < 10. mg/kg 10. 114501500Lead (furnace method) 16.8 mg/kg 0.7 115501500Selenium (furnace method) 1.1 mg/kg 0.7 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS RECEIVED* 29.7 X by w.t. 0.1- 135327000Antimony < 7. mg/kg 7. 164427000Cadmium < 0.7 mg/kg 0.7 . 164927000Chromium 35. mg/kg 1. 165127000Copper 80. mg/kg 3. 165327000Manganese 211. mg/kg 1. 165827000Zinc 42. mg/kg 3. 167227000

(2-ethylhexyl)phthalate < 470. ug/kg 470. 900140000

i COPY TO Paul C. Rizzo Associates . ATTN: Mr. Ken Bird1 COPY-TO Data Package Group

_t

•an Asscoa-o- Kx Questions? Contact Environmental Respectfully Submittedr/Ac.-l&uto"'' " Client Services at (717) 656-2301 Lancaster Laboratories, Inc.Stoogica! i E-vircrmentai — . j • . . ,Reviewed and Approved by:

See Reverse Side For Explanation Timothy S. Oostdyk, B.A. 43Of Symbols And Abbreviations And u ' /-/v/uc -*,;,-_*». «Our Standard Terms And Conditions Manager GCjfjN 3 Q 3 Q <£ g

" Cd ci ;f

Page 155: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

_____ ANALYSIS REPORT

Lancaster Laboratories ^425N HotondPike,Lancastw.RA 17601-5994 (717)666-2301

LLI Sample No. SW 1587978Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Moaroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-14 Grab Soil Sample Time Collected 1305Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 12,000. mg/kg 50. 013807500Cyanide, Total < 0.1 mg/kg 0.1 023704000Arsenic (furnace method) 4. mg/kg 1. 114504000Lead (furnace method) 69.2 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture • 24.4 7. by wt. 0.1 135301200pH 6.82 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400

romium 24. mg/kg 1. • 165101400per 49. mg/kg 2'. 165301400.ganese 1,730. mg/kg 1. 165801400

290. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ' ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timothv <? Onsrrivk R A 1^1Of Symbols And Abbreviations And i imotny b. UOS tayk, B. A. 44Our Standard Terms And Conditions Manager GC/Mj

African Co, r.,, ..t uatwatones. trc

Page 156: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster Laboratories ^LLI Sample No. SV 1587978

Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-14 Grab Soil Sample Time Collected 1305Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 15,000. mg/kg 70. 013840000Cyanide, Total < 0.1 mg/kg 0.1 023740000Arsenic (furnace method) 5. mg/kg 1. 114501500Lead (furnace method) 91.6 mg/kg 0.7 115501500Selenium (furnace method) < 0.7 mg/kg 0.7 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS RECEIVED* 24.4 7. by wt. 0.1 135327000Antimony < 7. mg/kg 7. 164427000Cadmium < 0.7 mg/kg 0.7 164927000Chromium 32. mg/kg 1. 165127000Copper 65. mg/kg 3. 165327000Manganese 2,290. mg/kg 1. 165827000Zinc ' 383. mg/kg 3. 167227000"s(2-ethylhexyl)phthalate < 440. ug/kg 440. 900140000

i COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.

:%.?•%£**'*~wor™a Reviewed and Approved by:

See Reverse Side For Explanation Timothy S. Oostdyk, B.A.Of Symbols And Abbreviations And .. J /-/-/ucOur Standard Terms And Conditions Manager GC/MS

Mencer An-ertcan COLPCI! ofifXtecenaert L.iDor3icr;*.s -re

Page 157: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster Laboratories1 >_•_» I Pte, Lancaster. F* 17601-5994 .717>06a-2aOJ

LLI Sample No. SV 1587979Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-13 Grab Soil Sample Time Collected 1350Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 22,000. mg/kg 50. 013807500Cyanide, Total <0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 61.2 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture 58.1 7, by wt. 0.1 135301200pH . . - 6.23 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400

romium 70. ' mg/kg 1. 165101400per ' ' 122. mg/kg 2. 165301400ganese 562. mg/kg 1. 165801400

Zinc • 171. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Member American Council ofindependent laccratones. Inc.

