limited phase ii environmental site...

Limited Phase II Environmental Site Assessment

L and M Land, LLC

August 19, 2016

Prepared By:

P. O. Box 1407

Long Beach, MS 39560

(228) 518-0905

Prepared For:

L and M Land, LLC

7412 Kome Place

Diamondhead, MS 39525

Subject Site Description: Parcel H and Lot 8 (or Lot 9 Blk 103), Block 103 Gulfview Subdivsion

Also Known As Parcel: 164Q-0-20-017.000;

Lots 1 and 2, and Part of Lots 3-8, Block 102 Gulfview Subdivsion


Lots 1-6 and 9-16, Block 94 Gulfview Subdivsion


Lakeshore, Hancock County, MS

Prepared by:

Culpeper and Associates, LLC

P. O. Box 1407

Long Beach, MS 39560

(228) 518-0905

Date: August 19, 2016

TABLE OF CONTENTS

1. Executive Summary

2. Introduction

2.1 Background

2.2 General Site Description

2.3 Standard of Care

2.4 Assumptions

2.5 Reliance

2.6 Limiting Conditions and Methodologies Used

3. Field Activities and Methods

4. Results

4.1 Observations of Site and Soil Sample Characteristics

4.2 Soil Sample Analytical Results

5. Recommendations

APPENDICES

Appendix A Warranty Deeds and Survey Plat

Quadrangle Map

Google Earth Aerial With Sample Locations

Appendix B Analytical Data Tables (3)

Table For Samples 1-11



Appendix C Laboratory Analytical Report and Supporting

Documentation

1.0 Executive Summary

A Limited Phase II Environmental Site Assessment (ESA) was completed by Culpepper

and Associates, LLC during June and July 2016 at the site owned by L and M Land, LLC

in Hancock County, MS. As a result of the Macondo Canyon 252 (MC252) crude oil

spill event beginning in April 2010, contamination to the adjacent Gulf of Mexico, its

tributaries, and shorelines occurred. After multiple storm surge events in summer 2010,

some of the residual oil persisting on the shoreline near the subject site was carried inland

into the bayous, estuaries, and adjacent lands. Presence of MC252 contamination has

been established on the subject site1. Consequently, a Phase II ESA was requested by the

interest owner of the subject site, L and M Land, LLC. Limited sampling was conducted

in order to determine the present contamination condition of the soils impacted by crude

contaminated storm surge. Analytical results were screened for each chemical of concern

(COC) utilizing the lowest applicable Tier 1 Target Remediation Goal (TRG) identified

by Mississippi Department of Environmental Quality’s Risk Evaluation Procedures For

Voluntary Cleanup and Redevelopment of Brownfield Sites. The presence of

contamination below the applicable TRG was confirmed. The presence of contamination

above the applicable TRG’s was not identified by any of the samples collected. Based on

the results of this Limited Phase II ESA no further testing is recommended. The

remediation recommendations of Pardue should be completed if not already done so.

2.0 Introduction

Culpepper and Associates, LLC has completed a Limited Phase II Environmental Site

Assessment (ESA) at an approximate 6.1-acre vacant property located in Lakeshore,

Hancock County, MS on behalf of L and M Land, LLC.

The purpose of this Limited Phase II ESA was to evaluate the potential for Recognized

Environmental Conditions (RECs) that may exist as a result of the MC252 event for the

purpose of providing sufficient information regarding the nature and extent of any

potential contamination and to assist in making informed business decisions about the

property; and where applicable, providing the level of knowledge necessary to satisfy the

innocent purchaser defense under The Comprehensive Environmental Response,

Compensation, and Liability Act (CERCLA).

2.1 Background

The subject site is approximately 6.1 acres in size and is vacant property owned by Curtis

W. Murray per online tax assessor land records and is located adjacent to tidally affected

waterways in Lakeshore, Hancock County, MS. Beginning on April 20, 2010, The

Macondo Well Blowout, aka Deepwater Horizon Oil Spill, BP Oil Spill, etc. (MC252),

began releasing heavy crude as a result of control failure until control was regained in

1 Pardue, John H., Evaluation of the presence of MC252 oil on private properties located in Lakeshore, MS,

October 12, 2011.

July 2010 and declared sealed in late summer 2010. Moderate oil contamination of the

Lakeshore Beach was confirmed as indicated by Pardue. Concurrent with the MC252

event, two named tropical events occurred in June and July 2010, Hurricane Alex and

Hurricane Bonnie. Consequently, tidal surge inundated the tidal tributaries, marshes, and

adjacent private lands including the subject site located west of the seawall and Beach

Boulevard.

An investigation was conducted at the subject site in 2011 by John Pardue, PHD, PE.

The evaluation was conducted to “assess whether residual oil contamination remained on

these properties and it could be remediated”. Pardue summarized as a result of the

investigation that “Three locations were identified with potential crude oil

contamination.2

Due to the previous investigative results, the property owner requested that a limited

Phase II ESA be conducted to evaluate any potential contamination of the subject site

above Tier 1 TRG’s.

2.2 General Site Description

The subject site (Site) is comprised of approximately 6.1 acres located in Lakeshore,

Hancock County, MS. The site’s legal description is provided in the two Warranty Deeds

in Appendix A. The parcel numbers of the subject site provided by Hancock County

Assessor Geoportal is as follows, 164Q-0-20-017.000, 164Q-0-20-014.000, and 164Q-0-

20-002.000. The site also contains abandoned public rights-of-way.

The site is situated in the area of Lakeshore, MS and is a conglomeration of several

properties. The site is a part of Gulfview Subdivision which consists of numerous

undeveloped properties that appear to have been subdivided without consideration of

landscape constraints and on a strict grid pattern.

The landscape of the site includes tidally influenced waterways, estuarine marsh,

manmade upland, and natural chenier upland, and road and parking area adjacent to the

site on the east. A tidally influenced ditch was excavated many years ago and bisects the

site. Many spoil mounds are located adjacent to the manmade ditches. The site is inland

of a manmade seawall that was constructed along the waterfront to protect Beach Blvd.

from erosion. The seawall is located landward of a manmade beach. The tidal influence

is from Bayou Cadet to the south of the site approximately 0.5 miles. The site’s

elevations generally range from approximately +1’ (subject to mean high tide survey) to

+8’ MSL, and the site periodically experiences exposure to supratidal inundation from

storm generated surge events. Maps and aerial photographs are located in Appendix A.

2 Pardue, John H., Evaluation of the presence of MC252 oil on private properties located in Lakeshore, MS,

October 12, 2011.

2.3 Standard of Care

Culpepper and Associates’ services were performed in a manner consistent with

generally accepted practices of the profession undertaken in similar studies in the same

geographical area during the same period of time. Culpeper and Associates, LLC makes

no warranties, either express or implied, regarding the findings, conclusions or

recommendations.

Note that Culpepper and Associates does not warrant the work of laboratories, regulatory

agencies or other third parties supplying information used in the preparation of the report.

These Limited Phase II ESA services were performed in accordance with the Scope of

Work agreed with you, our client, as reflected in our proposal and were not restricted by

ASTM E1903-11.

2.4 Assumptions

Culpepper and Associates assumes the Property has been correctly and accurately

identified by the User.

Culpepper and Associates assumes that the User and any of its designated representatives

used good faith in answering questions about and in obtaining information for the

Property.

This report is not a comprehensive site characterization and should not be construed as

such. Conclusions reached regarding the conditions of the Property do not represent a

warranty that all areas within the Property are of a similar quality as may be inferred from

observable Property conditions and available Property history.

