laboratory report - · pdf file17461 derian avenue. suite 100, irvine, ca 92614 (949) 261-1022...

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17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For: Onyx Environmental, Azusa 107 S. Motor Ave. Azusa, CA 91702 Attention: Lori Wynd Sampled: Received: Issued: 08/21/06-08/30/06 08/22/06 09/11/06 15:29 The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report were performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless otherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain of Custody, 1 page, is included and is an integral part of this report. This entire report was reviewed and approved for release. Project: Boeing-SSFL BMP Media Test NELAP #01108CA California ELAP#1197 CSDLAC #10117 CASE NARRATIVE SAMPLE RECEIPT: Samples were received intact, at 22°C and with chain of custody documentation. HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in accordance with the TestAmerica Sample Acceptance Policy unless otherwise noted in the report. PRESERVATION: Samples requiring preservation were verified prior to sample analysis. Results were qualified where the sample container did not meet the method preservation requirements. QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers. COMMENTS: Results that fall between the MDL and RL are 'J' flagged. The samples were prepared in accordance with the EPA Method 1311 leaching procedure described for TCLP with the exception that the extraction fluid used was deionized water instead of the acetic acid solution described in the method. SUBCONTRACTED: Refer to the last page for specific subcontract laboratory information included in this report. Enclosed are complete final results. ADDITIONAL INFORMATION: MATRIX CLIENT ID LABORATORY ID IPH2374-01 WCSG PRGP-Sand Solid IPH2374-02 WCSG BR-Sand Solid IPH2374-03 WCSG HIRW-2'' minus rock Solid IPH2374-04 WCSG EV-COR 2'' minus rock Solid IPH2374-05 WCSG PRGP-Sand-Leachate Water IPH2374-06 WCSG BR-Sand-Leachate Water Michele Chamberlin Project Manager TestAmerica - Irvine, CA IPH2374 <Page 1 of 50>

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Page 1: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

LABORATORY REPORT

Prepared For: Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd Sampled:

Received:

Issued:

08/21/06-08/30/06

08/22/06

09/11/06 15:29

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report

were performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless

otherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This

report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain of Custody, 1 page, is included and

is an integral part of this report.

This entire report was reviewed and approved for release.

Project: Boeing-SSFL BMP

Media Test

NELAP #01108CA California ELAP#1197 CSDLAC #10117

CASE NARRATIVE

SAMPLE RECEIPT: Samples were received intact, at 22°C and with chain of custody documentation.

HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in accordance with the TestAmerica

Sample Acceptance Policy unless otherwise noted in the report.

PRESERVATION: Samples requiring preservation were verified prior to sample analysis. Results were qualified where the

sample container did not meet the method preservation requirements.

QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers.

COMMENTS: Results that fall between the MDL and RL are 'J' flagged. The samples were prepared in accordance with

the EPA Method 1311 leaching procedure described for TCLP with the exception that the extraction fluid

used was deionized water instead of the acetic acid solution described in the method.

SUBCONTRACTED: Refer to the last page for specific subcontract laboratory information included in this report.

Enclosed are complete final results.ADDITIONAL

INFORMATION:

MATRIXCLIENT IDLABORATORY ID

IPH2374-01 WCSG PRGP-Sand Solid

IPH2374-02 WCSG BR-Sand Solid

IPH2374-03 WCSG HIRW-2'' minus rock Solid

IPH2374-04 WCSG EV-COR 2'' minus rock Solid

IPH2374-05 WCSG PRGP-Sand-Leachate Water

IPH2374-06 WCSG BR-Sand-Leachate Water

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374 <Page 1 of 50>

Page 2: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

MATRIXCLIENT IDLABORATORY ID

IPH2374-07 WCSG HIRW-2'' minus rock-leachate Water

IPH2374-08 WCSG EV-COR 2'' minus rock-leachate Water

Reviewed By:

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 2 of 50>

Page 3: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

CORRECTIVE ACTION REPORT

Department:

Method:

QC Batch:

Date:

Matrix: Water

Pesticides

EPA 608

6I06055

09/07/2006

Identification and Definition of Problem:

LCS and LCSD recoveries for Dieldrin, Endrin, Endosulfan II, Endrin Aldehyde, and Methoxychlor were below

laboratory control limits.

Determination of the Cause of the Problem:

The LCS and LCSD were incorrectly run through a clean-up process before analysis.

Corrective Action Taken:

Although only the LCS and LCSD were processed incorrectly, there is no positive quality control for these

compounds. The blank was processed correctly and indicates no positive bias. The surrogate recoveries for all

samples were within acceptance limits and indicate no excessive losses of sample during extraction and analysis.

There was not sufficient sample available for reanalysis within holding time. Results have been qualified to

reference this corrective action report. All extraction personnel involved have been retrained on correct procedures.

Quality Assurance Approval: Date:Dave Dawes

09/08/2006 12:11 PM

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 3 of 50>

Page 4: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL RECOVERABLE PETROLEUM HYDROCARBONS (EPA 418.1)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: mg/l

EPA 418.1Total Recoverable Hydrocarbons 6H26059 1.0 ND 08/26/06 08/26/061.020.32

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: mg/l

Total Recoverable Hydrocarbons EPA 418.1 6H26059 0.421.0 J08/26/06 08/26/0610.31

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

EPA 418.1Total Recoverable Hydrocarbons 6I01066 0.96 ND 09/01/06 09/01/060.9620.30

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

EPA 418.1Total Recoverable Hydrocarbons 6I01066 1.0 ND 09/01/06 09/01/0610.31

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 4 of 50>

Page 5: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

EXTRACTABLE FUEL HYDROCARBONS (CADHS/8015 Modified)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: mg/l

EPA 8015BEFH (C13 - C22) 6H29100 0.48 ND 08/29/06 08/30/060.9520.043

Surrogate: n-Octacosane (40-125%) 62 %

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: mg/l

EFH (C13 - C22) EPA 8015B 6H29100 0.100.53 J08/29/06 08/30/061.060.048

Surrogate: n-Octacosane (40-125%) 59 %

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

EPA 8015BEFH (C13 - C22) 6I05053 0.47 ND 09/05/06 09/05/060.9430.042

Surrogate: n-Octacosane (40-125%) 71 %

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

EPA 8015BEFH (C13 - C22) 6I05053 0.48 ND 09/05/06 09/05/060.9620.043

Surrogate: n-Octacosane (40-125%) 81 %

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 5 of 50>

Page 6: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

VOLATILE FUEL HYDROCARBONS (EPA 5030/CADHS Mod. 8015)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06 P, pH

Reporting Units: mg/l

EPA 8015 Mod.GRO (C4 - C12) 6H24046 0.10 ND 08/24/06 08/24/0610.050

Surrogate: 4-BFB (FID) (65-140%) 69 %

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06 P1

Reporting Units: mg/l

EPA 8015 Mod.GRO (C4 - C12) 6H24050 0.10 ND 08/24/06 08/25/0610.050

Surrogate: 4-BFB (FID) (65-140%) 98 %

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

GRO (C4 - C12) EPA 8015 Mod. 6I08046 0.0890.10 J09/08/06 09/08/0610.050

Surrogate: 4-BFB (FID) (65-140%) 103 %

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

EPA 8015 Mod.GRO (C4 - C12) 6I08046 0.10 ND 09/08/06 09/08/0610.050

Surrogate: 4-BFB (FID) (65-140%) 102 %

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 6 of 50>

Page 7: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

ORGANOCHLORINE PESTICIDES (EPA 608)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: ug/l

EPA 608Aldrin 6H24103 0.14 ND 08/24/06 08/28/061.430.043

alpha-BHC EPA 608 6H24103 0.0170.014 B08/24/06 08/28/061.430.0014

EPA 608beta-BHC 6H24103 0.14 ND 08/24/06 08/28/061.430.021

EPA 608delta-BHC 6H24103 0.29 ND 08/24/06 08/28/061.430.029

EPA 608gamma-BHC (Lindane) 6H24103 0.14 ND 08/24/06 08/28/061.430.029

EPA 608Chlordane 6H24103 1.4 ND 08/24/06 08/28/061.430.29

EPA 6084,4'-DDD 6H24103 0.14 ND 08/24/06 08/28/061.430.029

EPA 6084,4'-DDE 6H24103 0.14 ND 08/24/06 08/28/061.430.036

EPA 6084,4'-DDT 6H24103 0.14 ND 08/24/06 08/28/061.430.050

EPA 608Dieldrin 6H24103 0.14 ND 08/24/06 08/28/061.430.021

EPA 608Endosulfan I 6H24103 0.14 ND 08/24/06 08/28/061.430.021

EPA 608Endosulfan II 6H24103 0.14 ND 08/24/06 08/28/061.430.057

EPA 608Endosulfan sulfate 6H24103 0.29 ND 08/24/06 08/28/061.430.029

EPA 608Endrin 6H24103 0.14 ND 08/24/06 08/28/061.430.029

EPA 608Endrin aldehyde 6H24103 0.14 ND 08/24/06 08/28/061.430.064

EPA 608Endrin ketone 6H24103 0.14 ND 08/24/06 08/28/061.430.029

EPA 608Heptachlor 6H24103 0.14 ND 08/24/06 08/28/061.430.043

EPA 608Heptachlor epoxide 6H24103 0.14 ND 08/24/06 08/28/061.430.043

EPA 608Methoxychlor 6H24103 0.14 ND 08/24/06 08/28/061.430.050

EPA 608Toxaphene 6H24103 7.1 ND 08/24/06 08/28/061.432.1

Surrogate: Tetrachloro-m-xylene (35-115%) 68 %

Surrogate: Decachlorobiphenyl (45-120%) 83 %

Surrogate: Tetrachloro-m-xylene (35-115%) 68 %

Surrogate: Decachlorobiphenyl (45-120%) 83 %

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 7 of 50>

Page 8: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

ORGANOCHLORINE PESTICIDES (EPA 608)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: ug/l

