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Page 1: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Lab reports

Page 2: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 537290

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 06/02/2019 12:00:00

Sampled by Customer

D100219-0010-1Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 760897Sample No:Tamar Produced water- Skimmer 2.2.19

RefrigeratedStorage conditions: Sampling time: 02/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

EPA 8270Cresol

Cresol 10.22 mg/L

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm11.5 <4

SM 4500 H+BpH pH units8.71

EPA 8270Phenols

Dimethylphenol-2-4 4.88 mg/L <0.02

Phenol 7.28 mg/L <0.02

Total results 12.16 mg/L <0.02

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.040 mg/L <0.025

Benzene 0.050 mg/L <0.025

Ethylbenzene 0.030 mg/L <0.025

MEK 0.150 mg/L <0.025

tert-Butyl alcohol 0.320 mg/L <0.025

Toluene 0.090 mg/L <0.025

Total VOCs 0.790 mg/L

VOC's-target list ראה תוצאות -

Xylene total 0.110 mg/L <0.025

SM 5310BTotal Organic carbon mg/L1137.70 <0.5

Page 1 of 2 Created on: 18/02/2019Certificate Of Analysis: 537290

Page 3: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm<4.0 <4

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Boris Gil Contaminants department lab analyst

Nazi Botershvili Environment department team leader

- End Of Certificate -

Page 2 of 2 Created on: 18/02/2019Certificate Of Analysis: 537290

Page 4: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

נובל אנרג'י שם הלקוח:

D100219-0010-1 קט )במעבדה(:מספר זיהוי הפרוי

2.2.19תאריך הדיגום:

11.2.19תאריך הדיווח:

Page 5: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 760897

Tamar Produced water-skimmer 2.2.19 הדוגמא:זיהוי

תאריך הבדיקה: 11.2.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Butanoic acid, 2-methyl- 000116-53-0 0.06

Pyridine, 3-methyl- 000108-99-6 0.13

1,3-Cyclopentadiene, 5-(1-methylethylidene)- 002175-91-9 0.07

Pentanoic acid 000109-52-4 0.08

Benzene, 1,3-dimethyl- 000108-38-3 0.04

Hexanoic acid, 2-methyl- 004536-23-6 0.02

Cyclohexanol, 2-methyl-, cis- 007443-70-1 0.16

cis-3-Methylcyclohexanol 005454-79-5 0.19

Cyclohexanone, 3-methyl- 000591-24-2 0.02

Pyridine, 3,5-dimethyl- 000591-22-0 0.44

Ethanol, 2-(2-ethoxyethoxy)- 000111-90-0 2.63

Indane 000496-11-7 0.37

Pyridine, 5-ethyl-2-methyl- 000104-90-5 0.24

Phenol, 2,6-dimethyl- 000576-26-1 0.55

Phenol, 2-ethyl- 000090-00-6 0.72

Phenol, 3,5-dimethyl-, methylcarbamate 002655-14-3 4.28

Phenol, 4-ethyl- 000123-07-9 2.55

Phenol, 3,5-dimethyl- 000108-68-9 3.69

Phenol, 2,3-dimethyl- 000526-75-0 4.92

Phenol, 3,4-dimethyl- 000095-65-8 3.20

Naphthalene 000091-20-3 1.41

Phenol, 2-propyl- 000644-35-9 0.29

Phenol, 3-(1-methylethyl)- 000618-45-1 4.85

Phenol, 2-ethyl-5-methyl- 001687-61-2 2.84

Phenol, 3,4,5-trimethyl- 000527-54-8 4.32

Phenol, 3-ethyl-5-methyl- 000698-71-5 1.94

Page 6: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Phenol, 2-ethyl-4-methyl- 003855-26-3 2.11

2-Methyl-2-octene 016993-86-5 0.25

Phenol, 2,3,5-trimethyl- 000697-82-5 1.05

Phenol, 2-methyl-5-(1-methylethyl)- 000499-75-2 2.96

Phenol, 2,4,6-trimethyl- 000527-60-6 0.87

Phenol, 3-methyl-5-(1-methylethyl)-, methylcarbamate 002631-37-0 5.05

Naphthalene, 2-methyl- 000091-57-6 2.28

1H-Inden-5-ol, 2,3-dihydro- 001470-94-6 2.95

Benzene, pentamethyl- 000700-12-9 1.52

Benzene, 1-ethyl-4-(1-methylethyl)- 004218-48-8 1.02

Benzene, 1-(1,1-dimethylethyl)-4-methoxy- 005396-38-3 0.82

Thymol 000089-83-8 0.64

Phenol, 2,3,5,6-tetramethyl- 000527-35-5 1.34

Dewar benzene, hexamethyl- 007641-77-2 3.25

Ethanol, 2,2'-dithiobis- 001892-29-1 2.66

6-Methyl-4-indanol 020294-32-0 3.33

Benzene, 1-methoxy-4-(1-methyl-2-propenyl)- 018272-83-8 3.72

Benzofuran, 2,3-dihydro-2,2,4,6-tetramethyl- 003698-49-5 0.43

Fluorene 000086-73-7 2.17

1-Isopropenylnaphthalene 001855-47-6 1.00

Pentamethylphenylacetonitrile 034688-70-5 0.43

1-Naphthalenol, decahydro-1,4a-dimethyl-7-(1-

methylethylidene)-, [1R-(1.alpha.,4a.beta.,8a.alpha.)]- 000473-04-1 0.37

Tricyclo[4.4.1.0(2,5)]undeca-1(10),3,6,8-tetraene, 11-(1-

methylethylidene)- 055836-29-8 0.44

Indeno[2,1-a]indene, 4b,5,9b,10-tetrahydro-, cis- 016293-79-1 0.37

10,11-Dihydro-5H-dibenzo(a,d)cycloheptene 000833-48-7 0.43

Anthracene 000120-12-7 0.56

[14]Annulene, 1,6:8,13-bis(methano)-, syn 085385-68-8 0.57

9H-Carbazole, 2-methyl- 003652-91-3 0.24

4-Methylcarbazole 003770-48-7 0.43

Carbazole, 2,6-dimethyl- 078787-80-1 0.18

N-(2-hydroxyethyl)dodecanamide 068140-00-1 0.10

83.53 סכ"ה

*הריכוז חושב לפי שטח בתגובה של נפטלן.

Page 7: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

End of Certificate

Page 8: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 537284

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 06/02/2019 12:00:00

Sampled by Customer

D100219-0010Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 760898Sample No:Tamar Produced water- Skimmer 5.2.19

RefrigeratedStorage conditions: Sampling time: 05/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

EPA 8270Cresol

Cresol 10.84 mg/L

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm10.9 <4

SM 4500 H+BpH pH units8.58

EPA 8270Phenols

Dimethylphenol-2-4 5.04 mg/L <0.02

Phenol 7.02 mg/L <0.02

Total results 12.06 mg/L <0.02

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.080 mg/L <0.025

Benzene 0.110 mg/L <0.025

Ethylbenzene 0.050 mg/L <0.025

MEK 0.220 mg/L <0.025

tert-Butyl alcohol 0.370 mg/L <0.025

Toluene 0.220 mg/L <0.025

Total VOCs 1.260 mg/L

VOC's-target list ראה תוצאות -

Xylene total 0.210 mg/L <0.025

SM 5310BTotal Organic carbon mg/L192.05 <0.5

Page 1 of 2 Created on: 18/02/2019Certificate Of Analysis: 537284

Page 9: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm4.0 <4

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Boris Gil Contaminants department lab analyst

Nazi Botershvili Environment department team leader

- End Of Certificate -

Page 2 of 2 Created on: 18/02/2019Certificate Of Analysis: 537284

Page 10: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

נובל אנרג'י שם הלקוח:

D100219-0010 קט )במעבדה(:מספר זיהוי הפרוי

5.2.19תאריך הדיגום:

