kitsault mine project environmental assessment · * mdl adjusted due to sample matrix. all...

KITSAULT MINE PROJECT ENVIRONMENTAL ASSESSMENT

APPENDICES

VE51988 – Appendices

APPENDIX 3 Sediments Analytical Results

ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600

AMEC Earth & Environmental

Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010

Soil Analysis

EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:

Report Date:2227 Douglas Road

10-1182410-1182310-1182210-11821-DLab #: 10-11821

CL Site 2 Comp 1CL Site 1 Comp 3CL Site 1 Comp 2CL Site 1 Comp 1Client ID:Date of CL Site 1 Comp 1

2010-09-03 00:002010-08-31 00:002010-08-31 00:00Lab DuplicateSample Date:Analytical ReferenceAnalysis 2010-08-31 00:00

MDLParameter MethodAnalyst (yyyy/m/d) Units

---*< 0.50*< 0.50*< 0.500.05Acenaphthene EPA 3550/8270CPC 2010/09/14 *< 0.50µg/g (ppm)

---*< 0.50*< 0.50*< 0.500.05Acenaphthylene EPA 3550/8270CPC 2010/09/14 *< 0.50µg/g (ppm)

---*< 0.050*< 0.050*< 0.0500.005Anthracene EPA 3550/8270CPC 2010/09/14 *< 0.050µg/g (ppm)

---*< 1.0*< 1.0*< 1.00.1Benzo(a)anthracene EPA 3550/8270CPC 2010/09/14 *< 1.0µg/g (ppm)

---*< 0.50*< 0.50*< 0.500.05Benzo(a)pyrene EPA 3550/8270CPC 2010/09/14 *< 0.50µg/g (ppm)

---*< 1.00*< 1.00*< 1.000.10Benzo(b)fluoranthene EPA 3550/8270CPC 2010/09/14 *< 1.00µg/g (ppm)

---*< 1.0*< 1.0*< 1.00.12-Methylnaphthalene EPA 3550/8270CPC 2010/09/14 *< 1.0µg/g (ppm)

---*< 0.10*< 0.10*< 0.100.01Chrysene EPA 3550/8270CPC 2010/09/14 *< 0.10µg/g (ppm)

---*< 1.0*< 1.0*< 1.00.1Dibenzo(a,h)anthracene EPA 3550/8270CPC 2010/09/14 *< 1.0µg/g (ppm)

---*< 0.40*< 0.40*< 0.400.04Fluoranthene EPA 3550/8270CPC 2010/09/14 *< 0.40µg/g (ppm)

---*< 0.50*< 0.50*< 0.500.05Fluorene EPA 3550/8270CPC 2010/09/14 *< 0.50µg/g (ppm)

---*< 1.0*< 1.0*< 1.00.1Indeno(1,2,3-cd)pyrene EPA 3550/8270CPC 2010/09/14 *< 1.0µg/g (ppm)

---*< 0.15*< 0.15*< 0.150.015Naphthalene EPA 3550/8270CPC 2010/09/14 *< 0.15µg/g (ppm)

---*< 0.50*< 0.50*< 0.500.05Phenanthrene EPA 3550/8270CPC 2010/09/14 *< 0.50µg/g (ppm)

---*< 0.50*< 0.50*< 0.500.05Pyrene EPA 3550/8270CPC 2010/09/14 *< 0.50µg/g (ppm)

---*< 0.50*< 0.50*< 0.500.05Benzo(k)fluoranthene EPA 3550/8270CPC 2010/09/14 *< 0.50µg/g (ppm)

---*< 0.1*< 0.1*< 0.10.1Benzo(g,h,i)perylene EPA 3550/8270CPC 2010/09/14 *< 0.1µg/g (ppm)

---1111101070.1Surrogate 1 Recovery --PC 2010/09/14 107%

---1231131200.1Surrogate 2 Recovery --PC 2010/09/14 118%

* MDL adjusted due to sample matrix.

All Analytical results pertain to samples analyzed as received.

EPA: U.S. Environmental Protection Agency. 1997. Test Methods of Evaluation of Solid Waste 3rd Ed through Update III. Office Solid Waste Emergency Response, U.S. Environmental

Protection Agency, Washington, D.C.

MDL - Method Detection Limit

Page 1 of 20

** All samples will be disposed of after 30 days following analysis. Please

contact the lab if you require additional sample storage time. (Samples

deemed hazardous will be returned to the client at their own expense or

disposal will be arranged.) **

Report reviewed by:

Jesse Dang, B.Sc.ManagerLaboratory Services

Charlene RollheiserDirector of QA/QCLaboratory Services

ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010

Soil Analysis

EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1182910-1182810-1182710-11826Lab #: 10-11825

Sad Lake Site 1

Comp 3

Sad Lake Site 1

Comp 2

Sad Lake Site 1

Comp 1

CL Site 2 Comp 3Client ID:Date of CL Site 2 Comp 2

2010-09-02 00:002010-09-02 00:002010-09-02 00:002010-09-03 00:00Sample Date:Analytical ReferenceAnalysis 2010-09-03 00:00


------------0.05Acenaphthene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.05Acenaphthylene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.005Anthracene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.1Benzo(a)anthracene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.05Benzo(a)pyrene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.10Benzo(b)fluoranthene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.12-Methylnaphthalene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.01Chrysene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.1Dibenzo(a,h)anthracene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.04Fluoranthene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.05Fluorene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.1Indeno(1,2,3-cd)pyrene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.015Naphthalene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.05Phenanthrene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.05Pyrene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.05Benzo(k)fluoranthene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.1Benzo(g,h,i)perylene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

------------0.1Surrogate 1 Recovery --PC 2010/09/14 ---%

------------0.1Surrogate 2 Recovery --PC 2010/09/14 ---%






Page 2 of 20





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010

Soil Analysis

EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1183410-1183310-1183210-11831Lab #: 10-11830

LLC 2LLC 1SLO3SLO2Client ID:Date of SLO 1



< 0.05< 0.05------0.05Acenaphthene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.05< 0.05------0.05Acenaphthylene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.005< 0.005------0.005Anthracene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.1< 0.1------0.1Benzo(a)anthracene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.05< 0.05------0.05Benzo(a)pyrene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.10< 0.10------0.10Benzo(b)fluoranthene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.1< 0.1------0.12-Methylnaphthalene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.01< 0.01------0.01Chrysene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.1< 0.1------0.1Dibenzo(a,h)anthracene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.04< 0.04------0.04Fluoranthene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.05< 0.05------0.05Fluorene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.1< 0.1------0.1Indeno(1,2,3-cd)pyrene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.015< 0.015------0.015Naphthalene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.05< 0.05------0.05Phenanthrene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.05< 0.05------0.05Pyrene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.05< 0.05------0.05Benzo(k)fluoranthene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

