*i»»^p &« ve »••••««m^d . recfwed · engineering co. ms. marti harding-smith barr...

QUALITY ANALYTICALLABORATORIES. INC.

October 8, 1994

*i»»^p« 'mrnmm »••••««M .&i vEDr;OV 18 1994SPFD ESAIICHREGION VII

RECFWEDOCT 0 1 1994

BARRENGINEERING CO.

Ms. Marti Harding-SmithBarr Engineering Company8300 Norman Center Dr.Minneapolis, MN 55437-1026

RE: Analytical Data for: Barr Engineering CompanyLaboratory Reference Number: R8621

Dear Ms. Harding-Smith:

On August 26, 1994, QAL, Inc. received samples with a requestfor analysis. The analytical results and associated qualitycontrol data are enclosed.

It is our policy to store your samples for 30 days from thedate -of this letter. If extended storage is required,special arrangements can be accommodated upon earlynotification. The disposition of samples identified ashazardous will require special handling and you will becontacted if necessary.

QAL, Inc. appreciates your business and looks forward toserving you again. If you have any questions concerning yourreport or need any additional information, please call me at(916)244-5227.

Sincerely,

Mark CichyProject Manager/Client Services

Enclosures

xc: Mr. Don Richard

S00074681SUPERFUND RECORDS

Quality AnalyticalLaboratories Inc.

5090 Caterpillar Road.Redding, CA 96003-1412

916244-5227Fax No. 916244-4109

TABLE OF CONTENTS

QXL Reference No. R8621

Page

List of Organic Data Qualifiers . . . . . . . . . . . . . . . . . . . . . iList of Sample ID Qualifiers . . . . . . . . . . . . . . . . . . . . . iiList of Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . iiiClient Sample Cross -Reference . . . . . . . . . . . . . . . . . . . . . iv

INORGANIC DATACase Narrative (s) . . . . . . . . . . . . . . . . . . . . . . . . . l

Analytical Sample Results . . . . . . . . . . . . . . . . . . . 2-14

Quality Control DataResults of Blank (s) . . . . . . . . . . . . . . . . . . . 15-19

VOLATILE ORGANIC DATACase Narrative . . . . . . . . . . . . . . . . . . . . . . . . 20-21


Quality Control DataResults of Blank (s) . . . . . . . . . . . . . . . . . . . 35-36

SEMIVOLATILE ORGANIC DATACase Narrative . . . . . . . . . . . . . . . . . . . . . . . . 37-38


Quality Control DataResults of Blank (s) . . . . . . . . . . . . . . . . . . . . 52

Copy of Chain-of-Custody . . . . . . . . . . . . . . . . . . . . . . 53-54

5090 Caterpillar Road, 916244-5227Laboratories inc. Redding. CA 96003-1412 Fax No. 916 244-4109

ORSAHIC DATA QtJALiriERS

U -- Indicates the compound was analyzed for but not detected. The numberadjacent to the "D" qualifier indicates the reporting limit for thatcompound. The reporting limit can vary from sample to sample dependingon dilution factors or percent moisture adjustment when indicated.

J -- -Indicates an estimated value. It is used when the data indicates thepresence of a compound below the stated reporting limit.

C -- This flag applies to OC analytes only. The "C" flag indicates thepresence of this compound has been confirmed by OC/MS analysis.

B -- This flag is used when the analyte is found in the associated blank aswell as the sample. This notation indicates possible blankcontamination and suggests the data user evaluate these compounds andtheir amounts carefully.

E -- This qualifier indicates that the value reported exceeds the linearcalibration range for that compound. Therefore, the sample should bereanalyzed at an appropriate dilution. The "E" qualified amount is anestimated concentration, and the results of the dilution will bereported on a separate Form I.

D -- This qualifier indicates compounds which have been identified during adiluted reanalysis. "D" qualifiers are used for samples that have beenanalyzed initially at a lesser dilution than required for accuratequantitation.

Quality Analytical 5090 Cote/pitar Pood. 916244-5227Laboratories Inc. KsdaTng. CA 96003-1412 Fax No. 916 244^4109

ORGANIC LAB SAMPLE H> QOALITCXRS

The qualifiers that nay be appended to the Lab Sample ZD for organic analysesare defined below:

DL Dilution Run. Indicates the sample contained compounds exceeding thecalibration range. The sample was diluted and re-analyzed. Bothresults are reported.

R Rerun. The sample was re-analyzed. The "R" is not used if thewas also re-extracted.

RE Re-extraction Analysis. The sanple was re-extracted and re-analyzed.

MS Matrix Spike (may be followed by a digit to indicate multiple matrixspikes within a sample set)

MSD Matrix Spike Duplicate (may be followed by a digit to indicate multiplematrix spike duplicates within a sample set)

DUP Duplicate extraction and analysis. The sample was extracted andanalyzed in duplicate.

ii

Quatty AnatyUcct 5O9O Catwpfar Rootti 9162444227LaboiatortfSlne. R***ng. CA 96003-1412 Fax No. 916 2444109

Check appropriate analysis metbod(s) and/or preparation metbod(s)

QAL Lab Reference No.

Parameter Method

Halogenated Volatile Organics . . . . . . . . . . o 601. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . O 5030A/8010A

Aromatic Volatile Organics . . . . . . . . . . . . O 602. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . O 5030A/8020

Phenols - Determinative .............. a 604. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . O 8040A- Extraction . . . . . . . . . . . . . . . . . . . . . . a 3520A/3550- Clean-Up . . . . . . . . . . . . . . . . . . . . . . D 3640/3650A

Color. Pest./PCB - Determinative . . . . . . . . D 608. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D 8080. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . O CLP-Extraction . . . . . . . . . . . . . . . . . . . . . . O 3520A/3550

Clean-Up . . . . . . . . . . . . . . . . . . . . . . D 3620A/3640/3660A

Organo-P Pesticides - Determinative . . . . . . . O 8140A- Extraction . . . . . . . . . . . . . . . . . . . . . . D 3520A/3550- Oean-Up . . . . . . . . . . . . . . . . . . . . . . D 3620A/3640

Chlorinated Herbicides . . . . . . . . . . . . . . . D 8150A

Volatile Organics . . . . . . . . . . . . . . . . . . D 624. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D 524.2. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . X8240A

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . CJ CLP

Volatile Organics, Low Level . . . . . . . . . . . O CLP

Volatile Organics by GC/MS . . . . . . . . . . . D 8260

Semivolatile Org.- Determinative . . . . . . . . . O 625. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . X 8270A. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D CLP- Extraction . . . . . . . . . . . . . . . . . . . . . . g ^25^3550/3580A- Clean-Up . . . . . . . . . . . . . . . . . . . . . . D 354U/3650A/3660A

Method Source

40 CFR 136SW-846, 3rd Ed.

40 CFR 136SW-846. 3rd Ed.

40 CFR 136SW-846, 3rd Ed.SW-846. 3rd Ed.SW-846. 3rd Ed.

40 CFR 136SW-846. 3rd Ed.SOWOLM01.9SW-846. 3rd Ed.SW-846. 3rd Ed.

SW-846, 3rd Ed.SW-846. 3rd Ed.SW-846, 3rd Ed.

SW-846, 3rd Ed.

40 CFR 136EPA-600/4-88-039, 10/93SW-846, 3rd Ed.SOW OLM01.9

Superfund Analytical Methods for LowConcentration Water for Organics Analysis.10/92

SW-846. 3rd Ed.