12.2.19תאריך הדיווח:

Page 11: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 760898

Tamar Produced water-Skimmer 5.2.19 הדוגמא:זיהוי

תאריך הבדיקה: 11.2.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

2-Furanmethanol 000098-00-0 0.02

Pyridine, 3-methyl- 000108-99-6 0.07

Pentanoic acid 000109-52-4 0.03

Pentanoic acid, 2-methyl-, butyl ester 006297-41-2 0.06

Cyclohexanol, 3-methyl- 000591-23-1 0.07

Pyridine, 3,5-dimethyl- 000591-22-0 0.12

Ethanol, 2-(2-ethoxyethoxy)- 000111-90-0 1.75

Pyridine, 2,5-dimethyl- 000589-93-5 0.22

Indane 000496-11-7 0.05

2(3H)-Furanone, 5-ethyldihydro-5-methyl- 002865-82-9 0.21

Pyridine, 3-ethyl-4-methyl- 000529-21-5 0.15

Phenol, 2,6-dimethyl- 000576-26-1 0.52

Phenol, 2-ethyl- 000090-00-6 0.47

Phenol, 4-ethyl- 000123-07-9 2.27

Phenol, 3,5-dimethyl- 000108-68-9 3.29

Phenol, 2,3-dimethyl- 000526-75-0 4.01

Phenol, 3,4-dimethyl- 000095-65-8 2.98

Naphthalene 000091-20-3 0.86

Phenol, 3-(1-methylethyl)- 000618-45-1 4.35

Phenol, 2-ethyl-5-methyl- 001687-61-2 0.69

Phenol, 3-ethyl-5-methyl- 000698-71-5 2.24

Phenol, 2-ethyl-4-methyl- 003855-26-3 1.88

N-Trifluoroacetyl glycine 000383-70-0 0.20

Phenol, 2,4,6-trimethyl- 000527-60-6 0.97

Phenol, 2-methyl-5-(1-methylethyl)- 000499-75-2 1.59

Phenol, 2,3,5-trimethyl- 000697-82-5 1.13

Page 12: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Phenol, 3-methyl-5-(1-methylethyl)-, methylcarbamate 002631-37-0 3.66

Phenol, 3,4,5-trimethyl- 000527-54-8 2.86

Naphthalene, 1-methyl- 000090-12-0 1.57

1H-Inden-5-ol, 2,3-dihydro- 001470-94-6 2.55

Benzene, pentamethyl- 000700-12-9 0.74

Phenol, 3,5-diethyl- 001197-34-8 1.46

Benzene, hexamethyl- 000087-85-4 1.64

6-Methyl-4-indanol 020294-32-0 4.25

Dewar benzene, hexamethyl- 007641-77-2 1.38

Benzene, 1,2-diethyl-3,4-dimethyl- 054410-75-2 0.58

Benzene, 1-methoxy-4-(1-methyl-2-propenyl)- 018272-83-8 1.84

Silane, trichloroethenyl- 000075-94-5 2.19

Benzofuran, 2,3-dihydro-2,2,4,6-tetramethyl- 003698-49-5 1.36

Fluorene 000086-73-7 1.66

Benzene, 1-methyl-2-(2-phenylethenyl)- 074685-42-0 0.47

4,4'-Dimethylbiphenyl 000613-33-2 0.35

10,11-Dihydro-5H-dibenzo(a,d)cycloheptene 000833-48-7 0.26

Anthracene 000120-12-7 0.34

Indeno[2,1-a]indene, 4b,5,9b,10-tetrahydro-, cis- 016293-79-1 0.36

9H-Carbazole, 2-methyl- 003652-91-3 0.10

3-Methylcarbazole 004630-20-0 0.18

Ethane, 1-phenoxy-2-(8-quinolylsulfonyl)- 1000294-06-4 0.12

Benzenamine, 3-(2-phenylethenyl)-, (E)- 014064-82-5 0.09

N-(4-Methoxyphenyl)-2-hydroxyimino-acetamide 1000143-61-3 0.11

Carbazole, 2,4,6-trimethyl- 078787-88-9 0.06

60.39 סכ"ה

*הריכוז חושב לפי שטח בתגובה של נפטלן.

Page 13: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

End of Certificate

Page 14: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 539804

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-1Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763267Sample No:Tamar Produced water 10.2.19

RefrigeratedStorage conditions: Sampling time: 10/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

EPA 8270Cresol

Cresol 3.33 mg/L

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm12.2 <4

SM 4500 H+BpH pH units8.43

EPA 8270Phenols

Dimethylphenol-2-4 1.20 mg/L <0.02

Phenol 3.10 mg/L <0.02

Total results 4.3 mg/L <0.02

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.200 mg/L <0.025

1,3,5-Trimethylbenzene 0.040 mg/L <0.025

Benzene 0.210 mg/L <0.025

Ethylbenzene 0.110 mg/L <0.025

MEK 0.400 mg/L <0.025

tert-Butyl alcohol 0.810 mg/L <0.025

Toluene 0.460 mg/L <0.025

Total VOCs 2.730 mg/L

VOC's-target list ראה תוצאות -

Page 1 of 2 Created on: 26/02/2019Certificate Of Analysis: 539804

Page 15: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Xylene total 0.500 mg/L <0.025

SM 5310BTotal Organic carbon mg/L225.70 <0.5

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm8.0 <4

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Natalia Arkhipova Contaminants department lab analyst

Nazi Botershvili Environment department team leader

- End Of Certificate -

Page 2 of 2 Created on: 26/02/2019Certificate Of Analysis: 539804

Page 16: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

NOBEL_ENERGY שם הלקוח:

D140219-0022-1 קט )במעבדה(:מספר זיהוי הפרוי

10.02.19תאריך הדיגום:

25.02.19תאריך הדיווח:

Page 17: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 763267

Tamar Produced Water 10.02.19 הדוגמא:זיהוי

תאריך הבדיקה: 19.02.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Fluorene 000086-73-7 1.98

Benzene, hexamethyl- 000087-85-4 0.78

Phenol, 2-ethyl- 000090-00-6 0.57

Naphthalene 000091-20-3 1.65

Naphthalene, 2-methyl- 000091-57-6 2.24

Phenol, 3,4-dimethyl- 000095-65-8 3.44

Phenol, 2,5-dimethyl- 000095-87-4 4.82

Pyridine, 5-ethyl-2-methyl- 000104-90-5 0.14

Benzene, 1,3-dimethyl- 000108-38-3 0.16

Phenol, 3,5-dimethyl- 000108-68-9 4.01

Pyridine, 3-methyl- 000108-99-6 0.10

Ethanol, 2-(2-ethoxyethoxy)- 000111-90-0 1.77

Anthracene 000120-12-7 0.86

Cyclotetracosane 000297-03-0 0.59

Indane 000496-11-7 0.79

Phenol, 2-methyl-5-(1-methylethyl)- 000499-75-2 2.12

Phenol, 2,3,5,6-tetramethyl- 000527-35-5 2.16

Phenol, 3,4,5-trimethyl- 000527-54-8 3.02

Phenol, 2,4,6-trimethyl- 000527-60-6 3.02

Phenol, 2,6-dimethyl- 000576-26-1 0.45

Naphthalene, 2,6-dimethyl- 000581-42-0 1.64

Pyridine, 3,5-dimethyl- 000591-22-0 0.27

3,3'-Dimethylbiphenyl 000612-75-9 1.28

Phenol, 3-(1-methylethyl)- 000618-45-1 5.24

Benzene, 1-ethyl-3-methyl- 000620-14-4 0.07

Phenol, 3-ethyl- 000620-17-7 2.59

Page 18: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Tricosane 000638-67-5 0.20

