july 2010 snl blade workshop

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    Program: Recent Results

    Montana State University

    July 20-22, 2010

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    Thanks

    To Sandia/DOE for support since 1989

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    Research Group

    CoPI Research Engineer: Daniel Samborsky,

    Post Doc: Aaron Sears FEA Adhesives

    Grad Student: Tiok Agastra Processing, Complex Structure Coupon Testing and FEA

    Undergraduate Assistants: Patrick Flahertyand David Buswell

    Sandia PIs: Tom Ashwill, Josh Paquette

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    Standard laminates re resentin s ars skins

    Fatigue Topics

    and webs

    Adhesive joints

    Core/sandwich areas Damage growth at flaws

    Ply delamination at details like ply drops and

    joints, and near adhesive joints, , , ,

    Processing effects

    Loading conditions/

    Sandwich Panel

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    Public Database

    at gue ata ase(SNL Website or MSU program

    /composites/) Over 190 Materials 11,500+ test results

    Updates each March ren s ana yze n pu ca ons

    and contractor reports onwebsite; Draft of current

    contractor report

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    More Detailsontractor reports an pu cat ons onwww.coe.montana.edu/composites/; additional informationincluding resins, adhesives, fabrics, etc.

    Contact: [email protected].

    on rac or epor an ecen apers on e s e:1. 2010 Sandia Contractor Report (Draft), Mandell, et al.

    2. 2010 Sandia Blade Workshop Presentation, Mandell.. , , , ,

    Samborsky, paper and presentation, program overview.4. SAMPE 2010, Seattle, paper 398, Agastra and Mandell, Complex StructuredCoupons.

    - -. , , , , ,Laminates.6. AIAA SDM 2010, Orlando, paper AIAA-2010-2821, Sears, et al, Adhesives.

    7. ACS 2010, Cocoa Beach, Selection of Blade Materials, Mandell, Presentation.

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    Presentation Topics

    Summary of recent results:

    1. Standard laminate fati ue:

    fabric and resin effects.. ,

    complex structured coupons

    -

    structures).

    . .

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    Standard Laminate Fatigue

    , = .1. Glass fiber laminates mostsensitive to tensile part offatigue cycles2. Clean failure modesfor materials com arisons

    R = Min Stress/Max Stress

    Ref. 1

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    MSU resin infusion process with hard mold on one side

    (panels also supplied by industry)

    Ref. 1

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    VectorplyELT5500Fabric,FrontandBackViews

    a r c , gsm

    Ref. 5

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    PPG-Devold L1200/G50-E07 (MSU Fabric H, 1261 gsm)

    Front ac

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    Strain-cycles trends for eight MD laminates, UD fabrics1200-2400 gsm, Hybon 2026 sized strands, filament

    , , .

    Studies involving systematic fabricvariation with Devold and OCV in progress

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    Data Representation

    on yc e

    Strain Parameter,Power Law Exponent,

    - ,Polyester (UP) vs

    Epoxy (EP)

    MultidirectionalLaminates;TT: Database Laminate

    Note: Strains shown onfigures are Initial Strainsfrom extensometer in

    [45/0/45/0/45]the first few fatigue

    cyclesRef. 1, 5

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    Resin Comparison, Same Fabrics

    Vinyl esters: intermediatepDCPD (Materia): similar to epoxy

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    UP and EP resins with and w/out 90-strands removedin gage section before infusion, UD laminates

    Significant effect only for UP resin laminates

    epoxy

    polyester

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    Typical Infused Laminate Property RatiosPolyester (UP) to Epoxy (EP)*

    Property Ratio UP/EP

    Axial Tensile Modulus (UD) 1.0

    .

    Axial (UD) Static Tensile Strength 0.90Axial (MD) Static Tensile Strength 0.95

    ransverse tat c ens e rac ngStrain

    0.42

    Axial (UD) 106 Cycle Strain (R = 0.1) 0.51Axial (MD) 106 Cycle Strain (R = 0.1) 0.65

    Axial (MD) 106 Cycle Stress (R = 0.1) 0.61

    Axial (Biax) 106 Cycle strain (R = 0.1) 0.91

    Interlaminar GIc (0-0 interface) 0.55

    Interlaminar GIIc (0-0 interface) 0.48

    ,Threshold Fatigue Strain (R = -1)

    .

