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Page 1: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

SDMSDocID 2024203

Page 2: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

2024203

February 14, 2001

Teal CrossPENCO65 North Nimitz Highway, Pier 14Honolulu, HI 96817TEL: (808)545-5195FAX (808)524-2307

Order No.: 0101185RE: Alenaio Stream Sludge

Dear Teal Cross:

Environmental Laboratory of the"? affil£feceived 3 samples onT/§W2,®I 12:30:00 PM for the.'&'^$&f^J<?s*t>& S.Wi]aY-!*95tir y *• *&**$

analyses presented in the foi

All data presented in theitems tested by the labowritten approval of the

There were no problespecifications except

Applicable samplesreport. Samples will bli

the s^Hes'lis received and to the:»|pce4^ ]̂pt fh full, without the

•«• !'M »t-jliiwvV" '"•

'^•^'focjated'QC met laboratory'v;*-11!* !"r'i' •'

/ilV,-'':;,.!'̂ 1

£,",j-! -t\ I i ̂

at no extraJc'h^Ffor a'perlod of 30 days following the finalposed of after 3,0 days, unless notified otherwise in writing.

"CTi-I- -.' ' • ' . *'- -"If you have any questions regarding mes^lesfe''results, please feel free to call.

Very truly yours,ENVIRONMENTAL LABORATORY OF THE PACIFIC

Aidan Scott

Project Manager

Oceanic Analytical Laboratory, Inc. 930 Mapunapuna Street, #100, Honolulu, Hawaii 96819 Tel: (808) 831-3090

Page 3: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: 14-Feb-Ol

CLIENT:Project:Lab Order:

Date Received:

Lab Sample ID0101185-01A0101185-01B0101185-02A0101185-02B0101 185-03 A0101185-03B

PENCOAlenaio Stream Sludge0101185

1/30/2001

Client Sample ID1/30-2C Silt 3XC1/30-2Ci/30-ic Sir 3*1/30-1C

1/30-3 - S!w.<t̂ c <t>1/30-3

Work Order Sample Summary

Collection DateWf^i C -Sexrtfyyi* ( // 1/29/2001 5:30:00 PM

« 1/29/2001 5:30:00 PM"0 vvif C S i 4^ 1/29/2001 5:30:00 PM

1/29/2001 5:30:00 PM•^osr-Cj/W^ 2c^l (0^.^1^1/1/29/2001 5:30:00 PM

1/29/2001 5:30:00 PM

Sample On Hold

DDDDD

X

Page 4: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: 14-Feb-oi

CLIENT: PENCO

Project: Alenaio Stream Sludge CASE NARRATIVELab Order: 0101185

Samples were analyzed using the methods outlined in the following references:

Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846, 3rd Edition.

All method blanks, laboratory spikes, and/or matrix spikes met quality assurance objectives.

S02: The surrogate recovery for this sample cannot be accurately quantified due to interference fromcoeluting organic compounds present in the sample.

S04: The surrogate recovery for this sample is outside of established control limits due to a samplematrix effect.

Page 5: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Febl4,2001

Client: PENCOWork Order: 0101185

Project: Alenaio Stream Sludge

Lab ID: 0101185-01A

Client Sample ID: 1/30-2C S>QCCC^ *' <^ £ C <~~

Tag Number:Collection Date: 01/29/200117:30

Matrix: SLUDGE

Reporting Dilution Date Date BatchAnalyses

HERBICIDES, TCLP LEACHED2,4,5-TP (Silvex)