EPA 608Aldrin 6H24103 0.18 ND 08/24/06 08/28/061.820.055

alpha-BHC EPA 608 6H24103 0.0120.018 B, J08/24/06 08/28/061.820.0018

EPA 608beta-BHC 6H24103 0.18 ND 08/24/06 08/28/061.820.027

EPA 608delta-BHC 6H24103 0.36 ND 08/24/06 08/28/061.820.036

EPA 608gamma-BHC (Lindane) 6H24103 0.18 ND 08/24/06 08/28/061.820.036

EPA 608Chlordane 6H24103 1.8 ND 08/24/06 08/28/061.820.36

EPA 6084,4'-DDD 6H24103 0.18 ND 08/24/06 08/28/061.820.036

EPA 6084,4'-DDE 6H24103 0.18 ND 08/24/06 08/28/061.820.045

EPA 6084,4'-DDT 6H24103 0.18 ND 08/24/06 08/28/061.820.064

EPA 608Dieldrin 6H24103 0.18 ND 08/24/06 08/28/061.820.027

EPA 608Endosulfan I 6H24103 0.18 ND 08/24/06 08/28/061.820.027

EPA 608Endosulfan II 6H24103 0.18 ND 08/24/06 08/28/061.820.073

EPA 608Endosulfan sulfate 6H24103 0.36 ND 08/24/06 08/28/061.820.036

EPA 608Endrin 6H24103 0.18 ND 08/24/06 08/28/061.820.036

EPA 608Endrin aldehyde 6H24103 0.18 ND 08/24/06 08/28/061.820.082

EPA 608Endrin ketone 6H24103 0.18 ND 08/24/06 08/28/061.820.036

EPA 608Heptachlor 6H24103 0.18 ND 08/24/06 08/28/061.820.055

EPA 608Heptachlor epoxide 6H24103 0.18 ND 08/24/06 08/28/061.820.055

EPA 608Methoxychlor 6H24103 0.18 ND 08/24/06 08/28/061.820.064

EPA 608Toxaphene 6H24103 9.1 ND 08/24/06 08/28/061.822.7

Surrogate: Tetrachloro-m-xylene (35-115%) 61 %

Surrogate: Decachlorobiphenyl (45-120%) 73 %

Surrogate: Tetrachloro-m-xylene (35-115%) 61 %

Surrogate: Decachlorobiphenyl (45-120%) 73 %

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 8 of 50>

Page 9: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

ORGANOCHLORINE PESTICIDES (EPA 608)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: ug/l

EPA 608Aldrin 6I06055 0.33 ND 09/06/06 09/06/063.330.10

alpha-BHC EPA 608 6I06055 0.00920.033 B, J09/06/06 09/06/063.330.0033

EPA 608beta-BHC 6I06055 0.33 ND 09/06/06 09/06/063.330.050

EPA 608delta-BHC 6I06055 0.67 ND 09/06/06 09/06/063.330.067

EPA 608gamma-BHC (Lindane) 6I06055 0.33 ND 09/06/06 09/06/063.330.067

EPA 608Chlordane 6I06055 3.3 ND 09/06/06 09/06/063.330.67

EPA 6084,4'-DDD 6I06055 0.33 ND 09/06/06 09/06/063.330.067

EPA 6084,4'-DDE 6I06055 0.33 ND 09/06/06 09/06/063.330.083

EPA 6084,4'-DDT 6I06055 0.33 ND 09/06/06 09/06/063.330.12

EPA 608Dieldrin 6I06055 0.33 ND 09/06/06 09/06/063.330.050

EPA 608Endosulfan I 6I06055 0.33 ND 09/06/06 09/06/063.330.050

EPA 608Endosulfan II 6I06055 0.33 ND 09/06/06 09/06/063.330.13

EPA 608Endosulfan sulfate 6I06055 0.67 ND 09/06/06 09/06/063.330.067

EPA 608Endrin 6I06055 0.33 ND 09/06/06 09/06/063.330.067

EPA 608Endrin aldehyde 6I06055 0.33 ND 09/06/06 09/06/063.330.15

EPA 608Endrin ketone 6I06055 0.33 ND 09/06/06 09/06/063.330.067

EPA 608Heptachlor 6I06055 0.33 ND 09/06/06 09/06/063.330.10

EPA 608Heptachlor epoxide 6I06055 0.33 ND 09/06/06 09/06/063.330.10

EPA 608Methoxychlor 6I06055 0.33 ND 09/06/06 09/06/063.330.12

EPA 608Toxaphene 6I06055 17 ND 09/06/06 09/06/063.335.0

Surrogate: Tetrachloro-m-xylene (35-115%) 62 %

Surrogate: Decachlorobiphenyl (45-120%) 81 %

Surrogate: Tetrachloro-m-xylene (35-115%) 62 %

Surrogate: Decachlorobiphenyl (45-120%) 81 %

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 9 of 50>

Page 10: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

ORGANOCHLORINE PESTICIDES (EPA 608)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: ug/l

EPA 608Aldrin 6I06055 0.29 ND 09/06/06 09/06/062.860.086

alpha-BHC EPA 608 6I06055 0.00610.029 B, J09/06/06 09/06/062.860.0029

EPA 608beta-BHC 6I06055 0.29 ND 09/06/06 09/06/062.860.043

EPA 608delta-BHC 6I06055 0.57 ND 09/06/06 09/06/062.860.057

EPA 608gamma-BHC (Lindane) 6I06055 0.29 ND 09/06/06 09/06/062.860.057

EPA 608Chlordane 6I06055 2.9 ND 09/06/06 09/06/062.860.57

EPA 6084,4'-DDD 6I06055 0.29 ND 09/06/06 09/06/062.860.057

EPA 6084,4'-DDE 6I06055 0.29 ND 09/06/06 09/06/062.860.071

EPA 6084,4'-DDT 6I06055 0.29 ND 09/06/06 09/06/062.860.10

EPA 608Dieldrin 6I06055 0.29 ND 09/06/06 09/06/062.860.043

EPA 608Endosulfan I 6I06055 0.29 ND 09/06/06 09/06/062.860.043

EPA 608Endosulfan II 6I06055 0.29 ND 09/06/06 09/06/062.860.11

EPA 608Endosulfan sulfate 6I06055 0.57 ND 09/06/06 09/06/062.860.057

EPA 608Endrin 6I06055 0.29 ND 09/06/06 09/06/062.860.057

EPA 608Endrin aldehyde 6I06055 0.29 ND 09/06/06 09/06/062.860.13

EPA 608Endrin ketone 6I06055 0.29 ND 09/06/06 09/06/062.860.057

EPA 608Heptachlor 6I06055 0.29 ND 09/06/06 09/06/062.860.086

EPA 608Heptachlor epoxide 6I06055 0.29 ND 09/06/06 09/06/062.860.086

EPA 608Methoxychlor 6I06055 0.29 ND 09/06/06 09/06/062.860.10

EPA 608Toxaphene 6I06055 14 ND 09/06/06 09/06/062.864.3

Surrogate: Tetrachloro-m-xylene (35-115%) 53 %

Surrogate: Decachlorobiphenyl (45-120%) 80 %

Surrogate: Tetrachloro-m-xylene (35-115%) 53 %

Surrogate: Decachlorobiphenyl (45-120%) 80 %

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 10 of 50>

Page 11: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL PCBS (EPA 608)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: ug/l

EPA 608Aroclor 1016 6H24103 1.4 ND 08/24/06 08/25/061.430.29

EPA 608Aroclor 1221 6H24103 1.4 ND 08/24/06 08/25/061.430.14

EPA 608Aroclor 1232 6H24103 1.4 ND 08/24/06 08/25/061.430.36

EPA 608Aroclor 1242 6H24103 1.4 ND 08/24/06 08/25/061.430.36

EPA 608Aroclor 1248 6H24103 1.4 ND 08/24/06 08/25/061.430.36

EPA 608Aroclor 1254 6H24103 1.4 ND 08/24/06 08/25/061.430.36

EPA 608Aroclor 1260 6H24103 1.4 ND 08/24/06 08/25/061.430.57

Surrogate: Decachlorobiphenyl (45-120%) 93 %

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: ug/l

EPA 608Aroclor 1016 6H24103 1.8 ND 08/24/06 08/25/061.820.36

EPA 608Aroclor 1221 6H24103 1.8 ND 08/24/06 08/25/061.820.18

EPA 608Aroclor 1232 6H24103 1.8 ND 08/24/06 08/25/061.820.45

EPA 608Aroclor 1242 6H24103 1.8 ND 08/24/06 08/25/061.820.45

EPA 608Aroclor 1248 6H24103 1.8 ND 08/24/06 08/25/061.820.45

EPA 608Aroclor 1254 6H24103 1.8 ND 08/24/06 08/25/061.820.45

EPA 608Aroclor 1260 6H24103 1.8 ND 08/24/06 08/25/061.820.73

Surrogate: Decachlorobiphenyl (45-120%) 85 %

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: ug/l

EPA 608Aroclor 1016 6I06055 3.3 ND 09/06/06 09/06/063.330.67

EPA 608Aroclor 1221 6I06055 3.3 ND 09/06/06 09/06/063.330.33

EPA 608Aroclor 1232 6I06055 3.3 ND 09/06/06 09/06/063.330.83

EPA 608Aroclor 1242 6I06055 3.3 ND 09/06/06 09/06/063.330.83

EPA 608Aroclor 1248 6I06055 3.3 ND 09/06/06 09/06/063.330.83

EPA 608Aroclor 1254 6I06055 3.3 ND 09/06/06 09/06/063.330.83

EPA 608Aroclor 1260 6I06055 3.3 ND 09/06/06 09/06/063.331.3

Surrogate: Decachlorobiphenyl (45-120%) 84 %

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 11 of 50>

Page 12: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL PCBS (EPA 608)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: ug/l

