jotun a/s · · 2009-03-06/10/ sfs 8145 – 1989 – anticorrosive painting. surface preparation...

TECHNICAL REPORT

JOTUN A/S

SIMULATED BALLAST TANK TESTING OF JOTACOTE UNIVERSAL ON SWEEP BLASTED ZINC SILICATE SHOP

PRIMED SUBSTRATE

REPORT NO. BGN-R2706231 REVISION NO. 01

DET NORSKE VERITAS

DET NORSKE VERITAS

TECHNICAL REPORT

Head Office: Veritasvn. 1, N-1322 HØVIK, Norway

DET NORSKE VERITAS AS REGION NORDIC COUNTRIES Materials Tech. and Condition Management Johan Berentsens vei 109-111, P.O. Box 7400, N-5020 Bergen, Norway Tel: +47 55 94 36 00 Fax: +47 55 94 36 02 http://www.dnv.com Org. No: NO 945 748 931 MVA

Date of first issue: Project No.:2006-06-07 74527169 Approved by: Organisational unit:Hans-Erik Berge Head of Section

Failure Investigation and Condition Management

Client: Client ref.:Jotun A/S Odd Arntzen / Thoralf Undrum

Summary:

Det Norske Veritas AS has upon the request of Jotun A/S performed simulated ballast tank testing of Jotacote Universal on sweep blasted shop primed substrate.

System specification:

15 - 20 µm Muki Z 2001 grey zinc silicate shop primer (weathered for 2 weeks and then lightly sweep blasted according to SFS 8145 /10/)

150 µm Jotacote Universal Al

150 µm Jotacote Universal Al Grey

The testing has been performed according to the DNV procedure, Testing and classification of ballast tank coatings (revision 2, 2002) /1/.

Jotacote Universal applied to sweep blasted zinc silicate shop primed substrate has been given class B1 in a classification system from B1 to B6, in which B1 is the superior grade.

Report No.: Subject Group:BGN-R2706231 E7 Indexing terms Report title: Key words Service Area

Verification

Market Sector

Simulated ballast tank testing of Jotacote Universal on sweep blasted zinc silicate shop primed substrate

Coatings Testing

Work carried out by: Birgith Schei

Work verified by: Trond Haugen

Date of this revision: Rev. No.: Number of pages:2006-06-07 01 3

No distribution without permission from the client or responsible organisational unit (however, free distribution for internal use within DNV after 3 years)

No distribution without permission from the client or responsible organisational unit.

Strictly confidential Unrestricted distribution

© 2002 Det Norske Veritas AS All rights reserved. This publication or parts thereof may not be reproduced or transmitted in any form or by any means, including photocopying or recording, without the prior written consent of Det Norske Veritas AS.

aacaabn2.doc

DET NORSKE VERITAS

Report No: BGN-R2706231, rev. 01

TECHNICAL REPORT

Table of Content Page

1 INTRODUCTION ....................................................................................................... 1

2 SCOPE OF WORK...................................................................................................... 1

3 WORK CARRIED OUT PRIOR TO EXPOSURE..................................................... 1 3.1 Identification 1 3.2 Application 1 3.2.1 Procedure 1 3.2.2 Coding 1 3.3 Dry film thickness 1 3.4 Pin hole detection 2

4 EXPOSURE CONDITIONS........................................................................................ 2

5 TESTS CARRIED OUT AFTER EXPOSURE........................................................... 2

6 TEST RESULTS.......................................................................................................... 2

7 CONCLUSION............................................................................................................ 3

8 REFERENCES............................................................................................................. 3

Appendix A Test procedure Appendix B Application / Product data Appendix C Detailed test results Appendix D Photo documentation

Page i Reference to part of this report which may lead to misinterpretation is not permissible.

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DET NORSKE VERITAS


TECHNICAL REPORT

1 INTRODUCTION Ballast tanks are generally known to be susceptible to coating degradation and corrosion attacks. Relevant tests have therefore been developed for classification of ballast tank coatings. The coating system Jotacote Universal applied to sweep blasted zinc silicate shop primed substrate has been tested in accordance with the procedures for these tests.