2.5 Reliance

This assessment was conducted on behalf of and for the exclusive use of L and M Land,

LLC. This report, and the findings contained herein, shall not, in whole or part, be

disseminated or conveyed to or used by any other party without the prior written consent

of Culpepper and Associates, LLC

2.6 Limiting Conditions and Methodologies Used

No ESA can eliminate all uncertainty. Furthermore, any sample, either surface or

subsurface, taken for chemical analysis may or may not be representative of a larger

population. Professional judgment and interpretation are inherent in the process and

uncertainty is inevitable. Additional assessment may be able to reduce the uncertainty.

Even when Phase II ESA work is executed with an appropriate site-specific standard of

care, certain conditions present especially difficult detection problems. Such conditions

may include, but are not limited to, complex geological settings, the fate and transport

characteristics of certain hazardous substances and petroleum products, the distribution of

existing contamination, physical limitations imposed by the location of utilities and other

man-made objects, and the limitations of assessment technologies.

Phase II ESAs do not generally require an exhaustive assessment of environmental

conditions on a property. There is a point at which the cost of information obtained and

the time required to obtain it outweigh the usefulness of the information and, in fact, may

be a material detriment to the orderly completion of transactions. If hazardous substance

or petroleum releases are confirmed on a parcel of property, the extent of further

assessment is related to the degree of uncertainty that is acceptable to the User with

respect to the real estate transaction.

Measurements and sampling data only represent the site conditions at the time of data

collection. Therefore, the usability of data collected as part of this Phase II ESA may

have a finite lifetime depending on the application and use being made of the data. An

Environmental Professional should evaluate whether the generated data are appropriate

for any subsequent use beyond the original purpose for which it was collected.

3.0 Field Activities and Methods

Culpepper and Associates, LLC conducted field activities June 22, 29, and July 5, 2016.

Initially, a site visit was conducted to evaluate the site for obvious signs of oil

contamination, to evaluate site characteristics, and to plan the sampling protocol. Upon

completion, the field approach for sample collection was developed. Accessibility was

limited in areas inundated by tidal waters located west of the ditch in the marsh, thus it

was not practicable to sample in much of this area. The remaining portion of the site was

sampled on transects and at 100-foot intervals along those transects where practicable. A

limited number of 27 sample locations were identified along these transects where access

allowed. In areas of restricted access, the sample was relocated to the closest accessible

area. During sampling activities, composite samples were acquired by hand auger at the

27 locations to a depth of 24”. Composite samples were placed in 27 clean glass

containers and subsequently labeled. The samples were given standard care during

possession prior to delivery to the laboratory. Sampling activities and product

descriptions were recorded, sampling sites were marked with pin flags and flagging tape,

and GPS coordinates were recorded at each site. Standard decontamination procedures

were conducted after each sample collection. There were no other sampling plan

deviations.

The 27 samples were delivered to Gulf Coast Analytical Laboratories, LLC of Baton

Rouge, LA for semi-volatiles mass spectrometry (EPA 8270C SIM) and semi-volatiles

gas chromatography (EPA 8015C DRO) analysis as described in the report and chain of

custody located in Appendix C. The laboratory analysis was conducted for diesel range

organic (DRO) compounds and polycyclic aromatic hydrocarbon (PAH) compounds

typically found in petroleum and crude based materials.

4.0 Results

4.1 Observations of Site and Soil Sample Characteristics

The 27 sample sites were located in estuarine wetland, and non-wetland areas. Most

sample sites were vegetated and were covered with various organic leaf litter and/or

detrital matter. An area near the east property boundary contained un-vegetated fill

material. The fill generally is clean fine sandy fill, however some broken asphalt was

observed on the surface in a small limited area. Soil sample locations can be found

presented as Appendix A. The soil lithology observed at the sample sites generally

consists of organics, sand, sand, sandy silt, sandy clay, silt, silty sand, silty clay, clayey

silt, clayey sand, and clay to 24” depth below land surface. The samples ranged from

saturated in wetland areas to dry in upland areas. A majority of the samples contained

some moisture but were not saturated. Redoximorphic features were prevalent in

samples collected from apparent wetland areas. No areas of obvious oiling or

contamination were identified in the field.

4.2 Soil Sample Analytical Results

Soil samples 1 through 27 that were collected as described above were evaluated at

GCAL utilizing semi-volatiles mass spectrometry (EPA 8270C SIM) and semi-volatiles

gas chromatography (EPA 8015C DRO) analysis to quantitatively determine the presence

of PAH and DRO in the samples.

The appropriate benchmark for screening analytical results is the lowest applicable Tier 1

unrestricted TRG’s. GCAL analysis of the soil samples collected at the subject site did

detect the presence of some COC constituents. GCAL analysis of the soil samples

collected at the subject site did not report concentrations of COC’s above TRG’s

published by MDEQ. The GCAL Laboratory Analytical Report is presented as Appendix

C. Summary tables of the GCAL analysis can be found presented as Appendix B.

5.0 Recommendations

This recommendation is based upon the results of the analysis conducted by GCAL of the

27 samples collected at the subject site and screening against MDEQ Tier 1 TRG’s for

unrestricted sites. Due to all samples being below respective TRG’s, no further testing is

recommended. The remediation plan recommended by Pardue should be completed if

not already done so.

APPENDIX A

MAPS & FIGURES (3)

APPENDIX B

ANALYTICAL DATA TABLES (3)

APPENDIX C

LABORATORY ANALYTICAL REPORT

L and M Land, LLC. USGS Quadrangle 7.5’ Series, St. Joe Pass

MDEQ Tier 1 TRG MDEQ Tier I TRG

SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7 SB-8 SB-9 SB-10

0-2' BLS 0-2' BLS 0-2' BLS 0-2' BLS 0-2' BLS 0-2' BLS 0-2' BLS 0-2' BLS 0-2' BLS 0-2' BLS

--- TPH ---

Diesel Range Organics 1.77 J 1.99 J < 1.31 1.34 J < 1.31 < 1.30 3.52 J < 1.31 < 1.29 2.55 J 350 300

--- PAH ---

1-Methylnaphthalene < 0.000837 < 0.000840 < 0.000840 < 0.000840 < 0.000840 < 0.000840 < 0.000840 < 0.000829 < 0.000840 < 0.000840 -- --

2-Methylnaphthalene < 0.000837 < 0.000840 < 0.000840 < 0.000840 < 0.000840 < 0.000840 < 0.000840 < 0.000829 < 0.000840 < 0.000840 40,900 1,560

Acenaphthene < 0.00164 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00163 < 0.00165 < 0.00165 123,000 4,690

Acenaphthylene < 0.00164 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00163 < 0.00165 < 0.00165 123,000 4,690

Anthracene 0.00300 J 0.000476 J 0.000531 J 0.000793 J 0.000597 J < 0.000420 0.00104 J < 0.000414 < 0.000420 0.00130 J 613,000 23,500

Benzo(a)anthracene 0.013 0.00303 J < 0.00165 0.00214 J 0.00222 J < 0.00165 0.00242 J < 0.00163 < 0.00165 0.00228 J 7.84 0.875

Benzo(a)pyrene 0.014 0.00324 J 0.000858 J 0.00248 J 0.00233 J 0.00118 J 0.00197 J 0.000435 J < 0.000420 0.00238 J 0.784 0.0875

Benzo(b)fluoranthene 0.018 0.0042 < 0.00165 0.00463 0.00278 J < 0.00165 0.00411 < 0.00163 < 0.00165 0.00482 7.84 0.875

Benzo(g,h,i)perylene 0.00716 < 0.000840 < 0.000840 < 0.000840 0.00207 J < 0.000840 < 0.000840 < 0.000829 < 0.000840 < 0.000840 61,300 2,350