< 0.1< 0.1------0.1Benzo(g,h,i)perylene EPA 3550/8270CPC 2010/09/14 ---µg/g (ppm)

119113------0.1Surrogate 1 Recovery --PC 2010/09/14 ---%

131123------0.1Surrogate 2 Recovery --PC 2010/09/14 ---%






Page 3 of 20





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010

Soil Analysis

EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1183910-1183810-1183710-11836Lab #: 10-11835

Composite SLOComposite SL Site 1Composite CL Site 2Composite CL Site 1Client ID:Date of LLC 3



------------0.05Acenaphthene EPA 3550/8270CPC 2010/09/14 < 0.05µg/g (ppm)

------------0.05Acenaphthylene EPA 3550/8270CPC 2010/09/14 < 0.05µg/g (ppm)

------------0.005Anthracene EPA 3550/8270CPC 2010/09/14 < 0.005µg/g (ppm)

------------0.1Benzo(a)anthracene EPA 3550/8270CPC 2010/09/14 < 0.1µg/g (ppm)

------------0.05Benzo(a)pyrene EPA 3550/8270CPC 2010/09/14 < 0.05µg/g (ppm)

------------0.10Benzo(b)fluoranthene EPA 3550/8270CPC 2010/09/14 < 0.10µg/g (ppm)

------------0.12-Methylnaphthalene EPA 3550/8270CPC 2010/09/14 < 0.1µg/g (ppm)

------------0.01Chrysene EPA 3550/8270CPC 2010/09/14 < 0.01µg/g (ppm)

------------0.1Dibenzo(a,h)anthracene EPA 3550/8270CPC 2010/09/14 < 0.1µg/g (ppm)

------------0.04Fluoranthene EPA 3550/8270CPC 2010/09/14 < 0.04µg/g (ppm)

------------0.05Fluorene EPA 3550/8270CPC 2010/09/14 < 0.05µg/g (ppm)

------------0.1Indeno(1,2,3-cd)pyrene EPA 3550/8270CPC 2010/09/14 < 0.1µg/g (ppm)

------------0.015Naphthalene EPA 3550/8270CPC 2010/09/14 < 0.015µg/g (ppm)

------------0.05Phenanthrene EPA 3550/8270CPC 2010/09/14 < 0.05µg/g (ppm)

------------0.05Pyrene EPA 3550/8270CPC 2010/09/14 < 0.05µg/g (ppm)

------------0.05Benzo(k)fluoranthene EPA 3550/8270CPC 2010/09/14 < 0.05µg/g (ppm)

------------0.1Benzo(g,h,i)perylene EPA 3550/8270CPC 2010/09/14 < 0.1µg/g (ppm)

------------0.1Surrogate 1 Recovery --PC 2010/09/14 112%

------------0.1Surrogate 2 Recovery --PC 2010/09/14 131%






Page 4 of 20





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010

Soil Analysis

EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


Lab #: 10-11840

Client ID: Date of Composite LLC

krikfikfifkrikfikfifSample Date:Analytical Reference krikfikfifkrikfikfifAnalysis 2010-09-01 00:00

krikfikfifkrikfikfifMDLParameter Method krikfikfifkrikfikfifAnalyst (yyyy/m/d) Units

niiiniiiniiiniiiniiiniiiniiiniii0.05Acenaphthene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.05Acenaphthylene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.005Anthracene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.1Benzo(a)anthracene EPA 3550/8270C krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.05Benzo(a)pyrene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.10Benzo(b)fluoranthene EPA 3550/8270C krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.12-Methylnaphthalene EPA 3550/8270C krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.01Chrysene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.1Dibenzo(a,h)anthracene EPA 3550/8270C krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.04Fluoranthene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.05Fluorene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.1Indeno(1,2,3-cd)pyrene EPA 3550/8270C krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.015Naphthalene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.05Phenanthrene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

niiiniiiniiiniiiniiiniiiniiiniii0.05Pyrene EPA 3550/8270C niiiniiiniiiniiiniiiniiiniiiniiiPC 2010/09/14 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.05Benzo(k)fluoranthene EPA 3550/8270C krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.1Benzo(g,h,i)perylene EPA 3550/8270C krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.1Surrogate 1 Recovery -- krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---%

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.1Surrogate 2 Recovery -- krikfikfifkrikfikfifkrikfikfifkrikfikfifPC 2010/09/14 ---%






Page 5 of 20





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010

Soil Analysis - ICP/MS Metals

EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1182410-1182310-1182210-11821-DLab #: 10-11821




25703400333031700.5Sulphur (Total) Carter 15.3.2TY 2010/09/22 3070µg/g (ppm)

311002880027800263001.0Aluminum BCMEBM 2010/09/22 26200µg/g (ppm)

1.81.21.41.40.1Antimony BCMEBM 2010/09/22 1.5µg/g (ppm)

27.020.934.433.10.05Arsenic BCMEBM 2010/09/22 28.9µg/g (ppm)

2171681911960.1Barium BCMEBM 2010/09/22 181µg/g (ppm)

1.01.01.11.00.1Beryllium BCMEBM 2010/09/22 1.1µg/g (ppm)

0.50.80.4*< 0.40.1Bismuth BCMEBM 2010/09/22 *< 0.4µg/g (ppm)

1.83.16.26.90.5Boron BCMEBM 2010/09/22 8.4µg/g (ppm)

3.631.251.411.240.01Cadmium BCMEBM 2010/09/22 1.32µg/g (ppm)

51703350282028205Calcium BCMEBM 2010/09/22 2500µg/g (ppm)

47.743.444.141.10.05Chromium BCMEBM 2010/09/22 35.1µg/g (ppm)

57.61061231200.05Cobalt BCMEBM 2010/09/22 104µg/g (ppm)

54.327380.169.10.01Copper BCMEBM 2010/09/22 59.7µg/g (ppm)

824002050002780001920005Iron BCMEBM 2010/09/22 188000µg/g (ppm)

38.551565.749.60.10Lead BCMEBM 2010/09/22 44.4µg/g (ppm)

63602740290027301Magnesium BCMEBM 2010/09/22 2340µg/g (ppm)

36305570574070400.10Manganese BCMEBM 2010/09/22 7000µg/g (ppm)

0.130.140.190.170.02Mercury EPA 7471ALL 2010/09/22 0.16µg/g (ppm)

8.95.75.05.40.1Molybdenum BCMEBM 2010/09/22 5.0µg/g (ppm)

11780.882.377.30.10Nickel BCMEBM 2010/09/22 66.1µg/g (ppm)

10902170258025605.0Phosphorus BCMEBM 2010/09/22 2170µg/g (ppm)

5084645715661Potassium BCMEBM 2010/09/22 486µg/g (ppm)

2.883.364.104.000.01Selenium BCMEBM 2010/09/22 3.37µg/g (ppm)

0.361.620.990.910.05Silver BCMEBM 2010/09/22 0.76µg/g (ppm)

132145114991Sodium BCMEBM 2010/09/22 83µg/g )ppm)

43.927.322.522.30.50Strontium BCMEBM 2010/09/22 19.7µg/g (ppm)

0.320.200.350.420.05Thallium BCMEBM 2010/09/22 0.41µg/g (ppm)

2.81887.73.70.1Tin BCMEBM 2010/09/22 3.4µg/g (ppm)

2001762532250.5Titanium BCMEBM 2010/09/22 194µg/g (ppm)

39.333.833.831.90.05Vanadium BCMEBM 2010/09/22 26.9µg/g (ppm)

Page 6 of 20





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ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600

* MDL adjusted due to sample matrix interference.