2,4-0SUIT: DCAA

ICP METALS, TCLP LEACHEDArsenic

Barium

Cadmium

ChromiumLead

SeleniumSilver

MERCURY, TCLP LEACHEDMercury

PESTICIDES, TCLP LEACHEDChlordane

Endrin

gamma-BHC

HeptachlorHeptachlor epoxide

MethoxychlorToxaphene

Sum DecachlorobiphenylSum Tetrachloro-m-xylene

Result

ND

ND

163

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

88.8

73.2

Limit Units Factor Prepared Analyzed ID Analyst Qual Notes

SW1311/81500.00500 mg/L

0 00500 mg/L40-140 %REC

SW1 31 1/601 OA0.500 mg/L

1.00 mg/L

0.0500 mg/L

0.0500 mg/L0.200 mg/L

0.500 mg/L

0.0500 mg/L

SW1 31 1/74700.000500 mg/L

SW1311/8080A0.00500 mg/L

0.000500 mg/L

0.000250 mg/L

0.000250 mg/L

0.000250 mg/L0.00250 mg/L

0.0250 mg/L50-150 %REC50-150 %REC

1 2/9/2001 2/12/2001 3331 RTK

1

1 S S02

1 2/8/2001 2/8/2001 3322 TKL

1

1

1

1

11

1 2/7/2001 2/7/2001 3314 MFB

1 2/6/2001 2/12/2001 3306 RTK

1

1

1

1

111

1

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

I of 9

Page 6: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Feb 14, 2001

Client: PENCO

Work Order: 0101185

Project: Alenaio Stream Sludge

Lab ID: 0101185-01A

Analyses

SEMIVOLATILES, TCLP LEACHED1 ,4-Dichlorobenzene

2,4,5-Trichlorophenol2,4,6-Trichlorophenol

2,4-DinitrotoJueneHexachlorobenzene

Hexachlorobutadiene

HexachloroethaneNitrobenzene

Pentachlorophenol

Pyridine

Cresols, TotalSum 2,4,6-Tribromopheno!Sum 2-FluorobiphenylSurr: 2-Fluorophenol

Sum 4-Terphenyl-dl4

Sum Nitrobenzene-d5Surr: Phenol-d6

ResultReporting

Limit Units

Client Sample ID: 1/30-2C

Tag Number:

Collection Date: 01/29/2001 17:30

Matrix: SLUDGE

Dilution Date Date BatchFactor Prepared Analyzed ID Analyst Qual Notes

SW1311/8270AND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

80.2

86.2

63.1

100

87.5

62.5

0.0500 mg/L

0.0500 mg/L

0.250 mg/L

0.0500 mg/L

0.0500 mg/L

0.0500 mg/L

0.0500 mg/L

0.0500 mg/L

0.250 mg/L

0.0500 mg/L0.0500 mg/L

10-123 %REC43-116 %REC21-100 %REC

33-141 %REC35-114 %REC

10-94 %REC

1 2/7/2001 2/10/2001 3310 EOF

1

11

1

1

1

1

1

1

1

11

11

1

1

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

2 of 9

Page 7: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Feb 14, 2001

Client:Work Order:Project:Lab ID:

PENCO0101185

Alenaio Stream Sludge

0101185-01B

Client Sample ID: 1/30-2CTag Number:

Collection Date: 01/29/200117:30Matrix: SLUDGE

Analyses ResultReporting

Limit UnitsDilution Date Date BatchFactor Prepared Analyzed ID Analyst Qual Notes

VOLATILES, TCLP LEACHED1,1-Dichloroethene

1,2-DichIoroethane1,4-Dichlorobenzene

2-Butanone

Benzene

Carbon tetrachlorideChlorobenzene

Chloroform

Tetrachloroethene

Trichloroethene

Vinyl chloride

Sum 1,2-Dichloroethane-d4Sum 4-Bromofluorobenzene

Surr. Dibromofluoromethane

Surr: Toluene-d8

SW1311/8260ANDNDNDNDNDNDNDNDNDNDND110102104104

0.0400

0.04000.0400

0.5000.0400

0.0400

0.04000.0400

0.0400

0.0400

0.0200

68-144

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

%REC72-140 %REC

76-133 %REC77-146 %REC

2/6/2001 2/13/2001 R8729 KAL

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

3 of 9

Page 8: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Febl4,2001

Client: PENCO

Work Order: 0101185

Project: Alenaio Stream Sludge

Lab ID: 0101185-02A

Client Sample ID: 1/30-1C ^ c <r-h<j[J( -//>-Tag Number:

Collection Date: 01/29/2001 17:30

Matrix: SLUDGE

Reporting Dilution Date Date BatchAnalyses

HERBICIDES, TCLP LEACHED2,4,5-TP (Silvex)2,4-D

Surr: DCAA

ICP METALS, TCLP LEACHEDArsenicBariumCadmiumChromiumLeadSeleniumSilver

MERCURY, TCLP LEACHEDMercury

PESTICIDES, TCLP LEACHEDChlordaneEndringamma-BHCHeptachlorHeptachlor epoxideMethoxychlorToxaphene

Sum DecachlorobiphenylSum Tetrachloro-m-xylene

Result

ND

ND

65.9

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

87.273.3

Limit Units Factor Prepared Analyzed ID Analyst Qual Notes

SW1311/81500.00500 mg/L0.00500 mg/L40-140 %REC

SW1311/6010A0.500 mg/L1 .00 mg/L

0.0500 mg/L0.0500 mg/L

0.200 mg/L0.500 mg/L

0.0500 mg/L

SW1 31 1/74700.000500 mg/L

SW1 311/8080 A0.00500 mg/L

0.000500 mg/L0.000250 mg/L0.000250 mg/L0.000250 mg/L0.00250 mg/L

0.0250 mg/L50-150 %REC50-150 %REC

1 2/9/2001 2/12/2001 3331 RTK1

1

1 2/8/2001 2/8/2001 3322 TKL1

1

1

1

1

1

1 2/7/2001 2/7/2001 3314 MFB

1 2/6/2001 2/12/2001 3306 RTK1

1

1

1

1

1

1

1

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

4 of 9

Page 9: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Febl4,2001

Client: PENCO

Work Order: 0101185

Project: Alenaio Stream Sludge

Lab ID: 0101185-02A

Analyses

SEMIVOLATILES, TCLP LEACHED1 ,4-Dichlorobenzene2,4,5-Trichlorophenol2,4,6-Trichlorophenol2.4-DinitrotolueneHexachlorobenzeneHexachlorobutadieneHexachloroethane

NitrobenzenePentachlorophenolPyridineCresols, Total

Sum 2,4,6-TribromophenolSum 2-FluorobiphenylSurr: 2-FIuorophenolSurr: 4-Terphenyl-d14Surr: Nitrobenzene-d5Surr: Phenol-d6

ResultReporting

Limit Units

Client Sample ID: 1/30- 1CTag Number:

Collection Date: 01/29/2001 17:30

Matrix: SLUDGE

Dilution Date Date BatchFactor Prepared Analyzed ID Analyst Qua! Notes

SW1311/8270ANDNDNDNDNDNDNDNDNDNDND

74.088.364.698.887.664.0

0.05000.05000.250

0.05000.05000.05000.05000.05000.250

0.05000.050010-12343-11621-10033-14135-114

10-94

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

%REC%REC%REC%REC%REC%REC

1 2/7/2001 2/10/2001 3310 EOF1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

5 of 9

Page 10: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Feb 14, 2001

Client:Work Order:

Project:Lab ID:

PENCO0101185

Alenaio Stream Sludge

0101185-02B

Client Sample ID: 1/30-1CTag Number:

Collection Date: 01/29/200117:30Matrix: SLUDGE

Analyses ResultReporting

Limit UnitsDilution Date Date BatchFactor Prepared Analyzed ID Analyst Qual Notes

VOLATILES, TCLP LEACHED1,1-Dichloroethene1,2-Dichloroethane1,4-Dichlorobenzene2-ButanoneBenzeneCarbon letrachlorideChlorobenzeneChloroformTetrachloroetheneTrichloroethene

Vinyl chlorideSum 1,2-Dichloroethane-d4Surr: 4-BromofluorobenzeneSum DibromofluoromethaneSurr: Toluene-d8

SW1311/8260ANDNDNDNDNDNDNDNDNDNDND110100106106

0.0400

0.04000.0400

0.5000.04000.04000.04000.04000.04000.04000.0200

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

68-144 %REC72-140 %REC76-133 %REC77-146 %REC

2/12/2001 2/13/2001 R8729 KAL

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

6 of 9

Page 11: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Feb 14, 2001

Client: PENCO

Work Order: 0101185

Project: Alenaio Stream Sludge

Lab ID: 0101185-03A

Client Sample ID: 1/30-3 ; S'u t̂ {-^ !.DcVu..CTag Number: "^ h< ? u? * M. C

Collection Date: 01/29/2001 17:30

Matrix: SOLID

Reporting Dilution Date Date BatchAnalyses

HERBICIDES, TCLP LEACHED2.4,5-TP (Silvex)