Benzo(k)fluoranthene 0.00705 0.00195 J 0.000795 J 0.00166 J 0.00113 J 0.000924 J 0.00157 J < 0.000414 < 0.000420 0.00169 J 78.4 8.75

Chrysene 0.017 0.00341 < 0.00165 0.00332 0.00239 J < 0.00165 0.00335 < 0.00163 < 0.00165 0.00380 784 87.5

Dibenz(a,h)anthracene 0.00445 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00165 < 0.00163 < 0.00165 < 0.00165 0.784 0.0875

Fluoranthene 0.034 0.00389 0.000918 J 0.00400 0.00424 0.00166 J 0.00405 < 0.000414 < 0.000420 0.00475 81,700 3,130

Fluorene 0.000986 J < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000414 < 0.000420 < 0.000420 81,700 3,130

Indeno(1,2,3-cd)pyrene 0.011 < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000414 < 0.000420 < 0.000420 7.84 0.875

Naphthalene 0.000436 J < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000420 < 0.000414 < 0.000420 < 0.000420 247 194

Phenanthrene 0.021 < 0.000840 < 0.000840 0.00140 J 0.00160 J < 0.000840 0.00106 J < 0.000829 < 0.000840 0.00138 J 61,300 2,350

Pyrene 0.031 0.00353 < 0.000840 0.00321 J 0.00375 0.00136 J 0.00358 < 0.000829 < 0.000840 0.00376 61,300 2,350

Notes:

LAKESHORE, HANCOCK COUNTY, MISSISSIPPI

LABORATORY ANALYTICAL SUMMARY

SOUTH BEACH BOULEVARD SITE

Data Reporting Qualifiers:

Regulatory Comparison

Unrestricted = Refers to the use of the site (ie. unrestricted use may be used as residential or industrial/commercial)

TPH = Total Petroleum Hydrocarbons

PAH = Polynuclear Aromatic Hydrocarbons

-- = No established regulatory value

Tier 1 TRG = Target Remediation Goal (TRG) protective of human health and the environment for restricted use and unrestricted use of a site, established in February 28, 2002.

All concentrations are reported in mg/kg.

BLS = Below Land Surface

J = Indicates the result is between the laboratory Method Detection Limit (MDL) and the laboratory Limit of Quantitation (LOQ).

Sample Information

Compounds Soil - Restricted Soil - Unrestricted

Restricted = Refers to the use of a site (ie. restricted use may be used as industrial/commercial)

NA = Not Analyzed

Regulatory Comparison is for informational purposes only.

Refer to the complete analytical laboratory report for a complete report of the results.

MDEQ = Mississippi Department of Environmental Quality.

Page 1 of 1

P. O. Box 1407

Long Beach, MS 39560 (228) 518-0905

[email protected]

August 19, 2016

Mr. Kirk Ladner

L and M Land, LLC

7412 Kome Place

Diamondhead, MS 39525

RE: Phase II ESA For Approximately 6.1 Acres Adjacent To South Beach Blvd., Hancock

County, MS; Invoice # 16020

For professional services rendered, please remit for the following:

Services Fee/Time

1) Project Manager/ Sr. Scientist 38.0 Hrs @ $125.00/ Hr. $4,750.00

2) Project Geologist 27.50 Hrs @ $100.00/Hr. $2,750.00

3) Laboratory Analysis: PAH and DRO (TPH) $4,400.00

Subtotal: $11,900.00

PM Adjustment For Budget* ($1,900.00)

Retainer: ($2,500.00)

Total Due: $7,500.00

*The adjustment for budget was due to a change in sampling protocol after project commencement.

After in-depth site evaluation it was decided to increase the number of samples and broaden the

constituent range from initial proposal planning to gain a greater level of confidence in the study

results. This cost change was absorbed by adjustment to PM labor costs.

Thank you for the opportunity to provide your planning and environmental services.

Culpepper and Associates, LLC

Billy J. Culpepper

Cover

ANALYTICAL RESULTS

PERFORMED BY

GCAL, LLC 7979 Innovation Park Dr. Baton Rouge, LA 70820

Report Date 07/21/2016

GCAL Report 216070103

9999999999

Project South Beach Blvd Site 16.09350

Deliver To Additional Recipients Phillip Foster NONE Geo Terra Engineering PO Box 40515 Mobile, AL 36640 (251)422-9756

NELAP CERTIFICATE NUMBER: 01955

DOD ELAP CERTIFICATE NUMBER: L14-243

Page 1 of 49GCAL Report#: 216070103

Revision 2

Report#: 216070103

Project ID: South Beach Blvd Site 16.09350 Report Date: 07/21/2016

Laboratory Endorsement Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.

Common Abbreviations that may be Utilized in this Report

ND Indicates the result was Not Detected at the specified reporting limit DO Indicates the result was Diluted Out MI Indicates the result was subject to Matrix Interference TNTC Indicates the result was Too Numerous To Count SUBC Indicates the analysis was Sub-Contracted FLD Indicates the analysis was performed in the Field DL Detection Limit DL Diluted analysis – when appended to Client Sample ID LOD Limit of Detection LOQ Limit of Quantitation RE Re-analysis CF HPLC or GC Confirmation 00:01 Reported as a time equivalent to 12:00 AM

Reporting Flags that may be Utilized in this Report

J or I Indicates the result is between the MDL and LOQ J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria U Indicates the compound was analyzed for but not detected B or V Indicates the analyte was detected in the associated Method Blank Q Indicates a non-compliant QC Result (See Q Flag Application Report) * Indicates a non-compliant or not applicable QC recovery or RPD – see narrative E The result is estimated because it exceeded the instrument calibration range E Metals - % diference for the serial dilution is > 10% P RPD between primary and confirmation result is greater than 40

Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results are presented within this report. This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited. I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following signature. Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if applicable.

Authorized Signature GCAL Report 216070103


Revision 2

Report#: 216070103


Certifications

Certification Certification Number

DOD ELAP L14-243

Alabama 01955

Arkansas 12-060-0

Colorado 01955

Delaware 01955

Florida E87854

Georgia 01955

Hawaii 01955

Idaho 01955

Illinois 200048

Indiana 01955

Kansas E-10354

Kentucky 95

Louisiana 01955

Maryland 01955

Massachusetts 01955

Michigan 01955

Mississippi 01955

Missouri 01955

Montana N/A

Nebraska 01955

New Mexico 01955

North Carolina 618

North Dakota R-195

Oklahoma 9403

South Carolina 73006001

South Dakota 01955

Tennessee 01955

Texas T104704178

Vermont 01955

Virginia 460215

USDA Soil Permit P330-10-00117


Revision 2

Report#: 216070103


Case Narrative

Client: Gulf Coast Labnet Report: 216070103

Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed on the Report Sample Summary page of this report. Receipt of the sample(s) is documented by the attached chain of custody. This applies only to the sample(s) listed in this report. No sample integrity or quality control exceptions were identified unless noted below.

This report was revised 07/20/16. Samples included in GCAL 217070913 are moved to this report.

This report was revised 07/19/16. DRO was added as a reportable analyte to all samples.

SEMI-VOLATILES MASS SPECTROMETRY

In the EPA 8270C SIM analysis, the recoveries for the surrogates are below the lower control limit for sample 21607010315 (SB-15). The sample was re-extracted and re-analyzed with similar recoveries.

In the EPA 8270C SIM analysis, samples 21607010311 (SB-11), 21607010313 (SB-13), 21607010316 (SB-16), 21607010319 (SB-19), 21607010321 (SB-21) and 21607010308 (SB-8) had one surrogate recovery outside control limits in the base-neutral fraction.