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timothv S Oostdvk B AOf Symbols And Abbreviations And iimoiny a. UOStaVK, B.A.Our Standard Terms And Conditions Manager GC/MS fl R 3 Q 3 8 3 I

Page 158: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster'Laboratories•_„LLI Sample No. SW 1587979

Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-13 Grab Soil Sample . Time Collected 1350Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY UT. BASIS QUANTITATION LAB CODETotal Organic Carbon 53,000. mg/kg 100. 013840000Cyanide, Total < 0.2 mg/kg 0.2 023740000Arsenic (furnace method) < 10. mg/kg 10. 114501500Lead (furnace method) 146. mg/kg 1. 115501500Selenium (furnace method) < 1. mg/kg 1. 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS RECEIVED* 58.1 2bywt. 0.1 135327000Antimony < 10. mg/kg 10. 164427000Cadmium < 1. mg/kg 1. 164927000Chromium . 168. mg/kg 2. 165127000Copper 292. mg/kg 5. 165327000Manganese 1,340. mg/kg 2. 1658270007-inc 409. mg/kg 5. 167227000

;(2-ethylhexyl)phthalate < 790. ug/kg 790. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved by:

See Reverse Side For Explanation Timothy S. Oostdyk, B.A.Of Symbols And Abbreviations And u- - J,. AV/MC- ~ /-, /-_ <-, n o /•>Our Standard Terms And Conditions Manager GC/MSg R 3 Q 3 8 3 2

.noeosndent Laccraicnes .n

Page 159: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

___________ ANALYSIS REPORT

Lancaster Laboratories,, „„,425 IfcirHolwdPiie, Lancaster. Rr\17601-59»t (717166 2301

LLJ Saaple No. SV 1587980Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-12 Grab Soil Sample . Time Collected 1400Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 24,000. mg/kg 50. 013807500Cyanide, Total < 0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 713. mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture 53.2 % by wt. 0.1 135301200pH " 5.87 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400"vromium , 132. mg/kg 1. 165101400«per 144. mg/kg 2. 165301400

ganese 237. mg/kg 1. 165801400c 153. mg/kg 2. 167201400

Bis(.2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Veneer Amer car Council of-ascender, Uaooratones 're.

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timothv S Oo^rrivk R AOf Symbols And Abbreviations And t, Y *' ,z2S V 'Our Standard Terms And Conditions Manager OC/Mb Q Q Q O

Page 160: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster Laboratories ,„„„„„„.PMe;Lancaalv,m. 176O1-5994 <?r7) 660-2311

LLI Sanple No. Stf 1587980Paul C. Rizzo Associates-PA • Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-12 Grab Soil Sample Time Collected 1400Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 51,000. mg/kg 100. 013840000Cyanide, Total < 0.2 mg/kg 0.2 023740000Arsenic (furnace method) < 10. mg/kg 10. 114501500Lead (furnace method) 1,520. mg/kg 1. 115501500Selenium (furnace method) < 1. 'mg/kg 1. 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS" RECEIVED* 53.2 X by wt. 0.1 135327000Antimony < 10. mg/kg 10. 164427000Cadmium . < 1. mg/kg 1. 164927000Chromium 282. mg/kg " 2. 165127000Copper 307. mg/kg 4. 165327000Manganese 506. mg/kg 2. 165827000Zinc 327. mg/kg 4. 167227000

(2-ethylhexyl)phthalate < 710. ug/kg 710. ' 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully Submitted.'.'34A-"sSr'0' Client Services at (717) 656-2301 Lancaster Laboratories, Inc.

" Reviewed and Approved by:

See Reverse Side For Explanation Timothy S. Oostdyk, B.A.Of Symbols And Abbreviations And M_ ,_ 'Our Standard Terms And Conditions Manager

M ,"-te' Arnercan Ca.nc-i _tnceoence"! Latoratcres .nc.

HH

&R3Q383U

Page 161: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

SIS REPORT

ancasterLabomtories ,fji-M i lutort Plte. Lancaster, f* 17601-599* .7t7l66B-23_«

LLI Sample No. SW 1587981Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-10 Grab Soil Sample Time Collected 1440Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon , 15,000. mg/kg 50. 013807500Cyanide, Total < 0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 611. mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture 38.1 7, by wt. 0.1 135301200pH 6.43 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400romium 124. mg/kg 1. 165101400pper 161. mg/kg 2. 165301400.nganese 803. mg/kg 1. 165801400

.Zinc 184. mg/kg 2. 167201400Bi-s(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Memcer American Council ofiraecenaent LdOoratonas. inc.