40 CFR 136SW-846. 3rd Ed.SOW OLM01.9SW-846. 3rd Ed.SW-846. 3rd Ed.

'Each of the extraction methods indicated applies only to samples of the appropriate matrix.

he clean-up methods indicated do not necessarily apply to all samples in the deliver group. Refer to the case narrative orsample report for specific information.

m

Parameter Method Method Source

PAH - Determinative . . . . . . . . . . . . . . . . D 610. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D 8310- Extraction . . . . . . . . . . . . . . . . . . . . . . O 3520A/3550- Clean-Up . . . . . . . . . . . . . . . . . . . . . . D 3630A

Chlorinated Phenols (CPAR) ........... O Internal

PCBs/Oil . . . . . . . . . . . . . . . . . . . . . . . O Internal

TFH/Gasoline . . . . . . . . . . . . . . . . . . . . Q CA LUFT. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D AK Modified ORO. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D WI Modified GRO

TFH/Diesel . . . . . . . . . . . . . . . . . . . . . . D CA LUFT. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . n AK Modified DRO. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D WI Modified DRO

Formaldehyde . . . . . . . . . . . . . . . . . . . . D 8315

TCLP Extraction . . . . . . . . . . . . . . . . . . X 1311

40 CFR 136SW-846, 3rd Ed.SW-846. 3rd Ed.SW-846. 3rd Ed.

CPAR Project Report 825-1, Canadian Pulpand Paper Research Institute, 3/79

EPA-600/4-8 1-045

CA LUFT Manual, 5/88ADEC PUBL-AK 101. 2/93WI DNR PUBL-SW-140. 7/93

CA LUFT Manual. 5/88ADEC PUBL-AK 101,1/93WI DNRPUBL-SW-141, 7/93

SW-846 3rd Ed.. Proposed Update

SW-846. 3rd Ed.

11/92

Each of the extraction methods indicated applies only to samples of the appropriate matrix.

The clean-up methods indicated do not necessarily apply to all samples in the deliver group. Refer to the case narrative orsample report .for specific information.

ill

Simple ID Cross-reference Table

ML, Inc.Lab Sample IDR8621001R8621002R8621003R8621004R8621005R8621006R8621007R8621008R8621009RB621010RB621011R8621012R8621013RS621S01DRS621B01MSR8621801MSDR8621S01S

FSFSFSFSFSFSFSFSFSFSFSFSFSOUPNSOUSDMSI

ClientSanple IDTM-3ATH-3BTM-3CTM-4ATM-4BTM-4CTM-5ATM-5BTM-5CTM-6ATM-66TM-6CMD-2DUPLICATEMATRIX SPIKEMS DUPLICATEMATRIX SPIKE

CollectDate08/25/9408/25/9408/25/9408/25/9406/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/94

Sample Matrix Additional DescriptionSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoil

TCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLPTCLP

EXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACTEXTRACT

iv

Ouattty AnalyticalLaboratories Inc.

5090 CatwpHar Rood.Redding. CA 96003-1412

916244-5227Fax No. 916 2444109

CASE NARRATIVEInorganics

Laboratory Reference Number: R8621

Client/Project: PARR________________________________

I. Holding Time;All holding times were met.

II. Preparat ion /D ioe«t ion Except ions ;None.

III. Analysis!

A. Calibration:All acceptance criteria were met.

B. Blanks:All acceptance criteria were met.

C. ICP Interference Check SamplerAll acceptance criteria were met.(Not applicable for General Chemistry) .

D. Spike Samplers);All acceptance criteria were met.

B. Duplicate Samplers);All acceptance criteria were met.

F. Laboratory Control Samplers);All acceptance criteria were met.

G. ICP Serial Dilution:Not required for this level data package.(Not applicable for General Chemistry).

H. Other:Not Determined (ND) is reported for the RPD when the sampleconcentrations are below the reporting limits.

IV. Document at ion Except ions ;None.

V. I certify that this data package is in compliance with the terms andconditions agreed to by the client and QAL, Inc., both technically andfor completeness, except for the conditions detailed above. Release ofthe data contained in this hardcopy data package has been authorized bythe Laboratory Manager or his designee, as verified by the followingsignature.

SIGNED:FredR. Bickell

Inorganics Supervisor

Quality Analytical 5090 CaterpHar Road. 9 16 244-5227Laboratories Inc. Redding. CA 96003- 14 12 Fax No. 916 244-4109

00001

Report of Analytical ResultsINORGANICS

Date Collected: 08/25/94Date Received: 08/26/94Sample Matrix: SoilSample Description: TCLP EXTRACT

Client Saaple ID: TM-3ALab ReferenceNu«: R8621Lab Saaple 10: RB621001

CATEGORY NAMEAnalytical Parameter Result unit. »«fortJ'W Date of Analytical«~uit units Level Analysis Nethod(s)

TCU» ArsenicTCL> iarius '

SPA200.7/W6010

TCLP LeadTCLP MercuryTCLP SeleniumTCLP Silver

< 0.025< 0.0002< 0.035< 0.0020

•0/L•0/L•Q/L•B/L

0.0250.00020.0350.0020

09/12 409/08/9409/12 409/12/94

tPA200,7/«l6010«PA200.7/S«6010EPA200.7/SU6010EPA245.1/SW7470EPA200.7/SUM10EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories (HAL), inc. •-

Report of Analytical Result*INORGANICS

Date Collected: 08/25/94Date Received: 08/26/94Sanple Matrix: SoilSaaple Description: TCLP EXTRACT

Client Sample ID: TH-3»Lab ReferenceNui: R8621Lab Saaple ID: R8621002

CATEGORY NAMEAnalytical Parameter Result Units

ReportingLevel

Date ofAnalysis

AnalyticalMethod(s)

CATIONSTttP ArsanicTOP lariuaTCLPTCt»TCLP LeadTCLP MercuryTCLP SeleniuaTCLP Silver

< 0.0016< 0.0030< 0.025< 0.0002< 0.035< 0.0020

0 0010 09/12/94

•B/L•0/L•B/L•0/L

0.00300.0250.00020.0350.0020

09/12/9409/08/9409/12/9409/12/94

EPA200.7/SU6010CM200.7/SU60TO£1*200.7/8*010EPA200.7/SW6010EPA200.7/SU6010EPA245.1/SU7470EPA200.7/SU6010EPA200.7/SU6010

< 1516)

Quality Analytical Laboratories COAL). Inc. — Redding

00003

Raport of Analytical RatuLtaINORGANICS

Data Collactad: 06/25/94Data Received: 06/26/94Sanple Matrix: SoilSaeple Description: TCLP EXTRACT

Cliant Saapla ID: TM-3CLab ReferenceNi*: R6621Lab Saapla ID: R8621003

CATEGORY NAMEAnalytical Parameter

Raporting Data of AnalyticalRaault Units Laval Analysis Nathod(s)

Id? ChroailtJiTCLP LaadTCLP NarcuryTCLP SalaniwTCLP Silver

< 0.025< 0.0002< 0.035< 0.0020

•B/L•0/L•0/L•B/L

0.0250.00020.0350.0020

09/12/9409/08/9409/12/9409/12/94

JPA200.7/SU60TO7/SU6010

lPA200.r/SU»107/W6010

EFA200.7/SU6010EPA245.1/SU7470EPA200.7/SU6010EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories (OAL), Inc. — Reddings

00004%,

••port of Analytical Result*INORGANICS

Data Coltactad: 08/25/94Date Received: 08/26/94Saapla Matrix: SoilSaapla Daacription: TCLP EXTRAa

Ctlant Saapla ID: TM-4ALab RafarancaNua: R8621Lab Saapla ID: R8621004

CATEGORY NAMEAnalytical Paraavtar

Reporting Data of AnalyticalRaault untta Laval Analytic Nathod(a)

TOPTO* -TOI»C»d«tiaiTCLPChroarfuaTCLP LaadTCLP NarcuryTCLP Salanii«iTCLP Sllvar

0.030< 0.0002< 0.035< 0.0020

•8/L•0A•0/L•8/L

0.0250.00020.0350.0020

09/12/94 EPA200.7/SU601009/06V94 EPA245.1/8W747009/12/94 EPA200.7/SU601009/12/94 EPA200.7/SU6010

( 1516)Quality Analytical Laboratoriaa (OAL), Inc. — Raddino

oooo:


Date Collected: 06/25/94Date Received: 08/26/94Sample Matrix: SoilSanple Description: TCLP EXTRACT

