m200h mgc analytical report, volume 2 of …1 28.380 30.300 37.34 bv 0 179645376 21.257 i 2 37.340...

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ng and Analytic*) Contract

M200H MGC ANALYTICAL REPORTRAYMARKSITE

STRATFORD. CONNECTICUTAPRIL 2000 I

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U.S. EPA Work Assignment No.: 0-201LOCKHEED MARTIN Work Order No.: Rl A00201

U.S. EPA Contract No.: 68-C99-223

OFFICE OF EMERGENCY AND REMEDIAL RESPONSE

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M200H MGC ANALYTICAL REPORT RAYMARKSITE

STRATFORD. CONNECTICUT APRIL 2000

2of3

r U.S. EPA Work Assignment No.: 0-201

LOCKHEED MARTIN Work Order No.: Rl A00201 r U.S. EPA Contract No.: 68-C99-223

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16077 29-A

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rea Report f'kno Start RT Stop Area Area% Flag f 1 28.380 30.300 37.340 179181680 21.215 BV

2 37.340 39.900 61.020 665415488 78.785 VB

External Standard Report

* Name Amount Units RT Min Max Mean %SD

Foxygen 20.551 % 30.300 0.000 635.565 23.462 304.680 * Nitrogen 77.745 % 39.900 0.000 856.321 74.016 181.602

rbhannel: A Current Time: Feb 28, 2001 09:51:38 •kethod: c:\mti\ezchrom\200\methods\raymark. |?ile : c:\mti\ezchrom\200\chrom\16077.1 'Data file creation time: Feb 28, 2001 09:49:22 •Instrument ID: 02402283 I^olumn Type: 10m MS5A Carrier Gas: He Kolumn Head Pressure: 29.6 psi ftJolumn temperature: 65 C Instrument Gain: LOW

•Sample Time: 30 seconds 1Cnject Time: 50 milliseconds Run Time: 100 seconds

f ff r r r

Area Report J

Pkno Start RT Stop Area Area% Flag -I

123

26.510 38.030 56.800

26.760 39.040 59.040

27.120 5890 44.800 1327165568 61.920 5205734

0.000 99.609 0.391

BB BB BB


1 Name Amount Units RT Min Max Mean %SD "1

Carbon Dioxide 2967.306 ppm 59.040 119487961615178768.000 877.053 4

Channel: BCurrent Time: Feb 28, 2001 09:51:38 Method: c:\mti\ezchrom\200\methods\raymark.File : c:\mti\ezchrom\200\chrom\16077.1Data file creation time: Feb 28, 2001 09:49:22 Instrument ID: 02402283Column Type: 8m PPQCarrier Gas: HeColumn Head Pressure: 16.7 psiColumn Temperature: 40 CInstrument Gain: LOWSample Time: 30 secondsInject Time: 80 millisecondsRun Time: 100 seconds

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1

1

1

1

1

f

ffffff r

16078 30-A

rea Report n

?kno Start RT Stop Area Area% Flag ~j

1 28.380 30.300 37.340 179645376 21.257 BV 2 37.340 39.900 61.020 665481856 78.743 VB nI


• 1 Name Amount Units RT Min Max Mean %SD

IOxygen 20.606 % 30.300 0.000 635.565 23.444 303.934 Nitrogen 77.753 % 39.900 0.000 856.321 74.040 180.957

tIlhannel: A Current Time: Feb 28, 2001 09:55:20 ethod: c:\mti\ezchrorn\200\methods\raymark. ile : c:\mti\ezchrom\200\chrom\16078.1

Data file creation time: Feb 28, 2001 09:53:04 Btnstrument ID: 02402283 Column Type: 10m MS5A Carrier Gas: He •Column Head Pressure: 29.7 psi Column Temperature: 65 C Instrument Gain: LOW

•Sample Time: 30 seconds TEnject Time: 50 milliseconds .un Time: 100 seconds

t

I

I

I

I

I

I

I

I

Area Report r

i

I

r Pkno1 Start

37.880

RT

39.050

Stop Area

56.650 1330558592

Area%

99.621

Flag

BV 2 56.650 59.050 61.930 4335116 0.325 VB r 3 85.290 88.010 98.250 720875 0.054 BE

External Standard Reportr _Name Amount Units RT Min Max Mean %SD

^'Carbon Dioxide 2471.048 ppm 59.050 119487961615081484.000 879.895

phannel: B Vurrent Time: Feb 28, 2001 09:55:20 J4ethod: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16078.1 Data file creation time: Feb 28, 2001 09:53:04 -instrument ID: 02402283 I olumn Type: 8m PPQ Carrier Gas: He •Column Head Pressure: 16.7 psi I 'olumn Temperature: 40 C Instrument Gain: LOW •Sample Time: 30 seconds I nject Time: 80 milliseconds Run Time: 100 seconds

r n r r

r r r r r

^ I I 1 16079 • 30-A DUP

rea Report

I? kno Start RT Stop Area Area% Flag

' 1 28.380 30.620 37.340 179291120 21.231 BV I 2 37.340 39.900 61.340 665176256 78.769 VB

f Uxternal Standard Report

" Name Amount Units RT Min Max Mean %SD

W^Oxygen• Nitrogen

20.564 77.715

% 30.620 % 39.900

0.000 635.565 0.000 856.321

23.425 303.198 74.064 180.320

Channel: A Current Time: Feb 28, 2001 09:59:01 Method: c:\mti\ezchrom\200\methods\raymark. Iplie : c:\mti\ezchrom\200\chrom\16079.1 uata file creation time: Feb 28, 2001 09:56:44 instrument ID: 02402283 T^olumn Type: 10m MS5A Carrier Gas: He •Column Head Pressure: 29.6 psi T !olumn Temperature: 65 C —Instrument Gain: LOW •Bample Time: 30 seconds 7 nject Time: 50 milliseconds lun Time: 100 seconds

Area Report

Pkno Start RT Stop Area Area% Flag

1 37.940 38.950 56.710 1329846400 99.574 BV 2 56.710 58.950 61.830 5028926 0.377 VB 3 85.990 88.550 98.150 654567 0.049 BE

External Standard Reoort

Name Amount Units RT Min Max Mean %SD

Carbon Dioxide 2866.524 ppm 58.950 119487961614985442.000 882.728

Channel: B Current Time: Feb 28, 2001 09:59:01 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16079.1 Data file creation time: Feb 28, 2001 09:56:44 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 40 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

• 16080 f* 31'A

f r r r rf

ea Report

rkno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 176309120 20.928 BV 2 37.340 39.900 61.020 666142656 79.072 VB


1 Name Amount Units RT Min Max Mean %SD

T'oxygen 20.211 % 30.620 0.000 635.565 23.405 302.495 f Nitrogen 77.833 % 39.900 0.000 856.321 74.088 179.687

V Channel: A Current Time: Feb 28, 2001 10:07:58 wethod: c:\mti\ezchrom\200\methods\raymark. 1?ile : c:\mti\ezchrom\200\chrom\16080.1 Data file creation time: Feb 28, 2001 10:05:42

•Instrument ID: 02402283 TColumn Type: 10m MS5A Carrier Gas: He

•Column Head Pressure: 29.6 psi | :olumn Temperature: 65 C —Instrument Gain: LOW Psample Time: 30 seconds | Inject Time: 50 milliseconds lun Time: 100 seconds

Area Report


1 37.900 39.070 56.510 1326259840 99.441 BV 2 56.510 58.910 61.950 7459887 0.559 VB





I 16081 32-A

r

lArea Report

[Pkno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 178442992 21.154 BV L 2 37.340 39.900 61.020 665087168 78.846 VB H



f\ Oxygen 20.464 % 30.620 0.000 635.565 23.386 301.776 1 Nitrogen 77.705 % 39.900 0.000 856.321 74.110 179.063

• Channel:A Current Time: Feb 28, 2001 10:12:32

•Method: c:\mti\ezchrorn\200\methods\raymark. •File : c:\mti\ezchrom\200\chrom\16081.1

Data file creation time: Feb 28, 2001 10:10:15 •instrument ID: 02402283 1 Column Type: 10m MS5A

Carrier Gas: He •column Head Pressure: 29.7 psi | Column Temperature:''65 C

Instrument Gain: LOW •6ample Time: 30 seconds | Inject Time: 50 milliseconds

Run Time: 100 seconds

r r r r

Area Report 1

Pkno Start RT Stop Area Area% Flag ~1

1 38.010 39.020 45.740 1325217664 99.446 BB 2 56.620 58.860 61.740 7385235 0.554 BB

1 External Standard Report


Carbon Dioxide 4209.638 ppm 58.860 119487961614796999.000 888.366 1 Channel: B Current Time: Feb 28, 2001 10:12:32 1 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16081.1 jlj Data file creation time: Feb 28, 2001 10:10:15 -I Instrument ID: 02402283 Column Type: 8m PPQ ' jj Carrier Gas: He 'I Column Head Pressure: 16.7 psi ^ Column Temperature: 41 C jl Instrument Gain: LOW ' ' Sample Time: 30 seconds _ Inject Time: 80 milliseconds | Run Time: 100 seconds

1

1

1

1

1

1

1

1

1

I^ 1 1 6082

r

rea Report

3kno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 177437264 21.072 BV 2 37.340 39.900 61.020 664599552 78.928 VB

-kternal Standard Report


Dxygen 20.344 % 30.620 0.000 635.565 23.367 301.073 Nitrogen 77.645 % 39.900 0.000 856.321 74.132 178.446

"Kannel: A .arrent Time: Feb 28, 2001 10:17:02

•lethod: c:\mti\ezchrom\200\methods\raymark. •lie : c:\mti\ezchrom\200\chrom\16082.1 Lata file creation time: Feb 28, 2001 10:14:45 •nstrument ID: 02402283 Column Type: 10m MS5A Larrier Gas: He

fcolumn Head Pressure: 29 .7 psi Tolumn Temperature: 65''C instrument Gain: LOW

•temple Time: 30 seconds •inject Time: 50 milliseconds xun Time: 100 seconds

Area Report


1 37.850 39.030 56.630 1325421952 99.340 BV 2 56.630 58.870 61.750 8810315 0.660 VB

U External Standard Report


!Carbon Dioxide 5021.944 ppm 58.870 119487961614704550.000 891.171

Channel: B Current Time: Feb 28, 2001 10:17:02 1 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16082.1 jT| Data file creation time: Feb 28, 2001 10:14:45 k| Instrument ID: 02402283 Column Type: 8m PPQ HJ Carrier Gas: He •.„>' Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

1

1

1

1

f AMB1121A

rr

rrfrfFf F

lArea Report

iPkno Start RT Stop Area Area% Flag

? 1 28.380 30.620 37.340 181735296 21.452 BV I 2 37.340 39.900 61.020 665443456 78.548 VB

'jxternal Standard Report

f Name Amount Units RT Min Max Mean %SD

IrOxygen 20.854 % 30.620 0.000 635.565 23.352 300.332 f*Nitrogen 77.748 % 39.900 0.000 856.321 74.155 177.834

Blhannel: A Current Time: Feb 28, 2001 10:28:27 Hfcjethod: c:\mti\ezchrom\200\methods\raymark. ¥^ile : c:\mti\ezchrom\200\chrom\AMB1121A.l Jata file creation time: Feb 28, 2001 10:26:11

Hjnstrument ID: 02402283 Vtolumn Type: 10m MS5A Carrier Gas: He •Column Head Pressure: 29.6 psi "Column Temperature: 65 C ^Instrument Gain: LOW •?ample Time: 30 seconds T inject Time: 50 milliseconds "lun Time: 100 seconds