BCME (Metals): British Columbia Ministry of Environment - Contaminated Sites Regulation, SALM Analytical Method 8, v1.0, 2001

BCME (pH1:1): British Columbia Ministry of Environment - Contaminated Sites Regulation, pH (1:1H2O), Method PHSED, v1.0, 2000. Note: All pH samples were extracted at a ratio of 1:2

H2O due to sample matrix.

Carter: Carter, Martin R., 2008. Soil Sampling and Methods of Analysis, Canadian Society of Soil Science. Ottawa




Page 7 of 20





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010


EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1182910-1182810-1182710-11826Lab #: 10-11825

Sad Lake Site 1

Comp 3

Sad Lake Site 1

Comp 2

Sad Lake Site 1

Comp 1








1381591512900.1Barium BCMEBM 2010/09/22 313µg/g (ppm)


*< 0.40.20.20.50.1Bismuth BCMEBM 2010/09/22 1.1µg/g (ppm)

2.31.91.92.10.5Boron BCMEBM 2010/09/22 2.8µg/g (ppm)




15.617.920.364.40.05Cobalt BCMEBM 2010/09/22 70.9µg/g (ppm)

35.652.554.462.10.01Copper BCMEBM 2010/09/22 90.4µg/g (ppm)


15.423.424.240.60.10Lead BCMEBM 2010/09/22 56.0µg/g (ppm)




2.13.13.18.60.1Molybdenum BCMEBM 2010/09/22 17.7µg/g (ppm)

34.938.540.51320.10Nickel BCMEBM 2010/09/22 151µg/g (ppm)




*< 0.400.480.470.370.05Silver BCMEBM 2010/09/22 0.62µg/g (ppm)



*< 0.400.170.160.310.05Thallium BCMEBM 2010/09/22 0.37µg/g (ppm)

0.70.70.94.30.1Tin BCMEBM 2010/09/22 6.2µg/g (ppm)

83.359.863.11930.5Titanium BCMEBM 2010/09/22 231µg/g (ppm)


Page 8 of 20





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ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600










Page 9 of 20





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010


EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1183410-1183310-1183210-11831Lab #: 10-11830








69.552.11903000.1Barium BCMEBM 2010/09/22 222µg/g (ppm)


32.738.10.30.50.1Bismuth BCMEBM 2010/09/22 0.2µg/g (ppm)

< 0.5< 0.51.13.40.5Boron BCMEBM 2010/09/22 1.3µg/g (ppm)




28.228.353.12530.05Cobalt BCMEBM 2010/09/22 84.4µg/g (ppm)

12312599.91430.01Copper BCMEBM 2010/09/22 78.1µg/g (ppm)


41542070.01130.10Lead BCMEBM 2010/09/22 74.8µg/g (ppm)




4093964.98.40.1Molybdenum BCMEBM 2010/09/22 5.1µg/g (ppm)

91.484.671.490.50.10Nickel BCMEBM 2010/09/22 69.6µg/g (ppm)




9.099.872.042.320.05Silver BCMEBM 2010/09/22 1.43µg/g (ppm)



0.210.200.500.800.05Thallium BCMEBM 2010/09/22 0.43µg/g (ppm)

7.44.10.64.10.1Tin BCMEBM 2010/09/22 0.7µg/g (ppm)

50845572.31130.5Titanium BCMEBM 2010/09/22 67.9µg/g (ppm)


Page 10 of 20





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ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600










Page 11 of 20





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988

9/9/2010


EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1183910-1183810-1183710-11836Lab #: 10-11835




------------0.5Sulphur (Total) Carter 15.3.2TY 2010/09/22 8840µg/g (ppm)

------------1.0Aluminum BCMEBM 2010/09/22 13800µg/g (ppm)

------------0.1Antimony BCMEBM 2010/09/22 6.2µg/g (ppm)

------------0.05Arsenic BCMEBM 2010/09/22 25.2µg/g (ppm)

------------0.1Barium BCMEBM 2010/09/22 87.2µg/g (ppm)

------------0.1Beryllium BCMEBM 2010/09/22 0.4µg/g (ppm)

------------0.1Bismuth BCMEBM 2010/09/22 22.6µg/g (ppm)

------------0.5Boron BCMEBM 2010/09/22 < 0.5µg/g (ppm)

------------0.01Cadmium BCMEBM 2010/09/22 13.5µg/g (ppm)

------------5Calcium BCMEBM 2010/09/22 8030µg/g (ppm)

------------0.05Chromium BCMEBM 2010/09/22 55.9µg/g (ppm)

------------0.05Cobalt BCMEBM 2010/09/22 20.2µg/g (ppm)

------------0.01Copper BCMEBM 2010/09/22 90.3µg/g (ppm)

------------5Iron BCMEBM 2010/09/22 40700µg/g (ppm)

------------0.10Lead BCMEBM 2010/09/22 288µg/g (ppm)

------------1Magnesium BCMEBM 2010/09/22 10000µg/g (ppm)

------------0.10Manganese BCMEBM 2010/09/22 853µg/g (ppm)

------------0.02Mercury EPA 7471ALL 2010/09/22 0.08µg/g (ppm)

------------0.1Molybdenum BCMEBM 2010/09/22 419µg/g (ppm)

------------0.10Nickel BCMEBM 2010/09/22 67.1µg/g (ppm)

------------5.0Phosphorus BCMEBM 2010/09/22 1580µg/g (ppm)

------------1Potassium BCMEBM 2010/09/22 2020µg/g (ppm)

------------0.01Selenium BCMEBM 2010/09/22 1.85µg/g (ppm)

------------0.05Silver BCMEBM 2010/09/22 5.99µg/g (ppm)

------------1Sodium BCMEBM 2010/09/22 250µg/g )ppm)

------------0.50Strontium BCMEBM 2010/09/22 45.0µg/g (ppm)

------------0.05Thallium BCMEBM 2010/09/22 0.20µg/g (ppm)

------------0.1Tin BCMEBM 2010/09/22 1.0µg/g (ppm)

------------0.5Titanium BCMEBM 2010/09/22 516µg/g (ppm)