2,4-DSurr: DCAA

ICP METALS, TCLP LEACHEDArsenicBarium

Cadmium

ChromiumLead

SeleniumSilver

MERCURY, TCLP LEACHEDMercury

PESTICIDES, TCLP LEACHEDChlordane

Endrin

gamma-BHCHeptachlor

Heptachlor epoxideMethoxychlor

ToxapheneSum Decachlorobiphenyl

Surr: Tetrachloro-m-xylene

Result

ND

ND

0

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

80.2

65.6

Limit Units Factor Prepared Analyzed ID Analyst Qual Notes

SW1311/81500.00500 mg/L

0.00500 mg/L40-140 %REC

SW1311I6010A0.500 mg/L1.00 mg/L

0.0500 mg/L

0.0500 mg/L0.200 mg/L

0.500 mg/L0.0500 mg/L

SW131 1/74700.000500 mg/L

SW1311/8080A0.00500 mg/L

0.000500 mg/L

0.000250 mg/L0.000250 mg/L

0.000250 mg/L

0.00250 mg/L0.0250 mg/L

50-150 %REC50-150 %REC

1 2/9/2001 2/12/2001 3331 RTK

1

1 S S04

1 2/8/2001 2/8/2001 3322 TKL11

1

1

1

1

1 2/7/2001 2/7/2001 3314 MFB

1 2/6/2001 2/12/2001 3306 RTK

1

1

11

1

1

11

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

7 of 9

Page 12: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Feb 14, 2001

Client: PENCO

Work Order: 0101185

Project: Alenaio Stream Sludge

Lab ID: 0101185-03A

Analyses

SEMIVOLATILES, TCLP LEACHED1 ,4-Dichlorobenzene

2,4,5-Trichlorophenol

2,4,6-Trichlorophenol2,4-Dinitrotoluene

Hexachlorobenzene^^

fe^Jyl4l/^?^.l'i-^^^^^*^^^Wfi^^*^^C^^^'~ ^®&

Pemacnlorophenol

PyridineCresols, Total

Sum 2,4,6-TribromophenolSurr: 2-FluorobiphenylSum 2-Fluoropheno!

Sum 4-Terphenyl-d14Surr: Nitrobenzene-d5Sum Phenol-d6

ResultReporting

Limit Units

Client Sample ID: 1/30-3Tag Number:

Collection Date: 01/29/2001 17:30

Matrix: SOLID

Dilution Date Date BatchFactor Prepared Analyzed ID Analyst Qua! Notes

SW1311/8270AND

ND

ND

ND

ND

ND^TA^Vl ilMj""̂ ^

ND

NDND

85.280.5

65.7

95.9

164

71.7

0.0500

0.0500

0.250

0.0500

0.05000.0500

* 0.0500

^ 0,0500

^ 0.250

0.05000.0500

10-12343-116

21-10033-141

35-114

10-94

mg/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

%REC%REC%REC%REC%REC%REC

1 2/7/2001 2/10/2001 3310 EOF

1

1

1

1

1

1

1

11

1

1

11

11 S S04

1

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

8 of 9

Page 13: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: Feb 14, 2001

Client:Work Order:

Project:Lab ID:

PENCO0101185

Alenaio Stream Sludge

0101185-03B

Client Sample ID: 1/30-3Tag Number:

Collection Date: 01/29/200117:30

Matrix: SOLID

Analyses ResultReporting

Limit UnitsDilution Date Date BatchFactor Prepared Analyzed ID Analyst Qual Notes

