laboratory microchem silliker private limited, a-513 ... fibre gafta 2003 [10:0] is: 12711 - 1989...

Laboratory

Microchem Silliker Private Limited, A-513, Microchem House, TTC Industrial Area, Mahape, Navi Mumbai, Maharashtra

Accreditation Standard ISO/IEC 17025: 2005

Discipline Chemical Testing

Issue Date 17.03.2014

Certificate Number T-0696 Valid Until 16.03.2016

Last Amended on 28.03.2014

of 60

S.No. Product / Material of Test

Specific Test Performed Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

I FOOD & AGRICULTURAL PRODUCTS

1 ANIMAL FEED & FEED STUFFS

Moisture IS: 7874 (Part - I) 1975 (Reaffirmed 1990)

2 - 20 %

Ash IS: 7874 (Part - I) 1975

(Reaffirmed 1990)

2 - 30 %

Acid Insoluble Ash IS: 7874 (Part - I) 1975

(Reaffirmed 1990)

0.01 - 5 %

Crude Fat IS: 7874 (Part - I) 1975

(Reaffirmed 1990)

0.5 - 60 %

Crude Protein IS: 7874 (Part - I) 1975

(Reaffirmed 1990)

1 - 70 %

Crude Fibre IS: 7874 (Part - I) 1975

(Reaffirmed 1990) 2 -30 %

2 STIMULANT FOODS

(Tea, Coffee, Cocoa powder)

Moisture IS: 1164 – 1986 (Reaffirmed 2012)/ DGHS 2005 : Man 4, Clause 1.2,4.2,5.2

1 - 10 %

Ash IS: 1164 - 1986 (Reaffirmed 2012)/ IS: 13854 - 1994 (ISO 1575 - 1987)/ DGHS 2005 : Man 4,Clause1.3,4.4,5.3

0.1 - 10

Acid Insoluble Ash IS: 1164 - 1986 (Reaffirmed 2012)/ IS: 13857 - 1993 (ISO: 1577 - 1987)/ DGHS 2005 : Man 4, Clause1.5,4.5,5.5

0.01 - 2 %

Laboratory







of 60




Crude Fibre IS: 1164 – 1986 (Reaffirmed 2012)/ DGHS 2005 : Man 4, Clause5.8

1 - 30 %

Water Extract IS: 13862 – 1999 (ISO: 9768 - 1994)/ DGHS 2005 : Man 4, Clause1.7,5.6

5 - 80 %

Water Soluble Ash of Total Ash

IS: 13855 - 1993 (ISO : 1576 - 1988)/ DGHS 2005 : Man 4 , Clause1.4,5.4

5 - 80 %

Water Insoluble Ash IS: 13855 - 1993 ISO : 1576 - 1988)/ DGHS 2005 : Man 4 Clause 1.4

0.1 - 10 %

Alkalinity of Water Soluble Ash

IS: 13856 - 1993 (ISO: 1578 - 1975)/ DGHS 2005 : Man 4, Clause1.6,4.6

0.1 - 10 %

Solubility in Hot Water DGHS 2005 : Man 4Clause3.4.1

To pass the test

Caffeine AOAC 962.13 19th Edition (MC/SOP/INS/23,Issue No.02 , Issue date: 01-09-2013)

0.1 - 5 %

Description (Appearance, colour)

FSSAI 11th Ed Clause 2.10 IS 1164 : 1986 (Reaff. 2012) IS 3633 : 2003/ IS 1163:1992

Descriptive

Extraneous Matter/Impurities

MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

Present/Absent

Laboratory







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added colouring matter DGHS 2005 :

Man 8 Clause 4.1, 4.2

Present/Absent

solubility in cold water DGHS 2005 : Man 4 Clause 1.7

Descriptive

Total Catechins ISO:14502-1 :2005 0.01 - 30 % 3 SNACKS &

CONVENIENCE PRODUCTS

Moisture IS: 15271 - 2003/ DGHS 2005 : Man 3, Clause:2.0

0.5 - 30 %

Ash DGHS 2005 : Man 3Clause8.3

0.1 - 10 %

Fat IS: 15271 – 2003

0.1 - 60 %

Acid Insoluble Ash IS: 15271 – 2003

0.01 - 2 %

Acid Value of extracted fat IS: 15271 – 2003

0.01 - 5 %

Crude Fibre GAFTA 2003 [10:0]

IS: 12711 - 1989 (Reaffirmed 1994)

1 - 30 %

Total Sugar DGHS 2005 : Man 4, Clause6.4

IS: 6287 - 1985 (Reaffirmed 1999) 0.5 - 50 %

4 MEAT & MEAT

PRODUCTS Moisture AOAC 950.46 (19th edition)/

IS: 5960 (Part V) – 2001

1 - 80 %

Ash AOAC 920.153 (19th edition)

0.1 - 10 %

Fat DGHS 2005 : Man -6, Clause

2.1& IS:5960(P-III) 1970

0.1 - 40 %


IS: 2537 - 1995 (Reaffirmed 2009)/ IS: 2536 - 1995 (Reaffirmed 2009)/ FSSAI 11th Ed Clause 2.5, 2.6

Descriptive

Laboratory







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discolouration and excessive disintegration

IS: 2537 -1995 (Reaffirmed 2009)

Present/Absent

Foreign matter IS: 2536 - 1995

(Reaffirmed 2009) Present/Absent

IS: 2537 -1995

(Reaffirmed 2009)

IS:5960(P-III) 1970

pH ISO: 1842 - 1991 (E)

By pH Meter

2 - 10

Stains & Contamination from the container

IS 11747 – 1986 IS 10697 – 1983 IS 12541 – 1988

Present/Absent

5 SOFT DRINKS -

CARBONATED, NON CARBONATED

pH ISO: 1842 - 1991 (E) By pH Meter/ DGHS 2005 : Man 5, Clause15.2

2 - 8

Total Solids AOAC 950.27 (19th edition)/

IS: 5781 - 1993 ( Reaff. 2003 )

0.1 - 25 %

Total Sugar IS: 6287 - 1985 (Reaffirmed 1999)/ DGHS 2005 : Man 4Clause6.4/ Man 5Clause2.6

0.1 - 25 %

Caffeine AOAC 962.13 19th Edition (MC/SOP/INS/23 Issue No.02 , Issue date: 01-09-2013)

10 - 1000 mg/L

Total Soluble Solids IS: 13815 – 2010

0.1-20 %

Laboratory







of 60




Test for absence of resin (sulphur test)

FSSAI 11th Edition 2.10.6 Passes the Test

Acid Value IS: 548 (Part 1) 1964

(Reaffirmed 2010)

0.1 - 10

Hydroxyl number IS: 548 (Part 1) 1964

(Reaffirmed 2010) 10 - 100

6 NUT & NUT

PRODUCTS Moisture AOAC 925.40 (19th edition)/

DGHS 2005 : Man 5Clause20.1

0.1 - 25 %

Ash AOAC 950.49 (19th edition)

0.1 - 10 %

Fat IS: 3579 - 1966 (Reaffirmed 2000)/

GAFTA 2003 [3.0]

1 - 70 %


1 - 30 %

Acid Insoluble Ash GAFTA 2003 [13:0]

0.01 - 5 %

7 STARCH & STARCH

PRODUCTS Moisture IS: 4706 (Part II) – 1978

(Reaffirmed 2005)/ IS: 1485 – 1993

0.1 - 50 %

Ash IS: 4706 (Part II) – 1978 (Reaffirmed 2005)/ IS: 1485 – 1993

0.1 - 10 %

Acid Insoluble Ash IS: 4706 (Part II) – 1978 (Reaffirmed 2005)/ IS: 1485 – 1993

0.01 - 2 %

Crude Fibre IS: 4706 (Part II) – 1978

(Reaffirmed 2005)

1 - 20 %

Laboratory







of 60




pH of Aqueous Extract IS: 4706 (Part II) – 1978

(Reaffirmed 2005)

3 - 10

Starch IS: 4706 (Part II) – 1978

(Reaffirmed 2005)

2 - 99 %

Protein IS: 4706 (Part II) – 1978

(Reaffirmed 2005)

1 - 30 %

Alcoholic Acidity IS: 4706 (Part II) – 1978

(Reaffirmed 2005)

0.1 - 5mL of 1N NaOH per 100g


FSSAI 11th Ed Clause 2.4 Descriptive

IS:1158-1973

(Reaffirmed 2010)

Added colouring matter DGHS 2005 :

Man-8 Clause 4.1, 4.2

Present/Absent

Calcium Carbonate DGHS 2005 : Man-3Clause8.7

0.1 - 5%


IS:1158-1973(Reaffirmed 2010) Present/ Absent

IS:1155-1968(Reaffirmed 2010)&

DGHS Man-3, Clause1.2.1/

DGHS 2005 : Man-3Clause1.2.1/

IS:1005-1992(Reaffirmed 2010)/

IS:1009-1979(Reaffirmed 2010)

8 FRUIT &

VEGETABLE PRODUCTS

Moisture IS3882 - 1966(Reaffirmed 2010)/ IS: 5781 - 1993(Reaffirmed 2003)/ DGHS 2005 : Man 5 Clause4.1

1 - 95 %

Brix IS: 13815 – 2010

2 - 90° Brix

Laboratory







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Total Ash IS: 13846 - 2009/ IS: 3500 - 1966(Reaffirmed 2005)/ DGHS 2005 : Man 5 Clause11.3

0.1 - 10 %

Acid Insoluble Ash IS: 13846 - 2009/ IS: 3500 - 1966(Reaffirmed 2005)/ DGHS 2005 : Man 5 Clause5.3

0.01 - 2 %

Total Solids / Dry Matter Content

IS: 3882 - 1966(Reaffirmed 2001)/ IS: 5781 – 1993(Reaffirmed 2003) DGHS 2005 : Man 5 Clause3.5

5 - 99 %

Sodium Chloride (Salt) IS: 2860 - 1964 (Reaffirmed 2003)