Area Report

Pkno Start RT Stop Area Area% Flag ~fl

1 37.890 39.060 56.820 13334680322 56.820 58.900 61.460 756435


99.943 0.057

BV VB TJ

I



Channel: B Current Time: Feb 28, 2001 10:28:27 Method: c:\mti\ezchrom\200\methods\raymark. File :. c:\mti\ezchrom\200\chrom\AMB1121A.l Data file creation time: Feb 28, 2001 10:26:11 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

rfr rfr

.ppp

AMB1121A CALIBRATE

rpP ppppppPi

F

f CAL1126A

.

rrrrr

f

f

rfrffrrrrrpr ff

r

CAL1126A CALIBRATE

mrea Report

5kno Start RT Stop Area Area% Flag

23.430 23.770 23.910 24588 0.014 BV 23.910 24.120 24.310 28466 0.016 VB 28.700 30.940 39.260 47467952 27.148 BV 39.260 41.820 55.260 65183304 37.280 W 55.260 59.100 80.220 29780494 17.032 VB 88.860 93.340 96.540 32363744 18.510 BE

eternal Standard Report

.Name Amount Units RT Min Max Mean %SD

rOxygen Nitrogen

5.010 4.990

% 30.940 % 41.820

0.000 635.565 0.000 856.321

22.991 300.579 72.951 178.462

Channel: A fcurrent Time: Feb 28, 2001 10:34:31 Ilethod: c:\mti\ezchrom\200\methods\raymark. J?ile : c:\mti\ezchrom\200\chrom\CAL1126A.l •bata file creation time: Feb 28, 2001 10:32:03 |r.nstrument ID: 02402283 (Column Type: 10m MS5A •barrier Gas: He I :olumn Head Pressure: 29.7 psi Column Temperature: 65 C Ptnstrument Gain: LOW | Sample Time: 30 seconds Inject Time: 50 milliseconds un Time: 100 seconds

Area Report


1 28.380 28.460 28.570 550 0.000 BV 2 37.910 39.830 42.710 261773920 65.768 BV 3 42.710 44.790 48.470 49452864 12.425 VB 4 55.990 58.230 62.710 86797840 21.807 BB



Carbon Dioxide49600.000 ppm58.230 119487961614173963.000 907.773

Channel: B Current Time: Feb 28, 2001 10:34:31 Method: c:\mti\ezchrom\200\methods\raymark. 1 File : c:\mti\ezchrom\200\chrom\CAL1126A.l Data file creation time: Feb 28, 2001 10:32:03 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He 1Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW 1Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds 1

1

n n n n

r* n

f. 16083 34-A

r

:ea Report

•jPkno Start RT Stop Area Area% Flag

I 28.380 30.620 37.340 179389648 21.271 BV • 2 37.340 39.900 60.380 663960448 78.729 VB

f External Standard Report

f Name Amount Units RT Min Max Mean %SD

f"Oxygen 20.672 % 30.620 0.000 635.565 22.977 299.854 Nitrogen 77.899 % 39.900 0.000 856.321 72.981 177.852

I Channel: A Current Time: Feb 28, 2001 10:53:36 •Method: c:\mti\ezchrom\200\methods\raymark. I ?ile : c:\mti\ezchrom\200\chrom\16083.1 ]Data file creation time: Feb 28, 2001 10:51:20 •instrument ID: 02402283 * Column Type: 10m MS5A —Carrier Gas: He Ppolumn Head Pressure: 29.7 psi f bolumn Temperature: 65 C —Instrument Gain: LOW Ppample Time: 30 seconds fInject Time: 50 milliseconds lun Time: 100 seconds

ft* ft ft ft ft Hfl

Area Report


1 37.910 38.920 56.520 1328512000 99.649 BV 2 56.520 58.760 61.800 4680700 0.351 VB





f r rff rrrfr rr

16084 35-A

rea Report Fkno Start RT Stop Area Area% Flag

1 28.380 30.300 37.340 180295296 21.358 BV 2 37.340 39.900 60.380 663869568 78.642 VB

-xternal Standard Report

Name Amount Units RT Min Max Mean %SD M

Oxygen Nitrogen

20.779 77.888

% 30.300 % 39.900

0.000 635.565 0.000 856.321

22.964 299.126 73.010 177.248

hannel: A urrent Time: Feb 28, 2001 10:58:55

ftethod: c:\mti\ezchrom\200\methods\raymark. lile : c:\mti\ezchrom\200\chrom\16084.1 "uata file creation time: Feb 28, 2001 10:56:39 instrument ID: 02402283 Column Type: 10m MS5A carrier Gas: He •fcolumn Head Pressure: 29.7 psi 1 olumn Temperature: 65 C instrument Gain: LOW iample Time: 30 seconds nject Time: 50 milliseconds iun Time: 100 seconds

1 1

krea Report


1 37.990 39.000 53.880 1327412992 99.769 BB 2 56.760 58.840 61.720 3076894 0.231 BB




Channel: B Current Time: Feb 28, 2001 10:58:56 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrotn\200\chrom\16084.1 Data file creation time: Feb 28, 2001 10:56:39 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

f16085 f36-A f

ff f ffff

r Report

kno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 180344752 21.349 BV 2 37.340 39.900 60.060 664385472 78.651 VB

ilxternal Standard Report fr, Name Amount Units RT Min Max Mean %SD rOxygen 20.785 % 30.620 0.000 635.565 22.951 298.403 Nitrogen 77.951 % 39.900 0.000 856.321 73.039 176.650

Channel: A 1 :urrent Time: Feb 28, 2001 11:03:35 Mlethod: c: \mti\ezchrom\200\methods\raymark. |Hle : c:\mti\ezchrom\200\chrom\16085.1 I Data file creation time: Feb 28, 2001 11:01:18 Instrument ID: 02402283 Column Type: 10m MS5A 'Carrier Gas: He •Column Head Pressure: 29.7 psi jbolumn Temperature: 65 C ^instrument Gain: LOW Bsample Time: 30 seconds ijlnject Time: 50 milliseconds **lun Time: 100 seconds

Area Report


1 25.850 26.380 27.050 26409 0.002 BB 2 37.930 38.940 56.700 1329298432 99.776 BV 3 56.700 58.780 61.660 2957242 0.222 VB




Channel: B Current Time: Feb 28, 2001 11:03:35 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16085.1 Data file creation time: Feb 28, 2001 11:01:18 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Injecc Time: 80 milliseconds Run Time: 100 seconds

rf rrfr r r

16087 3 8-A

:ea Report

fkno Start RT Stop Area Area% Flag

j1 28.380 30.300 37.340

2 37.340 39.900 60.060 180475712 663822208

21.376 78.624

BV VB

xternal Standard Report


'xygen 20.800 % 30.300 0.000 635.565 22.939 297.684 f0 IN Nitrogen 77.883 % 39.900 0.000 856.321 73.068 176.059

lannel: A 1 urrent Time: Feb 28, 2001 11:08:35 rethod: c:\mti\ezchrom\200\methods\raymark. ile : c:\mti\ezchrom\200\chrom\16087.l ata file creation time: Feb 28, 2001 11:06:19

•nstrument ID: 02402283 rblumn Type: 10m MS5A I arrier Gas: He rolumn Head Pressure: 29.7 psi olumn Temperature: 65 C _nstrument Gain: LOW f ample Time: 30 seconds nject Time: 50 milliseconds

-,un Time: 100 seconds

Area Report


1 37.940 38.950 56.710 1328835456 99.847 BV 2 56.710 58.790 61.510 2033370 0.153 VB




Channel: B Current Time: Feb 28, 2001 11:08:35 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrotn\200\chrom\16087.1 Data file creation time: Feb 28, 2001 11:06:19 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

fffffffrrr

rrrffr

16088 39-A

:ea Report

?kno Start RT Stop Area Area% Flag

1 22.760 22.980 23.220 5899 0.001 BB 2 28.380 30.620 37.340 179952304 21.314 BV 3 37.340 39.900 60.060 664328320 78.685 VB

external Standard Report

• Name Amount Units RT Min Max Mean %SD

I Oxygen 20.738 % 30.620 0.000 635.565 22.926 296.975 • Nitrogen 77.944 % 39.900 0.000 856.321 73.096 175.472

I Channel: A Current Time: Feb 28, 2001 11:11:39 Flethod: c:\mti\ezchrom\200\methods\raymark:. 1'?ile : c:\mti\ezchrom\200\chrom\16088.1 •Data file creation time: Feb 28, 2001 11:09:23 instrument ID: 02402283 1 Column Type: 10m MS5A Karrier Gas: He |!:olumn Head Pressure: 29.7 psi 'Jolumn Temperature: 65 C •instrument Gain: LOW |aample Time: 30 seconds 'inject Time: 50 milliseconds Blun Time: 100 seconds

Area Report


12 37.960 56.570

38.970 58.810

56.570 1328284928 61.530 2537481

99.809 0.191

BV VB




Channel: B Current Time: Feb 28, 2001 11:11:40 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16088.1Data file creation time: Feb 28, 2001 11:09:23Instrument ID: 02402283 Column Type: 8m PPQCarrier Gas: HeColumn Head Pressure: 16.7 psi Column Temperature: 41 CInstrument Gain: LOWSample Time: 30 seconds Inject Time: 80 millisecondsRun Time: 100 seconds

''

^ .f

*lj • I

T '• •

.MJ *

1

1

1

1

1

1

1

1

f

frrrfrrrrrfrfrrr

16089 40-A

Report fkno Start RT Stop Area Area% Flag f1 28.380 30.620 37.340 180812448 21.423 BV 2 37.340 39.900 59.740 663205632 78.577 VB f,External Standard Report r


f Oxygen 20.840 % 30.620 0.000 635.565 22.914 296.263 Nitrogen 77.808 % 39.900 0.000 856.321 73.124 174.894

II Zhannel: A Current Time: Feb 28, 2001 11:14:57 Pwethod: c:\mti\ezchrom\200\methods\raymark. fFile : c:\mti\ezchrom\200\chrom\16089.1 JData file creation time: Feb 28, 2001 11:12:41 ^Instrument ID: 02402283 ; Column Type: 10m MS5A Carrier Gas: He ftolumn Head Pressure: 29.7 psi * Column Temperature: 65 C Instrument Gain: LOW nSample Time: 30 seconds f Inject Time: 50 milliseconds lun Time: 100 seconds

Area Report


12 37.920 56.690

38.930 58.770

56.690 1328750592 61.490 1345185

99.899 0.101

BV VB




Channel: BCurrent Time: Feb 28, 2001 11:14:57Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16089.1Data file creation time: Feb 28, 2001 11:12:41Instrument ID: 02402283 Column Type: 8m PPQCarrier Gas: HeColumn Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

j *

Pj / "

^ I

I

.