Client Saaple ID: TM-4BLab ReferenceNun: R8621Lab Saaple ID: RB621005

CATEGORY NAMEAnalytical Parameter Result•cesuit unit.units

*«»rt1np Date of AnalyticalH,thod{g)

TCU>«arii»TCLP CadMiu»TCtF ttiraniuiTCLP LeadTCLP MercuryTCLP SeleniunTCLP Silver a

SRA200.7/M6010«AZOO;7/BI6010iPA200.7/SUB010£PA200.7/M6010»>A200.7/SW6010

09/Oe/»* EPA245.1/SW747009/12/94 EPA200.7/SM601009/12^4 EPA200.7/SW6010

C 1516)

Quality Analytical Laboratories (QAL), Inc. -- Redding

00006

Rtport of Analytical ResultsINORGANICS

Date Collected: 08/25/94Date Received: OB/26/94Sample Matrix: SoilSaaple Description: TCLP EXTRACT

Client Saaple ID: TM-4CLab ReferenceNiw: RB621Lab Saaple ID: R8621006


Reporting Date of AnalyticalResult Units Level Analysis Method(s)

CATIONSTCLP ArsenicTOP garluiTCLP CadarfiaiTCLP chro»lu»TCLP LeadTCLP MercuryTCLP SeleniumTCLP Silver

'

0.048< 0.0002< 0.035< 0.0020

BB/La«/La«/L

0.0250.00020.0350.0020

09/12/9409/08/9409/12/9409/12/94

€PA200,7/SU6010 .EPA200.7/SU5P1 0 'EPA200.7/SU6010EPA245.1/SU7470EPA200.7/SU6010EPA200.7/SW6010

< 1516)

Quality Analytical Laboratories (QAL), Inc. — Redding

OOC07



Client Saaple ID:Lab ReferenceNun:Lab Sample ID:

TN-5AR8621R8621007

CATEGORY NAMEAnalytical Parameter Result Units

ReportingLevel

Date of AnalyticalAnalysis Method(s)

:::: •:::;•'CATIONS':-w:TCU> ArsenicTCLHariurTOP CaderfuBTCIP ChroBftnTCLP LeadTCLP MercuryTCLP SeleniumTCLP Silver

m< 0.0030< 0.025< 0.0002< 0.035< 0.0020

•0/L•B/L•g/L•B/L

1 0010 09/12/9*'

0.0250.00020.0350.0020

09/12/9409/08/9409/12/9409/12/94

CPA200.7/SU6010EPA200.7/SW6010EPA200,7/SU6010EPA200.7/SW6010EPA200.7/SU6010EPA245.1/SU7470EPA200.7/SU6010EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories (OAL), Inc. -- ReddingOOC08



Client Sample ID: TN-SiLab Referenced: R8621Lab Saaple ID: R8621008


Reporting Date of AnalyticalResult Units Level Analysis MetnooXe)

CATIONSTCLP ArsenicTCLP BariuaTCLP CadhiuiTCIP ChromiuaTCLP LeadTCLP MercuryTCLP SelenimTCLP Silver

< 0,0010<o.oow< 0.025< 0.0002< 0.035< 0.0020

•B/L•S/L•B/L•B/L

0.00100,00100.00300.0250.00020.0350.0020

EPA200.7/SUM10EW200.7/SU6010

09/12/9409/08/9409/12/9409/12/94

EPA200.7/SU6010EPA200.7/SU6010EPA245.1/SU7470EPA200.7/SU6010EPA200.7/SU6010

1516)

Quality Analytical Laboratories (QAL), Inc. — Redding

00009


Pate Collected: 08/25/94Date Received: 08/26/94Sample Matrix: SoilSanple Description: TCLP EXTRACT

Client Sample 10: TM-5CLab ReferenceNin: R8621Lab Sanple ID: R8621009


Reporting Date of AnalyticalResult Unite Level Analysis Nethod(s)

CATIONSTCLP ArsenicTCLP SariuMTOP CadrfUBTCLP ChronftffTCLP LeadTCLP MercuryTCLP SeleniumTCLP Silver

0.0150,0010

OS/12/W

** 0.0030< 0.025< 0.0002< 0.035< 0.0020

•B/L

•g/L•B/L

D.00300.0250.00020.0350.0020

09/12/94

EPA200.7/SU6010iPA200.7/IW60rO

09/12 409/08/9409/12/9409/12/94

EPA200.7/SW6010EPA245.1/SV7470EPA200.7/SU6010EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories COAL), Inc. -- Redding

OOC10

Date Collected: 08/25/94Date Received: 08/26/94Sample Matrix: SoilSaaple Description: TCLP EXTRACT


Client Saapte ID:Lab Reference**:Lab Seaple ID:

TM-6AR8621R8621010


Reporting Date of AnalyticalResult Units Level Analysis Nethod(s)

CATIONSTOPArsenicTOP ««M«sTOP CadriuBTCLP ChroMiusTCLP LeadTCLP MercuryTCLP SelcniuiTCLP Silver

':< 0.0050

< 0.025< 0.0002< 0.035< 0.0020

•8/L•B/L•0/L•B/L

0.00100,00100.00500.0250.00020.0350.0020

09/12/9409/12/9409/12/9409/08/9409/12/9409/12/94

SPA200.7/SU6010€PA200.r/W6010iPA200,7/S«M>10EPA200.7/SU6010EPA200.7/SW6010EPA245.1/SU7470EPA200.7/SU6010EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories (QAL), Inc. -- Redding

00011


Date Collected: 08/25/94Date Received: 08/26/94Sanple Matrix: SoilSanple Description: TCLP EXTRACT

Client Sanple ID: TM-68Lab ReferenceNum: R8621Lab Saaple ID: R8621011


TCLP ,TttP toriUB

TCLP LeadTCLP MercuryTCLP Selenii*TCLP Silver

< 0.025< 0.0002« 0.035< 0.0020

1PA200.7/SW6010

0.0020EPA200.7/SW6010EPA200.7/SM6010

< 1516)

0-lfty Analytical Laboratories (QAL), inc. -. Rwjdin8

OOC12



Client Sample ID: TM-6CLab Referenced: R8621Lab Sample ID: R8621012



CATIONSTCLP ArsenicTOP BariumTCLP CadmiumTCLP ChromiumTCLP LeadTCLP MercuryTCLP SeleniumTCLP Silver

mm0.069

< 0.0002< 0.035< 0.0020

•0/L•B/L•0/L•0/L

0.00100,00100.00300.0250.00020.0350.0020

w/izm09/12/W09/12W09/12V9*09/12/9409/08/9409/12/9409/12/94

EPA200.7/SWMMOEPA200.7/SUD01DEPA200.7/SW6010

EPA200.7/SU6010EPA245.1/SW7470EPA200.7/SU6010EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories (QAL), Inc. — ReddingOOCJ3



Client Sanple ID: MD-2Lab ReferenceNun: R8621Lab Saaple ID: RB621013



CAT10MSTCIP ArsenicTOP *arfui

09/IZ/94

TCLP thraaJuaTCLP LeadTCLP MercuryTCLP SeleniuRTCLP Silver

< 0.025< 0.0002< 0.035< 0.0020

•B/L•g/t•BA•0/L

0.00100,00300.0250.00020.0350.0020

09/12/9409/08/9409/12/9409/12/94

£PA200,7/SU«nOEPA200.7/SM6010{PA200.7/XU6010CM200;7/IU6010EPA200.7/SU6010EPA24S.1/SU7470EPA200.7/SU6010EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories (GAL), Inc. — Redding 00014fan

i Ui

Raport of Analytical ResultsINORGANICS

Oat* Collected: None Client Sample ID: METHOD BLANKDate Received: None Lab Referenced: LABOCSample Matrix: Soil Lab Saaple ID: VariousSaaple Description:

CATEGORY NAME Reporting Data of AnalyticalAnalytical Parameter Result Units Level Analysis Mtthod(s)