SEMI-VOLATILES GAS CHROMATOGRAPHY

In the EPA 8015C DRO analysis, the recovery for the surrogate is below the lower control limit for samples 21607010306 (SB-6), 21607010309 (SB-9), 21607010311 (SB-11), 21607010313 (SB-13), 21607010314 (SB-14), 21607010315 (SB-15), 21607010316 (SB-16), 21607010317 (SB-17), 21607010319 (SB-19), 21607010320 (SB-20), 21607010321 (SB-21) 21607091302 (SB-23), 21607091304 (SB-25), and 21607091305 (SB-26). The samples were re-extracted and re-analyzed with similar recoveries for the surrogate.


Revision 2

Report#: 216070103


Sample Summary

GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time

21607010301 SB-1 Solid 06/29/2016 12:58 07/01/2016 09:55

21607010302 SB-2 Solid 06/29/2016 13:08 07/01/2016 09:55

21607010303 SB-3 Solid 06/29/2016 13:22 07/01/2016 09:55

21607010304 SB-4 Solid 06/29/2016 13:41 07/01/2016 09:55

21607010305 SB-5 Solid 06/29/2016 13:55 07/01/2016 09:55

21607010306 SB-6 Solid 06/29/2016 14:12 07/01/2016 09:55

21607010307 SB-7 Solid 06/29/2016 14:32 07/01/2016 09:55

21607010308 SB-8 Solid 06/29/2016 14:41 07/01/2016 09:55

21607010309 SB-9 Solid 06/29/2016 14:52 07/01/2016 09:55

21607010310 SB-10 Solid 06/29/2016 15:10 07/01/2016 09:55

21607010311 SB-11 Solid 06/29/2016 15:24 07/01/2016 09:55

21607010312 SB-12 Solid 06/29/2016 15:32 07/01/2016 09:55

21607010313 SB-13 Solid 06/29/2016 15:43 07/01/2016 09:55

21607010314 SB-14 Solid 06/29/2016 16:03 07/01/2016 09:55

21607010315 SB-15 Solid 06/29/2016 16:13 07/01/2016 09:55

21607010316 SB-16 Solid 06/29/2016 16:29 07/01/2016 09:55

21607010317 SB-17 Solid 06/29/2016 16:36 07/01/2016 09:55

21607010318 SB-18 Solid 06/29/2016 17:17 07/01/2016 09:55

21607010319 SB-19 Solid 06/29/2016 17:06 07/01/2016 09:55

21607010320 SB-20 Solid 06/29/2016 17:01 07/01/2016 09:55

21607010321 SB-21 Solid 06/29/2016 16:41 07/01/2016 09:55

21607091301 SB-22 Solid 07/05/2016 10:12 07/09/2016 10:38

21607091302 SB-23 Solid 07/05/2016 10:31 07/09/2016 10:38

21607091303 SB-24 Solid 07/05/2016 10:47 07/09/2016 10:38

21607091304 SB-25 Solid 07/05/2016 11:10 07/09/2016 10:38

21607091305 SB-26 Solid 07/05/2016 11:25 07/09/2016 10:38

21607091306 SB-27 Solid 07/05/2016 12:05 07/09/2016 10:38


Revision 2

Report#: 216070103


Detect Summary

Summary of Compounds Detected SB-1

SB-1 Collect Date 06/29/2016 12:58 GCAL ID 21607010301

Receive Date 07/01/2016 09:55 Matrix Solid

EPA 8270C SIM

EPA 8270C SIM

CAS# Parameter Result DL LOQ Units

120-12-7 Anthracene 0.00300J 0.000419 0.00329 mg/kg 56-55-3 Benzo(a)anthracene 0.013 0.00164 0.00329 mg/kg 50-32-8 Benzo(a)pyrene 0.014 0.000419 0.00329 mg/kg 205-99-2 Benzo(b)fluoranthene 0.018 0.00164 0.00329 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00716 0.000837 0.00329 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00705 0.000419 0.00329 mg/kg 218-01-9 Chrysene 0.017 0.00164 0.00329 mg/kg 53-70-3 Dibenz(a,h)anthracene 0.00445 0.00164 0.00329 mg/kg 206-44-0 Fluoranthene 0.034 0.000419 0.00329 mg/kg 86-73-7 Fluorene 0.000986J 0.000419 0.00329 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene 0.011 0.000419 0.00329 mg/kg 91-20-3 Naphthalene 0.000436J 0.000419 0.00329 mg/kg 85-01-8 Phenanthrene 0.021 0.000837 0.00329 mg/kg 129-00-0 Pyrene 0.031 0.000837 0.00329 mg/kg

EPA 8015C DRO

EPA 8015C DRO


GCSV-00-4 Diesel Range Organics 1.77J 1.30 3.99 mg/kg

SB-2



EPA 8270C SIM

EPA 8270C SIM


120-12-7 Anthracene 0.000476J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00303J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00324J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00420 0.00165 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00195J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00341 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00389 0.000420 0.00330 mg/kg 129-00-0 Pyrene 0.00353 0.000840 0.00330 mg/kg


Revision 2

Report#: 216070103


Summary of Compounds Detected



EPA 8015C DRO

EPA 8015C DRO



SB-3



EPA 8270C SIM

EPA 8270C SIM


120-12-7 Anthracene 0.000531J 0.000420 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.000858J 0.000420 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.000795J 0.000420 0.00330 mg/kg 206-44-0 Fluoranthene 0.000918J 0.000420 0.00330 mg/kg

SB-4



EPA 8270C SIM

EPA 8270C SIM


120-12-7 Anthracene 0.000793J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00214J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00248J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00463 0.00165 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00166J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00332 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00400 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00140J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00321J 0.000840 0.00330 mg/kg

EPA 8015C DRO

EPA 8015C DRO




Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


120-12-7 Anthracene 0.000597J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00222J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00233J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00278J 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00207J 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00113J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00239J 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00424 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00160J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00375 0.000840 0.00330 mg/kg

SB-6



EPA 8270C SIM

EPA 8270C SIM


50-32-8 Benzo(a)pyrene 0.00118J 0.000420 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.000924J 0.000420 0.00330 mg/kg 206-44-0 Fluoranthene 0.00166J 0.000420 0.00330 mg/kg 129-00-0 Pyrene 0.00136J 0.000840 0.00330 mg/kg

SB-7



EPA 8270C SIM

EPA 8270C SIM


120-12-7 Anthracene 0.00104J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00242J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00197J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00411 0.00165 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00157J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00335 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00405 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00106J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00358 0.000840 0.00330 mg/kg


Revision 2

Report#: 216070103





EPA 8015C DRO

EPA 8015C DRO



SB-8



EPA 8270C SIM

EPA 8270C SIM


50-32-8 Benzo(a)pyrene 0.000435J 0.000414 0.00326 mg/kg

SB-10



EPA 8270C SIM

EPA 8270C SIM


120-12-7 Anthracene 0.00130J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00228J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00238J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00482 0.00165 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00169J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00380 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00475 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00138J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00376 0.000840 0.00330 mg/kg

EPA 8015C DRO

EPA 8015C DRO




Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


56-55-3 Benzo(a)anthracene 0.00199J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00209J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00220J 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00122J 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.000923J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00188J 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00307J 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene 0.00523 0.000420 0.00330 mg/kg 129-00-0 Pyrene 0.00267J 0.000840 0.00330 mg/kg

SB-12



EPA 8015C DRO

EPA 8015C DRO



SB-13



EPA 8270C SIM

EPA 8270C SIM


206-44-0 Fluoranthene 0.000936J 0.000417 0.00328 mg/kg 129-00-0 Pyrene 0.000894J 0.000834 0.00328 mg/kg