Phenol, 3-ethyl-5-methyl- 000698-71-5 2.12

Benzene, pentamethyl- 000700-12-9 0.92

1-Phenyl-1-butene 000824-90-8 0.15

10,11-Dihydro-5H-dibenzo(a,d)cycloheptene 000833-48-7 0.49

Benzenemethanol, 4-(1,1-dimethylethyl)- 000877-65-6 0.73

Cyclopentanone, 2-methyl- 001120-72-5 0.09

9H-Fluorene, 2-methyl- 001430-97-3 0.50

1H-Inden-5-ol, 2,3-dihydro- 001470-94-6 2.74

Phenol, 2-ethyl-5-methyl- 001687-61-2 2.00

1-Isopropenylnaphthalene 001855-47-6 1.70

Ethanol, 2,2'-dithiobis- 001892-29-1 1.57

Phenol, 3-methyl-5-(1-methylethyl)-, methylcarbamate 002631-37-0 4.22

Benzene, 1-ethenyl-4-ethyl- 003454-07-7 1.01

Benzofuran, 2,3-dihydro-2,2,4,6-tetramethyl- 003698-49-5 1.62

Hexanoic acid, 6-bromo- 004224-70-8 0.04

Indeno[2,1-a]indene, 4b,5,9b,10-tetrahydro- 005695-17-0 0.59

1,2,3,4-Tetrahydrobenzo[a]fluorene 006567-09-5 0.23

(R)-(+)-3-Methylcyclopentanone 006672-30-6 0.06

Dibenzofuran, 4-methyl- 007320-53-8 1.04

1,4-Methanonaphthalene,1,4-dihydro-9-((1-methylethylidene)- 007350-72-3 0.56

Benzene, 1-ethenyl-3-ethyl- 007525-62-4 0.36

Dewar benzene, hexamethyl- 007641-77-2 2.17

1,2,3,4-Tetrahydro-2,3-dimethylquinoxaline 013311-77-8 0.56

cis-1-Chloro-9-octadecene 016507-61-2 0.78

Benzene, 1-methoxy-4-(1-methyl-2-propenyl)- 018272-83-8 2.45

1-Nonadecene 018435-45-5 0.32

6-Methyl-4-indanol 020294-32-0 3.66

Naphthalene, decahydro-1,6-dimethyl-4-(1-methylethyl)- 034315-85-0 0.31

Cyclohexane, 1-(1,5-dimethylhexyl)-4-(4-methylpentyl)- 056009-20-2 0.15

Benzene, 1-methyl-2-(2-phenylethenyl)- 074685-42-0 0.71

23,28-Bisnor-17.beta.(H)-hopane 1000101-35-0 0.40

11,12-Dibromo-tetradecan-1-ol acetate 1000130-78-5 0.22

N-(4-Methoxyphenyl)-2-hydroxyimino-acetamide 1000143-61-3 0.69

6.beta.Bicyclo[4.3.0]nonane, 5.beta.-iodomethyl-1.beta.-isopropenyl-

4.alpha.,5.alpha.-dimethyl-, 1000195-85-9 0.31

Pyridine-3-carboxamide, oxime, N-(2-trifluoromethylphenyl)- 288246-53-7 1.48

סה"כ 82.91

ן.וז חושב לפי שטח בתגובה של נפטל*הריכ

Page 19: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

End of Certificate

Page 20: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

This certificate replaces previous COA no. 537584

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 539022

Replacement Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-2Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763268Sample No:Tamar Produced water 13.2.19

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

In house

procedure;Based on:

EPA 8260

BTEX

Benzene 0.150 mg/L <0.025

Ethyl Benzene 0.120 mg/L <0.025

Toluene 0.380 mg/L <0.025

Total BTEX 1.200 mg/L

Xylene 0.550 mg/L <0.025

EPA 8270Cresol

Cresol 4.20 mg/L

In house procedure

GC/FID

Ethylene Glycol by GC/

FID

Ethylene Glycol 48 mg/L

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm9.7 <4

SM 3120BMetal by ICP

Phosphorus (P) <0.500 mg/L

In house procedure

GC/FID

Methanol mg/LNOT

DETECTED

Total nitrogen calculated

as N

-12.23

SM 4500 NO2-BNitrogen (Nitrite) as N mg/L<0.001

Home method for

Nitrate in high

organic environment

Nitrogen (Nitrate) as N mg/L<0.20

SM 4500 H+BpH pH units8.64

EPA 8270Phenols

Dimethylphenol-2-4 1.84 mg/L <0.02

Page 1 of 2 Created on: 24/02/2019Certificate Of Analysis: 539022

Page 21: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Phenol 2.90 mg/L <0.02

Total results 4.74 mg/L <0.02

SM 4500 NorgBNitrogen (organic) as N

by kj

mg/L12.23 <0.1

SM 5310BTotal Organic carbon mg/L157.10 <0.5

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm5.0 <4

SM 2540DTotal suspended solids

dried a

mg/L<1 <1

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Dmitry Pergament ICP department lab analyst

Natalia Arkhipova Contaminants department lab analyst

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 24/02/2019Certificate Of Analysis: 539022

Page 22: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 541423

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-3Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763269Sample No:Tamar Produced water 13.2.19

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

DIN 38 406Nitrogen (Ammonium) as

N

mg/L11.07 <0.05

SM5210B ; The

oxygen

measurement is

based on: SM 4500

O C & SM 4500 O G

BOD mg/L120.00 <0.5

SM 4500Cl- EChlorides mg/L<2.00 <2

OSPAR by -GC/FIDDispersed Mineral oil

content by GC-FID

Dispersed Mineral oil 3.6 mg/L

EPA 8270PAH

2 methyl naphthalene 0.31 mg/L

Acenaphtene 0.17 mg/L

Fluorene 0.24 mg/L

Naphtalene 0.64 mg/L

Phenanthrene 0.12 mg/L

Report results 1.48 -

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

EPA 8270SVOC

2,4-Dimethylphenol 1.84 mg/L <0.01

2-Methylnaphthalene 0.31 mg/L <0.01

2-Methylphenol 0.64 mg/L <0.01

3+4-Methylphenol 3.56 mg/L <0.01

Page 1 of 2 Created on: 03/03/2019Certificate Of Analysis: 541423

Page 23: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Acenaphtene 0.17 mg/L <0.01

Fluorene 0.24 mg/L <0.01

Naphtalene 0.64 mg/L <0.01

Phenanthrene 0.12 mg/L <0.01

Phenol 2.90 mg/L <0.01

Total SVOC

semiquantitative

10.42 mg/L

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.290 mg/L <0.025

1,3,5-Trimethylbenzene 0.060 mg/L <0.025

Benzene 0.150 mg/L <0.025

Ethylbenzene 0.120 mg/L <0.025

MEK 0.320 mg/L <0.025

n-Propylbenzene 0.030 mg/L <0.025

p-Isopropyltoluene 0.030 mg/L <0.025

tert-Butyl alcohol 0.780 mg/L <0.025

Toluene 0.380 mg/L <0.025

Total VOCs 2.710 mg/L

VOC's-target list ראה תוצאות -

Xylene total 0.550 mg/L <0.025

SM 4500 S2-FSulfides mg/L0.60 <0.2

In house

procedure;Based on:

SM 2540C

Dissolved solids dried at

103°

mg/L<50.00 <50

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Lush Cernes Food Chemistry and Pesticide Departments Manager

Natalia Arkhipova Contaminants department lab analyst

Nazi Botershvili Environment department team leader

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 03/03/2019Certificate Of Analysis: 541423

Page 24: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

NOBEL_ENERGY שם הלקוח:

D140219-0022-3 קט )במעבדה(:מספר זיהוי הפרוי

13.02.19תאריך הדיגום:

19.02.19תאריך הדיווח:

Page 25: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 763269

Tamar Produced Water 13.02.19 הדוגמא:זיהוי

תאריך הבדיקה: 14.02.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

(R)-(+)-3-Methylcyclopentanone 006672-30-6 0.05

1,2-Benzisothiazole, 3-(hexahydro-1H-azepin-1-yl)-, 1,1-

dioxide 309735-29-3 0.40

1,4-Methanonaphthalene,1,4-dihydro-9-((1-

methylethylidene)- 007350-72-3 0.29

10,11-Dihydro-5H-dibenzo(a,d)cycloheptene 000833-48-7 0.26

1H-Inden-5-ol, 2,3-dihydro- 001470-94-6 1.63

1H-Indene, 2,3-dihydro-1,6-dimethyl- 017059-48-2 0.26

1H-Indene, 2,3-dihydro-2-methyl- 000824-63-5 0.70

1-Isopropenylnaphthalene 001855-47-6 0.96

2,2'-Dimethylbiphenyl 000605-39-0 0.56

3-Methyl-4-isopropylphenol 003228-02-2 0.31

6-Methyl-4-indanol 020294-32-0 1.80

7-Methoxy-1-methyl-8(1H)-cycloheptapyrazolone 005952-95-4 0.27

Benzene, 1,3-dimethyl- 000108-38-3 0.09

Benzene, 1-ethenyl-3-ethyl- 007525-62-4 0.35

Benzene, 1-ethyl-3-methyl- 000620-14-4 0.04

Benzene, 1-ethyl-4-methoxy- 001515-95-3 0.44

Benzene, 1-methoxy-4-(1-methyl-2-propenyl)- 018272-83-8 1.21

Benzene, 1-methyl-2-(2-phenylethenyl)- 074685-42-0 0.36

Benzene, 1-methyl-4-(2-propenyl)- 003333-13-9 0.13

Benzene, 3-ethyl-1,2,4,5-tetramethyl- 031365-98-7 1.31

Benzene, pentamethyl- 000700-12-9 0.48

Benzofuran, 2,3-dihydro-2,2,4,6-tetramethyl- 003698-49-5 0.77

Cyclopentanone, 2-methyl- 001120-72-5 0.05

Dewar benzene, hexamethyl- 007641-77-2 0.91

Page 26: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Ethanol, 2-(2-ethoxyethoxy)- 000111-90-0 0.96

Ethanol, 2,2'-dithiobis- 001892-29-1 1.12

Ethanol, 2-butoxy- 000111-76-2 4.69

Ethanone, 1-(3,4-dimethylphenyl)- 003637-01-2 0.59

Indane 000496-11-7 0.64

Indeno[2,1-a]indene, 4b,5,9b,10-tetrahydro- 005695-17-0 0.40

Naphthalene, 1-methyl- 000090-12-0 1.37

Naphthalene, 2,6-dimethyl- 000581-42-0 0.95

Naphthalene, 2-ethenyl- 000827-54-3 0.70

p-(1-Butenyl)anisole, trans 061866-52-2 0.29

Phenol, 2,3,6-trimethyl- 002416-94-6 0.80

Phenol, 2,3-dimethyl- 000526-75-0 2.52

Phenol, 2,6-dimethyl- 000576-26-1 0.33

Phenol, 2-ethyl- 000090-00-6 0.29

Phenol, 2-ethyl-5-methyl- 001687-61-2 0.47

Phenol, 2-methyl-5-(1-methylethyl)- 000499-75-2 1.08

Phenol, 2-propyl- 000644-35-9 0.12

Phenol, 3,4,5-trimethyl- 000527-54-8 2.38

Phenol, 3,4-dimethyl- 000095-65-8 2.05

Phenol, 3,5-dimethyl- 000108-68-9 2.08

Phenol, 3-ethyl-5-methyl- 000698-71-5 1.16

Phenol, 3-methyl-5-(1-methylethyl)-, methylcarbamate 002631-37-0 2.55

Phenol, 4-(1-methylethyl)- 000099-89-8 2.52

Phenol, 4-ethyl- 000123-07-9 1.31

Pyridine, 3-methyl- 000108-99-6 0.06

trans-3-Methylcyclohexanol 007443-55-2 0.11

Tricyclo[4.4.1.0(2,5)]undeca-1(10),3,6,8-tetraene, 11-(1-

methylethylidene)- 055836-29-8 0.75

45.88סה"כ

*הריכוז חושב לפי שטח בתגובה של נפטלן.

End of Certificate

Page 27: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 540679

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 24/02/2019 12:00:00

Sampled by Customer

D240219-0054-1Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 767191Sample No:Tamar Produced water 16.2.19

RefrigeratedStorage conditions: Sampling time: 16/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

EPA 8270Cresol

Cresol 3.00 mg/L

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm9 <4

SM 4500 H+BpH pH units8.04

EPA 8270Phenols

Dimethylphenol-2-4 1.36 mg/L <0.02

Phenol 2.32 mg/L <0.02

Total results 3.68 mg/L <0.02

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.650 mg/L <0.025

1,3,5-Trimethylbenzene 0.100 mg/L <0.025

Benzene 0.380 mg/L <0.025

Ethylbenzene 0.220 mg/L <0.025

Isopropylbenzene 0.030 mg/L <0.025

MEK 0.800 mg/L <0.025

n-Propylbenzene 0.030 mg/L <0.025

p-Isopropyltoluene 0.030 mg/L <0.025

tert-Butyl alcohol 1.500 mg/L <0.025

Page 1 of 2 Created on: 27/02/2019Certificate Of Analysis: 540679

Page 28: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Toluene 0.940 mg/L <0.025

Total VOCs 5.580 mg/L

VOC's-target list ראה תוצאות -

Xylene total 0.900 mg/L <0.025

SM 5310BTotal Organic carbon mg/L129.20 <0.5

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm<4.0 <4

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Lush Cernes Food Chemistry and Pesticide Departments Manager

Natalia Arkhipova Contaminants department lab analyst

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 27/02/2019Certificate Of Analysis: 540679

Page 29: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

נובל אנרג'י שם הלקוח:

D240219-0054-1 קט )במעבדה(:מספר זיהוי הפרוי

16.2.19תאריך הדיגום:

25.2.19תאריך הדיווח:

Page 30: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 767191

Tamar Produced water 16.2.19 הדוגמא:זיהוי

תאריך הבדיקה: 24.2.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Cyclopentanone, 2-methyl- 001120-72-5 0.03

(R)-(+)-3-Methylcyclopentanone 006672-30-6 0.06

Pyridine, 3-methyl- 000108-99-6 0.07

Ethanol, 2-butoxy- 000111-76-2 5.03

Benzene, 1-ethyl-2-methyl- 000611-14-3 0.04

Ethanol, 2-(2-ethoxyethoxy)- 000111-90-0 1.31

Pyridine, 3,4-dimethyl- 000583-58-4 0.18

Indane 000496-11-7 0.83

Benzene, 1-ethenyl-3-ethyl- 007525-62-4 0.57

Pyridine, 3-ethyl-4-methyl- 000529-21-5 0.12

Phenol, 2,6-dimethyl- 000576-26-1 0.41

Phenol, 2-ethyl- 000090-00-6 0.36

Indan, 1-methyl- 000767-58-8 0.85

Phenol, 4-ethyl- 000123-07-9 1.80

Phenol, 3,5-dimethyl- 000108-68-9 2.96

Phenol, 2,3-dimethyl- 000526-75-0 3.50

Phenol, 3,4-dimethyl- 000095-65-8 2.72

Naphthalene 000091-20-3 1.27

Phenol, 3-(1-methylethyl)- 000618-45-1 3.30

Phenol, 2-ethyl-5-methyl- 001687-61-2 1.17

Phenol, 2-ethyl-4-methyl- 003855-26-3 2.24

Phenol, 2,4,6-trimethyl- 000527-60-6 1.89

Phenol, 2,3,5-trimethyl- 000697-82-5 0.94

Thymol 000089-83-8 1.35

4-Hydroxy-3-methylacetophenone 000876-02-8 3.38

Phenol, 3,4,5-trimethyl- 000527-54-8 2.69

Page 31: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Naphthalene, 2-methyl- 000091-57-6 1.72

