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R.S. Sandha On behalf of RRCAT team [email protected] Development of Industrial Linacs and Experimental Dosimetry at EB Processing Facility, Indore

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Page 1: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

R.S. Sandha – On behalf of RRCAT team

[email protected]

Development of Industrial Linacs and Experimental Dosimetry

at EB Processing Facility, Indore

Page 2: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

1. Accelerator & Beam Physics Section – Physics design

2. Accelerator Control Systems Division – Control system development

3. Accelerator Magnet Technology Division – Magnetic elements and collinear load development

4. Beam Diagnostics & Coolant Sys Division – Beam diagnostics and precision cooling system

5. Construction & Services Division – Radiological shielding and infrastructure systems

6. Design & Mfg Technology Division – Vacuum brazing and component manufacturing

7. Indus Operations & Alignment Section – Magnet Fiducialization and alignment

8. Industrial Accelerators Division – Facility design, Accel structure, beam experiments, dosimetry, processing

9. Laser Controls & Instrumentation Division – Search, secure & safety system; process interrupt

10. Power Converters Division – Scanning and magnetic supplies, HV measurements

11. Precision Power Supplies Division – Fire alarm and safety system.

12. Pulsed High Power Microwave Division – Electron gun and microwave system

13. Ultra High Vacuum Technology Section – Vacuum system

14. Health Physics Team – Radiation survey and Radiation Safety Duties.

15. RF Systems Division and Accelerator Physics Section for consultation on several technical matters

16. Indian Industries – for a large number of components for iterative developments

Acknowledgement

Page 3: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

1. Objectives

2. Development of industrial linacs

3. Beam, accelerator and process requirements

4. Details of Radiation Processing Facility (ARPF)

5. Dosimetry and EB processing

These points will be presented in this talk.

Outline

Page 4: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Introduction

Page 5: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

1. Develop 10 MeV rugged indigenous accelerators for societal application

2. Develop beam delivery systems for various applications

3. Develop associated systems for bulk radiation processing (process interrupt handling, energy filter,…)

4. Demonstrate technical suitability of the indigenous accelerators for various societal applications

5. Demonstrate economic viability of indigenous accelerator technology for Indian societal applications

Objectives

AFAD 2019, IUAC, New Delhi

Page 6: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Development of Industrial Linacs

RRCAT has developed two 10 MeV, 5 kW electron linacs for

electron beam radiation processing. The linacs have been

endurance tested for several hundred hours of operation.

AFAD 2019, IUAC, New Delhi

Page 7: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Linac-B1

Page 8: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Linac-B Linac-C

Type, Frequency 2π/3, Traveling Wave, 2856 MHz

Beam energy (max.), MeV 10 and 7.5

Beam Pulse Current, mA 200 350 / 475

Energy spread 10% 7% (for 90% particles)

Beam Pulse Duration, s 10 10

Pulse Repetition Rate, Hz 250 300

Average Beam Power, kW 5 10

Current Status Developed In-process

Electron linac specifications

AFAD 2019, IUAC, New Delhi

Page 9: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Electron linac systems

AFAD 2019, IUAC, New Delhi

Page 10: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

18 cell SUPERFISH

simulation - 5 MeV, 3 kW

9.5 / 7 MeV 10 kW

Cavities -

1 – prebuncher

5 – buncher

45 - regular

2D-Electromagnetic

design of Pre-buncher

cavity

Physics Design: 10 / 7.5 MeV Dual Energy 10 kW Electron Linac

AFAD 2019, IUAC, New Delhi

Page 11: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Engineering designs

Conceptual and engineering designs

AFAD 2019, IUAC, New Delhi

Page 12: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Tolerance < 10 microns, Roughness < 0.2 µm Ra

RF Coupler machining

Dimensional inspection Surface roughness

RF Coupler components RF Coupler machining

Industrial Linac: Machining and Dimensional QC

AFAD 2019, IUAC, New Delhi

Page 13: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Transverse deformation plot

Length (mm)

Te

mp

era

ture

, C

D

efo

rma

tio

n, m

icro

ns

Precision chiller (Capacity: 20 kW,

Temperature ± 0.5 ˚C) Temperature plot

-0.400

-0.300

-0.200

-0.100

0.000

0 10 20 30 40 50

De

lta

f, M

Hz

Cavity number

Frequency detuning of cavities

Industrial Linac: Thermal management

AFAD 2019, IUAC, New Delhi

Page 14: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Cavities stack brazing