------------0.05Vanadium BCMEBM 2010/09/22 44.5µg/g (ppm)

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EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


Lab #: 10-11840




krikfikfifkrikfikfifkrikfikfifkrikfikfif0.5Sulphur (Total) Carter 15.3.2 krikfikfifkrikfikfifkrikfikfifkrikfikfifLL 2010/09/20 ---µg/g (ppm)

krikfikfifkrikfikfif1.0Aluminum BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.1Antimony BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.05Arsenic BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.1Barium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.1Beryllium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.1Bismuth BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.5Boron BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.01Cadmium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif5Calcium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.05Chromium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.05Cobalt BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.01Copper BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

niiiniii5Iron BCME niiiniiiBM 2010/09/22 ---µg/g (ppm)

niiiniii0.10Lead BCME niiiniiiBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif1Magnesium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.10Manganese BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

niiiniiiniiiniii0.02Mercury EPA 7471A niiiniiiniiiniiiLL 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.1Molybdenum BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.10Nickel BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif5.0Phosphorus BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif1Potassium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.01Selenium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.05Silver BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif1Sodium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g )ppm)

krikfikfifkrikfikfif0.50Strontium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.05Thallium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

niiiniii0.1Tin BCME niiiniiiBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.5Titanium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfif0.05Vanadium BCME krikfikfifkrikfikfifBM 2010/09/22 ---µg/g (ppm)

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EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1182410-1182310-1182210-11821-DLab #: 10-11821




3882511941790.5Zinc BCMEBM 2010/09/22 154µg/g (ppm)

5.37---------0.10pH (1:1 H2O) BC BCMERC 2010/09/22 5.47pH units










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File No.:

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Attention:


10-1182910-1182810-1182710-11826Lab #: 10-11825

Sad Lake Site 1

Comp 3

Sad Lake Site 1

Comp 2

Sad Lake Site 1

Comp 1




98.31171203980.5Zinc BCMEBM 2010/09/22 490µg/g (ppm)

5.205.265.275.410.10pH (1:1 H2O) BC BCMERC 2010/09/22 5.26pH units










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EC-59337

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File No.:

Date Received:

Project No.

Attention:


10-1183410-1183310-1183210-11831Lab #: 10-11830




5886721301680.5Zinc BCMEBM 2010/09/22 131µg/g (ppm)

6.626.515.636.610.10pH (1:1 H2O) BC BCMERC 2010/09/22 5.85pH units










Page 18 of 20





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EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1183910-1183810-1183710-11836Lab #: 10-11835




------------0.5Zinc BCMEBM 2010/09/22 526µg/g (ppm)

------------0.10pH (1:1 H2O) BC BCMERC 2010/09/22 7.18pH units










Page 19 of 20





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EC-59337

10/1/2010

File No.:

Date Received:

Project No.

Attention:


Lab #: 10-11840




niiiniii0.5Zinc BCME niiiniiiBM 2010/09/22 ---µg/g (ppm)

krikfikfifkrikfikfifkrikfikfifkrikfikfif0.10pH (1:1 H2O) BC BCME krikfikfifkrikfikfifkrikfikfifkrikfikfifRC 2010/09/22 ---pH units










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Attention: Horne, Brad

Project No. VE51988

10/1/2010

File No.: EC-59337

Quality Control Standard

Report Date:

Analyst

Date of

Analysis

(yyyy/m/d)

Analytical

Parameter Units

Reference

Method MDL

Analyzed

Value

Advisory

Range

Target

Value

Reference

No.

0.60PC 9/14/2010 EPA 3550/8270C 0.05 0.215-0.840µg/g (ppm) 0.63 HS3BAcenaphthene

1.25PC 9/14/2010 EPA 3550/8270C 0.05 0.616-1.34µg/g (ppm) 0.76 HS3BAcenaphthylene

2.76PC 9/14/2010 EPA 3550/8270C 0.050 0.68-3.21µg/g (ppm) 1.86 HS3BAnthracene

7.91PC 9/14/2010 EPA 3550/8270C 0.1 4.35-8.82µg/g (ppm) 5.8 HS3BBenzo(a)anthracene

5.80PC 9/14/2010 EPA 3550/8270C 0.05 2.81-7.34µg/g (ppm) 4.8 HS3BBenzo(a)pyrene

12.80PC 9/14/2010 EPA 3550/8270C 0.10 5.91-28.00µg/g (ppm) 10.5 HS3BBenzo(b)fluoranthene

8.77PC 9/14/2010 EPA 3550/8270C 0.05 6.15-12.01µg/g (ppm) 6.83 HS3BChrysene

0.89PC 9/14/2010 EPA 3550/8270C 0.1 0.41-1.83µg/g (ppm) 0.6 HS3BDibenzo(a,h)anthracene

25.33PC 9/14/2010 EPA 3550/8270C 0.05 17.08-39.33µg/g (ppm) 17.7 HS3BFluoranthene

3.68PC 9/14/2010 EPA 3550/8270C 0.1 2.392-4.968µg/g (ppm) 3.3 HS3BIndeno(1,2,3-cd)pyrene

2.14PC 9/14/2010 EPA 3550/8270C 0.050 0.623-2.37µg/g (ppm) 1.3 HS3BNaphthalene

18.80PC 9/14/2010 EPA 3550/8270C 0.05 10.92-22.68µg/g (ppm) 15 HS3BPhenanthrene

18.00PC 9/14/2010 EPA 3550/8270C 0.05 11.66-27.01µg/g (ppm) 12 HS3BPyrene

12.80PC 9/14/2010 EPA 3550/8270C 0.10 5.91-28.00µg/g (ppm) 10.5 HS3BBenzo(k)fluoranthene

3.88PC 9/14/2010 EPA 3550/8270C 0.1 2.39-5.48µg/g (ppm) 3.0 HS3BBenzo(g,h,i)perylene* MDL adjusted due to sample matrix.


EPA: U.S. Environmental Protection Agency. 1997. Test Methods of Evaluation of Solid Waste 3rd Ed through Update III. Office Solid Waste Emergency Response, U.S. Environmental Protection

Agency, Washington, D.C.


Page 1 of 3

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AMEC Earth & Environmental has been accredited by the Canadian

Association for Environmental Analytical Laboratories (CAEAL) Inc. to

ISO/IEC 17025 for specific tests registered with the Association.

Scope of accreditation number 2349.





ANALYTICAL REPORT

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Project No. VE51988

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File No.: EC-59337


Report Date:

Analyst

Date of

Analysis

(yyyy/m/d)

Analytical

Parameter Units

Reference

Method MDL

Analyzed

Value

Advisory

Range

Target

Value

Reference

No.