1H-Inden-5-ol, 2,3-dihydro- 001470-94-6 2.47

Ethanone, 1-(3,4-dimethylphenyl)- 003637-01-2 0.93

Benzene, 1-ethyl-4-(1-methylethyl)- 004218-48-8 0.70

Phenol, 2,3,5,6-tetramethyl- 000527-35-5 1.36

Ethanol, 2,2'-dithiobis- 001892-29-1 1.92

Dewar benzene, hexamethyl- 007641-77-2 0.54

6-Methyl-4-indanol 020294-32-0 2.63

Benzene, hexamethyl- 000087-85-4 0.74

Benzene, 1-methoxy-4-(1-methyl-2-propenyl)- 018272-83-8 2.42

Quinoxalin-2(1H)-one, 3,4-dihydro-3,3-dimethyl- 080636-30-2 1.72

1,3,5-Cycloheptatriene, 3,4-diethyl-7,7-dimethyl- 1000156-99-7 0.43

2,2'-Dimethylbiphenyl 000605-39-0 0.67

Fluorene 000086-73-7 1.51

1-Isopropenylnaphthalene 001855-47-6 0.52

Benzene, 1-methyl-2-(2-phenylethenyl)- 074685-42-0 0.47

1,4-Methanonaphthalene,1,4-dihydro-9-((1-

methylethylidene)- 007350-72-3 0.57

Pentadecane 000629-62-9 0.30

10,11-Dihydro-5H-dibenzo(a,d)cycloheptene 000833-48-7 0.30

Phenanthrene 000085-01-8 0.35

Indeno[2,1-a]indene, 4b,5,9b,10-tetrahydro- 005695-17-0 0.46

9H-Carbazole, 2-methyl- 003652-91-3 0.17

Tetracosane, 3-ethyl- 055282-17-2 0.13

Benzenesulfonanilide 001678-25-7 0.24

E-14-Hexadecenal 330207-53-9 0.40

62.72 סכ"ה

*הריכוז חושב לפי שטח בתגובה של נפטלן.

Page 32: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

End of Certificate

Page 33: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 540659

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 24/02/2019 12:00:00

Sampled by Customer

D240219-0054-2Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 767192Sample No:Tamar Produced water 19.2.19

RefrigeratedStorage conditions: Sampling time: 19/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

EPA 8270Cresol

Cresol 2.70 mg/L

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm8.5 <4

SM 4500 H+BpH pH units8.29

EPA 8270Phenols

Dimethylphenol-2-4 0.72 mg/L <0.02

Phenol 1.84 mg/L <0.02

Total results 2.56 mg/L <0.02

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.170 mg/L <0.025

Benzene 0.140 mg/L <0.025

Ethylbenzene 0.050 mg/L <0.025

MEK 0.720 mg/L <0.025

tert-Butyl alcohol 1.700 mg/L <0.025

Toluene 0.340 mg/L <0.025

Total VOCs 3.490 mg/L

VOC's-target list ראה תוצאות -

Xylene total 0.370 mg/L <0.025

SM 5310BTotal Organic carbon mg/L141.00 <0.5

Page 1 of 2 Created on: 27/02/2019Certificate Of Analysis: 540659

Page 34: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm<4.0 <4

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Lush Cernes Food Chemistry and Pesticide Departments Manager

Natalia Arkhipova Contaminants department lab analyst

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 27/02/2019Certificate Of Analysis: 540659

Page 35: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

נובל אנרג'י שם הלקוח:

D240219-0054-2 קט )במעבדה(:מספר זיהוי הפרוי

19.2.19תאריך הדיגום:

25.2.19תאריך הדיווח:

Page 36: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 767192

Tamar Produced water 19.2.19 הדוגמא:זיהוי

תאריך הבדיקה: 24.2.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Cyclopentanone, 2-methyl- 001120-72-5 0.02

(R)-(+)-3-Methylcyclopentanone 006672-30-6 0.03

Benzene, 1,3-dimethyl- 000108-38-3 0.11

Ethanol, 2-butoxy- 000111-76-2 4.26

Pentanoic acid, 2-methyl- 000097-61-0 0.05

Benzene, 1-ethyl-3-methyl- 000620-14-4 0.04

Ethanol, 2-(2-ethoxyethoxy)- 000111-90-0 1.12

Pyridine, 3,5-dimethyl- 000591-22-0 0.04

Indane 000496-11-7 0.67

Benzene, (2-methyl-1-propenyl)- 000768-49-0 0.32

Phenol, 2,6-dimethyl- 000576-26-1 0.21

Phenol, 2-ethyl- 000090-00-6 0.21

Piperidine, 1,2,6-trimethyl-, cis- 002439-13-6 0.06

1H-Indene, 2,3-dihydro-4-methyl- 000824-22-6 0.59

Phenol, 3-ethyl- 000620-17-7 2.27

Naphthalene, 1,2,3,4-tetrahydro- 000119-64-2 0.26

Phenol, 2,3-dimethyl- 000526-75-0 1.74

Phenol, 3,4-dimethyl- 000095-65-8 1.31

Naphthalene 000091-20-3 0.94

Phenol, 4-(1-methylethyl)- 000099-89-8 1.61

Phenol, 2-ethyl-4-methyl- 003855-26-3 1.27

Phenol, 2-ethyl-6-methyl- 001687-64-5 0.27

Phenol, 3-ethyl-5-methyl- 000698-71-5 0.73

Phenol, 2-methyl-5-(1-methylethyl)- 000499-75-2 0.18

Thymol 000089-83-8 0.51

Phenol, 3-methyl-5-(1-methylethyl)-, methylcarbamate 002631-37-0 1.75

Page 37: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Phenol, 3,4,5-trimethyl- 000527-54-8 1.21

Naphthalene, 2-methyl- 000091-57-6 1.05

1H-Inden-5-ol, 2,3-dihydro- 001470-94-6 0.99

Ethanone, 1-(3,4-dimethylphenyl)- 003637-01-2 0.40

Benzene, pentamethyl- 000700-12-9 0.34

Phenol, 2,3,5,6-tetramethyl- 000527-35-5 0.53

Dewar benzene, hexamethyl- 007641-77-2 0.70

Ethanol, 2,2'-dithiobis- 001892-29-1 0.88

Naphthalene, 2,6-dimethyl- 000581-42-0 0.80

6-Methyl-4-indanol 020294-32-0 1.40

Benzene, 1-methoxy-4-(1-methyl-2-propenyl)- 018272-83-8 0.91

Naphthalene, 2-ethenyl- 000827-54-3 0.59

Benzene, ethylpentamethyl- 002388-04-7 0.31

Fluorene 000086-73-7 0.87

Naphthalene, 1-(2-propenyl)- 002489-86-3 0.45

2-(3-Isopropyl-4-methyl-pent-3-en-1-ynyl)-2-methyl-

cyclobutanone 1000193-37-3 0.15

9H-Fluoren-9-one, hydrazone 013629-22-6 0.27

4,4'-Dimethylbiphenyl 000613-33-2 0.44

10,11-Dihydro-5H-dibenzo(a,d)cycloheptene 000833-48-7 0.19

Phenanthrene 000085-01-8 0.40

Indeno[2,1-a]indene, 4b,5,9b,10-tetrahydro-, cis- 016293-79-1 0.28

Naphthalene, 3-benzyl-1,2-dihydro- 027019-11-0 0.09

Benzenesulfonanilide 001678-25-7 0.11

3-Heptadecene, (Z)- 1000141-67-3 0.03

Phenol, 2,2'-methylenebis[6-(1,1-dimethylethyl)-4-methyl- 000119-47-1 0.51

9-Tricosene, (Z)- 027519-02-4 0.27

34.75 סכ"ה

*הריכוז חושב לפי שטח בתגובה של נפטלן.

