lab s9::soo

80
LAB SLD Users Code Uo S9::SOO ALL COiJTAirlERS THIS FORM ACCOt1PANIES ARE COLLECTIVELY REFERRED TO AS "SA.'-1PLE". CERTIFICATE OF FIELD PERSONNEL Sample Type: Hater ll?J Soil 0 Other Water Supply and/or Code City & County u· ueQQut' · Collected (date & time) i30C:... gj-/-9 By (name) ---------------1 pH= / ; Conductivity= .... -:::: umho/cm at °C; Chlorine Dissolved Oxygen= .c: mg/1; Alkalinity= ., ....... -: ; Flow Rate= AVl Samyling Location, & Remarks (i.e. odors etc.) f5MW tl3 (Jvwtf 11eecr "( leJ-/ . (' ' . r:;·._ ·,..·, ' . t' .. ' I certify that the statements in this block accura ely ref e t the results of my field analyses, observations and activities. Signed u\ qy I certify that I w i tn e s sed · these f i e 1d ana 1 y s .... """'o¥b::::;:s o"""n-'s='-a n.cd;g::a=-ct-:-,, .... v...,..i ..,...t ,-=-· e-s-a -nd-=--c-o -nc-u \'Jith the statements in -this block. Signed ------------------ Method of Shipment to Laboratory ttq\A"- THIS FORM ACCOI-1PANI ES Z., septum vials \-•• s--c-s-.,...i d-.-e-n-=-t-.-i f""'i,_e,.d_a_s_: ____ _ specimen85"ofo7t..30l.; duplicate8fc/o9t1C>2. ; triplicate ; blank(s) , and amber glass jug(s) with teflon-lined cap(s) identif.ied as ------ and other container(s) (describe) identified as Containers are mar"ed as follows to indicate preservation (circle): ------ No preservation; sample stored at room temperature (-20°C). P-ICE: · Sample stored in an ice bath. -a 2 o 3 s 2 : Sample preserved with 3 mg Na 2 o 3 s 2 /40 ml and stored at room CERTIFICATE{$) OF SAMPLE RECEIPT I (we) certify that this sample was transferred from to ------------------- 1---------------- at (location) ______________ on (date & time) • and that the statements in this block are correct. Disposition of Sample • Seal (s) Intact: 1ief(;]f I Signature(s) ___ ___ t ( 1 t · ) tiQUID a oca 1 on c' t GRoun 8 on 1------------- · wtiRVEILLA·" (date & time) ________ and that the statements in this block Disposition of Sample ___________ Seal(s) Intact: Yes 0 No 0 Signature(s)

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Page 1: LAB S9::SOO

LAB NUt~BER

SLD Users Code Uo ~· S9::SOO ALL COiJTAirlERS ~~HICH THIS FORM ACCOt1PANIES ARE COLLECTIVELY REFERRED TO AS "SA.'-1PLE".

CERTIFICATE OF FIELD PERSONNEL Sample Type: Hater ll?J Soil 0 Other

------------------------~ Water Supply and/or Code No.~~-~~~~·~~~~~~~------------~~~--~~ City & County u· ueQQut' · Collected (date & time) i30C:... gj-/-9 By (name) ..:s·~,es ---------------1 pH= / ; Conductivity= ....-:::: umho/cm at ~ °C; Chlorine Residual=~-----t

Dissolved Oxygen= .c: mg/1; Alkalinity= .,.......-: ; Flow Rate= AVl Samyling Location, t~eth~ds & Remarks (i.e. odors etc.)

5oJ,V\~(~ Gc>tl~<-+~d--K-c'"" f5MW tl3 dvrl~ (Jvwtf .Je~t 11eecr ~d "( leJ-/

. (' ' . r:;·._ ~· ·,..·, ' . t' .. '

I certify that the statements in this block accura ely ref e t the results of my field analyses, observations and activities. Signed u\ qy I certify that I w i tn e s sed · these f i e 1 d ana 1 y s .... e~s ~, """'o¥b::::;:s :.;;.er..:..v-.~~a~t::...i o"""n-'s='-a n.cd;g::a=-ct-:-,,.... v...,..i ..,...t ,-=-· e-s-a -nd-=--c-o -nc-u \'Jith the statements in -this block. Signed ------------------Method of Shipment to Laboratory ttq\A"- \)e.h~..r~ THIS FORM ACCOI-1PANI ES Z., septum vials \-•• -.n-"'::t-=-e~f~l o.:...n_.:-~l7i n-e-d~d.,...i s--c-s-.,...i d-.-e-n-=-t-.-i f""'i,_e,.d_a_s_: ____ _ specimen85"ofo7t..30l.; duplicate8fc/o9t1C>2. ; triplicate ; blank(s) , and amber glass jug(s) with teflon-lined cap(s) identif.ied as ------and other container(s) (describe) identified as Containers are mar"ed as follows to indicate preservation (circle): ------r· • No preservation; sample stored at room temperature (-20°C). P-ICE: · Sample stored in an ice bath. - a2o3s2: Sample preserved with 3 mg Na 2o3s2/40 ml and stored at room temperatur~.

CERTIFICATE{$) OF SAMPLE RECEIPT I (we) certify that this sample was transferred from to -------------------1---------------- at (location) ______________ on

(date & time) • and that the statements in this block are correct.

Disposition of Sample • Seal (s) Intact: 1ief(;]f I V~tfJ Signature(s) i-(~;)-~;~ti-ty ___ -t-h-~t-_-t_h_-;; ___ ;a--;-~-;-;--~-~-;--t-;-~~-;_t_;~;~d-t;~~---------------~N-2-~ig85-----t~-

t ( 1 t · ) tiQUID w,1sr~1 a oca 1 on c' t GRoun8 on 1------------- · wtiRVEILLA·" ~I'ATER.

(date & time) ________ and that the statements in this block are'~Cforrect..

Disposition of Sample ___________ • Seal(s) Intact: Yes 0 No 0

Signature(s)

Page 2: LAB S9::SOO

""''"' O!lillill ~--~-~~ ~ Iii ~Mil ill 'Oo!l' I il ~~ ~ i M ~·~~ *lllii ~~!lAO~ . "- .. ... ~'"'''" ·-

Rt~RL YSES REOUES,.~ED LAB. N~Q· {)f_G . :)-cr i :..::;,.=;::, CE!::CK Tr.E /·..F:i)i:OPRI/,l~~"O:·:ES :C.:::LO~·: TO E:DI C\.1!:. THE T,.,,,,l Or A.::.;ALYTIC/;.1. SCREI::;s F.EQt;I!. 1,"HI::.:r:~:ER ?OS SIBLE LIST SPECIFIC CO~·lPOL~mS SUSPECTED OR REQUIRED.

..:.. ~

> ~ > w

EXTRRCTRBLES "'""' :>

P.URGERBLE I-' :>

:- t-' '- 1-'

:c:: t- <:: :-:- < r- < ,... ;_ 1- :-

' z ' z - ,__ < :::; . SCREEN < < SCREEN ;::l ;::::; ;::l C' c- c· s-

ALIPHATIC HYDROC.ARBON SCREEN ALIPHATIC HYDROCARBONS ARO~~TIC HYDROCARBO~ SCREEN CHLORH~ATED h"YDROCARBON PESTICIDES

~HALOGE~ATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

tX GAS CHROHATOGRAPH /1-Lt..S S SPECTRO!-U:TER h1DROCARBON FUEL SCREEN ORGN~OPHOSPHATE PESTICIDES POLYCHLORINATED BIPH~~LS (PCB's) POLYh~CLL~~ AROMATIC HYDROCARBONS

SPECIFIC COMPOUNDS SPECIF"IC •"·

COMPOUNDS

- -

p,-vt.P"'S · Lo K1~ Dr1 f, -k• .L. :.. - .!\. • 0 I (\MC.\Jf"i Y • ,of' I.J.D1c hiKod·h«.t/11_ I };·J -rnalff~~c IAA.. f-e--h Gh lo ~c e...J-lt+ttVJ.. ~ J J

ANALYTICAL RESULTS CONC- CONC-

COMPOUND ENTRATION COMPOUND ENTRATIC

Gc /Ms ?u~ea£~ II~ D 1 ~ /,/ :o e :fh en e Ia /A c; ).I

"' I I J - T r; c. /,{e-r-e e.fh (l-.-JL ~~c 1--f

v

Te fro. t.l! <h" o e-ft. e.-....f 8 .V'i (1!_ ./

* DETeCTION LIHIT

HJ1ARKS:

CETRIFICATE OF ANALYTICAL PERSONNEL Seal(s) Intact: Yes No . Seal(s) Broken by date 1 certify that I followed standard laboratory procedures on handling and analysis of this

sample unless otherwise noted and that the.statements in thi~~ck and the analytical dat• on this page accurately ref~ect the analyucal results for thl. '/~le. L -Date(s) of analysis 1/sv(<fj....- • Analysts signature flt~ P J.d.,.

Icertify that I have revie\o.'ed and co:-. ::ur with the analytical resultsCfor this sample and \o.Ti th the stateTTPnro::: in this block. :.~viewers Signat:1r~:

Page 3: LAB S9::SOO

,, ;19~s-LAB~~ATORY __ --c:-----­b\IJ\(OY)rYJ€~')"kf ~(cJ<.,~wtf j;1 1){5/(/V\

J/-e(jlfh i &J1tJJvc:~~'Jf-eu+ 0isr/u4~,LJ- LAB NUMBER o/ 6o~ /)

ALL CONTAINERS WHICH THIS FORM ACCOMPANIES ARE COLLECTIVELY REFERRED TO AS 11 SAMPLE 11•

CERTIFICATE OF FIELD PERSONNEL Sample Type: ~·Jater ~ Soil[] Other

------------------------------------~ Water Supply and/or Code No. BfAvr R, 'SLj)6r'f(jVlid (<:< b, City & County -:)L D/ !1/b.

1

Collected (date & time)fS)-/-{ Of30 By (name) J~w' r, /5-hvt.. 5~{"t0 pH= ,.----;Conductivity= -- umho/cm at- °C; Chlorine Residual=------------t Dissolved Oxygen= - mg/1; Alkalinity= -- ; Flow Rate= ,_ Sampling Location, Methods & Remarks (i.e. odors etc.) ------i

Bfcc"'~.) J-o qac'W'j)lvt '/ S<:<VtAfl~.)

I certify that the statements in this block accurately r~'f1ect'th~' r~·sUhs of· my field analyses, observatL.ns and activities. Signed 5Je~Sa~.5 t"-'·-' I certify that I witnessed these field analyses, observations and activities and concur \'Jith the statements in this block. Signed ____________________ _

Method of Shipment to Laboratory__!..;/);....t<~"'_:[=--.:G;:::;..,:.--"rv-:-:r~e~L~-..-::----.-.-:---~:--;-;--:;=...------­THIS FORM ACCOMPANIES ~septum vials with teflon-lined discs id~· ~ specimen ; duplicate ; triplicate ; blank(s)@_;oror3o, and amber glass jug(s) with teflon-lined cap(s) identified a , and other container(s) (describe) identified as . Containers are mar~ed as follows to indicate preservation (circle):

( ~JD..· ~ No preservation; sample stored at room temperature (-20°C). P-IC~ Sample stored in an ice bath. -~-~ 2 o 3 s 2 : Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

CERTIFICATt(S) OF SAI~PLE RECEIPT I (we) certify that this sample was transferred from to --------------------------1------------------------ at ( 1 oca t ion) ______________________ on (date & time) and that the statements in this block are correct. -----------Disposition of Sample . Seal (s) Intact: Yes 0 No[] Signature(s) ------------------I (we) certify that this sample was transferred from to ---------------------·--------------------at (location) _______________________ on (date & time) and that the statements in this block are correct. ---------------Disposition of Sample . Seal(s) Intact: Yes 0 No[] Signature(s)

Page 4: LAB S9::SOO

"'

"-' i

ANALYSES REQUESTED LAB. No.: ORG- 6L! PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. WHENEVER POSSIBLE LIST SPECIFIC CO}WOUNDS SUSPECTED OR REQUIRED.

._, ~ ~· ~ :> :> :> H H PURGEABLE H ~ EXTRACTABLE ~

<r: ~ H H

H H H H H H H ~ ~ ~ SCREENS ~ ~ SCREENS g. g 0'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HA ~c;t<:NATED HYDKOCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES rx GAS CHROMATOGRAPH/MASS SPECTROMETER HYDROCARBON FUEL SCREEN

ORGANOPHOSPHATE PESTICIDES POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS TRIAZINE HERBICIDES

SPECIFIC COMPOUNDS SPECIFIC COMPOUNDS

REMARKS: ...,__

ANALYTICAL RESULTS COMPOUND [PPBJ COMPOUND [PPBJ

I (-0;c4/;_....,r;;.r;;:.t~ene. tJD I I 1-Tr;c. L/cY'~~Ii~Ci"e PD -r c' .;.r, C< ( L 1 (}.-·n.' e. H, tL.J4.. uJ.D

fl) ,, I'> +L_ Q.r ? ~'-Y'j e n b f:?s j) e. ·k c -kcl * -·---·-

-

* DETECTION LIMIT £.-tt)' /./

REMARKS: /

- --

CERTIFICATE OF ANALYTICAL PERSONNEL Seal(s) Intact: Yes NO . Seal(s) broken by: date: - -I certify that I followed standard laboratory procedures on handling and analysis of this sample unless otherwise noted and that the statements in th~~ock and the analytical data on this page accurately reflect the analytical results for th . sample. ~ . Date(s) of analysis: .3/IJB_) . Analyst's signature: . mt?UJd·v ~-•--' I certify that I have reviewed and concur with the analytical resu~s fo~ this sample and with the statements in this block. Reviewers signature:

Page 5: LAB S9::SOO

//;;_;/of ~

P.G'"''"'- -- ironmental l~ovement Division '·.· ·/) .. · ..... E'..tJ./1 'lth & Environment Department _r. 01\ ;)_OV . Box 968 - Cr~vm Building

"' / ~;;,...). LA. TORY _______ _

LAB tiUI~BER ~~ . . ' •·. · .. ta Fe' r~ew f-lieX lCO 87504-0968

~ [Jt."i"" .. DtfJ AI TErn ION: .S}e: . .JIIL ~'\\!..) I'- BUREAU: Gcc•J<\~w~\.swc t dcac...•Cu"~ Wll~f<.. SLD Users Code tJo. Sy,soo

ALL COIJTAirlERS HHICH THIS FORM ACCOI1PANIES ARE COLLECTIVELY REFERRED TO AS "SAMPLE".

CERTIFICATE OF FIELD PERSONNEL Sample Type: \·Jater (gl Soil 0 Other Water Supply and/or Code No. \)1\) 'M YS'"'-W3 City & County A\ ~u ~ ~J<c..-\ ~ '-(.1 B~_~, ncJ, \ \ o

Collected (date & time8r0/09 0202. By (name) 5\:e..v'€~5Ct<e:-.S pH= _ ___- ; Conductivity= ~- umho/cm at ~ oc; Chlorine Residual= ---Dissolved Oxygen= ~ mg/1; Alkalinity= ....--· ' Flow Rate= i j_ 3 j Ptvl Sampling Location, Methods & Remarks (i.e. odors etc.)

:Sctw'\H (L c.<ri I -e.'--~~ ·Hv\1\J\ P..s M w J!. 3 Jv·nvt5 pv'IM.p h.5t-1 IZ Ml.ll\. t.~ (t-(f (Jv•"'p,~~tj be..')~IA. .

,. ( (; ., ' / r; _.. . {1·( / ~. ;-, (~ /<7 ; •,·_:. . ' . ' ' ' ( ·"- I

I certify that the statements in this block accurately re~ the results of my field analyses, observatiC.ns and activities. Signed ~W /ct-I certify that I witnessed·these field analyses, observations and activities and concur ~Jith the statements in -this block. Signed -Me-thod of Shipment to Laboratory t\C) "'-~ \) e.,h" ~s=..Q_d.. . THIS FORtlt ACC011PANIES ~ septum vials h 1 i..n teflon-1 ined discs identified as: specimen~501'o9o~~ dup1icate~6Jc9ozo·ZcSS triplicate ·; blank(s) ' and amberg ass jug(s) with teflon-lined cap(s) identified as , and other container(s) (describe) identified as . Containers are mar~ed as follows to indicate preservation (circle): NP· No preservation; sample stored at room temperature ~20°C).

C P-rcD Sample stored in an ice bath. l"-"Na203S2: Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

CERTIFICATE($) OF SAMPLE RECEIPT I (we) certify that this sample was transferred from ______________ to

I-------------------- at ( 1 ocat ion) _______________ on (date & time) t and that the statements in this block are correct.

Disposition of Sample . Seal (s) Intact: H'i:s 0 No 0 Signature(s) C f IV Eo i-(~;)-~;;tif;-th~t-thi~-~~~~;;-~;~-t~~~~f;~~;d-f~~;-------------ij[ih;-2~-;--~------t~-

at {location) LIOliLo v ~5 on ~-------------------------- . r~S~~ (date & time) ______________ and that the statements in this lSi}~ ~'®ttD~rrect.

L!lif~fk: 'AT£R Disposition of Sample _______________ . Seal(s) Intact: Yes LJ' No 0 s·i gna ture ( s)

Page 6: LAB S9::SOO

~- IU~ . _,iillll""" ~~-~~ li"loill!li: . -·- - ...~.!Wi .... "1011' ~iii 1111 "'-""~- ,"'·

Rt~RL YSES REouc-s:ED LAB. N,O. o e(; - .;;6 ' . . . ' ~ C~i:..C::

........... /~?::O?Rl/-.T~~..:.O:·:ES EELO:·: TO I!:DI C/,T.:. THE T '·""""' Or k:ALYTICAl. SCRE:::::;s F.EQ'CIL _ ' -. ..... .._ ............ .. ~ ........

1,!1!:::\E\'t:R ?OSSIBLE LIST SPECIFIC co~-n>oe:ns SUSPECTED OR REOUIRED.

(..:..;

> ~ ::> t.:.:

EXTRRCTRBLES - ::>

P-URGERBLE t-: ::>

'- 1-' '- 1-'

~ '- < <-< e- < ,_ t-: t-. - z ~ z

::: ::::; .SCREEN < < SCREEN ::;J ::;J

c- c- c· r--.-

ALIPHATIC HYDROC.A.REON SCREEN ALIPHATIC HYDROCARBONS ARO~~TIC HYDROCAR30N SCREEN CHLORD~ATED HYDROC.ARBON PESTICIDES ~~OGE~ATED HYDROCP.REON SCREEN CHLOROPHENOXY ACID HERBICIDES

rx GAS CHRO>L~TOGRAPn /NASS SPECTROHETER hl"DROCARBON FUEL SCREEN ORGAl\OPHOSPHATE PESTICIDES POLYCHLORINATED BIPH~~LS (PCB's) POL\~~CLL~ ARO}~TIC HYDROCARBONS

SPECIFIC COMPOUNDS SPECIF"IC ,·.

COMPOUNDS

- - ~

P-;:"•P~-..·c:. &x:.K y \ .for ') \ Q, &\oro ;J,.-\be~:t...J l, I J \1 Tc ,c=,b\occ ~+\,q Y' L J --~· -"-··"- .?,V'-~(\w'\4.("' 1 ·-r e kc.... c" I Mt'H~.~e n -t- ""

ANALYTICAL RESULTS CONC- CONC-

COMPOUND ENTRATION COMPOUND ENTRATIC

I' /- n I 'c h.!c-r-v e ~~. ~ n e ,;2. t(p 'j 1.1 I, / 1 / - Tr, (. L /c_.-y-u c: fia n ~ co JJL: lfi

Te Ire, c. k /err n c~ -Ji e,., e I() IL: /) {/

* DETECTION LIHIT

Et:'1-1PJ~.KS:

CETRIFICATE OF ANALYTICAL PERSONNEL Seal(s) Intact: Yes No . Seal(s) Broken by date I certify that I followed standard laboratory procedures on handling and analysis of this sarc.ple unless othendse noted and that the statements in this block and z analytical dat< on this page accurately reflect the analytical results for ~~mple. · Date(s) of analysis I ( 8 otts= . Analysts signature ,e?--r,.-v.t..,_ / ~?...---

!certify that I have reviewed and co~~ur with the analytical resultl)1for this sample and vdth the s t a tenPn r-~ in this block. :.c\'iewers Signature:

Page 7: LAB S9::SOO

1 84- 0498 -D

LABORATORY s· ~ D P.r. I 0 r< I fy ]_ LAB NUMBER OK -'ftfJ? /1; 4 e-

SLD Users Code tJo. 59~ tJ o COLLECTIVELY REFERRED TO AS 11 SAMPLE 11

CERTIFICATE OF FIELD PERSONNEL Sample Type: ~·Jater llil Soil 0 Other

------------------------------------~ Water Supply and/or Code No. NM iok.l ~~~~~==~~~~~~----------------------~

City & County ). /3 - ,')/o Collected (date & time) '840410 !/.30 By (name) ~Aj pH= f.~ ; Conductivity= {;50 umho/cm at 2l-J °C; Chlorine Residual=------1 Dissolved Oxygen= mg/1; Alkalinity= ; Flow Rate= Sampling Location, Methods & Remarks (i.e. odors etc.) -----------1

P/IJ m PerzsoAJ S-t-/-1. fYlr)fiJ. we II f s h1 4)- !f-4-·

I certify that the statements in this block accura el~ analyses, observaticins and activities. Signed I certify that I witnessed these field analys~~'f"L=-~~~=~L:-::--:-.,-:---:-----with the statements in this block. Signed ~~

t1ethod of Shipment to La bora to ry_-!-'/1~/l-'-AI:..=......,d~_C":----'-o/=-/ ,....v~e""'iR.=::e=--d~-,----..,......,-~~,.---.,.·------­THIS FORM ACCOMPANIES~ septum vials with teflon-lined discs identified as: specimen 1 ; duplicate I ; triplicate ; blank(s) and amber glass jug ( s) with tefl on-1 i ned cap( s) identified as -----and other container(s) (describe) identified as Containers are marked as follows to indicate preservation (circle): -------

No preservation; sample stored at room temperature (-20°C). Sample stored in an ice bath. Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

CERTIFICATE(SJ OF SAIWLE RECEIPT I (we) certify ~hat this sample was transferred from K~v ,·IV' L~l,~gf to

·2 fVl e '/ rK ( e u---- at ( 1 oca t ion ) __ S_'-_1_~------------- on (date & time) tjJ~[9(j if· S1)f?r- and that the statements in this block are correct. Disposition of Sample o ~ _.Jeal (s) Intact.: Yes ,0' No 0 . Signature(s) Kev-z.--. ~--- LZn~~.hh-.--------------------------------------------------------------~----u: ____________________ _ I (we) certify that this sample was transferred from R E G E 1 V E D. to •-------------------- at ( 1 ocat ion) on (date & time) ________ and that the statements i~~\1f~ ~%~ are correct. Disposition of Sample . Seal (s) Intact: Yes 0 No 0 -----------------------Signature(s) GROUND WATER/HAZARDOIIS WASTE

-------------~----------------------HIIKt-A1 ---------------------

Page 8: LAB S9::SOO

ANALYSES REQUbJTED LAB. Nl. 4-q~ - ._,.,

PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. TVHENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

~ g: :> ~ ~ EXTRRCTRBLES H :>

PURGERBLE'', H :>

~ H H H H < H

H < H < H H H H

~ ~ SCREEN ~ ~ SCREEN.-p p 5' CY 0' CY

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

X GAS CHROMATOGRAPH/:t-tASS SPECTROMETER HYDROCARBON FUEL SCREEN ORGANOPHOSPHATE PESTICIDES POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS

SPECIFIC COMPOUNDS SPE:CIF'IC COMPOUNDs''·

RE:t-tARKS:

ANALYTICAL RESULTS CONC- CONC-COMPOUND ENTRATION COMPOUND ENTRATION

C/+iLJJfW FOR Vl-1 3//-d/t ,/v

* DETECTION LIMIT t~<J l{ REltARKS: Nu t>f-kt>Jr 1'1A>''/;z4J,~e d..zle, fe_ J. ./0

v

CETRIFICATE OF ANALYTICAL PERSONNEL . · Seal(s) Intact:~) No . Seal(s) Broken by #c -:..J/1 date ~l/2 6/?'/ . I certify that llowed standard laboratory pro~dures on handling and analysis of this sample unless otherwise noted and that the statem~nts in this block and the analytical data on this page accurately reflect the analytical results for this~~Pt:l , Date(s) of analysis ij./26/Ff . Analysts signature ' -, :)...;;}t.iy !certify that I have reviewed and concur with the analyti~~~his sample and with the statellP.nf"R in this block. Reviewers Signature: / /?-; · '

~ ~{71/

Page 9: LAB S9::SOO

..