DGHS 2005 : Man 5 Clause1.7

0.2 - 20 %


1 - 30 %

Drained weight IS: 2860 - 1964 (Reaffirmed 2003) /


30 - 90 %

Hydroxymethyl furfural (HMF)

ISO: 7466 - 1986 0.1 - 100 mg/Kg

Total Soluble Solids IS: 13815 - 2010/ IS: 2860 - 1964 (Reaffirmed 2003)/ DGHS 2005 : Man 5 Clause1.6

0.1 - 60 %

Water Insoluble Solids IS: 13845 – 2003

0.1 - 50 %

Added Sugar DGHS 2005 : Man 5 Clause2.6

0.5 - 80 %

Total Sugar DGHS 2005 : Man 4 ,Clause6.4 / Man 5, Clause2.6

0.5 - 80 %

Laboratory







of 60





IS: 5861 - 1993/ IS: 4624 - 1978 (Reaffirmed 2005)

Descriptive

IS: 14267(P-3) - 1995

FSSAI 11th Ed Clause 2.3

Extraneous matter IS: 4624 - 1978 (Reaffirmed 2005)/ IS: 3579 - 1966 (Reaffirmed 2000)/ DGHS 2005 : Man-3 clause -1.1.2

Present/Absent

Foreign matter DGHS 2005 : Man-3 clause1.1.2

Present/Absent

Added colouring matter DGHS 2005 : Man-8 clause4.1,4.2

Present/Absent

Drained weight DGHS 2005 : Man-5 Clause1.4

50 - 90 %

Solid pack DGHS 2005: Man-5 Clause2.9.4

50 - 90%

Liquid pack DGHS 2005 :Man-5 Clause2.9.4

30 -90 %

Acidity of extracted fat IS: 548(Part - I) – 1964

(Reaffirmed 2010)

0.05 - 5 %

Fruits and vegetable content

IS: 3500 – 1966 (Reaffirmed 2005)

1 - 90%

Dry fruit content IS 3500 – 1966 (Reaff. 2005)

1 - 50 %

Empty shells


0.01 - 10 %

Filled quantity of Container DGHS 2005 : Man-5 Clause1.3

70 - 99%

Non edible seeds MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

0.01 - 10 %

Laboratory







of 60




Oil content IS: 3509 – 1966

(Reaffirmed 2003)

0.1 - 99 %

Peel in suspension IS: 5861 – 1993

1 - 20 %

Peroxidase Test DGHS 2005 :Man-5 Clause17.5

Positive/ Negative

Reducing Sugar DGHS 2005 : Man-4 Clause6.4.1

0.1 - 95 %

Sugared raisins MC/SOP/CHE/03 Issue No. 01,

Issue date: 02-04-2014

0.01 - 10 %

Unopened shells MC/SOP/CHE/03 Issue No. 01,

Issue date: 02-04-2014 0.01 - 10 %

9 MILK & DAIRY

PRODUCTS AND INFANT FOODS

Moisture IS: 16072 - 2012/ IS: 2785 – 1979(Reaffirmed 2010)/ DGHS 2005 : Man 1 Clause2.1.1, 4.1.1, 5.1.1, 9.1.1, 11.0.2, 12.02, 15.1, 16.1

1 - 90 %

Total Solids IS: 14542 - 1998/ IS: 2802 - 1964(Reaffirmed 2004)/ IS: 13334 (Part II) 1992/ IS: 1479 (Part II) 1961(Reaffirmed 2009)/ DGHS 2005 : Man 1 Clause1.6

8 - 99 %

Total Ash IS: 1479 (Part II) 1961 (Reaffirmed 2009)/ IS: 12299 - 1998/ IS: 14433 - 2007 Annex. B

0.1 - 10 %

Acid Insoluble Ash GAFTA 2003 [13:0]/ DGHS 2005: Man 1 Clause 9.7.0 / IS: 12299 - 1998 / IS: 14433 - 2007 Annex. C

0.01 - 2 %

Laboratory







of 60




Milk Fat IS: 12299 - 1998 / IS: 11721- 2013/ DGHS 2005 : Man 1 Clause1.7.1,2.02,2.1.2,3.2,5.1.2,4.2,6.3.0,8.2.0,9.2.0,10.03,11.0.5,12.07,13.03,15.2,16.2/ IS: 3509 - 1966(Reaff. 2003)/ IS: 2785 – 1979(Reaff. 2010)/ IS: 10484 - 1983(Reaff. 1999)/ IS: 2802 - 1964(Reaff. 2009)/ IS: 1479 (Part II) – 1961 (Reaff. 2009)

0.1 - 99 %

SNF IS: 1479 (Part I) – 1960 (Reaffirmed 2003)/ IS: 12299 - 1998/ DGHS 2005 : Man 1 Clause11.0.5

5 - 10%

Milk Protein IS: 1479 (Part II) - 1961(Reaffirmed 2009)/ DGHS 2005 : Man 1 Clause2.1.3,6.5.0

1 - 50 %

Crude Fibre GAFTA 2003 [10:0]/

AOAC 962.09 (19th edition)

0.5 - 10 %

Added Starch IS: 1479 (Part I) – 1960 (Reaffirmed 2003)/ DGHS 2005 : Man 1 Clause1.2.2

Present / Absent

Added Formaldehyde IS: 1479 (Part II) – 1961(Reaffirmed 2009)/ DGHS 2005 : Man 1 Clause1.3

Present / Absent

Laboratory







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Added Sugar IS: 1479 (Part II) – 1961(Reaffirmed 2009)/ DGHS 2005 : Man 1 Clause1.2.1.0

Present / Absent

Urea in Milk and Milk products

IS: 1479 (Part II) – 1961(Reaffirmed 2009)/ DGHS 2005 : Man 1 Clause1.2.4.0

Present / Absent

pH IS: 1479 (Part II) – 1961(Reaffirmed 2009)/ DGHS 2005 : Man 1 Clause15.5

3 - 8

Salt IS: 1479 (Part II) – 1961(Reaffirmed 2009)/ DGHS 2005 : Man 1 Clause11.0.8

0.1 - 10 %

Carbonates DGHS 2005 : Man 1 / IS: 1479

(Part I) - 1960(Reaffirmed 2003)

Present / Absent

Sucrose DGHS 2005 : Man 1 Clause1.2.2.1

0.5 - 60 %

Lactose DGHS 2005 : Man 1 Clause15.6,17.0/ IS: 1479 (Part II) - 1961(Reaffirmed 2009)

0.5 - 80 %

Aflatoxin M1 Journal of Analytical Chemistry Vol 55 No.10.2000 PP 929-932 (MC/SOP/INS/22, Issue No.02 , Issue Date:04-11-2013 )

0.5 - 10000 mcg/kg

Melamine

ISO/TS 15495 – 2010

0.1 - 1000 mg/kg

Laboratory







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IS:1165-2002 / IS: 2785 – 1979(Reaffirmed 2010)/ IS: 2802 – 1964(Reaffirmed 2009)/ IS: 4884 - 1968(Reaffirmed 1999)/ IS: 5126 – 1996(Reaffirmed 1999)/ IS:15757-2007/ IS:14433-2007/ FSSAI 11th Ed Clause 2.1

Descriptive Test

Added colour DGHS 2005 : Man-8clause 4.1,4.2

Present / Absent

Extraneous matter/ Impurities

IS:1656-2007/ IS:14433 2007 Present / Absent

Solubility Index IS: 12759 – 1989 (Reaffirmed 1999)/ DGHS Man-1 Clause9.7.3

0.1 - 10 mL

Solubility IS: 12759 – 1989 (Reaffirmed 1999)/ DGHS Man-1 Clause9.7.3

90 - 99.9%

Baudouin test IS: 548 (Part I) 1964

(Reaffirmed 2010)

Positive/Negative

ButyrometerRefractometer at 40°C

IS: 548 (Part I) 1964 (Reaffirmed 2010)

40 - 50

Casein in protein DGHS 2005 : Man-1 Clause16.0

90 - 99.9 %

Citric acid IS: 1497 (P-II) 1961

(Reaffirmed 2009)

0.01 - 10 %

Free fatty acid ml/0.1NNaOH/gm.

IS: 548 (Part I) 1964 (Reaffirmed 2010)

0.01 - 10 %

Melting point IS: 548(Part - I) – 1964

(Reaffirmed 2010)/ DGHS: 2005 Man – 2 Clause 8.0

20 - 50°C

Laboratory







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Mineral Oils IS: 548(Part - I) – 1964 (Reaffirmed 2010)/ DGHS: 2005 Man – 2 Clause 28.0

Present / Absent

Reichert value IS: 548 (Part I) 1964

(Reaffirmed 2010)

10 - 50

Titrable acidity (0.1N NaOH / 10gm solids not Fat)

IS: 11766 – 1986 (Reaffirmed 2003)/ ISO 6092:1980

0.1 - 50 ml

Weight/Volume DGHS 2005 : Man-1 Clause6.3.0 400 - 600 g/L 10 FOOD GRAINS,

PULSES, CEREALS, SEEDS & RELATED PRODUCTS

Moisture IS: 1155 - 1968(Reaffirmed 2010)/ IS: 1009 - 1979(Reaffirmed 2010)/ IS: 3579 - 1966 (Reaffirmed 2000) / AOAC 925.40-19th edition/ DGHS 2005 : Man 3 Clause2.0

0.5 - 50 %

Total Ash IS: 1155 - 1968(Reaffirmed 2010)/ IS: 1009 - 1979(Reaffirmed 2010)/ DGHS 2005 : Man 3 Clause8.3/ GAFTA 2003 [12:0]

0.1 - 10 %

Acid Insoluble Ash IS: 1155 - 1968(Reaffirmed 2010)/ IS: 1009 - 1979(Reaffirmed 2010)/ DGHS 2005 : Man 3 Clause8.4/ GAFTA 2003 [13:0]

