[inorganic lab report, narrative, sample data …
TRANSCRIPT
LAB : Spectrfx
LAB NO. : 8712066
CL!ENT : Jacobs Engineering
Table o f Contents
Section I - Marrat i re
Section 11- Sample Data Sumnary Package and QC
Section 111-Analysls R a w Data
Secticn I V - D i g e s t i o n i D i s t i l l a t i o n
Logs
Page i
CHECKLIST
v/ s+iQl!u
Narrative
4 Copies of inorganic Traffic Reports
SPECTFIIX - HOUSTON 0Oe.CBNlRaNQ: - - 1 1 /
CHECKLIST
SFCTlON I1
JJ Sample Summary Sheet
d Cover Page 1ADS
L/ Form I IADS o
J 7
dC Report Forms u r- 0 0
S0ec:-ixIHouston Csn:rac: : /
4 r" Case No. : SXS No.: ----- SCG No.: .-"-- - E 7 A Sazple Na.
--%+- Lab Sanpta ID.
&7lZObb-02& . . -
/eze IC? iz:erele=ezZ csrrectians applied?
.e lease of t.4.e da=a csntained in Ltis hardccpy da:a packacje an& i n 'Ae puzer-readable dara s115rni:ted O R Z L o ~ p y d~sicet=e has been aut!!c=i~ed ky
he Laboratary Xariaqer o r the Manager's designee, as .yeriOLeQ by L\e,
Daze COVE2 YACZ -
I JcXS Y O .
Case Sc. : - - Cede: - SXS XO. : S3C Ha.: - -
- -
u& YO.
7 4 29-90-5 7443-36-0 7440-38-2 - . , . " 3 - 3 9 - : . - a 8 T - 0 - 4 I ,-f
7413-43-9 7440-70-2 7 4 40-47-3 7 4 4 0 - t a - 4 7440-$3-a 7 4 3 9 - 8 9 - 5 7429-92-1 743'1-95-4 7439-96-5 - 1 - 3 9 - 9 7 - 5 I
74 10-02-0 74 40-09-7 77a2-49-2 7 4 4 0 - 2 2 - 4 744C-i3-5 ,7440-23-0 7440-62-2 7445-66-5
C l a r i t y 3e:ere: - mar.-- - --e:
Cod.: - - - - -- Car6 ?la.: s)cS Y O . : I X NQ.: -
I,, I
J CcCe: - case xc . : - EXS Xo.: - S2G No. : -
1 Control L L a l t s : Mercury 8BO-120; CiL!er H e t a b 90-tlO: Cfanlde 84-115
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SPECf RIX - HOUSTON
I r n . ~ N K # X , N O : e r Y - 7 / -
I
CHECKLIST
ANALYTICAL RAW DATA:
- L/ . Furnace - M (AS) J
Furnace - AA (Pb) v/ -- Furnace - AA (Se) d='
nal y s i t Report f ~ e 01-12-$8 llt22:20 AM page 1
Q ad: EPA
ode: CONC Corr . Factmi-: 1
I n 5 p p m
U l i l r s p7rn
a 1 y s i s Report rue 01-12-28 11:~;: i 0 AM
, ad: EPA Sample Narn.2: I C W 3 / ~b vet-ator : t? Time: 01/12/38 11:25: 12 rnmcnt : da: CONC Corr. Factor: 1
'2
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; ocl: EPA Sample Name: ICB 1,. Time: 0 1 / 1 2 / 8 8 11:29:39 zrnrnent-: Bde: CONO C o r r . Factor: 1
- .