.

ffff pffff ff i

16100 41-A

rea Report r;kno Start RT Stop Area Area% Flag

t. 1 28.380 30.620 37.340 180369968 21.374 BV 2 37.340 39.900 59.740 663501696 78.626 VB


f,Name Amount Units RT Min Max Mean %SD

Oxygen 20.788 % 30.620 0.000 635.565 22.901 295.560 r;Nitrogen 77.844 % 39.900 0.000 856.321 73.151 174.320

I hannel: A •current Time: Feb 28, 2001 11:18:03 •ethod: c:\mti\ezchrom\200\tnethods\raymark. | ile : c:\mti\ezchrom\200\chrom\16100.1

file creation time: Feb 28, 2001 11:15:47 nstrument ID: 02402283 !olumn Type: 10m MS5A

Carrier Gas: He Plolumn Head Pressure: 29.7 psi I :oi'umn Temperature: 65 C instrument Gain: LOW llample Time: 30 seconds f nject Time: 50 milliseconds .un Time: 100 seconds

*fff r r r rf

Area Report

Pkno Start RT Stop Area Area% Flag ''I

1 37.920 38.930 56.530 1327997056 99.841 BV 2 56.530 58.770 61.490 2116952 0.159 VB j




Channel: B Current Time: Feb 28, 2001 11:18:03 1 Method: c:\mti\ezchrom\200\methods\raymark. _ File : c:\mti\ezchrom\200\chrom\16100.1 T Data file creation time: Feb 28, 2001 11:15:47 ' Instrument ID: 02402283 _ Column Type: 8m PPQ j Carrier Gas: He ' Column Head Pressure: 16.7 psi j. Column Temperature: 41 C | Instrument Gain: LOW ' Sample Time: 30 seconds m Inject Time: 80 milliseconds 1 Run Time: 100 seconds '

1

1

1

1

1

1

1

1

1

1 16101 P 42-A

r p

r ppppppp

fp

i

I

frea Report fkno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 180369584 21.360 BV 2 37.340 39.900 59.740 664070720 78.640 VB


.flame Amount Units RT Min Max Mean %SD

3xygen 20.788 % 30.620 0.000 635.565 22.889 294.861 Nitrogen 77.913 % 39.900 0.000 856.321 73.178 173.751

Tiannel:A larrent Time: Feb 28, 2001 11:21:28 ethod: c:\mti\ezchrom\200\methods\raymark. ile c:\mti\ezchrom\200\chrom\16101.1 ,ata file creation time: Feb 28, 2001 11:19:12 Instrument ID: 02402283 Dlumn Type: 10m MS5A

Parrier Gas: He >lumn Head Pressure: 29.6 psi olumh' Temperature: 65 C instrument Gain: LOW imple Time: 30 seconds nject Time: 50 milliseconds oan Time: 100 seconds

Area Report


123

37.910 56.680 90.920

38.920 58.760 93.640

56.680 1329353088 61.480 1742521 98.280 430126

99.837 0.131 0.032

BV VB BE


Name Amount Units RT Win Max Mean %SD f|

Carbon Dioxide 995.751 ppm58.760 119487961613522354.000 929.516

Channel: B Current Time: Feb 28, 2001 11:21:28Method: c:\mti\ezchrom\200\methods\raymark.File : c:\mti\ezchrom\200\chrom\16101.1 Data file creation time: Feb 28, 2001 11:19:12 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

j_ [Jj

1

r

rfr rrf

ff

16086 37-A

rea Report

ftoo Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 179094496 21.208 BV r. 2 37.340 39.900 60.060 665366976 78.792 VB

External Standard Report r rName Amount Units RT Min Max Mean %SD

Oxygen 20.636 % 30.620 0.000 635.565 22.876 294.179 Nitrogen 78.071 % 39.900 0.000 856.321 73.206 173.186

I rhannel: A Current Time: Feb 28, 2001 11:26:31 •Method: c:\mti\ezchrom\200\rnethods\raymark. I 7ile : c:\mti\ezchrom\200\chrom\16086.1 —Data file creation time: Feb 28, 2001 11:24:15 •Instrument ID: 02402283 I Column Type: 10m MS5A Carrier Gas: He Prolumn Head Pressure: 29.6 psi | Column Temperature: 65 C Instrument Gain: LOW Psample Time: 30 seconds f Inject Time: 50 milliseconds r.un Time: 100 seconds r r rf rfff

Area Report


1 56.540 58.620 61.340 2638063 -0.790 BB




Channel: B Current Time: Feb 28, 2001 11:26:31 Method: c: \mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16086.1 Data file creation time: Feb 28, 2001 11:24:15 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

ff r rf r r r r rf rf r r rf r r

16100A 41-ADUP

rea Report

("kno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 180265408 21.369 BV 2 37.340 39.900 59.100 663305600 78.631 VB

-xternal Standard Report


fbxygen 20.775 % 30.620 0.000 635.565 22.864 293.491 'Nitrogen 77.820 % 39.900 0.000 856.321 73.232 172.629

I fhchannel: A Current Time: Feb 28, 2001 12:00:29 plethod: c:\mti\ezchrom\200\methods\raymark. Vile : c:\mti\ezchrom\200\chrom\16100DUP.l Lata file creation time: Feb 28, 2001 11:58:13 •fistrument ID: 02402283 lolumn Type: 10m MS5A Carrier Gas: He lolumn Head Pressure: 29.6 psi olumn Temperature: 65 C instrument Gain: LOW imple Time: 30 seconds nject Time: 50 milliseconds tun Time: 100 seconds

Area Report


1 25.860 26.380 27.050 25074 0.002 BB 2 37.950 38.960 56.560 1327471872 99.821 BV 3 56.560 58.640 61.520 2358075 0.177 VB




Channel: B Current Time: Feb 28, 2001 12:00:30 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16100DUP.l Data file creation time: Feb 28, 2001 11:58:13 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.8 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

f r

f f r r rff

f

16102 43-A

rea Report


1 28.380 30.620 37.340 171680000 20.429 BV 2 37.340 39.900 60.060 668714432 79.571 VB



"oxygen 19.756 % 30.620 0.000 635.565 22.847 292.883 Nitrogen 78.464 % 39.900 0.000 856.321 73.262 172.070

'hannel: A Jurrent Time: Feb 28, 2001 12:06:01 Jethod: .c:\mti\ezchrom\200\methods\raymark. 'ile : c:\mti\ezchrom\200\chrom\16102.1

JlJata file creation time: Feb 28, 2001 12:03:45 •instrument ID: 02402283 I :olumn Type: 10m MS5A Carrier Gas: He •Column Head Pressure: 29.7 psi 1 !olumn Temperature: 65 C ^Instrument Gain: LOW •Sample Time: 30 seconds 1 .nject Time: 50 milliseconds

^un Time: 100 seconds

Area Report


1 37.950 38.960 44.240 1321036032 99.002 BV 2 56.400 58.640 61.680 13322770 0.998 BB




Channel: B Current Time: Feb 28, 2001 12:06:01 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrotn\16102.1 Data.file creation time: Feb 28, 2001 12:03:45 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain:'LOW r--nple Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

(Iff rf rrrr F r rf

r

16103 44-A

1

Lrea Report


1 28.380 30.620 37.340 180490624 21.382 BV

I! 2 37.340 39.900 59.100 663641600 78.618 VB


fName Amount Units RT Min Max Mean %SD

Oxygen 20.802 % 30.620 0.000 635.565 22.835 292.202 Nitrogen 77.861 % 39.900 0.000 856.321 73.288 171.523

ft I hannel: A Current Time: Feb 28, 2001 12:15:30 •ethod: c:\mti\ezchrom\200\methods\raymark. I 'ile : c:\mti\ezchrom\200\chrom\16103.1

file creation time: Feb 28, 2001 12:13:14 nstrument ID: 02402283 lolumn Type: 10m MS5A

Carrier Gas: He Molumn Head Pressure: 29.7 psi | Column Temperature: 65 C ^nstrument Gain: LOW Rample Time: 30 seconds | inject Time: 50 milliseconds

f.un Time: 100 seconds

ff r r r r r r

Area Report

r Pkno Start RT Stop Area Area% Flag

I I 37.980 38.990 56.590 1327432192 99.850 BV 2 56.590 58.830 61.550 2000379 0.150 VB

r I kternal Standard Report

r t &ame Amount Units RT Min Max Mean %SD

f£arbon Dioxide 1143.102 ppm 58.830 119487961613218546.000 940.197

Channel: B Hirrent Time: Feb 28, 2001 12:15:30 Lfethod: c:\mti\e2chrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16103.1 Fata file creation time: Feb 28, 2001 12:13:14 Instrument ID: 02402283 Column Type: 8m PPQ farrier Gas: He Lolumn Head Pressure: 16.7 psi Column Temperature: 41 C [ strument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds J in Time: 100 seconds

r r r r r r r r r

r r

16104 45-A

fffff r rffffff r

lArea Report

LPkno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 180591824 21.377 BV | 2 37.340 39.900 58.780 664187904 78.623 VB


1 Name Amount Units RT Win Max Mean %SD

^ Oxygen 20.814 % 30.620 0.000 635.565 22.824 291.525 f Nitrogen 77.927 % 39.900 0.000 856.321 73.314 170.981

Wchannel: A 'current Time: Feb 28, 2001 12:18:48 ^Method: c:\mti\ezchrom\200\methods\raymark. IFile : c:\mti\ezchrom\200\chrom\16104.1 ' bata file creation time: Feb 28, 2001 12:16:32 •[instrument ID: 02402283 fColumn Type: 10m MS5A

Carrier Gas: He •Column Head Pressure: 29.7 psi I Column Temperature: 65 C Instrument Gain: LOW

•Sample Time: 30 seconds * Inject Time: 50 milliseconds __Run Time: 100 seconds

Area Report


1 37.960 38.970 56.570 1328799616 99.826 BV 2 56.570 58.810 61.530 2313600 0.174 VB




Channel: B Current Time: Feb 28, 2001 12:18:49 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16104.1 Data file creation time: Feb 28, 2001 12:16:32 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.8 psi Column Temperature: 41 C Instrument Gain: LOW '' Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

ffffffFf fF FFF FFFF FF

16105 46-A

Urea Report

iPkno Start RT Stop Area Area% Flag

1 28 .060 30.300 37.340 180637552 21.334 BV I 2 37.340 39 .900 57.500r 666057344 78.666 VB


! Name Amount Units RT Min Max Mean %SD

f^Oxygen 20.820 % 30.300 0.000 635.565 22.813 290.852 f Nitrogen 78.152 % 39.900 0.000 856.321 73.341 170.441

1 Channel: A Current Time: Feb 28, 2001 13:29:50

Method: c:\mti\ezchrom\200\methods\raymark. f?ile : c:\mti\ezchrom\200\chrom\16105.1 ^Data file creation time: Feb 28, 2001 13:27:33 •Instrument ID: 02402283 * Column Type: 10m MS5A —Carrier Gas: He •Column Head Pressure: 29.7 psi * Column Temperature: 65 C —Instrument Gain: LOW •Sample Time: 30 seconds | Inject Time: 50 milliseconds lun Time: 100 seconds

Area Report


1 25.850 26.390 27.070 27283 0.002 BB 2 38.000 39.010 47.970 1332343424 99.733 BB 3 56.930 59.010 61.890 3542585 0.265 BB




Channel: B Current Time: Feb 28, 2001 13:29:50 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16105.1 Data file creation time: Feb 28, 2001 13:27:33 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 40 C' Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

m 16106

f

f r

ffff rff

iorea Report


f • 1 28.060 30.300 37.340 177088080 20.980 BV • 2 37.340 39.900 57.500 667011968 79.020 VB

fExternal Standard Report


ixygen 20.398 % 30.300 0.000 635.565 22.800 290.214 Nitrogen 78.264 % 39.900 0.000 856.321 73.368 169.904

ffhannel: A Current Time: Feb 28, 2001 13:33:11 Method: c:\mti\ezchrom\200\methods\raymark. f|ile : c:\mti\ezchrom\200\chrom\16106.1 jJata file creation time: Feb 28, 2001 13:30:55

istrument ID: 02402283 >lumn Type: 10m MS5A

^carrier Gas: He llolumn Head Pressure: 29.7 psi f lolumn Temperature: 65 C ^nstrument Gain: LOW •temple Time: 30 seconds * inject Time: 50 milliseconds JJun Time: 100 seconds

