john.e^ayres^^ 'joseph d. guertin; jr. goldberg •zoino ... · silresim site trustees -march...
TRANSCRIPT
V iniraquo mmjjouTntnmdashw
gt rDONALD -TVGOLDL WILUAM S ZOINO
bullJOSEPH D GUERTIN JRpound shy JOHNE^AYRES^^ MATTHEW JBARVENIKr-
WILUAM R BELOFFNICHOLAS A CAMPAGNA JR
GOLDBERG bullZOINO amp ASSOCIATES INC MATHEW A DIPILATO LAWRENCE FELDMAN
GEOTECHNICAL-GEOHYDRDLOGICAL CONSULTANTS JOSEPH P HEHIR ROBERT A-HELLER ROSS T McGILUVRAY MICHAEL A POWERS JAMES H REYNOLDS PAUL M SANBORN RICHARD M SIMON STEVEN J TRETTEL
CONSULTANTS WALTER E JAWORSKI STANLEY M BEMBEN
March 10 1986 File No A405404-CPC
Silresim Site Trustees Post Office Box 169 Acton Massachusetts 01720
Attention Mr James Rogers
Re Analytical Data Sampling Round
- Initial
Gentlemen
Attached please find a copy of the laboratory report from the initial round of groundwater samples at the Silresim site The samples were collected on December 4 1985 from the existing monitoring wells at the site installed by Perkins Jordan Inc in 1981 and 1982 A list of samples submitted for laboratory analysis including QAQC samples is attached asTable 1
I t i s n o t e d t h a t p e s t i c i d e s P C B s a n d 2 3 7 8 Tetrachlorodibenzo-p-dioxin (TCDD) wernot detected in any samples analyzed With only a few exceptions priority pollutant metals were not found in significant concentrations in the groundwater samples Low levels (8-170 ug1) of acid extractable organic compounds were found in two of the five monitoring wells tested Base neutral extractables were found at trace levels in most samples with elevated concentrations (up to 1900 ug1) in two monitoring wells
Results of volatile organic compound (VOC) analyses are generally consistant with previous data from the site Elevated levels of VOCs were found at wells MW-102B and MW-101A locations that
previously showed high concentrations MW-105A exhibited VOC concentrations substantially higher than any previously reported levels at that location VOC concentrations at wells MW-102A and MW-105B were similar to past data from these locations
T r a c e l e v e l s o f m e t h y l e n e c h l o r i d e w e r e f o u n d i n l a b o r a t o r y f i e l d s a m p l e r a n d t r i p b l a n k s a n d a d d i t i o n a l V O C s (chloroform 111 trichloroethane acetone and 2-butanone) were f o u n d a t c o n c e n t r a t i o n s r a n g i n g f r o m 3 t o 1 3 u g 1 i n t h e f i e l d
THE GEO BUILDING 320NEEDHAM STREETbull NEWTON UPPER FALLSMASSACHUSETTS 02164 (617) 969-0050 BUFFALONYbullBRIDGEPORTCTbullVERNONCTbull MANCHESTERNHbullPROVIDENCE RlbullTAMPAFL
AN EQUAL OPPORTUNITY EMPLOYER
Silresim Site Trustees - March 10 1986 File No A-405404 Page 2
and sampler blanks It is noted that both of these blanks were generated during sampling of MW-102B a location exhibiting eleyated levels of the same VOCs observed in the blanks this is believed to represent a worst case scenario with respect to potential sample cross contaminationby VOCs The contaminants found in the laboratory and trip blanks were notated within Westons Laboratory report additional VOCs found in field and sampler blanks will be similarly qualified in data entered into GZAs Data Base Management System
As noted in Westonscover letter sample aliquots for the baseneutral extractable pesticidePCB and TCDD fractions of well MW-105B were spiked with the standard spike mixture used by EPAs Contract Laboratory program - An unspiked aliquot of the sample was not analyzed however due to miscommunication between GZA and the laboratory Well MW-105B will therefore be resampled during the next scheduled groundwater sampling round and analyzed for the appropriate parameters
S h o u l d y o u h a v e a n y q u e s t i o n s o n t h e d a t a o r r e q u i r e a n y additional information please feel free to call
Very truly yours
GOLDBERG-ZOINO amp ASSOCIATES INC
2 Lawrence Feldmen
LFevm
GZ
1 Silresim Site Trustees - March 10 1986 - File No A-405404
Page 3
TABLE 1
SAMPLE INVENTORY (DECEMBER 4 1985)
GZA Sample ID No (Weston Sample Description)
StationSampleDescription
SCC-GWS-B-105A Well MW-105A
SCC-GWS-B-105B Well MW-105B
SCC-GWS-B-102A Well MW-102A
SCC-GWS-B-102B Well MW-102B
SCC-GWS-B-001A Well MW-102A (Blind Duplicate)
SCC-QAC-SB-001 Sampler Blank (Bailer)
SCC-QAC-FB-001 Filtration SystemBlank
SCC-QACmdashTB-001 Field Blank
SCC-GWS-B-101A Well MW-101A
GZ
28 February 1986
Mr Charles Lindberg Goldberg Zoina and Assoc The GEO Building 320 Needham Street Newton Upper Falls MA 02164
Dear Mr Lindberg
Please note the following items regarding our data reports of January 27 (metals VOAs and BNAs) and January 28 (TCDD)
1 The reported target compounds for VOA and BNA analyses were priority pollutants Since HSLs are needed we searched the original data for the additional analytes and have attached revised reports (Attachment I)
2 The EPA data qualifier B for target analytes detected in the laboratory blank has been added to the report forms where appropriate It is noted that the only targets present in the laboratory blanks were methylene chloride in the VOA blank and bisshy(2-ethylhexyl)phthalate in the BNA blank The blank levels of both these analytes was below the CLP Conshy tract Required Detection Limit
3 Attachment II is a revised TCDD data report on which the surrogate recoveries have been corrected to reflect the observed inconsistency between levels in the calibration standard received from the EPA and the surrogate spiking solution made up in our laborashy tory from neat compounds Also attached is a copy of the laboratory work sheet on which relevant calcushy lations were made and the mass chromatograms
4 Attachment III is the TCDD data report form for the re-extracted samples B-101A and B-102B Re-extracshytion and analyses were performed because of the very high recoveries obtained from the original analysis of these samples More reasonable recoveries were obtained in the re-analysis
5 BNA and TCDD fractions for sample B-105B were spiked with the CLP BNA matrix spike mix and 2378 TCDD respectively Unspiked sample was not analyzed for these parameters due to a miscommunication between GZA and WESTON Laboratory
6 Zinc was found in the method blank at a concentration of 0030 mgL This concentration is consistent with previous determinations of zinc in the laboratory water Certified ultra-pure reagents are used for digestion so that the reagents should not be a source of contamination A method blank is prepared by using an aliquot of laboratory water equivalent to the quantity of sample that is used in the analyses Any contamination in the laboratory water would then be observed on analysis of the method blank However when processing samples minimal amounts of laboratory water are used and any contributions from contaminatedlaboratory water should be much less than 10 of the concentration Consequently contrishy butions from laboratory water should be less than 0003 mgL and concentrations of zinc determined in the samples should be representative of the actual concentrations in the samples
7 Both the computer data base and the original notebook entries have been reviewed for accurate transcription of data for the manganese results The notebook and data base agree Sample 8512-327mdash0030(SCCmdashGWS-B-102A) was diluted by a factor of 10 at the instrument in order for the response to fall within the calibrated range of the instrument Sample 8512-327-0050(SCCshyGWSmdashB-001A) was diluted by a factor of 100 The result obtained for sample 0050 can be verified since this sample was also replicated and spiked The results for the replicate and spike are comparable to the initial result (the spike level was significantly less than the concentration in the sample)
If you have any questions please call me at (215) 524-0180
Very Truly Yours
ROY F WESTON INC
V1
Carter P Nulton PhD Organics Section Manager WESTON Analytical Laboratories
CPNrost
A
RFWSN
8512-327-0010 -0020 -0030 -0040
- -0050 -0050 Dup-0060 -0070 -0090
-0050
Date of Report January 28 1986
GOLDBERG ZOINO AND ASSOCIATES SUMMARY REPORT
FOR SAMPLES RECEIVED DECEMBER 5 1985
Concentration (mgL)
SAMPLE DESCRIPTION A1 Be Ba Ca Sr
SCC-GWS-B-105A lt 0 0 2 SCC-GWS-B-105B lt 0 0 2 SCC-GWS-B-102A lt 0 0 2
lt 0 0 2 lt01 743 1SCC-GWS-B-102B lt05 145 SCC-GWS-B-001A lt 0 0 2 Laboratory Duplicate lt 0 0 2 SCC-QAC-SB-001 lt 0 0 2 SCC-QAC-FB-001 lt 0 0 2 SCC-GWS-B-101A lt 0 0 2 Laboratory Blank lt05 lt 0 0 2 lt01 lt0005 lt005 Blank Spike mdash 100
Rec
Blank Spike Dup mdash 100 Rec
Matrix Spike 100 Rec
Earl M Hansen PhD Manager r
WESTON Analytical Laboratories
D A T S T U n - O r A y T I T N T GO D y E R O - v P [ A O a A A A O r - T f E A D A T A A bull bull y K i P P A K P F M T A A A T L A T A U [ T ) P E - p A T A A A A T F R 0 0 P 0 P - A V
) A1E A A A R A A 0I bull A A TEDiA -bull A - A A A |v| p ( [)| f f y n p y [ iM APATJ A
0 0 i A GP GA F P h g HGL iG7 AG i G G 1 A G L
E F U S N G E 3 C R 1 P T r U N
A A i 2-3 A )0 P 0 S0 A-G A A B bull- P 0A A ( bdquo 0 P 0 bdquo 06 I P A 0 A P -A) 10 A bdquo C P 76 j02XP AIAAGUIH mdashLi POAL OOAO S C C -G3U-B -bull 102A
i A A1 Pbdquo0pO
bull UO P bdquo 0 P 0
y [M-AP bdquoOOA
y y )P p OPO lt0 bdquo 02
P A 4 0A6
00 40 () ( ) A ()
OAP
A A f AUA -B- P 0A la A A C G 11 A-B bullbullbullbull 0 0 -i A
A T IPIx Ap 11ltE
lt bdquo 0 P 0 lt bdquo 0 i 0
069
lt bdquo 0 P ( ) lt bdquo 0 P 0
0 A 4
lt 0 0 A lt 0 0 5 0 0 6
- 0 1A P bdquo 0 P 0
bdquo 2i0
P 0 bdquo 02 lt () n gt)2
bdquo P49
7 AO 067 bdquo P A R
OAK SPIKE REGQUERY PSAX A3 bdquo AX -120 P0S7 74 5 9 P bdquo 0 0 0 A IP 005 A
R IPPL IC A I IP PR IPCISIGN
lt bdquo 0 P 0 NC
lt bdquo 0 P ( ) NC
lt bdquo 0 0 A NC
lt 0 P 0 AC
P 0 OP NC
bdquo 060 - P bdquo OPA
0() 4 () pC C bullbullbullbull A C-bull AB -OOP p bdquo 0 P 0 lt 0 P 0 lt 0 05 P bdquo 0 P 0 bdquo 032 bdquo 0 47 ( )070 () ( ) 9 ()
A CC- Q A CFB ()( ) - j A A A G W A B- P 0 P A
I1 IP TL ILiD B ANK
lt bdquo ( ) p ( ) lt bdquo 0 P 0 lt bdquo 0 P 0
lt 0 p 0 bdquo 0 2 4
lt 0i0
lt bdquo 0 0 A lt bdquo ( ) ( ) A lt bdquo 0 0 A
lt 0 P 0 ( ) -1 ( )
lt bdquo 0 P 0
lt 00 2 () ()
lt 0 bdquo 0 2
bdquo P24 Pi5bdquo 0
lt bdquo0 0 IT IP lL IOD SPIKE 063 023 bdquo 00A 304 bdquo P A3 4 4 4
Ap L K IP RIPCOOIPIPY P26 PPB 4 4 4 P027 7 6 0 P P4 NETHOP Bp TRIP
Ap IGF kFCOOFRY 066 P33
020 -104
00 A P P67
bdquo2P2 106
PA7 y iv v
bdquo P P P P P P
K PIN NA HI PB AlP SIP PIG7L PiGL tPGL PIG 71 PiGL PIGAL PIGL
R F W S N DIPS ORIP TIUN
P 2 -bull - bull 00 P 0 -0020 -0030 bullbullbullbull0040 - O O A O
ACC-GIJS-H- TOAA AAC-GUS-B --10AP ACC-GAl j -P- p 02A SCC--GUS-B - P 02B ACC-GUA-F-GOPA
4 bdquo A 9 bdquo 2 P9 bdquo P90 P 2 bdquo 3 P bdquo 3 P
lt bdquo P 0 lt bdquo P 0 lt bdquo PC bull P6(lt bdquo - i 0
lt bdquo 00 A P bdquo 005 lt ( oA lt bdquo00b lt bdquo 00 A
lt bdquo 060 lt 060 lt bdquo 060 lt bdquo 060 ( bdquo 0 6()
lt 00A lt 005 lt bdquo O f ) A
lt00A lt 00A
-00 AG -7) OAK
PI AIRIX ART KIP AP TKIP RECGUERY
430V7 c7
bdquo 0 P (J bdquo P P 3 P P2
bdquo 009 9 P bdquo 0
-00A Pi A TRIX AP TKE P bdquo 46 -00Al APIKIP RECGUERY AO ( ) -00AR -00AS
REPLICATE P R E C I A T O N
P bdquo 06 2 -i bdquo 4 OP
lt bdquo P 0 NO
lt bdquo 005 NC
bdquo Jo-J NC
lt 00A NC
-bull006()-0070 -0090
A C C -bull0 A A -PiR -00 P A G0-0 A 0bull-FB-00 P ACC--GU0-B- PC PA
NET LIOA B LANLP PIETHOD APIKiP
lt bdquo 0 P A lt 0 P A
P 0 bdquo 4 lt 0 P 5
bdquo 4 4 4
lt bdquo P 0 lt P 0 PAO lt bdquo PO bdquo 4 10
lt 005 lt bdquo 005 lt 005
lt 060 lt bdquo06()lt bdquo06()lt bdquo 060
bdquo P 07
lt 00b P bdquo 005 P bdquo 005 P 005
() (bull V ApIKE RECnUEKY P P4 P 03 P 077 9 9 o 0
PIETHOD SPIKE SPIKE REOOUERY
PIETHOD APIKIP
bdquo P22 i P2
420 P OA 2
P PS P P 57
bdquo 0 P P P P 27 bdquo 0 P 0
SPIKE KEOOUFRY P 02
DB- G- I 0
jvj f p r n w
- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4
0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A
0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B
lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O
SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037
B P T K F R E C O V E R Y AS 4 A
R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL
-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii
OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l
RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN
gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03
NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL
Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL
9 bull v bullbullbull8PIKE RFC GOER Y
RFUBN DESCRIPTION 8ULFIDE
8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A
PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
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lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
Silresim Site Trustees - March 10 1986 File No A-405404 Page 2
and sampler blanks It is noted that both of these blanks were generated during sampling of MW-102B a location exhibiting eleyated levels of the same VOCs observed in the blanks this is believed to represent a worst case scenario with respect to potential sample cross contaminationby VOCs The contaminants found in the laboratory and trip blanks were notated within Westons Laboratory report additional VOCs found in field and sampler blanks will be similarly qualified in data entered into GZAs Data Base Management System
As noted in Westonscover letter sample aliquots for the baseneutral extractable pesticidePCB and TCDD fractions of well MW-105B were spiked with the standard spike mixture used by EPAs Contract Laboratory program - An unspiked aliquot of the sample was not analyzed however due to miscommunication between GZA and the laboratory Well MW-105B will therefore be resampled during the next scheduled groundwater sampling round and analyzed for the appropriate parameters
S h o u l d y o u h a v e a n y q u e s t i o n s o n t h e d a t a o r r e q u i r e a n y additional information please feel free to call
Very truly yours
GOLDBERG-ZOINO amp ASSOCIATES INC
2 Lawrence Feldmen
LFevm
GZ
1 Silresim Site Trustees - March 10 1986 - File No A-405404
Page 3
TABLE 1
SAMPLE INVENTORY (DECEMBER 4 1985)
GZA Sample ID No (Weston Sample Description)
StationSampleDescription
SCC-GWS-B-105A Well MW-105A
SCC-GWS-B-105B Well MW-105B
SCC-GWS-B-102A Well MW-102A
SCC-GWS-B-102B Well MW-102B
SCC-GWS-B-001A Well MW-102A (Blind Duplicate)
SCC-QAC-SB-001 Sampler Blank (Bailer)
SCC-QAC-FB-001 Filtration SystemBlank
SCC-QACmdashTB-001 Field Blank
SCC-GWS-B-101A Well MW-101A
GZ
28 February 1986
Mr Charles Lindberg Goldberg Zoina and Assoc The GEO Building 320 Needham Street Newton Upper Falls MA 02164
Dear Mr Lindberg
Please note the following items regarding our data reports of January 27 (metals VOAs and BNAs) and January 28 (TCDD)
1 The reported target compounds for VOA and BNA analyses were priority pollutants Since HSLs are needed we searched the original data for the additional analytes and have attached revised reports (Attachment I)
2 The EPA data qualifier B for target analytes detected in the laboratory blank has been added to the report forms where appropriate It is noted that the only targets present in the laboratory blanks were methylene chloride in the VOA blank and bisshy(2-ethylhexyl)phthalate in the BNA blank The blank levels of both these analytes was below the CLP Conshy tract Required Detection Limit
3 Attachment II is a revised TCDD data report on which the surrogate recoveries have been corrected to reflect the observed inconsistency between levels in the calibration standard received from the EPA and the surrogate spiking solution made up in our laborashy tory from neat compounds Also attached is a copy of the laboratory work sheet on which relevant calcushy lations were made and the mass chromatograms
4 Attachment III is the TCDD data report form for the re-extracted samples B-101A and B-102B Re-extracshytion and analyses were performed because of the very high recoveries obtained from the original analysis of these samples More reasonable recoveries were obtained in the re-analysis
5 BNA and TCDD fractions for sample B-105B were spiked with the CLP BNA matrix spike mix and 2378 TCDD respectively Unspiked sample was not analyzed for these parameters due to a miscommunication between GZA and WESTON Laboratory
6 Zinc was found in the method blank at a concentration of 0030 mgL This concentration is consistent with previous determinations of zinc in the laboratory water Certified ultra-pure reagents are used for digestion so that the reagents should not be a source of contamination A method blank is prepared by using an aliquot of laboratory water equivalent to the quantity of sample that is used in the analyses Any contamination in the laboratory water would then be observed on analysis of the method blank However when processing samples minimal amounts of laboratory water are used and any contributions from contaminatedlaboratory water should be much less than 10 of the concentration Consequently contrishy butions from laboratory water should be less than 0003 mgL and concentrations of zinc determined in the samples should be representative of the actual concentrations in the samples
7 Both the computer data base and the original notebook entries have been reviewed for accurate transcription of data for the manganese results The notebook and data base agree Sample 8512-327mdash0030(SCCmdashGWS-B-102A) was diluted by a factor of 10 at the instrument in order for the response to fall within the calibrated range of the instrument Sample 8512-327-0050(SCCshyGWSmdashB-001A) was diluted by a factor of 100 The result obtained for sample 0050 can be verified since this sample was also replicated and spiked The results for the replicate and spike are comparable to the initial result (the spike level was significantly less than the concentration in the sample)
If you have any questions please call me at (215) 524-0180
Very Truly Yours
ROY F WESTON INC
V1
Carter P Nulton PhD Organics Section Manager WESTON Analytical Laboratories
CPNrost
A
RFWSN
8512-327-0010 -0020 -0030 -0040
- -0050 -0050 Dup-0060 -0070 -0090
-0050
Date of Report January 28 1986
GOLDBERG ZOINO AND ASSOCIATES SUMMARY REPORT
FOR SAMPLES RECEIVED DECEMBER 5 1985
Concentration (mgL)
SAMPLE DESCRIPTION A1 Be Ba Ca Sr
SCC-GWS-B-105A lt 0 0 2 SCC-GWS-B-105B lt 0 0 2 SCC-GWS-B-102A lt 0 0 2
lt 0 0 2 lt01 743 1SCC-GWS-B-102B lt05 145 SCC-GWS-B-001A lt 0 0 2 Laboratory Duplicate lt 0 0 2 SCC-QAC-SB-001 lt 0 0 2 SCC-QAC-FB-001 lt 0 0 2 SCC-GWS-B-101A lt 0 0 2 Laboratory Blank lt05 lt 0 0 2 lt01 lt0005 lt005 Blank Spike mdash 100
Rec
Blank Spike Dup mdash 100 Rec
Matrix Spike 100 Rec
Earl M Hansen PhD Manager r
WESTON Analytical Laboratories
D A T S T U n - O r A y T I T N T GO D y E R O - v P [ A O a A A A O r - T f E A D A T A A bull bull y K i P P A K P F M T A A A T L A T A U [ T ) P E - p A T A A A A T F R 0 0 P 0 P - A V
) A1E A A A R A A 0I bull A A TEDiA -bull A - A A A |v| p ( [)| f f y n p y [ iM APATJ A
0 0 i A GP GA F P h g HGL iG7 AG i G G 1 A G L
E F U S N G E 3 C R 1 P T r U N
A A i 2-3 A )0 P 0 S0 A-G A A B bull- P 0A A ( bdquo 0 P 0 bdquo 06 I P A 0 A P -A) 10 A bdquo C P 76 j02XP AIAAGUIH mdashLi POAL OOAO S C C -G3U-B -bull 102A
i A A1 Pbdquo0pO
bull UO P bdquo 0 P 0
y [M-AP bdquoOOA
y y )P p OPO lt0 bdquo 02
P A 4 0A6
00 40 () ( ) A ()
OAP
A A f AUA -B- P 0A la A A C G 11 A-B bullbullbullbull 0 0 -i A
A T IPIx Ap 11ltE
lt bdquo 0 P 0 lt bdquo 0 i 0
069
lt bdquo 0 P ( ) lt bdquo 0 P 0
0 A 4
lt 0 0 A lt 0 0 5 0 0 6
- 0 1A P bdquo 0 P 0
bdquo 2i0
P 0 bdquo 02 lt () n gt)2
bdquo P49
7 AO 067 bdquo P A R
OAK SPIKE REGQUERY PSAX A3 bdquo AX -120 P0S7 74 5 9 P bdquo 0 0 0 A IP 005 A
R IPPL IC A I IP PR IPCISIGN
lt bdquo 0 P 0 NC
lt bdquo 0 P ( ) NC
lt bdquo 0 0 A NC
lt 0 P 0 AC
P 0 OP NC
bdquo 060 - P bdquo OPA
0() 4 () pC C bullbullbullbull A C-bull AB -OOP p bdquo 0 P 0 lt 0 P 0 lt 0 05 P bdquo 0 P 0 bdquo 032 bdquo 0 47 ( )070 () ( ) 9 ()
A CC- Q A CFB ()( ) - j A A A G W A B- P 0 P A
I1 IP TL ILiD B ANK
lt bdquo ( ) p ( ) lt bdquo 0 P 0 lt bdquo 0 P 0
lt 0 p 0 bdquo 0 2 4
lt 0i0
lt bdquo 0 0 A lt bdquo ( ) ( ) A lt bdquo 0 0 A
lt 0 P 0 ( ) -1 ( )
lt bdquo 0 P 0
lt 00 2 () ()
lt 0 bdquo 0 2
bdquo P24 Pi5bdquo 0
lt bdquo0 0 IT IP lL IOD SPIKE 063 023 bdquo 00A 304 bdquo P A3 4 4 4
Ap L K IP RIPCOOIPIPY P26 PPB 4 4 4 P027 7 6 0 P P4 NETHOP Bp TRIP
Ap IGF kFCOOFRY 066 P33
020 -104
00 A P P67
bdquo2P2 106
PA7 y iv v
bdquo P P P P P P
K PIN NA HI PB AlP SIP PIG7L PiGL tPGL PIG 71 PiGL PIGAL PIGL
R F W S N DIPS ORIP TIUN
P 2 -bull - bull 00 P 0 -0020 -0030 bullbullbullbull0040 - O O A O
ACC-GIJS-H- TOAA AAC-GUS-B --10AP ACC-GAl j -P- p 02A SCC--GUS-B - P 02B ACC-GUA-F-GOPA
4 bdquo A 9 bdquo 2 P9 bdquo P90 P 2 bdquo 3 P bdquo 3 P
lt bdquo P 0 lt bdquo P 0 lt bdquo PC bull P6(lt bdquo - i 0
lt bdquo 00 A P bdquo 005 lt ( oA lt bdquo00b lt bdquo 00 A
lt bdquo 060 lt 060 lt bdquo 060 lt bdquo 060 ( bdquo 0 6()
lt 00A lt 005 lt bdquo O f ) A
lt00A lt 00A
-00 AG -7) OAK
PI AIRIX ART KIP AP TKIP RECGUERY
430V7 c7
bdquo 0 P (J bdquo P P 3 P P2
bdquo 009 9 P bdquo 0
-00A Pi A TRIX AP TKE P bdquo 46 -00Al APIKIP RECGUERY AO ( ) -00AR -00AS
REPLICATE P R E C I A T O N
P bdquo 06 2 -i bdquo 4 OP
lt bdquo P 0 NO
lt bdquo 005 NC
bdquo Jo-J NC
lt 00A NC
-bull006()-0070 -0090
A C C -bull0 A A -PiR -00 P A G0-0 A 0bull-FB-00 P ACC--GU0-B- PC PA
NET LIOA B LANLP PIETHOD APIKiP
lt bdquo 0 P A lt 0 P A
P 0 bdquo 4 lt 0 P 5
bdquo 4 4 4
lt bdquo P 0 lt P 0 PAO lt bdquo PO bdquo 4 10
lt 005 lt bdquo 005 lt 005
lt 060 lt bdquo06()lt bdquo06()lt bdquo 060
bdquo P 07
lt 00b P bdquo 005 P bdquo 005 P 005
() (bull V ApIKE RECnUEKY P P4 P 03 P 077 9 9 o 0
PIETHOD SPIKE SPIKE REOOUERY
PIETHOD APIKIP
bdquo P22 i P2
420 P OA 2
P PS P P 57
bdquo 0 P P P P 27 bdquo 0 P 0
SPIKE KEOOUFRY P 02
DB- G- I 0
jvj f p r n w
- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4
0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A
0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B
lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O
SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037
B P T K F R E C O V E R Y AS 4 A
R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL
-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii
OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l
RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN
gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03
NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL
Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL
9 bull v bullbullbull8PIKE RFC GOER Y
RFUBN DESCRIPTION 8ULFIDE
8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A
PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
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NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
1 Silresim Site Trustees - March 10 1986 - File No A-405404
Page 3
TABLE 1
SAMPLE INVENTORY (DECEMBER 4 1985)
GZA Sample ID No (Weston Sample Description)
StationSampleDescription
SCC-GWS-B-105A Well MW-105A
SCC-GWS-B-105B Well MW-105B
SCC-GWS-B-102A Well MW-102A
SCC-GWS-B-102B Well MW-102B
SCC-GWS-B-001A Well MW-102A (Blind Duplicate)
SCC-QAC-SB-001 Sampler Blank (Bailer)
SCC-QAC-FB-001 Filtration SystemBlank
SCC-QACmdashTB-001 Field Blank
SCC-GWS-B-101A Well MW-101A
GZ
28 February 1986
Mr Charles Lindberg Goldberg Zoina and Assoc The GEO Building 320 Needham Street Newton Upper Falls MA 02164
Dear Mr Lindberg
Please note the following items regarding our data reports of January 27 (metals VOAs and BNAs) and January 28 (TCDD)
1 The reported target compounds for VOA and BNA analyses were priority pollutants Since HSLs are needed we searched the original data for the additional analytes and have attached revised reports (Attachment I)
2 The EPA data qualifier B for target analytes detected in the laboratory blank has been added to the report forms where appropriate It is noted that the only targets present in the laboratory blanks were methylene chloride in the VOA blank and bisshy(2-ethylhexyl)phthalate in the BNA blank The blank levels of both these analytes was below the CLP Conshy tract Required Detection Limit
3 Attachment II is a revised TCDD data report on which the surrogate recoveries have been corrected to reflect the observed inconsistency between levels in the calibration standard received from the EPA and the surrogate spiking solution made up in our laborashy tory from neat compounds Also attached is a copy of the laboratory work sheet on which relevant calcushy lations were made and the mass chromatograms
4 Attachment III is the TCDD data report form for the re-extracted samples B-101A and B-102B Re-extracshytion and analyses were performed because of the very high recoveries obtained from the original analysis of these samples More reasonable recoveries were obtained in the re-analysis