1,400.00LL 9/20/2010 BCME/EPA 6010 0.5 1200-1700µg/g (ppm) 1430 SS#13Sulphur (Total)

10,600.00BM 9/22/2010 BCME 5.0 5550-15600µg/g (ppm) 12700 ERA D066-540Aluminum

103.00BM 9/22/2010 BCME 0.1 51.5-154.5µg/g (ppm) 151 ERA D066-540Antimony

107.00BM 9/22/2010 BCME 0.50 85.1-128µg/g (ppm) 120 ERA D066-540Arsenic

331.00BM 9/22/2010 BCME 1.0 262-400µg/g (ppm) 386 ERA D066-540Barium

74.10BM 9/22/2010 BCME 0.1 60.5-87.8µg/g (ppm) 79.1 ERA D066-540Beryllium

100.00BM 9/22/2010 BCME 0.5 90-110µg/L (ppb) 99.4 MS-CCV-HIGHBismuth

152.00BM 9/22/2010 BCME 0.5 112-192µg/g (ppm) 150 ERA D066-540Boron

244.00BM 9/22/2010 BCME 0.10 200-288µg/g (ppm) 280 ERA D066-540Cadmium

9,690.00BM 9/22/2010 BCME 5 7980-11400µg/g (ppm) 11100 ERA D066-540Calcium

80.60BM 9/22/2010 BCME 0.50 64.1-97µg/g (ppm) 91.0 ERA D066-540Chromium

58.80BM 9/22/2010 BCME 0.50 70.3-101µg/g (ppm) 97.0 ERA D066-540Cobalt

65.30BM 9/22/2010 BCME 0.10 52.5-78.1µg/g (ppm) 72.7 ERA D066-540Copper

18,400.00BM 9/22/2010 BCME 5 9310-27500µg/g (ppm) 23300 ERA D066-540Iron

107.00BM 9/22/2010 BCME 0.50 85.9-128µg/g (ppm) 123 ERA D066-540Lead

4,100.00BM 9/22/2010 BCME 1 3060-5130µg/g (ppm) 4630 ERA D066-540Magnesium

452.00BM 9/22/2010 BCME 0.50 365-539µg/g (ppm) 497 ERA D066-540Manganese

0.09LL 9/22/2010 EPA 7471A 0.02 0.08-0.11µg/g (ppm) 0.09 Mess-3Mercury

47.20BM 9/22/2010 BCME 0.5 36.8-57.5µg/g (ppm) 53.1 ERA D066-540Molybdenum

96.80BM 9/22/2010 BCME 0.50 77.2-116µg/g (ppm) 111 ERA D066-540Nickel

1,058.50BM 9/22/2010 BCME 5.0 882-1235µg/g (ppm) 998 SS#8Phosphorus

4,490.00BM 9/22/2010 BCME 5 3240-5740µg/g (ppm) 5020 ERA D066-540Potassium

177.00BM 9/22/2010 BCME 0.50 139-216µg/g (ppm) 208 ERA D066-540Selenium

46.20BM 9/22/2010 BCME 0.10 30.6-61.8µg/g (ppm) 53.3 ERA D066-540Silver

1,060.00BM 9/22/2010 BCME 1 782-1340µg/g (ppm) 1120 ERA D066-540Sodium

103.00BM 9/22/2010 BCME 0.50 81.7-125µg/g (ppm) 111 ERA D066-540Strontium

272.00BM 9/22/2010 BCME 0.50 220-325µg/g (ppm) 309 ERA D066-540Thallium

183.00BM 9/22/2010 BCME 0.5 141-224µg/g (ppm) 217 ERA D066-540Tin

409.00BM 9/22/2010 BCME 0.5 132-686µg/g (ppm) 472 ERA D066-540Titanium

115.00BM 9/22/2010 BCME 0.20 91.5-138µg/g (ppm) 133 ERA D066-540Vanadium

378.00BM 9/22/2010 BCME 0.5 296-460µg/g (ppm) 455 ERA D066-540Zinc

7.59RC 9/22/2010 BCME 0.01 6.831-8.349---- 7.67 SS#15pH (1:1 H2O) BC

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BCME (pH1:1): British Columbia Ministry of Environment - Contaminated Sites Regulation, pH (1:1H2O), Method PHSED, v1.0, 2000. Note: All pH samples were extracted at a ratio of 1:2 H2O

due to sample matrix.





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ANALYTICAL REPORT

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Burnaby, BC V5C 5A9

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VE51988.200.05

9/10/2010


EC-59369

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1204810-1204710-1204610-12045-DLab #: 10-12045

Composite ULCULC-3ULC-2ULC-1Client ID:Date of ULC-1



---716195022300.5Sulphur (Total) Carter 15.3.2LL 2010/09/20 2510µg/g (ppm)

---2700022400241001.0Aluminum BCMEBM 2010/09/22 24600µg/g (ppm)

---0.46.77.80.1Antimony BCMEBM 2010/09/22 7.6µg/g (ppm)

---16.82703440.05Arsenic BCMEBM 2010/09/22 349µg/g (ppm)

---1391812170.1Barium BCMEBM 2010/09/22 211µg/g (ppm)

---1.21.01.10.1Beryllium BCMEBM 2010/09/22 1.1µg/g (ppm)

---0.11.01.30.1Bismuth BCMEBM 2010/09/22 1.2µg/g (ppm)

---< 0.5< 0.5< 0.50.5Boron BCMEBM 2010/09/22 < 0.5µg/g (ppm)

---0.283.775.190.01Cadmium BCMEBM 2010/09/22 4.84µg/g (ppm)

---1320547071605Calcium BCMEBM 2010/09/22 6910µg/g (ppm)

---56.278.887.20.05Chromium BCMEBM 2010/09/22 88.8µg/g (ppm)

---36.836.244.10.05Cobalt BCMEBM 2010/09/22 44.7µg/g (ppm)

---30.31541100.01Copper BCMEBM 2010/09/22 111µg/g (ppm)

---4310068900795005Iron BCMEBM 2010/09/22 81000µg/g (ppm)

---15.31091200.10Lead BCMEBM 2010/09/22 115µg/g (ppm)

---707013700160001Magnesium BCMEBM 2010/09/22 16200µg/g (ppm)

---1610332038100.10Manganese BCMEBM 2010/09/22 3870µg/g (ppm)

---0.080.040.060.02Mercury EPA 7471ALL 2010/09/22 0.05µg/g (ppm)

---3.25.86.40.1Molybdenum BCMEBM 2010/09/22 6.4µg/g (ppm)

---50.61241550.10Nickel BCMEBM 2010/09/22 157µg/g (ppm)

---744122014705.0Phosphorus BCMEBM 2010/09/22 1490µg/g (ppm)

---429133016201Potassium BCMEBM 2010/09/22 1640µg/g (ppm)

---0.813.044.060.01Selenium BCMEBM 2010/09/22 4.14µg/g (ppm)

---0.051.872.720.05Silver BCMEBM 2010/09/22 2.63µg/g (ppm)