Area Report


1 37.910 38.920 56.680 1329233024 99.252 BV 2 56.680 58.920 61.960 10017870 0.748 VB




Channel : B Current Time: Feb 28, 2001 13:33: 12 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16106.1 Data file creation time: Feb 28, 2001 13:30:55 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 40 C Instrument Gain: LOW ' Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

n n

rr r ' 16108

f 49"A

frr r

frrrr nf

f

rea Report

}kno Start RT Stop Area Area% Flag

1 28.060 30.300 37.340 181754576 21.441 BV 2 37.340 39.900 57.180 665922112 78.559 VB

eternal Standard Report

NameL

Amount Units RT Win Max Mean %SD

T[ Dxygen 20.952 % 30.300 0.000 635.565 22.789 289.541 'Nitrogen I

78.136 % 39.900 0.000 856.321 73.394 169.374

^ aannel: A Larrent Time: Feb 28, 2001 13:36:18

c:\mti\e2chrom\200\methods\raymark. : c:\mti\ezchrom\200\chrom\16108.1

file creation time: Feb 28, 2001 13:34:02 istrument ID: 02402283 blumn Type: 10m MS5A .arrier Gas: He >lumn Head Pressure: 29.6 psi >lumn Temperature: 65 C

instrument Gain: LOW imple Time: 30 seconds iject Time: 50 milliseconds

lun Time: 100 seconds

Report


1 37.900 38.910 56.990 1334587264 99,926 BV 2 56.990 59.070 61.630 982231 0.074 VB


Name Amount Units RT Win Max Mean %SD


Channel: B Current Time: Feb 28; 2001 13:36:19 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16108.1 Data file creation time: Feb 28, 2001 13:34:02 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 40 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

frr 16109

50-A

rtrf

r

rr

•fcrea Report

fkno Start . RT Stop Area Area% Flag

1 28.060 30.300 37.340 175409232 20.750 BV 2 37.340 39.900 57.500 669921472 79.250 VB

External Standard Report t Name Amount Units RT Min Max Mean %SD

j Oxygen 20.199 % 30.300 0.000 635.565 22.775 288.925 Nitrogen 78.605 % 39.900 0.000 856.321 73.422 168.844

I Channel: A Current Time: Feb 28, 2001 13:39:49

Wethod: c:\mti\ezchrom\200\methods\raymark. I ile : c:\mti\ezchrom\200\chrom\16109.1 J3ata file creation time: Feb 28, 2001 13:37:32 Pknstrument ID: 02402283 *polumn Type: 10m MS5A Carrier Gas: He jPpolumn Head Pressure: 29.6 psi f column Temperature: 65 C ^Instrument Gain: LOW PjSample Time: 30 seconds f Inject Time: 50 milliseconds Wlun Time: 100 seconds

Area Report


1 25.860 26.400 27.050 24836 0.002 BB 2 37.940 38.950 56.710 1330974848 99.414 BV 3 56.710 58.950 61.830 7823120 0.584 VB





ff 16110 r 51-A

r pf ppppP ppr ppp

rea Report


f. 1 28.060 30.300 37.340 181435168 21.419 BV 2 37.340 39.900 57.180 665628416 78.581 VB


f,Name Amount Units RT Min Max Mean %SD

f:Oxygen 20.914 % 30.300 0.000 635.565 ' 22.765 288.263 Nitrogen 78.102 % 39.900 0.000 856.321 73.448 168.324

I hannel: A Current Time: Feb 28, 2001 13:45:04

•fethod: c:\mti\ezchrom\200\methods\raymark. I'ile : c:\mti\ezchrom\200\chrom\16110.1 J)ata file creation time: Feb 28, 2001 13:42:48 instrument ID: 02402283 f :olumn Type: 10m MS5A Carrier Gas: He Rolumn Head Pressure: 29 .6 psi * :olumn Temperature: 65 C ^instrument Gain: LOW sample Time: 30 seconds | inject Time: 50 milliseconds Jlun Time: 100 seconds

Report


1 37.970 38.980 56.900 1332972416 99.896 BV 2 56.900 58.980 61.540 1382507 0.104 VB




Channel: B Current Time: Feb 28, 2001 13:45:05 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16110.1 Data file creation time: .Feb 28, 2001 13:42:48 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 40 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

r rrrr

16111 51 -A DUP

r pr pr pppp.f ppp

rrea Report r_kno Start RT Stop Area Area% Flag

1 28.060 30.300 37.340 181781104 21.444 BV r 2 37.340 39.900 56.860 665917504 78.556 VB

External Standard Report r,Name Amount Units RT Min Max Mean %SD

f:Oxygen 20.955 % 30.300 0.000 635.565 22.755 287.603 Nitrogen 78.136 % 39.900 0.000 856.321 73.473 167.809

I hannel: A •Current Time: Feb 28, 2001 13:49:16 Method: c:\mti\ezchrom\200\methods\raymark. 1 ile : c:\mti\ezchrom\200.\chrom\16111.1 Jata file creation time: Feb 28, 2001 13:46:59 •nstrument ID: 02402283 I iolumn Type: 10m MS5A Carrier Gas: He Rolumn Head Pressure: 29.7 psi | lolumn Temperature: 65 C instrument Gain: LOW Mample Time: 30 seconds | ,nject Time: 50 milliseconds

:un Time: 100 seconds

Area Report


1 37.930 38.940 56.860 1333234560 99.944 BV 2 56.860 58.940 61.020 743628 0.056 W





i

n n r

16112 52-A

ffr

r

rr

r Report

r'kno Start RT Stop Area Area% Flag

i 1 28.380 30.300 37.340 181561760 21.444 BV 2 37.340 39.900 56.860 665106816 78.556 VB

L'xternal Standard Report rName Amount Units RT Min Max Mean %SD r1

Oxygen 20.929 % 30.300 0.000 635.565 22.745 286.949 Nitrogen 78.039 % 39.900 0.000 856.321 73.498 167.299

• I hannel: A Vurrent Time: Feb 28, 2001 13:55:38 liethod: c:\mti\ezchrom\200\methods\raymark. JPile : c:\mti\ezchrom\200\chrom\16112.1 •jjata file creation time: Feb 28, 2001 13:53:21 •nstrument ID: 02402283 olumn Type: 10m MS5A arrier Gas: He

llolumn Head Pressure: 29.7 psi I Eolumn Temperature: 65 C instrument Gain: LOW •ample Time: 30 seconds I nject Time: 50 milliseconds

iun Time: 100 seconds

n

P P P P P P P P

Area Report


1 25.860 26.370 27.060 25850 0.002 BE 2 37.940 38.950 56.710 1332356480 99.931 BV 3 56.710 58.790 61.510 897880 0.067 VB





f pp '

rr prrfrrrrrr

AMB0258P

rrea Report rkno Start RT Stop Area Area% Flag

1 28.380 30.300 37.340 181643376 21.451 BV r, 2 37.340 39.900 57.180 665158592 78.549 VB


Name Amount Units RT Win Max Mean %SD rOxygen 20.939 % 30.300 0.000 635.565 22.736 286.299 Nitrogen 78.045 % 39.900 0.000 856.321 73.522 166.795

• Channel: A "Current Time: Feb 28, 2001 14:05:50 ftethod: c:\mti\ezchrom\200\methods\raymark. pile : c:\mti\ezchrom\200\chrom\AMB0258P.l 'jata file creation time: Feb 28, 2001 14:03:34 Instrument ID: 02402283 l^olumn Type: 10m MS5A Carrier Gas: He •Column Head Pressure: 29.6 psi I Column Temperature: 65 C ^nstrument Gain: LOW •ample Time: 30 seconds I inject Time: 50 milliseconds ,un Time: 100 seconds f r r r r r r r r

Area Report


1 37.910 38.920 56.680 1332524288 99.944 BV 2 56.680 58.600 61.320 746575 0.056 VB




Channel: B Current Time: Feb 28, 2001 14:05:51 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\AMB0258P.l Data file creation time: Feb 28, 2001 14:03:34 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 41 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

rfr 1

r rrP pr pppppppr•

16089RES 40-A

•Area Report

?kno Start RT Stop Area Area% Flag f 1 28.380 30.300 37.340 180667600 21.416 BV

r, 2 37.340 39.900 56.540 662940672 78.584 VB


rName Amount Units RT Min Max Mean %SD

rOxygen 20.823 % 30.300 0.000 635.565 22/726 285.661 Nitrogen 77.775 % 39.900 0.000 856.321 73.545 166.297

Fzhannel: A 'Current Time: Feb 28, 2001 14:13:01 •Method: c:\mti\ezchrorn\200\methods\rayrnark. pile : c:\mti\ezchrom\200\chrom\16089RES.l *Jata file creation time: Feb 28, 2001 14:10:44 •Instrument ID: 02402283 Fbolumn Type: 10m MS5A " Carrier Gas: He pfcolumn Head Pressure: 29.7 psi Ibolumn Temperature: 65 C Instrument Gain: LOW •sample Time: 30 seconds I Inject Time: 50 milliseconds Run Time: 100 seconds r r r r r r r r r

Area Report


1 25.860 26.370 27.040 24617 0.00-2 BB 2 37.920 38.930 56.530 1328230528 99.890 BV 3 56.530 58.610 61.330 1434824 0.108 VB




Channel: B Current Time: Feb 28, 2001 14:13:01 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16089RES.l Data file creation time: Feb 28, 2001 14:10:44 Instrument ID: 02402283 T Column Type: 8m PPQ ' ' Carrier Gas: He _ Column Head Pressure: 16.7 psi | Column Temperature: 41 C ' Instrument Gain: LOW _ Sample Time: 30 seconds | Inject Time: 80 milliseconds Run Time: 100 seconds . «

1

1

1

1

1

1

1

1

r

P

rfP ppp

rr

r

f 16088RES

39-A

krea Report


1 28.380 30.300 37.340 180600272 21.401 BV 2 37.340 39.900 56.540 663301760 78.599 VB



Foxygen 20.815 % 30.300 0.000 635.565 22.716 285.027 'Nitrogen 77.819 % 39.900 0.000 856.321 73.567 165.804

FI hannel: A \Jurrent Time: Feb 28, 2001 14:19:45 ethod: c:\mti\ezchrom\200\methods\raymark. ile : c:\mti\ezchrom\200\chrom\16088RES.l

uata file creation time: Feb 28, 2001 14:17:29

Fnstrument ID: 02402283 olumn Type: 10m MS5A Carrier Gas: He •Column Head Pressure: 29.6 psi I lolumn Temperature: 65 C instrument Gain: LOW •fatnple Time: 30 seconds I.nject Time: 50 milliseconds iun Time: 100 seconds

Area Report


1 37.860 39.030 56.310 1327828608 99.886 BV 2 56.310 58.550 61.110 1516567 0.114 VB




Channel: B Current Time: Feb 28, 2001 14:19:45 1 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16088RES.l | Data file creation time: Feb 28, 2001 14:17:29 . •' Instrument ID: 02402283 ^ Column Type: 8m PPQ | Carrier Gas: He Column Head Pressure: 16.7 psi ,-. Column Temperature: 41 C ] Instrument Gain: LOW Sample Time: 30 seconds -— Inject Time: 80 milliseconds I Run Time: 100 seconds

1

1

n n n n n n n

fffrfrrrf rrr

16113 53-A

rea Report

?>kno Start RT Stop Area Area% Flag

1 22.750 23.000 23.270 6762 0.001 BB 2 28.380 30.620 37.340 178239264 21.233 BV 3 37.340 39.900 56.220 661196992 78.766 VB


FName Amount Units RT Min Max Mean %SD

Oxygen 20.535 % 30.620 0.000 635.565 22.704 284.417 ItNitrogen 77.563 % 39.900 0.000 856.321 73.588 165.318