5 BNA and TCDD fractions for sample B-105B were spiked with the CLP BNA matrix spike mix and 2378 TCDD respectively Unspiked sample was not analyzed for these parameters due to a miscommunication between GZA and WESTON Laboratory
6 Zinc was found in the method blank at a concentration of 0030 mgL This concentration is consistent with previous determinations of zinc in the laboratory water Certified ultra-pure reagents are used for digestion so that the reagents should not be a source of contamination A method blank is prepared by using an aliquot of laboratory water equivalent to the quantity of sample that is used in the analyses Any contamination in the laboratory water would then be observed on analysis of the method blank However when processing samples minimal amounts of laboratory water are used and any contributions from contaminatedlaboratory water should be much less than 10 of the concentration Consequently contrishy butions from laboratory water should be less than 0003 mgL and concentrations of zinc determined in the samples should be representative of the actual concentrations in the samples
7 Both the computer data base and the original notebook entries have been reviewed for accurate transcription of data for the manganese results The notebook and data base agree Sample 8512-327mdash0030(SCCmdashGWS-B-102A) was diluted by a factor of 10 at the instrument in order for the response to fall within the calibrated range of the instrument Sample 8512-327-0050(SCCshyGWSmdashB-001A) was diluted by a factor of 100 The result obtained for sample 0050 can be verified since this sample was also replicated and spiked The results for the replicate and spike are comparable to the initial result (the spike level was significantly less than the concentration in the sample)
If you have any questions please call me at (215) 524-0180
Very Truly Yours
ROY F WESTON INC
V1
Carter P Nulton PhD Organics Section Manager WESTON Analytical Laboratories
CPNrost
A
RFWSN
8512-327-0010 -0020 -0030 -0040
- -0050 -0050 Dup-0060 -0070 -0090
-0050
Date of Report January 28 1986
GOLDBERG ZOINO AND ASSOCIATES SUMMARY REPORT
FOR SAMPLES RECEIVED DECEMBER 5 1985
Concentration (mgL)
SAMPLE DESCRIPTION A1 Be Ba Ca Sr
SCC-GWS-B-105A lt 0 0 2 SCC-GWS-B-105B lt 0 0 2 SCC-GWS-B-102A lt 0 0 2
lt 0 0 2 lt01 743 1SCC-GWS-B-102B lt05 145 SCC-GWS-B-001A lt 0 0 2 Laboratory Duplicate lt 0 0 2 SCC-QAC-SB-001 lt 0 0 2 SCC-QAC-FB-001 lt 0 0 2 SCC-GWS-B-101A lt 0 0 2 Laboratory Blank lt05 lt 0 0 2 lt01 lt0005 lt005 Blank Spike mdash 100
Rec
Blank Spike Dup mdash 100 Rec
Matrix Spike 100 Rec
Earl M Hansen PhD Manager r
WESTON Analytical Laboratories
D A T S T U n - O r A y T I T N T GO D y E R O - v P [ A O a A A A O r - T f E A D A T A A bull bull y K i P P A K P F M T A A A T L A T A U [ T ) P E - p A T A A A A T F R 0 0 P 0 P - A V
) A1E A A A R A A 0I bull A A TEDiA -bull A - A A A |v| p ( [)| f f y n p y [ iM APATJ A
0 0 i A GP GA F P h g HGL iG7 AG i G G 1 A G L
E F U S N G E 3 C R 1 P T r U N
A A i 2-3 A )0 P 0 S0 A-G A A B bull- P 0A A ( bdquo 0 P 0 bdquo 06 I P A 0 A P -A) 10 A bdquo C P 76 j02XP AIAAGUIH mdashLi POAL OOAO S C C -G3U-B -bull 102A
i A A1 Pbdquo0pO
bull UO P bdquo 0 P 0
y [M-AP bdquoOOA
y y )P p OPO lt0 bdquo 02
P A 4 0A6
00 40 () ( ) A ()
OAP
A A f AUA -B- P 0A la A A C G 11 A-B bullbullbullbull 0 0 -i A
A T IPIx Ap 11ltE
lt bdquo 0 P 0 lt bdquo 0 i 0
069
lt bdquo 0 P ( ) lt bdquo 0 P 0
0 A 4
lt 0 0 A lt 0 0 5 0 0 6
- 0 1A P bdquo 0 P 0
bdquo 2i0
P 0 bdquo 02 lt () n gt)2
bdquo P49
7 AO 067 bdquo P A R
OAK SPIKE REGQUERY PSAX A3 bdquo AX -120 P0S7 74 5 9 P bdquo 0 0 0 A IP 005 A
R IPPL IC A I IP PR IPCISIGN
lt bdquo 0 P 0 NC
lt bdquo 0 P ( ) NC
lt bdquo 0 0 A NC
lt 0 P 0 AC
P 0 OP NC
bdquo 060 - P bdquo OPA
0() 4 () pC C bullbullbullbull A C-bull AB -OOP p bdquo 0 P 0 lt 0 P 0 lt 0 05 P bdquo 0 P 0 bdquo 032 bdquo 0 47 ( )070 () ( ) 9 ()
A CC- Q A CFB ()( ) - j A A A G W A B- P 0 P A
I1 IP TL ILiD B ANK
lt bdquo ( ) p ( ) lt bdquo 0 P 0 lt bdquo 0 P 0
lt 0 p 0 bdquo 0 2 4
lt 0i0
lt bdquo 0 0 A lt bdquo ( ) ( ) A lt bdquo 0 0 A
lt 0 P 0 ( ) -1 ( )
lt bdquo 0 P 0
lt 00 2 () ()
lt 0 bdquo 0 2
bdquo P24 Pi5bdquo 0
lt bdquo0 0 IT IP lL IOD SPIKE 063 023 bdquo 00A 304 bdquo P A3 4 4 4
Ap L K IP RIPCOOIPIPY P26 PPB 4 4 4 P027 7 6 0 P P4 NETHOP Bp TRIP
Ap IGF kFCOOFRY 066 P33
020 -104
00 A P P67
bdquo2P2 106
PA7 y iv v
bdquo P P P P P P
K PIN NA HI PB AlP SIP PIG7L PiGL tPGL PIG 71 PiGL PIGAL PIGL
R F W S N DIPS ORIP TIUN
P 2 -bull - bull 00 P 0 -0020 -0030 bullbullbullbull0040 - O O A O
ACC-GIJS-H- TOAA AAC-GUS-B --10AP ACC-GAl j -P- p 02A SCC--GUS-B - P 02B ACC-GUA-F-GOPA
4 bdquo A 9 bdquo 2 P9 bdquo P90 P 2 bdquo 3 P bdquo 3 P
lt bdquo P 0 lt bdquo P 0 lt bdquo PC bull P6(lt bdquo - i 0
lt bdquo 00 A P bdquo 005 lt ( oA lt bdquo00b lt bdquo 00 A
lt bdquo 060 lt 060 lt bdquo 060 lt bdquo 060 ( bdquo 0 6()
lt 00A lt 005 lt bdquo O f ) A
lt00A lt 00A
-00 AG -7) OAK
PI AIRIX ART KIP AP TKIP RECGUERY
430V7 c7
bdquo 0 P (J bdquo P P 3 P P2
bdquo 009 9 P bdquo 0
-00A Pi A TRIX AP TKE P bdquo 46 -00Al APIKIP RECGUERY AO ( ) -00AR -00AS
REPLICATE P R E C I A T O N
P bdquo 06 2 -i bdquo 4 OP
lt bdquo P 0 NO
lt bdquo 005 NC
bdquo Jo-J NC
lt 00A NC
-bull006()-0070 -0090
A C C -bull0 A A -PiR -00 P A G0-0 A 0bull-FB-00 P ACC--GU0-B- PC PA
NET LIOA B LANLP PIETHOD APIKiP
lt bdquo 0 P A lt 0 P A
P 0 bdquo 4 lt 0 P 5
bdquo 4 4 4
lt bdquo P 0 lt P 0 PAO lt bdquo PO bdquo 4 10
lt 005 lt bdquo 005 lt 005
lt 060 lt bdquo06()lt bdquo06()lt bdquo 060
bdquo P 07
lt 00b P bdquo 005 P bdquo 005 P 005
() (bull V ApIKE RECnUEKY P P4 P 03 P 077 9 9 o 0
PIETHOD SPIKE SPIKE REOOUERY
PIETHOD APIKIP
bdquo P22 i P2
420 P OA 2
P PS P P 57
bdquo 0 P P P P 27 bdquo 0 P 0
SPIKE KEOOUFRY P 02
DB- G- I 0
jvj f p r n w
- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4
0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A
0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B
lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O
SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037
B P T K F R E C O V E R Y AS 4 A
R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL
-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii
OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l
RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN
gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03
NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL
Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL
9 bull v bullbullbull8PIKE RFC GOER Y
RFUBN DESCRIPTION 8ULFIDE
8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A
PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
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Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
28 February 1986
Mr Charles Lindberg Goldberg Zoina and Assoc The GEO Building 320 Needham Street Newton Upper Falls MA 02164
Dear Mr Lindberg
Please note the following items regarding our data reports of January 27 (metals VOAs and BNAs) and January 28 (TCDD)
1 The reported target compounds for VOA and BNA analyses were priority pollutants Since HSLs are needed we searched the original data for the additional analytes and have attached revised reports (Attachment I)
2 The EPA data qualifier B for target analytes detected in the laboratory blank has been added to the report forms where appropriate It is noted that the only targets present in the laboratory blanks were methylene chloride in the VOA blank and bisshy(2-ethylhexyl)phthalate in the BNA blank The blank levels of both these analytes was below the CLP Conshy tract Required Detection Limit
3 Attachment II is a revised TCDD data report on which the surrogate recoveries have been corrected to reflect the observed inconsistency between levels in the calibration standard received from the EPA and the surrogate spiking solution made up in our laborashy tory from neat compounds Also attached is a copy of the laboratory work sheet on which relevant calcushy lations were made and the mass chromatograms
4 Attachment III is the TCDD data report form for the re-extracted samples B-101A and B-102B Re-extracshytion and analyses were performed because of the very high recoveries obtained from the original analysis of these samples More reasonable recoveries were obtained in the re-analysis
5 BNA and TCDD fractions for sample B-105B were spiked with the CLP BNA matrix spike mix and 2378 TCDD respectively Unspiked sample was not analyzed for these parameters due to a miscommunication between GZA and WESTON Laboratory
6 Zinc was found in the method blank at a concentration of 0030 mgL This concentration is consistent with previous determinations of zinc in the laboratory water Certified ultra-pure reagents are used for digestion so that the reagents should not be a source of contamination A method blank is prepared by using an aliquot of laboratory water equivalent to the quantity of sample that is used in the analyses Any contamination in the laboratory water would then be observed on analysis of the method blank However when processing samples minimal amounts of laboratory water are used and any contributions from contaminatedlaboratory water should be much less than 10 of the concentration Consequently contrishy butions from laboratory water should be less than 0003 mgL and concentrations of zinc determined in the samples should be representative of the actual concentrations in the samples
7 Both the computer data base and the original notebook entries have been reviewed for accurate transcription of data for the manganese results The notebook and data base agree Sample 8512-327mdash0030(SCCmdashGWS-B-102A) was diluted by a factor of 10 at the instrument in order for the response to fall within the calibrated range of the instrument Sample 8512-327-0050(SCCshyGWSmdashB-001A) was diluted by a factor of 100 The result obtained for sample 0050 can be verified since this sample was also replicated and spiked The results for the replicate and spike are comparable to the initial result (the spike level was significantly less than the concentration in the sample)
If you have any questions please call me at (215) 524-0180
Very Truly Yours
ROY F WESTON INC
V1
Carter P Nulton PhD Organics Section Manager WESTON Analytical Laboratories
CPNrost
A
RFWSN
8512-327-0010 -0020 -0030 -0040
- -0050 -0050 Dup-0060 -0070 -0090
-0050
Date of Report January 28 1986
GOLDBERG ZOINO AND ASSOCIATES SUMMARY REPORT
FOR SAMPLES RECEIVED DECEMBER 5 1985
Concentration (mgL)
SAMPLE DESCRIPTION A1 Be Ba Ca Sr
SCC-GWS-B-105A lt 0 0 2 SCC-GWS-B-105B lt 0 0 2 SCC-GWS-B-102A lt 0 0 2
lt 0 0 2 lt01 743 1SCC-GWS-B-102B lt05 145 SCC-GWS-B-001A lt 0 0 2 Laboratory Duplicate lt 0 0 2 SCC-QAC-SB-001 lt 0 0 2 SCC-QAC-FB-001 lt 0 0 2 SCC-GWS-B-101A lt 0 0 2 Laboratory Blank lt05 lt 0 0 2 lt01 lt0005 lt005 Blank Spike mdash 100
Rec
Blank Spike Dup mdash 100 Rec
Matrix Spike 100 Rec
Earl M Hansen PhD Manager r
WESTON Analytical Laboratories
D A T S T U n - O r A y T I T N T GO D y E R O - v P [ A O a A A A O r - T f E A D A T A A bull bull y K i P P A K P F M T A A A T L A T A U [ T ) P E - p A T A A A A T F R 0 0 P 0 P - A V
) A1E A A A R A A 0I bull A A TEDiA -bull A - A A A |v| p ( [)| f f y n p y [ iM APATJ A
0 0 i A GP GA F P h g HGL iG7 AG i G G 1 A G L
E F U S N G E 3 C R 1 P T r U N
A A i 2-3 A )0 P 0 S0 A-G A A B bull- P 0A A ( bdquo 0 P 0 bdquo 06 I P A 0 A P -A) 10 A bdquo C P 76 j02XP AIAAGUIH mdashLi POAL OOAO S C C -G3U-B -bull 102A
i A A1 Pbdquo0pO
bull UO P bdquo 0 P 0
y [M-AP bdquoOOA
y y )P p OPO lt0 bdquo 02
P A 4 0A6
00 40 () ( ) A ()
OAP
A A f AUA -B- P 0A la A A C G 11 A-B bullbullbullbull 0 0 -i A
A T IPIx Ap 11ltE
lt bdquo 0 P 0 lt bdquo 0 i 0
069
lt bdquo 0 P ( ) lt bdquo 0 P 0
0 A 4
lt 0 0 A lt 0 0 5 0 0 6
- 0 1A P bdquo 0 P 0
bdquo 2i0
P 0 bdquo 02 lt () n gt)2
bdquo P49
7 AO 067 bdquo P A R
OAK SPIKE REGQUERY PSAX A3 bdquo AX -120 P0S7 74 5 9 P bdquo 0 0 0 A IP 005 A
R IPPL IC A I IP PR IPCISIGN
lt bdquo 0 P 0 NC
lt bdquo 0 P ( ) NC
lt bdquo 0 0 A NC
lt 0 P 0 AC
P 0 OP NC
bdquo 060 - P bdquo OPA
0() 4 () pC C bullbullbullbull A C-bull AB -OOP p bdquo 0 P 0 lt 0 P 0 lt 0 05 P bdquo 0 P 0 bdquo 032 bdquo 0 47 ( )070 () ( ) 9 ()
A CC- Q A CFB ()( ) - j A A A G W A B- P 0 P A