---542022601Sodium BCMEBM 2010/09/22 263µg/g )ppm)

---12.139.753.40.50Strontium BCMEBM 2010/09/22 51.8µg/g (ppm)

---0.190.250.310.05Thallium BCMEBM 2010/09/22 0.31µg/g (ppm)

---1.011.51.30.1Tin BCMEBM 2010/09/22 1.3µg/g (ppm)

---44.04295470.5Titanium BCMEBM 2010/09/22 558µg/g (ppm)

---47.258.770.70.05Vanadium BCMEBM 2010/09/22 72.4µg/g (ppm)

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BCME (pH1:1): British Columbia Ministry of Environment - Contaminated Sites Regulation, pH (1:1H2O), Method PHSED, v1.0, 2000. Note: All samples were extracted at a ratio of 1:2






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EC-59369

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1204810-1204710-1204610-12045-DLab #: 10-12045

Composite ULCULC-3ULC-2ULC-1Client ID:Date of ULC-1



---1073764330.5Zinc BCMEBM 2010/09/22 436µg/g (ppm)

---5.276.236.660.10pH (1:1 H2O) BC BCMERC 2010/09/22 6.51pH units









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Project No. VE51988.200.05

10/1/2010

File No.: EC-59369


Report Date:

Analyst

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Analysis

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Analytical

Parameter Units

Reference

Method MDL

Analyzed

Value

Advisory

Range

Target

Value

Reference

No.
































7.59RC 9/22/2010 BCME 0.01 6.831-8.349---- 7.67 SS#15pH (1:1 H2O) BC

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BCME (pH1:1): British Columbia Ministry of Environment - Contaminated Sites Regulation, pH (1:1H2O), Method PHSED, v1.0, 2000. Note: All samples were extracted at a ratio of 1:2 H2O due to

sample matrix.





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VE51988.200.005

9/14/2010


EC-59383

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1211310-1211210-12111Lab #: 10-12110

Composite SLISLI-3SLI-2Client ID: Date of SLI-1

2010-09-11 00:002010-09-11 00:002010-09-11 00:00Sample Date:Analytical Reference krikfikfifAnalysis 2010-09-11 00:00

MDLParameter Method krikfikfifAnalyst (yyyy/m/d) Units

---16606790.5Sulphur (Total) Carter 15.3.2 krikfikfifkrikfikfifTY 2010/09/22 711µg/g (ppm)

---22700243001.0Aluminum BCME krikfikfifBM 2010/09/22 24900µg/g (ppm)

---6.50.50.1Antimony BCME krikfikfifBM 2010/09/22 0.4µg/g (ppm)

---25525.90.05Arsenic BCME krikfikfifBM 2010/09/22 10.0µg/g (ppm)

---1961770.1Barium BCME krikfikfifBM 2010/09/22 155µg/g (ppm)

---1.01.00.1Beryllium BCME krikfikfifBM 2010/09/22 1.1µg/g (ppm)

---1.20.10.1Bismuth BCME krikfikfifBM 2010/09/22 0.1µg/g (ppm)

---< 0.5< 0.50.5Boron BCME krikfikfifBM 2010/09/22 < 0.5µg/g (ppm)

---4.010.680.01Cadmium BCME krikfikfifBM 2010/09/22 0.32µg/g (ppm)

---604021105Calcium BCME krikfikfifBM 2010/09/22 1730µg/g (ppm)

---95.545.40.05Chromium BCME krikfikfifBM 2010/09/22 59.0µg/g (ppm)

---40.564.00.05Cobalt BCME krikfikfifBM 2010/09/22 26.6µg/g (ppm)

---26157.70.01Copper BCME krikfikfifBM 2010/09/22 26.7µg/g (ppm)

---68600783005Iron BCME niiiBM 2010/09/22 30300µg/g (ppm)

---13221.30.10Lead BCME niiiBM 2010/09/22 18.5µg/g (ppm)

---1460060101Magnesium BCME krikfikfifBM 2010/09/22 7550µg/g (ppm)

---3590143000.10Manganese BCME krikfikfifBM 2010/09/22 1810µg/g (ppm)

---0.040.080.02Mercury EPA 7471A niiiniiiLL 2010/09/22 0.09µg/g (ppm)

---6.53.70.1Molybdenum BCME krikfikfifBM 2010/09/22 3.5µg/g (ppm)

---14352.80.10Nickel BCME krikfikfifBM 2010/09/22 50.0µg/g (ppm)

---12706385.0Phosphorus BCME krikfikfifBM 2010/09/22 773µg/g (ppm)

---14304711Potassium BCME krikfikfifBM 2010/09/22 500µg/g (ppm)

---2.840.640.01Selenium BCME krikfikfifBM 2010/09/22 0.77µg/g (ppm)

---2.15*< 0.100.05Silver BCME krikfikfifBM 2010/09/22 0.33µg/g (ppm)

---218471Sodium BCME krikfikfifBM 2010/09/22 67µg/g )ppm)

---45.019.20.50Strontium BCME krikfikfifBM 2010/09/22 15.3µg/g (ppm)

---0.280.170.05Thallium BCME krikfikfifBM 2010/09/22 0.21µg/g (ppm)

---39.75.40.1Tin BCME niiiBM 2010/09/22 1.0µg/g (ppm)

---41064.20.5Titanium BCME krikfikfifBM 2010/09/22 45.3µg/g (ppm)

---62.735.90.05Vanadium BCME krikfikfifBM 2010/09/22 46.4µg/g (ppm)

Page 1 of 3





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600










Page 2 of 3





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


Burnaby, BC V5C 5A9

Horne, Brad

VE51988.200.005

9/14/2010


EC-59383

10/1/2010

File No.:

Date Received:

Project No.

Attention:


10-1211310-1211210-12111Lab #: 10-12110

Composite SLISLI-3SLI-2Client ID: Date of SLI-1

2010-09-11 00:002010-09-11 00:002010-09-11 00:00Sample Date:Analytical Reference krikfikfifAnalysis 2010-09-11 00:00

MDLParameter Method krikfikfifAnalyst (yyyy/m/d) Units

---4541200.5Zinc BCME niiiBM 2010/09/22 97.1µg/g (ppm)

---6.385.290.10pH (1:1 H2O) BC BCME krikfikfifkrikfikfifRC 2010/09/22 5.39pH units










Page 3 of 3





Report reviewed by:



ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600


2227 Douglas Road

Burnaby, BC V5C 5A9


Project No. VE51988.200.005

10/1/2010

File No.: EC-59383


Report Date:

Analyst

Date of

Analysis

(yyyy/m/d)

Analytical

Parameter Units

Reference

Method MDL

Analyzed

Value

Advisory

Range

Target

Value

Reference

No.
