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timothv S Oostdvk B AOf Symbols And Abbreviations And iimotny b. UOStOyK, fl.A.Our Standard Terms And Conditions Manager SQ&nJ Q 3 8 3 5

Page 162: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

^ ALYSIS REPORT

Lancaster Laboratories , „«.LLI Saaple No. SV 1587981

Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-10 Grab Soil Sample Time Collected 1440Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 24,000. mg/kg 80. 013840000Cyanide, Total < 0.2 mg/kg 0.2 023740000Arsenic (furnace method) < 8. mg/kg 8. 114501500Lead (furnace method) 987. mg/kg 0.8 115501500Selenium (furnace method) < 0.8 mg/kg 0.8 116401500TCL Volatiles. (Soil) attached 117827000Moisture *A*S RECEIVED* 38.1 % by wt. 0.1 135327000Antimony < 8. mg/kg 8. 164427000Cadmium < 0.8 mg/kg 0.8 164927000Chromium 200. mg/kg 2. 165127000'Copper • 259. mg/kg 3. 165327000Manganese 1,300. mg/kg 2. 165827000Zinc 297. mg/kg 3. 167227000-'s(2-ethyIhexyl)phthalate < 530. • ug/kg 530. 900140000

i COPY TO Paul C. Rizzo Associates ATTN: -Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved by:

See Reverse Side For Explanation Timothy S. Oostdyk, B.A. 'Of Symbols And Abbreviations And u««»/»«.- r-r-xwc

___ Our Standard Terms And Conditions Manager bwnsAmer .an Cou"C i .f TSf flHOUOUOD

t Laboraicr as inc

Page 163: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

. , ANALYSIS REPORT

ancasterLaboratories ^LLI Sample No. Stf 1587982

Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-11 Grab Soil Sample Time Collected 1440Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal.Organic Carbon 13,000. mg/kg 50. 013807500Cyanide, Total <0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 585. mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles' (Soil) attached 117827000Moisture 41.5 % by wt. 0.1 135301200pH 6.07 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400< 0.5 mg/kg 0.5 164901400

rornium 112. mg/kg 1. 165101400per 191. mg/kg 2. 165301400ganese . 384. , mg/kg 1. 165801400

Zinc , ' 140. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Menoer Amencar Council offrcfeoencert Lacoratores. ine

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancastr- atories, Inc.270 04757 250.00 126100 Reviewe. >proved by:

See Reverse Side For Explanation Timothy S 'dyk, B.A.Of Symbols And Abbreviations And u--.„-,<*.. r -~.-xA.-i.-..-.-.Our Standard Terms And Conditions Manager Go, "$ R 3 Q 3 8 3 7

Page 164: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

f. 3fSfcfi IS REPORT&•

master Laboratories m,wLLI Sample No. SV 1587982

Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-11 Grab Soil Sample Time Collected 1440Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY UT. BASIS QUANTITATION LAB CODETotal Organic Carbon 22,000. mg/kg 90. 013840000Cyanide, Total < 0.2 mg/kg 0.2 023740000Arsenic (furnace method) < 9. mg/kg 9. 114501500Lead (furnace method) 999. mg/kg 0.9 115501500Selenium (furnace method) < 0.9 mg/kg 0.9 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS RECEIVED* 41.5 %bywt. 0.1. 135327000Antimony < 9. mg/kg 9. 164427000Cadmium < 0.9 mg/kg 0.9 . 164927000Chromium 191. mg/kg 2. 165127000Copper 327. mg/kg 3. 165327000Manganese 657. mg/kg 2. 165827000Zinc 239. mg/kg 3. 167227000

-.(2-ethylhexyl)phthalate < 560. ug/kg 560. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY- TO Data Package Group

Questions? Contact Environmental Respectfully Submitted~ -_ ,-ccn-c-ianor Client Services at (717) 656-2301 Lancaster Laboratories, Inc.Chemical BtoiCGtcat i £rvircnmenlal T» j j j » j _Reviewed and Approved by:

See Reverse Side For Explanation Tlmothv "? (.ostdvlt B A .JOOf Symbols And Abbreviations And limotny b. UostayK, B.A. o«-»Our Standard Terms And Conditions Manager

Men-cer American C3Lncii af'noecencent L3Doraiones ;nc

Page 165: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

^^______ ANALYSIS REPORT

Lancaster Laboratories ^Ht-teid P*e, Lancaster, W 176O1-59G* (717)656-2301

LLI Sample No. SU 1587983Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-11D Grab Soil Sample Time Collected 1450Hunterstown Road Site . P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 14,000. rag/kg 50. 013807500Cyanide, Total < 0.1 mg/kg 0.1 023704000Arsenic (furnace method) 4. mg/kg 1. 114504000Lead (furnace method) 518. mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture " 55.0 % by wt. 0.1" 135301200pH 6.13 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. "164401400r-dmium < 0.5 mg/kg 0.5 164901400

omium 131. mg/kg 1. ' 165101400er 168. mg/kg 2. 165301400ganese 443. mg/kg 1. 165801400