Tue 01-12-88 11:31:37 AM
cgd: EPA Sarnple Name: ICSA Overator: -I Tlrne: 01/12/88 l l : X : 15 arnent. : 3e: CONC C s r r . Factor: 1
P n a l y s i s R w o r C fue 01-12-88 il:37r21 AM i
h .od: EFG Sample Name: fCSAB C!:/12/3& 11:SS:23
Corr. Factor: 1
Factor: 1
page 1
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. I I EVA Srmr l r Nrmrr ICSABF , T i r n r ~ 3 1 / 1 3 / 8 8 16t32123 m + n t i Jr.:ct.s Enq. r: CONC Corr. Factor I I
ern 8.3 1 3 0 Nr5de3 M.32790 A 1 3632 Y-7664 C.3 179 V-2924 i t s ~ c m F cm P P ~ w m PPB P P ~ r r m a* , 4 3 3 .5706 4 9 9 . 6 5 0 0 . 1 <. rJoo0 430.4 ,5114 IV . 0 111 .:I !:I 0107 .6 . 9 . 0471 - 8 , 0 0 0 9 S Ls . O C Z l 1.832 ,1214 , 1 7 1 9 4 . 3 2 9 ,1471 . 1735 &,'I,
41.b'/* qg.olt L , 4 2 3 6 ,5430 4.5';. 2 6.3*'*,s3.5 c ' . 0090 48.3.8 .5120 ,4326 .5732 500.1 5 0 0 . 7 4 3 1 . 0 . S t 0 7
: : : I z,; : . ".. - - , . - I . . _ U D _
.a . - 7 7 . t ., P . . '.- .- ,. . - . ag L ". - , : ' I Z 2 a ; t L
Wr. S ? A - - A -.. ? 0:: i t 2 L -. E?.\ O E 0 O C ' 8 cs: ' 3 3:: m ; ? ~ 9 C 0 O C 2 4 C ' l ,* 4
xs :PA R'J 3 " 5 ma:^ 8:: c G : ? e - - ,,. 5?.\ A'/ '. 3:5 a ~ f L SC : C::4
vn S ? X - - ,. E P A
? - - . .,. r , . - - - .. " - I - - . - - I :'I
- . , ' 1 . . . . . . . . . . . . . - . . ... - * I., -.. - - 1 -
P s r k Offset
CL? Re3:: r l ' e 2
A; :?A - C 0 : 5 21;': P e a k Offset 00007~1
SPECTRIX HOUSTON D . c . ~ $366 4- 06 bb7b - O b
AA INSTRUMENT LOG
ELEMENT 4 5 SOW# 727 DATE 1 -7-89
M&e;#: ps*n-Fmer
/ Wave!ertpb lq3.7 m Larrp: EDL VenCof&@n-Ffmer power % ~ r * t S 5
Sit 0.7 m ~ i i g Car A N HCL Serial#
.- Fame: Fuel Oxid ,- Hydr'%e Cold V t p r
REMARKS. 10 d of 1000 wrn Std #( ) in 10 rnl vol. BaSk = I gm inL s:d. I ml 01 in!. std. tn 10 ml vol Rask s 100 @I 05 mi of int. M. n KJ ml vel Rask 8 50 ppb 0 rnI 01 m. ski. in 10 ml vol flask a 25 ppb 0.10 ml of inl. sld. m 10 rnl vol flask 10 ppb 0.0 ml 01 int. rtd. tn 10 ml vol 0 ppb (&I. 5k)
Anelysi Name, ~ C A -
Spectrix DC # 4
FURNACE . A RAW DATA
ELEMENT- AS
INSTRUMENT - P.E. 560
WCKGRCCWD CORRECTION (YiN) - Y (02)
PLATFORM (YdN) - Y
PEAK AREA
MATFllX MOClFlER - (M.M) (Y/N) Y
NP€'CONC. - M Q ( N O ~ ) ~ N H ~ H ~ P O J ~ %
M.I*L'SAMPLERATlO- ?OuV1000rrl
ANALUICAL SPIKE (A.S.) CONC. 1 mk A.S./SAMPLE FIAT10 10 uUl000 ul
ANALYST - &&)
DATE- 1 - 7-88
FURNACE . A RAW DATA
ELEMENT- AS
INSTRUMENT - P.E. 560
m C K G R a N O CORRECTION (YiN) - Y (02)
PLATFORM (YiN) - Y
PEAK AREA
MATRIX MOClFlER - (M.M) WIN) - Y
NPECONC. M6,(NO3)2NHdH2POd4%
M.MiSA!,IPLE RATIO - 10 uW1000 ul
ANALYTICAL SPIKE (A.S.) CONC. - 1
A.S.lSA!APLE RATIO - 10 uU1000 ul
ANALYST - &e* DATE- f q - g g
Spectrix DC #
ELEMENT- AS
INSTRUMENT - P.E. 560