I1 IP TL ILiD B ANK
lt bdquo ( ) p ( ) lt bdquo 0 P 0 lt bdquo 0 P 0
lt 0 p 0 bdquo 0 2 4
lt 0i0
lt bdquo 0 0 A lt bdquo ( ) ( ) A lt bdquo 0 0 A
lt 0 P 0 ( ) -1 ( )
lt bdquo 0 P 0
lt 00 2 () ()
lt 0 bdquo 0 2
bdquo P24 Pi5bdquo 0
lt bdquo0 0 IT IP lL IOD SPIKE 063 023 bdquo 00A 304 bdquo P A3 4 4 4
Ap L K IP RIPCOOIPIPY P26 PPB 4 4 4 P027 7 6 0 P P4 NETHOP Bp TRIP
Ap IGF kFCOOFRY 066 P33
020 -104
00 A P P67
bdquo2P2 106
PA7 y iv v
bdquo P P P P P P
K PIN NA HI PB AlP SIP PIG7L PiGL tPGL PIG 71 PiGL PIGAL PIGL
R F W S N DIPS ORIP TIUN
P 2 -bull - bull 00 P 0 -0020 -0030 bullbullbullbull0040 - O O A O
ACC-GIJS-H- TOAA AAC-GUS-B --10AP ACC-GAl j -P- p 02A SCC--GUS-B - P 02B ACC-GUA-F-GOPA
4 bdquo A 9 bdquo 2 P9 bdquo P90 P 2 bdquo 3 P bdquo 3 P
lt bdquo P 0 lt bdquo P 0 lt bdquo PC bull P6(lt bdquo - i 0
lt bdquo 00 A P bdquo 005 lt ( oA lt bdquo00b lt bdquo 00 A
lt bdquo 060 lt 060 lt bdquo 060 lt bdquo 060 ( bdquo 0 6()
lt 00A lt 005 lt bdquo O f ) A
lt00A lt 00A
-00 AG -7) OAK
PI AIRIX ART KIP AP TKIP RECGUERY
430V7 c7
bdquo 0 P (J bdquo P P 3 P P2
bdquo 009 9 P bdquo 0
-00A Pi A TRIX AP TKE P bdquo 46 -00Al APIKIP RECGUERY AO ( ) -00AR -00AS
REPLICATE P R E C I A T O N
P bdquo 06 2 -i bdquo 4 OP
lt bdquo P 0 NO
lt bdquo 005 NC
bdquo Jo-J NC
lt 00A NC
-bull006()-0070 -0090
A C C -bull0 A A -PiR -00 P A G0-0 A 0bull-FB-00 P ACC--GU0-B- PC PA
NET LIOA B LANLP PIETHOD APIKiP
lt bdquo 0 P A lt 0 P A
P 0 bdquo 4 lt 0 P 5
bdquo 4 4 4
lt bdquo P 0 lt P 0 PAO lt bdquo PO bdquo 4 10
lt 005 lt bdquo 005 lt 005
lt 060 lt bdquo06()lt bdquo06()lt bdquo 060
bdquo P 07
lt 00b P bdquo 005 P bdquo 005 P 005
() (bull V ApIKE RECnUEKY P P4 P 03 P 077 9 9 o 0
PIETHOD SPIKE SPIKE REOOUERY
PIETHOD APIKIP
bdquo P22 i P2
420 P OA 2
P PS P P 57
bdquo 0 P P P P 27 bdquo 0 P 0
SPIKE KEOOUFRY P 02
DB- G- I 0
jvj f p r n w
- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4
0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A
0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B
lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O
SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037
B P T K F R E C O V E R Y AS 4 A
R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL
-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii
OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l
RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN
gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03
NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL
Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL
9 bull v bullbullbull8PIKE RFC GOER Y
RFUBN DESCRIPTION 8ULFIDE
8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A
PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
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V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
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lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
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5 9
AbL S K
TV
3 0
AA
AAshy
oal
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9 6
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out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
6 Zinc was found in the method blank at a concentration of 0030 mgL This concentration is consistent with previous determinations of zinc in the laboratory water Certified ultra-pure reagents are used for digestion so that the reagents should not be a source of contamination A method blank is prepared by using an aliquot of laboratory water equivalent to the quantity of sample that is used in the analyses Any contamination in the laboratory water would then be observed on analysis of the method blank However when processing samples minimal amounts of laboratory water are used and any contributions from contaminatedlaboratory water should be much less than 10 of the concentration Consequently contrishy butions from laboratory water should be less than 0003 mgL and concentrations of zinc determined in the samples should be representative of the actual concentrations in the samples
7 Both the computer data base and the original notebook entries have been reviewed for accurate transcription of data for the manganese results The notebook and data base agree Sample 8512-327mdash0030(SCCmdashGWS-B-102A) was diluted by a factor of 10 at the instrument in order for the response to fall within the calibrated range of the instrument Sample 8512-327-0050(SCCshyGWSmdashB-001A) was diluted by a factor of 100 The result obtained for sample 0050 can be verified since this sample was also replicated and spiked The results for the replicate and spike are comparable to the initial result (the spike level was significantly less than the concentration in the sample)
If you have any questions please call me at (215) 524-0180
Very Truly Yours
ROY F WESTON INC
V1
Carter P Nulton PhD Organics Section Manager WESTON Analytical Laboratories
CPNrost
A
RFWSN
8512-327-0010 -0020 -0030 -0040
- -0050 -0050 Dup-0060 -0070 -0090
-0050
Date of Report January 28 1986
GOLDBERG ZOINO AND ASSOCIATES SUMMARY REPORT
FOR SAMPLES RECEIVED DECEMBER 5 1985
Concentration (mgL)
SAMPLE DESCRIPTION A1 Be Ba Ca Sr
SCC-GWS-B-105A lt 0 0 2 SCC-GWS-B-105B lt 0 0 2 SCC-GWS-B-102A lt 0 0 2
lt 0 0 2 lt01 743 1SCC-GWS-B-102B lt05 145 SCC-GWS-B-001A lt 0 0 2 Laboratory Duplicate lt 0 0 2 SCC-QAC-SB-001 lt 0 0 2 SCC-QAC-FB-001 lt 0 0 2 SCC-GWS-B-101A lt 0 0 2 Laboratory Blank lt05 lt 0 0 2 lt01 lt0005 lt005 Blank Spike mdash 100
Rec
Blank Spike Dup mdash 100 Rec
Matrix Spike 100 Rec
Earl M Hansen PhD Manager r
WESTON Analytical Laboratories
D A T S T U n - O r A y T I T N T GO D y E R O - v P [ A O a A A A O r - T f E A D A T A A bull bull y K i P P A K P F M T A A A T L A T A U [ T ) P E - p A T A A A A T F R 0 0 P 0 P - A V
) A1E A A A R A A 0I bull A A TEDiA -bull A - A A A |v| p ( [)| f f y n p y [ iM APATJ A
0 0 i A GP GA F P h g HGL iG7 AG i G G 1 A G L
E F U S N G E 3 C R 1 P T r U N
A A i 2-3 A )0 P 0 S0 A-G A A B bull- P 0A A ( bdquo 0 P 0 bdquo 06 I P A 0 A P -A) 10 A bdquo C P 76 j02XP AIAAGUIH mdashLi POAL OOAO S C C -G3U-B -bull 102A
i A A1 Pbdquo0pO
bull UO P bdquo 0 P 0
y [M-AP bdquoOOA
y y )P p OPO lt0 bdquo 02
P A 4 0A6
00 40 () ( ) A ()
OAP
A A f AUA -B- P 0A la A A C G 11 A-B bullbullbullbull 0 0 -i A
A T IPIx Ap 11ltE
lt bdquo 0 P 0 lt bdquo 0 i 0
069
lt bdquo 0 P ( ) lt bdquo 0 P 0
0 A 4
lt 0 0 A lt 0 0 5 0 0 6
- 0 1A P bdquo 0 P 0
bdquo 2i0
P 0 bdquo 02 lt () n gt)2
bdquo P49
7 AO 067 bdquo P A R
OAK SPIKE REGQUERY PSAX A3 bdquo AX -120 P0S7 74 5 9 P bdquo 0 0 0 A IP 005 A
R IPPL IC A I IP PR IPCISIGN
lt bdquo 0 P 0 NC
lt bdquo 0 P ( ) NC
lt bdquo 0 0 A NC
lt 0 P 0 AC
P 0 OP NC
bdquo 060 - P bdquo OPA
0() 4 () pC C bullbullbullbull A C-bull AB -OOP p bdquo 0 P 0 lt 0 P 0 lt 0 05 P bdquo 0 P 0 bdquo 032 bdquo 0 47 ( )070 () ( ) 9 ()
A CC- Q A CFB ()( ) - j A A A G W A B- P 0 P A
I1 IP TL ILiD B ANK
lt bdquo ( ) p ( ) lt bdquo 0 P 0 lt bdquo 0 P 0
lt 0 p 0 bdquo 0 2 4
lt 0i0
lt bdquo 0 0 A lt bdquo ( ) ( ) A lt bdquo 0 0 A
lt 0 P 0 ( ) -1 ( )
lt bdquo 0 P 0
lt 00 2 () ()
lt 0 bdquo 0 2
bdquo P24 Pi5bdquo 0
lt bdquo0 0 IT IP lL IOD SPIKE 063 023 bdquo 00A 304 bdquo P A3 4 4 4
Ap L K IP RIPCOOIPIPY P26 PPB 4 4 4 P027 7 6 0 P P4 NETHOP Bp TRIP
Ap IGF kFCOOFRY 066 P33
020 -104
00 A P P67
bdquo2P2 106
PA7 y iv v
bdquo P P P P P P
K PIN NA HI PB AlP SIP PIG7L PiGL tPGL PIG 71 PiGL PIGAL PIGL
R F W S N DIPS ORIP TIUN
P 2 -bull - bull 00 P 0 -0020 -0030 bullbullbullbull0040 - O O A O
ACC-GIJS-H- TOAA AAC-GUS-B --10AP ACC-GAl j -P- p 02A SCC--GUS-B - P 02B ACC-GUA-F-GOPA
4 bdquo A 9 bdquo 2 P9 bdquo P90 P 2 bdquo 3 P bdquo 3 P
lt bdquo P 0 lt bdquo P 0 lt bdquo PC bull P6(lt bdquo - i 0
lt bdquo 00 A P bdquo 005 lt ( oA lt bdquo00b lt bdquo 00 A
lt bdquo 060 lt 060 lt bdquo 060 lt bdquo 060 ( bdquo 0 6()
lt 00A lt 005 lt bdquo O f ) A
lt00A lt 00A
-00 AG -7) OAK
PI AIRIX ART KIP AP TKIP RECGUERY
430V7 c7
bdquo 0 P (J bdquo P P 3 P P2
bdquo 009 9 P bdquo 0
-00A Pi A TRIX AP TKE P bdquo 46 -00Al APIKIP RECGUERY AO ( ) -00AR -00AS
REPLICATE P R E C I A T O N
P bdquo 06 2 -i bdquo 4 OP
lt bdquo P 0 NO
lt bdquo 005 NC
bdquo Jo-J NC
lt 00A NC
-bull006()-0070 -0090
A C C -bull0 A A -PiR -00 P A G0-0 A 0bull-FB-00 P ACC--GU0-B- PC PA
NET LIOA B LANLP PIETHOD APIKiP
lt bdquo 0 P A lt 0 P A
P 0 bdquo 4 lt 0 P 5
bdquo 4 4 4
lt bdquo P 0 lt P 0 PAO lt bdquo PO bdquo 4 10
lt 005 lt bdquo 005 lt 005
lt 060 lt bdquo06()lt bdquo06()lt bdquo 060
bdquo P 07
lt 00b P bdquo 005 P bdquo 005 P 005
() (bull V ApIKE RECnUEKY P P4 P 03 P 077 9 9 o 0
PIETHOD SPIKE SPIKE REOOUERY
PIETHOD APIKIP
bdquo P22 i P2
420 P OA 2
P PS P P 57
bdquo 0 P P P P 27 bdquo 0 P 0
SPIKE KEOOUFRY P 02
DB- G- I 0
jvj f p r n w
- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4
0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A
0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B
lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O
SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037
B P T K F R E C O V E R Y AS 4 A
R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL
-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii
OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l
RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN
gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03
NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL
Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL
9 bull v bullbullbull8PIKE RFC GOER Y
RFUBN DESCRIPTION 8ULFIDE
8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A
PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
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lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
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I M I W
At-AMU o o J O )QltA O
6 6 3 0
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out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
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3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
A
RFWSN
8512-327-0010 -0020 -0030 -0040
- -0050 -0050 Dup-0060 -0070 -0090
-0050
Date of Report January 28 1986
GOLDBERG ZOINO AND ASSOCIATES SUMMARY REPORT
FOR SAMPLES RECEIVED DECEMBER 5 1985
Concentration (mgL)
SAMPLE DESCRIPTION A1 Be Ba Ca Sr
SCC-GWS-B-105A lt 0 0 2 SCC-GWS-B-105B lt 0 0 2 SCC-GWS-B-102A lt 0 0 2
lt 0 0 2 lt01 743 1SCC-GWS-B-102B lt05 145 SCC-GWS-B-001A lt 0 0 2 Laboratory Duplicate lt 0 0 2 SCC-QAC-SB-001 lt 0 0 2 SCC-QAC-FB-001 lt 0 0 2 SCC-GWS-B-101A lt 0 0 2 Laboratory Blank lt05 lt 0 0 2 lt01 lt0005 lt005 Blank Spike mdash 100
Rec
Blank Spike Dup mdash 100 Rec
Matrix Spike 100 Rec
Earl M Hansen PhD Manager r
WESTON Analytical Laboratories
D A T S T U n - O r A y T I T N T GO D y E R O - v P [ A O a A A A O r - T f E A D A T A A bull bull y K i P P A K P F M T A A A T L A T A U [ T ) P E - p A T A A A A T F R 0 0 P 0 P - A V
) A1E A A A R A A 0I bull A A TEDiA -bull A - A A A |v| p ( [)| f f y n p y [ iM APATJ A
0 0 i A GP GA F P h g HGL iG7 AG i G G 1 A G L
E F U S N G E 3 C R 1 P T r U N
A A i 2-3 A )0 P 0 S0 A-G A A B bull- P 0A A ( bdquo 0 P 0 bdquo 06 I P A 0 A P -A) 10 A bdquo C P 76 j02XP AIAAGUIH mdashLi POAL OOAO S C C -G3U-B -bull 102A
i A A1 Pbdquo0pO
bull UO P bdquo 0 P 0
y [M-AP bdquoOOA
y y )P p OPO lt0 bdquo 02
P A 4 0A6
00 40 () ( ) A ()
OAP
A A f AUA -B- P 0A la A A C G 11 A-B bullbullbullbull 0 0 -i A
A T IPIx Ap 11ltE
lt bdquo 0 P 0 lt bdquo 0 i 0
069
lt bdquo 0 P ( ) lt bdquo 0 P 0
0 A 4
lt 0 0 A lt 0 0 5 0 0 6
- 0 1A P bdquo 0 P 0
bdquo 2i0
P 0 bdquo 02 lt () n gt)2
bdquo P49
7 AO 067 bdquo P A R
OAK SPIKE REGQUERY PSAX A3 bdquo AX -120 P0S7 74 5 9 P bdquo 0 0 0 A IP 005 A
R IPPL IC A I IP PR IPCISIGN
lt bdquo 0 P 0 NC
lt bdquo 0 P ( ) NC
lt bdquo 0 0 A NC
lt 0 P 0 AC
P 0 OP NC
bdquo 060 - P bdquo OPA
0() 4 () pC C bullbullbullbull A C-bull AB -OOP p bdquo 0 P 0 lt 0 P 0 lt 0 05 P bdquo 0 P 0 bdquo 032 bdquo 0 47 ( )070 () ( ) 9 ()
A CC- Q A CFB ()( ) - j A A A G W A B- P 0 P A
I1 IP TL ILiD B ANK
lt bdquo ( ) p ( ) lt bdquo 0 P 0 lt bdquo 0 P 0
lt 0 p 0 bdquo 0 2 4
lt 0i0
lt bdquo 0 0 A lt bdquo ( ) ( ) A lt bdquo 0 0 A
lt 0 P 0 ( ) -1 ( )
lt bdquo 0 P 0
lt 00 2 () ()
lt 0 bdquo 0 2
bdquo P24 Pi5bdquo 0
lt bdquo0 0 IT IP lL IOD SPIKE 063 023 bdquo 00A 304 bdquo P A3 4 4 4
Ap L K IP RIPCOOIPIPY P26 PPB 4 4 4 P027 7 6 0 P P4 NETHOP Bp TRIP