Cusil, 810 C, 5min

2-stage brazing of RF couplers

I stage- Palcusil, 820 C, 5min

II stage- Cusil, 810 C, 5min

Final brazing

Cusil, 810 C, 5min

1st & 2nd cycle 3rd cycle 4th cycle

Industrial Linac: 10 MeV Structure Fabrication

AFAD 2019, IUAC, New Delhi

Page 15: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

110

115

120

125

130

135

0 5 10 15 20 25 30 35 40 45 50

Ph

ase

ad

van

ce

Cavity number

Phase advance per cell measured using Bead-Pull method

Bead pull setup

Industrial Linac: RF qualification

AFAD 2019, IUAC, New Delhi

Page 16: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Control rack Gun PS Klystron Gun Modulator

Linac-B1 with its subsystems under testing at RRCAT

AFAD 2019, IUAC, New Delhi

Page 17: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Operating Parameters

Beam Power : 5 kW

Beam Energy : 9 MeV

Beam current : 270 mA

Pulse Width : 10 µs

Endurance test: 30 – 8 hr shifts

Shifted to ARPF after endurance testing at RRCAT

Linac-B1: 8-hour shift operation test

AFAD 2019, IUAC, New Delhi

Page 18: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Linac-B1: Endurance test - 90 Hours non-stop operation

AFAD 2019, IUAC, New Delhi

Page 19: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Linac-B2

Page 20: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Linac-B2 under qualification at RRCAT

AFAD 2019, IUAC, New Delhi

Electron Gun Solenoids

Beam Monitor Electron window and target

Page 21: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

• As per regulations, maximum electron energy < 10 MeV (< 7.5 MeV in x-ray).

BPM

Chromatic

magnet

BPM

PSM

BPM

MESUREMENT SLIT FARADAY

CUP SLIT

CT CT

Beam Diagnostics

Typical result of Beam Profile Measurement

AFAD 2019, IUAC, New Delhi

Page 22: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

6 kW operation

9 kW operation (Short duration)

Endurance test Linac-B2

AFAD 2019, IUAC, New Delhi

Page 23: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Date of operation: 20-21, Dec 2017, Uninterruptedly for 32 Hrs.

10 AM

Dec 20, 2017 6 PM

Dec 20, 2017

2 AM

Dec 21, 2017 10 AM

Dec 21, 2017

6 AM

Dec 20, 2017

Beam ON Time (Hrs.)

Endurance test Linac-B2: Nonstop 32 hrs. operation

AFAD 2019, IUAC, New Delhi

Page 24: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Facility

Page 25: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

EB Radiation Processing Facility at Indore

RRCAT is developing a Radiation Processing Facility at Indore

Fruits & Vegetable Market using these linacs. Facility has been

commissioned with the first linac. Second linac is planned to be

commissioned this year (2019).

The facility has a product handling system, dosimetry system, and

all the necessary infrastructure for demonstrating radiation

processing using the electron linacs.

Several applications of the electron beam will be demonstrated.

Medical

sterilization

Microbial

hygienation

Phytosanitary

irradiation

Mutation

breeding

AFAD 2019, IUAC, New Delhi

Page 26: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Targeted Radiation Processing Applications at the Facility

Radioactive source like Cobalt-60

Electron Accelerator applications

Imaging Radiotherapy Surface processing < 3 MeV Bulk processing 10 MeV

Food cans Medical sterilization Quarantine - Fresh fruit

Insect Disinfestation pulses, dried food

Municipal waste treatment

microbial decontamination Spices, herbs

Delay ripening

Page 27: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

EB Radiation Processing Facility at Indore

AFAD 2019, IUAC, New Delhi

Page 28: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Facility Layout

AFAD 2019, IUAC, New Delhi

Page 29: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Equipment room

Linac-B1 during installation

AFAD 2019, IUAC, New Delhi

Page 30: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Linacs-B1 and B2 after installation

Page 31: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Dosimetry and

EB Processing

Page 32: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Product density

(g/cc)

Single side Double side

1 3.5 cm 8 cm

0.5 7 cm 16 cm

0.4 9 cm 20 cm

0.3 12 cm 26 cm

0.2 18 cm 42 cm

0.15 23 cm 55

Single sided

Double sided

Product

box

Product

box

Electron beam

Electron beam Electron beam

Electron Beam Irradiation Schemes

AFAD 2019, IUAC, New Delhi

Page 33: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Parameters affecting dose and dose uniformity