EPA 608Aroclor 1016 6I06055 2.9 ND 09/06/06 09/06/062.860.57

EPA 608Aroclor 1221 6I06055 2.9 ND 09/06/06 09/06/062.860.29

EPA 608Aroclor 1232 6I06055 2.9 ND 09/06/06 09/06/062.860.71

EPA 608Aroclor 1242 6I06055 2.9 ND 09/06/06 09/06/062.860.71

EPA 608Aroclor 1248 6I06055 2.9 ND 09/06/06 09/06/062.860.71

EPA 608Aroclor 1254 6I06055 2.9 ND 09/06/06 09/06/062.860.71

EPA 608Aroclor 1260 6I06055 2.9 ND 09/06/06 09/06/062.861.1

Surrogate: Decachlorobiphenyl (45-120%) 83 %

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 12 of 50>

Page 13: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: mg/l

Barium EPA 200.7 6H24112 0.0170.010 08/24/06 08/25/0610.0060

Boron EPA 200.7 6H24112 0.0260.050 J08/24/06 08/25/0610.0080

EPA 200.7Iron 6H24112 0.040 ND 08/24/06 08/25/0610.015

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: mg/l

Barium EPA 200.7 6H24112 0.0540.010 08/24/06 08/25/0610.0060

Boron EPA 200.7 6H24112 0.0950.050 08/24/06 08/25/0610.0080

Iron EPA 200.7 6H24112 5.30.040 08/24/06 08/25/0610.015

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

Barium EPA 200.7 6H30102 0.00630.010 J08/30/06 09/01/0610.0060

Boron EPA 200.7 6H30102 0.0370.050 J08/30/06 09/01/0610.0080

Iron EPA 200.7 6H30102 0.110.040 08/30/06 09/01/0610.015

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

EPA 200.7Barium 6H30102 0.010 ND 08/30/06 09/01/0610.0060

Boron EPA 200.7 6H30102 0.0560.050 08/30/06 09/01/0610.0080

Iron EPA 200.7 6H30102 0.170.040 08/30/06 09/01/0610.015

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: ug/l

Antimony EPA 200.8 6H24115 1.42.0 J08/24/06 08/24/0610.050

EPA 200.7Arsenic 6H24112 5.0 ND 08/24/06 08/25/0614.4

EPA 200.7Beryllium 6H24112 2.0 ND 08/24/06 08/25/0610.90

EPA 200.8Cadmium 6H24115 1.0 ND 08/24/06 08/24/0610.025

Copper EPA 200.8 6H24115 0.402.0 J08/24/06 08/24/0610.25

EPA 200.8Lead 6H24115 1.0 ND 08/24/06 08/24/0610.040

EPA 200.7Manganese 6H24112 20 ND 08/24/06 08/25/0617.0

EPA 245.1Mercury 6H28054 0.20 ND 08/28/06 08/28/0610.050

EPA 200.7Nickel 6H24112 10 ND 08/24/06 08/25/0612.0

EPA 200.8Selenium 6H24115 2.0 ND 08/24/06 08/24/0610.30

EPA 200.8Silver 6H24115 1.0 ND 08/24/06 08/24/0610.025

EPA 200.8Thallium 6H24115 1.0 ND 08/24/06 08/24/0610.15

EPA 200.7Zinc 6H24112 20 ND 08/24/06 08/25/06115

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 13 of 50>

Page 14: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: ug/l

Antimony EPA 200.8 6H24115 0.192.0 J08/24/06 08/24/0610.050

Arsenic EPA 200.7 6H24112 4.45.0 J08/24/06 08/25/0614.4

EPA 200.7Beryllium 6H24112 2.0 ND 08/24/06 08/25/0610.90

Cadmium EPA 200.8 6H24115 0.0341.0 J08/24/06 08/24/0610.025

Copper EPA 200.8 6H24115 3.42.0 08/24/06 08/24/0610.25

Lead EPA 200.8 6H24115 1.51.0 08/24/06 08/24/0610.040

Manganese EPA 200.7 6H24112 5220 08/24/06 08/25/0617.0

EPA 245.1Mercury 6H28054 0.20 ND 08/28/06 08/28/0610.050

Nickel EPA 200.7 6H24112 2.810 J08/24/06 08/25/0612.0

EPA 200.8Selenium 6H24115 2.0 ND 08/24/06 08/24/0610.30

EPA 200.8Silver 6H24115 1.0 ND 08/24/06 08/24/0610.025

EPA 200.8Thallium 6H24115 1.0 ND 08/24/06 08/24/0610.15

EPA 200.7Zinc 6H24112 20 ND 08/24/06 08/25/06115

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: ug/l

Antimony EPA 200.8 6H30101 0.282.0 J08/30/06 09/01/0610.050

EPA 200.7Arsenic 6H30102 5.0 ND 08/30/06 09/01/0614.4

EPA 200.7Beryllium 6H30102 2.0 ND 08/30/06 09/01/0610.90

EPA 200.8Cadmium 6H30101 1.0 ND 08/30/06 09/01/0610.025

EPA 200.8Copper 6H30101 2.0 ND 08/30/06 09/01/0610.25

Lead EPA 200.8 6H30101 0.0841.0 J08/30/06 09/01/0610.040

EPA 200.7Manganese 6H30102 20 ND 08/30/06 09/01/0617.0

EPA 245.1Mercury 6H31063 0.20 ND 08/31/06 08/31/0610.050

EPA 200.7Nickel 6H30102 10 ND 08/30/06 09/01/0612.0

EPA 200.8Selenium 6H30101 2.0 ND 08/30/06 09/01/0610.30

Silver EPA 200.8 6H30101 0.0361.0 B, J08/30/06 09/01/0610.025

EPA 200.8Thallium 6H30101 1.0 ND 08/30/06 09/01/0610.15

EPA 200.7Zinc 6H30102 20 ND 08/30/06 09/01/06115

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 14 of 50>

Page 15: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: ug/l

Antimony EPA 200.8 6H30101 1.42.0 J08/30/06 09/01/0610.050

EPA 200.7Arsenic 6H30102 5.0 ND 08/30/06 09/01/0614.4

EPA 200.7Beryllium 6H30102 2.0 ND 08/30/06 09/01/0610.90

Cadmium EPA 200.8 6H30101 0.0261.0 J08/30/06 09/01/0610.025

EPA 200.8Copper 6H30101 2.0 ND 08/30/06 09/01/0610.25

Lead EPA 200.8 6H30101 0.0861.0 J08/30/06 09/01/0610.040

EPA 200.7Manganese 6H30102 20 ND 08/30/06 09/01/0617.0

EPA 245.1Mercury 6H31063 0.20 ND 08/31/06 08/31/0610.050

EPA 200.7Nickel 6H30102 10 ND 08/30/06 09/01/0612.0

EPA 200.8Selenium 6H30101 2.0 ND 08/30/06 09/01/0610.30

Silver EPA 200.8 6H30101 0.0501.0 B, J08/30/06 09/01/0610.025

Thallium EPA 200.8 6H30101 0.151.0 J08/30/06 09/01/0610.15

EPA 200.7Zinc 6H30102 20 ND 08/30/06 09/01/06115

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 15 of 50>

Page 16: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: mg/l

Ammonia-N (Distilled) EPA 350.2 6H28102 0.840.50 08/28/06 08/28/0610.30

Chloride EPA 300.0 6H24119 0.730.50 08/24/06 08/24/0610.15

Fluoride EPA 300.0 6H24119 0.160.50 J08/24/06 08/24/0610.15

EPA 300.0Nitrate-N 6H24119 0.11 ND 08/24/06 08/24/0610.060

EPA 300.0Nitrite-N 6H24119 0.15 ND 08/24/06 08/24/0610.090

EPA 300.0Nitrate/Nitrite-N 6H24119 0.15 ND 08/24/06 08/24/0610.080

EPA 413.1Oil & Grease 6H26050 4.8 ND 08/26/06 08/26/0610.90

Sulfate EPA 300.0 6H24119 8.00.50 08/24/06 08/24/0610.45

Surfactants (MBAS) SM5540-C 6H24129 0.0600.10 J08/24/06 08/24/0610.044

Total Dissolved Solids SM2540C 6H25113 25010 08/25/06 08/25/06110

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: mg/l

Ammonia-N (Distilled) EPA 350.2 6H28102 1.10.50 08/28/06 08/28/0610.30

Chloride EPA 300.0 6H24119 0.150.50 J08/24/06 08/24/0610.15

EPA 300.0Fluoride 6H24119 0.50 ND 08/24/06 08/24/0610.15

EPA 300.0Nitrate-N 6H24119 0.11 ND 08/24/06 08/24/0610.060

EPA 300.0Nitrite-N 6H24119 0.15 ND 08/24/06 08/24/0610.090

EPA 300.0Nitrate/Nitrite-N 6H24119 0.15 ND 08/24/06 08/24/0610.080

EPA 413.1Oil & Grease 6H26050 4.9 ND 08/26/06 08/26/0610.92

Sulfate EPA 300.0 6H24119 1.40.50 08/24/06 08/24/0610.45

Surfactants (MBAS) SM5540-C 6H24129 0.0480.10 J08/24/06 08/24/0610.044

Total Dissolved Solids SM2540C 6H25113 1610 08/25/06 08/25/06110

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

EPA 350.2Ammonia-N (Distilled) 6H31122 0.50 ND 08/31/06 08/31/0610.30

Chloride EPA 300.0 6H30139 0.180.50 J08/30/06 08/30/0610.15

EPA 300.0Fluoride 6H30139 0.50 ND 08/30/06 08/30/0610.15

EPA 300.0Nitrate-N 6H30139 0.11 ND 08/30/06 08/30/0610.060

EPA 300.0Nitrite-N 6H30139 0.15 ND 08/30/06 08/30/0610.090

EPA 300.0Nitrate/Nitrite-N 6H30139 0.15 ND 08/30/06 08/30/0610.080

EPA 413.1Oil & Grease 6H31070 6.7 ND 08/31/06 08/31/0611.3

Sulfate EPA 300.0 6H30139 0.610.50 08/30/06 08/30/0610.45

SM5540-CSurfactants (MBAS) 6H30098 0.10 ND 08/30/06 08/30/0610.044

Total Dissolved Solids SM2540C 6H31083 2010 08/31/06 08/31/06110

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 16 of 50>

Page 17: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: mg/l

Ammonia-N (Distilled) EPA 350.2 6H31122 4.20.50 08/31/06 08/31/0610.30

Chloride EPA 300.0 6H30139 0.200.50 J08/30/06 08/30/0610.15

EPA 300.0Fluoride 6H30139 0.50 ND 08/30/06 08/30/0610.15

EPA 300.0Nitrate-N 6H30139 0.11 ND 08/30/06 08/30/0610.060

EPA 300.0Nitrite-N 6H30139 0.15 ND 08/30/06 08/30/0610.090

EPA 300.0Nitrate/Nitrite-N 6H30139 0.15 ND 08/30/06 08/30/0610.080

EPA 413.1Oil & Grease 6H31070 4.7 ND 08/31/06 08/31/0610.89

Sulfate EPA 300.0 6H30139 0.520.50 08/30/06 08/30/0610.45

SM5540-CSurfactants (MBAS) 6H30098 0.10 ND 08/30/06 08/30/0610.044

Total Dissolved Solids SM2540C 6H31083 2410 08/31/06 08/31/06110

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: pH Units

pH EPA 150.1 6H24125 11.2NA 08/24/06 08/24/0610.00

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: pH Units

pH EPA 150.1 6H24125 9.46NA 08/24/06 08/24/0610.00

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: pH Units

pH EPA 150.1 6H30092 9.29NA 08/30/06 08/30/0610.00

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: pH Units

pH EPA 150.1 6H30092 9.51NA 08/30/06 08/30/0610.00

Sample ID: IPH2374-05 (WCSG PRGP-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: ug/l

