in-situ cryogenic nano-mechanical tests ln 2 or lhe in 77 k4 k temperature controller (pid) : heater...

3
itu cryogenic nano-mechanical tests LN 2 or LHe in 77 K 4 K Temperature controller (PID) : heater control Cold finger Indenter tip sample electron gun SEM chamber (UHV) Mechanical data acquisition Cu wire out Bi-polar heater heater Tip cooling assembly Si diode temperature sensors Ceramic block Current in-situ cryogenic mechanical testing set-up at Caltech (designed by L. Meza) The world’s first time cryogenic nanomechanical measurement Seok-Woo Lee (Postdoc)

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Page 1: In-situ cryogenic nano-mechanical tests LN 2 or LHe in 77 K4 K Temperature controller (PID) : heater control Cold finger Indenter tip sample electron gun

in-situ cryogenic nano-mechanical tests

LN2 or LHe

in

77 K 4 K

Temperaturecontroller (PID): heater control

Coldfinger

Indentertipsample

electron gun

SEM chamber(UHV)

Mechanical dataacquisition

Cu wire

out

Bi-polarheater

heater

Tip coolingassembly

Si diodetemperaturesensors

Ceramic block

Current in-situ cryogenic mechanical testingset-up at Caltech (designed by L. Meza)

The world’s first time cryogenic nanomechanical measurement

Seok-Woo Lee(Postdoc)

Page 2: In-situ cryogenic nano-mechanical tests LN 2 or LHe in 77 K4 K Temperature controller (PID) : heater control Cold finger Indenter tip sample electron gun

in-situ cryogenic nano-mechanical tests

Current in-situ cryogenic mechanical testingset-up at Caltech (designed by L. Meza)

Fundamental understanding ofmechanical behavior of materials atlow temperatures for space applications

COLD!!

Page 3: In-situ cryogenic nano-mechanical tests LN 2 or LHe in 77 K4 K Temperature controller (PID) : heater control Cold finger Indenter tip sample electron gun

D

in-situ cryogenic nano-mechanical tests

SIZE EFFECTS at different temperatures

Nanopillar Size effects size-dependent strength

S.-W. Lee et al. Phil. Mag. (2012)

Theoretical estimation for W

What are you going to do with me?

1. Fabrication of nanostructures

Different sizesDifferent materials

2. Nano-mechanical testing at different temperatures

3. Data analysis (stress-strain) and fundamental understanding(atomistic, dislocation dynamics)

Welcome any enthusiastic SURF students !!!Welcome any enthusiastic SURF students !!!Seok-Woo Lee, [email protected] Lee, [email protected]