An overview of the procedure is given in Appendix A.

2 SCOPE OF WORK The following work and tests have been performed: • Identification of the coating system • Film thickness measurements and pin hole detection on panels before testing • 180 days testing in condensation chamber • 180 days testing in wave tank • Evaluation of results after testing, including blister detection (when applicable), undercutting

from scribe, adhesion and coating flexibility • Evaluation of cathodic protection during testing (wave tank)

3 WORK CARRIED OUT PRIOR TO EXPOSURE

3.1 Identification The coating system was identified by infrared scanning (by means of a Perkin Elmer FTIR Spectrometer Paragon 1000), by determination of specific gravity (according to ISO 2811–1 /2/ by means of a Erichsen Mod. 290/1 Pyknometer) and by determination of volatile/non-volatile content (according to ISO 3251 /3/).

3.2 Application 3.2.1 Procedure Two coats (specified dry film thickness 150 µm per coat) of Jotacote Universal were applied to the sweep blasted zinc silicate shop primed panels.

The applicability was evaluated by visual examination with regard to application easiness and application pattern.

3.2.2 Coding The panels were coded as shown in Figure B-1, Appendix B.

3.3 Dry film thickness The dry film thickness measurements were carried out by means of an Elcometer 456 dry film thickness unit before testing.

Page 1 Reference to part of this report which may lead to misinterpretation is not permissible.

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DET NORSKE VERITAS


TECHNICAL REPORT

3.4 Pin hole detection Pin hole detection was performed on the coated test panels before testing. The detection was carried out by means of an Elcometer 269 Pinhole detector at 90 volts.

4 EXPOSURE CONDITIONS The testing was carried out according to DNV procedure, Testing and classification of ballast tank coatings (revision 2, 2002) /1/. A summary of the procedure is given in Appendix A.

5 TESTS CARRIED OUT AFTER EXPOSURE Evaluation of blisters and rust, adhesion, undercutting from scribe and flexibility was carried out according to Appendix A, § 5.

6 TEST RESULTS The results of the product identification are given in Table 1.

The application data are given in Appendix B, while the results of the examination of the coated test panels schematically are given in Table 2 and more detailed in Appendix C. Pictures of the panels after exposure are enclosed as Appendix D.

Table 1 Results of analyses (Product identification)

Product Batch no. IR identification

(main components)

Specific gravity (g/cm3)

Volatile / non-volatile components

(% by weight) Jotacote Universal

base Al red 4870615.32.03.78-A Epoxy 1.44 16.2/83.8

Jotacote Universal base Al grey 4870615.32.03.78-A Epoxy 1.43 15.5/84.5

Jotacote Universal cure 4870615.32.03.78-B Amine 0.97 33.4/66.6

Page 2 Reference to part of this report which may lead to misinterpretation is not permissible.

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DET NORSKE VERITAS


TECHNICAL REPORT

Page 3

Table 2 Results of examination of the coated test samples Dry film thickness

(µm) Average

of all panels

Pin holes (number) Measured

on the panel with

anode

Blisters and rust

after testing

All panels 1)

Adhesion values (MPa)

Average - top panel

2)

Corrosion creep from

scribe Average

maximum (mm) 3)

Wave tank panels

Flexibility Average top

panel

Cathodic disbond-

ment (mm)

Weight loss (g) / Current demand (mA/m2)

bottom panel

274 ± 37 0 0 7 3.3 3) ≤ 1.15% 0 0.3352 / 0.90

1) Does not include panels for chloride level test. 2) Confer Table C-3 for details. 3) Evaluated by scraping with a knife. Confer the evaluation in § 7 and the detailed results in Table C-4.

7 CONCLUSION Based on the requirements given in the DNV procedure - Testing and classification of ballast tank coatings - revision 2, 2002 and the results from the testing, Jotacote Universal coating from Jotun A/S applied to zinc silicates shop primed substrate has been given the classification B1 in a classification system from B1 to B6, in which B1 is the superior grade.