BACKGRCCND CORRECTION (YIN) - Y (02)
PLATFORM (Y/N) - Y
PEAK AREA
MATillX MGDlFlER - (M.M) F I N ) - Y
TYPECONC. - Mg(N03)2NW4H2PQ&%
M.M/SAMPLE RATIO - 10 ~V7000 UI
ANALYTICAL SPIKE ( A S . ) CBNC. - 1 mg/L
A.S.;SAMPLE RATIO - 10 u1/1000 ul
ANALYST - DATE- /-.7--B%
FURNACE - AA
ELEMENT- As
INSTRUMENT - P.E. 560
BACKGRaND CORRECTION (YIN) - Y (02)
PLATFORM (Y/N) - Y
PEAK AREA
MATRIX MOOlFlER - (M.M) WIN) - Y
TYP WCQNC. - Ms(NO~)~M-L+H~PO&%
M.M/SAMPLE RATIO - 10 w o o 0 UI
ANALYTICAL SPIKE (AS.) CONC. - 1 rngn
A.S.,'SAMPLE RATIO - 10 ~111000 ul
ANALYST - D A T E - I -7-8g
Furnace 1 (la871
IE'i?: PE WC':ELEN;TH (NY ) : 2s 5 . Z, SLI7 ( t d K ; : 0.7 54-52 T'uPE u::n PLh77OEM - MAX FQGEP !+EfiTIb:G - C a S Sf3P - FlAT?,lX P3D,
' rE&T TLP?: 500 A13MIZE TLR?; 193; C%WACT. MASS (PC1 t 2 .O
--r.. =. -.- fVR'*4CE f i Y E lNYEiY4L (J-IM _c c s - c y ~ c ; - - .. ':c - =&mp i i j ~ ~ I;rSFLSW FEAD FE*fOFi.DEF
5 0 2 : ? 3 i c - - 7 - 1 3G s - 1 C 30C - - * e - d - - o?o : s 2s aoc - J l iO0 0 . 0 - - 5 2650 I I 3CC. - - - P - - - - I - - 330 - - - - - - - - - 1 30C - - - - - - - - - I - - 300 - 9 - - - - I - - 35C -
.- .- ............................................................................ I - 3 . No) i iMeDE' / . m 6 . 6 COLfeVAPe= L3e03 S
+ * 6 ~ f + 6 b b 4 * * * b ~ + 4 * 4 * 4 V * * ~ * * * ~ 4 4 * ~ b * * * V * 4 4 t V * 4 ~ + 4 4 t * 6 ~ b + & b 4 V 4 b ~ 4 ~ b ~ b 4 4 4 * a 4 e . C 5 C A C ' t 5 X P 3 ~ b * 4 e 4 ~ C * ~ ~ * + ~ ~ ~ 0 ~ b b ~ * 4 * * * t ~ ~ * ~ 4 * @ + V C b t ~ e * ~ ~ O b ~ 9 4 4 e t ~ 4 ~ t b ~ ~ 4 b b b b ~ 4 b s ~ v ~ ~ 4 ~ ~ 4
0 0 0 2 . ! 2s a . l l?! .......................................................................... . O # k ? C 573. EL :. =%.a UJ/P : IEF. VLL.. I. 1! % i ~ m ~ e * ~ b e b e e ~ ~ ~ ~ ~ ~ e e * e - i ~ o v ~ c a e ~ + ~ c e * + * e ~ e ~ ~ a ~ ~ ~ ~ ~ ~ ~ ~ ~ s m * ~ e ~ ~ ~ & ~ s * ~ * ~ ~ t + ~ ~ * i
3 . 2 SYXJOAFD t e ~ s e ~ ~ e ~ e 4 n ~ ~ 4 4 ~ 4 ~ b 4 ~ ~ ~ 1 1 4 4 O ~ ~ ~ 4 ~ t ~ ~ t ~ t ~ O e b b ~ v ~ e + f e b + @ ~ @ ~ e 4 4 4 e ~ ~ + 6 ~ ~ 4 + ~ b ~ ~ e ~ ~
0 0 0 3 r i . l YC,. - ............................................................................ I r q . r 3fD.DE':.*$o.e / / S F X t V P ? . m 3.31 % * ~ ~ ~ ~ ~ e e ~ ~ * + ~ ~ e ~ ~ ~ ~ ~ ~ b ~ ~ f ~ * ~ v ~ e c ~ s ~ ~ e ~ ~ e ~ ~ e ~ ~ ~ ~ e ~ + ~ t ~ ~ ~ e ~ ~ ~ t e ~ ~ e ~ e ~ ~ ~ ~ ~ ~ + e ~ ~ +
e 00 iz i -9.1 2 4 , 2
. . . . - . - I - - - . - - - . - - - - - - - . - - - . . . ~ - ~ - - - - - . . . - . - . . . * uv= 26. 1 STD. DE'.'. s a $ n * t * C O E F . V A P . = 10.32% l.[r$Z ~ * . * * * * ~ + * * * * * 4 * * * * * + t e t C t * o t t + * b * * * + t + + * Q b * * b * b + ~ * t * * * * ~ * $ t * t ~ * t * ~ t t * * $ * * * * * ~