ICAP ·SCREEN

lab Number: f..l tYl 12o Sample Code :._...:_(J_S...:_M...:.....:...:\A.J::.__-.....::t,::::..!A~---

Date Submitted: 4/ 11 } tcif

By: ¥ Date Reported:._· -'+-/.:_1'1.!.-j/~~...:.i./1 ____ _

By: to 'f

Detennination Concentration (~g/ml)

Aluminum <o.,o Barium D I I (

Beryllium ..,( O. lO

Boron o.;xf Cadmium <·o./Q

Calcium G. _ ..

, !J.

Chromium <0.10

Cobalt <tJ.tO

Copper <CJ.!{)

Iron <o. tCJ

Lead <a.,a Magnesium ·f.~

Manganese <:'D110

Molybdenum <'Ci.l/J

Nickel <o, 1{)

Silicon a~-.

Silver <CJI LCJ

Strontium o.t/-~ Tin <o..Jo Vanadium <::a. ICJ

Yttrium <0.1{)

Zinc <a, 1 tJ

Page 10: LAB S9::SOO

ATOMIC ABSORPTION ANALYSES

Arsenic < {), 00 ~/- pg/ml

Selenium <!.. o. Do<;·- pg/ml

Mercury <. {), Do o S- p.g/ml

Page 11: LAB S9::SOO

< REPO~T TO: l·!ate·r Pollution Control Bureau Environmenta1 ~provement Oivisio~ Health ?! Env), ..,nment Department

LAB ~NU!1BER _!fJt- ~;jr]t)_~ .. ·----

P. 0. Uox 968 - Crown Building DATE ~H:\.tiVED --!/--j/_~ f_y[_ __ _ 9.~ TE REPORTED _§_j.li/- ~'f._})\f 'JED Santa F~, l~i·l 87503

R E C E \ IITTE1HI ON: D~ vG f3v &.u--__ _ Initials

\·JATER OR ~~THJATER ANALYSES-ENERGY DEVELOPHENT t~ONITORING PROGRAM -n I• • '· i' ::>f(i\lS \'1 ;\·) · .

Lat/Long ___ 0 ____ '_' 0 . I II T R __ s ___ _ Station/We 11 Code fSA/1 {_,L/ - (o ~ NPDES No-------­

Co 11 ected S.tV(Y( ;o ~9'.20 By Cc.A--a;;>~:.J kA""" t3 fA~ r Date Time Name

Outfall No --:---

Ct Lv//1 uJ Unit

Pumping Conditions ~'~~-~---~~-d--~---~-~-~~-~-~-~~~~­\·iater Level ;.:r:;·,9'{~' fro~ A1 f /V' )/L~ bc•e pH ( 00400) 9-, s-

Svrfd.e -----~--Conductivity Staff Gage Height --------­

Control Structure ---------(Uncorrected) __ --:t-_o_c_1 --~~J.A....:mho

0 is charge ______ ......,_ __ viater Temp (00010) I r °C

Conductivity at Samp 1 e Type --=-~:......r....:::c>-;._h _____ _ 2 5 oc ( 00094) _____ ____;::...vJTI:;._ h~

From NF, A-HN03 sample:

[]Arsenic, total

0 Barium, total

[]Cadmium, total

[] Lead, tota 1

C !.'1olybdenum, tot

[]Selenium, total

Ouranium, total

Ovanadium, total

0Zinc, total

METAL ANALYSES -

-------A 0~ te d( From F, A-HN03 sample: .. · ·--~ na yze ---

)..!.. g/ 1 ~Arsenic, dissolved ~5.o ~g/1 , pg/1 Barium, dissolved J,I..Q/1

' ,u9/l 0 Cadmium, dissolved Mg/ 1

' ' p..Q/1 EZJ Lead, dissolved ,u..g/1

I

p.g/1 g) t~1o1ybdenum, diss ) .u-911

.!-49/1 !S4 Selenium, diss <_r;, 0 p.g/1 '

,&.A.Q/1 [] Uranium, diss I ,.,..g/1

J.ol91 1 0 Vanadi urn, di ss I !.1.9/1

,M.Q/ 1 gzinc, dissolved J..C.911 •

Date Analy_zed

Lff-u L"'~ '

~Ltt:f Lw I '

Remarks _...:t:.(J1::::......:.;4_t _u_/1-"_,_.~....,_u_.N'\ ____ ~-~~-------~--~---~~-C. f.{ (C a !'- 1 u.A/\

This form accompanies 1 sample(s) marked as follows to indicate field treatment (circle):

NF, ~··\·!hole sample; acidified with 5 r.1l cone HN0/1 /-~--A-HNO~: )iltered sample (0.45rmembrane filter); acidified v.riih 5 ml ~- cone HN0~3f-l

Page 12: LAB S9::SOO

,,

/ R~?ORT TO: Water Pollution CQntrol Bureau E~vironmental r~provement Division Health r. En vi. ~ment Ocpartrent P. 0. dox 968 - Crown Building Santa Fe, NM 87503 .4 TTEiH I 0:~: Del_'! e <f?>o O .v-·

__ _ :f C-_D _ lJ .{f r~ _ _( C}t'; f s·?w() _ _____________ .:..._ _________ _..:...:.:...:.......;~.;__....;__::....:....:....___::.:......:.....;.....;.::___;-·. ·--- ·········

'y!AIER OR \·lAS TE\~ATER AN.!l.L YSES-ENERGY DEVELOP!"1EiH I•WNITORING PROGRA!•l

~~ Lat/Long 0 1/p .. 11 ;

0 r: T R S ___ _

r!1

Station/\·iell Code ps.M v-JI..JkJt NPDES No . --·--- Outfall No __ _ \Y Cell ected ~'ltrYICJ crr::z.o By uA.~7t~---~3v---e../ CtVJ/fl,~

Date Time ~~N~a~m~e~~~~--~~U~n~i.~~------

Pumping Conditions _'__!.....{ ;;:..., d=·_:_.:.j_e_:d:...... ---------------------

1-:a ter Leve 1 1 .:<. 5'.15"/ fr.,~ ;1-1 P "--.<>'a ~-x, ....,_ wrf.:.c e. pH ( 00400) _....:...-~_ .. ..::.s--____ _

Staff Gage Height.--------­

Control Structure

Conductivity (Uncorrected) 7-00 .Pmho

Discharge

Sar.:ple Type ·'

~-!ater Temp (00010) _..:...1...:...7-_____ °C

Conductivity at zsoc (00094) ..u-mho

GENERAL vJATER CHEf.iiSTRY AND NITROGEH At~.!l.l YSES r -... -... -.. -.-...... -.. -. ----_'-., ______ D_a_t_e _____ l?9-__ p---_j.JI...,....,..._'O.-K'...,....t-O-::J,_ ___ ---------- Date

~~~~~-' ~~~ samp1_~: Analyzed ~- From F, NA sample: ,, ---Analyzed 1)4 io:agnes i um ( 00925 ) ____ mg/1

~c(~?;;m6~~5)---~) . ...r .. mho --- g) 8icarbonate(00440) mg/1

QTo~al ____ mg/1 ___ ..0 Calcium (00915) mg/1

nonfilterable P4 Chloride (00940) mg/1 residue (suspended)(OOS30)

From NF, A-H 2so4 sample:

0 i~i tra te + ____ mg/1 nitrite, total (00630)

0 Amii:onia, total (00610)

mg/1 ----

0 Chemica 1 ···-~ ~·--·· ~---- -·~··--·mg/.1 .. ""-""-""<---

oxygen derri-~[ntr ·.'r _:. :. , , ! ( 00340) ! : '! . ,, ; . ' - . .: :' ; ~

~ Potassium (00935) mg/1 ___ _

.@ Sod i urn ( 009 30) mg/1

~ Su1 fate (00945) mg/1 ----(3 Tota 1 filter- mg/1

ab 1 e residue ----(dissolved)( 70300)

fQ ( Q_J· b;_ r1 .>l . ....j.Q _______ _ '4----' . -·~ ~· .-· -~-"~ ----, \ rom F :-·A-H

2SO

4 sampJ e:

~ !litrate + 3. 3 <? mg/1 J;g-nitrite, dissolved fH (00631)

IVY~. . d. ~ rJil'TIOn 1 a, 1 S-:

solved (00608)_1

.12$1 :yo t.~ I ~-4< -~

tJ.,IP mg/1

Page 13: LAB S9::SOO

- - . - .. ·-. ---Environmental Improvement Division He a 1 th ~ Env · •nmcnt Dcpartrent P. 0. ~ox 96~ - Crown Building Santa Fe, NM 87503 ATTEUTIO:~: .I2cl'!e ~dO .e.r--

Y.'ATER OR HAS TEHATER AN.A.L YSES-ENERGY DEVELOPJljENT J··10NITORING PROGRAH

Sample Location (Yv~ Pt-<.>oAJ c;/.4/!0N ....

~~ Lat/Long 0 t / II • 0 &: T R s

------~u~n~*~-' ----------PS.M vJi@\A NPDES No . Outfall No

I 1 Station/Hell Code

~Y Collected "3-'-/ o-f 10 crt :.:zo By aMS7r_-0&"" ;v-e.l Gr (/._.) /1-1 vJ ---Date Time ~-7.N-arn~.e~~~~-----~~Un~i~t---------

Pumping Conditions ----r3d : )e d

Staff Gage Height.------------­Control Structure

Discharge

Sample Type ·'

Conductivity (Uncorrected) 100 .Pmho

~-later Temp (00010) /7 °C _ _;_,;, ______ _ Conductivity at

2 5 oc ( 00094} - ,.o-mho

GENERAL vJATER CHEf.liSTRY AND NITROGEi1 Atj.A.LYSES

~:-F-, -~~~~sa-;1_~;- .: ) Date Analyzed

~Condgctivity ,Umho l£l (25Jf)(00095) --

0Tofal mg/1 nonfilterable residue (suspended)(00530)

From NF, A-H2so4 sample:

0 !{itrate + ---~mg/1 ____ _ nitrite, total (00630)

0 1\ • /1 1"\m;r,on 1 a , ---~mg

total (00610)

0 Cheml·ca1 ffir-,~-1'1·. 11 r · .. ; . ·.· · :. • "lt..~ r~\ .. ~.r ~~ :· ,:

oxygen eman nil __ Ll --~- : . , ; J , • · r I . . .

--e1 r 'CJ~lt?.b___ ;: • :z '-t If-/ It, An~layteze"' From F, NA sample: ~ _,..---- " ~ /•lagnesium (00925) 6. 3 mg/1 s/;; ~ 8 i carbon ate ( 004 40) ;9tf, 0 mg/ 1 S/;b

;

~ Ca 1 ci urn ( 00915} ~;-7, .:< mg/1 ,:;-/ ;;

P4 Chloride - (00940) 'j3J?J mg/1 r?-7 ~ Potassium (00935) }. frO mg/1 1'-Q Sodium (00930) po mg/1 _..;.;,.,~--E;l Sulfate (00945) (07~~ mg/1 .5/1... B Tot a 1 fi 1 ter- 5/6 mg/1 sji·'il

able residue (dissolved)(70300) C'J 1.:::/;

/2__(~~~-k:--~. < "'l (="'---

c_~rom F, A-H 2so4 sa_n:pJ'1:

~ !litrate + .....-----mg/1 nitrite, dissolved (00631)

d d -----H-0-IL~J " .1"! •• - • • . - .• :

( 00340) ~',\, 11u!tJ 5 1984 :l . v d :\ ..

· · . A l...: JS:rt-JillTlonia, dis-: ____ mg/1 CP.•JUN9 \!~TE~iHAi.ARU6tlS \ •• \~ •. : solved (00608).

1 BliRBJ 11\A ~ f< /'"' L& -:rotd I "f~ -This form accomj')anies A sample(s) marked as follo1·:s to indicate

~: \-lr.Jol e salilpl e (n·o· filtration) @ i~o acid added (F) EiJ~ered in field v1ith O.ll5unembrane filter

,: -· · · ·· r·..... · · , : . _ 1 •• " "' , 1 1 r r~ ,~ 1

f'ield treatment:

Page 14: LAB S9::SOO

1ijf0 84- 0499 -D

REPORT TO: Environmental Improvement Division Health & Environment Department P.O. Box 968 - Crown Building Santa Fe, New Mexi ~504-0968 ATTENTION: ., - I e

elf· ~99 /?; 1· c/ LABORATORY

5Lr-"·'i;'}~P,_n -:r-t tn-(~r,_-f -~--LAB NUMBER .

BUREAU: C> l-U SLD Users Code tlo. 5Ci ~t3L"' ALL CONTAINERS WHICH THIS FORM ACCOMPANIES ARE COLLECTIVELY REFERRED TO AS "SAMPLE".

CERTIFICATE OF FIELD PERSONNEL Sample Type: ~Jater [2:' Soil 0 Other

r ----------~------------------------~ Water Supply and/or Code No. I ~~~~4=~~~--~~~~---------------------4 Ci ty & County A/- B - eR. A

Collected (date & time) 'i!tfOL/Jo 12. ") pH= 7-, S ; Conductivity= t-oo umho/cm at Dissolved Oxygen= mg/1; Alkalinity= Sampling Location, Methods & Remarks (i.e.-o-d.-o-r-s""'"'e"""7t-c-.-.,------

~JY1~J ~ <1c.t fY\H\ LJ t 1/ P~ ;v\ Lu -· bfi

I certify that the statements in this block accur t l}.refl analyses, observati0ns and activities. Signed----J!.-Ao:~~~~==:J:at::~~ I certify that I witnessed these field anal -:--:"7"'0--an-d.,.--co_n_c_u with the statements in this block. Signed ..._...,.,'----Method of Shipment to L_.aboratory ~c. rV\£ : t w/1 ~··f.) -t f ·--.--------THIS FORM ACCOMPANIES ,~septum vials with teflon-linej 'dlscs identif·ed as: specimen I ; duplicate I ; triplicate / /; blank(s) and amber glass jug(s) with teflon-lined cap(s) id~'ntified as -----and other container(s) (describe) identified a~, Containers are marl::ed as follows to indicate preservatior· (circle): -------NP: No preservation; sample stored at room temperature (-20°C).

-ICE: Sample stored in an ice bath. P-Na2 3s2: Sample preserved w th 3 mg Na 2o3s2/40 ml and stored at room temperature.

CERTIFICATE(S) OF SAI1PLE RECEIPT I (we) certify that this sample was transferred from Kevi_JJ L&~bc=.R.'t to

·}! M7 ~-he~"' at (location) ..S U) on (date & t1me) 'ljlo/flY c.f:sve,...... and that the statements in this block are correct. Disposition of Sample, I)K. _.;9eal (s) Ipt,act: Yes ral No 0 Signature(s) ~~ --..:·q./4.---~ >>rJ~e*...,Jit,~lc>L=ju::..__ _______ _ ------------------------------------------------------~-----·--------------------------I (we) certify that this samp I e was transferred from R E C E I V E D _ to

·---------------------------- at (location) on (date & time) ________ and that the statements tnP.Vh2s3 ~~ are correct. Disposition of Sample . Seal(s) Intact: Yes 0 No 0 Signature ( s) GROUND WATER/~AZARDOUS WASTE

-~------------------------------------------ .... REAY _

Page 15: LAB S9::SOO

ANALYSES REQUb., I TED LAB. Nt t.f-qo , I PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. l~ENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

[,~ 4q1· ~ g: v :> ~ g: EXTRRCTRBLES H :>

PURGERBLE''· H

~ H ~ H

H ~ H ~ H H H H

~ ~ SCREEN ~ ~ SCREEN·' g ~ ~ 0' 0' 0'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

'X GAS CHROMATOGRAPH/~~SS SPECTROMETER HYDROCARBON FUEL SCREEN ORGANOPHOSPHATE PESTICIDES POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS

SPECI~_IC COMPOUNDS SPE:CIF'IC COMPOUNDs•'·

Rm~KS:

ANALYTICAL RESULTS CONC-

COMPOUND CONC-

COMPOUND ENTRATION ENTRATION

) , 1- rWJ.-'1.{~~ I L/- ~ 1.-t_~

II i-T,. J)J ::rl~_,..<1__ t;/ c~f_ V-<L-'

D:t:.o.-eJJ 0 .1-J "~- /() /1 :?0-'-"-4 /t

/ C/

* DETECTION LIMIT I WL/1 REl~KS : /'/o ~fl._t., ~/"(\ uJ;-&.. ,p,__----t;:J:;I /0

I ()

-----. CETRIFICATE OF ANA ~YTiff-L PERSONNEL . , ;'-) \ ---1 _,, /' (

Seal(s) Intact: ~j No . Seal (s) Broken by --J · date 1-//J (;;;, 6 f . I certify that I~~llowed standard laboratory proce~ res on handling and analysis of this sample unless otherwise noted and that the statements in this block and the analytical data on this page accurately ,re~l~ct the analytical results for th~~saLJ~~ Date(s) of analysis 11-'--£/8~' . Analysts signature \Jv"" - . ' Icertify that I have reviewed and concur with the analy~c<fosults~ this sample and with the statetTPnrR in this block. Reviewers Signature: /J- '

-- ' ? -e?l-- J.h--

Page 16: LAB S9::SOO

!CAP ·SCREEN

Lab Number :._--JHL....:..' _M...;.._tf,.L...Ez:!loo;.;l _____ _ Sample Code : _ _..:p_~.:::...:..:.M.:....\V~--S.:_ .... .....:.A __ _

Date Submitted: 1/ It l ~Lj. By = _ ____.B_.;__&-l~ril~l'f'.:__ _____ _

Date Reported : __ fo-1,/r._l_'l--~../_t:.....'f~·----By: m1

Determination Concentration (~g/ml)

Aluminum ..( tJ,tO

Barium 0. I €

Beryllium <o.Jo

Boron o, '31

Cadmium ~ {)~ 10

Calcium l~t.

Chromium <o.;o

Cobalt <D,IO

Copper <o. ;o

Iron <o.tO

Lead <o,;o

Magnesium lb. Manganese o. l"" Molybdenum <o,,o

Nickel <o,t::> Silicon :J£ Silver <o. 10

Strontium o.to Tin <c!J,JCJ

Vanadium < t),j{) Yttrium < O.to

Zinc <tJ,ILJ

Page 17: LAB S9::SOO

•·

ATOMIC ABSORPTION ANALYSES

Arsenic < 0. 0 (;) t:.;' pg/ml

~

Selenium < t>, D D ~ pg/ml

Mercury < q, O£"l0 <;._... pg/ml

Page 18: LAB S9::SOO

; REPO~T TO: \·/a ter Po 11 uti on Control Bureau LAB 1\UiiBER _j;tjl~ __ /~~'-,1-Environmental ~~provement Divisic1 ~·~ Health .~~ En vi ,rr;ent Depa rtmGnt Of\TE R:.. _IV ED /./ _ d.:::J' .u! P. 0. !3ox 968- Crm'l'n Building -r T----S~~~a Fe.: .~~i·i ~87503 - .. , ~.tnE REPORr~o e:.:, It_! J \'\/ -.lnf.:_

. ' IE DJ\ I I ttHI Oil. uAu Jf:..;j Be :j("'/Z.. -+ t- In1 ti a1 s !{ [ L• '1... ' . . . - /)_ n r. r- c \ \, ~ \ ·· · .. --f;L- 'r---!t1e>7- c~7 -.s-7-so.o

,_ . \tATER 'OR WASTHJATER ANALYSES-ENERGY DEYELOPI<\ENT 1<\0NITORI NG PROGRAM

-'•. , .. ~-r.-.\~:. \'!.\';if f) IV !1'1 f.£') ;?I! s7: t: ?1) c:r'cu;·:D »~mp1 e· .. Loc·a t ion ___ r ______________________ _ U~L<. ~:\ J

Lat/Long

Station/Well Code

Collected

0 I II_, 0 I II T R s 9 < 'I> ------- -----rs /f./liD - S/7 NPDES No . > ' I I . --- _Out fa 11 f31ZJ4t: 9 /~fC-C By J::/: I'./ ;c. lit(( ' ' I I

oa;,e / 1 /1}me Name Unit )vall~

Pu-~i~ Conditions -~~~~~~~~~~----------~~----\ c p U 11 1 \·!a ter Le ve 1 } 4 f.·, {/) ;;;((J Jl ~ -:r( pH ( 00400) __ ?._~ _:::.1 ___ _

Staff Gage Height --------­

Control Structure ---------

0 is charge --r---rr---t----'-:---

Conductivity f3 5D ( U nco rr ect e d) --..._...,..,.----__:_).A_mho

~later Temp (00010) C)C) °C

Conductivity at (~t<t( b ' Sample Type--------- 250( ( 00094) ..,vJTiho. ______ _...:__

METAL A1JAL YSES ~ -------------

From NF, A-HN03 sample: Date (rom F, A-Hi-m- s~m~ Date Analyzed Anal~zed

[]Arsenic, totul ..ug/1 ~Arsenic, dissolved -< ~. 0 ,,u. g/ 1 *I '2.1:, ,Ja--t 0 Barium, total M Barium,

[]Cadmium, total

0 Lead, tot a 1

0 l·iolybdenum, tot

0 Sel eni urn, total

[]Uranium, total

0 Vanadi urn, tota 1

[]Zinc, total

~g/1

,u g/1

.u-9/1 .

.u911

p.g/1

}-1.9/ 1

--...&;Ag/1

--~J..'-9/1

Remarks 'X2i 1/W/'/]ftJU?V} ~ ChntrrY~~

dissolved ).1..9/1 E- Cadmium, dissolved

I

M9/1 I

~Lead, dissolved I ,U.9/ 1

tRf ~lo l ybdenum, dis s ,u.g/ 1 I

~'selenium, diss L.. .;-. 0 p.g/1 . 0 Uranium, diss

I E-A-911

0 Vanadi urn, di ss ----r,Mg/1 )SQ' Zinc, dissolved ---lf-911

This form accompanies " I sample(s) marked as follov.:s to indicate field treatment (circle): T.&tl!iOS \~ho 1 e samp 1 e; acidified with 5 ~ 1 cone Hti03/l / __ F, A-HN0

3: Filtered sample (0.45.)-Amernbrane filter); acidified \'-.lith 5 ml

cone HN03;1 .

<+L t1 L ft'f I

Page 19: LAB S9::SOO

''''' • ,,_,. < ."M '•'·' .,._ •. -,_.r<h,.•~••-,'V.>i• - ... ··-·-· --·---E:1vironmental Improvement Division He a 1 th ~ Env.; 'lment iJC!partrent DATE RE,..-·lVED /t!..r!;_;__;..2_/ d.}_ 11 -1/-J d P. 0. tiox 96b Crown Building . ~ ~ Sant~ Fe,' ;n-i ~87503 1\ DATE RE?ORTEU ~ ?dsJ!:r_ ATTE~lTIO~~= __jj_f}U 1~ Bo~e!Z.;. __ ._ Initials

. . -.. --· ----. . --~t,_h_" __ t(#!z -~ _0:?s_~-~---------rJATER OR HAS TE\~ATER AN.!l.L YSES-ENERGY DEVELOPI"ENT HONITORJNG PROGRAH

Sample Location

Lat/Long

Station/Well Code

Collected

Pumping Conditions

-~\-later Level

Staff Gage Height_-----...'"--­Control Structure

Conductivity 0 0 :7""\ -- -

( U nco r r e c ted ) _O;;,__:;;/--=(___../::;...__ __ P-_mho ·

Discharge

Sample Type

~-!ater Temp (00010) ~ · °C

Conductivity at 2soc {00094) _

GENERAL WATER CHHliSTRY AND NITROGEt~ A~ALYSES

Date J Analyzed rom F, NA sample:

·'!' .. ~}lagnesium · (00925) ~ 8icarbonate(00440)

&J_calcium (00915)

~Chloride - (00940)

·~ Condgct i vity ).JJnho ~ (25 C~(00095) ---

0 Tota ~ mg/1 nonfilterable residue (suspended)(00530) fM. Po tass i urn (00935)

r&l_sodi urn (00930) ~Sulfate (00945)

From NF, A-H2so4 sample:

~Total filter-able residue

0 t{i tra te + ___ __;mg/1 nitrite, total

~ (t!-:~blved) 0300) (00630)

0 ~ . /1 ,-.mmom a , ____ mg total (006lb) ---

r.a-mho

Date .----Analyzed

mg/1 mg/1

mg/1

mg/1

mg/1

mg/1 mg/1 mg/1

t3--!litrate + ~, 3 ':?- mg/1 f(r~ nitrite, dissolved (00631)

O.!Lf mg/1

,.. . . ,, """\

This form accom[)anie~~;.i:.:;.J d- sc:mple(s) marked as follm·Js to indicate field treatment:

~ _ .1·-Jh ... ol e sa;npl:. (n·o· f.i ltrati_on) ~ r~o acid added ~~~11 ~ered 1n Tield vnth 0.4~)-A mer.1brc:r:e ill L.er -

., '.' ~ r- . • I ' "" .' • . .• ~ '? ... ' .- . ., . .. ,__ c: (\ I l

Page 20: LAB S9::SOO

c P.~?ORT TO: \·later Pollution Ccmtro1 Bureau LAB'"I~u!'.1"BERJi..:L_i~?;;j/ E:-~vironmental r...,provement Division ,....., """"'"--'J;~----Hea 1 th ~ En vi., .. 11cnt Ll~partrent D.C\TE REC ED -fl~~f/(. P. 0. t)ox 968- Cro':m Guilding · /---

~ ~~ ~~r; ~:l :~~.853 !1~2~ BotfOZ., DATE RE? omu ;( :'f/' :::_;n ~.1; . · .~cb .. .I~!Z .e&£k .s~s_;:y__~ ..

r!ATER OR HA.STE\~ATER AN.C\LYSES-ENERGY DEVELOPHENT HONITORING PROGRAI•i

Sample Location

Lat/Long

Station/Well Code

Call ected

Pumping Conditions

~i; l·:ater Level

Staff Gage Height . -------;---­

Control Structure

Discharge

Sample Type . '

CHD-liSTRY AND

Date HA sample: _ Analyzed

'l2{cond~ctivity ,.t •• Lmho ~ (25 C~(00095) ---- ---

[] Tota~ mg/1 nonfilterable · ---residue (suspended)(00530)

From NF, A-H2so4 sample:

0 !{i tra te + ____ mg/1 r.itrite, total (00630)

Conductivity ( d) C?q7"1 ll h Uncorrecte ~;/C-/ ~m o

~·!ater Temp (00010) -~dc)..:::;:r;..~----· °C

Conductivity at 2 soc ( 00094)

/ ~ rom F, NA sample:

P-mho

_:t/.~.3 Date ·- Analyzed

~Jlagnesium (00925) !Lf.;,~ mg/1 'c"//;

~ Bicarbonate(00440) 167./ mg/1 o'1t7 )

&a-calcium (00915) C'-5_. :{ mg/1 ; / ,

~-Chloride (00940)

~ Potassium (00935)

~Sodium (00930)

~Sulfate (00945) S-Tota 1 fi 1 ter-

able residue

t4. (.., ? mg/1

£2. q mg/1 l ("'--; '7' /l · i.::; ; •. · mg St/{, mg/1

! 1

s- /.1 s)-; '3

d C~;!jz~~~~o-~ t) 0 .~mmonia, ____ mg/1 1 ~-

total (00610) r__~-:~~-~samp1e: 0 Chemical rm.~l,(Br-_··~~---:r·~,--,.------,- ~:litrate + _______ mg/1

---~~r~)~ "'"' ~-,.J.,, .. ~ .. ~ ... ,~ . .,m ...,. ( 00340) ~I -- ----1:.' •• l.< _J ____ ~\ I i I ( 00631)

\ JUrl 5 1984 Ill li oxygen demand ]' '( '1i ·"21 <'· '•, '1/f) cJ, ': 1 nitrite, di sso 1 ved

l _______ __,ill ct__A'iL'Tion i a , dis-: ____ mg /l

GRuUN[J t~AH~/H.~ZAROOUS WASTE ~J~d (00 0~) f\J, ~-- ~ Trois 7orm acco~;nnies d- sample(s) marked as follov:s to indicate f'ield treatment:

iiF: \·ihol e sa:r,pl~. (,no f_i.l,trat_i_on) . ~ r~o acid added ]_"':~red :n ;-,e1d 1-n:n 0,4~,.u.mer.1Drar:e Tilter

( . \ ·- c- n 'j .. .. - ~ -l : :.: - ...! ' I.: ~ h '? ,........., ,... r-. .-.,.. u c n I 1

Page 21: LAB S9::SOO

ALL CONTAINERS WHICH THIS FORM ACCOMPANIES ARE COLLECTIVELY REFERRED TO AS "SAt1PLE".

Sample Type: Hater~

pH= --- ; Conductivity= -- umho/cm at °C; -------- ------

I certify that the statements in this block a cu analyses, observatiC.ns and activities. Signed::...-.p:::::-.~~~~;..:::;:~~'-l-7::::r.--:-:-----;-­I certify that I witnessed these field anal with the statements in this block. Signed