0.01 - 2 %

Crude Fibre IS: 1155 - 1968(Reaff. 2010)/


1 - 30 %

Gluten Content IS: 1155 - 1968(Reaffirmed 2010)/ IS: 1009 - 1979(Reaffirmed 2010)/ DGHS 2005 : Man 3 Clause8.5.1,10.1

0.5 - 30 %

Laboratory







of 60




Alcoholic acidity IS: 1155 - 1968(Reaffirmed 2010)/ IS: 1009 - 1979(Reaffirmed 2010)/ DGHS 2005 : Man 3 Clause8.6

0.1 - 5 mL of 1N NaOH per 100g or 0.1 - 5%

Uric acid IS: 4333 - 1970 Part 5 (Reaffirmed 2005)/ DGHS 2005 : Man 3 Clause3.0

0.1 - 100 mg/Kg

Oil Content IS: 3579 - 1966 (Reaff. 2000)/

AOAC 922.06 (19th edition)

0.1 - 30 %

Acid value of extracted fat IS: 3579 - 1966

(Reaffirmed 2000)

0.05 - 5 %

Starch IS: 4706 (Part II) –

1978(Reaffirmed 2005)

0.2 - 60 %

Extraneous matter IS: 4333 (Part I) – 1996 (Reaffirmed 2012)/ IS: 3579 - 1966 (Reaffirmed 2000)

0.05 - 10 %

Other foodgrains IS: 4333 (Part I) – 1996 (Reaffirmed 2012)/ IS: 3579 - 1966 (Reaffirmed 2000)

0.05 - 10 %

Damaged grains IS: 4333 (Part I) – 1996 (Reaffirmed 2012)/ IS: 3579 - 1966 (Reaffirmed 2000)

0.05 - 10 %

Discoloured grains IS: 4333 (Part I) – 1996 (Reaffirmed 2012)/ IS: 3579 - 1966 (Reaffirmed 2000)

0.05 - 10 %

Laboratory







of 60




Insect damaged grains IS: 4333 (Part I) – 1996 (Reaffirmed 2012)/ IS: 3579 - 1966 (Reaffirmed 2000)

0.05 - 10 %

Shrivelled / Shrunken / Broken

IS: 4333 (Part I) – 1996 (Reaffirmed 2012)/ IS: 3579 - 1966 (Reaffirmed 2000)

0.05 - 10 %

Foreign matter IS: 4333 (Part I) – 1996 (Reaffirmed 2012)/ IS: 3579 – 1966 (Reaffirmed 2000)

0.05 - 10 %

Admixture IS: 4333 (Part I) – 1996 (Reaffirmed 2012)/ GAFTA 2003 (35.0)

0.05 - 10 %

Weevilled grain IS: 4333 (Part I) – 1996

(Reaffirmed 2012)

0.05 - 10 %



DGHS 2005 : Man-8 clause 4.1,4.2

IS: 2813 – 1995 (Reaffirmed 2010)/ IS: 4684 – 1983

Added colour DGHS 2005 : Man-8 clause 4.1.,4.2

Present/ Absent

Added starch IS 4706 (Part 1) 1978 (Reaffirmed 1995)

Present/ Absent

Laboratory







of 60




Admixture (Unwholesome substances)

DGHS 2005 : Man-3, Clause1.1.2.1/ IS: 2813 – 1995 (Reaff. 2010)

Present/ Absent

Cocoa powder DGHS 2005 :Man-4 Clause 15.7

1 - 20%

Foreign matter IS: 2813 – 1995(Reaffirmed 2010)/

DGHS 2005 : Man-3 Clause1.1.2.1

0.01 - 20 %

Extraneous Matter/ Impurities

IS: 1485 – 1993 (Reaffirmed 2005)/

Present/Absent

AOAC 2001.11 (19th edition)/

IS: 1484 – 1974 (Reaffirmed 2005)/ IS: 46864- 1983/ DGHS 2005 : Man-3 Clause1.2.1

Hexane AOAC 89-6, 1475-1482 (MC/SOP/INS/40, Issue No. 02, Issue Date : 09-12-2013 )

0.1 - 1000mg/kg

Oxalic acid MC/SOP/CHE/04 Issue No. 01 & Issue Date 02.04.2014 (based on Handbook of analysis and QC for fruit and vegetable products by S Ranganna)

0.01 - 10 %

Protein AOAC 2001.11 (19th edition)

0.1 - 90 %

Solubility IS: 12769 - 1989

(Reaffirmed 2004) 70 - 99 %

Laboratory







of 60




11 BAKERY & CONFECTIONERY PRODUCTS

Moisture IS: 12711 - 1989/ IS: 1011 - 2002/ IS: 6287 – 1985 (Reaffirmed 1999)/ DGHS 2005 : Man 4 Clause14.2,15.2

1 - 50 %

Acidity of extracted fat IS: 1011 - 2002/ IS: 12711 – 1989

(Reaffirmed 1994)

0.1 - 3 %

Total Solids IS: 12711 - 1989(Reaff. 1994)/

IS:1483-1988(Reaff. 2005)

50 - 99 %

Protein AOAC 2001.11 (19th edition)

0.05 - 10 %

Fat IS: 12711 - 1989/ IS: 6287 – 1985

(Reaffirmed 1999)

0.1 - 50 %

Ash IS: 12711 – 1989 (Reaffirmed 1994)/ DGHS 2005 : Man 4 Clause1.3

0.1 - 5 %

Acid Insoluble Ash IS: 12711 – 1989 (Reaffirmed 1994)/ IS: 1011 - 2002/ IS: 1483 – 1988 (Reaffirmed 1994)/ IS: 6287 – 1985 (Reaffirmed 1999)/ DGHS 2005 : Man 4 Clause13.3

0.01 - 2 %

Crude Fibre IS: 12711 – 1989 (Reaffirmed 1994)/ IS: 1483 – 1988

1 - 30 %

Brix IS: 13815 – 2010

10 - 80 °Birx

Sugar/ Sucrose IS: 6287 – 1985(Reaff. 1999)/

DGHS 2005 : Man 4 Clause14.6 10 - 99 %

Laboratory







of 60




Reducing Sugar DGHS 2005 : Man 4

Clause14.7,15.2/ IS: 6287 – 1985

0.1 - 95 %

Starch IS: 4706 (Part II) –


0.2 - 50 %

Sulphated ash AOAC 900.02 (19th edition)/ IS: 6287 – 1985(Reaffirmed 1999)/ DGHS 2005 : Man 4 Clause13.2

0.01 - 2 %

Alcoholic Acidity IS: 12711 – 1989 (Reaffirmed 1994)

0.1 - 5 mL of 1N NaOH per 100g or 0.1 - 3%

Cocoa Solids DGHS 2005 : Man-4 Clause15.7

0.1 - 30%

Edible wholesome substances


0.1 - 50 %

Extraneous Matter/ Impurities

IS: 6747 - 1981(Reaff. 2005)/ IS: 1163 - 1992 (Reaff. 2009)

Present/Absent

Gum Content DGHS 2005 : Man-4 Clause14.6 &

IS:6747-1981

0.1 - 30 %

Milk Fat IS: 1163 - 1992

(Reaffirmed 2009)

0.1 - 50%

Milk Solids DGHS 2005 : Man-4 Clause15.4/

IS:1163-1992(Reaffirmed 2009)

0.1 - 20 %

Vegetable fat AOAC 996.06 (19th edition)

Present/Absent

Laboratory







of 60




12 HONEY & HONEY PRODUCTS

Specific Gravity IS: 4941 - 1994 (Reaffirmed 2002)

1 - 1.5

Moisture IS: 4941 – 1994

(Reaffirmed 2002)

0.1 - 20 %

Total Reducing Sugar IS: 4941 - 1994

(Reaffirmed 2002)

30 - 80 %

Ash IS: 4941 - 1994

(Reaffirmed 2002)

0.1 - 10 %

Acidity IS: 4941 - 1994(Reaff. 2002)

0.1 - 10 %

Fructose Glucose Ratio IS: 4941 - 1994

(Reaffirmed 2002)

0.8 - 1.5

Fiehes Test (qualitative) IS: 4941 - 1994

(Reaffirmed 2002)

Present / Absent

Aniline Chloride test (qualitative)

DGHS 2005:Man-4 Clause6.6.2 Present / Absent

Sucrose IS: 4941 - 1994

(Reaffirmed 2002)

30 - 80 %

Hydroxymethyl furfural (HMF)

IS: 4941 - 1994 (Reaffirmed 2002)

1 - 200 mg/Kg

Foreign matter IS: 4941 - 1994

(Reaffirmed 2002)

Present / Absent

extraneous matter IS: 4941 - 1994 (Reaffirmed 2002)

Present / Absent

Laboratory







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Colour IS: 4941 - 1994

(Reaffirmed 2002)

Descriptive

Chloramphenicol Journal of Chromatography B, 807 (2004) 343-356 (MC/SOP/INS/27, Issue No. 02, Issue Date: 23-09-2013)

0.1 - 10000 mcg/Kg

Sulfonamides (Sulfadiazine, Sulfamethoxazole, Sulfamerazine, Sulfadimidine, Sulfadimethoxzine, Sulfapyridine, Sulfathiazole, Sulfamethizole, Sulfaguanidine)

Journal of Chromatography A, 1205 (2008) 10-516 (MC/SOP/INS/33, Issue No. 02, Issue Date: 27-09-2013)

2 - 10000 mcg/Kg

Tetracycline group (Oxytetra, tetracycline, chlortetracycline and doxycycline, 4-Epitetracyclin, 4-Epioxytetracyclin and 4-Epichlortetracyclin)

AOAC 995.09 19th Edition (MC/SOP/INS/31, Issue No. 02, Issue Date : 23-09-2013)

10 - 10000 mcg/kg

Nitrofuran metabolite (AHD,AMOZ,AOZ,SEM)

Journal of Chromatography B, 807 (2004) 343-356 & EC 657 (MC/SOP/INS/28, Issue No. 02, Issue Date: 25-12-2013)