Chromium VI EPA 218.6 6H24120 151.0 08/24/06 08/24/0610.10

EPA 335.2Total Cyanide 6H24157 5.0 ND 08/24/06 08/24/0612.2

Sample ID: IPH2374-06 (WCSG BR-Sand-Leachate - Water) Sampled: 08/24/06Reporting Units: ug/l

EPA 218.6Chromium VI 6H24120 1.0 ND 08/24/06 08/24/0610.10

EPA 335.2Total Cyanide 6H24157 5.0 ND 08/24/06 08/24/0612.2

Sample ID: IPH2374-07 (WCSG HIRW-2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: ug/l

EPA 218.6Chromium VI 6H30095 1.0 ND 08/30/06 08/30/0610.10

EPA 335.2Total Cyanide 6H30137 5.0 ND 08/30/06 08/31/0612.2

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 17 of 50>

Page 18: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

MDL

Limit

Sample ID: IPH2374-08 (WCSG EV-COR 2'' minus rock-leachate - Water) Sampled: 08/30/06Reporting Units: ug/l

EPA 218.6Chromium VI 6H30095 1.0 ND 08/30/06 08/30/0610.10

EPA 335.2Total Cyanide 6H30137 5.0 ND 08/30/06 08/31/0612.2

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 18 of 50>

Page 19: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

SHORT HOLD TIME DETAIL REPORT

Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: WCSG PRGP-Sand-Leachate (IPH2374-05) - Water

1 08/24/2006 10:45 08/22/2006 18:50 08/24/2006 15:00 08/24/2006 15:40EPA 150.1

1 08/24/2006 10:45 08/22/2006 18:50 08/24/2006 15:00 08/24/2006 16:00EPA 218.6

2 08/24/2006 10:45 08/22/2006 18:50 08/24/2006 15:30 08/24/2006 16:55EPA 300.0

2 08/24/2006 10:45 08/22/2006 18:50 08/24/2006 17:19 08/24/2006 17:56SM5540-C

Sample ID: WCSG BR-Sand-Leachate (IPH2374-06) - Water

1 08/24/2006 10:45 08/22/2006 18:50 08/24/2006 15:00 08/24/2006 15:40EPA 150.1

1 08/24/2006 10:45 08/22/2006 18:50 08/24/2006 15:00 08/24/2006 16:11EPA 218.6

2 08/24/2006 10:45 08/22/2006 18:50 08/24/2006 15:30 08/24/2006 17:11EPA 300.0

2 08/24/2006 10:45 08/22/2006 18:50 08/24/2006 17:19 08/24/2006 17:56SM5540-C

Sample ID: WCSG HIRW-2'' minus rock-leachate (IPH2374-07) - Water

1 08/30/2006 11:30 08/22/2006 18:50 08/30/2006 14:20 08/30/2006 14:35EPA 150.1

1 08/30/2006 11:30 08/22/2006 18:50 08/30/2006 15:00 08/30/2006 16:01EPA 218.6

2 08/30/2006 11:30 08/22/2006 18:50 08/30/2006 20:00 08/30/2006 20:17EPA 300.0

2 08/30/2006 11:30 08/22/2006 18:50 08/30/2006 15:25 08/30/2006 17:57SM5540-C

Sample ID: WCSG EV-COR 2'' minus rock-leachate (IPH2374-08) - Water

1 08/30/2006 11:30 08/22/2006 18:50 08/30/2006 14:20 08/30/2006 14:35EPA 150.1

1 08/30/2006 11:30 08/22/2006 18:50 08/30/2006 15:00 08/30/2006 16:12EPA 218.6

2 08/30/2006 11:30 08/22/2006 18:50 08/30/2006 20:00 08/30/2006 20:33EPA 300.0

2 08/30/2006 11:30 08/22/2006 18:50 08/30/2006 15:25 08/30/2006 17:57SM5540-C

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 19 of 50>

Page 20: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Extraction

Start Date

Extraction

End Date

TCLP EXTRACTION (DI WATER) - Zero Headspace (ZHE)

Data

QualifiersBatch

Sample ID: IPH2374-01 (WCSG PRGP-Sand - Solid) Sampled: 08/21/068/26/20068/25/2006EPA 1311-ZHEExtraction 6H25119

Sample ID: IPH2374-02 (WCSG BR-Sand - Solid) Sampled: 08/21/068/26/20068/25/2006EPA 1311-ZHEExtraction 6H25119

Sample ID: IPH2374-03 (WCSG HIRW-2'' minus rock - Solid) Sampled: 08/21/068/30/20068/29/2006EPA 1311-ZHEExtraction 6H29131

Sample ID: IPH2374-04 (WCSG EV-COR 2'' minus rock - Solid) Sampled: 08/21/068/30/20068/29/2006EPA 1311-ZHEExtraction 6H29131

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 20 of 50>

Page 21: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Analyte Method

Extraction

Start Date

Extraction

End Date

TCLP EXTRACTION (DI WATER) - Metals

Data

QualifiersBatch

Sample ID: IPH2374-01 (WCSG PRGP-Sand - Solid) Sampled: 08/21/068/24/20068/23/2006EPA 1311-Met-DIExtraction 6H23140

Sample ID: IPH2374-02 (WCSG BR-Sand - Solid) Sampled: 08/21/068/24/20068/23/2006EPA 1311-Met-DIExtraction 6H23140

Sample ID: IPH2374-03 (WCSG HIRW-2'' minus rock - Solid) Sampled: 08/21/068/30/20068/29/2006EPA 1311-Met-DIExtraction 6H29130

Sample ID: IPH2374-04 (WCSG EV-COR 2'' minus rock - Solid) Sampled: 08/21/068/30/20068/29/2006EPA 1311-Met-DIExtraction 6H29130

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 21 of 50>

Page 22: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL RECOVERABLE PETROLEUM HYDROCARBONS (EPA 418.1)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H26059 Extracted: 08/26/06

Blank Analyzed: 08/26/2006 (6H26059-BLK1)

Total Recoverable Hydrocarbons mg/l1.0ND 0.31

LCS Analyzed: 08/26/2006 (6H26059-BS1) M-NR1

Total Recoverable Hydrocarbons mg/l1.05.07 65-1205.000.31 101

LCS Dup Analyzed: 08/26/2006 (6H26059-BSD1)

Total Recoverable Hydrocarbons 20mg/l1.04.84 65-1205.000.31 97 5

Batch: 6I01066 Extracted: 09/01/06

Blank Analyzed: 09/01/2006 (6I01066-BLK1)

Total Recoverable Hydrocarbons mg/l0.96ND 0.30

LCS Analyzed: 09/01/2006 (6I01066-BS1) M-NR1

Total Recoverable Hydrocarbons mg/l0.964.77 65-1204.810.30 99

LCS Dup Analyzed: 09/01/2006 (6I01066-BSD1)

Total Recoverable Hydrocarbons 20mg/l0.964.88 65-1204.810.30 101 2

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 22 of 50>

Page 23: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

EXTRACTABLE FUEL HYDROCARBONS (CADHS/8015 Modified)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H29100 Extracted: 08/29/06

Blank Analyzed: 08/30/2006 (6H29100-BLK1)

EFH (C13 - C22) mg/l2.5ND 0.22

EFH (C13 - C40) mg/l2.5ND 0.22

1.00 40-125Surrogate: n-Octacosane mg/l0.694 69

LCS Analyzed: 08/30/2006 (6H29100-BS1) M-NR1

EFH (C13 - C40) mg/l0.500.490 40-1200.750 J0.045 65

0.200 40-125Surrogate: n-Octacosane mg/l0.131 66

LCS Dup Analyzed: 08/30/2006 (6H29100-BSD1)

EFH (C13 - C40) 25mg/l0.500.480 40-1200.750 J0.045 64 2

0.200 40-125Surrogate: n-Octacosane mg/l0.118 59

Batch: 6I05053 Extracted: 09/05/06

Blank Analyzed: 09/05/2006 (6I05053-BLK1)

EFH (C13 - C22) mg/l0.47ND 0.042

EFH (C13 - C40) mg/l0.47ND 0.042

0.189 40-125Surrogate: n-Octacosane mg/l0.157 83

LCS Analyzed: 09/05/2006 (6I05053-BS1) M-NR1

EFH (C13 - C40) mg/l0.480.588 40-1200.7210.043 82

0.192 40-125Surrogate: n-Octacosane mg/l0.134 70

LCS Dup Analyzed: 09/05/2006 (6I05053-BSD1)

EFH (C13 - C40) 25mg/l0.470.518 40-1200.7080.042 73 13

0.189 40-125Surrogate: n-Octacosane mg/l0.114 60

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 23 of 50>

Page 24: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

VOLATILE FUEL HYDROCARBONS (EPA 5030/CADHS Mod. 8015)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24046 Extracted: 08/24/06

Blank Analyzed: 08/24/2006 (6H24046-BLK1)

GRO (C4 - C12) mg/l0.10ND 0.050

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.00837 84

LCS Analyzed: 08/24/2006 (6H24046-BS1)

GRO (C4 - C12) mg/l0.100.664 65-1400.8000.050 83

0.0300 65-140Surrogate: 4-BFB (FID) mg/l0.0302 101

Matrix Spike Analyzed: 08/24/2006 (6H24046-MS1) Source: IPH1750-03

GRO (C4 - C12) mg/l0.100.182 60-1450.220 ND0.050 83

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.0102 102

Matrix Spike Dup Analyzed: 08/24/2006 (6H24046-MSD1) Source: IPH1750-03

GRO (C4 - C12) 20mg/l0.100.190 60-1450.220 ND0.050 86 4

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.0107 107

Batch: 6H24050 Extracted: 08/24/06

Blank Analyzed: 08/24/2006 (6H24050-BLK1)