Zinc 165. . mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate 1,300. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timor hv <_ On<;rHvk R AOf Symbols And Abbreviations And

^mber American Council of:ncecendent Laooratones. !nc

M.™ r r / « no Q o ftOur Standard Terms And Conditions Manager GC/ ft 3 0 3 8 3 9

Page 166: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster Laboratories m, eIntend Pfrs.Lanc--5tor.FK 178m 59iJ* tfl ea -QOt

LLI Sample No. SU 1587983Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-11D Grab Soil Sample ' Time Collected 1450Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 30,000. mg/kg 100. 013840000Cyanide, Total < 0.2 mg/kg 0.2 023740000Arsenic (furnace method) 10. mg/kg 2. 114501500Lead (furnace method) 1,150. mg/kg 1. 115501500Selenium (furnace method) < 1. mg/kg 1. 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS RECEIVED* 55.0 7. by wt. 0.1 135327000Antimony , < 10. mg/kg 10. 164427000Cadmium < 1. mg/kg 1. 164927000Chromium 291. mg/kg 2. 165127000Copper 373. mg/kg 4. 165327000Manganese 984. mg/kg 2. 165827000Zinc 367. mg/kg 4. 167227000s(2-ethylhexyl)phthalate 2,880. ug/kg 730. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird.1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully Submitted. .,cr, c-«H.,.a-.on"or Client Services at (717) 656-2301 Lancaster Laboratories, Inc.-- Bdcc iE-.,™,* Reviewed and Approved by:

See Reverse Side For Explanation Timothy S. Oostdyk, B.A... • ......Of Symbols And Abbreviations And u^~~~~~ /-/-/uo . ». »^^_ Our Standard Terms And Conditions Manager GC/MS^ 0 o n ,. n O<J

'/emcer1 American Council ofinOec«raent i_3Doratones IPC

Page 167: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

. ___ ANALYSIS REPORT

ancasfer'Laboratories• „,.,.NMrHoInd P*_v Lancaster, PA 17601-5994 (717) 656-2301

LLI Sample No. SV 1587984Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive ' Date Submitted 10/17/90Monrtfeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-9 Grab Soil Sample Time Collected 1445Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 14,000. mg/kg 50. 013807500Cyanide, Total <0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 94.2 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture 26.1 % by wt. 0.1 135301200pH - 6.66 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 . mg/kg 0.5 164901400

•omium . 34. mg/kg 1. 165101400per . ' 39. mg/kg 2. 165301400ganese 248. mg/kg 1. 165801400

Zinc • 63. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Memoer American Council jf'tt Latxratones. me

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation TimothvS Oo<?rHvk RA -•-Of Symbols And Abbreviations And 1imotny 3. UOS tayK., fl.A. -Our Standard Terms And Conditions Manager GC/M | fl 3 Q 3 Q {4 I

Page 168: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT•

far/ f\Sr tlsj INCUWOHArED

LLI Sample No. SW 1587984Paul C. Rizzo Associaies-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-9 Grab Soil Sample . Time Collected 1445Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 18,000. mg/kg 70. 013840000Cyanide, Total < 0.1 mg/kg 0.1 023740000Arsenic (furnace method) < 1. mg/kg 7. 114501500Lead (furnace method) 128. mg/kg 0.7 115501500Selenium (furnace method) < 0.7 mg/kg 0.7 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS RECEIVED* 26.1 % by wt. 0.1 135327000Antimony < 7. mg/kg 7. 164427000Cadmium < Q.7 mg/kg 0.7 164927000Chromium 45. mg/kg 1. 165127000Copper ' 52. mg/kg 3. 165327000Manganese 335. mg/kg 1. 165827000Zinc 85. mg/kg 3. 167227000X2-ethylhexyl)phthalate < 450. ug/kg 450. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group •

can association -or Questions? Contact Environmental Respectfully SubmittedL. ...r>Acc-wau.,*- Client Services at (717) 656-2301 Lancaster Laboratories, Inc._h_r-_-ai 8ioio_K:ai A Envircnrenlal _ . , , , ,•leas =f.tann. Reviewed and Approved by:

Memcer American Counc.i of'ncecendent Laboratories tnc

See Reverse Side For Explanation T.m<.rhv <; _.<.<: rHvl. R AOf Symbols And Abbreviations And i imotny b. UOStayK, B.A. ....Our Standard Terms And Conditions Manager GC/flS_ o rj O p j O *-* *

Page 169: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster Laboratories „ 0,,, ,»„„Hr» It-Mnni P*«. Lancaster.R* 176O1-590* (717)656-2301

LLI Sample No, SW 1587985Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-8 Grab Soil Sample ' Time Collected 1445Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 5,200. mg/kg 50. 013807500'Cyanide, Total <0.1 mg/kg 0.1 023704000Arsenic (furnace method) 5. mg/kg 1. 114504000Lead (furnace method) 262. mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture " 23.2 % by wt. 0.1 135301200pfl 6.80 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400< 0.5 mg/kg 0.5 164901400

romium 39. mg/kg 1. 165101400/per 25. mg/kg 2. 165301400'nganese 811. mg/kg 1. 165801400

Zinc • 79. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.

. 270 64757 250.00 126100 Reviewed and Approved by:

MemBen American Co-ncii ofIndeoendent Laboratories, me

! Ej?P!anati°" Timothy S. Oostdyk, B.A.Of Symbols And Abbreviations And ,, /,/,,_,,-. >_. «. . ^Our Standard Terms And Conditions Manager GC/MS RR3038U3

Page 170: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

A ANALYSIS REPORT

Lancaster"Laboratories ^Hc....ndPi Lancaster,FW176O1-5994 (717)666-2301

LLI Sample No. SW 1587985Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-8 Grab Soil Sample Time Collected 1445Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 6,800. mg/kg 70. 013840000Cyanide, Total < 0.1 mg/kg 0.1 023740000Arsenic (furnace method) 7. , mg/kg 1. 114501500Lead (furnace method) 341. rag/kg 0.7 115501500Selenium (furnace method) < 0.7 mg/kg 0.7 116401500TCL Volatiles (Soil) attached 117827000Moisture *A3 RECEIVED* 23.2 % by wt. 0.1 135327000Antimony < 7. mg/kg 7. 164427000Cadmium . < 0.7 mg/kg 0.7 164927000Chromium 50. mg/kg - 1. 165127000Copper 33. mg/kg 3. 165327000Manganese 1,060. mg/kg 1. '165827000Zinc 103. mg/kg 3. 167227000

i(2-ethylhexyl)phthalate < 430. ug/kg 430. ' 900140000

i COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

.n A«or,aw -or Questions? Contact Environmental Respectfully Submitted, Acc.-M,t.Sr Client Services at (717) 656-2301 Lancaster Laboratories, Inc.

-ne- _ai Bicioqical 4 Environmental _ , , , , ,•.«.s :>( 'e_t,n. Reviewed and Approved by:

Ve cer Ame"can Council .ft Laooralcnes me

See Reverse Side For Explanation iMmnrriv «; <v.cf..vlr R AOf Symbols And Abbreviations And A imotnv J. °° stdy k, B.A. r-oOur Standard Terms And Conditions Manager GC/MS

Page 171: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

Lancaster'Laboratories ,25 New-Holland Pike, Lancaster, PA 17601-599* (717) 6S-f-2301

LLI Sample No. Stf 1587986Paul C. Rizzo Associates-PA ' Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-6 Grab Soil Sample Time Collected 1500Hunters town Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal Organic Carbon 3,900. mg/kg 50. 013807500Cyanide, Total <0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 4.2 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture 29.0 % by wt. 0.1 135301200pH 6.73 . 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400r*dmium 0.5 mg/kg 0.5 164901400

omium 28. mg/kg 1. 165101400per 9. mg/kg 2. 165301400.ganese 1,020. mg/kg I. 165801400

Zinc 67. mg/kg ' 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.

250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timothv <? OosrHvlf R A (>0Of Symbols And Abbreviations And 1 imotny b. UOStdyiC, fl.A. WOur Standard Terms And Conditions Manager GC/MS

Member- American Council oftvaeoemect LaDoratones. inc.