5 - 0 0 1 3 46. i 4 7 . 3 -------.----.-----..--..*----* . -1 1 1 - - - - - - . . . - - - - - 1 _ - I - . - I - . - - - - - - . * - - . - . - - - -
-1 .- , L 5 ~ 3 . DE.:. LL 4 COEF. vnt? . = 2 .59 r
00 Y.4 - 2 . 2
- 1 . ' 370. DE?,. = L C ~ C3EF.VAR.a 89 .69 %
5 4 . 2 M
5 3 . 1 E T D . C E r r r * O 43 C O E F . v A R , = 1 .87 0
0 0 0 5 4 9 . 4 48, f
- - - . - - - - - * * - - - - - . * - - . - - - - - - - - - - - - - - . - - - - - * - - - - - - - - - . - - - - - - - - - - - - - - - - * - - - - -
4ru= 43. a S I O . D E ~ ~ ~ ~ ~ ~ % ~ ~ ~ COEF.VAP.= 7 I ~ * * * + * * * + + * * + * * + + + I + + * * * + * * * * + * ++* * t . * + * * + + C t i + * * + * + * C C * + * + C + * * + * + * + + 4 * * * + *
33 O O Q Z - 0 , a
JZX - 1 . 5 - - - " - - - - - - - * - - - - . - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - . - * - - - - - - - - . - - - - - - - - - - . - *
- 1 . 0 5TD. DE:. = L C # COEf.VAR,r 33.09 r /
Spectrix DC #,, - -
ELEMENT- Pb
INSTRUMENT - P.E. 563
BACKGRWD -2 2 L C
fi 6.444 3 6 4 6 3 f3%a CORRECTION (Y/N) - Y (D2) g L . 9 8 - 1.31
l . I J~c J 3 1 3 . ~ 3 , P i 3
PLATFORM (YIN) - Y J. ~'*fi/'r 9.31 (I
f i 0.4 4 83 7 / G
PEAK AREA s~*tp;1.178 /" 3 i ~ 1 f ~ I I = d 8 0 1 L " i'" i-iif: 2 3. 8
MATRIX trlOGlFlER - (M.M) (Y/N) - Y 1 W B f s 0 . 4 44 4
SL."/k. ).)b TYPECONC. - M Q ( N O ~ ) ~ N H ~ H ~ P O ~ / ~ % ; U ~ ~ , 8 . 1 .. X ' ~ n ~ l l b . B 1; 1 0 %
M.M/SAMPLE RATIO - 10 u!11300 ul f+. .oqq$1 :;/ SLJ,4.1.33
ANALYTICAL SPIKE (A.S.) CONC. - ! mg/L ,c us f&.ldS :,-
A.S./SAMPLE RATIO - 10 uli1000 ul ~ l ~ ~ ~ t l 3 . 1 * , i L
ANALYST - DATE -
Furnace 1 (1.207)
000088
ELEWENTt S E WAVELENCTH ( WM I I 1 9 6 t 0 I L t ? IWMII be? PYRO COATED TUBE WITH PLATFORM - HAX POWER WEATtNC - GAS STOP WlTRlX MOD. FRETREAT ?EMPI 9 0 0 ATOMlZE VEfiPt Zf00 CHARACT. RASS O C I 30.0
t , TSCMN!QUEI ZECnAN 21 LMP CUFRENT I f l A i ~ 0 3 SICNAL PROCESSINCI PEA) AREA 4 , CALIBRATION1 LINEAR 5, T IME ~SECONDSII 5,O 6 1 READ DELAY tSECONDSIt 0.0 7 , SCffZOY FORMTI 8.0 GRAPHICS 8 , P l l I N T f R t ALL MAIN VALUE8 S. RECUR3ER S ~ C N A L I 0.2 C l N T A83 LO m PECORDEF EXPI 1000
1 1 , S T A T t S T I C f t 2 AVERACE k CV 12. NOMINAL WElCWT t . 0 13, ROLLOvER(ABS,r l.SOO 1 4 , BC SCALE1 L t O
Li. S 2 t I ¶ , S S l 226 sat
PROCRAMMIX MODE HCA 600 WEA PIETH I 0 5 - SE DATEt . CP 0
ELEMEhlTt SE WAblELEFICTH ( W ~ I F ~ ) I (96.0 S L f T t W 1 1 0.7 f- PYRO COATED TUBE U l T H PLATFORbI - MAX POWER HEATlNC - CAS STOP - MATRIX M C L . ~ PRETREAT TEttF: 900 AT2HlZE TEMPI 2100 CFARACT, MASS (PC1 30.OC,
STEP FURNACE T tME I NTEFNAL NUFIPEP TEMPERATURE RAMP HOLD CASf LOW READ PECOPbE?