    *Vf = 0.5 to 0.6, UD Fabrics D and H, Biax Fabrics M and P

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    Complex Coupons With Ply Drops

    Thi kn T rin

    Ref. 4

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    Delamination TestinMixed Mode Delamination Testing, Different Resins

    Ref. 1, 5

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    Complex Structured Coupons with Ply

    ,Purpose: Mini-substructuretest. Sim lified less costl

    approach to substructuretesting. Efficient comparisonsof resins, fabrics, geometric

    details in structural context..coupons represent morerealistic internal (infused) blade

    standard laminate tests

    Ref. 1, 4

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    Complex Structured Coupon with Ply Drops(See 2009 SDM, AIAA-2009-2411; and 2010 SAMPE paper 398)

    Damage

    ComponentsAlternate Geometries

    Ref. 1, 4

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    Damage Growth Curves

    Static Fatigue, R = 0.1

    Damage Growth with DifferentResins Correlates withInterlaminar G G

    Simulation

    Ref. 4

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    1 PD = 1.3 mmat gue

    (R=0.1, Pmax=55.6 kN)a c

    2 PD = 2.6 mm

    4 PD = 5.2 mm Ref. 1, 4

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    THRESHOLDS

    -results for three resins:epoxy (EP-1), polyester (UP-1)and pDCPD; R = -1.

    Near threshold results (5-mm delamination length L1 in 106 cycles), R = -1,

    ResinMax. Force, kN, and thin

    side average strain (%)

    Force Change

    From EpoxyObserved Damage

    wo p es roppe a one pos on.

    Epoxy EP-1 19 (0.18%) ___ L1, L2, crack at ply ends

    Polyester UP-1 14 (0.13%) -26%L1, L2, biax cracking, crack at

    ply ends

    p . , crac a p y en s

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    Blade

    Initial Test Parameters

    Characterize Nominally Good Quality Joints(Most Contain Significant Porosity)

    Range of Uniaxial Loading Conditions (R-values)

    ange o rac o e x y I II Failure Modes; Crack initiation and Growth

    Strength-lifetime or Fracture Mechanics-da/dN

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    Strength-Lifetime Lap Shear Test

    es ve - , yc es e , yc es r g(Non-symmetrical Specimen Clamped in Hydraulic Grips)

    Ref. 1, 6

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    Simulated blade joint study, see AIAA paper AIAA-2009-1510

    Joint strength statistics and criticalflaws; failure modes; eometr

    Fatigue exponentsPorosity modeling

    Ref. 1, 6

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    ,

    Test,

    Mixed Mode I and II Cracked Lap Sheares

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    Adhesives and GIc from DCB Test

    Designation Adhesive Cure temp GIc, J/m2

    ADH-1Hexion

    ADH-5 Rhino 405 70 938

    ADH-6 3M W1100 70 1626

    DCB Test

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    CLS Adhesive Fracture S ecimens

    Ref. 6

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    Std. 50 mm 100 mm w/steel

    50 mm w/steel G-Calibrations of CLS Specimens

    at 4.45 kN Tension LoadStd. 50 mm

    50 mmw/steel

    100 mmw/steel

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    Adhesive Thickness Effect on Mode Mixit

    0.80

    shortgeometry(2"lap)3.8mm,steel

    0.60

    0.70

    0.5mm1mm2mm

    3.8mm(testedgeom)

    0.5 mm

    0.40

    0.50

    2/

    GT

    8mm 2 mm

    0.20

    0.30

    8 mm

    0.00

    0.10

    0 5 10 15 20 25 30 35 40

    cracklength(mm)

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    Maximum GT (tension half of cycle) vs da/dN, R = -1

    Ref. 6

    ADH 1 Adh i R 0 1 d 1 t d b M d

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    ADH-1 Adhesive, R = 0.1 and -1, separated by ModeMixity Range (reversed loading 10X higher crack velocity)

    R = 0.1 R = -1

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    PreliminaryIn Progress:

    Define static Gc andfatigue crack growth

    range of modes (GI/GII)and R-values experienced

    (data for ADH-1).

    C k P th (N l t C k Di ti )

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    CLS Crack Paths on Section Normal to Crack

    Crack Path (Normal to Crack Direction)

    Direction Near Adhesive / Laminate Interface

    CRACK PATH:

    A. Cohesive in adhesiveB. Cohesive along peel surfaceC. Adhesive along strand surface

    Expanded View of Path B

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    CLS, ADH-1, laminate side CLS, ADH-1, adhesive side

    Peel Surface CLS, ADH-5, laminate side

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    , ,

    Environment

    o e ng

    Further Test Development