~~~-------+~-----Method of Shipment to Laboratory · ~ THIS FORM AC C0f1P AN I ES 3 ~ septum v 1 a r-s uw..~.ti .,_.t hf-"'i9.'t-e"""fl.==o:....:n"*-~l 1.-J'. n=e,.dg~·~s,...-d...,.i...,.de_n...,.t-.-i """f ,.,.-. e......,d,_a_s_: ____ _ specimen X ; duj)Ticate )( . __ ; triplicate ~; blank(s) and amber glass jug(s) with tenon-lined cap(s) identifie as ------and other container(s) (describe) identified as Conta1ners are marked as follows to ind1cate preservation (circle): ------

No preservation; sample stored at room temperature (-20°C). Sample stored in an ice bath. Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

CERTIFICATE S OF SAf~PLE s mple was transferred from to

~~~~~~~~~---r-

1....{,.~~~~~~~~~:::.;:::.-+-+--- at ( 1 oca t ion )___..~~::..-L.-~..,.a....-=-..~.=.::~=-- on statements in this block are correct .

. -#'::i/fl!f.~:t.LL.~~-----· Seal (s) Intact: Yes)8l No 0 Dispos iti o Signature(s) I (we) cert i-fy--1-t:::.:h>\-a t-t~h ...Jli s..,_:....u:>=:;..u.._-+-t'--t--~-~~-;-f-;;~;d- f~~~ -:;;rlM~YL.,$;;;l --------~~-•-------r--r---r----w-R+E et p.p~am ion) on (date & time) ~~~ and that the statements in this block are correct. Disposition of Sample 1 A 1004 • Seal (s) Intact: Yes 0 No 0 --------~~H)~~'(~x~~~-~.u~o~---Signature(s)

GROUND WA }lUREAU

r

Page 22: LAB S9::SOO

- -·-"' . .,..._..--.-·· - ··-· --· -~

ANFIL.. 't'SES • , ... r· U' , .. ,._.,j L....:·- ,!.....&... LAB. 1'-JC~.F () I~G- .. , +1'l "------··---PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. liHENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

j:zl ~ :> j:zl ~ EXTRACT ABLES H :>

PURGERBLE''· H

~ H ~ H

H ~ H ~ H H H H

~ ~ SCREEN ~ ~ SCREEN·, & 0' 0' g ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

'X GAS CHROMATOGRAPH/~fASS SPECTROMETER HYDROCARBON FUEL SCREEN

- ORGANOPHOSPHATE PESTICIDES POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS

SPECIF.IC COMPOUNDS SPE:CIF"IC COMPOUNDS, ..

REMARKS: Wcr . 1 " c'Id . -£1-L (/

---

·ANALYTICAL RESULTS CONC- CONC-

COMPOUND ENTRATION COMPOUND ENTRATION

-.

* DETECTION LIMIT l//4/1 REUARKS: #1/;) " """"/ ~ .... rk.id /t/

I (/

. CETRIFICATE OF l)~ALYTICAL PERSONNEL ' I / ~ t( Seal(s) Intact:~ No . Seal(s) Broken by l ~# . date ~ U J . I certify that I allowed standard laboratory pro edures on handhng and analyss of this sample unless otherwise noted and that the state ents in this block and the analytical data on this page accurately ~jf2le~c~ the analytical results for thi~~ Date(s) of analysis ~~ ~ s~jlz-f . Analysts signature

sample and Ice r t ify that 1 have reviewed and cone u r with the an a 1 y t i ca 1 ~ ~r>s ults ~this with the stateiiP.nt~ in this block. Reviewers Signature: ;J -< (;;' -;;£~ •' JJ / ) • j ; •• (>;:./ .~./ 'p --

- ·- ...

Page 23: LAB S9::SOO

!CAP ·SCREEN

Lab Number :_.!._tjL-.:...-;n-!..-___:.Jf..:...J ....:...SJ __

Date Submitted: i.f b I / '6t-{ --~~,~~,~------

By =_..J..loiB~~=-Fr::..L.~f--____ _

Determination

Aluminum

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead

Magnesium

Manganese

Molybdenum

Nickel

Silicon

Silver

Strontium

Tin

Vanadium

Yttrium

Zinc

Sample Code: p$ M W - .1-f.- A-Date Reported: . {:, /11 / ~If

r\.--v\ cr r I By: D I I

----~~~---------------------

Concentration (llg/ml)

<O.IO

o. /0

<o.,o o.;xf

< O,ID

,, s. <o. 10

<' 0, I ()

< 0.10

< o. /()

<' o~ L D

J(p,

Q,g4 <.fJ,,o <o.tO

lq' <Ot~D

o. r,(,

<' 0./0

<' o. ,o <o.JtJ

< 0,10

Page 24: LAB S9::SOO

Arsenic .< o, oo:;'"

Selenium < D, I)O 5

pg/ml

pg/ml

pg/ml

ATOMIC ABSORPTION ANALYSES

Page 25: LAB S9::SOO

& REPO~T TO: Water Pollution Control Bureau ,.--· Environmental improvement Divisio~ 'Health~ Env. nment Department P. 0. Uox 968 - Crown Building

f. C E \ \J ED Santa Fe, r~i·b 87503 .._ , R · I1TTE,nroN: fJUJ/0 l~cl((f<

<) \j

"'-" r •• tJA1k~ 50\~i'Jf~STHJATER ANALYSES-ENERGY DEVELOPt~ENT I~ONITORING PROGRAM

GROUN9 w:::~\~~;{:::tion pjU tV} Pe-; < /77 ?t,<f: 51

Lat/Long

Station/Well Code

Collected

0 I II • 0 . I II T R s PS fYl Lv- 4fJ ~PDES No. --;- Outfall -No __ _ e4"D4~·7 J4SO By /?eJ;fCJjClrt'r~ d(./J {;(,{/ j/1( U

Date . ~~ Ntt"e · Unit

Pumpin~ Conditions ~~~-~~~~--· ~~~~~~~~~~~~~~~~~~~~ 'I :....t-t /Ct.i, 13\--:., c1:4<,'/Jii} pH (00400) /.7<' tYjJfll 1 \·iater Level o '--- · ~-------

Stc.ff Gage Height--------­Control Structure

Conductivity ~~.··. (Uncorrected) __ c_ <c_.(___/ ---~J..A_mho

-------------0 is charge ---+___,....-+~-·..:..,· =----

1-Jater Temp (00010) - °C

Conductivity at Samp 1 e Type _ _;;_{;)_P_J_/) ___ · • __ 250C (00094) -----~..wn;:._ h~

ti.ETAL Ar;AL YSES

~om NF, A-HN03 samp 1 e: A Da1 t.~-~-------E!~r11!, A-HN03 sam0J: A Da1 te d '\ na yzeu - .. _____ na yze

0 Arsenic, tot a 1 ---=-.ug/1 rX1 Arsenic, di sso 1 ved <.S. o,P..911 4/zc:, /r:v 0 Barium~ total _ug/1 tzl Bari urn, dissolved . ---,r.,Mg/1 _

1

_

1 _

D Cc.dmium, total ,~.~.g/1 ~Cadmium, dissolved ---r,.u911 0 Lead, tot a 1 ,,u.9/l ~ Lead, d i sso 1 ved ,.tr.9/l

C !·iolybdenum, tot p.g/1 !&' t~lolybdenum, diss ---r.p.g/1 OSelenium, total .!Ag/1 ~Selenium, diss < s. 0 p.g/1 '-lj;q J f4

' I I

Ouranium, total 0 Uranium, diss ----FJA91 1 Ovanadium, total 0 Vanadium, diss ---r.~-~.9/1 0Zinc~ total ,N· Zinc, dissolved ---lf-911 ---

. reAl) Ov, U~r&u

This form accomoanies sample(s) marked as follows to indicate field treatment (circle): _ _.___ ~___J{L_~-HE9~ \·lho1 e sample; aci di fi ed with 5 r,,l cone HN0/1

'::: __ ~Fil":ered sample (0.45rmembrane filter); acidified with cone HN03fl

5 ml

Page 26: LAB S9::SOO

~/ R':?ORT TO: ~·later Pollution C('lntrol Bureau LAB IW!·lBER /t/1~ /';XU E:wironmental T"11provement Division ' 1

- /

Health 1'.. Envi tment ucpartrent D.C\TE R.El. /ED ---1/- j/_:::_j t).' P. 0. bOX 968- Cro· .. m Building ....,/;z:;:. __

Santa F2, Ni·1bW503. t> D.;;.TE REPORTED -~5/Jr ~_:fi!/ __ .4TTEilTIOli: _(j_U) 0 LSVdC'~ . nitia1s

--- .. -~b_l;(sPJJ~i~Q_ - :f/50{) -. ·-·- .. ---i-!ATER OR i·JASTE\1ATER At\ALYSES-ENERGY DEVELOP!11ENT 1·10NITORING PROGRA~i

Sample Location

Lat/Long 0 11 ;

0 t: T R S

Station/Hell Code esm [,U- 4fJ NPDES No -~-- -- _Outfall -No __ _

Call ected 04-D4o7 !4-JD By {?o!i0(/c0a.<J'~fl (::2/-t./ /ji;A.:J Date , ?fne NWef7 Un 1 t 7

Pumping Conditions ~~~~~~·~~~~~~~~~~~~~~~~~~~~~~~~~ 't£-pM-'(;I·Iater Level /DB- 13(:f~ 9:4~ IY(Y/ pH (00400) _7~.-ZL_ __ _ Staff Gage Height

Control Structure

Discharge

Sample Type \ . '

Conductivity (Uncorrected) 8f?::::2 Pmho

~-!ater Temp (00010) -----~~~-°C Conductivity at

2 soc ( 00094) · ...v-mho

GENERAL \~P..TER CHEt·li STRY AND N I TROG Ei~ P.t~AL Y S ES ,.,_-__ _ / -r=-~ < ____ _

Fr~~~~_:am~~ An~~~~ed ------- ....--'

~c(~~~~l~bgs) ___ J-,mho ---

[] Tota1 mg/1 nonfilterable · residue (suspended)(OOS30)

From NF, A-H2so4 sample:

0 r~i tra te + ___ __;mg/1 nitrite, total (00630)

0 Amiilonia, ___ __;mg/1 total (00610)

0 Chemical ___ _:mg/1 oxyaen demand-- , ... ·· · -- ... '-( oo34o) i'

I >

t i '. 'J ~ ••

- 1 ''j

' . . '

.• 1 :;

- g. {L£<171_2£.i - An~~~~ed .-~from F, N"A sa_l!l2]_e; _ _) ~ i·\agnes-1Lm ( 00925 ) ____ mg/1

l:Zl Bicarbonate(00440) mg/1

12?1 Calcium (00915) mg/1

~Chloride (00940) mg/1

b4 Potassium (00935) mg/1 ___ _

~Sodium (00930) mg/1

sa·su1fate (00945) mg/1 (Sl'Total filter- mg/1

able residue ~ (dissllved~-0300) ~ ~&frncuf.p_

~;1::~;;2~~~: 3 . ~ '/ I j nitrite, dissolved

(00631)

0, 6 J. mg/l

-,· 1s-~

Page 27: LAB S9::SOO

\·IHer Ponut10n Contro1 Bureau LJ..\d hU!·l!.H:.k /..t...4J _ j £)t1d E:w iron menta 1 Irn'"~rovemen t Division "' ' 7 J

Health~ Envirt.. -:nt iJ~partrent D.A.TE RECE. ,~D -!/441/£-P. 0. dox 963 - Cro~·m 13ui lding ,. Lu ·-~--L-. .1-Sant~ Fe, NH~ W503. b ,() DATE P.EPORTED _{('.fl!..!__.::_ :_~_::_~ ATTEiH!Ol~: _uJYU) fd. ~Vd'C'r--- -_ ._ Initials

-· --. ~b_k_~_~c0z_. :f150D -··---·· ... r!ATER QR HASTEHATER ANALYSES-ENERGY DEVELOPI"ENT 1·10NITORING PROGRAt·1

Sample Location

Lat/Long 0 11 ;

0 ll T R S ___ _

Station/Hell Code esm Lv- 4ft NPDES No -----:--:- -- . Outfall No --,--

Collected I?A:o4o7 J4JD By {?o'::IB_/c~as§-17 0U.J /,1/uJ Date , }ifne Nlf.le'l Un 1 t 1

Pumping Conditions ~~~~~~·~~~~~~~---------~~-----~ ~pr/{bJiater Level /OB, 13(Y ?:4~ 19(1 Staff Gage Height

Control Structure

Discharge

Sample Type ' ..

pH ( 00400) _7~--Z~---Conductivity

(Uncorrected) ..

Pmho

~-later Temp (00010) _______ °C

Conductivity at · 2soc (00094) · ;~Amho

GENERAL WATER CHEHIS1RY AND NITROGEI1 At~ALYSES

~~~~~--------A-n~-~-~-~e-d--------~F---~~Q~~-:I?.~r=~-~A--~~~am~~-1-e~-;----o-.~b-b----~--An~~~~ed - ~ 1·\agnesiur.l (00925) __ o<_"/_,_,)_ mg/1 _;-j~; ·

,)2( CondHct i vity ,.u.mho ¢ (250~(00095) _ ------0 Total mg/l __ _

nonfilterable residue (suspended)(00530)

From.NF, A-H2so4 sample:

0 Hitrqte + ____ mg/1 __ _ nitrite, total (00630}

0 " . /1 ,...mmon1a, _____ mg __ _ total (00610)

0 Chemical oxygen demand (00340)

t;Zt 8icarbonate(00440) /8':2// mg/1 £//6 ;

I2J. Ca 1 c i urn ( 00915 ) _ _:_c;.,;_/_;;,. f!_', _mg/ 1 ~;-; ; '

~ Chloride (00940) 9:1.9 mg/1 · 1 t/2z {;4 Potassium (00935) iV. c1 [){'Sod i urn ( 00930) qq.3 f;LY Sulfate ( 00945) ('15/, 5 [Sf' Tot a 1 fi 1 ter- 6'/f..

able residue . 1 ~ (diss~:~300)___f:___ -"'------~---'-------- - -----. -.. --

c:E[Qm _·y·, ___ A-H~:

j

mg!l qk mg/1 __ r..,..'-mg/1 5~ /J.. mg/1 5 j;..~

~!litrate + --,-----mg/1 __ _ nitrite, dissolved ~00631)

____ mg/1

This form accompanies ~ sample(s) marked as fol1o1·1s to indicate field treatment:

..-JJF: \o/hole sample (no filtration) ~) 1\o acid added ~'\ i='-i1+cY"orl ~n -F4olri Hith n llt:; .. mPmhr2r.;> ;ilter

Page 28: LAB S9::SOO

REPORT TO: Environmental Improvement Division Health & Environment Department P.O. Box 968 - Crown Building Santa Fe, N~ Mex i o 8. 04-09p8 ATTENTION· D V J _ eK

LABORATORY -::::::;t:Lr-i5~P..--n (-6f-, tz-~-~-;;)_-

LAB NUMBERO!ftf- 1/fi' -1/f}Jl C,

BUREAU: SLD Users Code tlo. S'J b e;--0 ALL CONTAINERS WHICH THIS FORM ACCOMPANIES ARE COLLECTIVELY REFERRED TO AS "SAMPLE".