Ap IGF kFCOOFRY 066 P33
020 -104
00 A P P67
bdquo2P2 106
PA7 y iv v
bdquo P P P P P P
K PIN NA HI PB AlP SIP PIG7L PiGL tPGL PIG 71 PiGL PIGAL PIGL
R F W S N DIPS ORIP TIUN
P 2 -bull - bull 00 P 0 -0020 -0030 bullbullbullbull0040 - O O A O
ACC-GIJS-H- TOAA AAC-GUS-B --10AP ACC-GAl j -P- p 02A SCC--GUS-B - P 02B ACC-GUA-F-GOPA
4 bdquo A 9 bdquo 2 P9 bdquo P90 P 2 bdquo 3 P bdquo 3 P
lt bdquo P 0 lt bdquo P 0 lt bdquo PC bull P6(lt bdquo - i 0
lt bdquo 00 A P bdquo 005 lt ( oA lt bdquo00b lt bdquo 00 A
lt bdquo 060 lt 060 lt bdquo 060 lt bdquo 060 ( bdquo 0 6()
lt 00A lt 005 lt bdquo O f ) A
lt00A lt 00A
-00 AG -7) OAK
PI AIRIX ART KIP AP TKIP RECGUERY
430V7 c7
bdquo 0 P (J bdquo P P 3 P P2
bdquo 009 9 P bdquo 0
-00A Pi A TRIX AP TKE P bdquo 46 -00Al APIKIP RECGUERY AO ( ) -00AR -00AS
REPLICATE P R E C I A T O N
P bdquo 06 2 -i bdquo 4 OP
lt bdquo P 0 NO
lt bdquo 005 NC
bdquo Jo-J NC
lt 00A NC
-bull006()-0070 -0090
A C C -bull0 A A -PiR -00 P A G0-0 A 0bull-FB-00 P ACC--GU0-B- PC PA
NET LIOA B LANLP PIETHOD APIKiP
lt bdquo 0 P A lt 0 P A
P 0 bdquo 4 lt 0 P 5
bdquo 4 4 4
lt bdquo P 0 lt P 0 PAO lt bdquo PO bdquo 4 10
lt 005 lt bdquo 005 lt 005
lt 060 lt bdquo06()lt bdquo06()lt bdquo 060
bdquo P 07
lt 00b P bdquo 005 P bdquo 005 P 005
() (bull V ApIKE RECnUEKY P P4 P 03 P 077 9 9 o 0
PIETHOD SPIKE SPIKE REOOUERY
PIETHOD APIKIP
bdquo P22 i P2
420 P OA 2
P PS P P 57
bdquo 0 P P P P 27 bdquo 0 P 0
SPIKE KEOOUFRY P 02
DB- G- I 0
jvj f p r n w
- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4
0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A
0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B
lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O
SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037
B P T K F R E C O V E R Y AS 4 A
R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL
-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii
OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l
RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN
gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03
NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL
Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL
9 bull v bullbullbull8PIKE RFC GOER Y
RFUBN DESCRIPTION 8ULFIDE
8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A
PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
D A T S T U n - O r A y T I T N T GO D y E R O - v P [ A O a A A A O r - T f E A D A T A A bull bull y K i P P A K P F M T A A A T L A T A U [ T ) P E - p A T A A A A T F R 0 0 P 0 P - A V
) A1E A A A R A A 0I bull A A TEDiA -bull A - A A A |v| p ( [)| f f y n p y [ iM APATJ A
0 0 i A GP GA F P h g HGL iG7 AG i G G 1 A G L
E F U S N G E 3 C R 1 P T r U N
A A i 2-3 A )0 P 0 S0 A-G A A B bull- P 0A A ( bdquo 0 P 0 bdquo 06 I P A 0 A P -A) 10 A bdquo C P 76 j02XP AIAAGUIH mdashLi POAL OOAO S C C -G3U-B -bull 102A
i A A1 Pbdquo0pO
bull UO P bdquo 0 P 0
y [M-AP bdquoOOA
y y )P p OPO lt0 bdquo 02
P A 4 0A6
00 40 () ( ) A ()
OAP
A A f AUA -B- P 0A la A A C G 11 A-B bullbullbullbull 0 0 -i A
A T IPIx Ap 11ltE
lt bdquo 0 P 0 lt bdquo 0 i 0
069
lt bdquo 0 P ( ) lt bdquo 0 P 0
0 A 4
lt 0 0 A lt 0 0 5 0 0 6
- 0 1A P bdquo 0 P 0
bdquo 2i0
P 0 bdquo 02 lt () n gt)2
bdquo P49
7 AO 067 bdquo P A R
OAK SPIKE REGQUERY PSAX A3 bdquo AX -120 P0S7 74 5 9 P bdquo 0 0 0 A IP 005 A
R IPPL IC A I IP PR IPCISIGN
lt bdquo 0 P 0 NC
lt bdquo 0 P ( ) NC
lt bdquo 0 0 A NC
lt 0 P 0 AC
P 0 OP NC
bdquo 060 - P bdquo OPA
0() 4 () pC C bullbullbullbull A C-bull AB -OOP p bdquo 0 P 0 lt 0 P 0 lt 0 05 P bdquo 0 P 0 bdquo 032 bdquo 0 47 ( )070 () ( ) 9 ()
A CC- Q A CFB ()( ) - j A A A G W A B- P 0 P A
I1 IP TL ILiD B ANK
lt bdquo ( ) p ( ) lt bdquo 0 P 0 lt bdquo 0 P 0
lt 0 p 0 bdquo 0 2 4
lt 0i0
lt bdquo 0 0 A lt bdquo ( ) ( ) A lt bdquo 0 0 A
lt 0 P 0 ( ) -1 ( )
lt bdquo 0 P 0
lt 00 2 () ()
lt 0 bdquo 0 2
bdquo P24 Pi5bdquo 0
lt bdquo0 0 IT IP lL IOD SPIKE 063 023 bdquo 00A 304 bdquo P A3 4 4 4
Ap L K IP RIPCOOIPIPY P26 PPB 4 4 4 P027 7 6 0 P P4 NETHOP Bp TRIP
Ap IGF kFCOOFRY 066 P33
020 -104
00 A P P67
bdquo2P2 106
PA7 y iv v
bdquo P P P P P P
K PIN NA HI PB AlP SIP PIG7L PiGL tPGL PIG 71 PiGL PIGAL PIGL
R F W S N DIPS ORIP TIUN
P 2 -bull - bull 00 P 0 -0020 -0030 bullbullbullbull0040 - O O A O
ACC-GIJS-H- TOAA AAC-GUS-B --10AP ACC-GAl j -P- p 02A SCC--GUS-B - P 02B ACC-GUA-F-GOPA
4 bdquo A 9 bdquo 2 P9 bdquo P90 P 2 bdquo 3 P bdquo 3 P
lt bdquo P 0 lt bdquo P 0 lt bdquo PC bull P6(lt bdquo - i 0
lt bdquo 00 A P bdquo 005 lt ( oA lt bdquo00b lt bdquo 00 A
lt bdquo 060 lt 060 lt bdquo 060 lt bdquo 060 ( bdquo 0 6()
lt 00A lt 005 lt bdquo O f ) A
lt00A lt 00A
-00 AG -7) OAK
PI AIRIX ART KIP AP TKIP RECGUERY
430V7 c7
bdquo 0 P (J bdquo P P 3 P P2
bdquo 009 9 P bdquo 0
-00A Pi A TRIX AP TKE P bdquo 46 -00Al APIKIP RECGUERY AO ( ) -00AR -00AS
REPLICATE P R E C I A T O N
P bdquo 06 2 -i bdquo 4 OP
lt bdquo P 0 NO
lt bdquo 005 NC
bdquo Jo-J NC
lt 00A NC
-bull006()-0070 -0090
A C C -bull0 A A -PiR -00 P A G0-0 A 0bull-FB-00 P ACC--GU0-B- PC PA
NET LIOA B LANLP PIETHOD APIKiP
lt bdquo 0 P A lt 0 P A
P 0 bdquo 4 lt 0 P 5
bdquo 4 4 4
lt bdquo P 0 lt P 0 PAO lt bdquo PO bdquo 4 10
lt 005 lt bdquo 005 lt 005
lt 060 lt bdquo06()lt bdquo06()lt bdquo 060
bdquo P 07
lt 00b P bdquo 005 P bdquo 005 P 005
() (bull V ApIKE RECnUEKY P P4 P 03 P 077 9 9 o 0
PIETHOD SPIKE SPIKE REOOUERY
PIETHOD APIKIP
bdquo P22 i P2
420 P OA 2
P PS P P 57
bdquo 0 P P P P 27 bdquo 0 P 0
SPIKE KEOOUFRY P 02
DB- G- I 0
jvj f p r n w
- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4
0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A
0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B
lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O
SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037
B P T K F R E C O V E R Y AS 4 A
R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL
-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii
OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l
RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN
gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03
NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL
Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL
9 bull v bullbullbull8PIKE RFC GOER Y
RFUBN DESCRIPTION 8ULFIDE
8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A
PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
DB- G- I 0
jvj f p r n w
- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4
0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A
0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B
lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O
SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037
B P T K F R E C O V E R Y AS 4 A
R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL
-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii
OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l
RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN
gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03
NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL
Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL
9 bull v bullbullbull8PIKE RFC GOER Y
RFUBN DESCRIPTION 8ULFIDE
8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A
PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
DATE OF REPORT December 13 1985
RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Dilut ion Factor NS = Not Spiked
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185
ugL MATRIX SP 05 05
ND ND UL ND
05
05 obsc
05 JUL
05 47
05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50
1 0 50 Ttr 50 50 50
TTTT 1 0
100 100 10 100 ND = Not Detected lt detection limit
0050 B001A
12485 12685 121185
NP
1 0
0060 SB001 12485 IP685
121185
MM
iO
Approved By
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
DATE OF REPORT December 13 1985
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
FOR GZA
WATER-PESTICIDEPCB SUMMARY REPORT
WO NO 0010-10-09
NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t
Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
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-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ATTACHMENT I
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002219GCMS FILE NAME CLIENT
SCC-GWS-B-IQ5A MATRIX WATER
GZA
SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010
DILUTION FACTOR 500 RFYI =
DATE COLLECTED DECEMBER A 1985
PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985
WORK ORDER it
UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane
75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U
75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U
75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone
10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U
75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U
67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J
107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U
78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane
106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5
106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane
Total Xylenes 5000 I
SURROGATE RECOVERY
1 1-DICH10R0ETHANE du 106
TOLUENE d8 109
p-BROMOFLUOROBENZENE 1 1 5
Data report ing quali f iers
U - NOT DETECTED COMMENT NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT
B - ANALYTE PRESENT IN BLANK
2-2-^ APPROVED BY u lt mdash ^ar1 Hansenraquo
Manager WESTON Analy t ica l Laborator ies
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT ZA GCMS FILE NAME 1217W0Q2220
SAMPLE DESC SCC-GWS-B-l05B MATRIX Water
RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or
DATE
DATE
rOLLECTEDDecember 4 1985
ANALYZED December 11 1985
DILUTION FACTOR I
PH NA Z MOISTURE NA
WORK ORDER Hbull
CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]
74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J
74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U
79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J
124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U
75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane
67-64-1 Acetone 6 J 71-43-2 Benzene H
75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U
75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U
75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U
156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U
127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane
79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u
106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5
56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20
106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U
75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17
SURROGATE RECOVERY
1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT
B - ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY
Ear l M Hansen PhD P- Manager
WESTON Analy t ica l Laborator ies
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W00221 8
SAMPLE DESC SCC-GWS-B-102A MATRIX Water
RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA
WORK ORDER
CAS 9 Ldr wgXgCAS Number Circle One)Numbtr
7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane
10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride
124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J
75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene
67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U
75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U
75-35-4 75-34-3 1 1-Dichloroethane 10 u
591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u
106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u
127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u
79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J
71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J
56-23-5 10 U108-06-4 Vinyl Acetate
100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i
Total Xylenes 7 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120
Data repor t ing qua l i f ie rs
COMMENT U NOT DETECTED
NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT
ANALYTE PRESENT IN BLANKB
APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME I217W002216
SAMPLE DESC SCC-GWS-B-102B MATRIX Water
RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One
DATE COLLECTED December 4 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA X MOISTURE NA
WORK ORDER
ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J
79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k
75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone
10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL
110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone
156-60-5 Trans-1 2-Oichloroethene 610 k k k
k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene
107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k
78-93-3 2-Butanone k k k
106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k
106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde
100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u
100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes
75-69-4 Trichlorofluoromethane 8 J
SURROGATE RECOVERY
1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146
Data repor t ing qua l i f ie rs
COMMENT shyNOT DETECTEDU undetermined possible interference
NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ
B ANALYTE PRESENT IN BLANK
DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002217
SAMPLE DESC Lab
SCC-GWS -B-102Bn im MATRI X Water
RFW 8512-327-OO^ORP METHOD~^LOw) MEDLEVEL CLP (C i rc le On
DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER
CAS Number 74-67-3 74-83-9
Chloromethane Bromomethane
ugKfl ^Circle OneI
10000 u 10000 u
CAS Number 78-67-5 10061-02-6
^ygI)bruqKfl ICircle One)
1 2-Dichloropropene Trans-1 3-Dichloropropene
10000 u 10000 u
75-01-4 75-00-3
Vinyl Chloride
Chloroethine
10000 10000
u u
79-01-6 124-48-1
Trichloroethene Dibromochloromethane
52000 l 0000 u
75-09-2 67-64-1 75-15-0 75-35-4 75-34-3
Methytene Chloride
Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane
200000 B 1200000
10000 u 860 J
10000 u
79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2
11 2-Trichloroethane
Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform
8200 93000 10000 10000 10000
J
u u u
156-60-5 67-66-3
Trans-1 2-Dichloroethene
Chloroform
10000 3300
u J
591-78-6 106-10-1
4-Methyl-2-Pentanone
2-Hexanone 29000 10000 u
107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000
78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J
71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000
56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000
106-06-4 75-27-4
Vinyl Acetate Bromodichloromethane
10000 10000
U u
100-41-4
100-42-5
Ethylbenzene Styrene
12000 700 J
Total Xylenes 29000
SURROGATE RECOVERY
1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122
Data repor t ing qua l i f ie rs
COMMENTU - NOT DETECTED NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W002215
SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _
RFV
DATE COLLECTED
8512-327-0050
DECEMBER k 1985
METHOD
DILUTION
MED
FACTOR
LEVEL
1
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER H_
lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone
10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide
10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u
67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u
107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u
10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u
10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS F ILE NAME 1217W0022 1 A
SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter
RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One
DATE COLLECTED December k 1985 DILUTION FACTOR 1
DATE ANALYZED December 18 1985 PH NA MOISTURE NA
WORK ORDER sectbull - bull
CAS (up^or ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number
78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane
79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane
79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u
11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u
Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 92
TOLUENE dB mi p-BROMOFLUOROBENZENE 111
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT
NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK
DATE z z 8 r 6
APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD
Manager WESTON Analy t ica l Laborator ies
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC
METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985
Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA
WORK ORDER _
j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr
78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane
79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone
10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether
75-35-4 1 1 -Dichloroethene 10 u 10 [J
75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ
591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U
106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u
71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u
10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u
SURROGATE RECOVERY 98 11-DICHLOROETHANE du
TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U
Data repor t ing qua l i f ie rs
U
NR j B
-
---
NOT DETECTED
NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT
THAN DETECTION IN BLANK
L IMIT
C0MMENT_
-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD
Manager WESTON Analy t ica l Laborator ies
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON
ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS
1217W002221 CLIENT GZA GCMS F ILE NAME
SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water
RFW = DATE rn i 1 FCTED
8 A I 7 - ^ 7 - n n q n
December k 1985
METHOD
DILUTION
LOW MED
FACTOR
LEVEL
000
CLP (C i rc le 0
DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA
WORK ORDER if
^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS
(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane
10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane
10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride
124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride
10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone
10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u
75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane
0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3
Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u
67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J
107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane
56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J
108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane
Total Xylenes 3 6 0 075-27-4
75-69-4 Tr i ch1oro f1uoro- 5000 methane
SURROGATE RECOVERY
11-DICHLOROETHANE du 104 TOLUENE dg 1 00
ToFp-BROMOFLUOROBENZENE
Data repor t ing qua l i f ie rs
U - NOT DETECTED COMMENT_ NR - NOT REQUESTED
J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK
7- ~ ^ APPROVED BYDATE
Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
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5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
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OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS F ILE NAME 1217W002212
CLIENT
SAMPLE DESC T r ip B lank M A T R I X W a t e r
RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One
DATE
DATE
COLLECTED
ANALYZED
December
December
A 1985
17 1985
DILUTION FACTOR
PH NA
1
MOISTURE NA
WORK ORDER H
(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6
Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride
Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone
10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U
110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4
75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u
67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u
71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u
SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8
p-BROMOFLUOROBENZENE 109
Data repor t ing qua l i f ie rs
COMMENTNOT DETECTED
NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT
U
J ANALYTE PRESENT IN BLANKB
APPROVED BY DATE Ear l M Hansen PhD
Manager WESTON Analy t ica l Laborator ies
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
74-87-3
ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY
VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
C L I E N T GZA GCMS F ILE NAME 1217W002139
SAMPLE DESC Lab B lank MATRIX Water
RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One
DATE COLLECTED NA DILUTION FACTOR 1
DATE ANALYZED December 17 1985 PH NA MOISTURE N A
WORK ORDER
(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number
78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U
10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride
124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u
75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u
67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u
75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone
10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u
106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u
SURROGATE RECOVERY
11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98
Data repor t ing qua l i f ie rs
bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD
NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ
B - ANALYTE PRESENT IN BLANK
^2 Cgt APPROVED BY mdash Z mdash Hansen
Manager WESTON Ana ly t ica l Labora tor ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT SAMPLE DESC _
DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER
GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986
GCMS FILE NAME
MATRIX
METHOD
DETECTION LIMIT D F
LOWMED
0106B1603
Water
LEVEL CLP
10 ugLlx
( C i r c l e O n e )
ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf
83 32 9 Acenaphthene NDPnenol 2 U
ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol
32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene
541-73-1 1 4-Dichlorobenzene
606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol
184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei
95-50-1 95-48-7 2-Methylphenpi
86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne
06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7
86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20
ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3
85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol
120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene
20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate
20-82-1
91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene
95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene
91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene
131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc
13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By DATE February 28 1986 Earl M Hansen PhD
iManager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~
8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED
D F UWORK ORDER
ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr
83 32-9 AcenaphthcnePhenol A8 A O
0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2
111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u
5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7
100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1
7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U
I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u
00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether
67-72-1 Nitrobenzene
118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone
187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U
105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr
1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane
1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol
129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U
120-82-1
91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U
106-47-8 HexachlorobutaOiene
117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88
218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate
77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene
68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene
95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene
91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M
1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie
191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U
3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED
D F 1WORK ORDER
[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor
83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u
108-95 2 j(-2-Chloroethyl)Ether
00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene
541 73-1 4-Dichlorobenzene
606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether
95-50-1 95-48-7 2-Methylphenol
186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether
06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J
59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene
88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u
10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene
99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE mdashEarl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr
8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5
DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6
D F l x amp 1OxWORK ORDER
ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____
83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I
95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u
541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene
606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene
98-95-3 78-59-1 Isophprone 1700
87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U
85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene
120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate
91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline
[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate
87-68 3 59-50-7 4-Chloro-3-Methylphenol
218-01-9 Chrysene91-57-6 2-Methylnaphthalene
117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene
05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene
95 95-4 E0-32-8 Benzo(a(Pyrene
91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene
88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene
99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED
Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
CLIENT GZA GCMS FILE NAME 0111B1656
SAMPLE DESC _ RFW DATE COLLECTED
SCC-GWS-B-OOIA 8512-327-0050 December U 1985
MATRIX
METHOD
^
LOHMED
Water
LEVEL CLP (Circle One DATE DATE WORK
EXTRACTED ANALYZED ORDER
December 8 1985 January 11 1986 DETECTION LIMIT
D F l x io UgL
CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna
83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene
606-20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol
184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U
106-44-5 4-Methylphenol
621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U
98-95-3 78-59-1 Ispphprpne
87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U
120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate
206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1
ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3
106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate
87-68 3 59-50-7 4-Chloro-3-Methytphenol
[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U
95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U
50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine
( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds
U = NR =
NOT DETECTED NOT REQUESTED
J B
= PRESENT = ANALYTE
AT LESS THAN DETECTION LIMIT FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WEsectTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v
G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O
DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5
DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER
CAS (ug tor ugKg CAS Cygj^or ug Kg
Number ^Circle Or) Number (Circle On1
Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U
95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene
95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate
95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether
39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene
106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol
Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene
120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene
91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U
87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate
91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene
88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene
Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8
99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE V $pound Earl M Hansen PhD
Manager WESTON Analytical Laboratories
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ
METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985
DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER
CAS I gtr ug Kg CAS ug |^gtr ug tg
Number irele One) Number Circle One1
106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U
95-57-8
11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl
10 80
u 1-28-5 00-02-7 4-Niirpphenpl
2 4-Dinitrophenpi
V 5 0 5 0
U U
541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U
06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene
00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene
95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate
95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei
39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene
106-44-5 621-64 7
4-Methylphenol N-Niuoso-Di-n-Propylamine
100-01-6 534-52-1
4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )
5 0 U 5 0 U
67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei
78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene
88-75-5 05-67-9
2-Nitrpphenol 2 4-Dimethylphenol
1 0
1 0
U
U
(87-86-5 85-01-8
Pentachlorpphenol Phenanthrene
5 0 10
U u
65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene
111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene
120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene
91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate
106-47-8 87-68 3
4-Chlorpaniline Hexachlorobutadiene
1 0
1 0
U
U
B1-94-1 56-55-3
3 3-Dichlorobenncine I Benzolta)Anthracene
2 0 U 10 u
59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate
91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene
77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate
88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene
95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene
91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene
88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene
131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene
206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene
99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )
C a n n o t M D L = M D L =
be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
DATE February 28 1986 Approved By
Earl M Hansen PhD Manager WFSTON Analytical labnratnripr
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY
SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS
GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank
NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985
DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER
CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr
83 32-8 AcanaphthenePhenol 10 U 10 U
111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U
95 57-8
106-95-2
2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U
106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene
100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene
1 2-Dichlorobenzene 84-66-2 Diethylphthalate
2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene
4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U
101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene
78-59-1 Isophorone 118-74-1 Hexachlprobenzene
88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U
105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U
111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate
120-83-2 2 4-Dichlorophenol 206-44-0 Fluoranthene
120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene
106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U
87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U
59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J
91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U
77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate
2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2
95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene
91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111
131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene
208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s
( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s
U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK
Approved By DATE February 28 1986 ^^-^Earl M Hansen PhD
Manager WESTON Analytical Laboratories
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy
_ Contract No
Case No G2h_ Contract Laboratory mdash
IraquoTraquottlaquoCshy
V O L A T I L E SEMI-VOLATILE yen
ttM TPAf rtc
laquoa iocuim -o
lt ltot I-iit)
IJ OICMLOHOshy
lrlaquo-IXI
NII40shyMNttNt-O
(gtbull- gt llaquogt
t-fLU00 bullIPHCNTL
( 4 9 shy
ItROK Ntinoi-M
3 3
I-Ill
(II-IMI
3 ~ T
(laquobullshy
AAA
Atrade
I M I W
At-AMU o o J O )QltA O
6 6 3 0
^5 A2gt
Ay
AOshy
5 9
AbL S K
TV
3 0
AA
AAshy
oal
AL53shy
3
3LA yshy
rsb
y s
JSJL
-Al^
jIQJZJOL
06 fO 6 v b 0
9 6
VO
6 gt 6
O A
amp 0
y y
OSAA
_^Zi lt=A
o o
AlSL
6A yen
3AL S O 6 5 a-a
a o 9 a
out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides
Comments
cnou ii 7 8 6
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY
^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A
FRACTION
bull VOA SMO
SAMPLE NO
BN SMO
SAMPLE NO
ACID SMO
SAMPLE NO
PEST SMO
SAMPLE NO
COMPOUND
1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene
N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT
CONC SPIKE ADDED lugI
joj
w wo
r
SAMPLE RESULT
to
CONC 0S
SJL JW 1SL 31
Ai2_ 21 AA J13 13 12 JUL
REC
33 1CL 33 13 88 ~Jo JR A332 1377 A3
CONCB S D
3L 4A3 ARshyAL A3 18shylS1A1
R E C
A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L
RPO
33 11 13
ILL
A3 12 _a_ 122Q
14 14 1 3
38 40 31 38
28 50 42 40 42 50 15 20 2 2 18 2 1 27
61145 7 1120 75 1 30
JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6
36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7
^ASTERISKED VALUES ARE OUTSIDE QC LIMITS
RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_
outside QC limits outside QC limits outside QC limits outside QC limits
RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of
outside QC limits outside QC limits outside QC limits outside QC limits
uOnvmnis
4M
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ATTACHMENT II
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
TABLE 1 TCDD DATA REPORT FORI1 GZA
Report Date February 2 R 1986 Lab Roy F Weston
Column CP-SIL-88 Batch 8512-327
GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur
Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml
216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455
B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918
1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110
227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113
1 0279 124071000 ND 002 1886 1117 83 3400 582247
B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822
1886B-101A 0090 1000 ND 014
bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before
extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis
FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected
DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank
Please Note Surroqate Recoveries have been corrected as described in the cover letter
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
SHEET o f
CLIENTSUBJECT yrKh SL c r wO NOshy
TASK NO_TASK DESCRIPTION
DEPT DATE APPROVED BYPREPARED BY DEPT DATE
DEPT DATE MATH CHECK BY
METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S
(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0
JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy
3 ^ - 9 33 ^ 3 31
SJ2 pound 3 gltJ-O 5 r
Xl
laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0
$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL
C S ~ 7 amp amp s gt J azs-o
625-0^ x
0JY3 XV x y
A ~ bull ^ ^VLLcf mdash
bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3
347 698
1000n 827 698
323 323897 plusmn 0 580
379 14185 31027
14272
RIC
312 1962
11426 v-
T
338 560 2965
A
355 544 1060
^T y-v
mdashp_ TV- y
308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