SB-14



EPA 8270C SIM

EPA 8270C SIM


208-96-8 Acenaphthylene 0.00185J 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.00342 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00482 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00554 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00888 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00387 0.000840 0.00330 mg/kg


Revision 2

Report#: 216070103





EPA 8270C SIM (Continued)


207-08-9 Benzo(k)fluoranthene 0.00339 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00733 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.016 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene 0.00768 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00451 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.012 0.000840 0.00330 mg/kg

SB-15



EPA 8270C SIM

EPA 8270C SIM


120-12-7 Anthracene 0.000585J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00232J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00223J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00286J 0.00165 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00132J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00292J 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00588 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00232J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00557 0.000840 0.00330 mg/kg

SB-17



EPA 8270C SIM

EPA 8270C SIM


206-44-0 Fluoranthene 0.000484J 0.000420 0.00330 mg/kg

SB-18



EPA 8270C SIM

EPA 8270C SIM


50-32-8 Benzo(a)pyrene 0.000823J 0.000416 0.00327 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00182J 0.00163 0.00327 mg/kg


Revision 2

Report#: 216070103







207-08-9 Benzo(k)fluoranthene 0.000755J 0.000416 0.00327 mg/kg 206-44-0 Fluoranthene 0.00191J 0.000416 0.00327 mg/kg 129-00-0 Pyrene 0.00169J 0.000832 0.00327 mg/kg

EPA 8015C DRO

EPA 8015C DRO


GCSV-00-4 Diesel Range Organics 4.35 1.31 4.00 mg/kg

SB-19



EPA 8270C SIM

EPA 8270C SIM


50-32-8 Benzo(a)pyrene 0.000696J 0.000420 0.00330 mg/kg 206-44-0 Fluoranthene 0.00148J 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.000940J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00154J 0.000840 0.00330 mg/kg

SB-20



EPA 8270C SIM

EPA 8270C SIM


207-08-9 Benzo(k)fluoranthene 0.00129J 0.000419 0.00329 mg/kg

SB-23



EPA 8270C SIM

EPA 8270C SIM


191-24-2 Benzo(g,h,i)perylene 0.00170J 0.000834 0.00328 mg/kg 53-70-3 Dibenz(a,h)anthracene 0.00166J 0.00164 0.00328 mg/kg


Revision 2

Report#: 216070103







193-39-5 Indeno(1,2,3-cd)pyrene 0.00156J 0.000417 0.00328 mg/kg

SB-27



EPA 8270C SIM

EPA 8270C SIM


206-44-0 Fluoranthene 0.000648J 0.000416 0.00327 mg/kg


Revision 2

Report#: 216070103


Sample Results

Sample Results SB-1



EPA 8270C SIM

EPA 8270C SIM

Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch

07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 15:14 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000837 0.00329 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000837 0.00329 mg/kg 83-32-9 Acenaphthene ND 0.00164 0.00329 mg/kg 208-96-8 Acenaphthylene ND 0.00164 0.00329 mg/kg 120-12-7 Anthracene 0.00300J 0.000419 0.00329 mg/kg 56-55-3 Benzo(a)anthracene 0.013 0.00164 0.00329 mg/kg 50-32-8 Benzo(a)pyrene 0.014 0.000419 0.00329 mg/kg 205-99-2 Benzo(b)fluoranthene 0.018 0.00164 0.00329 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00716 0.000837 0.00329 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00705 0.000419 0.00329 mg/kg 218-01-9 Chrysene 0.017 0.00164 0.00329 mg/kg 53-70-3 Dibenz(a,h)anthracene 0.00445 0.00164 0.00329 mg/kg 206-44-0 Fluoranthene 0.034 0.000419 0.00329 mg/kg 86-73-7 Fluorene 0.000986J 0.000419 0.00329 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene 0.011 0.000419 0.00329 mg/kg 91-20-3 Naphthalene 0.000436J 0.000419 0.00329 mg/kg 85-01-8 Phenanthrene 0.021 0.000837 0.00329 mg/kg 129-00-0 Pyrene 0.031 0.000837 0.00329 mg/kg

CAS# Surrogate Conc. Spiked Conc. Rec Units % Recovery Rec Limits

4165-60-0 Nitrobenzene-d5 0.1660 .112 ug/Kg 67 44 - 125 321-60-8 2-Fluorobiphenyl 0.1660 .096 ug/Kg 58 46 - 115 1718-51-0 Terphenyl-d14 0.1660 .122 ug/Kg 73 58 - 133

EPA 8015C DRO

EPA 8015C DRO


07/12/2016 15:00 590438 EPA 3550C 1 07/14/2016 02:53 MEF2 590609




84-15-1 o-Terphenyl 1.66 .902 ug/Kg 54 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-2



EPA 8270C SIM

EPA 8270C SIM


07/06/2016 11:00 589927 EPA 3550C 1 07/06/2016 16:54 BLY 590098


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.000476J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00303J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00324J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00420 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00195J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00341 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00389 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene ND 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00353 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/12/2016 15:00 590438 EPA 3550C 1 07/14/2016 03:07 MEF2 590609




84-15-1 o-Terphenyl 1.67 .89 ug/Kg 53 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-3



EPA 8270C SIM

EPA 8270C SIM


07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 15:52 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.000531J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.000858J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.000795J 0.000420 0.00330 mg/kg 218-01-9 Chrysene ND 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.000918J 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene ND 0.000840 0.00330 mg/kg 129-00-0 Pyrene ND 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/12/2016 15:00 590438 EPA 3550C 1 07/14/2016 03:22 MEF2 590609


GCSV-00-4 Diesel Range Organics ND 1.31 4.00 mg/kg


84-15-1 o-Terphenyl 1.67 .79 ug/Kg 47 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-4



EPA 8270C SIM

EPA 8270C SIM


07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 16:11 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.000793J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00214J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00248J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00463 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00166J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00332 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00400 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00140J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00321J 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/12/2016 15:00 590438 EPA 3550C 1 07/14/2016 03:36 MEF2 590609




84-15-1 o-Terphenyl 1.67 .829 ug/Kg 50 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-5



EPA 8270C SIM

EPA 8270C SIM


07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 16:30 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.000597J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00222J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00233J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00278J 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00207J 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00113J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00239J 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00424 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00160J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00375 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/12/2016 15:00 590438 EPA 3550C 1 07/14/2016 03:49 MEF2 590609




84-15-1 o-Terphenyl 1.67 .849 ug/Kg 51 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-6



EPA 8270C SIM

EPA 8270C SIM


07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 16:49 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene ND 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00118J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.000924J 0.000420 0.00330 mg/kg 218-01-9 Chrysene ND 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00166J 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene ND 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00136J 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/11/2016 13:45 590205 EPA 3550C 1 07/11/2016 19:10 MEF2 590420




84-15-1 o-Terphenyl 1.66 .429 ug/Kg 26* 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-7



EPA 8270C SIM

EPA 8270C SIM


07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 17:08 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.00104J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00242J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00197J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00411 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00157J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00335 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00405 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00106J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00358 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/12/2016 15:00 590438 EPA 3550C 1 07/14/2016 04:19 MEF2 590609




84-15-1 o-Terphenyl 1.67 .838 ug/Kg 50 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-8