8 REFERENCES

/1/ DNV - Testing and classification of ballast tank coatings - revision 2, 2002

/2/ ISO 2811-1, 1997 – Determination of density

/3/ ISO 3251, 2003 – Determination of non-volatile-matter content

/4/ ISO 8502-6, 1995 – Tests for the assessment of surface cleanliness, Extraction of soluble contaminants for analysis – The Bresle method

/5/ ISO 8501-1, 1988 – Rust grades and preparation grades of uncoated steel substrates after overall removal of previous coatings

/6/ ISO 6270, 1980 - Determination of resistance to humidity, continuous condensation

/7/ ISO 4628 – 1982, parts 1, 2 and 3 - Evaluation of degradation of paint coatings

/8/ ISO 4624 – 2002 - Pull-off test for adhesion

/9/ ASTM D522 – 2001 - Standard test methods for mandrel bend test of attached organic coatings

/10/ SFS 8145 – 1989 – Anticorrosive painting. Surface preparation methods of blast cleaned and shop primer coated steel substrates and preparation grades for respective treatments

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Reference to part of this report which may lead to misinterpretation is not permissible.

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DET NORSKE VERITAS

APPENDIX A

TEST PROCEDURE

Page A-1 Report No. BGN-R2706231, rev.

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TESTING OF BALLAST TANK COATINGS - OVERVIEW OF TEST PROCEDURE

1 TEST PANELS • Cold-rolled 3 mm thick steel, grit blasted to Sa 2,5, according to ISO 8501-1:1988 (Swedish

Standard SIS 055900). Painted on the reverse side. • Substrate alternatives:

1. No further treatment 2. Pre-rusted and steel wire brushed / high pressure washed

The panels are pre-rusted in a salt fog chamber. The panels correspond to Rust grade C in ISO 8501-1:1988 after pre-rusting. The panels are then high pressure washed (50-100 bar and 13 ltr freshwater/min) and steel wire brushed to St3 according to the above mentioned standard.

3. Pre-rusted and hydro jetted The panels are pre-rusted in a salt fog chamber. The panels correspond to Rust grade C in ISO 8501-1:1988 after pre-rusting. The panels are then hydro jetted at 2000 bar (30 000 p.s.i.) and quickly dried to avoid flash rust.

4. Moist The panels have a 300 µm WFT Coaltar epoxy applied in a width of approximately 60 mm in the middle of the test panels. The panels are pre-rusted in a salt fog chamber. The surface of the blast cleaned areas of the test panels correspond to Rust Grade C in ISO 8501-1 after pre-rusting. The panels are washed with fresh water at 100 bar. One blast cleaned and pre rusted area is washed only, while the other is wire brushed to St 2 according to ISO 8501-1:1988 (Swedish Standard SIS 055900) after washing. Immediately before application of the test coating the panels are first dipped in distilled water and then stippled with a wet and wrung cotton cloth

5. Shot blasted and shop primed A zinc shop primer with low zinc content is applied to a dry film thickness of 15 - 20 µm, measured on a plane steel panel according to ISO 2808:1991. The shop primed test panels are then exposed to outdoor marine atmosphere for 14 days. Prior to application of the test coating, the shop primed surface is washed with tap water and dried.

• Application of test coating according to the coating producer’s data sheets. • Curing at 18-24 °C and a relative humidity between 40 % and 60 % for 2 weeks before

exposure-testing.

2 TEST METHODS

2.1 Ballast wave tank test In accordance with the DNV procedure, Testing and Classification of Coatings.

Exposure cycles: 2 weeks in seawater with wave movements followed by 1 week with high relative humidity (some seawater left in the bottom of the tank) to a total exposure time as given in § 3.


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A sketch of the test panels are given in Fig. 1, while the test equipment is shown in Fig. 2. A sketch of the test panels are given in Fig. 1, while the test equipment is shown in Fig. 2.

200 mm

BGN-R2706231, rev.

01 01

Fig. 1 The test panels Fig. 1 The test panels

Fig. 2 The wave tank test equipment Fig. 2 The wave tank test equipment

2.2 Condensation chamber test 2.2 Condensation chamber test The test is carried out in accordance with ISO 6270, 1980. The test is carried out in accordance with ISO 6270, 1980.