Channel: A •Current Time: Feb 28, 2001 14:53:15 T let hod: c:\mti\ezchrom\200\methods\raymark. Pile : c:\mti\ezchrom\200\chrom\16113.1 ;>ata file creation time: Feb 28, 2001 14:50:59 ;nstrument ID: 02402283 Column Type: 10m MS5A Carrier Gas: He Column ftead Pressure: 29.6 psi

Column Temperature: 65 C mnstrument Gain: LOW I Sample Time: 30 seconds JEnject Time: 50 milliseconds' Pkun Time: 100 seconds

f f r rf r r r

Area Report


1 37.870 39.040 56.000 1320975360 99.526 BV 2 56.000 58.240 61.120 6285500 0.474 VB





16107

f 48-A

rrr rrrr r r rrrr

rea Report rkno Start RT Stop Area Area% Flag

t 1 28.380 30.620 37.340 180398160 21.421 BV 2 37.340 39.900 55.900 661742656 78.579 VB

External Standard Report rName Amount Units RT Min Max Mean %SD rOxygen 20.791 % 30.620 0.000 635.565 22.694 283.793 Nitrogen .77.629 % 39.900 0.000 856.321 73.609 164.835

r hannel: A Current Time: Feb 28, 2001 14:58:52 Bfaethod: c:\mti\ezchrom\200\methods\raymark. f ile : c:\mti\ezchrom\200\chrom\16107.1 Data file creation time: Feb 28, 2001 14:56:35 •Instrument ID: 02402283 fColumn Type: 10m MS5A * Carrier Gas: He •column Head Pressure: 29.7 psi Ibolumn Temperature: 65 C Instrument Gain: LOW •Cample Time: 30 seconds Itnject Time: 50 milliseconds ~.un Time: 100 seconds

r ppr pppp

Area Report M

Pkno Start RT Stop Area Area% Flag M

1 25.860 26.360 27.030 24032 0.002 BB 2 37.990 39.000 44.600 1322705920 99.905 BB 3 56.280 58.360 60.920 1231889 0.093 BB 1

External Standard Report 1



Channel: B Current Time: Feb 28, 2001 14:58:52 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16107.1 Data file creation time: Feb 28, 2001 14:56:35 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 42 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds _

"

1

1

1 Li

1

fl

n f!

16114 54-A

p

f. f

F

F

rea Report


1 28.380 30.620 37.340 174082432 20.744 BV

f 2 37.340 39.900 56.860 664997824 79.244 W 3 56.860 58.780 62.620 99812 0.012 VB

ternal Standard Report

T

fName Amount Units RT Min Max Mean %SD

f.Oxygen 20.041 % 30.620 0.000 635.565 22.680 283.223 Nitrogen 78.026 % 39.900 0.000 856.321 73.632 164.353

Channel: A •fcurrent Time: Feb 28, 2001 15:04:28 fwiethod: c:\mti\ezchrom\200\methods\raytnark. File : c:\mti\ezchrom\200\chrom\16114.1

Bpata file creation time: Feb 28, 2001 15:02:12 ftnstrument ID: 02402283 Column Type: 10m MS5A •Carrier Gas: He I Column Head Pressure: 29.6 psi Column Temperature: 65 C •instrument Gain: LOW I Sample Time: 30 seconds Inject Time: 50 milliseconds

•Run Time: 100 seconds

Area Report -"I

Pkno Start RT Stop Area Area% Flag •*!

123

37.950 43.440 55.920

38.960 44.720 58.160

43.440 1318214656 47.280 255670 61.200 8644617

99.329 0.019 0.651

BV VB BB 1

External Standard Report *l



Channel: B Current Time: Feb 28, 2001 15:04:28 Method: c:\mti\ezchrom\200\methods\raymark.File : c:\mti\ezchrom\200\chrom\16114.1Data file creation time: Feb 28, 2001 15:02:12 Instrument ID: 02402283Column Type: 8m PPQCarrier Gas: He Column Head Pressure: 16.7 psiColumn Temperature: 42 CInstrument Gain: LOW Sample Time: 30 secondsInject Time: 80 millisecondsRun Time: 100 seconds

.

1

1 T >

r|

MJ H '

j| ' • —

1

1

1

1

1

1

1

'

1

fFf r

pppppp

16115 55-A

f

rea Report


1 28.380 30.620 37.340 177650512 21.170 BV 2 37.340 39.900 55.580 661504896 78.830 VB


t


Oxygen 20.465 % 30.620 0.000 635.565 22.669 282.628 Nitrogen 77.600 % 39.900 0.000 856.321 73.653 163.879

l hannel: A •Current Time: Feb 28, 2001 15:09:12 •jtethod: c:\mti\ezchrotn\200\methods\raymark. Ir'ile : c:\mti\ezchrom\200\chrom\16115.1 *bata file creation time: Feb 28, 2001 15:06:56 Instrument ID: 02402283 |;Column Type: 10m MS5A * Carrier Gas: He •Column Head Pressure: 29.7 psi 1 lolumn Temperature: 65 C —Instrument Gain: LOW •6ample Time: 30 seconds | Inject Time: 50 milliseconds .Run Time: 100 seconds

Area Report *

Pkno Start RT Stop Area Area% Flag "1

1 37.960 38.970 54.810 13194195202 56.090 58.170 61.050 5596252


99.578 0.422

BB BB fl

r



Channel: BCurrent Time: Feb 28, 2001 15:09:12 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16115.1 ' Data file creation time: Feb 28, 2001 15:06:56 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 42 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

[j

1

1

1

1

1

1

F rrfffrrrr

16116 56-A

.rea Report

r knof 1 Start

28.380

RT

30.620

Stop

37.340

Area

174397168

Area%

20.878

Flag

BV r. 2 37.340 39.900 55.900

Jxternal Standard Report

660937216 79.122 VB

* Name Amount Units RT Min Max Mean %SD rOxygen 20.079 % 30.620 0.000 635.565 22.655 282.063 Nitrogen 77.531 % 39.900 0.000 856.321 73.673 163.410

Channel: A Current Time: Feb 28, 2001 15:12:16 ftethod: c:\mti\ezchrom\200\methods\raymark. pile :. c:\mti\ezchrom\200\chrom\16116.1 iJata file creation time: Feb 28, 2001 15:10:00

Instrument ID: 02402283 I .olumn Type: 10m MS5A Varrier Gas: He •Column Head Pressure: 29.7 psi I lolumn Temperature:' 65 C Instrument Gain: LOW

•ample Time: 30 seconds I nject Time: 50 milliseconds ".un Time: 100 seconds

Area Report


1 37.930 38.940 55.740 1315072000 98.927 BV 2 55.740 58.140 61.180 14248761 1.072 VB 3 65.180 65.980 68.060 8458 0.001 BE





f

r r r pppprffff

16117 57-A

rea Report rkno Start RT Stop Area Area% Flag

t 1 28.380 30.620 37.340 180186096 21.424 BV 2 37.340 39.900 55.580 660868672 78.576 VB

xternal Standard Report rName Amount Units RT Min Max Mean %SD

f:Oxygen 20.766 % 30.620 0.000 635.565 22.646 281.456 Nitrogen 77.523 % 39.900 0.000 856.321 73.693 162.945

rlannel: A .urrent Time: Feb 28, 2001 15:17:51 ethod: c:\mti\ezchrom\200\methods\raymark. ile : c:.\mti\ezchrom\200\chrom\16117 .1

rwata file creation time: Feb 28, 2001 15:15:35 Instrument ID: 02402283 | olumn Type: 10m MS5A Xarrier Gas: He olumn Head Pressure: 29.7 psi olumn Temperature: 65 C instrument Gain: LOW •tample Time: 30 seconds I nject Time: 50 milliseconds tun Time: 100 seconds

Area Report ^

Pkno Start RT Stop Area Area% Flag "1

1 37.920 38.930 56.050 1323054464 99.903 BV 2 56.050 58.290 60.850 1279483 0.097 VB 1



Carbon Dioxide 731.151 ppm 58.290 119487961612066361.000 984.299 1 Channel: B Current Time: Feb 28, 2001 15:17:52 Si Method: c:\mti\ezchrom\200\methods\raymark. <_ File : c:\mti\ezchrom\200\chrom\16117.1 ,| Data file creation time: Feb 28, 2001 15:15:35 < " Instrument ID: 02402283 Column Type: 8m PPQ ?1 Carrier Gas: He ' Column Head Pressure: 16.7 psi , Column Temperature: 42 C , 1 Instrument Gain: LOW Sample Time: 30 seconds ^ Inject Time: 80 milliseconds i I Run Time: 100 seconds

1 1 1

f

r

rrrrrfr

16118 58-A

rea Report [kno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 178609600 21.276 BV 2 37.340 39.900 55.900 660883456 78.724 VB

.xternal Standard Report

L Name Amount Units RT Min Max Mean %SD

Oxygen 20.579 % 30.620 0.000 635.565 22.635 280.865 Nitrogen 77.525 % 39.900 0.000 856.321 73.712 162.484

(nannel: A Lurrent Time: Feb 28, 2001 15:22:26 ftethod: c:\mti\ezchrom\200\methods\raymark. Tile : c:\mti\ezchrom\200\chrom\16118.1 Lata file creation time: Feb 28, 2001 15:20:10 Instrument ID: 02402283 lolumn Type: 10m MS5A L.arrier Gas: He •olumn Head Pressure: 29.7 psi f !olumn Temperature: 65 C"

instrument Gain: LOW Cample Time: 30 seconds nject Time: 50 milliseconds

tun Time: 100 seconds

Area Report


1 37.970 38.980 48.580 1319037824 99.720 BB 2 56.100 58.180 61.060 3700987 0.280 BB





r rrrr r r prr

pr pP pPp

16119 59-A

r

r.rea Report rkno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 179801728 21.409 BV 2 37.340 39.900 55.580 660056064 78.591 VB


' Name Amount Units RT Min Max Mean %SD

I^Oxygen 20.720 % 30.620 0.000 635.565 22.625 280.268 f Nitrogen 77.424 % 39.900 0.000 856.321 73.731 162.028

I 1 Zhannel: A 1 Current Time: Feb 28, 2001 15:26:50 • ethod: c:\mti\ezchrom\200\methods\raymark. i file : c:\mti\ezchrom\200\chrom\16119.1 Data file creation time: Feb 28, 2001 15:24:34

•instrument ID: 02402283 1 Column Type: 10m MS5A Carrier Gas: He •tolumn Head Pressure: 29.7 psi 1 Column Temperature: 65 C Instrument Gain: LOW

•Sample Time: 30 seconds I Inject Time: 50 milliseconds "lun Time: 100 seconds

Area Report


1 37.910 38.920 56.040 1321859072 99.887 BV 2 56.040 58.120 61.000 1500371 0.113 VB





P pppppp

rrrrr ppppp

Pp

16120 60-A

•ft.r« Report


1 28.380 30.620 37.340 179355472 21.384 BV

r 2 37.340 39.900 55.580 659367424 78.616 VB

Jxternal standard Report rName Amount Units RT Min Max Mean %SD

Oxygen 20.667 % 30.620 0.000 635.565 22.616 279.679 fNitrogen 77.340 % 39.900 0.000 856.321 73.749 161.576

|bhannel: A * Current Time: Feb 28, 2001 15:31:40 •kethod: c:\mti\ezchrom\200\methods\raymark. J^ile : c:\mti\ezchrom\200\chrom\16120.1 *Jata file creation time: Feb 28, 2001 15:29:24 instrument ID: 02402283 rbolumn Type: 10m MS5A ' Carrier Gas: He Kolumn Head Pressure: 29.7 psi Fbolumn Temperature: 65 C