Page 172: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

LancasterLaborato,nes,StSVr *\*W'-iVi-'i c*~*/wiS\Jl WV\Jr *\/J INCOHPOHAILO25 Nw* Hotond P*e, Lancaster. PA 17601-5994 (717) 656-23O1

LLI Sa»ple No- Stf 1587986Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-6 Grab Soil Sample Time Collected 1500Bunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 5,500. mg/kg 70. 013840000Cyanide, Total <0.1 mg/kg 0.1 023740000Arsenic (furnace method) < 7. mg/kg 7. 114501500Lead (furnace method) 6.0 mg/kg 0.7 115501500Selenium (furnace method) < 0.7 rag/kg 0.7 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS RECEIVED* 29.0 7. by wt. 0.1 135327000Antimony < 7. mg/kg 7. 164427000Cadmium 0.7 mg/kg 0.7 164927000Chromium 39. mg/kg 1. 165127000'Copper 13. mg/kg 3. 165327000Manganese 1,440. mg/kg 1. 165827000Zinc 94. mg/kg 3. 167227000"Ms(2-ethylhexyl)phthalate < 460. • ug/kg 460. 900140000

i COPY TO Paul C. Rizzo Associates ATTN:-Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved by:

See Reverse Side For Explanation Timothy S. Oostdyk, B.A.Of Symbols And Abbreviations And .. ~n /ueOur Standard Terms And Conditions Manager GC/Mb

Member American Council 3findependent Laooratones. Inc.

Page 173: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

ANALYSIS REPORT

ancasterLaboratories ^425 New Hofiand Pike, Lancaster, PA 17601-5994 (717) 656-2301

LLI Sample No. Stf 1587987Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 Discard Date 11/23/90

Collected 10/16/90 by CVSD-7 Grab Soil Sample Time Collected 1515Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODETotal. Organic Carbon 25,000. mg/kg 50. 013807500Cyanide, Total < 0.1 mg/kg 0.1 023704000Arsenic (furnace method) < 5. mg/kg 5. 114504000Lead (furnace method) 2,080. mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000TCL Volatiles (Soil) attached 117827000Moisture 51.7 7, by wt. 0.1 135301200pB 6.33 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

Antimony < 5. mg/kg 5. 164401400Cadmium < 0.5 mg/kg 0.5 164901400

romium 480. mg/kg 1. 1651014001 per 206. mg/kg 2. 165301400ganese . 191. mg/kg 1. 165801400

Zinc ' 114. mg/kg 2. 167201400Bis(2-ethylhexyl)phthalate < 330. ug/kg 330. 900140000

Internal standard peak areas were outside of the QC limits for both theinitial injection and the re-injection. The values reported here are fromthe initial injection of the sample.

1 COPY TO Paul C. Rizzo Associates ATTN: Mr. Ken Bird1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedClient Services at (717) 656-2301 Lancaster Laboratories, Inc.270 04757 250.00 126100 Reviewed and Approved by:

See Reverse Side For Explanation Timothv <? no<?ff.vk R AOf Symbols And Abbreviations And Tlmotny S. Oostdyk, B.A.Our Standard Terms And Conditions Manager GC/MS

Member American Council ofinoesedaen! uooratones. inc.

Page 174: iiii i pj-j--— · ID EPA SAMPLE NO. PESTICIDE ORGAN I CS ANALYSIS DATA SHEET Sample wt/vol: 1000

iNALYSIS REPORT

Lancaster'Laboratories™»,,DMc._end:P*e. Lancaster, PA 176O1-59B4 (717)6.56-2301

LLI Sample No. SV 1587987Paul C. Rizzo Associates-PA Date Reported 11/15/90300 Oxford Drive Date Submitted 10/17/90Monroeville, PA 15146 . Discard Date 11/23/90

Collected 10/16/90 by CVSD-7 Grab Soil Sample Time Collected 1515Hunterstown Road Site P.O. ENV-X-00196

Rel.RESULT LIMIT OF

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODETotal Organic Carbon 52,000. mg/kg 100. 013840000Cyanide, Total < 0.2 mg/kg 0.2 023740000Arsenic (furnace method) < 10. mg/kg 10. 114501500Lead (furnace method) 4,300. mg/kg 1. 115501500Selenium (furnace method) < 1. mg/kg 1. 116401500TCL Volatiles (Soil) attached 117827000Moisture *AS RECEIVED* 51.7 % by wt. 0.1 135327000Antimony < 10. rag/kg 10. 164427000Cadmium < 1. rag/kg 1. . 164927000Chromium 994. mg/kg 2. 165127000Copper 426. mg/kg 4. 165327000Manganese 395. mg/kg 2. 165827000Zinc 237. mg/kg 4. 167227000Ris(2-ethylhexyl)phthalate < 680. ug/kg 680. 900140000

Internal standard peak areas were outside of the QC limits for both theinitial injection and the re-injection. The values reported here are fromthe initial injection of the sample.

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