Test panels Test coating facing towards the tank medium

Heating 12 hours 50 ºC, 12 hours 20 ºC

35 ºC natural seawater

Cooling to give a temperature gradient of 20 ºC through the coating of one of the side panels

Wave movement

The artificial holidays are made down to bare metal by means of a milling cutter

Artificial holiday

400 mm

Artificial holiday

Sacrificial anode The two

side wall panels and the top panel (The side panels have a U-beam)

The bottom panel

U-beam

Page A-3 Report No.

DET NORSKE VERITAS

3 EXPOSURE TIME BALLAST WAVE TANK TEST AND CONDENSATION CHAMBER TEST

• 180 days for coatings applied to blast cleaned panels and shop primed panels.

• 120 days for coatings applied to pre-rusted and hydro jetted panels. • 60 days for coatings applied to pre-rusted and then wire brushed panels and pre-rusted

and then wire brushed, moist panels.

4 PHYSICAL TESTING AFTER EXPOSURE • Flexibility testing.

• Adhesion testing.

5 EVALUATION AND CLASSIFICATION OF COATINGS The evaluation is based on visual examination of blistering, rusting and undercutting from scribe. In addition adhesion and flexibility are determined. The following standards are used:

• ISO 4628 - 1982, parts 1, 2 and 3 • ISO 4624 - 2002 • ASTM D522 – 2001, method B.

The classification is given in Tables 1 and 2. Table 1 Classification of Semi-Hard Coatings

Semi-Hard Coatings classification

Area rusted Area blistered

Class C1 Ri 0 to Ri 1 (0 - 0.05 %) on all panels. Density 0 - 1

Class C2 Ri 2 to Ri 3 (0.5 - 1 %) on top and side wave tank panels, other panels maximum Ri 2 (0.5 %)

Density 2 - 3

Class C3 Ri 3 to Ri 4 (1 - 8 %) on top and side wave tank panels, other panels maximum Ri 3 (1 %)

Density 3 - 4

Class C4 Ri 4 to Ri 5 (8 – 50 %) on top and side wave tank panels, other panels maximum Ri 4 (8 %)

Density 4 - 5

Class C5 Ri 5 (40/50 %) on all panels Density 5

Class C6 More than 50 % of area rusted on all panels Density 5

Note: If under-rusting is revealed, the classification will be affected accordingly.


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Table 2 Classification of hard coatings

Average adhesion, adhesive failure1

Average adhesion cohesive failure2

Hard coatings

Classification system

Area blistered Area rusted

Corrosion creep from scribe (average of max creep –all panels) On blast-

cleaned panels

On all other substrates

On all substrates

Class B1 No blisters Ri 0 (0 %)

Less than 8 mm

Larger than 5 MPa

Larger than 3.5 MPa

Larger than 3 MPa

Class B2 Density 1 – 2 either on any of the wave tank panels or on any of the condensation chamber panels

Ri 1 (0.05 %) on any panel

Less than 10 mm

Larger than 4 MPa

Larger than 3 MPa

Larger than 2.5 MPa

Class B3 Density 1 – 2 on any of the wave tank panels and on any of the condensation chamber panels

Ri 2 (0.5 %) on any panel

Less than 12 mm

Larger than 3 MPa

Larger than 2.5 MPa

Larger than 2 MPa


Ri 3 (1 %) on any panel

Less than 15 mm

Larger than 2.5 MPa

Larger than 2 MPa

Larger than 1.5 MPa

Class B5 Density 3 – 4 on any of the wave tank panels and on any of the condensation chamber panels

Ri 4 (8 %) on any panel

Less than 20 mm

Larger than 2 MPa

Larger than 1.5 MPa

Larger than 1 MPa


Ri 5 (40/50 %) on any panel

Larger than 20 mm

Less than 2 MPa

Less than 1.5 MPa

Less than 1 MPa

1 Adhesive failure between substrate and coating or between coats for 60 % or more of the area. 2 Cohesive failure in coating for 40 % or more of the area.

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APPENDIX B

APPLICATION / PRODUCT DATA

Page B-1 Reference to part of this report which may lead to misinterpretation is not permissible.