CATIONS a;; ••: , , : ::;£><£, m <;: * :mmm^, :mtmmimw:m^9!vmmmm^m ;* •• •vmMzmti::;:m •;.;.::;.;; -Utfi<^^M?%mtiKi^^TOP i»MuBi;:;:;;; ^TCI*OB«i4;ii;iPlliIi;:;J iH»|J^^rat Cttraat^m^^^m^^Hf^TCLP Lead < 0.025 ag/L 0.025 09/12/94 EPA200.7/SW6010TCLP Mercury < 0.0002 «Q/L 0.0002 09/08/94 EPA245.1/SV7470TCLP Selenium < 0.035 ma/L 0.035 09/12/94 EPA200.7/SU6010TCLP Silver < 0.0020 BB/L 0.0020 09/12/94 EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories (OAL), Inc. •- Redding

H0015


Date Collected: NoneDate Received: NoneSample Matrix: SoilSample Description:

Client Saaple ID: R8671001DLab ReferenceNun: LABQCLab Sample ID: R8621001D



•.:.':.:. 'CATIONS :lTCLP ArsenicTCLP lariusTCLPTCLPTCLP LeadTCLP SeleniumTCLP Silver

mfmN DN DN D

EPA200.7/SU60JO

e>A200,'7/S«6010

RPORPDRPO

N/AN/AN/A

09/12/94 EPA200.7/SW601009/12/94 EPA200.7/SU601009/12/94 EPA200.7/SW6010

( 1516}

Quality Analytical Laboratories (QAL), Inc. •• Redding00016

Report of Analytical ResultgINORGANICS

Date Collected: NoneDate Received: NoneSample Matrix: SoilSample Deacriptfon:

Client Sample ID: RB621001SLab ReferenceNum: LABOCLab Sample ID: R8621001S


Reporting Date of AnalyticalResult Unit* Level Analysis Nethod(s)

CATIONSTCtP ArsenicTap lariumTCLP CadmiumTCLP ChromiumTCLP LeadTCLP SeleniumTCLP Silver

Xrec

96.6104.589.3

XrecXrecXrec

ill/*:::3*7*1i*/*aN/AN/AN/A

09/12W^yymmfovum*09/12/9409/12/9409/12/94

EPA200;T/W6010«>A200.7/ty6010iPA200.7/SU6010EPA200.T/5U6010EPA200.7/SU6010EPA200.7/SU6010EPA200.7/SU6010

( 1516)

Quality Analytical Laboratories (QAL). Inc. -- Redding 00017roe

teport of Analytical RctultcINORGANICS

Date Collected: None Client Sample 10: R8621002DDate Received: None Lab Referenced: LAMCSample Matrix: Soil Lab Sample ID: R8621002DSample DMcription:

CATEGORY NAME Reporting Date of AnalyticalAnalytical Parameter Result Unite Level Analysis Nethod(c)

r ::;: CATIONS' :X:::::;v iiliSS si;'M-if':'&'.• • v:;:':#.•'\-' S -'SMX f f Sa; %tii -3K?&fV:ZiV'v-':•:•;:t:-;':'?;••'• '•''.':: 1': ::::' -;;TCIF (CUi>i|

1516)

Quality Analytical Laboratories (GAL), Inc. •- Redding 00018

Report of Analytfcal ResultsINORGANICS

Date Collected: None Client Sample ID: R8621002SDate Received: None Lab ReferenceNin: LABOCSample Natrix: Soil Lab Saaple ID: RB621002SSanple Description:

CATEGORY NAME Reporting Date of AnalyticalAnalytical Parameter ResOlt Units Level Analysis Nethod(s)

CATIONS '•:•••• •• ...•':iv-':-:.;, :':';•:-•:•: ,::-:,>:-:;j;s:.,: /:\: >;:;M£s ^ :

TCLP H«-cury".': ':• I • :..::|;C;;|:: iM^MiM^^ ^ii^^y^iiyS

( 1516)

Quality Analytical Laboratories (QAD, Inc. •- Redding

00019

CASE NARRATIVEGC/MS VOLATILE SAMPLES

LABORATORY : QAL

CASE NO. : N/A

LAB REF. NO.: R8621

CLIENT: BARR ENGINEERING/DER

CONTRACT NO.: N/A

SDG NO.: N/A

I. RECEIPT

A. Date: August 26, 1994

B. Sample Information:

LABSAMPLE ID

R8621001R8621002R8621003R8621004R8621005R8621006R8621007R8621008R8621009R8621010R8621011R8621012R8621013V0831T01-BLKV0908W01-BLK

CLIENTSAMPLE ID

TM-3ATM-3BTM-3CTM-4ATM-4BTM-4CTM-5ATM-5BTM-5CTM-6ATM-6BTM-6CMD-2V0831T01-BLKV0908W01-BLK

SAMPLEMATRIX

SOILSOILSOILSOILSOILSOILSOILSOILSOILSOILSOILSOILSOILTCLP EXTWATER

DATESAMPLED

08/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/94N/AN/A

TCLPEXTRACTION

DATE

08/31/9408/31/9408/31/9408/31/9408/31/9409/01/9409/01/9409/01/9409/01/9409/01/9409/01/9409/02/9409/02/9408/31/94

N/A

ANALYSISDATE

09/07/9409/07/9409/07/9409/07/9409/07/9409/07/9409/07/9409/07/9409/07/9409/07/9409/08/9409/08/9409/08/9409/07/9409/08/94

c. DocumentationExceptions : No exceptions were encountered.

II. EXTRACTION

A. Holding Times: All holding times were met.

B. ExtractionExceptions : No exceptions were encountered.

III. ANALYSIS


B. AnalyticalExceptions : No exceptions were encountered.

Quality AnalyticalLaboratories Inc

5090 Caterpillar Road.Redding. CA 96003-1412

916244-5227Fax No. 916244-4109

VOLATILELAB REF. NO. R8621PAGE 2

IV. QUALITY CONTROL

A. Method Blank : The associated TCLP blank and water blank metacceptance criteria.

B. SurrogateRecoveries : All surrogate recoveries met acceptance criteria.

C. Matrix SpikeResults : All spike recoveries met acceptable advisory

limits.

V. I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness,except for the conditions detailed above. Release of the data containedin this hard copy data package has been authorized by the LaboratoryManager or his designee, as verified by the following signature.

Brian Geers DateManager, Organics Division

Quality Analytical 5O90 Caterpillar Road. 9 j$ 244-5227Laboratories Inc. Redding. CA 96003-1412 Fax No. 916 244-4109

00021

ORGANIC TCLP ANALYSIS DATA SHEET

Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 08/31/94-b Sample ID: R8621001 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/07/94ient Sample ID: TM-3A Percent Moisture: Dilution Factor: 1.0

VOLATILE COMPOUNDS

MATRIX SPIKE MATRIX SPIKE DUPLICATECAS Number mq/L PERCENT RECOVERY PERCENT RECOVERY75-01-4 Vinyl chloride ...... 0.050 U 104 9275-35-4 1,1-Dichloroethene .... 0.025 U 92 8267-66-3 Chloroform ........ 0.025 U 86 76107-06-2 1,2-Dichloroethane . . . . 0.025 U 88 7878-93-3 2-Butanone . . . . . . . . 0.050 U 90 8656-23-5 Carbon tetrachloride . . . 0.025 U 94 8279-01-6 Trichloroethene . . . . . 0.025 U 96 8471-43-2 Benzene . . . . . . . . . 0.048 90 78127-18-4 Tetrachloroethene . . . . 0.025 U 94 82108-90-7 Chlorobenzene . . . . . . 0.025 U 90 76

Toluene-d8 - SS . . . . . 991,4-Bromofluorobenzene - SS 97l,2-Dichloroethane-d4 - SS 94

U - Compound analyzed for but not detected.6 - Compound was detected in QC blank.J - Reported value less than quantisation limit.

SS - Surrogate Standard reported as percent recovery.