1 90 2 2 0 300 - 2 130 IS I0 300 . - 3 900 I0 25 300 - - 4 1100 0 3 0 C - 5 2630 I 3 300 - - 6 I - - 300 - - 7 -.-a I 0 300 - - 8 - - - - 1 -. 3QC - . 9 I - - 300 - -
..-..-......-1. 1.-.--.*-.........-.------..........*.-----.---.-..-.---.-..--
I - C, C s G i P7t. Pi?.'. 9.0 C?LF.VIW.. k 0 . M S b w e I 8 ~ 8 ~ 0 1 b 1 ~ 4 ~ ~ b b ~ b ~ ~ ~ ~ i P ~ ~ P ( . & 4 ~ a m & O b b @ ~ C 4 ~ * ~ ~ ~ ~ ~ a ~ ~ b ~ ~ ~ ~ & b ~ ~ e ~ 4 ~ ~ 4 ~ ~ ~ ~ b e 4 ~ ~ . ... ..... &LC GZEP.3 & ~ L ( Q * b V U I * ~ O I b @ C V C C b ~ ~ Q 8 ~ I ) i b C ~ ~ * b t i I L b D $ 4 ~ b * ~ b ~ ~ ~ L * * P C * $ ~ * ~ V ~ ~ ~ ~ ~ ~ ~ + 8 ~ b & ~ b ~ t b
. - . 0 0 0 2 . .;.s 9 . 2 4 0 .....-.... 1.1.-..*....--..---.-.......-.......*...-...........*~..~~-*~~~.~..
U S r i . 2a3 E t T , f . E , ~ . s l O + . O C;EF.vnP.- 0 . 6 4 r b ~ + ~ ~ r b ~ + ~ r ~ b ~ 4 b 4 * * * ~ ? m * C ~ e * * ~ 8 * ~ + ~ b ~ D * * * e D 6 * ~ b * ~ * B ~ 8 6 ~ B ~ ~ ~ m ~ * S D @ ~ 9 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ , .- . . 'J . . +. STAfrt4F3 1 ~ ~ e b ~ b e v ~ ~ ~ v * b ~ ~ L ~ & B 4 o a * ~ ~ ~ ~ ~ ~ ~ ~ C ~ ~ b * I I ~ b b * ~ ~ * b m * ~ ~ ~ 8 b ~ 8 f ~ J ~ ~ ~ + 4 4 4 o b e * D ~ ~ b ~ * D ~
0 0 0 s - !. . . t . 2
. m 5 . 6 3%. DE:'. &4A C:,EF.\AP. - S , S € X w/ I ~ * * . O . ~ * * * E , ~ * * * * * * C 1 1 * i e * . P * O C . * * * , ~ * * C C * * * * ~ * * * * v ~ * * * * * * * * * * * * * * * * * * . ~ . * C * * ~ ~ ~
0 0 0 4 0: 2 5 . 0 24eb 0 (--..-*-..--.----I.-- Ic L 2 5 . 3 5Tto DEd. *25.6 : O E F . V A E , = 3 . 4 9 1 ~ b * * * + * * C + * * * b b * v * * i C f * * * * t * * * C * 4 * * * ~ * ~ * e * * * * 4 e ~ ~ 6 ~ 4 4 * * * * b * * * 4 f * 4 * * ~ ~ * v * 4 & * ~ *
0 , 0 0 0 5 C,
4 5 . 5 5 1 . 2
L = Z0.i 3 T D # 3E1'. * $8.. CQEF. vAP. = I +dE 1
0006 ? S . 2 5 5 . 9
t OE. i 5:; DE.'. = /or 6 C O E C . V A F . = 0 . 4 7 r
2. - 0 0 0 7 - . a : 9 2 . 4
x 9 2 . 0
. - ooota '2 8 t 2.3 - - - - . - - . - - . . - - - .~~~~- - . - - - - . . - - . . - - - - - - - . . . -.-.---.-..._-.--..-.-.-