GRO (C4 - C12) mg/l0.10ND 0.050

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.00937 94

LCS Analyzed: 08/24/2006 (6H24050-BS1)

GRO (C4 - C12) mg/l0.100.817 65-1400.8000.050 102

0.0300 65-140Surrogate: 4-BFB (FID) mg/l0.0362 121

Matrix Spike Analyzed: 08/24/2006 (6H24050-MS1) Source: IPH1762-06

GRO (C4 - C12) mg/l0.100.729 60-1450.220 0.430.050 136

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.00840 84

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 24 of 50>

Page 25: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

VOLATILE FUEL HYDROCARBONS (EPA 5030/CADHS Mod. 8015)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24050 Extracted: 08/24/06

Matrix Spike Dup Analyzed: 08/24/2006 (6H24050-MSD1) Source: IPH1762-06

GRO (C4 - C12) 20mg/l0.100.641 60-1450.220 0.430.050 96 13

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.0121 121

Batch: 6I08046 Extracted: 09/08/06

Blank Analyzed: 09/08/2006 (6I08046-BLK1)

GRO (C4 - C12) mg/l0.10ND 0.025

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.00990 99

LCS Analyzed: 09/08/2006 (6I08046-BS1)

GRO (C4 - C12) mg/l0.100.761 65-1400.8000.025 95

0.0300 65-140Surrogate: 4-BFB (FID) mg/l0.0381 127

Matrix Spike Analyzed: 09/08/2006 (6I08046-MS1) Source: IPH3064-15

GRO (C4 - C12) mg/l0.100.274 60-1450.220 0.0800.025 88

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.0104 104

Matrix Spike Dup Analyzed: 09/08/2006 (6I08046-MSD1) Source: IPH3064-15

GRO (C4 - C12) 20mg/l0.100.270 60-1450.220 0.0800.025 86 1

0.0100 65-140Surrogate: 4-BFB (FID) mg/l0.0102 102

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 25 of 50>

Page 26: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

ORGANOCHLORINE PESTICIDES (EPA 608)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24103 Extracted: 08/24/06

Blank Analyzed: 08/28/2006 (6H24103-BLK1)

Aldrin ug/l0.50ND 0.15

alpha-BHC ug/l0.0500.00947 J0.0050

alpha-BHC ug/l0.50ND 0.10

beta-BHC ug/l0.50ND 0.075

delta-BHC ug/l1.0ND 0.10

gamma-BHC (Lindane) ug/l0.50ND 0.10

Chlordane ug/l5.0ND 1.0

4,4'-DDD ug/l0.50ND 0.10

4,4'-DDE ug/l0.50ND 0.12

4,4'-DDT ug/l0.50ND 0.18

Dieldrin ug/l0.50ND 0.075

Endosulfan I ug/l0.50ND 0.075

Endosulfan II ug/l0.50ND 0.20

Endosulfan sulfate ug/l1.0ND 0.10

Endrin ug/l0.50ND 0.10

Endrin aldehyde ug/l0.50ND 0.22

Endrin ketone ug/l0.50ND 0.10

Heptachlor ug/l0.50ND 0.15

Heptachlor epoxide ug/l0.50ND 0.15

Methoxychlor ug/l0.50ND 0.18

Toxaphene ug/l25ND 7.5

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.57 63

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.10 84

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.57 63

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.10 84

LCS Analyzed: 08/28/2006 (6H24103-BS1) M-NR1

Aldrin ug/l0.501.57 35-1202.500.15 63

alpha-BHC ug/l0.0501.57 45-1202.500.0050 63

alpha-BHC ug/l0.501.57 45-1202.500.10 63

beta-BHC ug/l0.501.80 50-1202.500.075 72

delta-BHC ug/l1.01.68 50-1202.500.10 67

gamma-BHC (Lindane) ug/l0.501.59 40-1202.500.10 64

4,4'-DDD ug/l0.501.89 55-1202.500.10 76

4,4'-DDE ug/l0.501.77 50-1202.500.12 71

4,4'-DDT ug/l0.501.94 55-1202.500.18 78

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 26 of 50>

Page 27: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

ORGANOCHLORINE PESTICIDES (EPA 608)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24103 Extracted: 08/24/06

LCS Analyzed: 08/28/2006 (6H24103-BS1) M-NR1

Dieldrin ug/l0.501.87 50-1202.500.075 75

Endosulfan I ug/l0.501.81 50-1202.500.075 72

Endosulfan II ug/l0.502.03 55-1202.500.20 81

Endosulfan sulfate ug/l1.02.25 60-1202.500.10 90

Endrin ug/l0.502.02 55-1202.500.10 81

Endrin aldehyde ug/l0.502.12 55-1202.500.22 85

Endrin ketone ug/l0.502.03 55-1202.500.10 81

Heptachlor ug/l0.501.78 40-1152.500.15 71

Heptachlor epoxide ug/l0.501.81 50-1202.500.15 72

Methoxychlor ug/l0.502.01 55-1202.500.18 80

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.65 66

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.05 82

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.65 66

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.05 82

LCS Dup Analyzed: 08/28/2006 (6H24103-BSD1)

Aldrin 30ug/l0.501.89 35-1202.500.15 76 18

alpha-BHC 30ug/l0.501.87 45-1202.500.10 75 17

alpha-BHC 30ug/l0.0501.87 45-1202.500.0050 75 17

beta-BHC 30ug/l0.502.06 50-1202.500.075 82 13

delta-BHC 30ug/l1.01.88 50-1202.500.10 75 11

gamma-BHC (Lindane) 30ug/l0.501.89 40-1202.500.10 76 17

4,4'-DDD 30ug/l0.502.09 55-1202.500.10 84 10

4,4'-DDE 30ug/l0.502.01 50-1202.500.12 80 13

4,4'-DDT 30ug/l0.502.14 55-1202.500.18 86 10

Dieldrin 30ug/l0.502.13 50-1202.500.075 85 13

Endosulfan I 30ug/l0.502.08 50-1202.500.075 83 14

Endosulfan II 30ug/l0.502.25 55-1202.500.20 90 10

Endosulfan sulfate 30ug/l1.02.46 60-1202.500.10 98 9

Endrin 30ug/l0.502.30 55-1202.500.10 92 13

Endrin aldehyde 30ug/l0.502.16 55-1202.500.22 86 2

Endrin ketone 30ug/l0.502.22 55-1202.500.10 89 9

Heptachlor 30ug/l0.502.11 40-1152.500.15 84 17

Heptachlor epoxide 30ug/l0.502.11 50-1202.500.15 84 15

Methoxychlor 30ug/l0.502.21 55-1202.500.18 88 9

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.96 78

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 27 of 50>

Page 28: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

ORGANOCHLORINE PESTICIDES (EPA 608)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24103 Extracted: 08/24/06

LCS Dup Analyzed: 08/28/2006 (6H24103-BSD1)

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.24 90

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.96 78

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.24 90

Batch: 6I06055 Extracted: 09/06/06

Blank Analyzed: 09/06/2006 (6I06055-BLK1)

Aldrin ug/l0.50ND 0.15

alpha-BHC ug/l0.50ND 0.10

alpha-BHC ug/l0.0500.0221 J0.0050

beta-BHC ug/l0.50ND 0.075

delta-BHC ug/l1.0ND 0.10

gamma-BHC (Lindane) ug/l0.50ND 0.10

Chlordane ug/l5.0ND 1.0

4,4'-DDD ug/l0.50ND 0.10

4,4'-DDE ug/l0.50ND 0.12

4,4'-DDT ug/l0.50ND 0.18

Dieldrin ug/l0.50ND 0.075

Endosulfan I ug/l0.50ND 0.075

Endosulfan II ug/l0.50ND 0.20

Endosulfan sulfate ug/l1.0ND 0.10

Endrin ug/l0.50ND 0.10

Endrin aldehyde ug/l0.50ND 0.22

Endrin ketone ug/l0.50ND 0.10

Heptachlor ug/l0.50ND 0.15

Heptachlor epoxide ug/l0.50ND 0.15

Methoxychlor ug/l0.50ND 0.18

Toxaphene ug/l25ND 7.5

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.60 64

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.26 90

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.60 64

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.26 90

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 28 of 50>

Page 29: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

ORGANOCHLORINE PESTICIDES (EPA 608)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6I06055 Extracted: 09/06/06

LCS Analyzed: 09/06/2006 (6I06055-BS1) M-NR1

Aldrin ug/l0.502.16 35-1202.500.15 86

alpha-BHC ug/l0.0502.13 45-1202.500.0050 85

alpha-BHC ug/l0.502.13 45-1202.500.10 85

beta-BHC ug/l0.502.46 50-1202.500.075 98

delta-BHC ug/l1.02.25 50-1202.500.10 90

gamma-BHC (Lindane) ug/l0.502.15 40-1202.500.10 86

4,4'-DDD ug/l0.502.52 55-1202.500.10 101

4,4'-DDE ug/l0.502.30 50-1202.500.12 92

4,4'-DDT ug/l0.502.34 55-1202.500.18 94

Dieldrin ug/l0.50ND 50-1202.50 N-20.075

Endosulfan I ug/l0.502.53 50-1202.500.075 101

Endosulfan II ug/l0.501.08 55-1202.50 N-20.20 43

Endosulfan sulfate ug/l1.02.46 60-1202.500.10 98

Endrin ug/l0.50ND 55-1202.50 N-20.10

Endrin aldehyde ug/l0.501.22 55-1202.50 N-20.22 49

Endrin ketone ug/l0.502.82 55-1202.500.10 113

Heptachlor ug/l0.502.38 40-1152.500.15 95

Heptachlor epoxide ug/l0.502.27 50-1202.500.15 91

Methoxychlor ug/l0.500.243 55-1202.50 N-2, J0.18 10

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l2.17 87

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.51 100

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l2.17 87

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.51 100

LCS Dup Analyzed: 09/06/2006 (6I06055-BSD1)