Page 38: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

End of Certificate

Page 39: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 540686

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 24/02/2019 12:00:00

Sampled by Customer

D240219-0054Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 767193Sample No:Tamar Produced water 22.2.19

RefrigeratedStorage conditions: Sampling time: 22/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

EPA 8270Cresol

Cresol 3.48 mg/L

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm7.8 <4

SM 4500 H+BpH pH units8.37

EPA 8270Phenols

Dimethylphenol-2-4 1.20 mg/L <0.02

Phenol 3.60 mg/L <0.02

Total results 4.80 mg/L <0.02

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.640 mg/L <0.025

1,3,5-Trimethylbenzene 0.090 mg/L <0.025

Benzene 0.270 mg/L <0.025

Ethylbenzene 0.160 mg/L <0.025

Isopropylbenzene 0.030 mg/L <0.025

MEK 1.600 mg/L <0.025

n-Propylbenzene 0.030 mg/L <0.025

p-Isopropyltoluene 0.030 mg/L <0.025

tert-Butyl alcohol 2.000 mg/L <0.025

Page 1 of 2 Created on: 27/02/2019Certificate Of Analysis: 540686

Page 40: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Toluene 0.600 mg/L <0.025

Total VOCs 6.140 mg/L

VOC's-target list ראה תוצאות -

Xylene total 0.690 mg/L <0.025

SM 5310BTotal Organic carbon mg/L158.80 <0.5

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm<4.0 <4

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Lush Cernes Food Chemistry and Pesticide Departments Manager

Natalia Arkhipova Contaminants department lab analyst

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 27/02/2019Certificate Of Analysis: 540686

Page 41: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

נובל אנרג'י שם הלקוח:

D240219-0054 קט )במעבדה(:מספר זיהוי הפרוי

22.2.19תאריך הדיגום:

25.2.19תאריך הדיווח:

Page 42: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 767193

Tamar Produced water 22.2.19 הדוגמא:זיהוי

תאריך הבדיקה: 24.2.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Cyclopentanone, 2-methyl- 001120-72-5 0.09

(R)-(+)-3-Methylcyclopentanone 006672-30-6 0.11

Androstan-17-one, 3,11-dihydroxy-,

(3.alpha.,5.beta.,11.beta.)- 000739-26-4 0.05

Ethanol, 2-butoxy- 000111-76-2 7.39

trans-3-Methylcyclohexanol 007443-55-2 0.14

Benzene, 1-ethyl-2-methyl- 000611-14-3 0.05

Ethanol, 2-(2-ethoxyethoxy)- 000111-90-0 1.20

Indane 000496-11-7 0.67

Benzene, 2-ethyl-1,3-dimethyl- 002870-04-4 0.08

Benzene, 1-methyl-2-(2-propenyl)- 001587-04-8 0.26

Indan, 1-methyl- 000767-58-8 0.51

Hexadecane, 7,9-dimethyl- 021164-95-4 0.15

Hexane, 2,3,4-trimethyl- 000921-47-1 0.57

Hexadecane 000544-76-3 0.41

Phenol, 2-ethyl- 000090-00-6 0.56

Phenol, 2,5-dimethyl- 000095-87-4 3.88

1H-Indene, 2,3-dihydro-4-methyl- 000824-22-6 1.31

Phenol, 4-ethyl- 000123-07-9 1.17

Phenol, 3,5-dimethyl- 000108-68-9 1.42

Naphthalene, 1,2,3,4-tetrahydro- 000119-64-2 0.50

Phenol, 3,4-dimethyl- 000095-65-8 1.42

Naphthalene 000091-20-3 1.18

Docosane, 11-butyl- 013475-76-8 0.13

Dodecane, 1-fluoro- 000334-68-9 0.15

Phenol, 3-(1-methylethyl)-, methylcarbamate 000064-00-6 1.81

Page 43: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Phenol, 2-ethyl-4-methyl- 003855-26-3 1.17

2H-1-Benzopyran, 3,4-dihydro-2,2-dimethyl- 001198-96-5 0.23

Phenol, 2,4,6-trimethyl- 000527-60-6 1.43

Thymol 000089-83-8 1.68

Phenol, 3,4,5-trimethyl- 000527-54-8 1.14

Naphthalene, 2-methyl- 000091-57-6 1.03

1H-Inden-5-ol, 2,3-dihydro- 001470-94-6 0.81

Ethanone, 1-(4-ethylphenyl)- 000937-30-4 0.65

Phenol, 2,3,5,6-tetramethyl- 000527-35-5 0.58

Dewar benzene, hexamethyl- 007641-77-2 0.42

Ethanol, 2,2'-dithiobis- 001892-29-1 1.04

Naphthalene, 1,4-dimethyl- 000571-58-4 0.80

5-Hydroxy-3-methyl-1-indanone 057878-30-5 0.25

6-Methyl-4-indanol 020294-32-0 1.28

Benzene, 1-methoxy-4-(1-methyl-2-propenyl)- 018272-83-8 1.04

Benzene, 1,3,5-triethyl- 000102-25-0 0.84

Benzene, 1-methyl-2-(phenylmethyl)- 000713-36-0 0.55

Fluorene 000086-73-7 0.73

1-Isopropenylnaphthalene 001855-47-6 0.67

Benzene, 1-methyl-2-(2-phenylethenyl)- 074685-42-0 0.13

N-(4-Methoxyphenyl)-2-hydroxyimino-acetamide 1000143-61-3 0.12

4,4'-Dimethylbiphenyl 000613-33-2 0.26

Indeno[2,1-a]indene, 4b,5,9b,10-tetrahydro- 005695-17-0 0.19

10,11-Dihydro-5H-dibenzo(a,d)cycloheptene 000833-48-7 0.08

Phenanthrene 000085-01-8 0.10

Benzenesulfonanilide 001678-25-7 0.08

Cycloeicosane 000296-56-0 0.07

Phenol, 2,2'-methylenebis[6-(1,1-dimethylethyl)-4-methyl- 000119-47-1 0.43

43.05

*הריכוז חושב לפי שטח בתגובה של נפטלן.

Page 44: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

End of Certificate

Page 45: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 544743

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 04/03/2019 14:10:00

Sampled by Customer

D050319-0023Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 773353Sample No:Tamar Product water 1.3.19

RefrigeratedStorage conditions: Sampling time: 01/03/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

EPA 8270Cresol

Cresol 5.06 mg/L

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm9.8 <4

EPA 8270Phenols

Dimethylphenol-2-4 2.44 mg/L <0.02

Phenol 3.09 mg/L <0.02

Total results 5.53 mg/L <0.02

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.440 mg/L <0.025

1,3,5-Trimethylbenzene 0.070 mg/L <0.025

Benzene 0.490 mg/L <0.025

Ethylbenzene 0.170 mg/L <0.025

Isopropylbenzene 0.030 mg/L <0.025

MEK 0.920 mg/L <0.025

MIBK 0.060 mg/L <0.025

n-Propylbenzene 0.030 mg/L <0.025

p-Isopropyltoluene 0.030 mg/L <0.025

tert-Butyl alcohol 1.290 mg/L <0.025

Page 1 of 2 Created on: 12/03/2019Certificate Of Analysis: 544743

Page 46: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Toluene 0.750 mg/L <0.025

Total VOCs 5.010 mg/L

VOC's-target list ראה תוצאות -

Xylene total 0.730 mg/L <0.025

SM 5310BTotal Organic carbon mg/L253.60 <0.5

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm<4.0 <4

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Keren Rachel Ben David Contaminants department lab analyst

Lush Cernes Food Chemistry and Pesticide Departments Manager

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 12/03/2019Certificate Of Analysis: 544743

Page 47: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

נובל אנרג'י שם הלקוח:

D050319-0023 קט )במעבדה(:מספר זיהוי הפרוי

1.3.19תאריך הדיגום:

10.3.19תאריך הדיווח:

Page 48: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 773353

Tamar Product water 1.3.19 הדוגמא:זיהוי

תאריך הבדיקה: 6.3.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Pyridine, 3-methyl- 000108-99-6 0.09

Pyridine, 3,5-dimethyl- 000591-22-0 0.01

Cyclohexanol, 2-methyl-, cis- 007443-70-1 0.04

Cyclohexanone, 3-methyl- 000591-24-2 0.01

Pyridine, 3,4-dimethyl- 000583-58-4 0.16

Ethanol, 2-(2-ethoxyethoxy)- 000111-90-0 0.39

Benzene, cyclopropyl- 000873-49-4 0.12

Pyridine, 3-ethyl-4-methyl- 000529-21-5 0.06

Pyridine, 5-ethyl-2-methyl- 000104-90-5 0.02

Phenol, 2,6-dimethyl- 000576-26-1 0.17

Phenol, 2-ethyl- 000090-00-6 0.27

Phenol, 3-ethyl- 000620-17-7 0.95

Phenol, 3,5-dimethyl- 000108-68-9 1.30

Phenol, 3,5-dimethyl-, methylcarbamate 002655-14-3 1.59

Phenol, 3,4-dimethyl- 000095-65-8 1.20

Naphthalene 000091-20-3 0.46

Phenol, 2-propyl- 000644-35-9 0.08

Phenol, 2-(1-methylethyl)- 000088-69-7 1.63

Phenol, 3-ethyl-5-methyl- 000698-71-5 1.14

Benzene, 1-ethyl-4-methoxy- 001515-95-3 0.35

Phenol, 2,4,6-trimethyl- 000527-60-6 0.38

Phenol, 2-methyl-5-(1-methylethyl)- 000499-75-2 0.76

Phenol, 2,3,5,6-tetramethyl- 000527-35-5 0.98

2,5-Diethylphenol 000876-20-0 1.44

Phenol, 3,4,5-trimethyl- 000527-54-8 1.01

3-Methyl-4-isopropylphenol 003228-02-2 0.63

1H-Inden-5-ol, 2,3-dihydro- 001470-94-6 0.96

Benzene, pentamethyl- 000700-12-9 0.31

Benzene, hexamethyl- 000087-85-4 0.75

Page 49: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Benzene, 1,2-diethyl-3,4-dimethyl- 054410-75-2 0.78

6-Methyl-4-indanol 020294-32-0 0.93

Benzofuran, 2,3-dihydro-2,2,4,6-tetramethyl- 003698-49-5 0.40

Fluorene 000086-73-7 0.42

1-Isopropenylnaphthalene 001855-47-6 0.24

3,3'-Dimethylbiphenyl 000612-75-9 0.11

1,4-Methanonaphthalene,1,4-dihydro-9-((1-

methylethylidene)- 007350-72-3 0.08

4,4'-Dimethylbiphenyl 000613-33-2 0.16

Anthracene 000120-12-7 0.09

N-(4-Methoxyphenyl)-2-hydroxyimino-acetamide 1000143-61-3 0.06

Indeno[2,1-a]indene, 4b,5,9b,10-tetrahydro-, cis- 016293-79-1 0.10

3-Methylcarbazole 004630-20-0 0.04

20.69 סכ"ה

*הריכוז חושב לפי שטח בתגובה של נפטלן.

End of Certificate

Page 50: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 538015

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-4Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763270Sample No:Tamar Open Drain- Oil water separator 13.2.19

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

In house

procedure;Based on

EPA 1664

G&O-FTIR ppm5.3 <4

SM 4500 H+BpH pH units9.31

In house

procedure;Based on

EPA 1664

Total petroleum

hydrocarbons

ppm<4.0 <4

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 1 of 1 Created on: 20/02/2019Certificate Of Analysis: 538015

Page 51: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 542048

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-5Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763271Sample No:Tamar Open Drain- Oil water separator 13.2.19

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

DIN 38 406Nitrogen (Ammonium) as

N

mg/L<0.05 <0.05

SM5210B ; The

oxygen

measurement is

based on: SM 4500

O C & SM 4500 O G

BOD mg/L399.00 <0.5

In house

procedure;Based on:

EPA 8260

BTEX

Benzene NOT

DETECTED

mg/L <0.025

Ethyl Benzene 0.040 mg/L <0.025

Toluene 0.070 mg/L <0.025

Total BTEX 0.400 mg/L

Xylene 0.290 mg/L <0.025

SM 4500Cl- EChlorides mg/L320.80 <2

In house procedure

GC/FID

Ethylene Glycol by GC/

FID

Ethylene Glycol NOT

DETECTED

mg/L

SM 3120BICP

2/ Phosphorus (P) 10.595 mg/L

2/ Zinc (Zn) 1.859 mg/L

Total nitrogen calculated

as N

-5.81

SM 4500 NO2-BNitrogen (Nitrite) as N mg/L<0.001

Home method for

Nitrate in high

organic environment

Nitrogen (Nitrate) as N mg/L<0.20

Page 1 of 2 Created on: 04/03/2019Certificate Of Analysis: 542048

Page 52: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

In house

procedure;based on

EPA

Scan by GC/MS

Scan by GC/MS ראה נספח -

Scan by GC/MS Report see appendix -

In house

procedure;Based on:

EPA 8260B

VOC

1,2,4-Trimethylbenzene 0.210 mg/L <0.025

1,3,5-Trimethylbenzene 0.050 mg/L <0.025

Ethylbenzene 0.040 mg/L <0.025

Toluene 0.070 mg/L <0.025

Total VOCs 0.660 mg/L

VOC's-target list ראה תוצאות -

Xylene total 0.290 mg/L <0.025

SM 4500 S2-FSulfides mg/L0.60 <0.2

In house

procedure;Based on:

SM 2540C

Dissolved solids dried at

103°

mg/L1180.00 <50

SM 4500 NorgBNitrogen (organic) as N

by kj

mg/L5.81 <0.1

SM 5310BTotal Organic carbon mg/L267.70 <0.5

SM 2540DTotal suspended solids

dried a

mg/L38.0 <1

SM 2130BTurbidity NTU46.10 <0.1

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Ludmila Eiderman ICP department team leader

Natalia Arkhipova Contaminants department lab analyst

Nazi Botershvili Environment department team leader

- End Of Certificate -

Page 2 of 2 Created on: 04/03/2019Certificate Of Analysis: 542048

Page 53: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

תעודת בדיקה

נובל אנרג'י שם הלקוח:

D140219-0022-5 קט )במעבדה(:מספר זיהוי הפרוי

13.02.19תאריך הדיגום:

4.3.19תאריך הדיווח:

Page 54: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

זיהוי הדגימה

בדיקה: מספר תעודת 763271

Tamar Open Drain-Oil water separator 13.2.19 :זיהוי הדוגמא

תאריך הבדיקה: 28.2.19

התגלו החומרים הבאים: MS/GC -בסריקה ב

Name of substance -Identification by NIST library CAS Semi Quant.* (mg/L)

Indane 000496-11-7 0.20

Indan, 1-methyl- 000767-58-8 0.08

Benzene, 1-ethenyl-4-ethyl- 003454-07-7 0.08

Phenol, 2,4-dimethyl- 000105-67-9 0.12

Phenol, 2,3-dimethyl- 000526-75-0 0.10

3-Cyclohexene-1-methanol, .alpha.,.alpha.4-trimethyl- 000098-55-5 0.35

Naphthalene, 2-methyl- 000091-57-6 0.10

Naphthalene, 1-methyl- 000090-12-0 0.12

Naphthalene, 2,3-dimethyl- 000581-40-8 0.06

1.23 סכ"ה

*הריכוז חושב לפי שטח בתגובה של נפטלן.