CERTIFICATE OF FIELD PERSONNEL Sample Type: Hater.ta' Soi 1 Other

--~~~----~------------------~,~ .Pt5

City & County ___ ~~..Q._-~""'-:1--~r-1-~------~-:-------t~-----------1 Co 11 ec t~d (date & time ) By ( name) -~---H~.f----=--'--..:::....~------t pH= ; Conductivity= °C;

Dissolved Oxygen= mg/1; Alkalinity= Sampling Location, Methods & Remarks (i .e.-o-d.,....o-rs_e_,..t-c ........ )----

. ~ Vl ~ ~ <;ft~ hllJ1'\ \;v 1?«---~ f\ Flow Rate= -----1

I certify that the statements in this block a analyses, observati0ns and activities. ~igned I c e rt i fy that I w i tnes sed these f i e 1 d ana 1 y ~rH--r-'9'-''+."':'*'""~--r~"71+..::...:-:--:-i -es--a-nd-:--c-o-nc-u with the statements in this block. Signe~_;.t.:lf..:;:.~b,...~~=-======-

Method of Shipment to Laboratory__J[2.;~~~~~'-+~3.-.-.----""'7"0----:~-=--.--:r------­THIS FORM ACC MPANIES .3 septum viils with eflon-lined)discs identified as: specimen ; duPTicate _ ; triplicate _ ; blank(s) and am erg ass jug(s) with te lon-lined cap(s) identified as -----and other container(s) (describe) identified 1s Containers are marked as follows to indicate preservation (circle): -------

No preservation; sample stored at room temperature ~20°C). Sample stored in an ice bath. Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

and that the statements in this block are correct. MAY141984 .Seal(s)Intact: YesO NoD

BUREAU

Page 29: LAB S9::SOO

~----,··· "--· , ....... ',~_,_ •... ··-fl\ ;1 r·' "•lf" ,~L

' ! ' : ~ eRG~ c-f92 il'•H l- I "-"'~ ""' i ... . ,. L ...... I ,

! :: . ..: I·: u / ·----· ----'~-· .. ··~· --~,··----PLEASE CHECK THE APPROPRIATE BOXES BELO\~ TO INDlU\l'E THE TYPE OF ANALYTICAL SCREENS REQUIRED.

l~ENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED. I

~ ~ p. ~ ~ EXTRACT ABLES H

PURGERBLE''· H

E H ~ H

~ E-1 ~ H E-1 H E-1

~ ~ SCREEN ~ ~ SCREEN., g _g ::::> 0'

ALIPHATIC HYDROCARBON SCREEN ALIPl~TIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

IX GAS CHROMATOGRAPH/l-1ASS SPECTROHETER HYDROCARBON FUEL SCREEN ORGANOPHOSPHATE PESTICIDES -POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROHATIC HYDROCARBONS

SPECIF.IC COMPOUNDS SPE:CI F"I C COMPOUNDS' ..

Rm1ARKS:

· ANAL.YT I CAL RESULTS COMPOUND

CONC- CONC-ENTRATION COMPOUND ENTRATION

. -

* DETECTION LIMIT /,~/~ REllARKS: tJo p ~PA f1...f...... {Jl;i;..;d /{/

u

~ CETRIFICATE OF u~ICAL PERSONNEL . Seal(s) Intact:~ No . Seal(s) Broken by , ,---- date f/J_~~ . I certify that lowed standard laboratory pn(.s:fedures on handling and analysis 'of this sample unless otherwise noted and that the statements in this block and the analytical data on this page accurately reflect the analytical results for th(~s~~~. Date(s) of analysis t};/L..) {jt/ . Analysts signature ~ A- rtA.--!certify that I have reviewed and concur with the analytical( esultsz this sample and with the stateiiP.ntR in this block. Reviewers Signature :-I ! A •• •

... " - . . ... ' r;l ~?~ 1",- -

Page 30: LAB S9::SOO

.· !CAP ·SCREEN

Lab Number : __ /L..1~..L.!..M..:__J.f..J...' -=-2-=-t;--~-Date Submitted: </-.(, /~Lf

----~~~-~-,...........:.-

By :_-+J3~c).:..,fr.et':.....~...-______ _

sample code : __ ..~....P_.::S:~M..!:..!......:.~.:!:L_-----=-3 __ _

Date Reported: b /; CJ /£-'Lf

1--~~+-~-~-,~~-------

By: _ _:....m~. ______ _

Detennination Concentration (lJg/ml)

Aluminum ..(0,~0

Barium <o, ;CJ

Beryllium <o,,o

Boron o.n Cadmium <.o./D

Calcium /;(,J,

Chromium <(C;.tO

Cobalt < CJ, I t:J

Copper ~O.tO

Iron < {), ;0

Lead <o.,tJ Magnesium 1?.-Manganese < CJ,10

Molybdenum ..(_ 0 I tO

Nickel ..( 0, tO

Silicon 3s:.-Silver <..o,o Strontium D.~~-

Tin -<({),tO

Vanadium <o,tO

Yttrium < CJ,tO

Zinc <o,,o

Page 31: LAB S9::SOO

·.

ATOMIC ABSORPTION ANALYSES

Arsenic <_ (). C.i C> S:_... pg/ml

I ,.--

Selenium < 0 . 0 0 ~ pg/ml

Mercury / c:··-< p. c) 66::. pg/ml

Page 32: LAB S9::SOO

oc"o'or'

< REPO~T TO: Water Pollution Control Bureau Environmenta' ·~provement Divisic~ Health~ Envr. ~nment Departm~nt

r-.r - '

'/ HECEIVED ' ..... ... P. 0. Uox 968 - Crown Building

n::: ):~:~ Sa~~a Fe, l~i·i 8~50~ ;.._., I\ T I t IH I ON : l:Jb) 0 i ~ Yli~(-PJ.:._/B_;:;_ ... --

iJ.fl. TE REPORTED _fj.J q /-l':L. _ _:_ \ ,.

,_, _, k () _ Initials ~L-8 -~~}e17 C-1?-;F<:? 55~ . -·- .. ~- -- - - -- ·- .. - ~ - -

HATER OR WASTHJATER ANALYSES-ENERGY DEVELOPHENT t~ONITORING PROGRAM

Samp 1 e Location P ~ /}1/tt) ·-- _?,

Lat/Long ___ 0 ____ •_• 0 II T R __ s ___ _ Station/Well Code------- NPDES Outfall No __ _

Co 11 ected E 4-o4: /! By -~.:..-...r--+----~~....-!.2..~.:-:1)~-:=::=~=------Date Unit

Pumping Conditions -~~~~~~· ~~-~~~~~~~~-------------\rtVlJft ~Jater Level

Staff Gage Height --------­

Control Structure --------­

Discharge ----:::----"-:--­Samp 1 e Type -~~'-"tu~o o..:..f!_:;;_T_ .. , __ ·' __

METAL ANALYSES

Date (:" Analyzed ·

From NF, A-HN03 sample:

[]Arsenic, total

[]Barium, total

[]Cadmium, total

----'-..0. g/ 1 --­__ .....c.:..u91l

--~..u g/1 ---[] Lead, tota 1

[] t·iolybdenum, tot

[]Selenium, total

Ouranium, total

----.~=.P.. g/ l ---__ ---J!p.g/1 --­

__ ---J.}Ag/1 ---

------+~g/1 ---[]vanadium, total ,ug/1 __ _

[]Zinc, total ,.u.g/1 __ _

v' pH ( 00400) _ _.....:7~-':..._7~---Conductivity ~

(Uncorrected) )(! b ).Amho

\·Ia ter Temp ( 00010) __ ,.::...._;t.....:.':....:L'::::....l _<_)<"'...::--=-_0c Conductivity at

2soc (00094) ------=-...v.rn_bc

from F, A=HNo3 sample:) .. ~··~~ ~--""" _______ ________

t8:J Arsenic, dissolved .1_ b. D ,o.g/1 f

Date Analyzed

IZ:J Bari urn, dissolved p.g/1 I

S)rJfsll-

~ Cadmium, dissolved --~i,~..g/1 __ _

[Sf Lead, dissolved ,.u.g/1 __ _

0. l'lolybdenum, diss

0. Selenium, di'ss

0 Uranium, diss

0 Vanadi urn, di ss

~Zinc, dissolved ----fJ. g/l ---

-----i,J.1.9/l ----

Remarks ~ · Q Lvc?rl ;.){)1/)1_.

,'i~L ( [!Jil&rni AA&1

·-;j;·(A f \c~ ed( <y?!(; !7) ,!1 > ;s:" ~""

t' f l; q:t{~tku~ TeA f' ~J,1£<-<J as follows to indicate field

& ·1/yff?~ * y Y' C2- 1\rx(cc~ru!!:~ This form accompanies J sample(s) marked treatment (circle):

, Nf:, A-H~: \·!hole sample; acidified with 5 r.1l cone HN0/1 \'-f, A-HNO~) Filtered sample (0.45)-"-membrc:ne filter); acidified \vith

----· cone HN0/1 5 ml

Page 33: LAB S9::SOO

<"' P.~ .... JRI IU: Fv11u.ii..;, _;,.'ll .. rui t:lureou Lr.:... n~·--l..." £:1v i ronment.a 1 lrnnrovement Division ·----He a 1 th ~ En~i rcq 2nt U2p~rtr,ent D.l\TE RECL, .. >D ?!l!.-.J/~f2.t2.~ IJ-//-f/-P. 0. dox 9oS- Cro~·m Bu1ld1ng CJ~~/,A/~ / Santa Fe, i·H·I 87503 _ DATE REPORTED ~:5/fJ/&tf Am:mo:l: ~v 1!;) l'oO'fl? __ SIL-t u~-~it~96&v

- . - .. . . _____________________ :__.....:.·.:.:....:·· ·;__;_· ...:..· _:_____:__.:....;..;__:.._;_;....:.:.;;_--=- - ·-·- ... ······-

r!ATER OR HAS TEHATER ANALYSES-ENERGY DEVELOPNENT 1·10NITOR1NG PROGRAI•l

sample Location ll-'21 :G?'71 ~1:&_~;'1 PNIY' ft1f! 7\ 11)-t'Pf-11,-:;') /c-e; f(/ [f)- j;

Lat/Long

Station/Well Code

Collected

0 I II • 0 ll T R s -------~j~~---' --------- -------

')Y f 4trV NPDES No . ... . Out fa 11 No

f?4-otr/~ sy R&:-2_ hw { --oate Time Nar.i'e II Unit

JSM ~&Q C&4Y'f 1212 u:m& Pumping Conditions

~-w1'h11 \·:ater Level

Staff Gage Height

Control Structure

Discharge

Sample Type

. pH ( 00400) __ 7.;._;.~~7 __ _ Conductivity ~

( Un cor re c ted ) ___;J:...:../:...:..J__;_(_; ___ P._mho ·

~-later Temp (00010) ;;5 c °C

Conductivity at 2soc (00094) · P-mho

GENERAL WATER CHEHISTRY AND NITROGEit At~ALYSES ~~~-------------------------------------~--~-----C~J----~------------oate

Date - '""~ ' rAArl..- -~~ d From N , Frol'!l__F, NA _sRmpl e: --......, - 1"\na ,yze Analyzed ~ 7-

~~}'lagnesium (00925) ______ mg/1 0 Cond~ctivity ___ __:.:)J .. mho ___ _ ~ (25 ~~0095) 0 Total , ______ mg/1 __ _

non fil terab 1 e residue (suspended)(00530)

From.NF, A-H2so4

sample:

0 l~i tra te + ---~mg/1 · nitrite, total

(00630)

0 AmiiiOnia, ___ ......;mg/1 total (006lb)

0 Chemical -., . ,1 .. ~r~~ .. JU9~1 ____ _

oxygen~~~'~D ;~~ 1 r \v·) ~~" :: D

g£ 8icarbonate(00440) ____ mg/1

@.Calcium (00915) mg/1

:g) Chloride (00940) mg/1 __ _

_0 Potassium (00935) mg!l _____ ____; ---[S;J"Sodi urn (00930) mg/1 54 Sulfate (00945) mg/1 ---

Q Tota 1 fi 1 ter- mg/1 able residue

1<)( (disso;red)(7.030jD ~~~--&-t(yt~---ce/ --­

Froi]l_x_,_ A-H 2S~pl e:

C)r_!litrate + 2.'ll/ mg/1 t/.t'? nitrite, dissolved ' (00631) { 00340}',' · ..... ,1. ' ..... J'.c. · ~-• ·: .\. .. , .. i -"--1 .. ,_' :!

~'· ~ / I: I ~)

!\\I :·"''.'1°\084 li\\l rvr11 . / t.\q ' · 1 ~- \) .) · · 11,0 ~" t"J"Thllom a, dis-: 0. ;2. 3 mg!l s~--- :l

.J.\.•-~--··-··· .. ., ......... -,..·--~---A· s~v~ (0~08) f2 ~J; ' i c .. ~jjh~: \ ·::··: .~;.·~;r.·;:,e:_~;.~1Uli~ VJ0.SlE ~ f .. 1 ~ ~ ~ ~ t3

-~.: ;;~ / \.}>\o-e:~/d/~J::=uu ~ ~ '-rhis form accompanies d-s..ample(s) marked as follO\':S to indicate field treatment:

A_:· \·Jhole sample (no filtration) G'! l~o acid added ~ r:,+ored in field with 0.45~membrene'filter

Page 34: LAB S9::SOO

~ R~?ORT TO: Water Pollution CQntrol Bureau E:1vironmental 1 "1'1provement Division Health ~ Envi 1ment D2partrent P. 0. dox 968 - Crown Building Santa Fe, i·lt·l 87 503 .4TTEiiTIO:i: _1:)5) I) I~-~ \-!l~CDR-,_)­

\ _____________________ :..__.:....._~...:._:~.:.__....:.._:_:_:__:...._:__._;_;_:____.:;- - ---- -- .... -

i-iATER OR \-JASTE\~ATER AN.4LYSES-ENERGY DEVELOPi·iENT 1•10NITORJNG PROGRAI•i

Sample Location

Lat/Long

Station/Well Code

Collected

Pumping Conditions ---i/; ·\::1 ~l (/f'l \1 \·:ate r Lev e 1

Staff Gage Height

Control Structure

Discharge

Sample Type

Conductivity ) (Uncorrected) /// ( ..,Umho

~-later Temp (00010) _.J.-.;;;<;.... . .;,..~2<;....-_'--_;;_-L:;_~ ___ - °C

Conductivity at 2soc (00094) · ,.o..mho

GENER4L WATER CHHiiSTRY AND NITROGEi~ ANALYSES

\ (';\ oat~ ( '~ ,,12., <(hHr~-cJ1._J o*g).._ lf/f~~te d From NF;~ sample: rom.F, NA sp.mple: ------....: ___ ....-'--1-fr.na 1yze

Analyzed i·:a9"nesf[m (00925) /2 .. L: mg/1 c;/ · 0 Conductivity )...t • .rnho fV! 1 · !>. - -\5l (2So,C~ooogs) ________ LJ. Bicarbonate(00440) /oeo-0 mg/1 /f/!7 QTotaly mg/1 .tzlcalcium (00915) /.:i·'-.(mg/1 :~/

nonfilterable gJ Chloride (00940) 7/,;;._ mg/1 4/J..l residue (suspended) (00530) • fZl Po tass; urn ( 009 35) '

From NF, A-H2so4 sample:

0 l~i tra te + ___ __:mg/1 nitrite, total (00630)

0 Amii>On i a, ___ __:mg/1 total (00610)

0 Chemical oxygen demand (00340)

--=---(J,'J.'-' mg/1

(52J .. Sodium ( 00930) 54 Sulfate (00945 )---'--=.....--

q;;, I D mg/l :lo7~ I mg/1

Q Tot a 1 filter- 61'3 mg/1 able residue

~-(t;~~:e~~~~{ From F, A-H 2

so4 sa.mpl e: ___ __)-

0 __. ... ;--

mg/l [51' 1litrate + ----nitrite, dissolved (00631)

' ' ,,

~( "Z.-> I I (

5/1 I

5[' 5" j

t:J; 7 ,,j , ____ ----f

This form accompanies ~)~ample(s) marked as follows to indicate field treatment:

~: 1-iho 1 e sampl_e. (no fiHrat.i_on) . (~\. i~o acid added • ,. F 11 t ere d 1 r n e l d vn t h (i, Li::: u rr.em) r:;;: e i 1l 1.. e r

f; tY ('" n'' • r, -. ..: ...: .: .: ..: ,..,. ..J \.I .:: .0.. h ') m j / r r\ t"'\ ,... w c: r, / l

Page 35: LAB S9::SOO

·_ c 84- 0504 -D

REPORT TO: Environmental Improvement Division Health & Environment Department P.O. Box 968 - Crown Building Santa Fe, Ne M xico 87 4-0 68

LABORATORY_--r--1";-----r--­

LAB NUMBERj) th 9 :2 ATTENTION: } J £)t_ /1

BUREAU: _ ~k SLD Users Code tJo., rJlJ/-zVTJ

Sample Type: ~Jater )21 Water Supply and/or Code No.~~~~~~~~~~~~~~~~~~~~~~~~ City & County L_

----~=-~~~~~~~~~~~~----~---------------------1 Co 11 ec ted (date & t i me)--~-~~~.:___,___.._::::_-=--pH= 7/7 ; Conductivity=

--<-4.-1.-"-"-

Dissolved Oxygen= mg/1; Alkalinity= ; Flow Rate= Sampling Location, Methods & Remarks (i.e. odors etc.) . . 1J . /) /}------~--i pfi)J11. ~07&-~ ~vth-7 IY/!hJ. ltkee -If,$ bj)&(_~]? ~-?~/d.~ d-~/ ~ ;xd.G--( 1\t'o ~£.e/ I certify that the statements in this block a curately.r s of my field analyses, observaticins and activities. Signed I certify that I w i tn es sed these f i e 1 d ana lys-e-s~, ::-JJ.-bUs e;...<r....::v;...J.,a.,_t ..,....i o+-n""'-s~~~~....,...,....,~:-e-s_a_n_d.--c o_n_c_u with the statements in this block. Signed Method of Shipment to La bora tory t~c.t~"'~--d......,~,.---.,0::;;:::;n,.-· ----c..-.---­THIS FORM ACCOMPANIES~ septum vials with tefl~cs identified as: specimen J ; duplicate ) ; triplicate L ; blank(s) and ambervglass jug(s) with teflon-lined cap(s) identified as -----and other container(s) (describe) identified as Containers are marked as follows to indicate preservation (circle): ~-----No preservation; sample stored at room temperature (-20°C). Sample stored in an ice bath.

Sample preserved with 3 mg Na 2o3s2/40 ml and stored at room temperature.

CERTIFICATE($) OF SAI~PLE RECEIPT I (we) certify that this sample was transferred from to -----------------1---------------- at ( 1 ocat ion) _______________ ~~~- on (date & time) ________ and that the statements in this block are correct. Disposition of Sample . Seal (s) Intact: Yes 0 No 0 Signature{s)

----------~--------

I (we) certify that this sample was transferred from to ~------~~--------1------------- at (location) ___ ..:...:cR_E_C_E_I V_E_D _______ on

(date & time) and that the statements in this block are correct. --------Disposition of Sample Seal (sJv1g_ftft2&~SUvres 0 No 0 Signature(s)

Page 36: LAB S9::SOO

ANALYSES REQUl fED LAB. NC~) ~o4 PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. 'VHENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED. CJ'; ,

'11 ~~, ~

r:tl g; :> r:tl g; EXTRACT ABLES H :>

PURGERBLE'', H

~ H E--1 H

~ < t1 E--1 E--1 H E--1 H E--1

~ ~ SCREEN ~ ~ SCREEN' ::::::> 0' 0' 0' 0'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

IX GAS CHROMATOGRAPH/HASS SPECTROMETER HYDROCARBON FUEL SCREEN ..; ORGANOPHOSPHATE PESTICIDES

POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS

SPECIFIC COMPOUNDS SPE'CiriC COMPOUNDs···

REMARKS:

ANALYTICAL RESULTS CONC-

COMPOUND CONC-

COMPOUND ENTRATION ENTRATION

/, 1- .l.0:1tw...cxJ.e,y...;z__ ::; tO A1 &

t.!.J-0~~"~L-~ 79o:::Jl -r_;t~~-Ovv.·-12 -

/0 i-

J 5' () t.d./1

CGhrc• ~cr""" (,'/Cf /)( /./--<1 .

./(/

* DETECTION LIMIT __s:,/-d /J! REH.ARKS: 1)~1 17~-..Ll--<. .J/~<L A--&.: d;;.l. --~

I i./

., CETRIFICATE OF ANAAYTICAL PERSONNEL Seal (s) Intact:~~) No . Seal (s) Broken by rlJ_ -11 date i/>o)ftf·; 5,/, );;?'t' . I certify that allowed standard laboratory p edures on handling and analysis of this sample unless otherwise noted and that the statements in this block and the analytical data on this page accurately reflect the analytical results for thilJ. samp+el J Date(s) of analysis lf-!]e/r,- 't · '//; -,;j· i . Analysts signature ':c,-\J/_,.:,_L,hJ!.:-vr/ !certify that I have revie&ed and concur with the analytical rjults c.r!jtis sample and with the statellP.nr~ in this block. Reviewers Signature: .fm , l

.e.;;-e L- ~ ~

Page 37: LAB S9::SOO

• • ICAP ·SCREEN

Lab Number: /-J fY1 ~~4 --~~~~~--------

Date Submitted: 4 /u / tf; r , By: ----------------------

Determination

Aluminum

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead

Magnesium

Manganese

Molybdenum

Nickel

Silicon

Silver

Strontium

Tin

Vanadium

Yttrium

Zinc

Sample Code :. ___ (J~'S...:.M...:....:.IAJ_~__;_:;:(.::..__ __ _

Date Reported: __ · _G+j_t_q-J/t...-.:..'f'fL------­

By: mi

Concentration (JJg/ml)

<.o ,o <o ,o

s.·o~,o

0.~(

.(o,tD

13~. <o.t o <o.tD

:S (). 10

<Q 1 1CJ

<O. I() d..fJ. 0./0

<{).!0 <.D tO

2-l <D. I 0

o .. <6..Z, ~o, ,o ~ 0,1 D <o,,z, < IJ. tD

Page 38: LAB S9::SOO

Arsenic <. D I ooC: pg/ml

Selenium 0 , 0 Ob pg/ml

Mercury z Q, DOD~- pg/ml

ATOMIC ABSORPTION ANALYSES

.. .. :

Page 39: LAB S9::SOO

f -

\·!a ter Po 11 uti on Contra 1 Bureau LAB 1\UllBER 1/ frj ~-,:_'> t/-Environmenta, ·'1lprovement Divisic:1 --- ·-;-;;-;·~-Health .r: Env1. .... nment Department 0/\TE R'~vc::IVED .L/ji[L!?:!:__ P. 0. L\ox 968- Crown Building --- ---·-Sa~~a Fe, l~i·l~ 7~03/. ,1 _"_ Q.L\TE REPORTED __ fo}!_J_L!_y_~_:_

~ REPO~H TO:

, .

I1T 1 t1HION: 0 U l :t l\rX-r-- . . ; l ~- -£ Ini,t_ia1s n ',: '}, '-:~'_-,-; - - - -.. -- ---- ___ _:_J __ :_) L~~~'>J t'-8 -- -~ .. 57. PO--<)

......,, ,·

(l:ROUND WkL::.rJUn.Ettu:Ofti\'fJASTHJATER ANALYSES-ENERGY DEVELOPt~ENT t~ONITORING PROGRAM

) Sa mp 1 e L o cat i on --4ol~~---~-.l...llooo"""'-"'"""""""'-~--"-'~--l..--J!-4..1-:..o..:::....:........,.~"'""--f-4'--'-~~"f:::-_..s;:;=--

Lat/Long ___ 0 ____ •_• ; 0 u T R S -- ----Station/Well Code NPDES No. Outfall No ---

Co 11 ected S1- e4- li C~;!JV By /2?Jvff2) / . I) s:: Date ' Time Nameh _., {:::>

1

'iini t

Pumping Conditions-~} __ --=~~?~-/--~~~-l~~=/~~~~-~~~·-~~-~-~-~-,-~_-~_7_,_~~~-------ty7tf1Jt\·later Level ) DB, 4 72 y(/)t)y fr,»l.,d-/f.X; 'f pH (00400) _.;._7_, -1-----

Staff Gage Height --------- ' Conductivity (Uncorrected) )ZJd--() J.Amho

Control Structure ---------vlater Temp (00010) c)<"f: °C

Discharge ------:---..!..:---- -'""""'-~-----/ n Conductivity at

Samp 1 e Type -"":-"'; 9~,'-""IM= .. 7"""t)&--=""""' "'----- 2 5 oc ( 00094) ,v.mho. ______ _..:.__

METAL ANALYSES

___ __;;_..0. g/ 1

__ -4.).1 g I 1

From NF, A-HN03 sample:

[]Arsenic, total

0Barium, tota1

Date Analyzed

[] Cadmi urn, tota 1

[] Lead, tot a 1

[] 1-iolybdenum, tot

[] Se 1 en i urn, tota 1

[]Uranium, total

Ovanadium, total

0Zinc, total

-----&:.0. gj 1 ---

--__c • .u.g/1 ---__ ___,c;P. g/l

---J'.&A91 1 ___ ...,.g/1

__ --J;.ug/ 1

__ ....,cM-9/l

Date Analyzed Fr~_~)ample:

[ll Arsenic, dissolved

rc;;lsarium, dissolved

<~.{) ,,ug/1 9tt IR'f

__ __,.,,u.g/1 ----!E---Cadmium, dissolved ----,ci·,~ .. g/1 (B:."Lead, dissolved ,.ug/1

(Ci)lo1ybdenum, diss

~-Selenium, diss

0 Uranium, diss

0 Vanadium, di ss

~_Zinc, dissolved

-----r:,J.J-91 1 p..g/1 .