Form I

Quality Analytical 5090 Caterpillar Road. p ;<$ 244-5227Laboratories Inc Redding. CA 96003-1412 Fax No 916244-4109

00,099


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 08/31/94Lab Sample ID: R8621002 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/07 "<Client Sample ID: TM-3B Percent Moisture: Dilution Factor: _>

VOLATILE COMPOUNDS

CAS Number mg/L CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene ..... 0.025 U71-43-2 Benzene . . . . . . . . . 0.052127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U


U - Compound analyzed for but not detected.B - Compound was detected in QC blank.J - Reported value less than quantitation limit.


Form I

Quality Analytical 5090 Caterpillar Road. 9 J6 244-5227Laboratories Inc. Redding. CA 96003-1412 * ^« ttprt ;<5 244-4109

ORGANIC TCLP ANALYSIS DATA SHEETLaboratory Name: QAL/LRD Concentration: LOW Date Extracted: 08/31/94•b Sample ID: R8621003 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/07/94

^ .ent Sample ID: TM-3C Percent Moisture: Dilution Factor: 1.0

VOLATILE COMPOUNDSCAS Number mg/L CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.058127-18-4 Tetrachloroethene .... 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U

Toluene-d8 - SS ..... 991,4-Bromofluorobenzene - SS 96l,2-Dichloroethane-d4 - SS 92



Form I

Qualify Analytical 5090 Caterpillar Road. 9 ;<5 244-5227Laboratories Inc. Redding. CA 96003-1412 fax No 916 244-4109


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 08/31/94Lab Sample ID: R8621004 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/0 "MClient Sample ID: TM-4A Percent Moisture: Dilution Factor: 0

VOLATILE COMPOUNDSCAS Number mg/L CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.130127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U


U - Compound analyzed for but not detected.B - Compound was detected in QC blank.J - Reported value less than quantitation limit.SS - Surrogate Standard reported as percent recovery.

Form I

Quality Analytical 5090 Caterpillar Road. 9 j6 244-5227Laboratories Inc. Redding, CA 05003-1412 Fax No. 916 244-4109

00025

Laboratory Name: QAL/LRDp»b Sample ID: R8621005

ent Sample ID: TM-4B


Concentration: LOWSample Matrix: TCLP EXTRACTPercent Moisture:VOLATILE COMPOUNDS

Date Extracted:Date Analyzed:Dilution Factor:

CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.054127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U


CAS Number

08/31/9409/07/94

1.0

mg/L



Form I

Qualify AnalyticalLaboratories inc


916 244-5227Fax No. 916244-4109

00026


Laboratory Name': QAL/LRD Concentration: LOW Date Extracted: 09/01/94Lab Sample ID: R8621006 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/07 '"4Client Sample ID: TM-4C Percent Moisture: Dilution Factor: _^>

VOLATILE COMPOUNDS

CAS Number mg/L CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.057127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U



Form I

Quality Analytical 5090 Caterpillar Road, 9 244-5227Laboratories Inc Redding. CA 96003-1412 Fax No. 916 244~4109

00027


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/01/94/ab Sample ID: R8621007 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/07/94

ient Sample ID: TM-5A Percent Moisture: Dilution Factor: 1.0VOLATILE COMPOUNDS

CAS Number mg/LCAS Number75-01-4 Vinyl chloride ......75-35-4 1,1-Dichloroethene . . . .67-66-3 Chloroform . . . . . . . .107-06-2 1,2-Dichloroethane . . . .78-93-3 2-Butanone ........56-23-5 Carbon tetrachloride . . .79-01-6 Trichloroethene . . . . .71-43-2 Benzene . . . . . . . . .127-18-4 Tetrachloroethene ....108-90-7 Chlorobenzene . . . . . .

mg/L0.050 U0.025 U0.025 U0.025 U0.050 U0.025 U0.025 U0.0490.025 U0.025 U



Form I

Quality Analytical 5O90 Caterpillar Road, p 14 244-5227Laboratories inc Redding. CA 96O03-1412 fax No 916 244-4109

ORGANIC TUP ANALYSIS DATA SHEET

Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/01/94Lab Sample ID: R8621008 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/07 'Client Sample ID: TM-5B Percent Moisture: Dilution Factor: ,- j

VOLATILE COMPOUNDS

CAS Number mg/L CAS Number mq/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.057127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U




Form I

Quality Analytical 5090 Caterpillar Road. 9 ;$ 244-5227Laboratories Inc. Redding. CA 96003-1412 fox NO. 916 244-4109

00029


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/01/94Ub Sample ID: R8621009 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/07/94

ient Sample ID: TM-5C Percent Moisture: Dilution Factor: 1.0VOLATILE COMPOUNDS

CAS Number mg/L CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene .... 0.025 U67-66-3 Chloroform . ....... 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.056127-18-4 Tetrachloroethene .... 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U

Toluene-d8 - SS ..... 1001,4-Bromofluorobenzene - SS 96],2-Dichloroethane-d4 - SS 91



Form I

Quality Analytical 5090 Caterpillar Road. 916244 5227Laboratories Inc. Redding. CA 96003-1412 FOX No p;6 244-4109

00050

Laboratory Name: QAL/LRDLab Sample 10: R8621010Client Sample ID: TM-6A

ORGANIC TCLP ANALYSIS DATA SHEETConcentration: LOWSample Matrix: TCLP EXTRACTPercent Moisture:

VOLATILE COMPOUNDS


CAS Number mg/L CAS Number75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.075127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U


09/01/9409/07 '4

mg/L


Form I


5090 Caterpillar Pood.Redding. CA 96003-1412 916244-5227

Fax No. 916244-4109

00031


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/01/94( \b Sample JD: R8621011 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/08/94*-lient Sample ID: TM-6B Percent Moisture: Dilution Factor: 1.0

VOLATILE COMPOUNDS

CAS Number mg/L CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.120127-18-4 Tetrachloroethene . . . . 0.025 U1D8-90-7 Chlorobenzene ...... 0.025 U

Toluene-d8 - SS ..... 961,4-Bromofluorobenzene - SS 96l,2-Dichloroethane-d4 - SS 92



Form I

Quality Analytical 5090 Caterpillar Road. 9 ;<5 244-5227Laboratories Inc. Redding. CA 96003-1412 Fax No 916244-4109

00032


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/02/94Lab Sample ID: R8621012 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/OP "4Client Sample ID: TM-6C Percent Moisture: Dilution Factor:

VOLATILE COMPOUNDS

CAS Number mg/L CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane .... 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.093127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U




Form I

Quality Analytical 5090 Caterpillar Road. p 244-5227Laboratories Inc. Redding. CA 96003- J412 Fax No. 9 \t> 244-4109

00033 /


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/02/94( b Sample ID: R8621013 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/08/94

.lent Sample ID: MD-2 Percent Moisture: Dilution Factor: 1.0

VOLATILE COMPOUNDS

CAS Number mg/L CAS Number mq/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene .... 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane .... 0.025 U78-93-3 2-Butanone ........ 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene ..... 0.025 U71-43-2 Benzene . . . . . . . . . 0.120127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene ...... 0.025 U

Toluene-d8 - SS . . ... 991,4-Bromofluorobenzene - SS 97l,2-Dichloroethane-d4 - SS 89



Form I

Quality Analytical 5090 Caterpillar Rood. y ]$ 244 $227Laboratories Inc. Redding, CA 96003-1412 fax No 916 244-4109

00034


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 08/31/94Lab Sample ID: V0831T01-BLK Sample Matrix: TCLP EXTRACT Date Analyzed: 09/07 ""•Client Sample ID: V0831T01-BLK Percent Moisture: Dilution Factor: _^j

VOLATILE COMPOUNDSCAS Number mg/L CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane .... 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.025 U127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U




Form I

Quality Analytical 5O90 Caterpillar Road. 9162445227Laboratories Inc. Redding. CA 96003-1412 Fax NO. 916 244-4109

00035

Laboratory Name: QAL/LRD'*b Sample ID: V0908W01-BLK

lent Sample ID: V0908W01-BLK


Concentration: LOWSample Matrix: WATERPercent Moisture:

VOLATILE COMPOUNDS


CAS Number mg/L75-01-4 Vinyl chloride . . . . . . 0.050 U75-35-4 1,1-Dichloroethene . . . . 0.025 U67-66-3 Chloroform . . . . . . . . 0.025 U107-06-2 1,2-Dichloroethane . . . . 0.025 U78-93-3 2-Butanone . . . . . . . . 0.050 U56-23-5 Carbon tetrachloride . . . 0.025 U79-01-6 Trichloroethene . . . . . 0.025 U71-43-2 Benzene . . . . . . . . . 0.025 U127-18-4 Tetrachloroethene . . . . 0.025 U108-90-7 Chlorobenzene . . . . . . 0.025 U

Toluene-dS - SS ..... 991,4-Bromofluorobenzene - SS 97l,2-Dichloroethane-d4 - SS 94

CAS Number

09/08/941.0

mg/L



Form I


5O90 Caterpillar Road.Redding. CA 96003-1412

916244-5227Fax No 916244-4109

CASE NARRATIVEGC/MS SEMIVOLATILE SAMPLES

LABORATORY : QAL

CASE NO. : N/A

LAB REF. NO.: R8621

CLIENT:

CONTRACT NO.:

SOG NO.:

BARR/DER

N/A

N/A

I. RECEIPT

A. Date: August 26, 1994

B. Sample Information:

LABSAMPLE ID

R8621001R8621002R8621003R8621004R8621005R8621006R8621007R8621008R8621009R8621010R8621011R8621012R8621013R0909TA1-BLK

CLIENTSAMPLE ID

TM-3ATM-3BTM-3CTM-4ATM-4BTM-4CTM-5ATM-5BTM-5CTM-6ATM-6BTM-6CMD-2R0909TA1-BLK

SAMPLEMATRIX

SOILSOILSOILSOILSOILSOILSOILSOILSOILSOILSOILSOILSOILTCLP EXT

DATESAMPLED

08/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/9408/25/94

N/A

EXTRACTIONDATE

09/09/9409/09/9409/09/9409/09/9409/09/9409/09/9409/09/9409/09/9409/09/9409/09/9409/09/9409/09/9409/09/9409/09/94

ANALYSISDATE

09/12/9409/12/9409/12/9409/12/9409/12/9409/12/9409/12/9409/12/9409/12/9409/12/9409/13/9409/13/9409/13/9409/12/94

C. DocumentationExceptions : Please note the extraction date above is the method

extraction date. The TCLP extraction was performedon 09/06/94.

II. EXTRACTION


B. ExtractionExceptions No exceptions were encountered.

III. ANALYSIS


B. AnalyticalExceptions No exceptions were encountered.

Qualrty AnalyticalLaboratories Inc.

5090 Caterpillar Road.Redding. CA 96003-1412 916244-5227

Fax No. 916 244-4109

00037

SEMIVOLATILELAB REF. NO. R862IPAGE 2

IV. QUALITY CONTROL

A. Method Blank : The associated TCLP blank met acceptance criteria.

B. SurrogateRecoveries : All surrogate recoveries met acceptance criteria.

C. Matrix SpikeResults : The MS/MSD recoveries are presented on sample

R8621001.

V. I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness,except for the conditions detailed above. Release of the data containedin this hard copy data package has been authorized by the LaboratoryManager or his designee, as verified by the following signature.

BrieTn Geers ~~ DateManager, Organics Division

Quality Analytical 5090 Caterpillar Road. 9 ;<} 244-5227Latxircftories Inc Redding. CA 96003-1412 fax NO 9 ;$ 244-4109


Laboratory Name: QAL/LRDLab Sample 10: R8621001Client Sample ID: TM-3A

Concentration: LOWSample Matrix: TCLP EXTRACTPercent Moisture:


09/09/9409/1P/94

0

CAS Number106-46-795-48-7106-44-567-72-198-95-387-68-388-06-295-95-4121-14-2118-74-187-86-5110-86-1

1,4-Dichlorobenzene .2-Methyl phenol . . . .4-Methyl phenol . . . .Hexachloroethane . . .Nitrobenzene . . . . .Hexachlorobutadiene .2,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4-Dinitrotoluene . .Hexachlorobenzene . .Pentachlorophenol . .Pyridine . . . . . . .Nitrobenzene-d5 - SS .2-Fluorobiphenyl - SSTerphenyl-dl4 - SS . .Phenol -d5 - SS . . . .2-Fluorophenol - SS .2,4,6-Tribromophenol -

SEMIVOLATILEmg/L

. . 0.050 U

. . 0.049 J

. . 0.046 J

. . 0.050 U

. . 0.050 U0.050 U0.050 U0.250 U0.050 U0.050 U0.250 U

. . 0.250 U

. . 92

. . 95

. . 100

. . 84

. . 83SS 85

COMPOUNDSMatrix Spike

Percent Recovery86938611110190931021046911461

Matrix Spike DuplicatePercent Recovery

83827789908891100878110278

UBJSS**

Compound analyzed for but not detected.Compound was detected in QC blank.Reported value less than quantitation limit.Surrogate Standard reported as percent recovery.4-Methylphenol and 3-Methylphenol coelute and arereported as a total of the individual isomers.

Form I

Qualify AnalyticalLaboratories Inc.

5090 Caterpillar Road.Redding. CA 96003-1412 916244-5227

fax No. 916 244-4109

00039

Laboratory Name:.Mb Sample ID:• ent Sample ID:


QAL/LRD Concentration: LOWR8621002 Sample Matrix: TCLP EXTRACTTM-3B Percent Moisture:

SEMIVOLATILE COMPOUNDS

Date Extracted: 09/09/94Date Analyzed: 09/12/94Dilution Factor: 1.0

CAS Number106-46-795-48-7106-44-567-72-198-95-387-68-388-06-295-95-4121-14-2118-74-187-86-5110-86-1

1,4-Dichlorobenzene .2-Methylphenol . . . .4-Methvl phenol . . . .Hexachloroethane . . .Nitrobenzene . . . . .Hexachlorobutadiene .2,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4-Dinitrotoluene . .Hexachlorobenzene . .Pentachlorophenol . .Pyridine . . . . . . .Nitrobenzene-d5 - SS .2-Fluorobiphenyl - SSTerphenyl-d]4 - SS . .Phenol -d5 - SS . . . .2-Fluorophenol - SS .2,4,6-Tribromophenol -

mg/L. . 0.050 U. . 0.046 J. . 0.041 J. . 0.050 U. . 0.050 U

0.050 U0.050 U0.250 U0.050 U0.050 U0.250 U

. . 0.250 U

. . 87

. . 88

. . 97

. . 78

. . 76SS 82

UBJSS**


Form I

Quolrty AnalyticalLaboratories Inc


916244-5227Fax No 916244-4109

00040


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/09/94Lab Sample ID: R8621003 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/1? "HClient Sample ID: TM-3C Percent Moisture: Dilution Factor:

SEMI VOLATILE COMPOUNDS

CAS Number mg/L106-46-7 1,4-Dichlorobenzene . . . 0.050 U95-48-7 2-Methylphenol . . . . . . 0.057106-44-5 4-Methylphenol . . . . . . 0.05467-72-1 Hexachloroethane . . . . . 0.050 U98-95-3 Nitrobenzene . . . . . . . 0.050 U87-68-3 Hexachlorobutadiene . 0.050 U88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol121-14-2 2,4-Dinitrotoluene .118-74-1 Hexachlorobenzene .87-86-5 Pentachlorophenol

0.050 U0.250 U0.050 U0.050 U0.250 U

110-86-1 Pyridine . . . . . . . . . 0.250 U

Nitrobenzene-d5 - SS . . . 892-Fluorobiphenyl - SS . . 91Terphenyl-dl4 - SS . . . . 83Phenol-d5 - SS . . . . . . 832-Fluorophenol - SS . . . 832,4,6-Tribromophenol - SS 90