Aldrin 30ug/l0.501.95 35-1202.500.15 78 10

alpha-BHC 30ug/l0.0502.03 45-1202.500.0050 81 5

alpha-BHC 30ug/l0.502.03 45-1202.500.10 81 5

beta-BHC 30ug/l0.502.28 50-1202.500.075 91 8

delta-BHC 30ug/l1.02.08 50-1202.500.10 83 8

gamma-BHC (Lindane) 30ug/l0.501.96 40-1202.500.10 78 9

4,4'-DDD 30ug/l0.502.37 55-1202.500.10 95 6

4,4'-DDE 30ug/l0.502.12 50-1202.500.12 85 8

4,4'-DDT 30ug/l0.502.23 55-1202.500.18 89 5

Dieldrin 30ug/l0.50ND 50-1202.50 N-20.075

Endosulfan I 30ug/l0.502.31 50-1202.500.075 92 9

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 29 of 50>

Page 30: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

ORGANOCHLORINE PESTICIDES (EPA 608)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6I06055 Extracted: 09/06/06

LCS Dup Analyzed: 09/06/2006 (6I06055-BSD1)

Endosulfan II 30ug/l0.500.824 55-1202.50 N-20.20 33 27

Endosulfan sulfate 30ug/l1.02.19 60-1202.500.10 88 12

Endrin 30ug/l0.50ND 55-1202.50 N-20.10

Endrin aldehyde 30ug/l0.500.835 55-1202.50 N-20.22 33 37

Endrin ketone 30ug/l0.502.55 55-1202.500.10 102 10

Heptachlor 30ug/l0.502.16 40-1152.500.15 86 10

Heptachlor epoxide 30ug/l0.502.09 50-1202.500.15 84 8

Methoxychlor 30ug/l0.50ND 55-1202.50 N-20.18

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.99 80

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.43 97

2.50 35-115Surrogate: Tetrachloro-m-xylene ug/l1.99 80

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.43 97

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 30 of 50>

Page 31: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL PCBS (EPA 608)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24103 Extracted: 08/24/06

Blank Analyzed: 08/25/2006 (6H24103-BLK1)

Aroclor 1016 ug/l5.0ND 1.0

Aroclor 1221 ug/l5.0ND 0.50

Aroclor 1232 ug/l5.0ND 1.2

Aroclor 1242 ug/l5.0ND 1.2

Aroclor 1248 ug/l5.0ND 1.2

Aroclor 1254 ug/l5.0ND 1.2

Aroclor 1260 ug/l5.0ND 2.0

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.19 88

LCS Analyzed: 08/25/2006 (6H24103-BS2) M-NR1

Aroclor 1016 ug/l5.018.0 45-11520.01.0 90

Aroclor 1260 ug/l5.020.6 55-11520.02.0 103

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.65 106

LCS Dup Analyzed: 08/25/2006 (6H24103-BSD2)

Aroclor 1016 30ug/l5.011.0 45-11520.0 R-71.0 55 48

Aroclor 1260 25ug/l5.012.7 55-11520.0 R-72.0 64 47

2.50 45-120Surrogate: Decachlorobiphenyl ug/l1.51 60

Batch: 6I06055 Extracted: 09/06/06

Blank Analyzed: 09/06/2006 (6I06055-BLK1)

Aroclor 1016 ug/l5.0ND 1.0

Aroclor 1221 ug/l5.0ND 0.50

Aroclor 1232 ug/l5.0ND 1.2

Aroclor 1242 ug/l5.0ND 1.2

Aroclor 1248 ug/l5.0ND 1.2

Aroclor 1254 ug/l5.0ND 1.2

Aroclor 1260 ug/l5.0ND 2.0

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.24 90

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 31 of 50>

Page 32: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL PCBS (EPA 608)

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6I06055 Extracted: 09/06/06

LCS Analyzed: 09/06/2006 (6I06055-BS2) M-NR1

Aroclor 1016 ug/l5.016.8 45-11520.01.0 84

Aroclor 1260 ug/l5.018.2 55-11520.02.0 91

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.11 84

LCS Dup Analyzed: 09/06/2006 (6I06055-BSD2)

Aroclor 1016 30ug/l5.015.7 45-11520.01.0 78 7

Aroclor 1260 25ug/l5.017.0 55-11520.02.0 85 7

2.50 45-120Surrogate: Decachlorobiphenyl ug/l2.03 81

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 32 of 50>

Page 33: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

METALS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24112 Extracted: 08/24/06

Blank Analyzed: 08/25/2006 (6H24112-BLK1)

Arsenic ug/l5.0ND 4.4

Barium mg/l0.010ND 0.0060

Beryllium ug/l2.0ND 0.90

Boron mg/l0.050ND 0.0080

Iron mg/l0.040ND 0.015

Manganese ug/l20ND 7.0

Nickel ug/l10ND 2.0

Zinc ug/l20ND 15

LCS Analyzed: 08/25/2006 (6H24112-BS1)

Arsenic ug/l5.0490 85-1155004.4 98

Barium mg/l0.0100.486 85-1150.5000.0060 97

Beryllium ug/l2.0495 85-1155000.90 99

Boron mg/l0.0500.479 85-1150.5000.0080 96

Iron mg/l0.0400.499 85-1150.5000.015 100

Manganese ug/l20498 85-1155007.0 100

Nickel ug/l10483 85-1155002.0 97

Zinc ug/l20489 85-11550015 98

Matrix Spike Analyzed: 08/25/2006 (6H24112-MS1) Source: IPH2374-05

Arsenic ug/l5.0495 70-130500 ND4.4 99

Barium mg/l0.0100.498 70-1300.500 0.0170.0060 96

Beryllium ug/l2.0502 70-130500 ND0.90 100

Boron mg/l0.0500.525 70-1300.500 0.0260.0080 100

Iron mg/l0.0400.498 70-1300.500 ND0.015 100

Manganese ug/l20500 70-130500 ND7.0 100

Nickel ug/l10484 70-130500 ND2.0 97

Zinc ug/l20494 70-130500 ND15 99

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 33 of 50>

Page 34: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

METALS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24112 Extracted: 08/24/06

Matrix Spike Dup Analyzed: 08/25/2006 (6H24112-MSD1) Source: IPH2374-05

Arsenic 20ug/l5.0496 70-130500 ND4.4 99 0

Barium 20mg/l0.0100.503 70-1300.500 0.0170.0060 97 1

Beryllium 20ug/l2.0509 70-130500 ND0.90 102 1

Boron 20mg/l0.0500.536 70-1300.500 0.0260.0080 102 2

Iron 20mg/l0.0400.498 70-1300.500 ND0.015 100 0

Manganese 20ug/l20502 70-130500 ND7.0 100 0

Nickel 20ug/l10485 70-130500 ND2.0 97 0

Zinc 20ug/l20498 70-130500 ND15 100 1

Batch: 6H24115 Extracted: 08/24/06

Blank Analyzed: 08/24/2006 (6H24115-BLK1)

Antimony ug/l2.0ND 0.050

Cadmium ug/l1.0ND 0.025

Copper ug/l2.0ND 0.25

Lead ug/l1.0ND 0.040

Selenium ug/l2.0ND 0.30

Silver ug/l1.0ND 0.025

Thallium ug/l1.0ND 0.15

LCS Analyzed: 08/24/2006 (6H24115-BS1)

Antimony ug/l2.089.9 85-11580.00.050 112

Cadmium ug/l1.090.2 85-11580.00.025 113

Copper ug/l2.079.6 85-11580.00.25 100

Lead ug/l1.079.9 85-11580.00.040 100

Selenium ug/l2.083.8 85-11580.00.30 105

Silver ug/l1.086.9 85-11580.00.025 109

Thallium ug/l1.080.2 85-11580.00.15 100

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 34 of 50>

Page 35: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

METALS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24115 Extracted: 08/24/06

Matrix Spike Analyzed: 08/24/2006 (6H24115-MS1) Source: IPH2351-07

Antimony ug/l2.086.4 70-13080.0 0.190.050 108

Cadmium ug/l1.085.8 70-13080.0 ND0.025 107

Copper ug/l2.080.1 70-13080.0 0.350.25 100

Lead ug/l1.080.1 70-13080.0 0.130.040 100

Selenium ug/l2.087.5 70-13080.0 4.10.30 104

Silver ug/l1.083.4 70-13080.0 ND0.025 104

Thallium ug/l1.079.8 70-13080.0 ND0.15 100

Matrix Spike Dup Analyzed: 08/24/2006 (6H24115-MSD1) Source: IPH2351-07

Antimony 20ug/l2.085.1 70-13080.0 0.190.050 106 2

Cadmium 20ug/l1.085.3 70-13080.0 ND0.025 107 1

Copper 20ug/l2.081.1 70-13080.0 0.350.25 101 1

Lead 20ug/l1.079.9 70-13080.0 0.130.040 100 0

Selenium 20ug/l2.087.5 70-13080.0 4.10.30 104 0

Silver 20ug/l1.083.6 70-13080.0 ND0.025 104 0

Thallium 20ug/l1.079.7 70-13080.0 ND0.15 100 0

Batch: 6H28054 Extracted: 08/28/06

Blank Analyzed: 08/28/2006 (6H28054-BLK1)

Mercury ug/l0.20ND 0.050

LCS Analyzed: 08/28/2006 (6H28054-BS1)

Mercury ug/l0.208.08 85-1158.000.050 101

Matrix Spike Analyzed: 08/28/2006 (6H28054-MS1) Source: IPH2653-03

Mercury ug/l0.209.02 70-1308.00 1.60.050 93

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 35 of 50>

Page 36: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

METALS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H28054 Extracted: 08/28/06

Matrix Spike Dup Analyzed: 08/28/2006 (6H28054-MSD1) Source: IPH2653-03

Mercury 20ug/l0.208.75 70-1308.00 1.60.050 89 3

Batch: 6H30101 Extracted: 08/30/06

Blank Analyzed: 09/01/2006 (6H30101-BLK1)

Antimony ug/l2.0ND 0.050

Cadmium ug/l1.0ND 0.025

Copper ug/l2.0ND 0.25

Lead ug/l1.0ND 0.040

Selenium ug/l2.0ND 0.30

Silver ug/l1.00.0851 J0.025

Thallium ug/l1.0ND 0.15

LCS Analyzed: 09/01/2006 (6H30101-BS1)