1 - 10000 mcg/kg

Streptomycin Journal of Chromatography A, 830 (1999) 345-351 (MC/SOP/INS/29, Issue No. 02, Issue Date : 04-11-2013)

10 - 10000 mcg/kg

Laboratory







of 60




13 OIL, FATS AND RELATED PRODUCTS

Moisture IS: 3508 – 1966 (Reaffirmed 2003)/ IS: 548 (Part I) 1964 (Reaffirmed 2010)

0.01 - 5 %

Acid value IS: 548 (Part I) 1964

(Reaffirmed 2010)

0.01 - 20 %

Free Fatty Acid IS: 548 (Part I) 1964

(Reaffirmed 2010)

0.01 - 10 %

Saponification Value IS: 548 (Part I) 1964

(Reaffirmed 2010)

80 - 300

Unsaponifiable Matter IS: 548 (Part I) 1964

(Reaffirmed 2010)

0.1 - 10 %

Iodine Value IS: 548 (Part I) 1964

(Reaffirmed 2010)

1 - 200

Peroxide Value IS: 548 (Part I) 1964

(Reaffirmed 2010)

0.1 - 25 mEq/Kg

Argemone Oil Test IS: 548 ( Part II) 1976

(Reaffirmed 2010)

Present / Absent

Beilliers Turbidity Temperature

IS: 548 ( Part II) 1976 (Reaffirmed 2010) / DGHS 2005 : Man 2 Clause14.0

10 - 80 °C

Melting Point IS: 548 ( Part II) 1976 (Reaffirmed 2010) / DGHS 2005 : Man 2 Clause8.0

20 - 80 °C

Baudouin Test IS: 548 ( Part II) 1976

(Reaffirmed 2010) / DGHS 2005 : Man 2 Clause15.0

Present / Absent

Laboratory







of 60




Ricebran oil IS: 548 ( Part II) 1976 (Reaffirmed 2010) / DGHS 2005 : Man 2 Clause18.0

Positive / negative at 10%

Linseed oil IS: 548 ( Part II) 1976 (Reaffirmed 2010) / DGHS 2005 : Man 2 Clause19.0


Detection of Adulterants IS: 548 ( Part II) 1976

(Reaffirmed 2010)

Positive / negative

Castor oil IS: 548 ( Part II) 1976

(Reaffirmed 2010)


Cotton Seed oil IS: 548 ( Part II) 1976

(Reaffirmed 2010)

Positive / negative at 0.1%

Cloud point DGHS 2005 : Man 2 Clause17.0

5 - 20 °C

Flash Point DGHS 2005 : Man 2 Clause6.0

200 - 300 °C

Anisidine Value ISO 6885 – 2006

1 - 45

Specific Gravity IS: 548 (Part I) 1964

(Reaffirmed 2010)

0.9 - 1.5

Mineral Oil DGHS 2005 : Man 2 Clause28.0

Present / Absent


IS:10633-1999 (Reaffirmed 2004)/ FSSAI 11th Ed Clause 2.2

Descriptive Test

Butyro - refractometer reading at 40°C

IS: 548(Part - I) - 1964 (Reaffirmed 2010)

30 - 80

DGHS 2005 : Man-2 Clause5.0

Laboratory







of 60




Refractive index at 40°C IS: 548(Part - I) - 1964 (Reaffirmed 2010)/ DGHS: 2005 Man - 2 Clause5.0

1.4300 - 1.4800

Fat IS: 548(Part - I) - 1964 (Reaffirmed 2010)/ DGHS:2005 Man - 2 Clause39.0

0.01 - 100 %

Hexane Journal of AOAC 89-6: 1475-1482 (MC/SOP/INS/40, Issue No. 02, Issue Date: 09-12-2013)

0.1 - 100mg/kg

Olive pomance oil test DGHS 2005 : Man-2 Clause25.0

Positive / Negative

Oryzanol content AOAC 984.20 (19th edition)

0.1 - 10 %

Polenske value IS: 548(Part - I) - 1964 (Reaffirmed 2010)/ DGHS: 2005 Man - 2 Clause13.0

1 - 50

Rancidity IS: 548(Part - I) - 1964 (Reaffirmed 2010)/ DGHS: 2005 Man – 2 Clause37.0

Descriptive Test

Semi Siccative oil Test DGHS 2005 : Man-2 Clause26.0

Positive / Negative

Sesame seed oil test DGHS 2005 : Man-2 Clause15.0

Positive / Negative

Sesame(til) oil IS: 548(Part - I) – 1964

(Reaffirmed 2010)

Positive / Negative

Teaseed oil test DGHS 2005 : Man-2 Clause24.0

Positive / Negative

Volatile matter IS: 548(Part - I) - 1964

(Reaffirmed 2010) 0.01 - 25 %

Laboratory







of 60




14 SPICES & CONDIMENTS, SPICE OILS & OLEORESINS, SAFFRON

Moisture Content IS: 1797 - 1985 (Reaffirmed 2009) / ASTA 2.0 / ASTA 2.1, 4th Edition 1997

0.5 - 20 %

Moisture & volatile matter IS: 5453 (Part I) 1996

(Reaffirmed 2009)

0.5 - 15 %

Extraneous matter IS: 1797 – 1985

(Reaffirmed 2009)

0.05 - 10 %

Total Ash IS: 1797 – 1985 (Reaffirmed 2009) / IS: 5453 (Part II) 1996 / ASTA 3.0, 4th Ed 1997

2 - 10 %

Acid Insoluble Ash IS: 1797 - 1985 (Reaffirmed 2009)/ IS: 5453 (Part II) 1996 (Reaffirmed 2012)

0.01 - 2 %

Sieve Analysis ASTA 10.0, 4th Ed 1997

0.1 - 99 %

Bulk Density ASTA 25.0, 4th Ed 1997

0.3 - 0.8 g/mL

Water insoluble ash IS: 1797 - 1985

(Reaffirmed 2009)

0.1 - 10 %

Crude fiber IS: 1797 - 1985 (Reaffirmed 2009)/ ASTA 7.0 4th Ed 1997

1 - 40 %

Starch ASTA 8.0, 4th Ed 1997

0.1 - 80 %

Salt IS: 1797 – 1985 (Reaffirmed 2009)

0.2 - 20 %

Laboratory







of 60




Volatile Oil ASTA 5.0/ IS: 1797 -


0.5 - 25 %

Capsaicin ASTA 21.3, 4th Ed 1997

1 - 1000000 SHU

Extraneous matter IS: 1797 - 1985 (Reaffirmed 2009)/ IS: 5453 (Part I) 1996 (Reaffirmed 2009)

0.1 - 10 %

Defective seeds DGHS 2005 : Man 3 Clause1.1.2.1

0.1 - 10 %

Insect damaged seeds DGHS 2005 : Man 3 Clause1.1.2.1

0.1 - 10 %

Curcumin ASTA 18.0,4th Edition 1997 /

Food Chemical Codex 7th Ed.

1 - 10 %

Lead Chromate DGHS 2005 : Man 10

Clause15.6

Present / Absent

Colour ASTA 20.1, 4th Ed 1997

1 - 200

Alcohol soluble extract IS: 1797 - 1985 (Reaffirmed 2009)/ ASTA 9.0,4th Edition 1997

0.5 - 25 %

Non-volatile ether extract IS: 1797 - 1985 (Reaffirmed 2009)

0.1 - 30 %

Cold water soluble extract IS: 1797 - 1985 (Reaffirmed 2009)

0.1 - 30 %

Bitterness, expressed as direct reading of the absorbance of picrocrocine at 257 nm, on dry basis

IS: 5453 (Part II) 1996 (Reaffirmed 2012)

20 - 80

Laboratory







of 60




Colouring strength, expressed as reading of the absorbance of crocine at 440 nm, on dry basis


50 - 200

Solubility in cold water IS: 1797 – 1985 (Reaffirmed 2009)

30 - 70 %

Safranal, expressed as direct reading of the absorbance at 330nm


20 - 50

Floral waste IS: 5453 (Part I) 1996 (Reaffirmed 2012)

0.1 - 15 %


IS:1798-2010/ IS:1908 - 2008/ IS: 13242 -1991/ IS: 4452 - 2009/ IS: 5453(P-I) – 1996 FSSAI 11th Ed Clause 2.9

Descriptive


DGHS 2005 : Man-10 Clause 2.0 Present / Absent

Added colouring matter DGHS 2005 : Man-8 Clause 4.1, 4.2/ IS: 13242 – 1991

Present / Absent

Added starch DGHS 2005 : Man-10 Clause 15.5

Present / Absent

Coal tar dyes DGHS 2005 : Man-8 Clause 4.1, 4.2

Present / Absent

Allylisothiocyanate DGHS2005: Man-10Clause12.0

0.1 - 10%

Laboratory







of 60




ammoniaccum resin IS: 7807 - 1975 (Reaff. 2003)

0.01 - 10 %

any other foreign resin IS: 7807 - 1975 (Reaffirmed 2003)

0.01 - 10 %

Black and Broken berries IS:1798-2010

0.01 - 10 %

Broken fruits, seed & fragments


0.01 - 10 %

Calcium as calcium oxide IS:1797-1985(Reaffirmed 2009) & DGHS Man-10 Clause8.0

0.01 - 10 %

Colophony and galbanum resin

IS: 7807 - 1975 (Reaffirmed 2003) 0.01 - 10 %

Curcuminoid ASTA.18, 4th Ed 1997

0.01 - 10 %

Damaged/discoloured fruits/Slices


0.01 - 20 %

Defective Rhizomes MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

0.01 - 10 %

Emty& malformed cpasules by count


0.01 - 10 %

Foreign seeds (edible seeds, vegetable matter, Argemone, Maxicana L seeds)