EPA 8270C SIM

EPA 8270C SIM


07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 17:27 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000829 0.00326 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000829 0.00326 mg/kg 83-32-9 Acenaphthene ND 0.00163 0.00326 mg/kg 208-96-8 Acenaphthylene ND 0.00163 0.00326 mg/kg 120-12-7 Anthracene ND 0.000414 0.00326 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00163 0.00326 mg/kg 50-32-8 Benzo(a)pyrene 0.000435J 0.000414 0.00326 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00163 0.00326 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000829 0.00326 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.000414 0.00326 mg/kg 218-01-9 Chrysene ND 0.00163 0.00326 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00163 0.00326 mg/kg 206-44-0 Fluoranthene ND 0.000414 0.00326 mg/kg 86-73-7 Fluorene ND 0.000414 0.00326 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000414 0.00326 mg/kg 91-20-3 Naphthalene ND 0.000414 0.00326 mg/kg 85-01-8 Phenanthrene ND 0.000829 0.00326 mg/kg 129-00-0 Pyrene ND 0.000829 0.00326 mg/kg


4165-60-0 Nitrobenzene-d5 0.1640 .093 ug/Kg 56 44 - 125 321-60-8 2-Fluorobiphenyl 0.1640 .096 ug/Kg 58 46 - 115 1718-51-0 Terphenyl-d14 0.1640 .091 ug/Kg 55* 58 - 133

EPA 8015C DRO

EPA 8015C DRO


07/12/2016 15:00 590438 EPA 3550C 1 07/14/2016 04:34 MEF2 590609




84-15-1 o-Terphenyl 1.67 .801 ug/Kg 48 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-9



EPA 8270C SIM

EPA 8270C SIM


07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 17:45 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene ND 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene ND 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.000420 0.00330 mg/kg 218-01-9 Chrysene ND 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene ND 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene ND 0.000840 0.00330 mg/kg 129-00-0 Pyrene ND 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/11/2016 13:45 590205 EPA 3550C 1 07/11/2016 19:55 MEF2 590420




84-15-1 o-Terphenyl 1.65 .353 ug/Kg 21* 45 - 130


Revision 2

Report#: 216070103


Sample Results SB-10



EPA 8270C SIM

EPA 8270C SIM


07/01/2016 13:00 589832 EPA 3550C 1 07/05/2016 18:04 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.00130J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00228J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00238J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00482 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00169J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00380 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00475 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00138J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00376 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/12/2016 15:00 590438 EPA 3550C 1 07/14/2016 05:17 MEF2 590609




84-15-1 o-Terphenyl 1.67 .87 ug/Kg 52 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 10:49 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene ND 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00199J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00209J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00220J 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00122J 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.000923J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00188J 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00307J 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene 0.00523 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene ND 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00267J 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/11/2016 13:45 590205 EPA 3550C 1 07/11/2016 20:39 MEF2 590420




84-15-1 o-Terphenyl 1.64 .372 ug/Kg 23* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 11:08 BLY 589958





EPA 8015C DRO

EPA 8015C DRO


07/13/2016 08:45 590439 EPA 3550C 1 07/14/2016 05:46 MEF2 590609




84-15-1 o-Terphenyl 1.67 .941 ug/Kg 56 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 11:27 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000834 0.00328 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000834 0.00328 mg/kg 83-32-9 Acenaphthene ND 0.00164 0.00328 mg/kg 208-96-8 Acenaphthylene ND 0.00164 0.00328 mg/kg 120-12-7 Anthracene ND 0.000417 0.00328 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00164 0.00328 mg/kg 50-32-8 Benzo(a)pyrene ND 0.000417 0.00328 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00164 0.00328 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000834 0.00328 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.000417 0.00328 mg/kg 218-01-9 Chrysene ND 0.00164 0.00328 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00164 0.00328 mg/kg 206-44-0 Fluoranthene 0.000936J 0.000417 0.00328 mg/kg 86-73-7 Fluorene ND 0.000417 0.00328 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000417 0.00328 mg/kg 91-20-3 Naphthalene ND 0.000417 0.00328 mg/kg 85-01-8 Phenanthrene ND 0.000834 0.00328 mg/kg 129-00-0 Pyrene 0.000894J 0.000834 0.00328 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/11/2016 11:20 590206 EPA 3550C 1 07/11/2016 22:34 MEF2 590420




84-15-1 o-Terphenyl 1.66 .522 ug/Kg 32* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 11:46 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene 0.00185J 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.00342 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00482 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00554 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00888 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00387 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00339 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00733 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.016 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene 0.00768 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00451 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.012 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/11/2016 11:20 590206 EPA 3550C 1 07/11/2016 22:49 MEF2 590420




84-15-1 o-Terphenyl 1.66 .469 ug/Kg 28* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/06/2016 11:00 589927 EPA 3550C 1 07/06/2016 17:13 BLY 590098


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene 0.000585J 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene 0.00232J 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.00223J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00286J 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00132J 0.000420 0.00330 mg/kg 218-01-9 Chrysene 0.00292J 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00588 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.00232J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00557 0.000840 0.00330 mg/kg


4165-60-0 Nitrobenzene-d5 0.1670 .082 ug/Kg 49 44 - 125 321-60-8 2-Fluorobiphenyl 0.1670 .068 ug/Kg 41* 46 - 115 1718-51-0 Terphenyl-d14 0.1670 .086 ug/Kg 51* 58 - 133

EPA 8015C DRO

EPA 8015C DRO


07/11/2016 11:20 590206 EPA 3550C 1 07/11/2016 23:03 MEF2 590420




84-15-1 o-Terphenyl 1.67 .472 ug/Kg 28* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 12:23 BLY 589958





EPA 8015C DRO

EPA 8015C DRO


07/11/2016 11:20 590206 EPA 3550C 1 07/11/2016 23:17 MEF2 590420




84-15-1 o-Terphenyl 1.64 .469 ug/Kg 29* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 12:42 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene ND 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene ND 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.000420 0.00330 mg/kg 218-01-9 Chrysene ND 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.000484J 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene ND 0.000840 0.00330 mg/kg 129-00-0 Pyrene ND 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/11/2016 11:20 590206 EPA 3550C 1 07/11/2016 23:30 MEF2 590420




84-15-1 o-Terphenyl 1.67 .413 ug/Kg 25* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 13:01 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000832 0.00327 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000832 0.00327 mg/kg 83-32-9 Acenaphthene ND 0.00163 0.00327 mg/kg 208-96-8 Acenaphthylene ND 0.00163 0.00327 mg/kg 120-12-7 Anthracene ND 0.000416 0.00327 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00163 0.00327 mg/kg 50-32-8 Benzo(a)pyrene 0.000823J 0.000416 0.00327 mg/kg 205-99-2 Benzo(b)fluoranthene 0.00182J 0.00163 0.00327 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000832 0.00327 mg/kg 207-08-9 Benzo(k)fluoranthene 0.000755J 0.000416 0.00327 mg/kg 218-01-9 Chrysene ND 0.00163 0.00327 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00163 0.00327 mg/kg 206-44-0 Fluoranthene 0.00191J 0.000416 0.00327 mg/kg 86-73-7 Fluorene ND 0.000416 0.00327 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000416 0.00327 mg/kg 91-20-3 Naphthalene ND 0.000416 0.00327 mg/kg 85-01-8 Phenanthrene ND 0.000832 0.00327 mg/kg 129-00-0 Pyrene 0.00169J 0.000832 0.00327 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/13/2016 08:45 590439 EPA 3550C 1 07/14/2016 07:26 MEF2 590609