** 4-Methylphenol and 3-Methylphenol coelute and arereported as a total of the individual isomers.

Form I

Quality Analytical 5090 Caterpillar Road. 9 ;^ 244-5227Laboratories Inc. Redding. CA 96003-1412 fax No 916 244-4109

00041

Laboratory Name: QAL/LRD;-b Sample ID: R8621004

<ent Sample ID: TM-4A





09/09/9409/12/94

1.0

CAS Number106-46-795-48-7106-44-567-72-198-95-387-68-388-06-295-95-4121-14-2118-74-187-86-5110-86-1

1,4-Dichlorobenzene .2-Methylphenol . . . .4-Methvlphenol . . . .Hexachloroethane . . .Nitrobenzene . . . . .Hexachlorobutadiene .2,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4-Dinitrotoluene . .Hexachlorobenzene . .Pentachlorophenol . .Pyridine . . . . . . .Nitrobenzene-d5 - SS .2-Fluorobiphenyl - SSTerphenyl-dl4 - SS . .Phenol -d5 - SS . . . .2-Fluorophenol - SS .2,4,6-Tribromophenol -

mg/L. . 0.050 U. . 0.064. . 0.057. . 0.050 U. . 0.050 U

0.050 U0.050 U0.250 U0.050 U0.050 U0.250 U

. . 0.250 U

. . 81

. . 89

. . 99

. . 90

. . 91SS 100


SS - Surrogate Standard reported as percent recovery.** 4-Methylphenol and 3-MethylphenoT coelute and are

reported as a total of the individual isomers.

Form I


5090 Caterpillar Road,Redding, CA 96003-1412

916244-5227Fax No 916244-4109

00042

Laboratory Name: QAL/LRDLab Sample ID: R8621005Client Sample ID: TM-4B




Date Extracted: 09/09/94Date Analyzed: 09/1 tDilution Factor:

CAS Number106-46-795-48-7106-44-567-72-198-95-387-68-388-06-295-95-4121-14-2118-74-187-86-5110-86-1

1,4-Dichlorobenzene .2-Methyl phenol . . . .4-Methyl phenol . . . .Hexachloroethane . . .Nitrobenzene . . . . .Hexachlorobutadiene .2,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4-Dinitrotoluene . .Hexachlorobenzene . .Pentachlorophenol . .Pyridine . . . . . . .Nitrobenzene-d5 - SS .2-Fluorobiphenyl - SSTerphenyl-dl4 - SS . .Phenol -d5 - SS . . . .2-Fluorophenol - SS .2,4,6-Tribromophenol -

mg/L. . 0.050 U. . 0.032 J. . 0.035 J. . 0.050-U. . 0.050 U

0.050 U0.050 U0.250 U0.050 U0.050 U0.250 U

. . 0.250 U

. . 80

. . 88

. . 92

. . 75

. . 79SS 86

U - Compound analyzed for but not detected.B - Compound was detected in QC blank.J - Reported value less than quantitation limit.SS - Surrogate Standard reported as percent recovery.** 4-Methylphenol and 3-Methylphenol coelute and are


Form I



916244-5227Fax No. 916244-4109

00043


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/09/94(' ~b Sample ID: R8621006 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/12/941 ient Sample ID: TM-4C Percent Moisture: Dilution Factor: 1.0


CAS Number mg/LJ06-46-7 1,4-Dichlorobenzene . . . 0.050 U95-48-7 2-Methylphenol . . . . . . 0.048 J106-44-5 4-Methylphenol . . . . . . 0.05067-72-1 Hexachloroethane . . . . . 0.050 U98-95-3 Nitrobenzene . . . . . . . 0.050 U87-68-3 Hexachlorobutadiene . 0.050 U-06-2 2,4,6-Trichlorophenol

95-95-4 2,4,5-Trichlorophenol121-14-2 2,4-Dinitrotoluene .118-74-1 Hexachlorobenzene .87-86-5 Pentachlorophenol

0.050 U0.250 U0.050 U0.050 U0.250 U

110-86-1 Pyridine . . . . . . . . . 0.250 UNitrobenzene-d5 - SS . . . 972-Fluorobiphenyl - SS . . 110Terphenyl-dl4 - SS . . . . 120Phenol-d5 - SS . . . . . . 932-Fluorophenol - SS . . . 952,4,6-Tribromophenol - SS 100


SS - Surrogate Standard reported as percent recovery.** 4-Methylphenol and 3-Methy?phenol coelute and are


Form I

Quality Analytical 5090 Caterpillar Road, 9 ;<j 244-5227Laboratories Inc. Redding. CA 96003-1412 fo* No 916 244-4109

00044


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/09/94Lab Sample ID: R8621007 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/1? ">4Client Sample ID: TM-5A Percent Moisture: Dilution Factor: 1

SEMI VOLATILE COMPOUNDS

CAS Number mg/L106-46-7 1,4-Dichlorobenzene . . . 0.050 U95-48-7 2-Methylphenol . . . . . . 0.016 J106-44-5 4-Methylphenol . . . . . . 0.050 U67-72-1 Hexachloroethane . . . . . 0.050 U98-95-3 Nitrobenzene . . . . . . . 0.050 U87-68-3 Hexachlorobutadiene . . . 0.050 U88-06-2 2,4,6-Trichlorophenol . . 0.050 U95-95-4 2,4,5-Trichlorophenol . . 0.250 U121-14-2 2,4-Dinitrotoluene . . . . 0.050 U118-74-1 Hexachlorobenzene . . . . 0.050 U87-86-5 Pentachlorophenol . . . . 0.250 U110-86-1 Pyridine . . . . . . . . . 0.250 U



SS - Surrogate Standard reported as percent recovery.** 4-Methylphenol and 3-Methylphenol coelute and are


Form I

Quality Analytical 5O90 Caterpillar Road. 91$ 244-5227Laboratories Inc. Redding. CA 96003-1412 fax No. 916 244-4109

00045 /,/


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/09/94Jab Sample ID: R8621008 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/12/94I 'ient Sample ID: TM-5B Percent Moisture: Dilution Factor: 1.0


CAS Number mg/L106-46-7 1,4-Dichlorobenzene . . . 0.050 U95-48-7 2-Methylphenol . . . . . . 0.015 J106-44-5 4-Methylphenol . . . . . . 0.050 U67-72-1 Hexachloroethane . . . . . 0.050 U98-95-3 Nitrobenzene . . . . . . . 0.050 U87-68-3 Hexachlorobutadiene . 0.050 U88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol121-14-2 2,4-Dinitrotoluene .118-74-1 Hexachlorobenzene .87-86-5 Pentachlorophenol

0.050 U0.250 U0.050 U0.050 U0.250 U

110-86-1 Pyridine . . . . . . . . . 0.250 U





Form I

Quality Analytical 5090 Caterpillar Road. p ;<5 244-5227Laboratories Inc Redding. CA 96003-1412 Fax No 916244-4109

00046 ,

Laboratory Name: QAL/LRDLab Sample ID: R8621009Client Sample ID: TM-5C





09/09/9409/1' 4

CAS Number mg/L106-46-7 1,4-Dichlorobenzene . . . 0.050 U95-48-7 2-Methylphenol . . . . . . 0.017 J106-44-5 4-Methylphenol . . . . . . 0.050 U67-72-1 Hexachloroethane . . . . . 0.050 U98-95-3 Nitrobenzene . . . . . . . 0.050 U87-68-3 Hexachlorobutadiene . . . 0.050 U88-06-2 2,4,6-Trichlorophenol . . 0.050 U95-95-4 2,4,5-Trichlorophenol . . 0.250 U121-14-2 2,4-Dinitrotoluene . . . . 0.050 U118-74-1 Hexachlorobenzene . . . . 0.050 U87-86-5 Pentachlorophenol . . . . 0.250 U110-86-1 Pyridine . . . . . . . . . 0.250 U