0.01 - 10 %

Mineral oil

DGHS 2005 : Man-10 Clause19.0 Present / Absent

Peroxidase test

DGHS 2005 : Man-5 Clause 17.5 Positive / Negative

Scorched, toasted & baked particles


Present / Absent

Laboratory







of 60




Test for argemone oil

DGHS 2005 : Man-10 Clause 18.0 Present / Absent

Headless, Tendrils, Khokar and Mother cloves


0.01 - 10 %

Immature & Shrivelled capsules


0.01 - 10 %

Light Seeds/Berries MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

0.01 - 10 %

Nutmeg in mace MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

0.01 - 10 %

Peperine content IS:1798-2010

0.01 - 10 %

P-hydroxy benzyl isothiocyanate

DGHS 2005 : Man-10 Clause12.0 0.1 - 10 %

Seed coatings MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

0.01 - 10 %

Split fruits MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

0.01 - 10 %

Total Nitrogen IS:5453(P-I) -1996 (Reaffirmed 2009)

0.01 - 20 %

Unripe & marked fruits MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

0.01 - 10 %

15 Ready-to-eat and

Ready-to-cook food Moisture USDA CLG-M01.03, 2009 0.1 - 90 %

Laboratory







of 60




16 SUGAR & BY PRODUCTS

Moisture IS: 15279 - 2003/ IS: 1151 - 2003/ DGHS 2005 : Man 4 Clause7.2

0.02 - 10 %

Total Ash IS: 12923 - 1990/ DGHS 2005 : Man 4 Clause7.3

0.1 - 5 %

Acid insoluble ash IS: 12923 - 1990/ DGHS 2005 : Man 4 Clause7.3

0.01 - 2 %

Water insoluble matter IS: 15279 – 2003

0.01 - 5 %

Sugar / Sucrose IS: 15279 - 2003/ DGHS 2005 : Man 4 Clause7.4

90 - 99.98 %

Reducing Sugar DGHS 2005 : Man 4 Clause 6.4.1/ IS: 15279 – 2003

0.01 - 1 %

Sulphur dioxide IS: 15279 - 2003/ DGHS 2005 : Man 4 Clause7.5

0.1 - 100 mg/Kg

Sulphated Ash IS: 15279 – 2003

0.01 - 5 %

Starch IS: 15279 – 2003

0.1 - 5 %


IS:4 941 – 1994 (Reaffirmed 2002)/ IS:1152-2003/ IS: 873 - 1974 (Reaffirmed 2010) FSSAI 11th Ed Clause 2.7

Descriptive

Foreign matter DGHS 2005 : Man-5 Clause1.1

Present / Absent

Assay /Purity of Sugar & Sweeteners

Food Chemical Codex 7th Ed. 90 - 100 %

Calcium oxide

DGHS 2005 : Man-4 Clause7.7

1 - 1000mg / 100g

Laboratory







of 60




Coaltar Colour DGHS 2005 : Man-8 Clause 4.1, 4.2

Present / Absent

Conductivity DGHS 2005 : Man-4 Clause7.6.3.3

10 - 500 mho/cm2

Extraneous matter IS: 4941 – 1994 (Reaffirmed 2002)/ IS:1151-2003/ IS:12923 – 1990

0.01 - 10 %


IS: 4941 - 1994 (Reaffirmed 2002)/ IS: 5982-2003

Present / Absent

Identification test for Saccharine

Food Chemical Codex 7th Ed. Passes the test

Limit tests in Saccharine Food Chemical Codex 7th Ed.

Passes the test

Melting point DGHS 2005 : Man 2 Clause 8.0

200 - 250°C

Methanol Journal of AOAC 89-6: 1475-1482 (MC/SOP/INS/40, Issue No. 02, Issue Date: 09-12-2013)

0.1 - 1000 mg/kg

Solubility IS 15279 – 2003

Passes the test

Total solid content DGHS 2005 : Man-4 Clause12.0

0.1 - 99.9 %

Total starch DGHS 2005 : Man-4 Clause11.0 0.1 - 99.9 %

17 ALCOHOLIC DRINKS & BEVERAGES

Residue on evaporation IS: 3752 – 2005

0.01 - 25 %

Ethyl Alcohol IS: 3752 – 2005

1 - 60 %

Ash content

IS: 3752 – 2005

0.1 - 2 %

Laboratory







of 60




Total Acidity IS: 3752 – 2005

0.01 - 10 %

Volatile Acidity IS: 3752 – 2005

1 - 150 g/100L

Furfural IS: 3752 – 2005

1 - 20 g/100L

Esters IS: 3752 – 2005

1 - 100 g/100L

Higher Alcohols IS: 3752 – 2005

1 - 1000 g/100L

Aldehydes IS: 3752 – 2005

0.1 - 50 g/100L

Methyl alcohol IS: 3752 – 2005

Positive / Negative at 0.1 %

Added colouring matter DGHS 2005 : Man-8 Clause 4.1, 4.2

Present / Absent

Foreign matter MC/SOP/CHE/03 Issue No. 01, Issue date: 02-04-2014

Present / Absent

18 SODIUM CHLORIDE,

SALT, IODIZED SALT & FORTIFIED SALTS

Moisture IS: 7224 - 2006/ IS: 253 - 1985 (Reaffirmed 2009)

0.1 - 10 %

Matter soluble in water other than sodium chloride

IS: 7224 - 2006/ IS: 253 - 1985 (Reaffirmed 2009)

0.1 - 5 %

Water insoluble substances IS: 7224 - 2006/ IS: 253 - 1985 (Reaffirmed 2009)

0.1 - 5 %

Sodium Chloride content IS: 7224 - 2006/ IS: 253 - 1985 (Reaffirmed 2009)

90 - 100 %

Laboratory







of 60




Iodine content IS: 7224 – 2006

5 - 100 mg/Kg

Colour IS:253-1985 (Reaffirmed 2009)

Descriptive


IS:253-1985 (Reaffirmed 2009)

Present / Absent

Matter insoluble in HCl IS:253-1985 (Reaffirmed 2009)

0.01 - 10 %

pH IS:253-1985 (Reaffirmed 2009)

2 - 10

Solubility IS:253-1985 (Reaffirmed 2009)

0.01 - 100 %

Calcium in Salt IS: 7224 – 2006

0.01 - 0.15%

Sulphate IS: 7224 – 2006

0.01 - 0.60 %

Magnesium IS: 7224 – 2006

0.01 - 0.10 %

Alkalinity IS: 7224 – 2006

0.01 - 0.15 %

Iron IS: 7224 – 2006

10 - 1000 mg/kg

19 Seafood Moisture DGHS 2005 : Man-6 Clause2.2

0.01 - 90 %

Ash insoluble in HCl DGHS 2005 : Man-6 Clause2.2

0.01 - 10 %


IS:2237-1997(Reaffirmed 2009) Present / Absent

pH (after incubation at 37°C for 7 days)

ISO: 1842 - 1991 (E) By pH Meter

2 - 10

Laboratory







of 60




Total Volatile Base Nitrogen DGHS 2005 : Man-6 Clause1.2 1 - 1000 mg/100g Chloramphenicol Journal of Chromatography B, 807

(2004) 343-356 (MC/SOP/INS/27, Issue No.02, Issue Date: 23-09-2013)

0.1 - 10000 mcg/Kg

Sulfonamides (Sulfadiazine, Sulfamethoxazole, Sulfamerazine, Sulfadimidine, Sulfadimethoxzine, Sulfapyridine, Sulfathiazole, Sulfamethizole, Sulfaguanidine)

MC/SOP/INS/32,Issue No. 02, Issue Date : 27-09-2013

10 - 10000 mcg/Kg

Tetracycline group (Oxytetra, tetracycline, chlortetracycline and doxycycline, 4-Epitetracyclin, 4-Epioxytetracyclin and 4-Epichlortetracyclin)

AOAC 995.09 19th Edition (MC/SOP/INS/30, Issue No. 02, Issue Date: 23-09-2013)

50 - 10000 mcg/kg

Nitrofuran metabolite (AHD,AMOZ,AOZ,SEM)

Journal of Chromatography B, 807 (2004) 343-356 & EC 657 (MC/SOP/INS/28, Issue No. 02, Issue Date: 25-12-2013)

1 - 10000 mcg/kg

Streptomycin Journal of Chromatography A, 830 (1999) 345-351 (MC/SOP/INS/29, Issue No. 02, Issue Date: 04-11-2013)

10 - 10000 mcg/kg

Laboratory







of 60




Histamine Journal of Chromatography A, 1032 (2004) 79-85 (MC/SOP/INS/26,Issue No. 02, Issue Date: 17-09-2013)

50 – 10000 mg/kg

Trimethoprim MC/SOP/INS/39,Issue No. 02,

Issue Date: 23-09-2013

1 – 2000µg/kg

Oxolinic acid MC/SOP/INS/53, Issue No. 02,

Issue Date: 06-01-2014

10 – 1000µg/kg

Furaltadone Journal of Chromatography B, 807 (2004) 343 - 356 (MC/SOP/INS/57, Issue No. 02, Issue Date: 25-12-2013)

0.5 - 1000 µg/kg

Furazolidone Journal of Chromatography B, 807 (2004) 343 - 356 (MC/SOP/INS/57, Issue No. 02, Issue Date: 25-12-2013)

0.5 - 1000 µg/kg

Nitrofurantoin Journal of Chromatography B, 807 (2004) 343 - 356 (MC/SOP/INS/57, Issue No. 02, Issue Date: 25-12-2013)

0.5 - 1000 µg/kg

Nitrofurazone Journal of Chromatography B, 807 (2004) 343 - 356 (MC/SOP/INS/57, Issue No. 02, Issue Date: 25-12-2013 )

0.5 - 1000 µg/kg

20 Other food products

and ingredients Description (Appearance, colour)


Acid Insoluble matter

DGHS 2005 : Man-3 Clause8.4 0.01 - 10 %

Laboratory







of 60




Ash insoluble in HCl

IS 1164 : 1986 (Reaff. 2012) 0.01 - 10 %

CO2 IS:1159-1981(Reaffirmed 2010)