20 June 2006, bsc/aacaabn2.doc

DET NORSKE VERITAS

Table B-1 Application data

Coating data: Shop primer 1st coat 2nd coat

Paint system:

Muki Z 2001 grey Jotacote Universal Al

Jotacote Universal Al Grey

Manufacturer: Jotun A/S

Date 31/08 - 05 14/09 - 05 15/09 - 05 Time 13:30 15:20 14:00 Surface preparation Blast cleaning NA NA Blasting standard Sa 2.5 NA NA Abrasive used AlSil A3 + steel shot

S 280 NA NA

Roughness (µm) Rmax 50-85 NA NA Batch No. curing agent A: FR315-110214 4870615.32.03.78-B 4870615.32.03.78-B Batch No. base B: FR345-109464 4870615.32.03.78-A 4870615.32.03.78-A Thinner name (if used) NA Thinner No. 17 Thinner No. 17 Batch No. thinner(if used) NA Not given Not given

Equipment used Graco King 68:1 Graco King 68:1 Graco King 68:1 Air pressure (bar) 100 170 170 Size nozzle (inches) 0.021 0.023 0.023

Fan width (º) 60 60 60

Mix. ratio (volume) A: B = 10 : 6.75 3 : 1 3 : 1 Volume solid (volume) 28 ± 2 72 72 Wet film thickness (µ) 55 - 70 225 225 - 250 Dry film thickness (µ) 15 - 20 150 See Table C1 Thinner (%) NA 3 3 Air temperature (ºC) 21 21 19 Humidity (% RH) 52 54 48 Steel temp. (ºC) 21 Not given Not given Dew point (ºC) 11 11 7 Comments: Present at application: Odd Arntzen and Gøran Holten - Jotun A/S, Jan Erik Fløysand - D&F Group (Painter), Øystein Sæther - DNV

The shop primer was lightly blast cleaned (sweep blasted) according to SFS 8145 /10/ before application of the 1st coat.



DET NORSKE VERITAS

Figure B-1 Test panels and coding

Zinc silicate shop primed J Customer code Condensation chamber 18 DNV code

Reference

Blast cleaned

J18ZR J18ZC1 J18ZC2

J18CC1 J18CC2

Chloride contamination

J18BC1 J18BR

Scribe

Holiday, 8 mm diam.

Anode Scribe Scribe

U-beam U-beam

J18ZW2 J18ZW3 J18ZW4 J18ZW1

Wave tank

Zinc silicate shop primed

Blast cleaned



DET NORSKE VERITAS

APPENDIX C

DETAILED TEST RESULTS

Page C-1 Report No. BGN-R2706231, rev.

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Table C-1 Dry film thickness (µm) Measuring point

J18 ZW1

J18 ZW2

J187 ZW3

J18 ZW4

J18 CC1

J18 CC2

J18 ZC1

J18 ZC2

J18 BC1

J18 ZR

J18 BR Total

1 246 274 294 332 262 224 256 238 266 222 218 2 268 296 350 384 264 238 258 256 250 226 238 3 222 276 274 346 292 264 248 260 284 224 230 4 234 286 276 318 266 228 266 262 292 234 286 5 280 306 314 364 272 222 326 272 256 248 284 6 224 260 280 342 252 214 273 236 298 236 238 7 248 278 272 346 296 280 258 242 252 238 236 8 316 280 304 374 268 258 278 292 246 256 264 9 228 270 280 348 256 254 260 270 248 238 222

10 258 258 286 358 320 274 11 306 296 326 356 246 248 12 256 286 278 344 250 224 13 274 266 276 326 14 294 284 308 316 15 237 272 266 364

Max 316 306 350 384 320 280 326 292 298 256 286 384Min 222 258 266 316 246 214 248 236 246 222 218 214Average 259 279 292 348 270 244 269 259 266 236 246 274StDev 30 14 24 20 22 22 23 18 20 11 26 37

Notes: Dry film thickness measured with Elcometer 456, calibrated on a smooth steel surface (0 point) and on a 511 µm thick foil.

20 µm have been subtracted for substrate correction for the zinc silicate shop primed panels before application of Jotacote Universal and 30 µm for the blast cleaned panels


01

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Figure C-1 Thickness measurement locations Figure C-1 Thickness measurement locations Measurement no.