Antimony ug/l2.072.5 85-11580.00.050 91

Cadmium ug/l1.073.8 85-11580.00.025 92

Copper ug/l2.078.9 85-11580.00.25 99

Lead ug/l1.077.1 85-11580.00.040 96

Selenium ug/l2.074.5 85-11580.00.30 93

Silver ug/l1.079.7 85-11580.00.025 100

Thallium ug/l1.077.8 85-11580.00.15 97

Matrix Spike Analyzed: 09/01/2006 (6H30101-MS1) Source: IPH2374-07

Antimony ug/l2.072.4 70-13080.0 0.280.050 90

Cadmium ug/l1.073.7 70-13080.0 ND0.025 92

Copper ug/l2.077.6 70-13080.0 ND0.25 97

Lead ug/l1.076.8 70-13080.0 0.0840.040 96

Selenium ug/l2.073.9 70-13080.0 ND0.30 92

Silver ug/l1.077.5 70-13080.0 0.0360.025 97

Thallium ug/l1.077.4 70-13080.0 ND0.15 97

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 36 of 50>

Page 37: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

METALS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H30101 Extracted: 08/30/06

Matrix Spike Dup Analyzed: 09/01/2006 (6H30101-MSD1) Source: IPH2374-07

Antimony 20ug/l2.072.5 70-13080.0 0.280.050 90 0

Cadmium 20ug/l1.074.1 70-13080.0 ND0.025 93 1

Copper 20ug/l2.078.1 70-13080.0 ND0.25 98 1

Lead 20ug/l1.077.9 70-13080.0 0.0840.040 97 1

Selenium 20ug/l2.074.3 70-13080.0 ND0.30 93 1

Silver 20ug/l1.078.6 70-13080.0 0.0360.025 98 1

Thallium 20ug/l1.078.2 70-13080.0 ND0.15 98 1

Batch: 6H30102 Extracted: 08/30/06

Blank Analyzed: 09/01/2006 (6H30102-BLK1)

Arsenic ug/l5.0ND 4.4

Barium mg/l0.010ND 0.0060

Beryllium ug/l2.0ND 0.90

Boron mg/l0.050ND 0.0080

Iron mg/l0.040ND 0.015

Manganese ug/l20ND 7.0

Nickel ug/l10ND 2.0

Zinc ug/l20ND 15

LCS Analyzed: 09/01/2006 (6H30102-BS1)

Arsenic ug/l5.0507 85-1155004.4 101

Barium mg/l0.0100.470 85-1150.5000.0060 94

Beryllium ug/l2.0501 85-1155000.90 100

Boron mg/l0.0500.465 85-1150.5000.0080 93

Iron mg/l0.0400.501 85-1150.5000.015 100

Manganese ug/l20495 85-1155007.0 99

Nickel ug/l10489 85-1155002.0 98

Zinc ug/l20485 85-11550015 97

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 37 of 50>

Page 38: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

METALS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H30102 Extracted: 08/30/06

Matrix Spike Analyzed: 09/01/2006 (6H30102-MS1) Source: IPH2374-08

Arsenic ug/l5.0496 70-130500 ND4.4 99

Barium mg/l0.0100.470 70-1300.500 ND0.0060 94

Beryllium ug/l2.0486 70-130500 ND0.90 97

Boron mg/l0.0500.523 70-1300.500 0.0560.0080 93

Iron mg/l0.0400.641 70-1300.500 0.170.015 94

Manganese ug/l20480 70-130500 ND7.0 96

Nickel ug/l10478 70-130500 ND2.0 96

Zinc ug/l20476 70-130500 ND15 95

Matrix Spike Dup Analyzed: 09/01/2006 (6H30102-MSD1) Source: IPH2374-08

Arsenic 20ug/l5.0493 70-130500 ND4.4 99 1

Barium 20mg/l0.0100.462 70-1300.500 ND0.0060 92 2

Beryllium 20ug/l2.0477 70-130500 ND0.90 95 2

Boron 20mg/l0.0500.515 70-1300.500 0.0560.0080 92 2

Iron 20mg/l0.0400.633 70-1300.500 0.170.015 93 1

Manganese 20ug/l20470 70-130500 ND7.0 94 2

Nickel 20ug/l10474 70-130500 ND2.0 95 1

Zinc 20ug/l20473 70-130500 ND15 95 1

Batch: 6H31063 Extracted: 08/31/06

Blank Analyzed: 08/31/2006 (6H31063-BLK1)

Mercury ug/l0.20ND 0.050

LCS Analyzed: 08/31/2006 (6H31063-BS1)

Mercury ug/l0.207.92 85-1158.000.050 99

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 38 of 50>

Page 39: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

METALS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H31063 Extracted: 08/31/06

Matrix Spike Analyzed: 08/31/2006 (6H31063-MS1) Source: IPH3070-18

Mercury ug/l0.207.98 70-1308.00 ND0.050 100

Matrix Spike Dup Analyzed: 08/31/2006 (6H31063-MSD1) Source: IPH3070-18

Mercury 20ug/l0.207.87 70-1308.00 ND0.050 98 1

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 39 of 50>

Page 40: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24119 Extracted: 08/24/06

Blank Analyzed: 08/24/2006 (6H24119-BLK1)

Chloride mg/l0.50ND 0.15

Fluoride mg/l0.50ND 0.15

Nitrate-N mg/l0.11ND 0.060

Nitrite-N mg/l0.15ND 0.090

Nitrate/Nitrite-N mg/l0.15ND 0.080

Sulfate mg/l0.50ND 0.45

LCS Analyzed: 08/24/2006 (6H24119-BS1)

Chloride mg/l0.504.97 90-1105.000.15 99

Fluoride mg/l0.504.82 90-1105.000.15 96

Nitrate-N mg/l0.111.19 90-1101.130.060 105

Nitrite-N mg/l0.151.47 90-1101.520.090 97

Sulfate mg/l0.5010.2 90-11010.00.45 102

Matrix Spike Analyzed: 08/24/2006 (6H24119-MS1) Source: IPH2351-07

Chloride mg/l0.504.94 80-1205.00 ND0.15 99

Fluoride mg/l0.504.81 80-1205.00 ND0.15 96

Nitrate-N mg/l0.111.19 80-1201.13 ND0.060 105

Nitrite-N mg/l0.151.46 80-1201.52 ND0.090 96

Sulfate mg/l0.5010.3 80-12010.0 ND0.45 103

Matrix Spike Dup Analyzed: 08/24/2006 (6H24119-MSD1) Source: IPH2351-07

Chloride 20mg/l0.504.91 80-1205.00 ND0.15 98 1

Fluoride 20mg/l0.504.80 80-1205.00 ND0.15 96 0

Nitrate-N 20mg/l0.111.18 80-1201.13 ND0.060 104 1

Nitrite-N 20mg/l0.151.44 80-1201.52 ND0.090 95 1

Sulfate 20mg/l0.5010.2 80-12010.0 ND0.45 102 1

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 40 of 50>

Page 41: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24120 Extracted: 08/24/06

Blank Analyzed: 08/24/2006 (6H24120-BLK1)

Chromium VI ug/l1.0ND 0.10

LCS Analyzed: 08/24/2006 (6H24120-BS1)

Chromium VI ug/l1.049.4 90-11050.00.10 99

Matrix Spike Analyzed: 08/24/2006 (6H24120-MS1) Source: IPH2351-07

Chromium VI ug/l1.047.3 90-11050.0 ND0.10 95

Matrix Spike Dup Analyzed: 08/24/2006 (6H24120-MSD1) Source: IPH2351-07

Chromium VI 10ug/l1.047.2 90-11050.0 ND0.10 94 0

Batch: 6H24125 Extracted: 08/24/06

Duplicate Analyzed: 08/24/2006 (6H24125-DUP1) Source: IPH2374-05

pH 5pH UnitsNA11.2 11.20.00 0

Batch: 6H24129 Extracted: 08/24/06

Blank Analyzed: 08/24/2006 (6H24129-BLK1)

Surfactants (MBAS) mg/l0.10ND 0.044

LCS Analyzed: 08/24/2006 (6H24129-BS1)

Surfactants (MBAS) mg/l0.100.242 90-1100.2500.044 97

Matrix Spike Analyzed: 08/24/2006 (6H24129-MS1) Source: IPH2351-07

Surfactants (MBAS) mg/l0.100.257 50-1250.250 ND0.044 103

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 41 of 50>

Page 42: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H24129 Extracted: 08/24/06

Matrix Spike Dup Analyzed: 08/24/2006 (6H24129-MSD1) Source: IPH2351-07

Surfactants (MBAS) 20mg/l0.100.259 50-1250.250 ND0.044 104 1

Batch: 6H24157 Extracted: 08/24/06

Blank Analyzed: 08/24/2006 (6H24157-BLK1)

Total Cyanide ug/l5.0ND 2.2

LCS Analyzed: 08/24/2006 (6H24157-BS1)

Total Cyanide ug/l5.0198 90-1102002.2 99

Matrix Spike Analyzed: 08/24/2006 (6H24157-MS1) Source: IPH2374-05

Total Cyanide ug/l5.0187 70-115200 ND2.2 94

Matrix Spike Dup Analyzed: 08/24/2006 (6H24157-MSD1) Source: IPH2374-05

Total Cyanide 15ug/l5.0197 70-115200 ND2.2 98 5

Batch: 6H25113 Extracted: 08/25/06

Blank Analyzed: 08/25/2006 (6H25113-BLK1)

Total Dissolved Solids mg/l10ND 10

LCS Analyzed: 08/25/2006 (6H25113-BS1)

Total Dissolved Solids mg/l10994 90-110100010 99

Duplicate Analyzed: 08/25/2006 (6H25113-DUP1) Source: IPH2351-07

Total Dissolved Solids 10mg/l1032.0 3010 6

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 42 of 50>

Page 43: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H26050 Extracted: 08/26/06

Blank Analyzed: 08/26/2006 (6H26050-BLK1)

Oil & Grease mg/l5.2ND 0.98

LCS Analyzed: 08/26/2006 (6H26050-BS1)

Oil & Grease mg/l5.019.4 65-12020.00.94 97

LCS Dup Analyzed: 08/26/2006 (6H26050-BSD1)