0.1 - 20 %

Cocoa butter DGHS 2005 :Man-4 Clause4.3.1

0.1 - 20 %

Free from creases & folds MC/SOP/CHE/03 Issue No. 01,

Issue date: 02-04-2014

Present / Absent

Extraneous

Matter/Impurities

IS:1164-1986(Reaffirmed 2012) Present / Absent

Moisture

(in Catechu and Gelatin)

IS 5719 - 2005 0.1 - 30 %

Nitrogen content AOAC2001-11 (19th edition)

0.01 - 20 %

Tannin content MC/SOP/CHE/04 Issue No. 01 & Issue Date 02.04.2014 (based on Handbook of analysis and QC for fruit and vegetable products by S Ranganna )

0.01 - 10 %

Total ash DGHS 2005 Man 3 Clause8.3

0.1 - 20 %

Alcohol insoluble residue IS: 1797 - 1985 (Reaffirmed 2009)

0.01 - 10 %

Water insoluble residue IS: 1797 - 1985 (Reaffirmed 2009)

0.01 - 10 %

21 MINERALS &

METALS in Food Products

Sodium AOAC 985.35 (19th edition)

0.1 - 1000 mg/kg

Potassium AOAC 985.35 (19th edition)

0.1 - 1000 mg/kg

Calcium AOAC 985.35 (19th edition) 0.1 - 1000 mg/kg

Phosphorous AOAC 995.11 (19th edition) 50 - 1000 mg/100g

Laboratory







of 60




Iron EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.01 - 1000 mg/kg

Zinc EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.01 - 1000 mg/kg

Copper EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.01 - 1000 mg/kg

Magnesium AOAC 985.35 (19th edition)

0.1 - 1000 mg/kg

Manganese EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.01 - 1000 mg/kg

Selenium Journal of AOAC International Vol. 94, No. 4, 2011 (MC/SOP/INS/36,IssueNo.02, Issue Date : 08-03-2014)

0.01 - 1000 mg/kg

Iodine EN 15111 – 2007

0.01 - 1000 mg/kg

Nickel EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.01 - 100 mg/Kg

Aluminium EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.01 - 100 mg/Kg

Tin EPA METHOD 200.2, 6020

(MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.005 - 100 mg/kg

Laboratory







of 60




Antimony EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.005 - 100 mg/kg

Arsenic EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.005 - 100 mg/kg

Cadmium EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.005 - 100 mg/kg

Chromium EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.01 - 100 mg/Kg

Lead EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No. 02, Issue Date: 20-08-2013)

0.01 - 100 mg/kg

Mercury EPA METHOD 200.2, 6020


0.01 - 100 mg/kg

22 NUTRITIONAL

LABELING & ANALYSIS (all categories of food products)

Energy / Calories FAO Food & Nutrition Paper 77, 2003

40 - 900 Kcal / 100g

Carbohydrates AOAC 986.25 (19th edition)

0.1 - 99 %

Total Fat IS: 1164 - 1986 (Reaffirmed 2012)/ IS: 1163 - 1992 (Reaffirmed 2009)/ IS: 6287 - 1985(Reaffirmed 1999)/ DGHS 2005 : Man 6 Clause2.1/ Man 4 Clause15.3/ GAFTA 2003 [3:0]/ AOAC 996.01 (19th edition)

0.1 - 99 %

Laboratory







of 60




Saturated Fat AOAC 996.01 / 996.06

(19th edition)

0.1 - 100 %

Monounsaturated Fatty Acids (MUFA)

AOAC 996.01 / 996.06 (19th edition)

0.1 - 100 %

Polyunsaturated Fatty Acids (PUFA)

AOAC 996.01 / 996.06 (19th edition)

0.1 - 100 %

trans Fat AOAC 996.01 / 996.06

(19th edition)

0.1 - 100 %

Individual Fatty Acids (C4 to C20)

AOAC 996.01 / 996.06 (19th edition)

0.1 - 100 %

Protein GAFTA 2003 [4:0]/ A

OAC 2001.11 (19th edition)

0.1 - 90 %

Cholesterol AOAC 994.10 (19th edition)

1 - 1000 mg/100g

Sugars IS: 6287 - 1985(Reaffirmed 1999)/ DGHS 2005 : Man 4 Clause14.7 & Man 5 Clause2.6

0.1 - 95 %

Total Dietary Fibre AOAC 985.29 / 991.43 (19th

edition)

0.1 - 95 %

Soluble Dietary Fibre AOAC 991.43 (19th edition)

0.1 - 95 %

Insoluble Dietary Fibre AOAC 991.43 (19th edition) 0.1 - 95 %

Laboratory







of 60




23 Food &Agri Products (All categories of foods: raw, processed food and any other agricultural products)

VITAMINS

Vitamin A AOAC 974.29 / 2001.13 (19th

edition)

50 - 10000 mcg/100 g

Vitamin E AOAC 981.17 & EN 12822 (MC/SOP/INS/18, Issue No. 02, Issue Date : 07-08-2013)

0.5 - 1000 mg/kg

Vitamin D2 AOAC 981.17 & EN 12822 (MC/SOP/INS/18, Issue No. 02, Issue Date : 07-08-2013)

0.5 - 1000 mg/kg

Vitamin D3 AOAC 981.17 & EN 12822 (MC/SOP/INS/18, Issue No. 02, Issue Date : 07-08-2013)

0.5 - 1000 mg/kg

Vitamin C AOAC 967.21 (19th edition)

1 - 1000 mg/kg

EN 14130 : 2003

0.5 - 1000 mg/100g

Vitamin B1 EN 14122 - 2003 (MC/SOP/INS/43, Issue No. 00, Issue Date : 16-07-2012)

1 - 1000 mg/kg

Vitamin B2 EN 14152 - 2003 (MC/SOP/INS/43, Issue No. 00, Issue Date : 16-07-2012)

1 - 1000 mg/kg

Vitamin B3 EN 15652 - 2003 (MC/SOP/INS/44, Issue No. 02, Issue Date: 06-01-2014)

1 - 1000 mg/kg

Vitamin B6 EN 14663 - 2003 (MC/SOP/INS/45, Issue No. 02, Issue Date: 06-01-2015)

1 - 1000 mg/kg

Laboratory







of 60




Vitamin B9 Application note of R-Biopharm for analysis of Folic Acid by HPLC (MC/SOP/INS/07, Issue No.02, Issue Date: 17-06-2013)

0.01 - 1000 ppm

Vitamin B5 Journal of Chromatography A, 778 (1997), 247-253 (MC/SOP/INS/05, Issue No. 01, Issue Date: 08-03-2013)

1 - 1000 mg/kg

Vitamin B12 AOAC 2011.08 (MC/SOP/INS/04, Issue No. 02, Issue Date: 13-10-2013)

0.001 mcg/g - 1 g/ g

Biotin EN 15607-2009

0.01 to 100 µg/100gm

Aflatoxins

Aflatoxin B1

AOAC 2005.08 (19th edition) 0.5 - 1000 µg/kg

Aflatoxin B2


Aflatoxin G1


Aflatoxin G2


Ochratoxin A


Naturally Occurring Toxins

Saffrole Journal of Ethnopharmacology, 102 (2005) 269-274 (MC/SOP/INS/17, Issue No.02, Issue Date: 19-08-2013)

2.5 - 1000 mg/kg

Agaric Acid Mycotoxin in fruits vegetables RivkaBarkai-Golan Nachman Paster (MC/SOP/INS/17, Issue No.02, Issue Date: 19-08-2013)

50 - 1000 mg/kg

Laboratory







of 60




Hypercene INA method 107.001 (MC/SOP/INS/17,Issue No.02, Issue Date: 19-08-2013)

1 - 1000 mg/kg

Hydrocyanic Acid EN - 1971L020 (MC/SOP/INS/17,Issue No.02, Issue Date: 19-08-2013)

Qualitative

Sugar Profile Sucrose

AOAC 980.13 (19th edition) 0.05 - 100 %

Glucose

AOAC 980.13 (19th edition) 0.1 - 100 %

Fructose

AOAC 980.13 (19th edition) 0.1 - 100 %

Maltose

AOAC 980.13 (19th edition) 0.1 - 100 %

Lactose

AOAC 980.13 (19th edition) 0.1 - 100 %

Antioxidents BHA AOAC 983.15


10 - 1000 mg/kg

BHT AOAC 983.15 (MC/SOP/INS/25, Issue No. 02, Issue Date: 04-09-2013)

10 - 1000 mg/kg

TBHQ AOAC 983.15 (MC/SOP/INS/25 Issue No. 02, Issue Date: 04-09-2013)

10 - 1000 mg/kg

Laboratory







of 60




Water Activity MC/SOP/CHE/02, Issue No. 02, Issue Date: 10-02-2014

0.1 - 1 Aw

Salt as NaCl MC/SOP/CHE/01, Issue No. 02, Issue Date: 26-09-2013

0.02 - 60 %

AOAC 986..26 (19th edition)

0.1 - 99%

Sulphur dioxide AOAC 990.28 (19th edition)

10 - 1000 mg/kg

DGHS 2005 : Man 5 Clause17.7 / Man 8 Clause 1.5

Acidity IS: 13844 - 2003/ IS: 11766 – 1986 (Reaffirmed 2003)/ IS: 1479 (Part I) 1960 (Reaffirmed 2003)/ IS: 2802 – 1964 (Reaffirmed 2009)/ IS: 2860 - 1964 (Reaffirmed 2009)/ AOAC 940.15 (19th edition)/ DGHS 2005 : Man 1 Clause9.3.0 / Man 5 Clause2.4

0.1 - 10 %

pH ISO: 1842 - 1991 (E) By pH Meter/ DGHS 2005 : Man 5 Clause 2.3/ IS: 2860 : 1964 (Reaffirmed 2008)/ IS: 12711 – 1989 (Reaffirmed 1994)/ IS: 4706 (Part II) – 1978(Reaffirmed 2005)/ IS: 1483 - 1988(Reaffirmed 2005)

2 - 10

Laboratory







of 60




Peroxide value IS: 15271 - 2003/ IS: 548 (Part I) 1964 (Reaffirmed 2010)/ IS: 3508 - 1966(Reaffirmed 2003)/ IS: 12711 – 1989(Reaffirmed 1994)

0.1 - 20 mEq / Kg

24A

PESTICIDES in Fruits, Vegetable, Food and Agri.products (Fruits: Grapes, Pomangrantes etc. Vegetables: Okra, Chilli etc Agri Products: Rice, Soybeanetc.)