Panel no.

8 9

6

7

5 4

2 3 1

20 mg NaCl

Panel no.

12 200mg NaCl

11

10

9 100 mg NaCl

8 7

6 50 mg NaCl

5

4

3

2

1

The condensation chamber panels, without salt contamination left, with salt contamination right

15 14 13

Panel no.

12 11 10

9 7 8

4 6 5

2 3 1

The wave tank panels


01 01

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Table C-2 Development of blisters and rust after exposure (according to §5, Appendix A)

Code Description Blister size

Blister density

Rust Comment

J18ZW1 Top wave tank panel with scribe 0 0 0

J18ZW2 Bottom wave tank panel with anode 0 0 0

J187ZW3 Side wave tank panel with scribe and U-beam

Cooling 0 0 0

J18ZW4 Side wave tank panel with scribe and U-beam

No cooling 0 0 0

J18ZC1 Condensation chamber 0 0 0

J18ZC2 Condensation chamber 0 0 0

J18CC1 Chloride level test

20 mg/m2

50 mg/m2

100 mg/m2

200 mg/m2

0

0

4

4

0

0

4

4

0

J18CC2 Chloride level test

20 mg/m2

50 mg/m2

100 mg/m2

200 mg/m2

0

0

4

4

0

0

4

4

0

Reference panels:

J18ZR: Zinc silicate shop primed reference panel

J18BR: Blast cleaned reference panel


01

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Table C-3 Results of the Pull-off Test (adhesion values in MPa)

Panel no. Test no.

Adhesion strength (MPa)

Fracture Average adhesion strength (MPa)

1 6 10 % B, 80 % C, 5 % D, 5 % -/Y

2 6 30 % B, 65 % C, 5 % -/Y

3 6 50 % B, 50 % C

4 7 5 % B, 65 % C, 30 % D

5 7 20 % B, 77 % C, 3 % D

Top wave tank panel

J18ZW1

6 7 20 % B, 75 % C, 5 % D

7

1 6 20 % B, 70 % C, 10 % -/Y

2 6 20 % B, 60 % C, 10 % D, 10 % -/Y

3 7 10 % B, 75 % C, 5 %, 5 % D, 5 % -/Y

4 7 10 % B, 60 % C, 30 % D

5 7 40 % C, 10 % C/D, 40 % D, 10 % -/Y

Reference panel (not exposed) J18ZR (measurements carried out after 6 months of in door exposure)

6 7 10 % B, 50 % C, 5 % C/D, 35 % D

7

A/B Fracture between the steel surface and the shop primer

B Fracture in the shop primer

B/C Fracture between the shop primer and the 1st coat.

C Fracture in the 1st coat.

C/D Fracture between the 1st and 2nd coat.

D Fracture in the 2nd coat

-/Y Fracture between the outer coat and the glue.


01

DET NORSKE VERITAS

Table C-4 Results of physical testing

Panel Corrosion creep from scribe

(mm)1)

Flexibility2) Comment

Top wave tank panel

J18ZW1 3.4 260 mm ≤ 1.15 %

elongation

Cooled side wave tank panel

J18ZW3 1.4 NA NA

Not cooled side wave tank panel

J18ZW4 5.2 NA NA

Reference panel (not exposed)

J18ZR NA 260 mm ≤ 1.15 %

elongation

1) Evaluated by scraping with knife.

2) Flexibility: Minimum diameter of mandrel for which any cracking in the coating occurs.

The diameter of the mandrels used is 260 mm, 150 mm, 75 mm and 40 mm

Table C-5 Results of Cathodic Protection (CP).