7.59RC 9/22/2010 BCME 0.01 6.831-8.349---- 7.67 SS#15pH (1:1 H2O) BC

Page 1 of 2

Report reviewed by:











ANALYTICAL REPORT

5667 - 70 Street

Edmonton, Alberta

Canada T6B 3P6

Tel: (780) 436-2152

Fax: (780) 377-3600




BCME (pH1:1): British Columbia Ministry of Environment - Contaminated Sites Regulation, pH (1:1H2O), Method PHSED, v1.0, 2000. Note: All samples were extracted at a ratio of 1:2 H2O due to

sample matrix.





Page 2 of 2

Report reviewed by:











DRAFT

[This report shall not be reproduced except in full without the written authority of the Laboratory.]

EC-59337252652

Job Reference: Project P.O. #:

Legal Site Desc: C of C Numbers:

15-SEP-10

Lab Work Order #: L931614

Date Received:AMEC EARTH & ENVIRONMENTAL

5667 - 70 STREETEDMONTON AB T6B 3P6

ATTN: JESSE DANG ~ CHEMISTRYDRAFT 29-SEP-10 15:34 (MT)Report Date:

Version:

Certificate of Analysis

ALS CANADA LIMITED Part of the ALS Group A Campbell Brothers Limited Company

____________________________________________

Maureen OlinekSenior Account Manager

ADDRESS: 9936-67 Avenue, Edmonton, AB T6E 0P5 Canada | Phone: +1 780 413 5227 | Fax: +1 780 437 2311

Phone: 780-436-2152

DRAFT

ALS LABORATORY GROUP ANALYTICAL REPORT

L931614 CONTD....

2PAGE

Result D.L. Units Extracted AnalyzedSample Details/Parameters

of

EC-59337

Qualifier* Batch

* Refer to Referenced Information for Qualifiers (if any) and Methodology.

4

L931614-1

L931614-2

L931614-3

L931614-4

L931614-5

L931614-6

L931614-10

L931614-11

CL SITE 1 COMP 1~10-11821



LLC 1~10-11833

LLC 2~10-11834

LLC 3~10-11835

COMPOSITE SLO SITE~10-11839

COMPOSITE LLC SITE~10-11840

CLIENT on 31-AUG-10

CLIENT on 31-AUG-10

CLIENT on 31-AUG-10

CLIENT on 01-SEP-10

CLIENT on 01-SEP-10

CLIENT on 01-SEP-10

CLIENT on 01-SEP-10

CLIENT on 01-SEP-10

Sampled By:

Sampled By:

Sampled By:

Sampled By:

Sampled By:

Sampled By:

Sampled By:

Sampled By:

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

Miscellaneous Parameters






Total Organic Carbon






% Gravel (>2mm)% Sand (2.00mm - 1.00mm)% Sand (1.00mm - 0.50mm)% Sand (0.50mm - 0.25mm)% Sand (0.25mm - 0.125mm)% Sand (0.125mm - 0.063mm)% Silt (0.063mm - 0.0312mm)% Silt (0.0312mm - 0.004mm)% Clay (<4um)

% Gravel (>2mm)% Sand (2.00mm - 1.00mm)% Sand (1.00mm - 0.50mm)

%

%

%

%

%

%

%%%%%%%%%

%%%

20-SEP-10

20-SEP-10

20-SEP-10

20-SEP-10

20-SEP-10

20-SEP-10

21-SEP-1021-SEP-1021-SEP-1021-SEP-1021-SEP-1021-SEP-1021-SEP-1021-SEP-1021-SEP-10

21-SEP-1021-SEP-1021-SEP-10

20-SEP-10

20-SEP-10

20-SEP-10

20-SEP-10

20-SEP-10

20-SEP-10


23-SEP-1023-SEP-1023-SEP-10

23.0

23.1

23.9

1.15

0.54

0.58

6.8310.013.216.112.45.496.3916.812.8

0.211.052.86

Particle size - Sieve and Pipette


0.10

0.10

0.10

0.10

0.10

0.10

0.100.100.100.100.100.100.100.100.10

0.100.100.10

Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

R1472236

R1472236

R1472236

R1472236

R1472236

R1472236

R1476166R1476166R1476166R1476166R1476166R1476166R1476166R1476166R1476166

R1476166R1476166R1476166

DRAFT


L931614 CONTD....

3PAGE


of

EC-59337

Qualifier* Batch


4

L931614-11 COMPOSITE LLC SITE~10-11840CLIENT on 01-SEP-10Sampled By:

SOIL

% Sand (0.50mm - 0.25mm)% Sand (0.25mm - 0.125mm)% Sand (0.125mm - 0.063mm)% Silt (0.063mm - 0.0312mm)% Silt (0.0312mm - 0.004mm)% Clay (<4um)

%%%%%%

21-SEP-1021-SEP-1021-SEP-1021-SEP-1021-SEP-1021-SEP-10

23-SEP-1023-SEP-1023-SEP-1023-SEP-1023-SEP-1023-SEP-10

16.032.717.813.313.22.78

Particle size - Sieve and Pipette0.100.100.100.100.100.10

Matrix:

R1476166R1476166R1476166R1476166R1476166R1476166

DRAFT

C-TOT-ORG-LECO-SK

PSA-PIPET-DETAIL-SK

Reference Information

Organic Carbon by combustion method


L931614 CONTD....

4PAGE of

EC-59337

Total Organic Carbon (C-TOT-ORG-LECO-SK, C-TOT-ORG-SK)

Total C and inorganic C are determined on separate samples. The total C is determined by combustion and thermal conductivity detection, while inorganic C is determined by weight lass after addition of hydrochloric acid. Organic C is calculated by the difference between these two determinations.

Reference for Total C:Nelson, D.W. and Sommers, L.E. 1996. Total Carbon, organic carbon and organic matter. P. 961-1010 In: J.M. Bartels et al. (ed.) Methods of soil analysis: Part 3 Chemical methods. (3rd ed.) ASA and SSSA, Madison, WI. Book series no. 5

Reference for Inorganic C:Loeppert, R.H. and Suarez, D.L. 1996. Gravimetric Method for Loss of Carbon Dioxide. P. 455-456 In: J.M. Bartels et al. (ed.) Methods of soil analysis: Part 3 Chemical methods. (3rd ed.) ASA and SSSA, Madison, WI. Book series no. 5

Particle size analysis involves the measurement of the proportions of the various primary soil particle sizes (ie. clay < 0.004 mm, silt 0.004-0.063 mm, sand 0.063-2.0 mm and gravel > 2.0 mm). In this method, the gravel and sand portions are determined by sieving, while the silt and clay portion is determined by sedimentation using Stokes Law, which relates the radius of the particles to the velocity of the sedimentation in water. Pretreatment of the soil with Calgon (sodium hexametaphosphate) is used to ensure the complete dispersion of the primary soil particles. Additional pretreatments may be necessary to remove cementing materials such as CaCO3 and organic matter.