Organochlorine (OC) AOAC 2007.01 19th Edition (MC/SOP/INS/34,Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Aldrin (expressed as Dieldrin)

Chlordane (cis& trans)

Chlorothalonil

DDT (all isomers, sum of p,p´-DDT, o,p´-DDT, p-p´-DDE and p,p´-TDE (DDD) expressed as DDT)

Dicofol (sum of p, p´ and o,p´ isomers)

Dieldrin (see Aldrin)

Endosulphan (All isomers, sum of alpha- and beta-isomers and endosulphan sulphate expressed as endosulphan)

Endrin

HCH (sum of isomers, except the gamma isomer)

Laboratory







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Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor)

AOAC 2007.01 19th Edition (MC/SOP/INS/34,Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Lindane (gamma-HCH)

Organophosphorus (OP) AOAC 2007.01 19th Edition (MC/SOP/INS/34,Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

4-bromo-2-chlorophenol (metabolite of Profenophos)

Acephate

Chlorfenvinphos

Chlorpyriphos Chlorpyriphos methyl Diazinon Dichlorvos

Dimethoate (Including Omethoate)

Edifenphos Ethion Etrimphos Fenitrothion

Fenthion (fenthion and its oxigen analogue, their sulfoxides and sulfone expressed as parent)

Iprobenphos

Malathion (sum of malathion and malaoxon expressed as malathion)

Methamidophos Monocrotophos

Omethoate (refer to Dimethoate)

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Oxydemeton methyl (sum of oxydemeton methyl and demeton-S-methylsulfone expressed as oxydemeton methyl)

AOAC 2007.01 19th Edition (MC/SOP/INS/34,Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Parathion ethyl

Parathion methyl (sum of Parathion methyl and paraoxon methyl expressed as Parathion methyl)

Phenthoate

Phorate (sum of phorate, its oxygen analogue and their sulfones expressed as phorate)

Phosalone Phosphamidon Pirimiphos-methyl Profenophos Propetamphos Quinalphos Temephos Thiometon

Triazophos

Synthetic Pyrethroids (SP) AOAC 2007.01 19th Edition (MC/SOP/INS/34,Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Allethrin and Bioallethrin Bifenthrin

Cyfluthrin (including other mixtures of constituent isomers sum of isomers)

Cypermethrin (including other mixtures of constituent isomers sum of isomers)

Deltamethrin

Laboratory







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Ethofenprox (Etofenprox) AOAC 2007.01 19th Edition (MC/SOP/INS/34,Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Fenpropathrin

Fenvalerate&Esfenvalerate (sum of RR & SS, Rs and SR isomers)

Lambda-cyhalothrin Permethrin (sum of isomers) tau- Fluvalinate

Transfluthrin

Triazines AOAC 2007.01 19th Edition (MC/SOP/INS/34,Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Atrazine

Flufenzine

Simazine

Acrylamino acid fungicides AOAC 2007.01 19th Edition

(MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Benalaxyl including other mixtures of constituent isomers including Benalaxyl-M (sum of isomers)

Metalaxyl&Metalaxyl-M Oxycarboxin

Propanil

Carbamates AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Bendiocarb Benfuracarb Benomyl (see carbendazim) Carbaryl

Carbofuran (sum of carbofuran and 3-hydroxy-carbofuran expressed as carbofuran)

Laboratory







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Carbosulfan AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Dazomet (Methylisothiocyanate resulting from the use of dazomet and metam)

Fenobucarb

Indoxacarb (sum of R and S isomers)

Iprovalicarb

Methomyl and Thiodicarb (sum of methomyl and thiodicarb expressed as methomyl)

Propoxur Thiobencarb (Benthiocarb)

Thiodicarb (see Methomyl)

Pyrimidines AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Fenarimol

Triazoles AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Cyazofamid Bitertanol Difenoconazole Flusilazole Hexaconazole Myclobutanil Paclobutrazol Penconazole Propiconazole Tebuconazole

Triadimefon (sum of triadimefon and triadimenol)

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Imidazole AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Fenamidone

Iprodione

Oxazole AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Famoxadone

Phthalimide AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Captafol

Captan

Benzimidazole AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Carbendazim (Including Benomyl)

Thiophanate-methyl

Nicotinoids AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Acetamiprid

Clothianidin (see thiamethoxam)

Imidacloprid Thiacloprid

Thiamethoxam (sum of thiamethoxam and clothianidin expressed as thiamethoxam)

Morpholine AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Dimethomorph

Tridemorph

Laboratory







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Substituted Thiourea AOAC 2007.01 19th Edition


0.01 - 1000 mg/kg

Difenthiuron

Diuron (Diuron including all components containing 3,4- dichloroaniline moiety expressed as 3,4-dichloroaniline)

Iodosulfuron-methyl (iodosulfuron-methyl including salts, expressed as iodosulfuron-methyl)

Isoproturon Linuron Lufenuron

Pencycuron

Benzoylphenyl Urea AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Flufenoxuron

Strobilurin AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Azoxystrobin Kresoxim methyl Pyraclostrobin

Trifloxystrobin

Phenyl Pyrazole AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Fipronil (sum of fipronil + sulfone metabolite (MB46136) expressed as fipronil)

Laboratory







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Chlorantraniliprole

Pyrazole AOAC 2007.01 19th Edition


0.01 - 1000 mg/kg

Fenpyroximate

Nitrophenyl ether AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Oxyfluorfen Dinitroaniline Pendimethalin

Trifluralin

Anilide/acetanilide and chloroacetanilide

AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Alachlor Butachlor Carboxin

Flufenacet (sum of all compounds containing the N fluorophenyl-N-isopropyl moiety expressed as flufenacet equivalent)

Metolachlor (with S-Metolachlor)

Novaluron

Miscellaneous AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg

Abamectin (sum of avermectin B1a, avermectinB1b and delta-8,9 isomer of avermectin B1a)

Azadirachtin Bifenazate Buprofezin

Cartap hydrochloride

Laboratory







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Chlorfenapyr AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg Diflubenzuron Dithianon Dodine Emamectin Benzoate Fenazaquin Flubendiamide Forchlorfenuron (CPPU) Hexythiazox Isoprothiolane Mandipropamid Metribuzin

Milbemectin (sum of MA4+8,9Z-MA4, expressed as milbemectin)

Oxadiazon Propargite Pyriproxyfen

Spinosad (Sum of Spinosyn A+D)

Spiromesifen Trichlorfon Tricyclazole Chlorobenzilate Formothion Aldicarb Fluchloralin Sulfosulfuron Ethoxysulfuron Chlorimuron-ethyl Diclofop-methyl Pretilachlor Methabenzthiazuron Imazethapyr Cyhalofop-butyl Triallate Anilophos

Laboratory







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Fenoxy-prop-p-ethyl AOAC 2007.01 19th Edition (MC/SOP/INS/34, Issue No.02, Issue Date: 27-09-2013)

0.01 - 1000 mg/kg clodinafop-propanyl Kitazin (Iprobenfos) Cymoxanil Quizalofop-ethyl Chlorfenopyr Metiram (CS2) Carpropamid Oxadiargyl Pyrazosulfuron ethyl

Clomazone

Dithiocarbamates (Mancozeb, Maneb, Propineb, Metiram, Thiram, Zineb and Ziram collectively estimated as CS2)

NRCG - EURL-SRM, VERSION 7.1 NOV 2013 (MC/SOP/INS/12,Issue No.02, Issue Date: 18-07-2013)

0.1 - 10000 mg/kg

24B PESTICIDES IN

Fruits, Vegetable, Food and Agri.products (Fruits: Grapes, Pomegranates etc. Vegetables: Okra, Chilli etc. Agri. Products: Rice, Soybean etc.)

Dinocap (sum of dinocap isomers and their corresponding phenols expressed as dinocap) and Meptyldinocap

NRCG - EURL-SRM, VERSION 7.1 NOV 2013 (MC/SOP/INS/14, Issue No.02, Issue Date: 25-09-2013)

0.01 - 1000 mg/kg

Plant Growth Regulators NRCG - EURL-SRM, VERSION 7.1 NOV 2013 (MC/SOP/INS/11,Issue No.02, Issue Date: 11-12-2013)

0.01 - 1000 mg/kg Gibberellic acid

1-Naphthylacetic acid (alphanapthyl acetic acid)

2,4-D (sum of 2,4-D and its

esters expressed as 2,4-D)

6-Benzyl adenineA Mepiquat Chloride Ethephon Paraquat Diquat

Chlormequat Chloride

(CCC)

Laboratory







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Homobrassinolide NRCG - EURL-SRM, VERSION 7.1 NOV 2013 (MC/SOP/INS/11,Issue No.02, Issue Date: 11-12-2013)

0.01 - 1000 mg/kg

Fosetyl-Al (sum fosetyl + phosphorous acid and their salts, expressed as fosetyl)

Uracil

Inorganic compound

Sulphur 184-B, BASF, Agricultural research

Station

0.5 - 10000 mg/kg

Hydrogen cyanamide (Cyanamide including salts expressed as cyanamide)

Analytical Letters vol 37, no.9 1981-1989,2004

0.05 - 10000 mg/kg

Polar Compounds

Glufosinate-ammonium (sum of glufosinate, its salts, MPP and NAG expressed as glufosinate equivalents)

NRCG - EURL-SRM, VERSION 7.1 NOV 2013 (MC/SOP/INS/41,Issue No.02, Issue Date: 28-12-2013)