End of Certificate

Page 55: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 538763

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-8Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763274Sample No:Tamar RedFox Snitary waste 8980

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

SM5210B ; The

oxygen

measurement is

based on: SM 4500

O C & SM 4500 O G

BOD mg/L10.00 <0.5

SM 4500 CIGChlorine (residual) mg/L<0.05

SM 9230A+CEnterococcus cfu/100mL26000

SM 9222DFecal coliforms cfu/100mL240000

SM 4500 H+BpH pH units7.02

SM 2540DTotal suspended solids

dried a

mg/L5.0 <1

SM 2130BTurbidity NTU6.55 <0.1

Test start - Microbiology tests: 14/02/19 11:36

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Page 1 of 2 Created on: 22/02/2019Certificate Of Analysis: 538763

Page 56: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Results on this certificate are authorized by

Elena Sokolov Microbiology department quality trustee

Nazi Botershvili Environment department team leader

Sima Aizendorf Microbiologu department lab analyst

- End Of Certificate -

Page 2 of 2 Created on: 22/02/2019Certificate Of Analysis: 538763

Page 57: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 542407

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-9Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763275Sample No:Tamar RedFox Snitary waste 8980

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

DIN 38 406Nitrogen (Ammonium) as

N

mg/L36.72 <0.05

SM 4500Cl- EChlorides mg/L113.00 <2

SM 3120BMetal by ICP

2/ Phosphorus (P) 8.949 mg/L

Total nitrogen calculated

as N

-40.42

SM 4500 NO2-BNitrogen (Nitrite) as N mg/L<0.001

Home method for

Nitrate in high

organic environment

Nitrogen (Nitrate) as N mg/L3.66

In house

procedure;Based on:

SM 2540C

Dissolved solids dried at

103°

mg/L420.00 <50

SM 4500 NorgBNitrogen (organic) as N

by kj

mg/L36.76 <0.1

SM 5310BTotal Organic carbon mg/L29.50 <0.5

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Page 1 of 2 Created on: 05/03/2019Certificate Of Analysis: 542407

Page 58: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Results on this certificate are authorized by

Ludmila Eiderman ICP department team leader

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 05/03/2019Certificate Of Analysis: 542407

Page 59: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 538760

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-6Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763272Sample No:Tamar RedFox Snitary waste 8985

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

SM5210B ; The

oxygen

measurement is

based on: SM 4500

O C & SM 4500 O G

BOD mg/L5.20 <0.5

SM 4500 CIGChlorine (residual) mg/L0.14

SM 9230A+CEnterococcus cfu/100mL90000

SM 9222DFecal coliforms cfu/100mL720000

SM 4500 H+BpH pH units7.59

SM 2540DTotal suspended solids

dried a

mg/L29.0 <1

SM 2130BTurbidity NTU28.40 <0.1

Test start - Microbiology tests: 14/02/19 11:36

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Page 1 of 2 Created on: 22/02/2019Certificate Of Analysis: 538760

Page 60: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Results on this certificate are authorized by

Elena Sokolov Microbiology department quality trustee

Nazi Botershvili Environment department team leader

Sima Aizendorf Microbiologu department lab analyst

- End Of Certificate -

Page 2 of 2 Created on: 22/02/2019Certificate Of Analysis: 538760

Page 61: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 541491

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-7Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763273Sample No:Tamar RedFox Snitary waste 8985

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

DIN 38 406Nitrogen (Ammonium) as

N

mg/L85.21 <0.05

SM 4500Cl- EChlorides mg/L204.90 <2

SM 3120BMetal by ICP

2/ Phosphorus (P) 20.250 mg/L

Total nitrogen calculated

as N

-136.95

SM 4500 NO2-BNitrogen (Nitrite) as N mg/L49.170

Home method for

Nitrate in high

organic environment

Nitrogen (Nitrate) as N mg/L1.62

In house

procedure;Based on:

SM 2540C

Dissolved solids dried at

103°

mg/L962.00 <50

SM 4500 NorgBNitrogen (organic) as N

by kj

mg/L86.16 <0.1

SM 5310BTotal Organic carbon mg/L34.30 <0.5

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Page 1 of 2 Created on: 03/03/2019Certificate Of Analysis: 541491

Page 62: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

Results on this certificate are authorized by

Ludmila Eiderman ICP department team leader

Nazi Botershvili Environment department team leader

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 03/03/2019Certificate Of Analysis: 541491

Page 63: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 537975

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022-10Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763276Sample No:Tamar Gray water 13.2.19

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

SM 9230A+CEnterococcus cfu/100mL<100

SM 9222DFecal coliforms cfu/100mL15000000

SM 4500 H+BpH pH units6.06

Test start - Microbiology tests: 14/02/19 11:36

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Natalya Kosin Microbiology department lab analyst

Sara Grossman Enviro department consultant

Sima Aizendorf Microbiologu department lab analyst

- End Of Certificate -

Page 1 of 1 Created on: 20/02/2019Certificate Of Analysis: 537975

Page 64: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

08-9308308 08-9300991, 08-9401439

18 Hacharash st., Ness Ziona, Israel, 7403125

www.bactochem.co.il [email protected]

Certificate Of Analysis: 541485

Final Report

Chain of Cust. Form no. Customer Netila Sample Acc. Time 13/02/2019 16:00:00

Sampled by Customer

D140219-0022Project:

Customer details

Name:

Address:

City:

Zip:

Name:

Contact details

Phone:

Mobile:

Fax:4672530

ABBA EVEN EVN12

NOBEL ENERGY

HERZLIYYA

Sample description: 763277Sample No:Tamar Gray water 13.2.19

RefrigeratedStorage conditions: Sampling time: 13/02/2019

Analysis RemarksMethodLOQ*UnitsSpecificationResult

DIN 38 406Nitrogen (Ammonium) as

N

mg/L9.17 <0.05

SM5210B ; The

oxygen

measurement is

based on: SM 4500

O C & SM 4500 O G

BOD mg/L204.00 <0.5

SM 4500Cl- EChlorides mg/L114.68 <2

SM 4500 CIGChlorine (residual) mg/L<0.05

In house

procedure;based on

EPA 418.1

Oil and Grease in Ftir ppm22.9 <0.3

SM 3120BMetal by ICP

2/ Phosphorus (P) 2.752 mg/L

SM 5540CAnionics surfatants mg/L0.08

Total nitrogen calculated

as N

-19.34

SM 4500 NO2-BNitrogen (Nitrite) as N mg/L<0.001

Home method for

Nitrate in high

organic environment

Nitrogen (Nitrate) as N mg/L<0.20

In house

procedure;Based on:

SM 2540C

Dissolved solids dried at

103°

mg/L750.00 <50

SM 4500 NorgBNitrogen (organic) as N

by kj

mg/L19.34 <0.1

SM 5310BTotal Organic carbon mg/L100.00 <0.5

In house

procedure;based on

EPA 418.1

Total petroleum

hydrocarbons (TPH)

mg/L1.8 <0.3

Page 1 of 2 Created on: 03/03/2019Certificate Of Analysis: 541485

Page 65: Lab reports · Boris Gil Contaminants department lab analyst Nazi Botershvili Environment department team leader ... Ethylbenzene 0.050 mg/L

Form No. F-603-09. Procedure QP-021

SM 2540DTotal suspended solids

dried a

mg/L52.5 <1

SM 2130BTurbidity NTU120.00 <0.1

Remarks

• The results are approved for samples tested only.

• The reference for the "specification limits" is stated in the footnotes.

• This report should be addressed as a whole and parts of it should not be copied.

• LOQ - Limit Of Quantification

• This report is submitted for the exclusive use of the person or corporation to whom is addressed, and

neither the report nor the name of these laboratories nor any members of its staff may be used in

connection with the advertising, sale or any product without the written permission of

Bactochem-Laboratories Ltd.

Results on this certificate are authorized by

Ludmila Eiderman ICP department team leader

Sara Grossman Enviro department consultant

- End Of Certificate -

Page 2 of 2 Created on: 03/03/2019Certificate Of Analysis: 541485