GCSV-00-4 Diesel Range Organics 4.35 1.31 4.00 mg/kg


84-15-1 o-Terphenyl 1.67 .984 ug/Kg 59 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 13:20 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000840 0.00330 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000840 0.00330 mg/kg 83-32-9 Acenaphthene ND 0.00165 0.00330 mg/kg 208-96-8 Acenaphthylene ND 0.00165 0.00330 mg/kg 120-12-7 Anthracene ND 0.000420 0.00330 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00165 0.00330 mg/kg 50-32-8 Benzo(a)pyrene 0.000696J 0.000420 0.00330 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00165 0.00330 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000840 0.00330 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.000420 0.00330 mg/kg 218-01-9 Chrysene ND 0.00165 0.00330 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00165 0.00330 mg/kg 206-44-0 Fluoranthene 0.00148J 0.000420 0.00330 mg/kg 86-73-7 Fluorene ND 0.000420 0.00330 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000420 0.00330 mg/kg 91-20-3 Naphthalene ND 0.000420 0.00330 mg/kg 85-01-8 Phenanthrene 0.000940J 0.000840 0.00330 mg/kg 129-00-0 Pyrene 0.00154J 0.000840 0.00330 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/11/2016 11:20 590206 EPA 3550C 1 07/12/2016 00:01 MEF2 590420




84-15-1 o-Terphenyl 1.64 .21 ug/Kg 13* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 13:39 BLY 589958


90-12-0 1-Methylnaphthalene ND 0.000837 0.00329 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000837 0.00329 mg/kg 83-32-9 Acenaphthene ND 0.00164 0.00329 mg/kg 208-96-8 Acenaphthylene ND 0.00164 0.00329 mg/kg 120-12-7 Anthracene ND 0.000419 0.00329 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00164 0.00329 mg/kg 50-32-8 Benzo(a)pyrene ND 0.000419 0.00329 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00164 0.00329 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000837 0.00329 mg/kg 207-08-9 Benzo(k)fluoranthene 0.00129J 0.000419 0.00329 mg/kg 218-01-9 Chrysene ND 0.00164 0.00329 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00164 0.00329 mg/kg 206-44-0 Fluoranthene ND 0.000419 0.00329 mg/kg 86-73-7 Fluorene ND 0.000419 0.00329 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000419 0.00329 mg/kg 91-20-3 Naphthalene ND 0.000419 0.00329 mg/kg 85-01-8 Phenanthrene ND 0.000837 0.00329 mg/kg 129-00-0 Pyrene ND 0.000837 0.00329 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/11/2016 11:20 590206 EPA 3550C 1 07/12/2016 00:15 MEF2 590420




84-15-1 o-Terphenyl 1.66 .394 ug/Kg 24* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/01/2016 14:00 589833 EPA 3550C 1 07/05/2016 13:58 BLY 589958




4165-60-0 Nitrobenzene-d5 0.1670 .086 ug/Kg 52 44 - 125 321-60-8 2-Fluorobiphenyl 0.1670 .07 ug/Kg 42* 46 - 115 1718-51-0 Terphenyl-d14 0.1670 .112 ug/Kg 67 58 - 133

EPA 8015C DRO

EPA 8015C DRO


07/13/2016 08:45 590439 EPA 3550C 1 07/14/2016 13:19 MEF2 590664




84-15-1 o-Terphenyl 1.67 .505 ug/Kg 30* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/13/2016 12:30 590522 EPA 3550C 1 07/15/2016 10:31 SMH 590681





EPA 8015C DRO

EPA 8015C DRO


07/14/2016 13:30 590633 EPA 3550C 1 07/14/2016 20:37 CLH 590664




84-15-1 o-Terphenyl 1.66 .84 ug/Kg 51 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/13/2016 12:30 590522 EPA 3550C 1 07/15/2016 10:50 SMH 590681


90-12-0 1-Methylnaphthalene ND 0.000834 0.00328 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000834 0.00328 mg/kg 83-32-9 Acenaphthene ND 0.00164 0.00328 mg/kg 208-96-8 Acenaphthylene ND 0.00164 0.00328 mg/kg 120-12-7 Anthracene ND 0.000417 0.00328 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00164 0.00328 mg/kg 50-32-8 Benzo(a)pyrene ND 0.000417 0.00328 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00164 0.00328 mg/kg 191-24-2 Benzo(g,h,i)perylene 0.00170J 0.000834 0.00328 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.000417 0.00328 mg/kg 218-01-9 Chrysene ND 0.00164 0.00328 mg/kg 53-70-3 Dibenz(a,h)anthracene 0.00166J 0.00164 0.00328 mg/kg 206-44-0 Fluoranthene ND 0.000417 0.00328 mg/kg 86-73-7 Fluorene ND 0.000417 0.00328 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene 0.00156J 0.000417 0.00328 mg/kg 91-20-3 Naphthalene ND 0.000417 0.00328 mg/kg 85-01-8 Phenanthrene ND 0.000834 0.00328 mg/kg 129-00-0 Pyrene ND 0.000834 0.00328 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/14/2016 13:30 590633 EPA 3550C 1 07/14/2016 20:50 CLH 590664




84-15-1 o-Terphenyl 1.66 .445 ug/Kg 27* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/13/2016 12:30 590522 EPA 3550C 1 07/15/2016 11:09 SMH 590681





EPA 8015C DRO

EPA 8015C DRO


07/12/2016 10:45 590373 EPA 3550C 1 07/13/2016 19:40 MEF2 590609




84-15-1 o-Terphenyl 1.67 .825 ug/Kg 50 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/13/2016 12:30 590522 EPA 3550C 1 07/15/2016 11:27 SMH 590681





EPA 8015C DRO

EPA 8015C DRO


07/14/2016 13:30 590633 EPA 3550C 1 07/14/2016 21:06 CLH 590664




84-15-1 o-Terphenyl 1.67 .522 ug/Kg 31* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/13/2016 12:30 590522 EPA 3550C 1 07/15/2016 11:46 SMH 590681





EPA 8015C DRO

EPA 8015C DRO


07/14/2016 13:30 590633 EPA 3550C 1 07/14/2016 21:20 CLH 590664




84-15-1 o-Terphenyl 1.67 .358 ug/Kg 21* 45 - 130


Revision 2

Report#: 216070103





EPA 8270C SIM

EPA 8270C SIM


07/13/2016 12:30 590522 EPA 3550C 1 07/15/2016 12:05 SMH 590681


90-12-0 1-Methylnaphthalene ND 0.000832 0.00327 mg/kg 91-57-6 2-Methylnaphthalene ND 0.000832 0.00327 mg/kg 83-32-9 Acenaphthene ND 0.00163 0.00327 mg/kg 208-96-8 Acenaphthylene ND 0.00163 0.00327 mg/kg 120-12-7 Anthracene ND 0.000416 0.00327 mg/kg 56-55-3 Benzo(a)anthracene ND 0.00163 0.00327 mg/kg 50-32-8 Benzo(a)pyrene ND 0.000416 0.00327 mg/kg 205-99-2 Benzo(b)fluoranthene ND 0.00163 0.00327 mg/kg 191-24-2 Benzo(g,h,i)perylene ND 0.000832 0.00327 mg/kg 207-08-9 Benzo(k)fluoranthene ND 0.000416 0.00327 mg/kg 218-01-9 Chrysene ND 0.00163 0.00327 mg/kg 53-70-3 Dibenz(a,h)anthracene ND 0.00163 0.00327 mg/kg 206-44-0 Fluoranthene 0.000648J 0.000416 0.00327 mg/kg 86-73-7 Fluorene ND 0.000416 0.00327 mg/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.000416 0.00327 mg/kg 91-20-3 Naphthalene ND 0.000416 0.00327 mg/kg 85-01-8 Phenanthrene ND 0.000832 0.00327 mg/kg 129-00-0 Pyrene ND 0.000832 0.00327 mg/kg