---r,IA9fl

----r=J-L g/l ---t-f-g/1

'9'' lt<t I

Remarks Lu_ J ·-yfA ... 1'J/I! --~~~--~~~~~~------~~~~~~~-~~----------

~ C]VL:f:rY/AA1.JA/V-r1

' t.. Mn JY1ie11J>/~/J This form accompanies sample(s) marked as follows to indicate field

---!--treatment (circle): ~~N~:. \·J~ole sample; acidified \'l'i~h 5 r.1l _cone HND3~l. . .

. ____ r, A-HN03: 'f1ltere.?, sample (0.45ymemorc.ne f1lter); ac1d1f1ed \'nth _________ .-tone H1~D/l

5 m1

Page 40: LAB S9::SOO

<· P.~PORT TO: ~·later Poliu-.1011 ~,...c1ntrol 1::\ureau E:l'tironmental Ir::::-~"'ovement Division ----------Health u Envi.ro•", ~nt ucpartrent DATE RECE. , vD ,U~j~f{ ~ fr[--jj ;L-p. 0. ~ox 968 - Cro~·m I3ui lding y-- <I ~ /

.SATanTEta.~lTFieQ,•'•.·N_H "'\87As~;l \ J? 0 !JATE PlPORTED ____ &~~-' u _ v _ 1~ ~ 0 lj F 1\.- . ('L l ,._ r:1 [) In 1 t 1a 1 s

\1 - .. · 2>1 J Cf)~-J ~ .5'<)6t;-1) - . - .. . . __:. ___________ ....;._ ______ .;___.:.____;:·...::.:.···:._· .;_-....:...· ....;.·_:._:_;_;____;_.:..;,:...;.:..:.___:-·- ·--- .. ··-···-

'r!ATER OR \·JAS TEHATER ANALYSES-ENERGY DEVELOPHEIH 1•10NITORING PROGRAf.l

Sample Location 2(k):S$n <0/A.{/ffn fJV!Yl /+1r;77 IVe£.£ P$MtJ -~

Lat/Long

Station/Well Code

Collected

II • 0 1: T ------------' ------------0 R __ s ___ _ ------ NPDES No...,---...:....___ . Outfall No __ _

£¥ff14_1/ 0c1 Pf?? By -·-+.17..;.J.;;O~l..f(c;._/+}-----:-:--~---Date Time Name 7 Unit

Pumping Conditions 0 · a-1?- c , -~/to ftt.f7l.e4/ ~~\·:ater Level lD840 Y!l&rr~fip CJ,;:::/p~fx:? pH (00400) _/.:::_J _I __ _

Staff Gage Height . -------- Conductivity · · ( Uncorrected) ---+1-loD..;;..V-~D..;;..__P.__,mho ·

Control Structure • -I ( ) d:±:: . oc ~·.ater Temp 00010 __ __.;;:2~---Di scharge ~. / b .. Conductivity at

Sample Type (ryf(& 25oc (00094) _ ,u.mho

GENERAL \~ATER CHHi!STRY AND NITROGE11 At~ALYSES -~~~=-------------------------------~~~~~~----~---------oate

Date ~~-\ ~u , Analyzed CFrom F, NA saf\)ple: Analyzed

d ~agnes-'ittr.Y' ( 00925 ) ____ mg/1 ~Conductivity .-(..r • .mho ___ ~ .. ~ (25°C~00095) --~ r:A.,Bicarbonate(00440) mg/1 0 Tota~ mg/1 ____ ~Calcium (00915) mg/1 __ _

nonfilterable · JlJ.Chloride . (00940) mg/1. __ _ residue (suspended)(OOS30) rn· lL:J. Potassium (00935) mg/1 ___ _

From

From NF, A-H2so

4 sample: lD. Sodi urn (00930) mg/1 __ _

tzJ Sulfate (00945) mg/l __ _ 0 l~i tra te + mg/1 __ _

nitrite, total (00630)

0 Amii10nia, mg/1 __ _ total (00610)

.QTota 1 fi 1 ter- mg/1 .J able residue ---

-a ($1fs!olved)(7~) ~~u-,4wrvdJ.~

Fro ~ample:

~ ..... , ' ';!J>k2 .} ;: '

This form accompafrl:·¥~ d--- sample(s) mat~ke:d as foll01·:s to indicate field treatment: . '?c

~F:· l·ihole sample (no· filtration) .... ( ::.~~~ l~o acid added (~:~ ~·'.:.ro,...orl .;.., -F.;olfi I·Jith n llt;" mPmhr~filtPr

Page 41: LAB S9::SOO

>•

/ R~?ORT TO: Water Pollution CQntrol Bureau E:-wironmental 1 "1'1provement Division Hea 1 th ~ En vi.. ment ucpartrent P. 0. dox 968 - Crown Building Santa Fe. NM 87503 .C. TTEiH I Ol~: _\:d_A ·J ) }-~ J? 0 '-1 f' fZ_

\I

-------------'------------~..:...,__;;~,;,_~:....:...:._-;_,:__:~___.,-.- ---- -· .... -

'r!ATER OR \·JAS TE\~ATER ANALYSES-ENERGY DEVELOPII•EIH t··10NITORING PROGRA~l

Sample Location

Lat/Long Station/Well Code

Co 11 ected

0 II n T ------0 R __ s ___ _

NPDES No Outfall No ---~ ----

8Lft/4. I { ocl '!lh By -~t.,.,..?I..La..:....jLf-FI_.,../}:__ ___ -:-:-...,.....,..----Date Time Name / Unit

Pumping Conditions ·-~k~.lzi/ ·t 4.1·]) (df.J~l/1~1-1 j)(JCt77l.r2f~ -~~y~rt.;~-:ater Level J[ti:40C:a,~r;gc)''t>~(c/ pH (00400) _/-=----; ___ _

Staff Gage Height . -------- Conductivity Control Structure (Uncorrected)

'' Discharge

Sampie Type

Water Temp (00010)

Conductivity at 25oc (00094) ~-Amho

GENERAL I~ATER CHEt·HSTRY AND NITROGEr~ M-JALYSES ~~~c~------------------------~~~-~~----~---------Date

' . . . Da t e _ _______.:: -::-~-~~ ~ \ l t.k01/..JJ62. C'J.. Lf '1 A From·'( '. iiA sam~~_:) Analyzed t fi om F, NA sample: nalyzed

- .agn-~ (00925) /c? . .5 mg/1 _-<;//t ·fZ1 Cond~ct i vity ,umho ·35:\ ... (25J,ll00095) ___ ~--------=------------ 54 Bicarbonate(00440) mg/1 0 Tota i'" mg/1 ___ f)1_ Ca 1 ci um (00915 )___,:...;.....:.....;__,;.__ I /7,6 mg/1

nonfiiterable ~EJ.Chloride (00940) _ _._,_.L.L..j.._ residue (suspended) (00530) '0, Potass i urn (00935 )

K4.f mg/1

From NF, A-H2so

4 sample:

0 r~itrate + _____ mg/1 ---nitrite, total (00630)

Ur-, r,,_.Onl·a ____ mg/1 1"'\i\ ll; I I '

total (00610)

-~~___; f{, s"'&' mg/l

Q. Sodi urn (00930) f;] Sulfate (00945 )-~1----

10 l/ mg/1 ·,l7j.O mg/1

Q Tot a 1 filter--· able residue ~ ~ts,!ol/ed)(7~300) - ,.,---~UJ.v,i'f'!l//;C;_

From.J , _ _A-H2-SO~.samp1 e:

75(, mg/1

a. -~--~

)/,.

+/d-.7 S"/-z_ I <)

s-/J_ I

5/;;z.r; i

-l.,.-7 '-.v/ I <..-

1'0( :~it rate + mg/1 ~-· ------- -------0 Chemica 1 ---+lrt+-.D~-:t-~m~-~)~'(\.7f/)-f~ic_;m:l_

oxygen demand ·, n ·;.---..l..l.-.. .. 2t.--U.. .... t. .. ,l __ _, I l I' li !• · '· .. l I .

(00340) li'L: ,., \\. _JUN 5 1984 ijlJI L --- l._0

GROUND \H';T[~,IHAZA~ilOUS WASE BoflEAJ

nitrite, dissolved (00631)

~\ '-'· form accomnanies ~ sample(s) ma1·ked as follows to indicate field treatment:

' ·> ''C' II' 1 1 ( . .C"l"- , ) ,,/\\ f' . •' dd d (!-:."\:~-'·,no e ~a~p :. n? 1.1 .... ratl~on , '""''"-:!~· ~o e:c1a a e

~;·.-::._.t.JJ. terec : n: _ T: e l C \:1: th,.. 0. 4 :J)J- fT:e::-:orc ~ i'rlL.er r·· 'C""n~. '·- .. - ... .r: ... ~ . ..J ,, .. -\..., .. r-ni ,..,...,,....,,_urn/'"\

Page 42: LAB S9::SOO

84- 0503 -O

REPORT TO: Environmental Improvement Division Health & Environment Department P.O. Box 968 - Crown Building Santa Fe, N w Mexic 8 04-09~8

LABORATORY ~ L cb -p-:n""""=;;;;;::;t~---v....,.~/-~---

LAB NUMBER (

ATTENTION: - . . , \ PJ< /)· BUREAU: ~J.t?. SLD Users Code tJo. ,5"C), tJ0

CERTIFICATE OF FIEU; PERSONNEL Sample Type: ~Jater .12{ Soil c;l., Other _

Water Supply and/ or Code No. fu f.--PZj f-74_--;:t:;:::{,.dz:> L.L-JLiLL~r__..L..-).-LJJ_+-JL.JI..:::._---S:~...../i._---1 City & County fJL/lJ..4~~ /(x!zfl ~ Collected (date & time) ~Sib By (name) /i2cr;.b:(J · pH= 2/; Conductivity= !0:;)4-Umho/cm at ;)Z'"f= °C; ChloMnfResidual=

Dissolved Oxygen= mg/1; Alkalinity= _ · ; Flow Rate=-------1 Samplin~ Location, Methods & Remar;ks (i.e. odors etc.) , ·A --h' n

r/J//YJ tf)/7::~ g:r~~ m~ ~AJe£/ ;!;;_ J ~_)~A ~ ~ c~1 ;;r-g{'lqnoA jJ-uel£,.1 ;lz; &h?

I certify that the statements in this block a cu at~·ly ref reJqt he;_,results 01 my field analyses, observatiC.ns and activities. Signed · .. - /r/ /<: '-- --1 certify that I witnessed the:>e field analyse , obs(~rvat1o s a Cl ac · and concu with the statements in this bl)ck. Signed Met hod of Shipment toJ;bo ra to "'Y /)

041 0..,..._ .---,r'e--,--:t____,C..-.1¢!--7--++---

THIS FORM ACCOMPANIES septum vihls witlrteflon-line iscs identified as: specimen 1 ; up icate 1 ; triplicate I ; blank(s) and amber glass jug(s) with teflon-lined cap(s) 'identified as

~,-----

and other container(s) (describe) identified as Containers are marked as follows to indicate preservation (circle): --·----

---'-<.. No preservation; sample stored at room temperature (-20°C). -ICE: Sample stored in an ice bath.

P-Na2o3s2: Sample preserved 1rith 3 mg Na2o3s2/40 ml and stored at room temperature.

CER'"IFICATE(S) OF SAI~PLE R1:CEIPT I (we) certify that this samplr was transferred from ------------to •------------·-- at (location) ______________ on (date & time)_______ and that the stateme1ts in this block are correct. Disposition of Sample ____________ . Sea! (s) Intact: Yes 0 No 0 Signature(s) ___________ _

I (we) certify that this sample was transferred from to --•------------ at (location) RECEIVED __ on

(date & time)_______ and that the statemen·:s in this block are correct.

Disposition of Sample ____________ . Sea· (~f1P:f~~dS84Yes 0 !lo 0 Signature(s)

- GROUNIJ-WAllRlliAZARlioU:S:WASI E BUREAU

Page 43: LAB S9::SOO

',

ANALYSES REQU""'_,JTED LAB. N-., 503 PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. TlliENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

,..... ~ ~--~

~( ._~(/ _5 ~ g: ::> ~ g: EXTRACT ABLES H ::> PURGERBLE\',

H

~ H E-< H E-< < ~ E-< < E-<

H E-< H E-<

~ ~ SCREEN ~ ~ SCREEN·' ::::::> ::::::> ::::::> 0' 0' 0' 0'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

IY GAS CHROMATOGRAPH/1-fASS SPECTROMETER HYDROCARBON FUEL SCREEN ORGANOPHOSPHATE PESTICIDES POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS

SP£CI~IC COMPOUNDS SPECitiC COMPOUNDS •'·

RE:t-fARKS:

ANALYTICAL RESULTS CONC- CONC-COMPOUND ENTRATION COMPOUND ENTRATION

I 1-(~-~-e • .e::ei\J2/'AR_ 12oo,_.L4/)

/ i /-L_ 'r:-AJ'M n ;;tl h'-1<

/U

J OSOOU-a.le

T_,.~_cJ~. I' /? -~

'o.:t..J.&~ ~ 2 i DON/JJ!

CHI-of--t~.- VI-- 2(": !i b -<'cJ..a:.,o-n~"...e_ _g{~/~

/ (/

* DETECTION LIMIT 2C~-a.lz RElfARKS: flf, dU!Jl'-- .-,, ~ d .,..,J J -t!v._ r~ pj;_.,;t;;JJ • -- u

f u

~~ ClTRIFICATE OF (IAL'AICAL PERSONNEL J/3<>/fN; . Seal (s) Intact ~ No . Seal (s) Broken by -:::1 date '1/c~/:?11- I 5/;l/>:..,-f-. I certify that allowed standard laboratory pr~dures on handling and analysis of1 this sample unless otherwise noted and t1at the statem~nts in this block and the analytical data on this page accu~ate~y r1eflec~ th_: Jnalytical resu~ts for thi~ ~ample. , Date(s) of analys1s 4/'?ti:r, f/Y/ff4 OJ. tt/rf. Analysts s1gnature ~ {).)~

sample and !certify that I have reviewed and -'cmcur with the analytical (r:SUits fo!'is with the stateiiP.nt-R in this block. Reviewers Signature:~~ L I PSfY1W-024 . 7~'- >--

Page 44: LAB S9::SOO

!CAP ·SCREEN

Lab Number: 1-J m ;} I q --~~~L---~------

Date Submit ted :. __ 4-1-j_,_, _,/,__~_l}_-__ I I

By: __ ~~~~~~~~-----------0

Determination

Aluminum

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead

Magnesium

Manganese

Molybdenum

Nickel

Silicon

Silver

Strontium

Tin

Vanadium

Yttrium

Zinc

Sample Code : __ _:_P_S_:;f,_:1_J{/..:_·_--=I=-A ___ _

Date Reported :._--=.b.,_;;.:.../ _;_q-'-j~~ t-J_:.__ __ _

m1 ' By: ---------------------------

Concentration (~g/ml)

.<.o,,o < 011()

< (), It)

{), 34 <(!J,,o

;)..57:).

<o.,c ..(o,IO

<0./0

<o,~o

<o,10 33.

<0./0

<o.Lo <.o, lc.7

21,

<O.tO /.3

<<!),I C

<...0,10

<o.IO

< CJ. 10

Page 45: LAB S9::SOO

ATOMIC ABSORPTION ANALYSES

Arsenic ~ 0, 00 c;- pg/ml

Selenium (!). tJ 33 pg/ml

Mercury < 0 , o Ot> $'..- pg/ml

Page 46: LAB S9::SOO

·'~.

J•

~ R~PO~T TO: .\·later Pollution Control Bur~au LAB NUliBER J/!ZL::_JI/f-~ Environmenta· ·~provement Divisio~

d F C f.\ \f E ~..:..;ea l th F: Env·,. -.Jnment Dep:rt~ent "- P. 0. Uox 968 - Crown Bu1ld1ng

Santa Fe, NM 87503 . '/1 TT E In I 0 N : D c~ v' c.. 13o '&·-="{_;;_,_.-./ __ _

0 ,, -1 ,... p ,,, 't-1 v c D / j - I J (J ;/ .• t ,,;__ ... ~.,L.."4?=----

Q/',TE REPORTED ~j_CJ)_ ~v __ 0J:~ Initials

.,::;',·:f~RDOUSWI\3Tt --- -- SL-rJ--us4<:.. ___ COJ)'i.- S~fs-do·· ·-GROUI~~~~~~--------------------------------------~--------

Bl\~A'W:R OR WASTHJATER ANALYSES-ENERGY DEVELOPHENT t~ONITORING PROGRAM

Sample Location f;vPl ft RS.o/'-J ~TAT;o/J'

Lat/Long ___ 0 ____ •_• 0 . I II T R __ s ___ _

Station/Hell Code p_s,Mw- :LA NPDES No. Outfall No --,---

Collected s-'iCly!O /5 yS- By L/1~10f.A:.T ~t-/-<IA~5G>-.J c.~· r-0/f/LJ Date Time Name Unit

Pumping Conditions ~~~~-~---· l_·e_~----------------------------------~ ~Jater Level /f 2. 5"( 1 l/ty/"'- .--01 ~o,"J· / d ~t~;:_(;., e pH ( 00400) __ 1-..:...· _,_f-:__ ___ _

Staff Gage Height --------­Controi Structure -----------------

. Discharge -----------=-=--Samp 1 e Type ......lG ..... '>.L--~"'-.J._L:_? ---------

t~ETAL ArlAL YSES

From NF, A-HN03 sample:

[]Arsenic, totul

[]Barium, total

__ ..:.....ug/1

__ __,._).J. g /1

Date Analyzed

0 Cadmi urn, tota 1

0 Lead, tota 1

0 !·ioiybdenum, tot

0 Selenium, total

[]Uranium, total

[]vanadium, total

[]Zinc; total

------1!..0. g/ 1 ---

--~_.u..g/1 ---

----"",ug/1 ~-­__ ___c}Ag/1 ---

-----c~g/1

~---J.p.g /1

--~).J..9/1 ---

Conductivity (Uncorrected) ___ ! s_· _o_o __ __:_,J..A.......;.mho

vlater Temp (00010) ;:2L'J °C

Conductivity at 2 50 c ( 00094) ---------=-..LAffi~ ho.

from~-F~ -~A-HN03 sa~pl"e·:·-, ,~ Date Analyzed

~Arsenic, crrssOTYed <.£.o ,u.g/1 j

:1:/~l:.ji<f g Barium, dissolved ).1..9/1

' ~Cadmium, dissolved ,u.911 ------1"-, Q Lead, dissolved p..g/1

--~. -----B l·~olybdenum, diss

~Selenium, diss

0 Uranium, diss

0 Vanadium, diss

~-zinc, dissolved

__ __,)-J..g/1 ~----

33 · ,P-911 Yfr1-:,1h ----F-f-911 ----.;.}·l 911 ---------~f911 -----

Remarks __ f&._::__/_~_L-_Iv_',;t-_1_1~'--'_v_'/\.._"'l _____________________________ _

f.i!!. c · rt:. o /L1 ' u #1

RQ r;vvo.tv ~ /f~[ > [ ,~-----~~~--~~--~~-----------------------------------------

This form accompanies ·,1_ sample(s) marked as follows to indicate field treat~ent (circle): ~ \·!hole sample; acidified with 5 r.1l cone HiW/1 ( F, A-HN0

3:).Filtered sample (0~45ymembrane filter); acidified \'l'ith

---.____" cone HN0/1 5 ml

Page 47: LAB S9::SOO

Environmental Improvement Division Health u Env~ 1ment O~partrent

,, ., ,,, ''""'~"''-H-'~.'<~"~~~-t<,,'"'"'A'01N"f~"'''*·"'"'"~'4~;;"·"'\'1>4 .~.-~"""}".''"·., ·~"''', .•.• ----------------P. 0. rlox 96b Crown Building Santa Fe, i'll·l 87503 .~TTEiiTIO:~: _f\he (;;off .v-

_ _ _ . SL-D v;E_re_ toi:> f_ 59 57:XJ ----------------· _-·_--_-----· _. -·-..:..--· --:·..:.·_:.....· ~--:.:.:,:--·_;_-..;..· ...:..·_.:...· ..:..·..:...· ·:...,._...;.·_;·..;..· ~--;:...----:-·- ·--- ········-

'rJATER OR HAS TE\~ATER ANALYSES-ENERGY DEVELDPI'1ENT 1··10NITOR1NG PROGRAH

Sample Location P;V/1.1 (-JVZ'xl/LI >rArro_.J ,

Lat/Long

Station/Well Code

Collected

0 II

{Y$/f//w- :tA ?5-'io.2f;o ! 3-Y'S

Date Time oC~, le c!

0 H T R S --------NPDES No--~

By L.A!VIeur /c t..AA.>s;(--"-"'

Name

--- ----Outfall No ---

0 CA.J/;-..1 t.U

Unit

/ ,. / '--1_ -:1_'

1r:z.'>Y 1"'0-----. .)vl()t"V.,s- J;:: ... v( ... (:: pH (00400) __ ,.;..._-_ -,- ___ _

..