IInstrument Gain: LOW Sample Time: 30 seconds Inject Time: 50 milliseconds lun Time: 100 seconds

f r r r r r r r

Area Report


1 37.930 38.940 55.900 1320262784 99.817 BV 2 55.900 58.140 60.860 2426475 0.183 VB





f 16121 § 61 -A

r r

frr

r pr r pf ppppp

•krea Report


1 28.380 30.620 37.340 180183856 21.440 BV 2 37.340 39.900 55.580 660235008 78.560 VB

External Standard Report t rName Amount Units RT Min Max Mean %SD rOxygen 20.766 % 30.620 0.000 635.565 22.606 279.087 Nitrogen 77.446 % 39.900 0.000 856.321 73.768 161.128

I Channel: A "jurrent Time: Feb 28, 2001 15:36:40 Aethod: c:\mti\ezchrom\200\methods\raymark. f ile : c:\mti\ezchrom\200\chrom\16121.1 *Jata file creation time: Feb 28, 2001 15:34:23 instrument ID: 02402283 iColumn Type: 10m MS5A ^Carrier Gas: He •Column Head Pressure: 2.9 . 7 psi I bolumn Temperature: 65 C instrument Gain: LOW Sample Time: 30 seconds tnject Time: 50 "milliseconds lun Time: 100 seconds

Area Report -

Pkno .Start RT Stop Area Area% Flag

1 37.880 38.890 56.010 1322018560 99.930 BV 2 56.010 58.090 60.650 925639 0.070 VB


Name Amount Units RT Min Max Mean

Carbon Dioxide 528.950 ppm 58.090 119487961611823846.000

%SD

994.393

1

1

1

Run Time: 100 seconds

Channel: B Current Time: Feb 28, 2001 15:36:40 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16121.1Data file creation time: Feb 28, 2001 15:34:23Instrument ID: 02402283 Column Type: 8m PPQCarrier Gas: HeColumn Head Pressure: 16.7 psi Column Temperature: 42 CInstrument Gain: LOW ''Sample Time: 30 secondsInject Time: 80 milliseconds^3* * * P «* mf*. . T ^ f* t± *—i^^*^ *3 r^

1 flj

', J

fl ! "

J j '

^ jl

*

n n n n n n n n n

r 16122

ft 61-ADUP

f r r r rrrrrfF fr

Lrea Report

Etno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 177688816 21.231 BV 2 37.340 39.900 55.580 659230080 78.769 VB

-kternal Standard Report


3xygen 20.470 % 30.620 0.000 635.565 22.596 278.517 Nitrogen 77.323 % 39.900 0.000 856.321 73.786 160.684

• nannel:A lurrent Time: Feb 28, 2001 15:41:25 •ethod: .c:\mti\ezchrom\200\methods\raytnark. tfile : c:\mti\ezchrom\200\chrom\16122.1 Lata file creation time: Feb 28, 2001 15:39:09 istrument ID: 02402283 >lumn Type: 10m MS5A irrier Gas: He

flblumn Head Pressure: 29.7 psi I plumn Temperature: 65 C instrument Gain: LOW Mample Time: 30 seconds Ipject Time: 50 milliseconds Kun Time: 100 seconds

Area Report


1 37.870 39.040 55.680 1317533824 99.615 BV 2 55.680 57.920 60.960 '5098588 0.385 VB





r r f.f

I! fl

16123 62-A

fi

f•ea Report pen Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 178988880 21.366 BV 2 37.340 39.900 55.580 658726208 78.634 VB

txternal Standard Report

f.Name Amount Units RT Min Max Mean %SD

JDxygen 20.624 % 30.620 0.000 635.565 22.586 277.941 'Nitrogen 77.262 % 39.900 0 .000 856.321 73.803 160.245

lliannel: A Lurrent Time: Feb 28, 2001 15:46:10 llsthod: c:\mti\ezchrom\200\methods\raymark. Ijile : c:\mti\ezchrom\200\chrom\16123.1 uata file creation time: Feb 28, 2001 15:43:54 •Instrument ID: 02402283 I olumn Type: 10m MS5A Carrier Gas: He •olumn Head Pressure: 29.7 psi I plumn Temperature: 65 C Instrument Gain: LOW Pample Time: 30 seconds 'nject Time: 50 milliseconds lun Time: 100 seconds

.rea Report


1 37.950 38.960 55.760 1317376768 99.811 BV 2 55.760 58.000 60.720 2494770 0.189 VB





1

*Arrrr

f rfr

16124 63-A

r r

rarea Report r Start RT Stop Area Area% Flag

28.380 30.620 37.340 178384016 21.313 BV 2 37.340 39.900 55.260 658581760 78.687 VB


Name Amount Units RT Min Max Mean %SD I pxygen 20.552 % 30.620 0.000 635.565 22.576 277.374 Nitrogen 77.244 % 39.900 0.000 856.321 73.820 159.809

I hannel: A \jurrent Time: Feb 28, 2001 15:55:22

thod: c:\mti\ezchrom\200\methods\raymark. ile : c:\mti\ezchrom\200\chrom\16124.1 ata file creation time: Feb 28, 2001 15:53:05 strument ID: 02402283 lumn Type: 10m MS5A arrier Gas: He lumn Head Pressure: 29.7 psi lumn Temperature: 65 C

instrument Gain: LOW nample Time: 30 seconds [ fnject Time: 50 milliseconds

fl.un Time: 100 seconds

fl fl fl P fl ft fl fl

^.rea Report


1 37.890 38.900 55.540 1317147136 99.707 BV 2 55.540 57.780 60.660 3870585 0.293 VB



Carbon Dioxide 2211.818 ppm 57.780 119487961611648277.0001001.896

Channel: B fl Current Time: Feb 28, 2001 15:55:22 '* Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16124.1 PI Data file creation time: Feb 28, 2001 15:53:05 ** Instrument ID: 02402283 . Column Type: 8m PPQ j| Carrier Gas: He *•-' Column Head Pressure: 16.7 psi Column Temperature: 43 C If Instrument Gain: LOW ' *•"' Sample Time: 30 seconds -~ Inject Time: 80 milliseconds I] Run Time: 100 seconds

F r r r r r r r r

f ffff r rr rr r r rfrffr

16125 64-A

:ea Report

i?kno Start RT Stop Area Area% Flag

' 1 28.380 30.620 37.340 179347456 21.415 BV • 2 37.340 39.900 55.900 658134080 78.585 VB rExternal Standard Report


OxygenNitrogen

20.667 77.190

% 30.620 % 39.900

0.000 635.565 0.000 856.321

22.566 276.802 73.837 159.377

1 hannel: A Current Time: Feb 28, 2001 15:58:52 •jethod: c:\mti\ezchrom\200\methods\rayrnark. 1 file : c:\mti\ezchrom\200\chrom\16125.1 JData file creation time: Feb 28, 2001 15:56:36 •instrument ID: 02402283 1 folumn Type: 10m MS5A Carrier Gas: He Molumn Head Pressure: 29.7 psi I Column Temperature: 65 C .instrument Gain: LOW P|ample Time: 30 seconds | inject Time: 50 milliseconds .Run Time: 100 seconds

area Report

>kno Start RT Stop Area Area% Flag

1 37.960 38.970 53.850 1316598528 99.759 BB 2 55.770 57.850 60.570 1315648 0.100 BB 3 65.690 68.090 94.490 1858894 0.141 BB




Channel: B :urrent Time: Feb 28, 2001 15:58:52 Method: c:\mti\ezchrom\200\methods\raymark. Pile : c:\mti\ezchrom\200\chrom\16125.1 Data file creation time: Feb 28, 2001 15:56:36 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Ti.me: 80 milliseconds Run Time: 100 seconds

f

_ 16126 I 65-A

I L

f1

Cc Cc

I c[£ t

rea Report

Start RT Stop Area Area% Flag

22.790 23.040 23.310 6628 0.001 BB 28.380 30.620 37.340 177648736 21.251 BV 37.340 39.900 55.260 658283648 78.748 VB

I kternal Standard Report

Tame Amount Units RT Min Max Mean %SD

-Oxygen 20.465 % 30.620 0.000 635.565 22.556 276.246 Ipitrogen 77.208 % 39.900 0.000 856.321 73.853 158.949

Cannel: A rrent Time: Feb 28, 2001 16:03:04 thod: c:\mti\ezchrom\200\methods\raymark.

: c:\mti\ezchrom\200\chrom\16126.1 ita file creation time: Feb 28, 2001 16:00:48 istrument ID: 02402283

n Type: 10m MS5A Ijarrier Gas: He T*olumn Head Pressure: 29.7 psi Column Temperature: 65 C ^instrument Gain: LOW Sample Time: 30 seconds f"pject Time: 50 milliseconds

in Time: 100 seconds

C C 0 C fl 0 0

.rea Report a ?kno Start RT Stop Area Area% Flag a

1 25.860 26.340 26.970 21344 0.002 BB 2 38.000 39.010 47.010 1312959232 99.625 BB 3 55.650 57.730 60.610 4913308 0.373 BB a 4 91.170 91.970 93.730 5810 0.000 BB oExternal Standard Report




fff * 16127

f 66'A

cccc #-»«

L cc ccc cc

•

n yrI

c area Report

Jcno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 179692144 21.432 BV c 2 37.340 39.900 55.260 658744960 78.568 VB

fternal Standard Report

jrame Amount Units RT Min Max Mean %SD

Oxygen 20.707 % 30.620 0.000 635.565 22.547 275.679 —Nitrogen 77.264 % 39.900 0.000 856.321 73.870 158.524 IL

lannel: A .Current Time: Feb 28, 2001 16:07:55 1 jethod: c:\mti\ezchrom\200\methods\raymark. •File : c:\mti\ezchrom\200\chrom\16127.1 J3ata file creation time: Feb 28, 2001 16:05:38 i nstrument ID: 02402283 •Column Type: 10m MS5A aarrier Gas: He olumn Head Pressure: 29.7 psi olumn Temperature: 65 C Q nstrument Gain: LOW ample Time: 30 seconds nject Time: 50 milliseconds

Time: 100 seconds

krea Report


1 37.980 38.990 44.430 1317780096 99.930 BB 2 55.790 57.710 60.430 928001 0.070 BB



Carbon Dioxide 530.299 ppm57.710 119487961611477834.0001009.344

Channel : B Current Time: Feb 28, 2001 16:07:55 Method: c: \mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16127.1 Data file creation time: Feb 28, 2001 16:05:38 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

* 16128 f 67-A

fff

ccccccc

cccc

c

»a Report


1 28.380 30.620 37.340 179584608 21.429 BV 2 37.340 39.900 55.260 658446336 78.571 VB


fame Amount Units RT Min Max Mean %SD

£Jxygen 20.695 % 30.620 0.000 635.565 22.538 275.116 itrogen 77.228 % 39.900 0.000 856.321 73.886 158.102

annel: A |*irrent Time: Peb 28, 2001 16:10:44 Lithod: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16128.1 f~kta file creation time: Feb 28, 2001 16:08:28 Uistrument ID: 02402283 Column Type: 10m MS5A 4 arrier Gas: He Lblumn Head Pressure: 29.7 psi Column Temperature: 65 C I instrument Gain: LOW Cample Time: 30 seconds Inject Time: 50 milliseconds rim Time: 100 seconds

Area Report j1

Pkno Start RT Stop Area . Area% Flag H

1 25.860 26.390 27.020 23967 0.002 BB 2 37.920 38.930 55.730 1318985216 99.922 BV 1 3 55.730 57.810 60.370 1006504 0.076 VB J