ReferenceY.P. Kalra, and D.G. Maynard, 1991. Methods Manual For Forest Soil and Plant Analysis,Northwest Region. Forestry Canada (modified sand, silt and clay size ranges)

ALS Test Code Test Description

Soil

Soil

SSSA (1996) p. 973

FORESTRY CANADA (1991) P. 46-48 MOD

Method Reference**

** ALS test methods may incorporate modifications from specified reference methods to improve performance.

Matrix

The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:

Laboratory Definition Code Laboratory Location

SK ALS LABORATORY GROUP - SASKATOON, SASKATCHEWAN, CANADA

Test Method References:

Chain of Custody Numbers:

GLOSSARY OF REPORT TERMSSurrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there.mg/kg - milligrams per kilogram based on dry weight of samplemg/kg wwt - milligrams per kilogram based on wet weight of samplemg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million.< - Less than.D.L. - The reporting limit.N/A - Result not available. Refer to qualifier code and definition for explanation.

Test results reported relate only to the samples as received by the laboratory.UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION.Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

4

DRAFT

Quality Control ReportPage 1 of

Client:

Contact:

AMEC EARTH & ENVIRONMENTAL5667 - 70 STREET EDMONTON AB T6B 3P6JESSE DANG ~ CHEMISTRY

Report Date: 29-SEP-10Workorder: L931614

Test Matrix Reference Result Qualifier Units RPD Limit Analyzed

C-TOT-ORG-LECO-SK

PSA-PIPET-DETAIL-SK

Soil

Soil

R1472236

R1476166

Batch

Batch

DUP

IRM

MB

IRM

WG1168422-1

WG1168422-2

WG1168422-3

WG1169160-2

L930732-7

2004_SOIL

FARM98




% Gravel (>2mm)

% Sand (2.00mm - 1.00mm)

% Sand (1.00mm - 0.50mm)

% Sand (0.50mm - 0.25mm)

% Sand (0.25mm - 0.125mm)

% Sand (0.125mm - 0.063mm)

% Silt (0.063mm - 0.0312mm)

% Silt (0.0312mm - 0.004mm)

% Clay (<4um)

0.70

1.43

<0.10

0.00

2.01

7.57

8.87

13.7

10.4

12.4

19.5

25.6

20-SEP-10

20-SEP-10

20-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

0.17 30

1.1-1.5

1-1.02

1-5

5-9

5.5-11.5

11-15

7.97-14.03

9.1-16.9

13-23

22.9-30.1

%

%

%

%

%

%

%

%

%

%

%

%

0.70

0.1

2

DRAFT

Quality Control ReportPage 2 ofReport Date: 29-SEP-10Workorder: L931614

Limit 99% Confidence Interval (Laboratory Control Limits)DUP DuplicateRPD Relative Percent DifferenceN/A Not AvailableLCS Laboratory Control SampleSRM Standard Reference MaterialMS Matrix SpikeMSD Matrix Spike DuplicateADE Average Desorption EfficiencyMB Method BlankIRM Internal Reference MaterialCRM Certified Reference MaterialCCV Continuing Calibration VerificationCVS Calibration Verification StandardLCSD Laboratory Control Sample Duplicate

Legend:

The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre-determined data quality objectives to provide confidence in the accuracy of associated test results.

Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

Hold Time Exceedances:

All test results reported with this submission were conducted within ALS recommended hold times.

ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.

2


EC-59369282656



15-SEP-10




ATTN: JESSE DANG ~ CHEMISTRYFINAL 23-SEP-10 16:16 (MT)Report Date:

Version:



____________________________________________



Phone: 780-436-2152


L931616 CONTD....

2PAGE


of

EC-59369

Qualifier* Batch


3

L931616-1 COMPOSITE ULC ~10-12048CLIENTSampled By:

SOIL


%%%%%%%%%



8.236.458.5920.226.011.29.369.060.99

Particle size - Sieve and Pipette0.100.100.100.100.100.100.100.100.10

Matrix:

R1476166R1476166R1476166R1476166R1476166R1476166R1476166R1476166R1476166

PSA-PIPET-DETAIL-SK



L931616 CONTD....

3PAGE of

EC-59369




Soil FORESTRY CANADA (1991) P. 46-48 MOD

Method Reference**


Matrix








3


Client:

Contact:




PSA-PIPET-DETAIL-SK Soil

R1476166BatchIRMWG1169160-2 FARM98

% Gravel (>2mm)

% Sand (2.00mm - 1.00mm)

% Sand (1.00mm - 0.50mm)

% Sand (0.50mm - 0.25mm)

% Sand (0.25mm - 0.125mm)

% Sand (0.125mm - 0.063mm)

% Silt (0.063mm - 0.0312mm)

% Silt (0.0312mm - 0.004mm)

% Clay (<4um)

0.00

2.01

7.57

8.87

13.7

10.4

12.4

19.5

25.6

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

1-1.02

1-5

5-9

5.5-11.5

11-15

7.97-14.03

9.1-16.9

13-23

22.9-30.1

%

%

%

%

%

%

%

%

%

2



Legend:






2


EC-59383282655



15-SEP-10




ATTN: JESSE DANG ~ CHEMISTRYFINAL 23-SEP-10 16:16 (MT)Report Date:

Version:



____________________________________________



Phone: 780-436-2152


L931617 CONTD....

2PAGE


of

EC-59383

Qualifier* Batch


3

L931617-1 COMPOSITE SLI ~10-12113CLIENTSampled By:

SOIL


%%%%%%%%%



15.112.613.612.311.25.7510.914.44.26

Particle size - Sieve and Pipette0.100.100.100.100.100.100.100.100.10

Matrix:

R1476166R1476166R1476166R1476166R1476166R1476166R1476166R1476166R1476166

PSA-PIPET-DETAIL-SK



L931617 CONTD....

3PAGE of

EC-59383




Soil FORESTRY CANADA (1991) P. 46-48 MOD

Method Reference**


Matrix








3


Client:

Contact:




PSA-PIPET-DETAIL-SK Soil

R1476166BatchIRMWG1169160-2 FARM98

% Gravel (>2mm)

% Sand (2.00mm - 1.00mm)

% Sand (1.00mm - 0.50mm)

% Sand (0.50mm - 0.25mm)

% Sand (0.25mm - 0.125mm)

% Sand (0.125mm - 0.063mm)

% Silt (0.063mm - 0.0312mm)

% Silt (0.0312mm - 0.004mm)

% Clay (<4um)

0.00

2.01

7.57

8.87

13.7

10.4

12.4

19.5

25.6

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

23-SEP-10

1-1.02

1-5

5-9

5.5-11.5

11-15

7.97-14.03

9.1-16.9

13-23

22.9-30.1

%

%

%

%

%

%

%

%

%

2



Legend:






2

kitsault mine project environmental assessment · * mdl adjusted due to sample matrix. all...

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