= \ # ? , EOD.DE. ' , =ZC$ C C E F . V A E . * %Z.L9 % * * * + ~ * * 3 * + * + + + * * + * * * * * * * * ~ * * * * r + + s C ? * ~ * + + * * + + * + + + * * * + & * . + * ' C * * b * * ~ € *
0009
e 49 .8
80 x 0 - c . z G6.3
= E E , 4 S ~ S . C ! Z ~ ~ ~ L G S + - I ~ ;CE;.VAE.r 4.37 Z
0 0 1 1 2 5 . 1 1 2 0 . 2 - - - - . - m - - . - s - - - - - - - - - - - - - * - - - - - - - - - - - - - - - - * - - - - - . - - - * - - - - . - - - - - - . - - - - - - - - - - -
C 122. a -- 2 1 . n . ~ r v , SLGSQP' C0EF.VAR.z 2.58 X ,*~***,t*t*++,+.*~**+*+****++*C+*** . ~ + * + * 4 t * * + * * * * * C * * * ~ * * t * * * t t * t ~ t t * + * b * *
k 2 . S bee tv E-50: REAKitNC GPEATEP THAN HfC4ES7 SYPNDAEC
OC3090
1 9 . 9 STB.9E./,= 1 O B r I U COEF,VAF.= 1.96 !& wy" . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ***I***
oo,"Z5 5 7 . 5
- - * - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - . * - - - - - * - - - - - - - - - - - - - - -
51 . G XD. orti . =ccJ&~dLf COEF,VAR. = 3-62 1 lal.)/9B.~, 103 ********+**+****+**+***+4*+***+++**+L****+***********4**************+***+****+**
0 0 2 G 3.4
- " - - - - - - - - - - - - - - - - - - " - - " - - - - - - " * - - - - - - - - - - - . * - - - - - - - - * - - - - - - " - - - - - - - . - - -
5 7 2 a b ~ : . = 6 ~ f i COEF.VAR.= 2 2 , X % N
Ln
I 1 9 . 6 2 ! , 2 P;
2 0 . 4
ooz2e, ' 5 . $3
. - - - - - - - - - - - - - - - - - - - - - - - - - - - * - - - - - - - - - - - - - - - - - - - + - - - - - - - - - - - - - - - - - - - - - - - - - - - - 2 2 , : ~ T G . I ) E / . = J ( , I $ ~ I COEF,VAE,= 0 P € 3 4
. . * + I C I + I + C + C * + + + * * * * * - C ~ ~ X * * * ~ ~ * ~ * ~ * ~ ~ * * * * * * * i
O O Z Y 2 % 2
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CHECKLIST
DIGEST~ONIDISTILLATION LOGS:
V' ICPlFlame AA Metals
/ Furance - AA Metals !
Mercury
/1)k Cyanide
Percent Solids
DATE c
METAL PREPARAT I O N WORKSHEET
METAL PREPARAi I O N WORKSHEET
WT.OR MLS ML. OF ML. OF F I N A L CONC. S P I K E INFORMATION: SAMPLE NH03 H2 0 2 VOLUFIE FACTOR ELEMENT & CONC. 1N
F I N A L VOLUME
I Pb 1 . 5 ppm, Fe 0 . 5 0 ppn 2 50 % Cu .15 pprn
a HE2CJRY PREP MAT ION 'rlORKSEET