Name Amount Units RT Min Max Mean %SD il

Carbon Dioxide

Channel: B

575.159 ppm 57.810 119487961611422119.0001011.815

0 Current Time: Feb 28, 2001 16:10:45 uuirieiiu i-Liue: reo 4a, z u u x J.D : xu : is —» Method: c:\mti\ezchrom\200\methods\raymark. Il File : c:\mti\ezchrom\200\chrom\16128.1 . * Data file creation time: Feb 28, 2001 16:08:28 . Instrument ID: 02402283 II Column Type: 8m PPQ Carrier Gas : He -j Column Head Pressure: 16.7 psi il Column Temperature: 43 C Instrument Gain: LOW ^\ Sample Time: 30 seconds li Inject Time: 80 milliseconds Run Time: 100 seconds «~j

I

L

* 16129 68-A

ff[

r*+ L C

C L

1r"

E C[CCCC[CC

c Report

no Start RT Stop Area Area% Flag (t 28.380 30.620 37.340 179538432 21.422 BV

37.340 39.900 55.260 658582976 78.578 VB

rternal Standard Report -Name Amount Units RT Min Max Mean %SD

)xygen 20.689 % 30.620 0.000 635.565 22.529 274.557 .-Nitrogen 77.245 % 39.900 0.000 856.321 73.902 157.683

lannel: A Purrent Time: Feb 28,.2001 16:13:54 I ethod: c:\mti\ezchrotn\200\methods\raymark. Tile : c:\mti\ezchrom\200\chrom\16129.1 Pata file creation time: Feb 28, 2001 16:11:38 tkstrument ID: 02402283 uolumn Type: 10m MS5A irrier Gas: He )lumn Head Pressure: 29.7 psi

Column Temperature: 65 C istrument Gain: LOW unple Time: 30 seconds

Enject Time: 50 milliseconds Time: 100 seconds

Area Report 3 Pkno Start RT Stop Area Area% Flag 3

1 2 3

37.960 55.770 93.370

38.970 57.690 95.930

52.090 1317544448 60.410 1116751 98.170 133981

99.905 0.085 0.010

BB BB BE J



Carbon Dioxide 638.159 ppm 57.690 119487961611366943.0001014.279 aChannel: B Current Time: Feb 28, 2001 16:13:54 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16129.1 Data file creation time: Feb 28, 2001 16:11:38 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column.Head Pressure: 16.7 psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

0 Li

u

tIIt c cccEE E E E£C E EEr»

16130

prea Report &«•'

no Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 178028752 21.300 BV

C 2 37.340 39.900 55.260 657795200 78.700 VB


lame Amount Units RT Min Max Mean %SD

^Oxygen 20.510 % 30.620 0.000 635.565 22.519 274.012 JJitrogen 77.149 % 39.900 0.000 856.321 73.918 157.269

mannel: A irrent Time: Feb 28, 2001 16:17:12 ithod: c:\mti\ezchrom\200\methods\raymark. Lie : c:\mti\ezchrom\200\chrom\16130.1 ita file creation time: Feb 28, 2001 16:14:56 istrument ID: 02402283 >lumn Type: 10m MS5A irrier Gas: He )lumn Head Pressure: 29.7 psi >lumn Temperature: 65 C

Instrument Gain: LOW I bmple Time: 30 seconds Tnject Time: 50 milliseconds

orin Time: 100 seconds Q

Q

Q

Area Report


1234

25.860 37.900 55.390 84.830

26.380 38.910 57.630 87.390

27.020 23745 55.390 1315212032 60.510 4376475 98.270 552339

0.002 99.625 0.332 0.042

BB BV VB BE

External Standard Report -r

Name Amount Units RT Min Max Mean %SD *"*

Carbon Dioxide 2500.905 ppm 57.630 119487961611312306.0001016.737 f]

Channel: BCurrent Time: Feb 28, 2001 16:17:12Method: c:\mti\ezchrom\200\methods\raymark.File : c:\mti\ezchrom\200\chrom\16130.1Data file creation time: Feb 28, 2001 16:14:56Instrument ID: 02402283 Column Type: 8m PPQCarrier Gas: HeColumn Head Pressure: 16.7 psi Column Temperature: 43 CInstrument Gain: LOWSample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

.

p, jj

|-| If

-i IJ

g~j Ij

0 E L

13

rrr

rrcr

c

ccr r

16132 70-A

rr

c

Report

Jcno Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 179022256 21.412 BV 2 37.340 39.900 54.940 657063360 78.588 VB

reafff External Standard Report

—Name Amount Units RT Min Max Mean %SD

""Oxygen 20.628 % 30.620 0.000 635.565 22.510 273.463 -Nitrogen 77.060 % 39.900 0.000 856.321 73.933 156.859

hannel: AL•Current Time: Feb 28, 2001 16:21:20 I ethod: c:\mti\ezchrotn\200\methods\raymark. %ile : c:\mti\ezchrom\200\chrom\16132.1 |Rata file creation time: Feb 28, 2001 16:19:04 I Instrument ID: 02402283 Tolumn Type: 10m MS5A Carrier Gas: He Ijolumn Head. Pressure: 29.7 psi tiolumn Temperature: 65 C f*nstrument Gain: LOW I ample Time: 30 seconds

Cinject Time: 50 milliseconds Hin Time: 100 seconds

C C f

C C C C

Area Report


1 13.330 13.430 13.520 702 0.000 BV 2 26.510 27.030 28.370 57796 0.004 BB 3 38.040 38.890 44.650 1310608128 99.881 BB 4 55.690 57.610 61.450 1506334 0.115 BB




Channel: B Current Time: Feb 28, 2001 16:21:21 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16132.1 Data file creation time: Feb 28, 2001 16:19:04 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: ..He Column Head Pressure: 16.7 psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

ff

f16133 71-A f

t cI cccc

c crcc

•lea Report

•^no 0 Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 178451088 21.367 BV 2 37.340 39.900 54.940 656703872 78.633 VB

Jap :ternal Standard Report

lame Amount Units RT Min Max Mean %SD

c'Oxygen 20.560 % 30.620 0.000 635.565 22.501 272.921 itrogen 77.016 % 39.900 0.000 856.321 73.948 156.452

"hannel: A Current Time: Feb 28, 2001 16:24:02 Ifethod: c:\mti\ezchrom\200\methods\raymark. Tile : c:\mti\ezchrom\200\chrom\16133.1

Gta file creation time: Feb 28, 2001 16:21:46 strument ID: 02402283 lumn Type: 10m MS5A

Jpirrier Gas: He Iplumn Head Pressure: 29.7 psi column Temperature: 65 C J*hst rument Gain: LOW Sample Time: 30 seconds

rInject Time: 50 milliseconds in Time: 100 seconds

ti itt c c r

1 Area Report

Pkno Start RT Stop Area Area% Flag 1 1 25.860 26.370 27.020 23577 0.002 BB 2 28.280 28.330 28.440 332 0.000 BV 13 37.910 38.920 55.560 1314179712 99.803 BV 4 55.560 57.640 60.520 2571163 0.195 VB 1External Standard Report



Channel: B Current Time: Feb 28, 2001 16:24:02 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16133.1 Data file creation time: Feb 28, 2001 16:21:46 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He.. Column Head Pressure: 16.7 psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

cf

A72

f f fc' 16134

c c c c c c 0 C C C

c c c

c ea Report

fcno Start RT Stop Area Area% Flag

f 1 28.380 30.620 37.340 177797344 21.299 BV 2 37.340 39.900 54.940 656971968 78.701 VB

»o rternal Standard Report

came Amount Units RT Min Max Mean %SD

rOxygen 20.482 % 30.620 0.000 635.565 22.491 272.387 j-Nitrogen 77.048 % 39.900 0.000 856.321 73.962 156.049

'hannel: A jaurrent Time: Feb 28, 2001 16:26:57 Ijethod: c:\mti\ezchrom\200\methods\raymark. Tile : c:\mti\ezchrom\200\chrom\16134.1 | ata file creation time: Feb 28, 2001 16:24:41 Instrument ID: 02402283 column Type: 10m MS5A farrier Gas: He l,olumn Head Pressure: 29.7 psi Column Temperature: 65 C Instrument Gain: LOW ample Time: 30 seconds Inject Time: 50 milliseconds

Clun Time: 100 seconds

C C

C C C C C

Area Report


1 37.960 38.970 44.570 1311633792 99.690 BB 2 55.450 57.690 60.570 3845572 0.292 BB 3 93.370 95.930 98.170 236742 0.018 BE





ff ccc c c cf cccccc c ccf

16135 73-A

I irea Report Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 175343856 21.067 BV 2 37.340 39.900 55.260 656988608 78.933 VB

kno


ttc 'Name Amount Units RT Min Max Mean %SD

Oxygen 20.191 % 30.620 0.000 635.565 22.481 271.873 'Nitrogen 77.051 % 39.900 0.000 856.321 73.977 155.648

Zhannel: A Current Time: Feb 28, 2001 16:30:13 Llethod: c:\mti\ezchrom\200\methods\raymark. r'ile : C:\mti\ezchrom\200\chrom\16135.1 r*)ata file creation time: Feb 28, 2001 16:27:57 Cnstrument ID: 02402283 Column Type: 10m MS5A Carrier Gas: He

lumn Head Pressure: 29.7 psi "Column Temperature: 65 C

Cnstrument Gain: LOW ample Time: 30 seconds Inject Time: 50 milliseconds

jplun Time: 100 seconds

t t t

t C

krea Report


1 37.940 38.950 55.270 1308669056 99.150 BV 2 55.270 57.510 60.550 9263672 0.702 VB 3 72.710 75.110 98.150 1956342 0.148 BE




Channel: B Current Time: Feb 28, 2001 16:30:14 Method: c:\mti\ezchrom\2 00\methods\raymark. File : c:\mti\ezchrom\200\chrom\16135.1 Data file creation time: Feb 28, 2001 16:27:57 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure:.. 16 . 7 psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

f i" f

16136 [ 74-A

cccc

ccccccccc

frea Report


f 1 28.380 30.620 37.340 177982928 21.332 BV 2 37.340 39.900 54.940 656374848 78.668 VB

f;ternal Standard Report

-$Iame Amount Units RT Min Max Mean %SD

ocygen 20.505 % 30.620 0.000 635.565 22.471 271.344 •Nitrogen 76.976 % 39.900 0 .000 856.321 73.991 155.251

Channel: A

G|>urrent Time: Feb 28, 2001 16:34:42 lethod: c:\mti\ezchrom\200\methods\raymark. Tile : c:\mti\ezchrom\200\chrom\16136.1

ta file creation time: Feb 28, 2001 16:32:26 strument ID: 02402283 lumn Type: 10m MS5A rrier Gas: He olumn Head Pressure: 29.7 psi iolumn Temperature: 65 C

ftistrument Gain: LOW I ample Time: 30 seconds

rinject Time: 50 milliseconds n Time: 100 seconds

c c r c c c c

Area Report


1 25.860 26.360 26.970 20996 0.002 BB 2 37.960 38.970 44.570 1310583552 99.780 BB 3 55.450 57.530 60^410 2865179 0.218 BB




Channel: B Current Time: Feb 28, 2001 16:34:42 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\16136.1 Data file creation time: Feb 28, 2001 16:32:26 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.. 7 psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

fII i*cc

cGCC

AMB0532P

fjrea Report

Ikno Start RT Stop Area Area% Flag

f 1 28.380 30.620 37.340 179729760 21.444 BV 2 37.340 39.900 55.260 658392704 78.556 VB

fjxternal Standard Report

[Name Amount Units RT Min Max Mean %SD I cOxygen 20.712 % 30.620 0.000 635.565 22.463 270.806 Nitrogen 77.221 % 39.900 0.000 856.321 74.006 154.855

lhannel: A Current Time: Feb 28, 2001 16:39:32 IJethod: c:\mti\ezchrom\200\methods\raymark.