VOLATILES, TCLP LEACHED1,1-Dichloroethene1,2-Dichloroethane

1,4-Dichlorobenzene

2-Butanone

Carbon tetrachloride

Chlorobenzene

ChloroformTetrachloroethene

Trichloroethene

Vinyl chloride

Surr: 1,2-Dichloroethane-d4

Surr 4-BromofluorobenzeneSum DibromofluoromethaneSurr Toluene-d8

NDNDNDND

NDNDNDNDNDND112103106103

SW1311/8260A0.400 mg/L 10

0.400 mg/L 10

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

%REC

0.400

5.00aoo

0.4000.4000.4000.400

0.400

0.200

68-144

72-140 %REC76-133 %REC77-146 %REC

10101010101010101010101010

2/12/2001 2/13/2001 R8729 KAL

Qualifiers: ND - Not Detected at the Reporting Limit

I - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

* - Value exceeds Maximum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

9 of 9

Page 14: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: 14-Feb-Ol

:LIENT: PENCO

•Vork Order: 0101185

'reject: Alenaio Stream Sludge

QC SUMMARY REPORTMethod Blank

Sample ID MB-3310

;iient ID:

\nalyte1 ,4-Dichlorobenzene>,4,5-Trichlorophenol1,4,6-TrichlorophenoI>,4-DinitrotolueneHexachlorobenzene•lexachlorobutadieneHexachloroethane\litrobenzeneDentachlorophenolPyridineOresols, Total

Surr: 2,4,6-TribromophenolSum 2-Fluorobiphenyl

Sum 2-FluorophenolSum 4-Terphenyl-d14Surr: Nitrobenzene-d5Sum Phenol-d6

Sample ID MB-3314

Client ID:

AnalyteMercury

Sample ID MB-3322

Client ID:

AnalyteArsenicBariumCadmiumChromiumLeadSeleniumSilver

Batch ID: 3310

ResultNDNDNDND

ND

ND

ND

ND

ND

ND

ND0.087580.043440.052140.054070.044840.03967

Batch ID: 3314

ResultND

Batch ID: 3322

ResultND

0.007915NDND

0.02312NDND

Test Code:

Run ID:

PQL DF0.010 10.010 10.050 10.010 10.010 10.010 10.010 10.010 10.050 10.010 10.010 1

0 10 10 10 10 10 1

Test Code:

Run ID:

PQL DF0.00050 1

Test Code:

Run ID:

PQL DF0.50 11.0 1

0.050 10.050 10.20 10.50 1

0.050 1

SW1311/8270A

MSD3_010209D

Spike SpikeValue RefVal

0.1 00.05 00.1 0

0.05 00.05 00.1 0

SW131 1/7470

MERC_010207B

Spike SpikeValue RefVal

SW1 31 1/601 OA

ICP1_010208C

Spike SpikeValue RefVal

Units: mg/L

SeqNo: 84478

%REC%REC Limits

'

87.6 10 12386.9 43 11652.1 21 100108 33 141

89.7 35 11439.7 10 94

Units: mg/L

SeqNo: 83958

%REC%REC Limits

Units: mg/L

SeqNo: 84274

%REC%REC Limits

Prep Date 2/7/2001

Analysis Date: 2/10/2001

RPDRefVal RPD

000000

Prep Date

RPDimit Qual Note

2/7/2001

Analysis Date: 2/7/2001

RPDRefVal RPD

Prep Date

RPDimit Qual Note

2/8/2001

Analysis Date: 2/8/2001

RPDRefVal RPD

RPDimit Qual Note

J

J

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

%REC-% Recovery

S - Spike Recovery outside established recovery limits

R - RPD outside established recovery limits

DF - Dilution Factor

RPD - Relative Percent Difference

Page 15: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

CLIENT: PENCOWork Order: 0101185Project: Alenaio Stream Sludge

QC SUMMARY REPORTMethod Blank

Sample ID BLK021301 Batch ID: R8729

Client ID:

Analyte1,1-Dichloroethene

1 ,2-Dichloroethane

1 ,4-Dichlorobenzene

2-ButanoneBenzeneCarbon tetrachlorideChlorobenzene

ChloroformTetrachloroethene

Trichloroethene

Vinyl chlorideSum 1,2-Dich!oroethane-d4Sum 4-Bromofluorobenzene

Sum Dibromofluoromethane

Sum Toluene-d8

ResultNDNDNDNDNDNDNDNDNDNDND

0.2012

0.20240.206

0.21

Test Code: SW1311/8260A

Run

PQL0.040

0.040

0.040

0.500.0400.040

0.040

0.040

0.040

0.0400.020

000

0

ID: MSD1_010213A

Spike SpikeDF Value RefVal

111111111111 0.2 01 0.2 01 0.2 01 0.2 0

Units: mg/L

SeqNo: 84734

%REC%REC Limits

101 68 144101 72 140103 76 133105 77 146

Prep Date 2/13/2001

Analysis Date: 2/13/2001

RPDRefVal

0000

RPDRPD Imit Qual Note

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

%REC - % Recovery

S - Spike Recovery outside established recovery limits

R - RPD outside established recovery limits

DF - Dilution Factor

RPD - Relative Percent Difference

Page 16: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: 14-Feb-Ol

CLIENT: PENCO

Work Order: 0101185

Project: Alenaio Stream Sludge

QC SUMMARY REPORT

Sample Matrix Spike

Sample ID 01 01 185-01 A MS Batch ID: 3314

Client ID: 1/30-2C

Analyte ResultMercury 0.0111

Sample ID 01 011 85-01 AMSD Batch ID: 3314

Client ID: 1/30-2C

Analyte ResultMercury 0.01 1 1

Sample ID 0101185-01AMS Batch ID: 3322

Client ID: 1/30-2C

Test Code:

Run ID:

PQL DF0.00050 1

Test Code:

Run ID:

PQL DF0.00050 1

Test Code:

Run ID:

SW1 31 1/7470

MERC_010207B

Spike SpikeValue RefVal

0.01 0

SW1 31 1/7470

MERC_010207B

Spike SpikeValue RefVal0.01 0

SW1 31 1/601 OA

ICP1_010208C

Units: mg/L

SeqNo: 83961

%REC%REC Limits

111 75 125

Units: mg/L

SeqNo: 83962

%REC%REC Limits

111 75 125

Units: mg/L

SeqNo: 84288

Prep Date 2/7/2001

Analysis Date: 2/7/2001

RPD RPDRefVal RPD imit Qual Note

0

Prep Date 2/7/2001

Analysis Date: 2/7/2001

RPD RPDRefVal RPD Imit Qual Note0.0111 0 20

Prep Date 2/8/2001

Analysis Date: 2/8/2001

AnalyteArsenic

BariumCadmium

Chromium

Lead

SeleniumSilver

Result0.9862

1.0991.02

0.9824

0.9867

1.10.09361

PQL0.501.0

0.0500.050

0.200.50

0.050

DF1111111

SpikeValue

111111

0.1

SpikeRefVal

00.09206

00000

%REC98.6101102

98.298.7110

93.6

%RECLimits

80808080808080

120120120120120120120

RPD RPDRefVal RPD imit Qual Note

0000000

Sample ID 0101185-01 AMSD Batch ID: 3322

Client ID: 1/30-2C

Test Code: SW1311/6010A

Run ID: ICP1 010208C

Units: mg/L

SeqNo: 84290

Prep Date 2/8/2001

Analysis Date: 2/8/2001

AnalyteArsenicBarium

Cadmium

Chromium

Lead

Selenium

Silver

Result1.0081.1071.031

0.98720.9886

1.0810.09694

PQL0.501.0

0.050

0.050

0.200.50

0.050

SpikeDF Value

1 11 11 11 11 11 11 0.1

SpikeRefVal

00.09206

00000

%REC101101103

98.798.9108

96.9

%RECLimits

808080

80808060

120120120120120120120

RPDRefVal0.9862

1.0991.02

0.98240.9867

1.10.09361

RPDRPD imit Qual Note2.16

0.744

1.080.4810.187

1.763.5

202020 *202020 *20

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

%REC - % Recovery

S - Spike Recovery outside established recovery limits

R - RPD outside established recovery limits

DF - Dilution Factor

RPD - Relative Percent Difference

Page 17: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

CLIENT: PENCO

Work Order: 0101185

Project: Alenaio Stream Sludge

QC SUMMARY REPORT

Sample Matrix Spike

Sample ID 01 01 207-01 BMS

Client ID:

Analyte1,1-Dichloroethene

Benzene

Chlorobenzene

Trichloroethene

Sum 1,2-Dichloroethane-d4

Sum 4-BromofluorobenzeneSum Dibromotluoromethane

Sum Toluene-d8

Sample ID 01 01 207-01 BMSD

Client ID:

Analyte1,1-DichloroetheneBenzene

ChlorobenzeneTrichloroethene

Sum 1 ,2-Dichloroethane-d4

Sum 4-BromofluorobenzeneSum Dibromofluoromethane

Sum Toluene-d8

Batch ID: R8729 Test Code:

Run ID:

Result0.1992

0.190.1986

0.223

0.2264

0.1978. 0.2054

0.2112

Batch ID: R8729

Result0.195

0.1848

0.19180.21760.22260.1962

0.21080.213

PQL0.040

0.040

0.040

0.040

0

0

0

0

DF1

1

1

1

1

11

1

Test Code:

Run

PQL0.0400.040

0.040

0.04000

0

0

ID:

DF11111111

SW1311/8260A

MSD1_010213A

SpikeValue

0.20.20.20.20.20.20.20.2

SpikeRefVal

000

0

0

0

0

0

SW1 31 1/8260 A

MSD1_010213A

SpikeValue

0.20.20.20.20.20.20.20.2

SpikeRefVal

00000000

Units: mg/L

SeqNo: 84748

%REC99.6

95

99.3

112

113

98.9

103

106

Units:

%RECLimits

60 140

60 140

60 140

60 140

68 144

72 140

76 133

77 146

mg/L

SeqNo: 84749

%REC97.5

92.4

95.9

109

111

98.1

105

106

%RECLimits

60 140

60 14060 140

60 140

68 144

72 140

76 133

77 146

Prep Date 2/13/2001

Analysis Date: 2/13/2001

RPDRef Val

0000

0

0

0

0

RPD

Prep Date

RPDimit Qual Note

2/13/2001

Analysis Date: 2/13/2001

RPDRefVal0.1992

0.19

0.19860.223

0

0

0

0

RPD2.132.77

3.48

2.45

0

0

0

0

RPDimit Qual252525

25

0

0

00

Note

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

%REC - % Recovery

S - Spike Recovery outside established recovery limits

R - RPD outside established recovery limits

DF - Dilution Factor

RPD - Relative Percent Difference

Page 18: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the Pacific Date: 14-Feb-Ol

CLIENT: PENCO

Work Order: 0101185

Project: Alenaio Stream Sludge

QC SUMMARY REPORTLaboratory Control Spike - generic

Sample ID LCS-3310

Client ID:

Analyte1 ,4-Dichlorobenzene

2,4-Dinitrotoluene

Pentachlorophenol

Sum 2,4,6-TribromophenolSum 2-Fluorobiphenyl

Sum 2-Fluorophenol

Sum 4-Terphenyl-d14Surr: Nitrobenzene-d5

Sum Phenol-d6

Sample ID LCSD-3310

Client ID:

Analyte1 ,4-Dichlorobenzene2,4-Dinitrotoluene.Pentachlorophenol

Surr: 2,4,6-TribromophenolSum 2-Fluorobiphenyl

Surr: 2-Fluorophenol

Sum 4-Terphenyl-d14Surr: Nitrobenzene-d5

Sum Phenol-d6

Sample ID LCS-3314

Client ID:

AnalyteMercury

Batch ID: 3310

Result0.0175

0.018250.0444

0.08517

0.04248

0.05343

0.04903

0.044780.04236

Batch ID: 3310

Result0.018630.01825

0.047860.086570.045860.05611

0.047030.046660.04122

Batch ID: 3314

Result0.011

Test Code:

Run ID:

PQL0.0100.0100.050

000000

DF1

1

1

1

1

1

1

1

1

Test Code:

Run

PQL0.0100.0100.050

0000

00

ID:

DF111111111

Test Code:

Run

PQL0.00050

ID:

DF1

SW1311/8270A

MSD3_010209D

SpikeValue0.025

0.025

0.050.1

0.050.1

0.05

0.05

0.1

SpikeRefVal

0

0

0

0

0

0

0

0

0

SW1311/8270A

MSD3_010209D

SpikeValue0.0250.0250.050.1

0.050.1

0.05

0.050.1

SpikeRefVal

00000

00

00

SW1 31 1/7470

MERC_

SpikeValue

0.01

010207B

SpikeRefVal

0

Units: mg/L

SeqNo: 84479

%REC7073

88.885.2

8553.498.189.642.4

Units:

%RECLimits

36 9724 969 103

10 12343 11621 10033 14135 11410 94

mg/L

SeqNo: 84480

%REC74.5

7395.786.691.756.194.193.341.2

Units:

%RECLimits

36 9724 969 103

10 12343 11621 10033 14135 11410 94

mg/L

SeqNo: 83959

%REC110

%RECLimits

80 120

Prep Date 2/7/2001

Analysis Date: 2/10/2001

RPDRefVal

000000000

Prep

RPD

Date

RPDimit Qual

J

Note

2/7/2001

Analysis Date: 2/10/2001

RPDRefVal0.0175

0.018250.0444

000000

RPD6.26

00000000

Prep Date

RPDimit Qual131327 J000000

Note

2/7/2001

Analysis Date: 2/7/2001

RPDRefVal

0RPD

RPDimit Qual Note

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

%REC - % Recovery

S - Spike Recovery outside established recovery limits

R - RPD outside established recovery limits

DF - Dilution Factor

RPD - Relative Percent Difference

Page 19: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

CLIENT:Work Order:Project:

PENCO0101185Alenaio Stream Sludge

QC SUMMARY REPORTLaboratory Control Spike - generic

Sample ID LCS-3322

Client ID:

Batch ID: 3322 Test Code: SW1311/6010A

Run ID: ICP1 010208C

Units: mg/L

SeqNo: 84281

Prep Date 2/8/2001

Analysis Date: 2/8/2001

AnalyteArsenic

Barium

Cadmium

ChromiumLead

SeleniumSilver

Result1.0041.0151.017

0.9769

0.97271.042

0.0942

PQL0.50

1.0

0.050

0.050

0.20

0.50

0.050

DF1

11

1

1

1

1

SpikeValue

• 111111

0.1

SpikeRefVal

00.00792

00

0.02312

00

%REC100

101

102

97.7

95

104

94.2

%RECLimits

80 12080 12080 12080 12080 12080 12080 120

RPD RPDRefVal RPD imit Qual Note

0000000

Sample ID LCS021301 Batch ID: R8729

Client ID:

Analyte1,1-DichloroetheneBenzeneChlorobenzene

Trichloroethene

Sum 1,2-Dichloroethane-d4

Surr: 4-BromofluorobenzeneSurr: Dibromofluoromethane

Sum Toluene-d8

Result0.21580.19060.2004

0.20220.2004

0.2016

0.2066

0.2106

Test Code:

Run ID:

PQL0.0400.0400.040

0.0400

0

0

0

DF1

11

11

1

1

1

SW1311/8260A

MSD1JM0213A

SpikeValue

0.20.20.20.20.20.20.20.2

SpikeRefVal

00000000

Units: mg/L

SeqNo: 84733

%REC%REC

0000

100101103105

Limits6570707068727677

135130130130144140133146

Prep Date 2/13/2001

Analysis Date: 2/13/2001

RPD RPDRefVal RPD imit Qual Note

00000000

Qualifiers: ND - Not Detected at the Reporting Limit

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

%REC - % Recovery

S - Spike Recovery outside established recovery limits

R - RPD outside established recovery limits

DF - Dilution Factor

RPD - Relative Percent Difference

Page 20: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

Environmental Laboratory of the ?ac\fic

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Page 21: Laboratory rpt, Alenaio Stream sludge, 3 samples collected ...Environmental Laboratory of the Pacific Date: Febl4,2001 Client: PENCO Work Order: 0101185 Project: Alenaio Stream Sludge

STATE OF HAWAII,t. DEPARTMENT OF HEALTH*' ENVIRONMENTAL HEALTH ADMINISTRATION

FFICE OF HAZARD EVALUATION AND EMERGENCY RESPONSE

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