379 3812 10283
89li
332
379 4280 8420
1000-1
334
312 347 369336 291 188 181125 950 295 bull 382281
mdash I 379
14185 31927
3335-1
RIC 312
333 3551962 560 5441142b 2965 1060
300 320 340 360 380 820 853 927 1000 1033
3812
332099 plusmn 0500
4280
334100 plusmn 0500
14272
400 SCAN 1107 TIME
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
139-1
DATA 0216Z84 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J
312 864 4568
0 BASE U 20
SCANS 300 TO 400
884
257 338 210 580
378 205 1209
257077 plusmn 0500
1000-|
379 6376 18358 6376
328 328098 plusmn 0500
311 343 361
281 255 442
743 701 2387 A =T
2238shy 14272
RIC 312 1962 338 355
11426 560 544 _---v 2965 1060 X bull bull i ^
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
310 342
1000n 1505 355
320 320096 plusmn 0500
854-i 303
322 322096 plusmn 0500
379 14185 31027
1427
R1C 312 1962 338 355
11426 560 544 2965 1060 S I I
I
300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
ATTACHMENT III
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
TABLE 1
GZA (re-extractions)
Lab Roy F Weston
Batch 8512-327
GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr
ID ID Cleanup ml Meas D L ID Date Time
ND 002 4600Z 2-16-36 1831mdash Blank 1 0
ND 006 4600Z 2-16-86 185C102B 0040 1 0
4600Z 2-16-86 1920101A 0090 1 0 ND 002
RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank
TCDD DATA REPORT FORM
Report Date February 29 1986
Column 30 meter DB-5
Rel Ion Abundance Surrogate
Acc 320 327 Relative Ion Abundance
321~257~ TIT 33
1 1 124 11870 5072 4651
96 69 15305 11060 11546
99 51 10356 28000 1 4628
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
TABLE 2 INITIAL CALIBRATION StMHAXY
TOD liOMr Resolution
Date laserXD
Sol IP
Measured RF Native Surrogate
Maan If Used Native Surrogate
Fercent Valley(Applies for FC only)
invk S ^ ~
V 7 8 mdash
J _ lt9 j f 3C
SO bullJ-J S S3
j y
QUALITY CONTROL SUMMARY
Mean Accuracy Surrogate Measurements
Accuracy FortifiedSpike Field Blank
tel Biff (Z) Duplicate Analysis
mdash
of regftt
Saaple mdash
Saaple mdashtrademdash
Solution ID Codes
FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal
IFB te 1B - 7 122983
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
DATA 0216Z83 1 CALI TC 3
MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
386-1 497
257 257077 plusmn 0500
1000-i 1286
328 328898 i 0500
378 15680 39342
15680
RIC
300 820
Q1 do lo 1026 6905
T 320 853
337 740 6319
340 927
3b0
4100
I 360
1000
I
~1 380
1033
394 622
2173
7 400 SCAN
1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
752shy 1386
320 313 331 347 365
320096 plusmn 0500
195 218 191 158 268 595595 t 543- 181
vQr mdash A A pound 5
1000n 1844
322
305 153
247
316 229 1399
334 140 423
345 167
190
362 138 420
322096 plusmn 0500
Sbm yi Vpound^ rV =F IS
8503-1 15680
RIC
318 360 1026 740 747 6905 6319 - - 4100
T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
904n
MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40
DATA 0216Z83 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 5009 12945 5024
332 332093 plusmn 0500
1000n 5560
334 334100 plusmn 0500
2820mdash| 15680
RIC
400 SCAN 1107 TIME820
300
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 496
10001 1136 497
323 394 323097 172 plusmn 0500 667
378 15680 39342 15680
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20
987-i 1768
257 257077 plusmn 0500
1000n 1792
328 328098 plusmn 0500
377 25902 67237 25952
RIC
317 339 361 1450 331 303 7098 717 1641 laquo-raquo
T I i
300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
801shy
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 4938
12923 4952
320
44
318 235 1131
T
346 203 501
320096 plusmn 0500
1000-1 6184
322
309 274 1222
346 190 381
322096 plusmn 0500
4197-1
377 25902 67237 25952
RIC
300 820
317 1450 7098
1 320 853
339 331 7171 i
340 927
361 303 1641
360 1000
380 1033
480 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1
318 247 1418
386 317 252 157
465 shy 811 T
317 1450 7098
1 300 320 820 853
DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3
40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833
5016
332099 plusmn 0500
335 346 367
128 176 217 247 415 573=rtrade
i 377 5792 14967
5792
334100 plusmn 0500
336 356 394 69 123 55 99 I 147
bull=r bull bull 214
377 25902 67237
25952
333 361 331 717 I
303 1641 f
T I 7 340 360 400 SCAN 927 1000 1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J
SCANS 300 TO 400
BASE U 20 3
1086
323097 plusmn 0500
365 71 147
I 377
25902 67237 25952
T 360 380 400 SCAN
1000 1033 1107 TIME
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
1000-1
DATA 0216Z81 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 6133 13810 6160
257 317 758 3307
3
347 290 1326
394 250 475
257077 plusmn 0500
428-1 2636
328
308 224 710bull _
328098 plusmn 0500
377 c
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40
DATA 0216281 Ml CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 16883 40730 16928
320096 plusmn 0500
309 315
gt437
389 295 1240
377 26781 56466 26816
322096 i 0500
305 406 1188 bull
316 473
gt1-145
333 163 269
348 268 920
367 151 183
377 65216 146362
3shy
65216
316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378
T
300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3
963-1
332
306 208 280
347 250 1167 zzz
1000-1
334
314 280 1070
329 159 159
FrE
347 212
bull 212
RIC
300 829
316 2984 23257
I 320 853
bull
329 378 522
346 1374
5307
340 927
363 184 486
377 4938 11333
377 65216 146362
389 298 1041
389 280
522
4768
332099 plusmn 0500
4952
334100 plusmn 0500
6521b
363
503
bull 954
360 1000
1
380 1033
389 1402 3378
490 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1
DATA 6216281 1 CALI TC 3
40 QUAN A 1 10 J 8
SCANS 390 TO
BASE U 28 3
400
1000-i 4776
323 323097 plusmn 0500
377 65216 146362 65216
RIC
329 346 363 389 378 1374 508 1402
1 522
T 1 5307 954 3378
380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
tr
fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400
021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
378 22748 37045 22752
257077 plusmn 0500
317 335 346 360 370 392
500 228 161 165 151 202 3308 I
T I I 715 bull 299 323
T 504 649
1254
309 203 824A
332 210
485
345 171 494
362 300 637
390 211
1111
328098 plusmn 0500
izz
378
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20
378 60352
1000-1 111640 60352
320 320096 plusmn 0500
316 332 360 234 328 217 910^ 775 1018
378 59520
986-1 134351 59520
322 322096 plusmn 0500
305 338 245 184 665 327j
378 152034
2520-1 324544
152064
RIC
317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU
I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20
847n 4288
332
1000-1
311 342 1176
332 227 763
=F
344 213 213
366 237 378
377 5064 8861
389 191 1001
332099 plusmn 0500
5064
334
308 180 482
319 261 740
331 183
575 -mdash fw
I lt m M raquoTm
347 168 527
360 216 913
390 171 846
334100 plusmn 0500
152064
RIC
317 1247
332 983 3828
346 854 3282
360 720 145h
300 820
320 853
340 927
360 1000
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40
DATA 0216Z80 tl CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 10512 21422 10512
323037 plusmn 0500
305 171 702 bull
317 232
I335J
T
I i bull
336 270
i568 bull
346 236 710
378 152034 324544
390 195 457 J
152064
RIC
360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1
Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340
1000 1033 1107 TIME820 853 927
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J
SCANS 380 TO
BASE U 20 3
400
377 50496 90700 50496
257 257077 plusmn 0500
307 88 351
+
348 105 309
39-i 1970
328 328098 plusmn 0500
345 63 63
mdash _ I _ I laquo
377 400896
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
876-1
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40
DATA 0216279 1 CALI IC 3
QUAN A 10 J 0
SCANS 300 TO
BASE U 20 3
400
377 151552 266999 151552
320 320096
plusmn 0500
1000-1
377 173054 332359 173056
322 322096
plusmn 0500
2317-n
377 409896 761478 400896
RIC
300 820
314O J
253 740
1 320 853
340 927
359 bull454 1146
360 1000
380 1033
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS 021686 151400 SAMPLE 2UL CAL STD 5 CONDS DX RANGE G 1 426 LABEL N -1 40
DATA 0216Z79 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 380 TO
BASE U 20 3
400
842-1 4528
332
314 63 63
346 96 184 bull
356 165
388 267 488
332999 plusmn 0500
10001
376 5376 10204 5376
334
319 27 27 bull
-3
354 108
204=
j
bull bull -c- I
377 400896 761478
388 213 1266
334100 plusmn 0500
400896
RIC
300 820
314 253 740
~7 320 853
~1 340 927
359 454 1146
T 360
1000 380
1033 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 21440
1000-1 48288
A 21440
323 323997
plusmn 0500
314 343 364
71 77 178
T 71 _
145 454 I
377 400896 761478 400896
RIC
359314 454253 1146 bull740
T ~11 400 SCAN300 320 340 360 380
1000 1033 1107 TIME820 853 927
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
403shy
257
DATAJ 0216Z8S 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J
310 1079 3102
346 490
3234
SCANS 300 TO
0 BASE U 20 3
359 565 3136
400
379 398 3155
1098
257077 plusmn 0500
1000shy
377 2724 11870 2724
328 328898 plusmn 0500
2749n 488
RIC
400 SCAN 1107 TIME820 853
300
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
672-1
MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
378 603 1284
J- ( C O lt9 -5~
60 673
328 320036 plusmn 0500
1000-1 1002
322 322036 plusmn 0500
7473mdashi 488
RIC
400 SCAN820 1107 TIME
300
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1
DATA 0216Z85 1 CALI TC 3
40 QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
785shy 1748
332 332099 plusmn 0500
1000n 2228
334 334100 plusmn 0500
336 l-i 7488
RIC
400 SCAN820 1107 TIME
300
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
18-j
DATA 0216Z86 1 CALI TC 3
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J
333 8267 16144
SCANS 300 TO
0 BASE U 20 3 357
11124 18068
400
11136
257 306 3044 15960
257077 plusmn 0500
1000-1
323 606208 1367690
606208
328
306 51072 105522
316 205824 385485
336 933 4267
351 537 924 j
379 5294 15305
392 8394 16868 bull bull
328098 plusmn 0500
1047-1
323 634880 1476660
634880
RIC
306 61568 158436
300 820
316 221696 45b38
332 10048 42600
~1 340 927
350 3136 16192
365 7616 27456
1 360
1060
bull
379 17287 72160 mdashj
380 1033
392 9392 12688
400 SCAN 1107 TIME
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
654-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1
323 2364 9118
40
DATA 9216286 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
2364
320 320096
plusmn 0500
1000-1 Oo6gt 3616
322 322096
plusmn 0500
pound mdash
929 634880 1476668
634880
RIC
306 61568
158436
316 221636 456328
r
I V
332 10048 42609 i
350 3136 18192
365 7616
27456
373 17287 72160
392 9392 12688 bull bull
mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME
300
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
1000-1
MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1
322 20268 39800
40
DATA 0216Z86 1 CALI TC 3
QUAN A 1 10 J 0
SCANS 300 TO
BASE U 20 3
400
20288
332 366 4912
133461884b
379 5624 11060wo
332099 plusmn 0500
213-1 4320
334 334100 plusmn 0500
329 634880 1476660
634880
RIC
300 820
358 3136 10192
360 1000
365 7616 27456
379 17287 72160 ^
380 1033
392 9392 12688 -imdashmdashV
bull bull mdashJ
400 SCAN 1107 TIME
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3
331 5384
35615060 34310001 4429 53844892 8878 16564
257 257077
plusmn 0500
789i 4248
328 328098 plusmn 0500
377 17549
347 77420 13891 17600
3269-1
8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r
3 pound T
300 320 340 360 408 SCAN820 853 927 1000 1107 TIME
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
316 2304
626-1 14061 2668
320 320096 plusmn 0500
10001 4264375
2723 7191
322 322096 plusmn 0500
377 17549
347 77429 13891 17660 80256
4128shy
t316 3613328819 85947662RIC 48631 7664826466 IA
bull n r y bull )
V vI N -vI
-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
laquo raquo
MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3
377 5622
1000H 28000 5720
332 332099
plusmn 0500
377 3470
617-1 14628 3528
334 334100
plusmn 0500
377 17549
3077-1 347 77420 13891 17600
RIC
300 820
316 8819 48691
A ft A
T 320 853
bullA 332 7662 26466 n
80256
v v V v v
361 8594 76648
V
i 1
340 927
360 1000
t t
AAA 400 SCAN
1107 TIME
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808
MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A
377 1 10 J 0 BASE U 20 3
4808