Oil & Grease 20mg/l5.018.3 65-12020.00.94 92 6

Matrix Spike Analyzed: 09/08/2006 (6H26050-MS1) Source: IPH2694-01 A-01

Oil & Grease mg/l5.018.9 65-12019.8 ND0.93 95

Matrix Spike Dup Analyzed: 09/08/2006 (6H26050-MSD1) Source: IPH2694-01 A-01

Oil & Grease 25mg/l5.019.3 65-12019.8 ND0.93 97 2

Batch: 6H28102 Extracted: 08/28/06

Blank Analyzed: 08/28/2006 (6H28102-BLK1)

Ammonia-N (Distilled) mg/l0.50ND 0.30

LCS Analyzed: 08/28/2006 (6H28102-BS1)

Ammonia-N (Distilled) mg/l0.5010.9 80-11510.00.30 109

Matrix Spike Analyzed: 08/28/2006 (6H28102-MS1) Source: IPH2351-07

Ammonia-N (Distilled) mg/l0.5010.9 70-12010.0 ND0.30 109

Matrix Spike Dup Analyzed: 08/28/2006 (6H28102-MSD1) Source: IPH2351-07

Ammonia-N (Distilled) 15mg/l0.5011.2 70-12010.0 ND0.30 112 3

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 43 of 50>

Page 44: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H30092 Extracted: 08/30/06

Duplicate Analyzed: 08/30/2006 (6H30092-DUP1) Source: IPH2374-07

pH 5pH UnitsNA9.36 9.290.00 1

Batch: 6H30095 Extracted: 08/30/06

Blank Analyzed: 08/30/2006 (6H30095-BLK1)

Chromium VI ug/l1.0ND 0.10

LCS Analyzed: 08/30/2006 (6H30095-BS1)

Chromium VI ug/l1.049.4 90-11050.00.10 99

Matrix Spike Analyzed: 08/30/2006 (6H30095-MS1) Source: IPH2374-08

Chromium VI ug/l1.048.5 90-11050.0 ND0.10 97

Matrix Spike Dup Analyzed: 08/30/2006 (6H30095-MSD1) Source: IPH2374-08

Chromium VI 10ug/l1.048.1 90-11050.0 ND0.10 96 1

Batch: 6H30098 Extracted: 08/30/06

Blank Analyzed: 08/30/2006 (6H30098-BLK1)

Surfactants (MBAS) mg/l0.10ND 0.044

LCS Analyzed: 08/30/2006 (6H30098-BS1)

Surfactants (MBAS) mg/l0.100.246 90-1100.2500.044 98

Matrix Spike Analyzed: 08/30/2006 (6H30098-MS1) Source: IPH3076-01

Surfactants (MBAS) mg/l0.100.256 50-1250.250 ND0.044 102

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 44 of 50>

Page 45: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H30098 Extracted: 08/30/06

Matrix Spike Dup Analyzed: 08/30/2006 (6H30098-MSD1) Source: IPH3076-01

Surfactants (MBAS) 20mg/l0.100.260 50-1250.250 ND0.044 104 2

Batch: 6H30137 Extracted: 08/30/06

Blank Analyzed: 08/31/2006 (6H30137-BLK1)

Total Cyanide ug/l5.0ND 2.2

LCS Analyzed: 08/31/2006 (6H30137-BS1)

Total Cyanide ug/l5.0197 90-1102002.2 98

Matrix Spike Analyzed: 08/31/2006 (6H30137-MS1) Source: IPH2374-07

Total Cyanide ug/l5.0193 70-115200 ND2.2 96

Matrix Spike Dup Analyzed: 08/31/2006 (6H30137-MSD1) Source: IPH2374-07

Total Cyanide 15ug/l5.0196 70-115200 ND2.2 98 2

Batch: 6H30139 Extracted: 08/30/06

Blank Analyzed: 08/30/2006 (6H30139-BLK1)

Chloride mg/l0.50ND 0.15

Fluoride mg/l0.50ND 0.15

Nitrate-N mg/l0.11ND 0.060

Nitrite-N mg/l0.15ND 0.090

Nitrate/Nitrite-N mg/l0.15ND 0.080

Sulfate mg/l0.50ND 0.45

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 45 of 50>

Page 46: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H30139 Extracted: 08/30/06

LCS Analyzed: 08/30/2006 (6H30139-BS1)

Chloride mg/l0.504.93 90-1105.000.15 99

Fluoride mg/l0.504.76 90-1105.000.15 95

Nitrate-N mg/l0.111.21 90-1101.130.060 107

Nitrite-N mg/l0.151.43 90-1101.520.090 94

Sulfate mg/l0.5010.3 90-11010.00.45 103

Matrix Spike Analyzed: 08/30/2006 (6H30139-MS1) Source: IPH2374-08

Chloride mg/l0.505.15 80-1205.00 0.200.15 99

Fluoride mg/l0.504.79 80-1205.00 ND0.15 96

Nitrate-N mg/l0.111.24 80-1201.13 ND0.060 110

Nitrite-N mg/l0.151.42 80-1201.52 ND0.090 93

Sulfate mg/l0.5010.8 80-12010.0 0.520.45 103

Matrix Spike Dup Analyzed: 08/30/2006 (6H30139-MSD1) Source: IPH2374-08

Chloride 20mg/l0.505.04 80-1205.00 0.200.15 97 2

Fluoride 20mg/l0.504.74 80-1205.00 ND0.15 95 1

Nitrate-N 20mg/l0.111.23 80-1201.13 ND0.060 109 1

Nitrite-N 20mg/l0.151.40 80-1201.52 ND0.090 92 1

Sulfate 20mg/l0.5010.6 80-12010.0 0.520.45 101 2

Batch: 6H31070 Extracted: 08/31/06

Blank Analyzed: 08/31/2006 (6H31070-BLK1)

Oil & Grease mg/l4.8ND 0.90

LCS Analyzed: 08/31/2006 (6H31070-BS1) M-NR1

Oil & Grease mg/l4.816.7 65-12019.20.90 87

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 46 of 50>

Page 47: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H31070 Extracted: 08/31/06

LCS Dup Analyzed: 08/31/2006 (6H31070-BSD1)

Oil & Grease 20mg/l5.018.8 65-12020.00.94 94 12

Batch: 6H31083 Extracted: 08/31/06

Blank Analyzed: 08/31/2006 (6H31083-BLK1)

Total Dissolved Solids mg/l10ND 10

Blank Analyzed: 08/31/2006 (6H31083-BLK2)

Total Dissolved Solids mg/l10ND 10

LCS Analyzed: 08/31/2006 (6H31083-BS1)

Total Dissolved Solids mg/l10998 90-110100010 100

Duplicate Analyzed: 08/31/2006 (6H31083-DUP1) Source: IPH2905-04

Total Dissolved Solids 10mg/l101310 130010 1

Batch: 6H31122 Extracted: 08/31/06

Blank Analyzed: 08/31/2006 (6H31122-BLK1)

Ammonia-N (Distilled) mg/l0.50ND 0.30

LCS Analyzed: 08/31/2006 (6H31122-BS1)

Ammonia-N (Distilled) mg/l0.5010.6 80-11510.00.30 106

Matrix Spike Analyzed: 08/31/2006 (6H31122-MS1) Source: IPH2374-07

Ammonia-N (Distilled) mg/l0.5010.6 70-12010.0 ND0.30 106

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 47 of 50>

Page 48: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS

METHOD BLANK/QC DATA

Data

QualifiersMDL

Batch: 6H31122 Extracted: 08/31/06

Matrix Spike Dup Analyzed: 08/31/2006 (6H31122-MSD1) Source: IPH2374-07

Ammonia-N (Distilled) 15mg/l0.5010.6 70-12010.0 ND0.30 106 0

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 48 of 50>

Page 49: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

DATA QUALIFIERS AND DEFINITIONS

A-01 For QC puoposes, analyzed 13 days later due to lab oversite.

B Analyte was detected in the associated Method Blank.

J Estimated value. Analyte detected at a level less than the Reporting Limit (RL) and greater than or equal to the

Method Detection Limit (MDL). The user of this data should be aware that this data is of limited reliability.

M-NR1 There was no MS/MSD analyzed with this batch due to insufficient sample volume. See Blank Spike/Blank Spike

Duplicate.

N-2 See corrective action report.

P The sample, as received, was not preserved in accordance to the referenced analytical method.

P1 Sample received and analyzed without chemical preservation.

pH pH = pH=10

R-7 LFB/LFBD RPD exceeded the method control limit. Recovery met acceptance criteria.

Relative Percent DifferenceRPD

Analyte NOT DETECTED at or above the reporting limit or MDL, if MDL is specified.ND

ADDITIONAL COMMENTS

For GRO (C4-C12):

GRO (C4-C12) is quantitated against a gasoline standard. Quantitation begins immediately following the methanol peak.

For Extractable Fuel Hydrocarbons (EFH, DRO, ORO) :

Unless otherwise noted, Extractable Fuel Hydrocarbons (EFH, DRO, ORO) are quantitated against a Diesel Fuel Standard.

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 49 of 50>

Page 50: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor

17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297

Onyx Environmental, Azusa

107 S. Motor Ave.

Azusa, CA 91702

Attention: Lori Wynd

Sampled:

Received:

08/21/06-08/30/06

08/22/06Report Number:

Project ID:

IPH2374

Boeing-SSFL BMP

Media Test

Certification Summary

Method Matrix

TestAmerica - Irvine, CA

Nelac California

N/ASoil N/AEPA 1311-Met-DI

N/ASolid N/AEPA 1311-Met-DI

XSolid XEPA 1311-ZHE

XWater XEPA 150.1

XWater XEPA 200.7

XWater XEPA 200.8

N/AWater XEPA 218.6

XWater XEPA 245.1

XWater XEPA 300.0

XWater XEPA 335.2

Water XEPA 350.2

XWater XEPA 413.1

XWater XEPA 418.1

XWater XEPA 608

XWater XEPA 8015 Mod.

XWater XEPA 8015B

XWater XSM2540C

XWater XSM5540-C

Nevada and NELAP provide analyte specific accreditations. Analyte specific information for TestAmerica may be obtained by contacting

the laboratory or visiting our website at www.testamericainc.com

Michele ChamberlinProject Manager

TestAmerica - Irvine, CA

IPH2374The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 50 of 50>

Page 51: LABORATORY REPORT - · PDF file17461 Derian Avenue. Suite 100, Irvine, CA 92614 (949) 261-1022 Fax:(949) 260-3297 LABORATORY REPORT Prepared For:Onyx Environmental, Azusa 107 S. Motor