Panel Cathodic disbondment 1)

(mm)

Blisters / rust

Rating

Zinc anode

weight loss (g) 2)

Current demand

(mA/ m2) 2)

J18ZW2 0 0 0.3352 0.90

Exposure time: 120 days (Total time 180 days. Each cycle consists of 2 weeks seawater immersion and 1 week exposure in air (See Appendix A))

Utilisation factor: 0.8

Consumption rate for Zn-anodes: 11.3 kg/A year 1) The cathodic disbondment is at present not used in the classification of the coating system. The parameter is being evaluated for inclusion in an upcoming revision 03, and is reported for future reference. 2) During 2002 (due to implementation of revision 02 of the test procedure, Appendix A) a holiday (8 mm diameter) was introduced to ballast tank coat panels with CP, as a part of the development of the test. This causes a higher current demand, as compared to previous measurements where no holiday was created in the coat.

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DET NORSKE VERITAS

APPENDIX D

PHOTO DOCUMENTATION

Page D-1 Report No. BGN-R2706231, rev.

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Fig. D1 The wave tank top panel, panel no. J18ZW1 - Corrosion creep from scribe

Fig. D2 The wave tank cooled side panel, panel no. J18ZW3 - Corrosion creep from scribe

Fig. D3 The wave tank uncooled side panel, panel no. J18ZW4 - Corrosion creep from scribe


01

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Fig. D4 The wave tank bottom panel, panel no. J18ZW2 – Cathodic disbondment


01

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FF

FF

R

Panel

BGN-R2706231, rev. 01 01

Dolly

ig. D5 The wave tank top panel, panel no. ig. D5 The wave tank top panel, panel no.

Panel


Panel


eport No.

J18ZW1 after adhesion testing (adhesion test 1) J18ZW1 after adhesion testing (adhesion test 1)

Dolly

FF


Dolly


Page D-4

DET NORSKE VERITAS
Panel
Dolly

Fig. D8 The wave tank top panel, panel no. J18ZW1 after adhesion testing (adhesion test 4) Fig. D8 The wave tank top panel, panel no. J18ZW1 after adhesion testing (adhesion test 4)

Panel Dolly

BGN-R2706231, rev. 01 01

Fig. D9 The wave tank top panel, panel no. J18ZW1 after adhesion testing (adhesion test 5) Fig. D9 The wave tank top panel, panel no. J18ZW1 after adhesion testing (adhesion test 5)

Panel Dolly

Fig. D10 The wave tank top panel, panel no6) Fig. D10 The wave tank top panel, panel no6)

Report No.

. J18ZW1 after adhesion testing (adhesion test . J18ZW1 after adhesion testing (adhesion test

Page D-5

DET NORSKE VERITAS

Panel

Dolly

Fig. D11 The not exposed reference panel, panel no. J18ZR after adhesion testing (adhesion test 1) Fig. D11 The not exposed reference panel, panel no. J18ZR after adhesion testing (adhesion test 1) Panel

Dolly

Fig. D12 The not exposed reference panel, panel no. J18ZR after adhesion testing (adhesion test 2) Fig. D12 The not exposed reference panel, panel no. J18ZR after adhesion testing (adhesion test 2) Panel

Dolly

Fig. D13 The not exposed reference panel, panel no. J18ZR after adhesion testing (adhesion test 3) Fig. D13 The not exposed reference panel, panel no. J18ZR after adhesion testing (adhesion test 3)


01 01

DET NORSKE VERITAS

BGN-R2706231, rev. 01 01

Fig. D14 The not exposed reference panel, panel no. J18ZR after adhesion testing (adhesion test 4) Fig. D14 The not exposed reference panel, panel no. J18ZR after adhesion testing (adhesion test 4)

Panel

Dolly

Dolly

Fig. D15 The not exposed retest 5) Fig. D15 The not exposed retest 5)

Fig. D16 The not exposed retest 6) Fig. D16 The not exposed retest 6)

Report No.

Panel

ference panel, panel no. J18ZR after adhesion testing (adhesion ference panel, panel no. J18ZR after adhesion testing (adhesion

Panel

Dolly

ference panel, panel no. J18ZR after adhesion testing (adhesion ference panel, panel no. J18ZR after adhesion testing (adhesion

Page D-7

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100 mg NaCl/m2 200 mg NaCl/m2

100 mg NaCl/m2 200 mg NaCl/m2

Fig. D 17 The blisters of the salt contaminated condensation chamber panels after exposure

J18CC1 top, and J18CC2 bottom

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Report No. BGN-R2706231, rev.

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