Nitrobenzene-d5 - SS . . . 942-Fluorobiphenyl - SS . . 91Terphenyl-d!4 - SS . . . . 84Phenol-d5 - SS . . . . . . 682-Fluorophenol - SS . . . 612,4,6-Tribromophenol - SS 75

U - Compound analyzed for but not detected.B - Compound was detected in QC blank.J - Reported value less than quantitation limit.SS - Surrogate Standard reported as percent recovery.** 4-Methylphenol and 3-Methylphenol coelute and are


Form I



916244-5227Fax No. 916244-4109

00047

Laboratory Name: QAL/LRD/-b Sample ID: R8621010

•ent Sample ID: TM-6A




Date Extracted: 09/09/94Date Analyzed: 09/12/94Dilution Factor: J.O

CAS Number106-46-795-48-7106-44-567-72-198-95-387-68-388-06-295-95-4121-14-2118-74-187-86-5110-86-1

1,4-Dichlorobenzene .2-Methylphenol . . . .4-Methvlphenol . . . .Hexachloroethane . . .Nitrobenzene . . . . .Hexachlorobutadiene .2,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4-Dinitrotoluene . .Hexachlorobenzene . .Pentachlorophenol . .Pyridine . . . . . . .Nitrobenzene-d5 - SS .2-Fluorobiphenyl - SSTerphenyl-dl4 - SS . .Phenol -d5 - SS . . . .2-Fluorophenol - SS .2,4,6-Tribromophenol -

mg/L. . 0.050 U. . 0.022 J. . 0.025 J. . 0.050 U. . 0.050 U

0.050 U0.050 U0.250 U0.050 U0.050 U0.250 U

. . 0.250 U

. . 93

. . 88

. . 83

. . 79

. . 77SS 79

UBJSS•**


Form I


5090 Caterpillar Road.Redding, CA 96003-1412

916244-5227Fax No 916244-4109

00048


Laboratory Name:Lab Sample ID:Client Sample ID:

QAL/LRDR8621011TM-6B




09/09/9409/1' 1

CAS Number106-46-795-48-7106-44-567-72-198-95-387-68-388-06-295-95-4121-14-2118-74-187-86-5110-86-1

mg/L0.050 U0.020 J0.019 J

1,4-Dichlorobenzene . .2-Methylphenol . . . . .4-Methylphenol . . . . .Hexachloroethane . . . . . 0.050 UNitrobenzene . . . . . . . 0.050 UHexachlorobutadiene . . . 0.050 U2,4,6-Trichlorophenol . . 0.050 U2,4,5-Trichlorophenol . . 0.250 U2,4-Dinitrotoluene . . . . 0.050 UHexachlorobenzene . . . . 0.050 UPentachlorophenol . . . . 0.250 UPyridine . . . . . . . . . 0.250 U


U - Compound analyzed for but not detected.B - Compound was detected in QC blank.J - Reported value less than quantitation lim i t .



Form I


5090 Caterpillar Road.Redding. CA 96003-1412 Fax

916244-5227916244-410916244-4)49

Laboratory Name: QAL/LRD»b Sample ID: R8621012lent Sample ID: TM-6C





CAS Number106-46-795-48-7106-44-567-72-198-95-387-68-388-06-295-95-4121-14-2118-74-187-86-5110-86-1

1,4-Dichlorobenzene .2-Methyl phenol . . . .4-Methvlphenol ....Hexachloroethane . . .Nitrobenzene . . . . .Hexachlorobutadiene .2,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4-Dinitrotoluene . .Hexachlorobenzene . .Pentachlorophenol . .Pyridine . . . . . . .Nitrobenzene-d5 - SS .2-Fluorobiphenyl - SSTerphenyl-dl4 - SS . .Phenol -d5 - SS . . . .2-Fluorophenol - SS .2,4,6-Tribromophenol -

mg/L. . 0.050 U. . 0.020 J. . 0.020 J. . 0.050 U. . 0.050 U

0.050 U0.050 U0.250 U0.050 U0.050 U0.250 U

. . 0.250 U

. . 95

. . 89

. . 88

. . 83

. . 80SS 84

UBJSS**


Form I


5O90 Caterpillar Road.Redding. CA 96003-1412

916244-5227Fax No 916244-4109

00050/1/, A


Laboratory Name: QAL/LRD Concentration: LOW Date Extracted: 09/09/94Lab Sample ID: R8621013 Sample Matrix: TCLP EXTRACT Date Analyzed: 09/1 4Client Sample ID: MD-2 Percent Moisture: Dilution Factor: —.0


CAS Number mq/L106-46-7 1,4-Dichlorobenzene . . . 0.050 U95-48-7 2-Methylphenol . . . . . . 0.020 J106-44-5 4-Methylphenol . . . . . . 0.050 U67-72-1 Hexachloroethane . . . . . 0.050 U98-95-3 Nitrobenzene . . . . . . . 0.050 U87-68-3 Hexachlorobutadiene . . . 0.050 U88-06-2 2,4,6-Trichlorophenol . . 0.050 U95-95-4 2,4,5-Trichlorophenol . . 0.250 U121-14-2 2,4-Dinitrotoluene . . . . 0.050 U118-74-1 Hexachlorobenzene . . . . 0.050 U87-86-5 Pentachlorophenol . . . . 0.250 U110-86-1 Pyridine . . . . . . . . . 0.250 U


U - Compound analyzed for but not detected.B - Compound was detected in QC blank. _J - Reported value less than quantitation limit.


** 4-Methylphenol and 3-Methylphenol coelute and arereported as a total of the individual isomers.

Form I

Quality Analytical 5090 Caterpillar Road. 9 7$ 244-5227Laboratories Inc. Redding. CA 96O03-1412 Fax No. 916 244-4109

00051

Laboratory Name:Lab Sample ID:

lent Sample ID:QAL/LRDR0909TAJ-BLKR0909TA1-BLK





CAS Number106-46-795-48-7106-44-567-72-198-95-387-68-388-06-295-95-4121-14-2118-74-187-86-5110-86-1

1,4-Dichlorobenzene .2-Methylphenol . . . .4-Methylphenol ....Hexachloroethane . . .Nitrobenzene .....Hexachlorobutadiene .2,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4-Dinitrotoluene . .Hexachlorobenzene . .Pentachlorophenol . .Pyridine . . . . . . .Nitrobenzene-d5 - SS .2-Fluorobiphenyl - SSTerphenyl-dl4 - SS . .Phenol -d5 - SS . . . .2-Fluorophenol - SS .2,4,6-Tribromophenol -

mg/L. . 0.050 U. . 0.050 U. . 0.050 U. . 0.050 U. . 0.050 U

0.050 U0.050 U0.250 U0.050 U0.050 U0.250 U

. . 0.250 U

. . 79

. . 83

. . 100

. . 82

. . 88SS 85

UBJSS**

Compound analyzed for but not detected.Compound was detected in QC blank.Reported value less than quantisation limit.Surrogate Standard reported as percent recovery.4-Methylphenol and 3-Methylphenol coelute and arereported as a total of the individual isomers.

Form I

Qualify AnalyticalLaboratories Inc


916244-5227Fax No. 916244-4109

00052 „

b'SOOO

\>m\

ID

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. * ,

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x x

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(612) 832-2600

Drivt

437-10

32a*•a.a

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Analyses R

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No. of VOC Containers

iNo. of Non-VOC ContainersNo. of Brass Liners

vu Total No. Of Containers

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CH2M HILLSAMPLE RECEIPT EXCEPTION REPORTSample Bate h Number Client/Project -yG

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—————— , — ... , , _ ._ ——

1 . No custody seal as required by project.

2. No chain-of-custody provided.

3. Analysis, description, date of collectionnot provided.

4. Samples broken or leaking on receipt.

5. Temperature of samples inappropriatefor analysis requested.

6. Container inappropriate foranalysis requested.

7. Inadequate sample volume._

8. Preservation inappropriate foranalysis requested.

9. Samples received out of holding timeor analysis requested.

10. Discrepancies between COC formand container labels.

1 1 . Other

Comments:

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Corrective Actions Taken:

00054

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