Conductivity (Uncorrected)

Water Temp (00010)

I s-o()

.2.Q)

Pumping Conditions

Hater level

Staff Gage Height

Control Structure Discharge

Sample Type Conductivity at

2soc (00094) ·;.-.mho

GENERAL WATER CHHliS1RY AND NITROG£11 A~ALYSES --------------------------------------~~~~r7~~-----------------oate

Date 1\nalyzed Analyzed From F, NA sample:

-- .

~~~: __ ~~~_s_ample: --~ ~ Condgctivity ,.u.mho

5 C)_f00095) --

fJCJ .._f? mg/1 nfilterable · sidue (suspended)(00530)

From.NF, A-H2so4 sample:

Ol~itrate+ nitrite, total {00630)

mg/1 __ _

0 " . /1 /"\mmon1a, ____ mg __ _ total (00610)

~ l·lagnesium 5) ____ mg/1

~ Bicarbonate(00440) mg/1

fSl Calcium (00915) mg/1

@Chloride (00940) mg/1

~ Potassium (00935) mg/1 ---BJ Sodium (00930) mg/1 Ej Sulfa.te (00945) mg/1

---

~Total filter- mg/1 able residue (dissolvedX70300) (A/fnQNAT[

From F, A-H2~?4 _samp'ie: )

~ !litrate + '""'1 ..... 7.._ . .:.;..g __ mg/1 i/'r nitrite, dissolved

0 Chemical mg/1 oxygen demand r::·"r--_· ..--.:----_ -··;· .. ·~~---.-. -·---~ . r } : ; ·~ ~ f r·\1 ·1 ( ·• . ~ , ~· : , . f . • • • _

(00340) fi '.•'-'i"l' ii '-.• '· ,· i-~ i1 : ( l .• ; . • : i \ ' : . ..-.,;: i i .

li i: \I r • " ' • .~. o 1 1, o It I ; , I i u : ' ! J. () I ~; ()' f i ' i ' i

tJ' .... _ .... ___ ----~..I'E~

(00631) '

~ ~omonia, dis~ solved (oo~qs)

76i~l 1{-/V [ ·•. '

This form accompanies ··'z sample(s) marked as follo\•:s to indicate field treatment:

__til: Hhole sample (no filtration) @ l~o acid added (_j;.l---Ei,lte red in field \'Ji t h 0. 4 5)-A me;;1brc: r: e · filter

f'l • ' r:"' r"' • r . • . • .: _.- : ~ • ! , , .: ~ .. t., ") l"r 1 r- • , ..-. ,... ! J C" 0, / "":

Page 48: LAB S9::SOO

~ RE?ORT TO: Water Pollution C0ntrol Bureau E1vironmentzl T~provement Division Health~ Env1 .1ment Dcpartrent P. 0. ~ox 968 - Crown Building Santa Fe, i'lt·1 87503 .l; TT E; HI 0: ~ : _!} f.~.:.v e (Z,c, If~-,--

D.C\TE RE,_ .. JED __ {i_~!/.~J-f--__ iJATE REPORTED _,~L2 (;; /£:_t_ _ _L9-

Initials

____ .. · S~-D uc;;tre ___________________ _:____:_:____:__:_.:;__:__:_:__;__....:..._:__;_;___~_:.:_::____;-·. ---- -· ....

YJATER OR \·lAS TE\~ATER ANALYSES-ENERGY DEVELOPi1iENT !·10NITORI NG PROGRAH

Sample Location P!VA-1 P~-r?.Su.-'Ll >r.4rro~

Lat/Long

Station/Well Code Cell ected

0 II 0 t: T R S ------- -- ----es/v1~-J- 1.1 NPDES No Outfall No

---~ ---~?.1.(CJ2.f!D !;:)//c;- By CA,NJfJL.rer/C tAA.ss;z_..J t;C-V/;..Jt.V

Date Time --~N~a-m_e _____ ;__ __ ~U~n~i.~~------

~8.;:,' 1-c. cf !f2.. '>Y / l/'o~ _1t1 ?7 c'V.,c:)-

1 J ~~-v(" ,~ pH ( 00400) __ 1-..:__' ·...:..1-_____ _

Pumping Conditions

Hater Level

Staff Gage Height

Control Structure

Discharge

Sample Type

Conductivity (Uncorrected) 1 c:s-o(.) ).Amho

\·!a ter Temp ( 00010) 2.D °C -----~-.. Conductivity at

250( (00094) · ,.v..mho

GENERAL WATER CHEt·liSTRY AND NIT?.OGEt~ At~ALYSES

--------------------------------------~r-1?-~~r~~,~------.c~,.-~-,_-?----~--oate Date · ~~: __ r~~, NA samp1 e: ___ --...,. An a 1 yz ed .__F_r_o_m_F....:,_NA_s_~~-pl-e':-) n a 1 yz ed

5;1 l·\agnesium--{'U0~5) __ ...;.__ s- /; ~~ ._3.) '7 mg/1 ~ Cond~ctivity ---~...umho

5 CH-00095) --

~Ju -cJ? mg/1 onfi lterab 1 e -----. -----esidue (suspended)(00530)

mg/1

~ Bicarbonate(00440)___;:....!..-::~-170-8 mg/1 f·;: 0 .:? ~ .'? ~ Calcium (00915) mg/1 -----

@"Chloride (00940) _ ........... -"-'-----jy;;z,c;- mg/1

-~ Potassium (00935) _...,._._ __ mg/l !0· '-/3 G::> mg/1 8J Sodium (00930) ----.,---

13:l Sul fa.te ( 00945) /'_' _ __..;;;..-=-..;.-'---mg/1 -·&0./

~Total filter­able residue (dissolved)( 7 0300)

( ,<f(C' r5o A/ .4 T [_

From F, -~-=--~2so 4 samp 1 e:

!2SJ !litra te + nitrite, dissolved (00631)

il7'-! mg/1

/I ' _, -

' / mg/l

mg/1 18J .l<m'Tlon i a, dis-:: solved (oo~qs)

EJ ~-~~I t{- /V

----

silo r_ ~- / '>/

This form accomrnnies 2- sample(s) marked as follO\·:s to indicate field treatment:

____Jll: ;.:hole sample (no filtration) (J]0) l~o acid added ~4ltered in .;ield \'lith 0.45)-Ame;;;~:cr,e·filter

LLW c:r,) • [,,..~,-~.;:.;,.,~ ,,•i+h ? m1 rr.nr W c:n 11

Page 49: LAB S9::SOO

0 7f/f:7~

84- osoo -0 c/f 5tJa~4G REPORT TO: Environmental Improvement Division

Health & Environment Department P.O. Box 968 - Crown Building Santa Fe, New Mexico 87504-0968 ATTENTION: 0Av·· J /3rl'l

LA BORA TORY--::__,.___..__,...,....__-.,.--...... 5Z 0 PI?. I 6/ll.l -t-y :z..

LAB NUMBER

BUREAU: G t.J + " t.J SLD Users Code tlo. S~ ' ~ o ALL CONTAINERS WHICH THIS FORM ACCOMPANIES ARE COLLECTIVELY REFERRED TO AS "SAMPLE".

Sample Type: ~Jater IXJ CERTIFICATE OF FIELD PERSONNEL

Soil 0 Other ----------------------------------~~ Water Supply and/or Code tV ~ 1\/ 5 +A l-1 ·.., .1(/

City & County_~'-'-"L_;/3=-~~.=..c.:"""""-~~:.....::;;_---------------------.---:--------f Collected (date & time)_Z'W--t'/...:::O:-.<I...:......:..I...::o_~~;.:.__- By (name) L~mhe/Z+ C/AA-SS~~ pH= J-. [ ; Conductivity= /5t~o umho/cm at :JO °C; Chlorine Residual= ____ __. Dissolved Oxygen= mg/1; Alkalinity= Sampling Location, Methods & Remarks ( i. e.-0-d~o-r_s_e....,t-c-. ...-) ------

Flow Rate= ---------1

Fe.fL~ollJ $-t-,4 • f}1tPN. CJe-1/ - / /f

I certify that the statements in this block accura ana lyses, observati C.ns and activities. Signed-//---,~-~~f...::.}¢;z::;c=:::t.L:~:2L..:,..---,-.,-,---,.---­I certify that I witnessed these field analy and concu with the statements in this block. Signed~.~!:::::_:::::__j,_::::::::~::::::_::::=::::===--Method of Shipment to Laboratory /1/1-AJc/ e..//v ~n. e J THIS FORM ACCOMPANIES ~ septum vials with teflon-lined discs identified as: specimen 1 ; 'CIUP'ficate ; triplicate I ; blank(s) and amber glass jug( s) with teflon-1 i ned cap( s) i dent ifi ed as -----and other container(s) (describe) identified as _____ _ Co~s are marked as follows to indicate preservation (circle):

) No preservation; sample stored at room temperature (-20°C). -ICE: Sample stored in an ice bath.

2 3s2: Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

CERTIFICATE{$) OF SAf~PLE RECEIPT I (we) certify that this sample was transferred from Kev,'tt/ L;~~,.,_betL. I to

'( Me.;Jerlle;l', at (location) SJ.-,() on (date & time) %/;oj8<f L/S() PM and that the statements in this block are correct. Disposition of Sample cJ/L =eal (s) I::: Yes ID No 0 . Signature(s) ~ ~ Ln-;~k. -------------------------------------------------------:g::=---------------------------1 (we) certify that this sample was transferred from to

·-------------------------- at (location) RECEIVED on (date & time) _________ and that the statements in this block are correct. Disposition of Sample Seal(s) In~\A:'{~3v~8fb No 0 Signature(s)

.c..-------------- --------·-····--··----·---"'"VVI1"' nl .. "l -"""'vu" ""'·'-.BUREAU

Page 50: LAB S9::SOO

ANALYSES REQUl, ..... fED LAB. Nt s·oo PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. lfHENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

0-~ y :;;;i_) C)

J:;<:l ~ I

:> J:;<:l ~ EXTRACT ABLES H :::>

PURGERBLEl'· H

~ H H H

~ <t: H H H <t: H H H H

~ ~ SCREEN ~ ~ SCREENO 5 :;:J 0' 0'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

% GAS CHROMATOGRAPH/:t-1ASS SPECTROMETER HYDROCARBON FUEL SCREEN ORGANOPHOSPHATE PESTICIDES POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS

SPECIFIC COMPOUNDS SPE:CIF"IC COMPOUNDs''·

REt-lARKS:

ANALYTICAL RESULTS CONC-

COMPOUND CONC-

COMPOUND ENTRATION ENTRATION

I } - <~-)Jr,r ~c-e---t~~ ~r;c~UJ/i' i I 1-'T~_}.f,:-v,.Jl'..a,,ul.- /0/t 5'/-0ULMI.- .-f?

r~-.J!IJ, #) J! ll v-.---.:L / v' "

{ 200 f;<-4 .· /1.1

/U

* DETECTION LIMIT /0/..Hl__/~ RE11ARKS: ~lJ t?fk«r tJ-A-~);-~,~ /.f.d;J.,L ,1, ,c

I v·

Iii? CETRIFICATE OF AN!fYTICAL PERSONNEL 'i p f j? J, __.( . / , r·(/, ·I

Seal(s) Intact: No . Seal(s) Broken by ~ ·~ . date +130;,l't/ 1 :?/~'e'?';-I certify that ollowed standard laboratory p~cedures on handling and analysis of this sample unless otherwise noted and that the statements in this block and the analytical data on this page accu~at~ly reflect the. analytical resu~ts for thi\ samp~~~Jlt Date(s) of analys1s lj(:Lt/yl{ ,' 'f/Jr/fiJ' 5/t//tf. Analysts s1gnature ) · 1 '/.:. :.,,j

Icertify that I have reviOwed and concur with the analyt~ ~ults for f9{s sample and with the statellPnt'R in this block. Reviewers Signature: . /;;- !u , P5 M uJ -( . 7-t:?__'Z.-- -u~

Page 51: LAB S9::SOO
Page 52: LAB S9::SOO

· .. :J ... ~• ,·L,,/..,.,.,u!l '-'l'll'-il.lt L>uteC!u

E~vironmental Tmprovement Division Health u Envi ment D~partrent P. 0. dox 968- Crown Building Santa Fe, Nl·l jl7503 .L.TTEilTIOl~: J)gv/J Bovre R_

- I

Lh .. ilu.·l • .:n .... ~ r I ',) 'L/ ........... /'('-? /. "----

DATE RECE. J --1--~,/_/_-~t/ , DATE REPORTED J/t/:ff_~ e9-_ . Initials

-.- .. SL.D . Us.cfl-. Ce>.d ~.59 $o.Q . ___ ........ .

~ATER OR \·JAS TE\4ATER ANALYSES-ENERGY DEVELOPHENT I··WNITORING PROGRAH

Sample Location

Lat/Long

Station/Well Code

Collected

0 R __ s ___ _ II • 0 II T -----------' ----------

f5/YIW- !A NPDES No Outfall No ---('/ o1Jo J/3D By .L&~be&f / CJAA.s.s~AJ Gb./-1/LJ

Date Time Name I Unit

Pumping Conditions J3A,'JeJ [)e.f#,.lo\·later Level 9J.S5/t til /liD Staff Gage Height . -------­Control Structure

pH (00400) _tt...:.'....l9~---. __ _ Conductivity . ·

(Uncorrected) -~' :::..5"~o _____ .P--=mbo ·

Discharge

Sample Type

~·later Temp (00010) ;2 'I · °C ---..!-----.. Conductivity at 2soc (00094) _

GENERAL WATER CHEI-liSTRY AND NITROGEI~ A~ALYSES

From ample: Date Analyzed

00 CondHctivity ___ _....:.; ... u.mho __ _ . ll1 ( cplf )( 0009 5)

0 Tota 1 mg/l ___ __ nonfilterable · residue (suspended)(OOS30)

!AOIZt ~

rom~mple: ~ /·lagnes1um (00925) ~ Bicarbonate(00440)

~ Calcium (00915)

[I] Ch 1 ori de - ( 00940)

GU Potassium (00935)

~Sodium (00930) . From NF, A-H2so4 sample: [K] Sulfate (

00945)

0 l~itrate + ____ mg/1 ___ [l] Total filter-nitrite, total able residue (00630) (dissolved)(70300)

0 ,., . /l It> G AeboAJA-ie nmmom a, ____ mg ____ m=o F total (00610) Cm ' A-H2.::0ample:

0 Chemicald d ---~or~~~., .J~Cj~lr·O]i~c--i'· -,"lKI !li~ra~e + d' 1

d

r---mho

o. '81 ~Date Analyzed

/~. '7 mg/1 f'/1 m.o mg/1 !:J If Z

I :[I, ,() mg/1 ~//I

DO·~ mg/1 ~1 f.'l7 mg/1 ~/3.:

I

2f J mg/1 (J

. (_{5. 7 mg/1 ~/.!-S'lt mg/1 2f1-1

0 -s/t7

mg/1 oxygen eman ~Tfil) ~J.r LJlJ c:3i, \_\! J. ;:!t~ ~~ !' ! I n1 tnte, 1 sso ve (00340) G' L::LL.: ....... .I .. -{ 1! (00631)

\ JUN 5 1984 11Uloo ~J11t1lonia, dis-: mg/1 l:_ ~ solved (00608) ___ ___,; ---

GP.uUNO VJ.mRjHAZARDOUS WASTE L8l · o tA

form accompanies _;;.· s_ample(.s) rnarke~· foll01·1s_ to indicate neld treatment: : \·Jhole sample (no· f1ltrat1on) i:A· No ac1d added

Filtered in field v1ith 0.45,.u..mer.Jbra ·- filter- .

This

so

Page 53: LAB S9::SOO

, «,/"'""~' "·'"" '''·'-·••H',''"''•"-"-'' ,_,_,,,~, t.I'UJ 11Wt1W'-1'

E~vironmental Improvement Division -Hea 1 th ~ Env nment lJ~partrent DATE Rf IVED /ilf...-J.:f4~~ ~ //0 ~ P. 0. dox 96b - Cro•:m Building ·t---~ / Sant~ Fe,, i'lt·l ,{3750.3 DATE REPORTED __t;P.- _ s:-.t5..i'ty .4TTEiHI Q,~: _J(_qy r J t3o v ~ t?.. fniti a 1 s ;r .

. . . . . ... --- .. 5,L D . Us. ell. Ce>.d ~ . 5'9 .$.Q.O ... ____ ·--·····-r.!ATER OR HAS TEHATER ANALYSES-ENERGY DEVELOPHENT 1·10NITORING PROGRAH

Sample Location

Lat/Long

Station/Well Code

Collected

0 II R __ s ___ _ II T ------0

P5 /Yl W- !A NPDES No . Outfall No ---$"'-/ ot./Jo J/30 By L&{M.begt J C !AIIsse.tJ GtJ- II LJ

Date Time Name 1 Unit

Pumping Conditions /31'1,'/e J /)efth-b\·later Level 9/- S ~=/t (iJ //10 Staff Gage Height_-------­Control Structure

Discharge

Sample Type ..

pH (00400)

Conductivity (Uncorrected)

Water Temp (00010)

Conductivity at 2 soc ( 00094)

t· 1 ..

,~0 .).lmho

~'I oc

P.mho

GENERAL \~ATER CHEI-liSTRY AND NITROGm At~ALYSES -~~-r---------------------~-~--r----------------------oate

ample: Date - Analyzed Analyzed From

~ Cond~ct i vi ty ,.umho __ _ Ill ( 2pJf )( 00095)

0 Tot a i mg/1 nonfilterable · ---residue (suspended)(00530)

____ mg/1

mg/1 ----____ mg/1

(OQ940) mg/1 __ _ . ~ Potassium (00935) mg/1 ---

From NF, A-H2so4 sample: ~Sodium (00930) mg/1 ~ Sulfate (00945) mg/1

0 t~i tra te + mg/1 nitrite, total

DO Total filter- mg/1 able residue ---

(00630)

0 AmiiiOn i a, mg/1 tota1 (00610)

0 Chemica 1 m.9LL. oxvgen dem9( ~·H01'1t)'1 ;".. -.·.,·', ~:~,.-,""'r~,--

,; Q~f!r.'-'l.':'','t.''·':','i.\ .. ,.· ... · .. ,. (00340) 'd./ t\ .... !: ......•• i ' ' ·~-~- ! tj'

Ji t' t.i~·.· • • .. • • • n 1 r, :1 ·l l • i

\ \ ! • 'f 1 r") ! ~tV l t H ~ l I '1 I. .c ' . .) . i iJ. ,,l:

1 '·~ ...... , >., , ... • >·•·-M·•_{·.,.,,:.,~

(dissolved)( 70300) ~ C, AeboloJAte

emF, A-H~. ample: --

(KJ !litrate + t9. & ~ mg/1 u/, &' nitrite, 'dissolved ~ (00631)

0, J. 5 mg/1 .-s-/s

f'ield treatment: for:'il cc~omrnnies .;)_ s_ample(.s) marke~· foll01·:s_ to indicate A= l·lnole sample (no· f11trat1on) i:A· No ac1d added f...U Fn~ered in field v;ith 0.45,.u. mer7lbra ·- filter .

' ' ' ,... ,_ ' ' ... , ., , .. ' ,.

This

Page 54: LAB S9::SOO

r ~ REPO~T TO:

.. Water Pollution Control Bureau Environmenta· 'mprovement Divisio~ Health .r! Env:J, Jnment Department

RECE\\IED P. 0. Box 968 - Crown Building Santa Fe, NM 87503 !\TTE1HION: DAvid Boye'--"_g..;;._ __

GROUN .-,,:n l;:~:JtJ~§us0\~1\~WSTHJATER ANALYSES-ENERGY DEVELOPI~ENT I~ONITORING PROGRAM

BUB.Ei\:J Sample Location PNtrl PcJ?sot.J 5'-tA-'f/oAJ

'

0 II T R S -- ----La t/ Long _____ 0 ____ 11

_

Station/Well Code

Collected

PsmtJ-7-If NPDES No. Outfall No ff LJ D t.f J 0 J /30 By ).111'>1hc::t2 f 2 C }AIISSe IV 6 f.J )/1_4) __

Date Time Name ' Unit

Pumping Conditions ~~~=~~;~j~G~J~~~~--~-~-----~------PepfA fu\·later Level 9/. SS # e__ ///0 pH ( 00400) _---~.1:.._;'.....:9 ___ _

Staff Gage Height--------­

Control Structure --------­Discharge

Conductivity (Uncorrected) t-5o ,v..mho

vlater Temp (00010) __ .:2._.;L/'---___ 0c ---------~.~- Conductivity at Samp l e Type __ G ............ P.~.A_:.b ____ _ 2 soc ( 00094) _____ _____:_,u..rn_ h~

METAL ANALYSES

Frcm NF, A-HN03 sample:

[]Arsenic, total

0 Bc.rium, total

D "-d · ' \..,c iill urn, total

0 Lead, total

[J :',::lybdenum, tot

0 Sel eni urn, total

Ouranium, total

0 Vanadi urn, total

0 Zinc, total

Rer~;arks gl A/ tA.Mr,t.Ju vn..

7X1 C A flo ~ro ,· u Wt

Date Analyzed

)..!..g/1

).l.g/1

)..1. g/1

. ,u. g/ 1

p..g/1

p..g/1

J:A-91 1

).lg/1

.1-'.91 1

00 Arsenic, dissolved 3o. _ug/1 , IE] Barium, dissolved

• J..~-911 [XJ Ca dmi urn, dissolved .u911

I

0 Lead, dissolved ' J.;.,g/1

[KJ t•',o1ybdenum, diss • .u.91 1

[Xj Selenium, diss < 5"-o p.g/1 '

0 Uranium, diss ,...g/1 I

0 Vanadium, diss .!.1.9/l I

00 Zinc, dissolved ,1.1.9/l I

This form accompan1es I sample(s) marked as follows to indicate field ~rc-~-~~~ (c1'rcle)· ~.,., ~,..c \,.. .. :=-~~ L. •

:::: \·!hole sc:mple; acidified with 5 r.1l cone HtW/1 Filtered sample (0.45ymembrc.ne filter); acidified with 5 ml cone HiW3fl

Date Analyzed

'f/2to(C'f I

Page 55: LAB S9::SOO

Lab Number: N M J-./21

Date Submit ted: ;.j, I 11 / t lf

By: ~~£&'::

Detennination

Aluminum

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead

Magnesium

Manganese

Molybdenum

Nickel

Silicon

Silver

Strontium

Tin

Vanadium

Yttrium

Zinc

!CAP ·SCREEN

Sample Code :_..:._P....;..S....;.M-=--l-l=-J _-___.:..1....:..A....!,..._ __

Date Reported :"_.{o_.+j_t_q--4-/_&-_'-f;_ ___ _

By: mj'

Concentration (l.lg/ml)

<o.ttJ ca.3t

<eJ·lO.

0./ <if <tJ, 10

(05, <D 1 I D

<o.to <o.,o <o,,o <o.to

I~.

.<o,to <! o. l 0

<a.1a Lt-D.

<O.dJ

Q.11 < 0./CJ

<o,tO

<o,1D <t), 10

Page 56: LAB S9::SOO

ATOMIC ABSORPTION ANALYSES

Arsenic _.:;_D.;_. ~03=-~ =-O _ __,pg/ml

Selenium ___ <(~o_.~o_o~s~-----~pg/ml

Mercury <~~0~.·~0~0~0~~~·~--~pg/ml

Page 57: LAB S9::SOO
Page 58: LAB S9::SOO

R E C E;.tBVr[;:ftER

CERTIFICATE OF FIELD PERSO~~~u Sample Type: \·Jater·fE Soil D Other

-----------------=~r-~-~~ vJater Supply and/or Code No. ~~%-:'1c,..,£C", ~ -:i.--City & County \\"-~"'-\_~tQ

7 ~s-~'\~

Collected (date & time) <'i()6\2~ '\2--'?£) \-1'-<::.~''--' pH= ; Conductivity= L\2\ umho/cm at 2D ~~ °C; Chlorine Residual=---------t

Dis\olved Oxygen= mg/1; Alkalinity= ; Flow Rate= ~ Sampling Location, Methods & Remarks (i.e. odors etc.) .

. \--(""" ~<;(_ \~ ..... "><._ --\>\~ ~ ~~~c:;::\_""''\""-- ~ ~~~ . {\O o~~, , ·~

certify that the statements in this block a urately rr fleet the-results of my field analyses, observatkns and activities. Signed~~,~=::::::;:,..-:--""'~::loll.L:~y..~:~=-..,....,-:------,;---­I certify that I \'Jitnessed these field analyse and concu i·:ith the statements in this block. Signed ---------------------i·1ethod of Shipment to Laboratory ~ -~~\:) THIS FORfv1 .AC c.or~PA.N I ES 1- septum-v-,..-. a'l_s_v_/1;-:. t'h--:-te-f;::-,1-o_n.....,-1'. i:-r-.e~d-d-;-i:-s-c-s-,.,.... d-:-e-n..,...t..,..F7• i:-e'd-a-~--:------specimen b ; duplicate 5" ; triplicate ; blank(s) and amber glass jug(s) with teflon-lined cap(s) identified as -----and other container(s) (describe) identified as Containers are man~ed as follm ... s to indicate preservation (circle): ---------

No preservation; sample stored at room temperature (-20°C). Sample stored in an ice bath. Sample preserved with 3 mg Na 2o3s2/40 ml and stored at room temperature.

CERTIFICATE(S) OF SA!~PLE RECEIPT . _ I (we) certify that this sample \'las transferred from- k-:Q.-.~~ ~§C:'-"'~~,c_ to

, ')C:;;'-N.;. \~~~ at (location) S\3:::::) on

(date & ti~C'-[;1\.'J ... :]:±:- \\.c~s-- and that the statements in this block are correct. /

Disposition ff ~ample d-1--- 0 seal (s) Ip~~es l3r No 0 . s 1 gna tu re ( s) -~ \ ~~~ l\.l\1"-..~ ----"U;;z:::..::_-r.,A-£:-,..;."A-__.!:;j_;;o(d~c,.~~'-~---"-"~------------~------------~--------~~--------------------------~---------------------------------I (we) certify that this ~mple was transferred from to

, __________________ at ( 1 ocat ion) ____________________ on

(date & time) and that the statements in this block are correct. ----------Disposition of Sample . Seal(s) Intact: Yes 0 No 0 Signature(s)

Page 59: LAB S9::SOO

'"'""""'" '"''"' ~""' "'"""'"'"'"'"'~' ""''"'''-'--~ff·'""""""'""·"''""'""\"~"-'· ''~'""'"--"""·~'-""~'~'"'' m-~·· '>'" '""' '""~'"'"'•"''~"'"-','',. '". "' ,,r.)'I<O,«>''-"~'""'N•,.-~,_.u,•'-<>>r,~.,....,~,,_,~,4<*""'"~·-><<»"-='·""'"' --~-- --·~ .. --... "'-'"~ ~-'"''"'""'"'"''""'' "'"'"'"""""~"'"'~'~"' "'""""'"'"""~~~"-·""'"""~-·~·~· ··~"· '"''''""·•·• .. -···"'-

ANALYSES REQUE~TED LAB. NO. _J - - ---- -- --PLEASE CHECK THE APPROPRIA1, . .OOXES BELOH TO INDICATE THE T': OF Al'-;ALYTICAL SCREENS REQU!?EP. HHENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REOUH.ED.

I

w r:=:: :> w :> r:=:: EXTRRCTRBLES H :> H :> t--< H PURGERBLE E'""' 1--'

< r < £-E'""' < r < t- £- H £-~.:J z H ~ SCREEN <:: < SCREEN < ::J c- ::J ;::J 0' c c·

ALIPHATIC lfYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROHATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPI IE:\'OXY ACID HERBICIDES

:x GAS CHRmL.\TOGRAPH/NAS S SPECTROHETER HYDROCARBO~ FUEL SCREEN ORGANOPHOSPHATE PESTICIDES POLYCHLORIXATED BIPHe;"YLS (PCB's) POLY:JUCLEAR ARm!ATIC HYDROC,\RBO:\S

SPECIFIC COMPOUNDS SPECIFIC COMPOUNDS r ~\.~ \.. w ~'-~~~¢-\-,,~e~ ~ ~ '·-....01,"-.\.\.~)~ ~--1'-12.

1

RE:1ARKS: I I

ANALYTICAL RESULTS •

CONC-COMPOUND

CONC-l COMPOUND ENTRATION ENTR.A. II O:J

~7 ( . ( d'" { f}-T"- c.. ,, r~..f !-, n ~' ;:> {_ I j;){) 1 ·:) L<'C. -12.. 4-.L { e c, cl e.~,

_I

10 (> /~-+1, Q__.,- cfecf -y-I o/

--

";'>. DETECTION LUiiT lp/o/.;

RE::'l.i\RKS: I

'

CETRlFICATE OF A::,\LYTICAL l'ERSUNNEL Seal(s) Intact: Yes ~~0 . Seal(s) Broken by date -----·-- --- -·----------I certify that I followed standard laboratory procedures on handling and analvsis of this sample unless othenlise noted and that the. statements in this block and the analytical data on this page accurately reflect the analytiu:l results for this sampl •/ Date(s) of analysis o1/lu/£'f . An.:1lysts si;.:n,Jture :l~~-L4-_J--/-l"--7'e...Y'-..c___ Icertify that I have rkvie\,'ed and concur with the <tn3lyticaV results f(yi' this sa:'~p1e ·3nd '-"i th the statel!Pnr" in this block. Revie\,'ers Signature: /)~- L

./( fll~A "'-

Page 60: LAB S9::SOO

·~

...,

RIC DATA: ORG1e63 11 SCANS 1 TO see e2/09/S4 15:57:0e CALI: C0209S4 14 SA~1PLE: ORG-1e63 5ML P&T RANGE: G 1J see LABEL: N 0J 4.e QUAN: A 0J 1.0 BASE: U 20J 3

1ee.0-, 14e 69632 I

::0 '~ ~..._.

~

~

{ )

1-~ I

't """'1 ),' ~ ~

t~ \1'1

RIC I ll \; ~ .....

~ l.,j

,.......,_ ~ -0

~ ~ - t v ~ <SI I

............. 1 l'- "

~

!

~ ~ ~ I

~ C'\ ~ <:::_~

~

" { - I !J {"'"\ '"""' _,-;

I ~ J> ~ - .... - - 227

631 "' 434 482 523

1e0 2e0 300 400 5e0 6e0 700 800 SCAN 3:2e 6:40 1e:00 13:20 16:40 2e:0e 23:20 26:40 TIME

Page 61: LAB S9::SOO

84- oso2 -c ~jYJ-o/rSoe2~t3.

REPORT TO: Environmental Improvement Division LABORATORY -j-.-, L...,-D-=--f};-IJ.-/o-1!--, .-t-11 -d-

LAB NUMBER ; Health & Environment Department P.O. Box 968 - Crown Building Santa Fe, Ne~Mexic9 87504-0968 ATTENTION: _ ~v' d {3o ?' e 1\ BUREAU:J;U / HJ.<) SLD Users Code tJo. S9£&V

ALL CONTAINERS WHICH THIS FORM ACCOMPANIES ARE COLLECTIVELY REFERRED TO AS "SAMPLE".

City & County __ "-'-~'---_., ....... ~=-=--'-'-~..t..-..;;;-------------.,___,.-__,. __ -f Co 11 ec ted (date & t i me ) 1'4 Q 'iO 9 7:.5.-S" By ( n arne) -~.:::..-r--=--"--+-"--....!.L-.:C..:.U."'-=-'~--1 pH= ; Conductivity= umho/cm at °C; Chlorine Residual= ------ -----~ Dissolved Oxygen= mg/1; Alkalinity= ; Flow Rate= Sampling Location, Methods & Remarks (i.e. odors etc.) ------1

5 ,I_ D BJ. A 'II )!5

I certify that the ~tatements in this block accu~ely ref}e/t ~he~~ts of my field analyses, observatic·ns and activities. Signed ~~ ~ ~--,..-----1 certify that I witnessed these field analyses, observations and activities and concu with the statements in this block. Signed ----------------t1ethod of Shipment to~a oratory THIS FORM ACCOMPANIES septum vials with teflon-lined discs identified as: specimen 1 ; uplicate ; triplicate ; blank(s) and amber glass jug(s) wi..,-th;---:-t--'e..,..fl,.-o_n __ ..-lined cap(s) identified as ------and other container(s) (describe) identified as Containers are marked as follows to indicate preservation (circle):

No preservation; sample stored at room temperature (-20°C). Sample stored in an ice bath. Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

CERTIFICATE(S) OF SAI1PLE RECEIPT I (we) certify that this sample was transferred from k'ev ,· .v LA Nl b <= R. .r to £ }Yt"'"%"''" \.e·,- at (location) _ _,-~-'-'-J--._::;...,:D;..<------------ on (date & time) :1: 'S'/o 1~ (Jj/of,pc/ and that the statements in this block are correct. Disposition of Sampl_e' = ~eal (s) In~a?t: Yes ill No 0 . Signature(s) ~ ~~ JS_}n.e La ~04Nl. -------------l------------------------------------------6'------------------------------I (we) certify that this sample was transferred from to

at (location) RECEIVED. on 1---------------------(date & time) and that the statements in this b,l,g~~ are corr.~ct. ----- ..,..rv 9.t:l 1"'~14 Disposition of Sample . Seal (s)111fhtcrt~: "ies 0 No 0 Signature(s)

----------------------·---------~-

Page 62: LAB S9::SOO

ANALYSES REQUL.,, TED LAB. Nt <CJ2~ ,, j

PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. l~ENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

Ocv'}c- )-0 ',:)._ JZ.1 ~ v :> JZ.1 ~ EXTRACT ABLES H :> PURGERBLE:',

H

~ H ~ H

f-1 ~ f-1 ~ H f-1 H f-1

~ ~ SCREEN ~ ~ SCREEN·" g. ~ ~ 0' 0' 0'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

--;., GAS CHROMATOGRAPH/HASS SPECTROMETER HYDROCARBON FUEL SCREEN ORGANOPHOSPHATE PESTICIDES POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS

SPECIFIC COMPOUNDS SPE:CIF'IC COMPOUNDS''·

REMARKS:

ANALYTICAL RESULTS CONC-

COMPOUND CONC-

COMPOUND ENTRATION ENTRATION

* DETECTION LIMIT I 1/-4_ /J REHARKS: tl 0 J!AY'~~~tL ~( /U

I J

. . CETRIFICATE OF ANf ~Y;;CAL PERSONNEL /1

'-:>tfo Seal(s) Intact~ 1 No . Seal(s) Broken by \ 4T date I c:~!/2t . I certify that · allowed standard laboratory pro~ures on handling and analysis of this sample unless otherwise noted and that the statements in this block and the analytical data on this page accurately ref:ect the analytical resu~ts for thi~samplr "j 1 Date(s) of analysis 1}/2. t/f?i . Analysts s1gnature _,.~--1_ r~-J. .JL;~ !certify that I have reviewed and concur with the analyt~~ults for~is sample and with the stateiiP.nrR in this block. Reviewers Signature: 'ff; k

·~;t'V I i

Page 63: LAB S9::SOO

~)'fP~ 84- 0501 -B t:JK e-s-o; 01.

REPORT TO: Environmental Improvement Division LABORATORY Health & Environment Department -_5.:-:d:':---l>;::---P.-:::12-· --:,£--P.O. Box 968 -Crown Building LAB NUMBER '"'!!.' J Santa Fe, New Mexico. ~7504-0968 ATTENTION: D41Lld B" v e g BUREAU: Ji0/221Z7 = SLD Users Code tJo. :596"tJO ALL CONTAINERS WHICH THIS FORM ACCOMPANIES ARE COLLECTIVELY REFERRED TO AS "SAMPLE".

CERTIFICATE OF FIELD PERSONNEL Sample Type: ~Jater liD Soil 0 Other -----------------------------------~ Water Supply ---L.JJL(t.!..J..._.L..$:.~~~__,.~2:&::~~--~L:::.4~/IJ~k~sJ_ __ --J

Collected (date & By (name) ,L/f}"J_),e;,e+-pH= ; Conductivity= umho/cm at °C; Chlorine Residual= ------1 Dissolved Oxygen= mg/1; Alkalinity= ; Flow Rate= Sampling Location, Methods & Remarks (i.e. o?ors etc.) t- K. L i< ·t o_.(_P_v0 __ .-WI--.---t

0 1 1 '"z Tk ~~ S{}.Nvlf'« ve-L <.ol (., .. _ 411 b'r lL.•·n c.- 'l.. r s 1t1. (.,{./ - T T 3 . (d:. DR..t' ... dt. ,·..;J- r: D ...... rl-.4- / .v > P N m ntl'l' t'.v /, I d(J. fllu a...,ro.&.D J~ oCt.(' e.... f'C..:__v :,.l u.~~c-:, VI D ~ (? r "'6.,J (..) l, "'""' ciu..;, ,{) &;fXe- .:.._:.~,.!. <.o ( Le.J <...0 - :lf.l· ~ I certify that the ~tatements in this block accur~~ly ref2e~t th~ results of my field analyses, observati0ns and activities. Signed ~ ~ I certify that I witnessed these field analyses,~t1ons and a~:t~i~v~i~t,~·e_s_a_n_d~co_n_c_u with the statements in this block. Signed --------------------Method of Shipment to Laboratory THIS FORM ACCOMPANIES I septum-v-,,..... a ...... l_s_w_,i,..,..t.,...h_,t,-e"""'f=-1 o-n-_ ...... ,-=-; -ne_d.........,.d..,...i s-c-s~i d..,...e-n·: i fi ed as: specimen i ; duplicate ; triplicate ; blank(s) and amber glass jug( s) with teflon-1 i ned cap( s) i dent i fi ed as ------and other container(s) (describe) identifie.j as Containers are marr:ed as follows to indicate preservation (circle): --------No preservation; sample stored at room temperature (-20"C). Sample stored in an ice bath. Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

CERTIFICATE{$} OF SAr~PLE RECEIPT I (we) certify that this sample was transferred from j(e.v/.v LA-~ bee-t to J2 VV\ ~l~ at (location) 5~ on

(date & t1me) 1/to!J~ ¥:j/ p~ and that the statements in this block are correct. Disposition of Sample .6/C

7 _.;Jl~al (s) Inltac_t: Yes fS'} No 0

Signature(s) /~ ~ _)( ),.1!.-u.YA h.u~ ·-------------------------------------------------------------01-------------·----------------I (we) certify that this sample was transferred from to 1---------------------------- at (location) RECEIVED on (date & time) and that the statements in this block lre correct. Disposition o_f_S_a-mp_l_e____ Seal (s) rWrA'\:-?.3 WWb No 0 Signature(s)

............. ., ..... ~.. ~·

l3UREAo----

Page 64: LAB S9::SOO

ANALYSES REQUL TED LAB. N( sol PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. l{HENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

Oc~ 5"0/ ~ g: " ::> ~ g: EXTRRCTRBLES H ::>

PURGERBLE~', H

~ H ~ H

H ~ H ~ H H H H

~ ~ SCREEN ~ ~ SCREEN' & CY g g

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS

AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES

HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

y:_ GAS CHROMATOGRAPH/HASS SPECTROHETER HYDROCARBON FUEL SCREEN ORGANOPHOSPl~TE PESTICIDES POLYCHLORINATED BIPHENYLS (PCB's) POLYNUCLEAR AROHATIC HYDROCARBONS

SPECIF".IC COMPOUNDS SPE:CiriC COMPOUNDS' ..

REHARKS:

ANALYTICAL RESULTS CONC-

COMPOUND CONC-

COMPOUND ENTRATION ENTRATION

!)..1~,~ rl"" J}, j}~ ,--.-,v.J:J't:f-">"x ? ·r-Q il T~~Y>'tC~~/~ {~lf

/0'

* DETECTION LIMIT l.~ /f_ REHARKS: tJ,, 17~'- e ;,(/1.-(j J).,..J;.e,. cU~J). /(/

I u

.. CETRIFICATE OF ANALYTICAL PERSONNEL . . I-,. Seal(s) Intact: ~J No . Seal(s) Broken by J1A date '{'ft7/t f . I certify that I followed standard laboratory p cedures on handling and analysis of this sample unless otherwise noted and that the statements in this block and the analytical data on this page accurately reflect the analytical results for this~qampCLJ ,:r

Date(s) of analysis 'f/2 7(S'f . Analysts signature t-'-. , Vu~/ Icertify that I have reviewed and concur with the analytical ~ults f~~is sample and with the stateiiPnt-~ in this block. Reviewers Signature k fn·~ ~

Page 65: LAB S9::SOO

REPORT TO: Environmental Improvement Division Health & Environment Department P.O. Box 968 - Crown Building Santa Fe, N w Mexico 87504-0968 ATTENTION:

0 84- 0489 -B

