link.springer.com10.1007/s11164... · web viewsynthesis of novel 9-((arylidene)...

SYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4- METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS POTIENTIAL ANTI BACTERIALS G. L. Balaji, K. Rajesh, R. Janardhan and V. Vijayakumar* 1 H NMR spectrum of 9-hydrazono-2,4,6,8-tetrakis(4-methoxyphenyl)- 3,7-diazabicyclo[3.3.1]nonane (2). *To whom correspondence should be addressed, e-mail: [email protected]

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SYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4-

METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS

POTIENTIAL ANTI BACTERIALS

G. L. Balaji, K. Rajesh, R. Janardhan and V. Vijayakumar*

1H NMR spectrum of 9-hydrazono-2,4,6,8-tetrakis(4-methoxyphenyl)-3,7-

diazabicyclo[3.3.1]nonane (2).

*To whom correspondence should be addressed, e-mail: [email protected]

Centre for Organic and Medicinal Chemistry, VIT University, Vellore 632 014, Tamil Nadu, India

Page 2: link.springer.com10.1007/s11164... · Web viewSYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4-METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS POTIENTIAL

13C NMR spectrum of 9-hydrazono-2,4,6,8-tetrakis(4-methoxyphenyl)-3,7-diazabicyclo[3.3.1]

nonane (2).

LC-MS of 9-hydrazono-2,4,6,8-tetrakis(4-methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonane (2).

Page 3: link.springer.com10.1007/s11164... · Web viewSYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4-METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS POTIENTIAL

1H NMR spectrum of 9-(benzylidenehydrazono)-2,4,6,8-tetrakis(4-methoxy phenyl)-3,7-

diazabicyclo[3.3.1]nonane (3a).

13C NMR spectrum of 9-(benzylidenehydrazono)-2,4,6,8-tetrakis(4-methoxy phenyl)-3,7-

diazabicyclo[3.3.1]nonane (3a).

Page 4: link.springer.com10.1007/s11164... · Web viewSYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4-METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS POTIENTIAL

1H NMR spectrum of 9-((4-methoxybenzylidene)hydrazono)-2,4,6,8-tetrakis(4-methoxyphenyl)-

3,7-diazabicyclo[3.3.1]nonane (3b).

13C NMR spectrum of 9-((4-methoxybenzylidene)hydrazono)-2,4,6,8-tetrakis(4-

methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonane (3b).

Page 5: link.springer.com10.1007/s11164... · Web viewSYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4-METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS POTIENTIAL

1H NMR spectrum of 9-((4-ethylbenzylidene)hydrazono)-2,4,6,8-tetrakis(4-methoxyphenyl)-3,7-

diazabicyclo[3.3.1]nonane (3c).

1H NMR spectrum of 9-((3-nitrobenzylidene)hydrazono)-2,4,6,8-tetrakis(4-methoxyphenyl)-3,7-

diazabicyclo[3.3.1]nonane (3d).

Page 6: link.springer.com10.1007/s11164... · Web viewSYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4-METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS POTIENTIAL

1H NMR spectrum of 9-((4-chlorobenzylidene)hydrazono)-2,4,6,8-tetrakis(4-methoxyphenyl)-

3,7-diazabicyclo[3.3.1]nonane (3e).

1H NMR spectrum of 9-((3,4-dimethoxybenzylidene)hydrazono)-2,4,6,8-tetrakis(4-

methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonane (3f).

Page 7: link.springer.com10.1007/s11164... · Web viewSYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4-METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS POTIENTIAL

13C NMR spectrum of 9-((3,4-dimethoxybenzylidene)hydrazono)-2,4,6,8-tetrakis(4-

methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonane (3f).

1H NMR spectrum of 9-((4-diethylaminobenzylidene)hydrazono)-2,4,6,8-tetrakis(4-

methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonane (3g).

Page 8: link.springer.com10.1007/s11164... · Web viewSYNTHESIS OF NOVEL 9-((ARYLIDENE) HYDRAZONO)-2,4,6,8-TETRAKIS (4-METHOXY PHENYL)-3,7-DIAZABICYCLO[3.3.1]NONANE AZINE DERIVATIVES AS POTIENTIAL

1H NMR spectrum of 9-((4-diethylaminobenzylidene)hydrazono)-2,4,6,8-tetrakis(4-

methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonane (3g).

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