EPA 8015C DRO

EPA 8015C DRO


07/14/2016 13:30 590633 EPA 3550C 1 07/14/2016 21:35 CLH 590664




84-15-1 o-Terphenyl 1.66 .25 ug/Kg 15* 45 - 130


Revision 2

Report#: 216070103


QC Summary

GC/MS Semi-Volatiles QC Summary GC/MS Semi-Volatiles

Analytical Batch 589958 Prep Batch 589832 Prep Method EPA 3550C

Client ID GCAL ID

Sample Type Prep Date

Analysis Date Matrix

MB589832 1587265 MB 07/01/2016 13:00 07/05/2016 14:17 Solid

LCS589832 1587266 LCS 07/01/2016 13:00 07/05/2016 14:36 Solid

LCSD589832 1587267 LCSD 07/01/2016 13:00 07/05/2016 14:55 Solid

EPA 8270C SIM Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added

Result %R RPD RPD Limit

1-Methylnaphthalene 90-12-0 ND 0.000840 0.167 0.134 80 43 - 111 0.167 0.124 74 8 30 2-Methylnaphthalene 91-57-6 ND 0.000840 0.167 0.130 78 39 - 114 0.167 0.121 73 7 30 Acenaphthene 83-32-9 ND 0.00165 0.167 0.124 74 44 - 111 0.167 0.119 71 4 30 Acenaphthylene 208-96-8 ND 0.00165 0.167 0.124 74 39 - 116 0.167 0.117 70 6 30 Anthracene 120-12-7 ND 0.000420 0.167 0.124 74 50 - 114 0.167 0.124 74 0 30 Benzo(a)anthracene 56-55-3 ND 0.00165 0.167 0.125 75 54 - 122 0.167 0.132 79 5 30 Benzo(a)pyrene 50-32-8 ND 0.000420 0.167 0.134 80 50 - 125 0.167 0.144 86 7 30 Benzo(b)fluoranthene 205-99-2 ND 0.00165 0.167 0.124 74 53 - 128 0.167 0.131 79 5 30 Benzo(g,h,i)perylene 191-24-2 ND 0.000840 0.167 0.115 69 49 - 127 0.167 0.121 73 5 30 Benzo(k)fluoranthene 207-08-9 ND 0.000420 0.167 0.127 76 56 - 123 0.167 0.134 80 5 30 Chrysene 218-01-9 ND 0.00165 0.167 0.125 75 57 - 118 0.167 0.132 79 5 30 Dibenz(a,h)anthracene 53-70-3 ND 0.00165 0.167 0.114 68 50 - 129 0.167 0.120 72 5 30 Fluoranthene 206-44-0 ND 0.000420 0.167 0.138 83 55 - 119 0.167 0.142 85 3 30 Fluorene 86-73-7 ND 0.000420 0.167 0.141 85 47 - 114 0.167 0.139 83 1 30 Indeno(1,2,3-cd)pyrene 193-39-5 ND 0.000420 0.167 0.115 69 49 - 130 0.167 0.121 73 5 30 Naphthalene 91-20-3 ND 0.000420 0.167 0.122 73 38 - 111 0.167 0.112 67 9 30 Phenanthrene 85-01-8 ND 0.000840 0.167 0.125 75 49 - 113 0.167 0.126 76 1 30 Pyrene 129-00-0 ND 0.000840 0.167 0.121 73 55 - 117 0.167 0.127 76 5 30 Surrogate 2-Fluorobiphenyl 321-60-8 .104 62 .167 .109 65 46 - 115 .167 .104 62 NA NA Nitrobenzene-d5 4165-60-0 .113 68 .167 .124 74 44 - 125 .167 .114 68 NA NA Terphenyl-d14 1718-51-0 .139 83 .167 .13 78 58 - 133 .167 .142 85 NA NA


Client ID GCAL ID



MB589833 1587268 MB 07/01/2016 14:00 07/05/2016 09:53 Solid

LCS589833 1587269 LCS 07/01/2016 14:00 07/05/2016 10:12 Solid

LCSD589833 1587270 LCSD 07/01/2016 14:00 07/05/2016 10:30 Solid

EPA 8270C SIM Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added




Revision 2

Report#: 216070103


GC/MS Semi-Volatiles QC Summary


Client ID GCAL ID



MB589927 1587605 MB 07/05/2016 11:30 07/06/2016 15:58 Solid

LCS589927 1587606 LCS 07/05/2016 11:30 07/06/2016 16:17 Solid

LCSD589927 1587607 LCSD 07/05/2016 11:30 07/06/2016 16:35 Solid

EPA 8270C SIM Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added




Client ID GCAL ID



MB590522 1590645 MB 07/13/2016 12:30 07/13/2016 13:19 Solid

LCS590522 1590646 LCS 07/13/2016 12:30 07/13/2016 13:57 Solid

LCSD590522 1590647 LCSD 07/13/2016 12:30 07/13/2016 14:35 Solid

EPA 8270C SIM Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added




Revision 2

Report#: 216070103


GC Semi-Volatiles QC Summary GC Semi-Volatiles


Client ID GCAL ID



MB590205 1588957 MB 07/11/2016 13:45 07/11/2016 16:59 Solid

LCS590205 1588958 LCS 07/11/2016 13:45 07/11/2016 17:27 Solid

LCSD590205 1588959 LCSD 07/11/2016 13:45 07/11/2016 17:41 Solid

EPA 8015C DRO Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added


Diesel Range Organics GCSV-00-4 ND 1.31 33.3 25.9 78 38 - 132 33.3 25.6 77 1 30 Surrogate o-Terphenyl 84-15-1 1.31 79 1.67 1.4 84 45 - 130 1.67 1.36 82 NA NA


Client ID GCAL ID



MB590206 1588960 MB 07/11/2016 11:20 07/11/2016 21:37 Solid

LCS590206 1588961 LCS 07/11/2016 11:20 07/11/2016 21:50 Solid

LCSD590206 1588962 LCSD 07/11/2016 11:20 07/11/2016 22:05 Solid

EPA 8015C DRO Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added




Client ID GCAL ID



MB590373 1589801 MB 07/12/2016 10:45 07/12/2016 14:58 Solid

LCS590373 1589802 LCS 07/12/2016 10:45 07/12/2016 14:44 Solid

LCSD590373 1589803 LCSD 07/12/2016 10:45 07/12/2016 13:21 Solid

EPA 8015C DRO Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added




Client ID GCAL ID



MB590438 1590228 MB 07/12/2016 15:00 07/14/2016 01:10 Solid

LCS590438 1590229 LCS 07/12/2016 15:00 07/14/2016 01:27 Solid

LCSD590438 1590230 LCSD 07/12/2016 15:00 07/14/2016 01:41 Solid

EPA 8015C DRO Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added




Client ID GCAL ID



MB590439 1590236 MB 07/13/2016 08:45 07/14/2016 01:55 Solid

LCS590439 1590237 LCS 07/13/2016 08:45 07/14/2016 02:09 Solid

LCSD590439 1590238 LCSD 07/13/2016 08:45 07/14/2016 02:24 Solid

EPA 8015C DRO Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added




Revision 2

Report#: 216070103


GC Semi-Volatiles QC Summary


Client ID GCAL ID



MB590633 1591098 MB 07/14/2016 13:30 07/14/2016 19:54 Solid

LCS590633 1591099 LCS 07/14/2016 13:30 07/14/2016 20:08 Solid

LCSD590633 1591100 LCSD 07/14/2016 13:30 07/14/2016 20:23 Solid

EPA 8015C DRO Units

Result mg/kg

DL Spike

Added Result %R

Control Limits%R

Spike Added




Revision 2

of 49GCAL Report#: 216070103

Revision 2

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