0.01 - 1000 mg/kg

Glyphosate II WATER

1 Drinking Water, Raw Water, Source Water, Packaged Drinking Water, Packaged Natural Mineral Water, Water for Food Processing Industries, Domestic Water, Irrigation Water, Distilled Water, Swimming pool water and

Colour IS: 3025 Part 4 - 1983 (Reaffirmed 2006)/ APHA 22nd Edition 2012 2120 B

1 - 70 Units

Odour IS: 3025 Part 5 - 1983 (Reaffirmed 2006)/ IS: 3025 Part 6 - 1983 (Reaffirmed 2002)/ APHA 22nd Edition 2012 2150

Agreeable

Laboratory







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Effluent Water, ETP/STP Water, water from any other source excluding drinking water Packaged Drinking Water Packaged Natural Mineral Water Raw water, Source Water, Drinking Water Water for Food Processing Industry

Taste IS: 3025 Part 7 - 1984 (Reaffirmed 2006)/ IS: 3025 Part 8 - 1984 (Reaffirmed 2002)/ APHA 22nd Edition 2012 2160-C

Agreeable

Turbidity IS: 3025 Part 10 - 1984 (Reaffirmed 2002)/ APHA 22nd Ed. 2012 2130 B

0.1 - 10 NTU

pH IS: 3025 Part 11 - 1983 (Reaffirmed 2002)/ APHA 22nd Ed. 2012 4500-H+ B

2 - 10

Total Dissolved Solids IS:3025 Part 16 – 1984 (Reaffirmed 2002)/ APHA 22nd Ed. 2012 2540 C

1 - 1000 mg/L

Total Suspended Solids IS: 3025 Part 17 - 1984 (Reaff. 2006)/ APHA 22nd Edition 2012 2540 D

1 - 1000 mg/L

Calcium IS: 3025 Part 40 - 1991 (Reaffirmed 2003)/ APHA 22nd Edition 2012 3500-Ca B/ISO 17294 -2003 Part 1 and 2

0.1 - 1000 mg/L

Magnesium IS: 3025 Part 46 - 1994

(Reaff. 2003) 0.1 - 1000 mg/L

APHA 22nd Edition 2012 3500- Mg B

ISO 17294 -2003 Part 1 and 2

Laboratory







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Electrical Conductivity APHA 22nd Edition 2012 2510 B 0.1 - 50000 µs/cm

IS: 3025 Part 14 – 1984 (Reaff. 2006)

Total Hardness APHA 22nd Edition 2012 2340 C 1 - 1000 mg/L

IS: 3025 Part 21 - 1983 (Reaffirmed 2009)

Alkalinity IS: 3025 Part 23 - 1986 (Reaffirmed 1998)/ APHA 22nd Edition 2012 2320 B

1 - 1000 mg/L

Chloride IS: 3025 Part 32 – 1988 (Reaffirmed 2003)/ APHA 22nd Ed. 2012 4500-Cl-B

0.1 - 10000 mg/L

Sulphate IS: 3025 Part 24 - 1986 (Reaffirmed 2003)/ APHA 22nd Ed. 2012 4500-SO4

2-

1 - 10000 mg/L

Oil & Grease IS: 3025 Part 39 - 1991/

APHA 22nd Edition 2012 5520

0.1 - 100 mg/L

Nitrate IS: 3025 Part 34 - 1988 (Reaffirmed 2003)/ APHA 22nd Ed. 2012 4500-NO3

-

0.1 - 100 mg/L

Fluoride IS: 3025 Part 60 – 2008

0.1 - 1000 mg/L

COD IS: 3025 Part 58 - 2006/

APHA 22nd Edition 2012 5220

Min. 5 mg/L

BOD IS: 3025 Part 44 - 1993 (Reaffirmed 2003)/ APHA 22nd Edition 2012 5210

Min.10 mg/L

Laboratory







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Cyanide IS: 3025 Part 27 Clause 2 - 1986 (Reaffirmed 1998)/ APHA 22nd Edition 2012 4500-CN-

Present/Absent

0.02 - 1 mg/L

Phenolic Substances / Compounds

IS: 3025 Part 43 clause 6- 1992 (Reaffirmed 2003)

Present/Absent

IS: 3025 Part 43 clause 6- 1992 (Reaffirmed 2003)/ APHA 22nd Edition 2012 6420

0.001 - 1 mg/L

Nitrite IS: 3025 Part 34 - 1988/

APHA 22nd Edition 2012 4500-NO2

-

0.01 - 1 mg/L

Borate IS: 13428 - H - 2005/

APHA 22nd Edition 2012 4500-B

0.025 - 50 mg/L

Residual Free Chlorine IS: 3025 Part 26 - 1986 (Reaffirmed 2003)/ APHA 22nd Edition 2012 4500-Cl-B

0.2 - 100 mg/L

Mineral Oil IS: 3025 Part 39 - 1991

(Reaffirmed 2003)

Present/Absent

0.01 - 10 mg/L

Anionic Surface active agents

Annex K of IS: 13428 - 2005 0.05 - 100 mg/L

Sulphide IS: 3025 Part 29 – 1986

(Reaffirmed 2003)

0.05 - 50 mg/L

Oxygen absorbed in 4 hrs at 27°C

IS: 3025 Part 63 - 2007 0.4 - 10 mg/L

Laboratory







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Sodium IS: 3025 Part 45 – 1995 (Reaffirmed 2003)/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Na B

1 - 500 mg/L

Potassium IS: 3025 Part 45 - 1995/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-K

1 - 500 mg/L

Aluminium IS: 3025 Part 55 : 2003 / IS 15302/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Al

0.001 - 100 mg/L

Boron Annex H of IS: 13428 - 2005/ ISO 17294 -2003 Part 1 and 2/ EPA method 200.2, 6020 (EPA METHOD 200.2, 6020 (MC/SOP/INS/21, Issue No.02, Issue Date: 20-08-2013)

0.001 - 100 mg/L

Iron IS: 3025 Part 53 - 2003 / IS 15303/ APHA 22nd Edition 2012 3500-Fe

0.001 - 100 mg/L

Manganese IS: 3025 Part 59 - 2006/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Mn

0.001 - 100 mg/L

Copper IS: 3025 Part 42 - 1992 (Reaffirmed 2003)/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Cu

0.001 - 100 mg/L

Laboratory







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Zinc IS: 3025 Part 49 : 1994 (Reaffirmed 2009)/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Zn

0.001 - 100 mg/L

Barium Annex F of IS: 13428 - 2005 / IS 15302/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Ba

0.001 - 100 mg/L

Silver Annex J of IS: 13428 – 2005 0.001 - 100 mg/L APHA 22nd Edition 2012 3500-Ag

ISO 17294 -2003 Part 1 and 2

Molybdenum (as Mo) IS 3025 (Part 2) : 2004

(ISO 11885 : 1996)

0.001 - 100 mg/L

Arsenic IS: 3025 Part 37 - 1988 (Reaffirmed 2003)/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-As

0.001 - 100 mg/L

Cadmium IS: 3025 Part 41 - 1992 (Reaffirmed 2003)/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Cd

0.005 - 100 mg/L

Chromium Annex J of IS 13428 - 2005/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Ed. 2012 3500-Cr

0.001 - 100 mg/L

Mercury IS: 3025 Part 48 - 1994 (Reaffirmed 2003)/ APHA 22nd Ed. 2012 3500-Hg

0.0001 - 100 mg/L

Laboratory







of 60




Nickel Annex L of IS: 13428 - 2005/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Ni

0.001 - 100 mg/L

Lead IS: 3025 Part 47 - 1994 (Reaffirmed 2003)/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Pb

0.005 - 100 mg/L

Antimony Annex G of IS 13428 - 2005 /

IS 15303 0.001 - 100 mg/L

APHA 22nd Edition 2012 3500-Sb

ISO 17294 -2003 Part 1 and 2

Selenium IS: 3025 Part 56 - 2003 / IS 15303 : 2003/ ISO 17294 -2003 Part 1 and 2/ APHA 22nd Edition 2012 3500-Se

0.001 - 100 mg/L

Trihalomethanes a) Bromoform b) Dibromochloromethane c) Bromodichloromethane d) Chloroform

APHA 22nd Edition 2012 - 6232 0.1 - 1000 µg/L

PAH

APHA 22nd Edition 2012 6440 0.02 - 1000 mcg/L

PCB

Annex M of IS: 13428 - 2005 0.02 - 1000 mcg/L

Laboratory







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2 PESTICIDES IN WATER {Water from any source : Drinking Water (as per IS 10500:2012), Raw Water, Source Water, Packaged Drinking Water (as per IS 14543:2004), Packaged Natural Mineral Water, Water for Food Processing Industries, Domestic Water, Irrigation Water, Distilled Water, Effluent Water, Swimming Pool Water, ETP/STP Water, etc. and any other water source}

2,4' - DDE AOAC 990.06 19th Editions 2012 (MC/SOP/INS/08, Issue No.02, Issue Date: 13-01-2014)

0.02 - 1000 mcg/L 2,4' - DDT 2,4' - D 2,4' - DDD 4,4' - DDD 4,4' - DDE 4,4' - DDT a - Endosulfan a - HCH B Endosulfan b - HCH d - HCH Dieldrin Aldrin Endosulfan Endosulfan sulphate gamma - HCH/Lindane Alachlor Atrazine Butachlor Chlorpyriphos Ethion Malathion AOAC 990.06 19th Editions 2012


0.02 - 1000 mcg/L Malaoxon Monocrotophos Paraoxon - Methyl Parathion Methyl Phorate Phoratesulphoxide Phoratesulfone Isoproturon

-X-X-X-X-X-X-X-X-X-X-X-X-X-X-X-X- *NOTE: The Laboratory has demonstrated competence for the stated scope for WATER. This however does not fully cover the specification requirements of BIS for the Packaged Drinking Water as per IS:14543 and the Packaged Natural Mineral Water IS:13428.

laboratory microchem silliker private limited, a-513 ... fibre gafta 2003 [10:0] is: 12711 - 1989...

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