1. Beam energy

2. Beam current

3. Beam spot size

4. Pulse repetition rate

5. Pulse width,

6. Scanning frequency,

7. Scanning width

8. Conveyor speed

9. Product distance from

window foil

10. Product density

Electron Beam Irradiation Scenario

AFAD 2019, IUAC, New Delhi

Page 34: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Dosimetry System

Alanine EPR Dosimetry

System

Dose Range:

0.05 to 50 kGy

Radiochromic

film dosimetry

systems

GaFchromic films

Dose range: 0.05-1 kGy

B3 films Dose range:

1 - 80 kGy

Alanine EPR dosimetry system Radiochromic film dosimetry system

Dosimetry Laboratory at RRCAT

AFAD 2019, IUAC, New Delhi

Page 35: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Energy measurement using RISO Al

wedge as per ASTM 51649

Surface dose uniformity along scan direction

Beam Parameters

Energy 9 MeV

SSD 20 cm

Conveyor

speed

0.5 m/min.

Scanning

parameters

8.0 A @

400msec.

±3% over the full box height = 43 cm

Do

se

Un

ifo

rmity s

trip

Radiation Field Characterization

AFAD 2019, IUAC, New Delhi

Page 36: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Quick-fly back Profile 1.Beam current

2.Beam spot size

3.Pulse repetition rate

4.Scanning frequency,

5.Scanning width

6.Conveyor speed

7.Product distance

from window foil

88 pulse/scan

=88 pulse/50 cm

= 0.6 cm centre

shift on foil

=0.9 cm on

product surface

Conv. Movement

1.3 cm shift/scan

Surface Dose Uniformity and Harmonization of Operating Parameters

AFAD 2019, IUAC, New Delhi

Page 37: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Experimental radiation processing Petri Dishes using 9 MeV

e-beam

Volumetric DUR 1.36

achieved in sterilization of

petri dishes irradiated with

electron beam

Volumetric Dose Measurement as per AERB/RF-RPF/SG-1

AFAD 2019, IUAC, New Delhi

Page 38: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

Conclusion

1. 10 MeV industrial linacs developed for medical sterilization and radiation processing of agricultural products.

2. Facility commissioned with Linac-B1.

3. Linac-B2 will be commissioned this year.

4. Approvals of the regulatory bodies and licensing bodies to be obtained for radiation processing.

5. Using add-on components, beam power and beam delivery systems of the two linacs will be improved.

AFAD 2019, IUAC, New Delhi

Page 39: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

1. The ability to double break DNA strands in living organisms such as cells, bacteria and insects making them sterile. • Radiotherapy for treatment of cancer,

• Disposable medical product sterilisation and antiseptic packaging

• Live insect elimination in food,

• Disinfection of the spices and herbs without fumigation,

• Quarantine for fruit flies /weevil in fruit,

• Fungus treatment in food – Salmonella, Listeria,

• E-coli elimination in foods.

2. Ability to penetrate with precisely determinable scattering • X-ray imaging for NDT, Cargo scanning, Medical imaging

3. Ability to form free radicals and form new bonds • Cross linking of polymers, curing, breakdown cellulose • Waste water treatment and Dye elimination • Flue gas treatment

4. Ability to produce mutation for mutation breeding of crop varieties

Properties of electron beam/x-rays which make them usable

However, an appropriate radiological shielding is required for protection

Page 40: Industrial Linacs and Experimental Dosimetry at EB ... Sandha.pdf · Cavities stack brazing Cusil, 810 C, 5min 2-stage brazing of RF couplers I stage- Palcusil, 820 C, 5min II stage-

1. Beam parameters. • Adjustable beam energy 7 MeV / 9.5 MeV

• Low energy spread

• High beam power (viability begins at ~ 50 kW)

2. Linac requirements • High stability, efficiency, reliability, robust

• Energy filter to eliminate particles higher than regulatory limits

• Low O&M costs and quick recovery after maintenance

3. Process requirements • Ability to handle process interrupt without discarding the product,

• Log the process data and store process data for long time.

• Qualification and routine dosimetry,

• Develop process compatible product packaging.

• Incoming and outgoing product testing and certification.

Important requirements for bulk radiation processing