~~~----~--~----BUREAU: G ro o,z. \J(aHc~ SLD Users Code tJo. 5Jr;oo ALL CONTAINERS WHICH THIS FORM ACCOMPANIES ARE COLLECTIVELY REFERRED TO AS "SAMPLE".

CERTIFICATE S OF SAr1PLE RECE sqmp e was transferred from __,(hf4~~~~~~b.L,4---- to

1--(~?.,p...:.f.4.4.~.....,4;;;.~~~~~~--:----r at ( 1 oca t ion )-----c::r"'h>"--'7~--=~~"F--''-T-=-'""""--- on this lock are correct.

-..P.....~~~~::__ ____ . Seal (s) Intact: Yes 181 NoD

Page 66: LAB S9::SOO

,' "

ANALYSES REQUl,_ fED LAB. N( < <9 ((. G - 4 84 PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. liHENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

~ ~ :> ~ ~ EXTRRCTRBLES H :>

PURGERBLE:'· H :>

~ H H H

~ ~ ~ H H H H H H

~ ~ SCREEN ~ ~ SCREEN' g g ;:::l 0' 0'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS AROMATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

"X GAS CHROMATOGRAPH/HASS SPECTROMETER HYDROCARBON FUEL SCREEN ORGANOPHOSPHATE PESTICIDES POLYCHLORINATED 'BIPHENYLS (PCB's) POLYNUCLEAR AROMATIC HYDROCARBONS

SPECIF"_IC COMPOUNDS SPE:CIF'IC COMPOUNDS''-

REHARKS:

ANALYTICAL RESULTS CONC-

COMPOUND CONC-

COMPOUND ENTRATION ENTRATION

/,/ /) -~n ,-" (

C~L£l#ZDFoR...M 1),--:!t B roUe d 1 e h kro iU<?+ltAI'I€. j,« if 6 _IM;j_ ::t bi 8 Rc•~tc c/iUJfo /Vi£ 71-tfM/12

/ t7 i' 3. CfA-<4 ~

T R I B f.r-lkc. 1l1 f Tlf It~£ l/~(/ (t_

' t.<4-/ / (/

* DETECTION LIMIT l~IL RE11ARKS: flo o+k~ ovv-q_e-1'fbl~ dof..,"f-.e). ,/v

I

CETRIFICATE OF ANALYTICAL PERSONNEL . , , Seal(s) Intact:~'No . Seal(s) Broken by Rt/;1,_ ee\,W date #s--'/C?jl . I certify that ollowed standard laboratory procedure'Jon handling and analy'Sis of this sample unless otherwise noted and that the statements in this block and the analytical data on this page accurately ~flic;/the analytical results for this{ta~pledZ Date(s) of analysis f 7 "r '8 - . Analysts signature-:J. / lftl Icertify that I have reviewed and concur with the analytical ~ultsFfor this sample and with the staternPntR in this block. Reviewers Signature: /'1 , .

r< In~~ L -' <::-"'I G! r /---

Page 67: LAB S9::SOO
Page 68: LAB S9::SOO

RtCElVEO

ers Code tJo. $;4 00 ALL CO:iTAit:ERS ',·JHICH THIS FORH ACCm1PANIES ARE C EFERRED TO AS II SAt-~PL E".

Sample Type: \·Jater D viater Supply and/or Code No .. ~

~~~~~~~~--~~~~~~~~~~~~~~~~H

City & County ~\~t_~"""-) ~'N"\~\,. C"'-"-'~ Collected (da:e & time) Cbo\'2..')....4 O'e:>SO By (name) ~-\<-\..-r--o--J-:;L pH= ; Conductivity= umho/cm at °C; Chlorine Residual= ------1 Dissolved Oxygen= mg/1; Alkalinity= ; Flow Rate=-------1 Saii,pl ing Location, t·ietho~s _& Remarks (i.e. odors etc.) __ . {I "'

lc:i\\ec'"\e~ 5;,"'~ ~'<.\"""~CO""--- ·2s' ~\~ ~" <.J~"'-.J -~\l~"'-~:.~-

I cert~fy that the statements in this block ac u tely reflect t~e results of my field analyses, observatLns and activities. Signed_~:::;::::::~~,---,-:~.:b.IS:~c:::::::~~==:----,..----­I certify that I \·Jitnessed these field analyses, concu with the statements in this block. Signed ---------------------f·1et hod of S h i prne n t to Labor a tor y_..-'6""!f-':Y._---:-""l:-':-S~ec-~'""~,_--=--=---:-~---:-:----,--:-:-,.--.-----------­T!-IIS f='ORH ACCOr·'PANIES ""Z.- SP.Dtum viClls vlith teflon·-1ined discs identified as: specimen ·:1 ; duplicate :1--- ; triplicate ; blank(s) and amber glass jug(s) with teflon-lined cap(s) identified as ----------and other container(s) (describe) identified as Containers are man:ed as follmvs to indicate preservation (circle): ------

No preservation; sample stored at room temperature (-20°C). Sample stored in an ice bath. Sample preserved with 3 mg tJa2o3s2/40 ml and stored at room temperature.

CERTIFICATE(S) OF SAr~PLE RECEIPT I (v1e) certify that this sample was transferred from~9»-1'K'> ~c,~">\-,'-< to

-·~~ \ at (location) ~'\S:) on ~~· ~'-~ -

(date & ~me) ~-yJ"?s, \\J..Ss- and that the statements in this block are correct.

Dispos. it ion of. ··.S _a_m.Tp"-le___ "''II- . Sea.l (s), I~t7.aT5t:rYes 19 .--- NoD . s· ~-- (s~· ~ ·· · /].._.,. -~~) -~~~~~~~=---~~~~--------------::_~:~_: ______ : _____________________ _ I (we) certify that this sample was transferred from to

, _______________ at {location) ________________ on

(date & ti~e) and that the statements in this block are correct. ------------Disposition of Sample . Seal (s) Intact: Yes D NoD Sigr,ature(s)

..... -... - -· ----- ------ c-

Page 69: LAB S9::SOO

'"'~''"'""~~""-""""''''""'·""""''"'~-.(~:'~--- -~-~'''"~"!:?:'.:::· ~ '"!:'"":!,'·';;•':;'.'::::.t".,..~' ';:~«•'<'-tt'f1mi'rtW2'"""'W'fC"'".~':. ';.'''".'" ••' · ··"''·.·::<:·· "'"'"r~nt'''TT»· 'J··--" -. '' 0 '''.,-'"''''"'"'''''••'···~~-~ • ..o:_·;o;t'""'"-~""~'""'i""""'MV""'"'\'?"'""""'""d''''-""" "''""~- -'·>'tt.""

ANALYSES REQUE~TED LAB. N9..: ':0._ ~l_, - _u:l~;<i .. .. I

1

PLEASE CHECK THE APPROPRIA1 30XES BELOH TO INDICATE THE TY\ F ,\1\;AL YTICAL SCREENS REQUIRED.

. HHENEVER POSSIBLE LIST SPECIFIC CQ}fPOUNDS SUSPECTED OR REOUIRED.

w ~

> w > w EXTRRCTRBLES H > H > E- H PURGERBLE ~ t-'

< E- < E-E- < ~ < 1-' E- ....... E-,_.] ~

,_::: ~ SCREEN < SCREEN <

~ ;::::; :::J :::J C' C' c C'

ALIPHATIC r:YDROCARBON SCREEN ALIPHATIC HYDROCARBOKS

ARO:L<\TIC E".lDROCARBON SCREEN CHLORINATED HYDROCARBO\' PESTICIDES

RA.LOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

l't.. GAS CHR0:1ATOGRAPH/HASS SPECTROHETER HYDROCAP.BON :fTEL SCREE::\

ORGANOPHOSPHATE PESTICIDES

""'""' POLYCHLORINATED B IPHE;.,"':'LS (PCB's)

I' POLY?WCLEAR AR0:1ATTC l:YllR()CARBONS

I

.•

SPECIFIC COMPOUNDS SPECIFIC COMPOUNDS

~ ·-\r-.\" c '-c ~ \-. (\ n' e:\ \.. ~\e ~e r ~ '( 'c ""'\ C\ c-e:\\-... , ~'-.l-

RHlARKS: l

~

ANALYTICAL RESULTS l COMPOUND

CONC- CONC- I ENTRATION COMPOUND El'TRATIO:l

r.tx~ <t/~"' \\)l.,.,__e \>~~·_\...,.~ ·re-+r"'cl C i. L-o-r- o ej::_( e-.-t, ONsL~j-I

~

~,..,.._:M\>....'(11' f./ u. rn Qr-~_::.._ G" {, P it.a -h ~{. e 1C__ ~ I'

V'~_:h ( ~.;,~ ~,,._'_,-\ ~ ~s i) o k. \or.. "n~ 0A._hl'Lio1} t, i.) 116:--.. lt OfY'Y'-vf ~ T

?/JA ~ ~ u-i)C">V- )).z-it- c.t• i'J

--o~r:~ ~~~ , inn- ( -( : ;#/II --;'{

DETECTION LHHT

RE?L\RKS:

CETRIFICATE OF A:\:\LYTICAL PERSON::-JEL

Sea1(s) Intact: Yes ~0 Seal(s) Broken ]:_-,v date . ----------------------analvs:rs~--tbis--I certify that I follov.led standard laboratory proccdurL'S on handling and

sample unless othenvise noted and that the statements in this block and the anahtical data ~ ~

on this page accu;ate05;f,lect the analytical rco.<l to for ~ ~'l~t'(/' ;I

/.

Date(s) ·of analys1.s 5 15 6 '/ • Anolysts · t~n;1ture . . "!f'?.4.JCL!:.:_._, · ,. I

I certify that I have revie\,'ed and concur \vith the , .1lvtica results for this sar:~p le .:md I \dth the stateJTPnr~ in this block. Revie\vers Signa:ur~~: ~} '/;·· L. · i

)~~--tv f./-~ . . ..

Page 70: LAB S9::SOO

RIC DATA: ORG1059B 11 SCANS 1 TO 1200 02/09/84 10:50:00 CALI: C020984 14 I

SAMPLE: ORG1059A RERUN. 1.5GRAM. 10 SEC. PURGE RANGE: G 1,1200 LABEL: N 0, 4.0 QUAN: A 0, 1.0 BASE: U 20, 3

100.0l 335 258560

i i ~

\ ' .; i .:r ., ~ ... " 378 "t

434

' j J I II¥ RIC I ~

~ J

1- J 1~~ ~ ~'¥.~ 214 ~'Z ~'-f

i-}\ ~ ·~ I ·~ ~

{' "4

,, ~

"'· I I I ~ i!J . u· ~ ~ I' .. .. i

.:.

I ~ JW uvv\. 635

863 976

200 400 600 800 1000 1200 SCAN 6:40 13:20 20:00 26:40 33:20 40:00 TIME

Page 71: LAB S9::SOO

100.0

RIC I

I . ..

I i

1 53 J - I ,·

RIC DATA: ORG1059 11 02/09/84 9:57:00 CALI: C020984 14 SAMPLE: ORG1059A. 5.0GRAMS. 1MIH. PURGE RANGE: G 1,1200 LABEL: N 0, 4.0 QUAH: A 0, 1.0 BASE: U 20, 3

335,

~ ~

~ t-

~ I,

I ...,. '6" '6-

122

't

1 ~ 198

~ ~

~

377

II ~ 1 n ·~X ~ <

'It- ~~

1Y ~

\ I II I\ I lll --~

I \ -~

. - ¥ - ---' --.-- 633

200 400 600 6:40 13:20 20:00

J ~ ~ ~ ~ I,

~

800 26:40

• SCANS 1 TO 1200

2559990

1000 1200 SCAH 33:20 40:00 TIME

Page 72: LAB S9::SOO

CERTIFICATE OF So i1 [3 Other _______ ---=---::::--------""='"--1

I·Jater Supply and/or Code No. ~~ - "Ye-~~"'-=> S~~:::~.(\~ ~~a·\"-)~1;.\.:...x:::. ~ Sample Type: ~·later D

City & County~\~~;~S\>ll..~ (~'->--~'\~ _ . Collected (date & time)~"2-;;; c:::f\;;>; ByTrJl;me) ~":,~~-.~,c.. pH= ; Conductivity= umho/cm at °C; Chlorine Residual= ------t Dissolved Oxygen= mg/1; Alkalinity= Flow Rate= SaGpling Location, f.lethods & Remarks (i.e. odJrs etc.) ------t

C..u\".e.c-\e~ ~o\ ~\o--e ~\~ s~~-'C... -~\'.."\-~ .. ~ ~~~~·

certify that the statements in this block a c ately fleet th& results of my field analyses, observati;.:-ns and activities. Signed~~~~~~~~~~~.....,....,.--:--~;------1 certify that I witnessed these field analyses, concu with the statements in this block. Signed --------------------1·1ethod of Shipment to Laboratory o-.....- -==\S '60

--~~~~~~--~--~~-~~~~-----------THIS FORtv1 ACCOi~PJl.NIES L- septum vials with teflon-lined discs identified as: soecimen c..... ; duplicate ·-z. ; triplicate ; blank(s) and amber glass jug(s) with teflon-lined cap(s) identified as ----------and other container(s) (describe) identified as Containers are man~ed as follows to indicate preservation (circle): ---------t' . ~Jo preservation; sample stored at room temperature (-20°C). P-ICE· Sample stored in an ice bath. -\ 2o3s2: Sample preserved with 3 mg Na2o3s2/40 ml and stored at room temperature.

CERTIFICATE(S) OF SAt~PLE RECEIPT _ I (1-..;e) certify that this sample \•laS transferred from"bo,;.~""t"-- ~~,~~ -:J \<._ to

r-· \--)~"'- ~~'\..t>--~~ at (location) ~Cv on (date & time) ~S\l-L:=\- \'GS.S: and that the statements in this block are correct.

"/

Disposition ~(Sa.mple~ oL- r ./ Seal(s) !?fac~; Yesff No 0 . ~·-, ~ ' ) '((Ji;-J(

~ ~ i~;~~~~~~~;?~~~ ;~ ~~t;;;~A~?--~------: ---------------- ----t~------------------------------- at (location) on (date & ti~e) and that the statements in this block are correct. ----------------Disposition of Sample Seal(s) Intact: Yes D No 0 Signature(s)

--- -- .. --.. ·-- ·---·-- ------·--· ort-

Page 73: LAB S9::SOO

I

PLEASE CHECK THE APPROPRIA'~." BOXES BELOW TO INDICATE THE Tl OF A..1\AJ~YTICAL SCREENS REQUIRED .

. HHENEVER POSSIBLE LIST SPECIFIC COl-fPOUNDS SUSPECTED OR REQUIRED.

w r ... ~

:> w > w EXTRRCTRBLES H :> H :> E-< H PURGERBLE E- H

< E- < E-E- < E- ~ H E- t-,...l z ,_..; ~ SCREEN < < SCREEN < ;::J c· ::?. ;:::)

0' ~ C"'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS

AROHATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES

HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

IY. GAS CHRO:'-LA.TOGRAPH/NASS SPECTROHETER liYDROC.\RBON Ft:EL SCREE:\ ( I ORGANOPHOSPHATE PESTICIDES

'1.' POLYCHLORINATED BIPi1ET\1'LS (PCB's)

'y POLYNUCLEAR AROHATIC liYDROCARBOl\S

SPECIFIC COMPOUNDS SPECIFIC COMPOUNDS

RD!ARKS:

ANALYTICAL RESULTS COMPOUND

CONC­ENTRATION COMPOUND

CO!\ C­ENTRA II ON

I' Oc• S':>; h fe _±_fie C of-+e-lrocUtro eli e._ pr,~..s .z.....f I

,,, DETECTIO:: LI~1IT

RCL.\F!KS:

CEIRIFICATE OF A~ALYTICAL PER~OXNEL

Sea1(s) Intact: Yes ~:o . Seal(s) Broken bv date I certify that I follov:ed standard laboratory: proccdu-;--;:;-s-;-;nll':''1nJl ing-and anai~·-sis---z;-r·-th{s-

sample unless othenvise noted and that the state8ents in this bl0ck and the analYtical data

on this page accurate}}. reflect the analytic2l r. «.,,11 ts for this sy.npl"'l/" /)

Date(s) of anal::sis .-;{);!{- { . Ana1yst::o ~i;.:nature U!'.d.t:t.i.t/d~_Y _______ ~---------· Icerti:'"y that I havett"E>\=ie'"'ed a:1d concur Hith the ;malytic3. r6u: ts for this sa~:ple and

Hith the stater;pnr~ in tllis block. Revie'''ers Signature: ~~j) / . 1( l7 e:;£ -~-/,_u--

I

Page 74: LAB S9::SOO

100.0

;,

RIC I II

1\..,

~ ~ ~

~

-.J! ...... ~

l ~ ~ ~

RIC DATA: ORG1060 123 02/09/84 13:09:00 CALI: C020984 14 SAMPLE: ORG1060A. 5GRAM. 5MIN PURGE RANGE: G 11 985 LABEL: N 01 4.0 QUAN: A 01 1.0 BASE: U 20~ 3

~ ('\.

$ ~ ;; ~ I ~

"V Q I \

~

~ ---156 "

~ ~ J.:.

'<.1

I 1.,;

~ l~ (~

14.. (j

'lie {'

l:. '1;:

~ j..,_

:t:: .. 'o' . -

{ I

217

200 6:40

292 340 406

400 13:20

600 20:00

704 774 830

800 26:40

SCANS 1 TO 985

271872

935

SCAN TIME

Page 75: LAB S9::SOO

~ ~ ::> ~ ::> ~ H ::> ...... ::> E- H PURGERBLE E- ......, <:; E- < t-E- < E- < H E- H '-,...J

~ ,....; ~ < SCREEN <

;:::J c ;:::J ;:::J C' C' C'

EXTRACT ABLES

SCREEN ALIPHATIC HYDROCARBON SCREEN ALIPilATIC HYDROCARBONS

r ARO}~TIC HYDROC.~BON SCREEN CHLO:Rll':ATED HYDROCARBON PESTlCilJES

HALOGt.::ATED HYDROCARBON SCREEN CHLORtWHENOXY ACID HERBICIDES

'y .. GAS CHRG::-1ATOGRAPH/H..;.ss SPECTROMETER HYDROCARBO;J rTEL SCREEN

ORGA;JOPHOSPHATE PESTICIDES

~ POLYCH: ORI;JATED BIPHH.1'LS (PCB' s)

}l POLY~ULLEAR ARmiATIC llYDRClCARBONS

SPECIFIC COMPOUNDS SPECIFIC COMPOUNDS

RPL'tRKS:

ANALYTICAL RESULTS COMPOUND

REHARKS:

CONC­ENTRATION COMPOUND

J

,., DETECTION LIHIT

CONC­ENTRATION

[)('t"'.SC~.l , I l

'I

t I

1---------------------------------·· CETRIFTCXfE OF A:\ALYTICAL PERSONNEL

Sea] (s) Intact: Yes No . Seal(s) Broken bv date I certify that I followed standard laboratory. pn)cec1un·-s-onlh-mclling and nnaY\-;-sisor-tT1fs-

sample unless othen.Jise noted and that the. state;;1ents in this block and the analYtical data

on this page accu:atel? r_ ~fleet the analytical resu~ts for t:~ samp-le///_ d {J Date(s) of analysl.s~/;5/tfV . An.::llysts s1gn~1ture /_A,~~_f£_~~-z;:.__f/, __________ _

Icertify that I have revie'Wedand concur with the :tnalytic.:11' J7est11 ts fozhi s sa::.p le nnd · •-lith the stateTIPnrs in this block. Reviewers Signaturt:: j/ ~ '] _ ·

f-/ I II fl-::712'1-- /---,/ L---------------------------L.~--_________ __

Page 76: LAB S9::SOO

TO: Environmc 83·10w -G nt DlVlSlon LABO~~)ORY_/._'c!J-ty{?~~-7_,_0_9--=3::..__ __ He a 1 th & pa rtment 7 ~' 1 c(3 P.O. Box 9b3- Crovm ·suilding RECEIV!£;§ :;0:·;~c:R Of\ /CJO?/ /J9r , Santa Fe, New Mexico 87504-0968 ATTErHION: ~'>\\15> ~,~,~-.J~'-BUREAU : (?'4Y~'}J £:, 1--'"2.-3.~

ALL COnTAINERS \·JHICH THIS

Samp 1 e Type: ~·Jater 0 I·Jater Supply

City & County ~~UL~~~~~--_q~~~~~~~~~~~---------------------4

Collected (date & time) t;Q\7"'2..-:=t ojSO -.:J ~c__ pH= ; Conductivity= umho/cm at 0

(; Chlorine Residual= ------t Dissolved Oxygen= mg/1; Alkalinity= ; Flow Rate= Sampling Location, r·1ethods & Remarks (i.e. odors etc.) -------t.

C<:>\\e c.\.c&_ $S,\ ~\~ ~\G~~1 ~u.~\v-ce

I certify that the statements in this b1ock ac

concu analyses, observatLns and activities. Signed __ ~~&.)::!~~___:~~~~~~"----:-----1 certify that I witnessed these field analyses, with the statements in this block. Signed -----------------------r~ethod of Shipment to ~aboratory 0\.;.-?t~~O T H I S FO Rivi AC COr~ PAN I E S ""2.- sept u m-·-v ,.,...::. a~l-'-s--..,,-.;--~-~J!0-1~ ~t-d:.:;:.:f"l o-n-_..,l....,.i -n c-d.--d:-:-i_s_c -s _,i,....d.-e-n..,...t -=-i ~"'"': i,....e-,d,--a s--: -------specimen 3 ; duplicate ?:> ; triplicate ; blank(s) ________ _ and amber glass jug(s) with teflon-lined cap(s) identified as.~~--------------and ether container(s) (describe) identified as Containers are maned as follm·JS to indicate preservation (circle): -----------

No preservation; samp1e stored at room temperature (-20°C). Sample stored in an ice bath. Sample preserved with 3 mg Na2o3s 2/40 ml and stored at room temperature.

CERTIFICATE(S) OF SAf~PLE RECEIPT . , I (we) certify that this sample \'.'as transferred from \y;.~"~ ~:;..,-··=~:"C"~\C. ... ~ to

"\~o'-'-~ '~~~ at (location) -~-ss~ on (date & ·~\me)~ \L. :;2-:-:t- \~'1.5 and that the statements in this block ar~_,.correct. Disposition~ Sample b'\L.._ . _seal (s) I~t;J: (Y(js 'kr· No 0 . Signature(s)'~ -&_),.. '"o"c.kh:-~--" ,~·2~<-<- ;(/LV I-.(~;)-~;~tif;-th~t-thi~-~~~-~~~-t~~~~f~~~~d-f~~~---t- - ---- -- - - to-

at {location) on 1------------------------------ ------------------------------(date & time) and that the statements in this block are correct. ---------------Disposition of Sample . Seal(s) Intact: Yes 0 No 0 Signature(s)

Page 77: LAB S9::SOO

100.0

RIC I II

~ ~

l'.~ l.tJ ~ '1:-

J ::::, .... \:j

~ 6 :t ~ ...., ~ ~~ . ~ "::: <...

~

L

RIC DATA: ORG1061 #1 02/09/84 14:13:00 CALI: C020984 14 SAMPLE: ORG1061A. 12GRAMS. 10 MIH PURGE RANGE: G 1~1000 LABEL: H 01 4.0 QUAN: A 01 1.0 BASE: U 20~ 3

(\

~ ~ .., ~ ~ ~ ~ ~

\,. 1::: ~ '{ J ~ ~

~ ~'I" ~ "' ~ ~ ~ ~

~ c'< ' " ~ ~ ~ '(1

~ ~ I t. '!-

" i ~ ~ I k I'( ~

/111 f\j {\ ~-

l.

l .,._ }.:! {'

217

200 6:40

316

c.. ~~

i 479

382 436. (\_ 526

400 13:20

638 688

600 20:00

800 26:40

SCANS

891

1 TO 1000

244480

974

1000 SCAN 33:20 TIME

Page 78: LAB S9::SOO

83-1062 -c c ?~PJ?.T iO: Env,r·urllilt.:lll..al ·.~nprovement Division

Health & Environment Department P.O. Box 968 - Crown Building Santa Fe, New Mexico 87504-0968 ATTENTION :·""})Q,\,)L*'-- ~,(",~~ ~

BUREAU: G'±-t~~:J:> 'Xk3'\Jlt .... v.ui..: l:ii·'SL U~~~s Code tJo. S0\(900

CERTIFICATE OF FIELD PERSONNEL Sample Type: ~Jater 0 Soil)S Other

Water Supply and/or Code No._~~~~~~-~~~~~~~~~~~~~~~~~~~~~r City & County~~~~~~~~+-~~~~~~~~~~~~----------------------; Collected (date & time)~Q.-25 c.'-~~

pH= ; Conductivity= umho/cm at °C; Chlorine Residual=--------1 Dissolved Oxygen= mg/1; Alkalinity= ; Flow Rate= Sampling Location, t~ethods & Remarks (i.e. odors etc.) . ------1

Lo~e~c.\. qa'- ~ \...:::u...>- \u~~..::.~-t'--<-E:.-

I certify that the statements in this block ace analyses, observati(·IIS and activities. Signed._~~~~~~~~~~~~'------,.---­I certify that I witnessed these field analyses, o and concu with the statements in this block. Signed -----------------~~ethod of Shipment to Laboratory t:>~ -:?ss~ TH I S FORM AC COMP AN I E S -z- sept um-v-,-=-. a~l-s-w-,"""'· t:>.h~t-e"'f l"o_n __ .,,..,...i n-e-d-;--;d-.-i -s c-s____,i-,d_e_n t;-i"f.,..,.i_e,..d -a--:s_: _____ _ specimen £\- ; duplicate 6.: ; triplicate ; blank(s) and amber glass jug(s) with teflon-lined cap(s) identified as ---------and other container(s) (describe) identified as Containers are man~ed as follows to indicate preservation (circle): ----------N · No preservation; sample stored at room temperature (-20°C).

-IC · Sample stored in an ice bath. P-Na 2o3s2: Sample preserved with 3 mg Na 2o3s2/40 ml and stored at room temperature.

CERTIFICATE(S) OF SAr~PLE RECEIPT I (we) certify that this sample was transferred from~···~ ~~.::.,r-....~,'-

. \ ")o-.,...~~\)."'-~ at (location) ~ u·~ on (dat-;& ti~;;?~ \~S) and that the statements in this block are correct.

Disposition o{~_Sample "'··C).)___ _ _.~al(s) In~};tQ·~YesO) No 0 . Signature(s) ~ .... _,.._-..w...-... .... "~ j".o.-..1\....~ • ~Ja-ZLs.-/lifl~_ ----------------------------~~----------------------~-------------------------------1 (we) certify that this samp~ was transferred from to

to

1 ________________ at (location) _____________________ on

(date & time) and that the statements in this block are correct. -------------Disposition of Sample . Seal(s) Intact: Yes 0 No 0 Signature(s)

Page 79: LAB S9::SOO

"-ANALYSES REQUf 'TED LAB. N~ -~--:, - \ () \.., '-.. _

PLEASE CHECK THE APPROPRIATE BOXES BELOW TO INDICATE THE TYPE OF ANALYTICAL SCREENS REQUIRED. '~ENEVER POSSIBLE LIST SPECIFIC COMPOUNDS SUSPECTED OR REQUIRED.

~ ~

:> ~ :> w EXTRACT ABLES H :> H :> E-< H PURGERBLE E-< H

< ~ < E-< E-< E-< < H E-< H E-<

~ ~ SCREEN ~ ~ SCREEN ::;J ::;J ::;J ::;J 0' 0' 0" 0'

ALIPHATIC HYDROCARBON SCREEN ALIPHATIC HYDROCARBONS

AROHATIC HYDROCARBON SCREEN CHLORINATED HYDROCARBON PESTICIDES

HALOGENATED HYDROCARBON SCREEN CHLOROPHENOXY ACID HERBICIDES

:r~. GAS CHROHATOGRAPH/}~SS SPECTROHETER HYDROCARBON FUEL SCREEN I ORGANOPHOSPHATE PESTICIDES

'f. POLYCHLORINATED BIPHENYLS (PCB's)

')( POLYNUCLEAR AROMATIC HYDROCARBONS f

SPECiriC COMPOUNDS SPECIFIC COMPOUNDS

'l'- ~ ~:,...._ '\0-1. ~~ 'c:rt' ~l\ ~- p ~ 1- -~-::_._t~~"oe-\~L~ o

REHARKS:

ANALYTICAL RESULTS CONC- CONC-

COMPOUND ENTRATION COMPOUND ENTRATION

Q ' ' (_j, .s \ \\.') tsv\ e_ ~ ~-\ \'!._ c:.:\d) [ /1-c e·-h---_ ] ftc:tc..L

~, .... :~ \)-<L~~-~--~ ; ..... ,..\. ~- '3Sf)"b {\.. ..so~ ..n'\. ~ \~~ LT ~- .frc. c/Lftn-o e.-.fl-a._z 7 -I !'a.. u..__ ,, A.J D ~, /J. _._o_Jj~ ri-i:/J ¥--

PJJA~ I Al~ 'J).JL fe<. if· D ' I

0<.-t<?'I~ I , > _1- 1·PPM --·:k DETECTION L HUT ! .k!£1 6

REHARKS:

'

CETRIFICATE OF ANALYTICAL PERSONNEL Seal(s) Intact: Yes No . Seal(s) Broken by _________________ date I certify that I followed standard laboratory procedurPs on hand 1 ing and analysiso(- this-

sample unless otherwise noted and that the statements in this block and the analytical data

on this page accuratel~r~eflect the analytical results for th~/amp 1//d_ Date(s) of analysis t ;fr.z/ . Analysts signature w ,t /~

and Icertify that I havee\dewed and concur with the analytical rest!'its for this sample

with the stateiTPnrs in this block. Reviewers Signature: /~---rJ~L

Page 80: LAB S9::SOO

100.0 19

RIC

IH :

' -

i

,.

RIC DATA: ORG1062 11 02/09/84 15:18:00 CALI: C020984 #4 SAMPLE: ORG-1062A. 10.2 GRAMS/ 10 MIN PURGE. RANGE: G 1, 808 LABEL: H 0, 4.0 QUAH: A 0, 1.0 BASE: U 20, 3

"· 1\._, r ~ ·if 1 ~ ~

~ 55 I{ 476

It 92-l~

273 312_ 3[9 _ ~6~L~ 569 217

100 3:20

200 6:40

300 10:00

400 13:20

500 16:40

600 20:00

637

SCANS 1 TO 808

700 23:20

.. 763

94080

800 SCAN 26:40 TIME