CCb"ile : c:\mti\ezchrom\200\chrom\AMB0532P.l ata file creation time: Feb 28, 2001 16:37:16 nstrument ID: 02402283 column Type: 10m MS5A arrier Gas: He olumn Head Pressure: 29.7 psi Column Temperature: 65 C

JTtnstrument Gain: LOW I Sample Time: 30 seconds Inject Time: 50 milliseconds .un Time: 100 seconds

f

C C f f C C C f

Area Report

PJcno Start RT Stop Area Area% Flag

1 24.430 24.510 24.600 534 0.000 BV 2 37.930 38.940 55.580 1316336896 99.947 BV 3 55.580 57.500 60.060 703088 0.053 VB



Carbon Dioxide 401.775 ppm57.500 119487961610995194.0001031.363

Channel: B Current Time: Feb 28, 2001 16:39:33 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\AMB0532P.l Data file creation time: Feb 28, 2001 16:37:16 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7.psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

C CAL0537P

fff

fCCC

CCCCCfCCCf

ftea Report f Start RT Stop Area Area% Flag

1 23.490 23.850 23.980 23934 0.014 BV

f 2 3

23.980 29.020

24.200 31.260

24.390 39.260

28958 46291304

0.017 27.213

VB BV

4 39.260 42.140 51.420 57766080 33.959 VB

f 5 6

54.940 88.860

59.100 93.340

79.900 96.540

30568478 35426364

17.970 20.826

BB BE

f|:ternal Standard Report

f Amount Units RT Min Max Mean %SD

0xygen 4.886 % 31.260 0.000 635.565 22.381 271.212 itrogen 4.422 % 42.140 0.000 856.321 73.682 155.305

Cannel: A rrent Time: Feb 28, 2001 16:43:57 thod: c:\mti\ezchrom\200\methods\raytnark.

61e : c:\mti\ezchrom\200\chrom\CAL0537P.l ta file creation time: Feb.. 28, 2001 16:41:41 Strument ID: 02402283 >lumn Type: 10m MS5A irrier Gas: He !olumn Head Pressure: 29.7 psi fSlumn Temperature: 65 C I nstrument Gain: LOW sample Time: 30 seconds JThject Time: 50 milliseconds 1 un Time: 100 seconds

C C C C C C C

Area Report


1 37.910 39.830 42.390 248297280 64.176 BV 2 42.390 44.470 47.990 50400868 13.027 VB 3 54.710 56.950 61.270 88201416 22.797 BB



Carbon Dioxide51304.605 ppm 56.950 119487961610944292.0001033.758

Channel: B Current Time: Feb 28, 2001 16:43:58 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\CAL0537P.l Data file creation time: Feb 28, 2001 16:41:41 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 43 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

J

J

J 1

*' CAL0622P

f

ffff

f

f

ccccffffffcf

crea Report Aft*,

l"|kno Start RT Stop Area Area% Flag

_ 1 23.540 23.860 23.990 24311 0.015 BV

f 2 23.990 24.210 24.390 27559 0.017 VB I 3 29.020 31.260 39.260 44362760- 26.910 BV _ 4 39.260 42.140 49.500 53725536 32.589 VB

55.260 59.100 76.380 29861174 18.114 BB f 5 W 6 88.860 93.020 96.540 36854036 22.355 BE

Cxternal Standard Report CName Amount Units RT Min Max Mean %SD

COxygen 4.682 % 31.260 0.000 635.565 22.299 271.628 Nitrogen 4.113 % 42.140 0.000 856.321 73.360 155.757

n

•Channel: A iturrent Time: Feb 28, 2001 17:29:48 "Method: c:\mti\ezchrom\200\methods\raymark. r^ile : c:\mti\ezchrom\200\chrom\CAL0622P.l I Data file creation time: Feb 28., 2001 17:27:31 "Instrument ID: 02402283 olumn Type: 10m MS5A arrier Gas: Ar

*fcolumn Head Pressure: 29.7 psi f*olumn Temperature: 65 C I instrument Gain: LOW sample Time: 30 seconds nject Time: 50 milliseconds .un Time: 100 seconds CC c f f c c f

Area Report n

Pkno Start RT Stop Area Area% Flag /"I

1 37.910 39.830 42.390 236393920 63.466 BV 2 42.390 44.310 50.070 49410604 13.266 W 3 54.390 56.630 60.950 86667568 23.268 BB

External Standard Report "I

Name Amount Units RT Min Max Mean %SD j"l

Carbon Dioxide49525.559 ppm 56.630 119487961610893854.0001036.149

1Channel: B UP Current Time: Feb 28, 2001 17:29:48 Method: c:\mti\ezchrom\200\methods\raymark. j~l File : c:\mti\ezchrom\200\chrom\CAL0622P.l J Data file creation time: Feb 28, 2001 17:27:31 Instrument ID: 02402283 [jj Column Type: 8m PPQ '-* Carrier Gas: He Column Head Pressure: 16.8 psi ._ I I Column Temperature: 44 C Instrument Gain: LOW _ Sample Time: 30 seconds I Inject Time: 80 milliseconds Run Time: 100 seconds _

J

a 3 i 3 3 3 3

CAL0622P £ CALIBRATE

fcc

C Ccccccfcfffff

frea Report

jcno Start RT Stop Area Area% Flag

2f1

3 4 5

23.540 23.990 29.020 39.260 55.260

23.860 24.210 31.260 42.140 59.100

23.990 24.390 39.260 49.500 76.380

24311 27559

44362760 53725536 29861174

0.015 0.017 26.910 32.589 18.114

BV VB BV VB BB

ff6 88.860 93.020 96.540 36854036 22.355 BE


I Amount Units RT Min Max Mean %SD

i O 5.010 % 31.260 0.000 635.565 22.141 272.413 I ptfitrogen 4.990 % 42.140 0.000 856.321 72.733 156.633

annel: A rrent Time: Feb 28, 2001 17:30:23

iethod: c:\mti\ezchrom\200\methods\raymark. jnile : c:\mti\ezchrotn\200\chrom\CAL0622P.l Ljata file creation time: Feb 28, 2.001 17:28:07 instrument ID: 02402283 J^olumn Type: 10m MS5A I,arrier Gas: Ar vTolumn Head Pressure: 29.7 psi

Column Temperature: 65 C nstrument Gain: LOW

oample Time: 30 seconds Cnject Time: 50 milliseconds

un Time: 100 seconds

f

r c t c

c

irea Report t] 3kno Start RT Stop Area Area% Flag

1 37.910 39.830 42.390 236393920 63.466 BV 2 42.390 44.310 50.070 49410604 13.266 W 3 54.390 56.630 60.950 86667568 23.268 BB o

External Standard Report a Name Amount Units RT Min Max Mean %SD o Carbon Dioxide49600 .000 ppm 56.630 119487961610794365.0001040.913

Channel: B Current Time: Feb 28, 2001 17:30:24 Method: c:\mti\ezchrom\200\methods\rayrnark. File : c:\mti\ezchrom\200\chrom\CAL0622P.l 0 Data file creation time: Feb 28, 2001 17:28:07 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.8 psi Column Temperature: 44 C Instrument Gain: LOW Sample Time: 30 seconds aInject Time: 80 milliseconds Run Time: 100 seconds a

i

i f i

iI"Ltcc LB0 c0 nL 0 QQ

AMB0626P

jrea Report

c

[to, Start RT Stop Area Area% Flag

1 28.380 30.620 37.340 179003152 21.452 BV 2 37.340 39.900 52.380 655413184 78.548 VB

fternal Standard Report

ame Amount Units RT Min Max Mean %SD

Oxygen 20.633 % 30.620 0.000 635.565 22.134 271.872 itrogen 76.882 % 39.900 0.000 856.321 72.752 156.233

ihannel: A

Current Time: Feb 28, 2001 17:33:38 ethod: c:\mti\ezchrom\200\methods\raytnark. ile : c:\mti\ezchrom\200\chrom\amb0626P.l

j«ata file creation time: Feb 28, 2001 17:31:22 •Instrument ID: 02402283 "tolumn Type: 10m MS5A rSarrier Gas: Ar Ijlolumn Head Pressure: 29.7 psi nbolumn Temperature: 65 C Instrument Gain: LOW Isample Time: 30 seconds inject Time: 50 milliseconds rLun Time: 100 seconds c c c c c £ c 0

Area Report


1 37.930 38.940 55.420 1313228544 99.931 BV 2 55.420 57.340 59.100 769718 0.059 W 3 59.100 60.540 65.660 134742 0.010 VB



Carbon Dioxide 440.511 ppm57 .340 119487961610745078.0001043.309

Channel: B Current Time: Feb 28, 2001 17:33:39 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrotn\amb0626P.l Data file creation time: Feb 28, 2001 17:31:22 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 44 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

fff

Cctccccc£CC

AMB0626P CALIBRATE

t C

f*.rea Report


f 1 28.380 30.620 37.340 179003152 21.452 BV 2 37.340 39.900 52.380 655413184 78.548 VB

^External Standard Report

CName Amount Units RT Min Max Mean %SD

COxygen 20.950 % 30.620 0.000 635.565 22.123 270.765 Nitrogen 78.080 % 39.900 0.000 856.321 72.800 155.420

lhannel: A ^Current Time: Feb 28, 2001 17:34:26 I Method: c:\mti\ezchrom\200\methods\raymark. "File : c:\mti\ezchrom\200\chrom\amb0626P.l j»Data file creation time: Feb 28, 2001 17:31:58 I Instrument ID: 02402283 •tolumn Type: 10m MS5A r-Carrier Gas: Ar I fcolumn Head Pressure: 29.7 psi H

rC^Column Temperature: 65 C

nstrument Gain: LOW ample Time: 30 seconds

j.nject Time: 50 milliseconds .un Time: 100 seconds

c c c t c c c c

Area Report


1 37.930 38.940 55.420 1313228544 99.931 BV 2 55.420 57.340 59.100 769718 0.059 W 3 59.100 60.540 65.660 134742 0.010 VB




Channel: B Current Time: Feb 28, 2001 17:34:26 Method: c:\mti\ezchrom\200\methods\raymark. File : c:\mti\ezchrom\200\chrom\amb0626P.l Data file creation time: Feb 28, 2001 17:31:58 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 44 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

I f

t

fttttt

16115A 55-ADUP

f*

LL£C£CC LCC

Report

jkno Start RT Stop Area Area% Flag

% 1 28.380 30.620 37.340 175082112 21.090 BV : 2 37.340 39.900 52.380 655102272 78.910 VB


-.Name Amount Units RT Min Max Mean %SD

•""Oxygen 20.486 % 30.620 0.000 635.565 22.116 270.243 . Nitrogen 78.042 % 39.900 0.000 856.321 72.824 155.018

•Channel: A I Current Time: Feb 28, 2001 17:38:06 I flethod: c:\mti\ezchrom\200\methods\raymark. ""File : c:\mti\ezchrom\200\chrom\16115A.l |Oata file creation time: Feb 28, 2001 17:35:49 I Instrument ID: 02402283 "Column Type: 10m MS5A i-Carrier Gas: Ar I Column Head Pressure: 29.7 psi UL.Llolumn Temperature: 65 C |"Instrument Gain: LOW I Sample Time: 30 seconds

CInject Time: 50 milliseconds un Time: 100 seconds

c c c c c c c c

Area Report

Pkno Start RT Stop Area Area% Flag f| J

1 37.990 39.000 44.440 1305469312 99.454 BB 2 55.160 57.400 60.280 7165399 0.546 BB 3



Carbon' Dioxide 4100.771 ppm57.400 119487961610599896.0001050.461 J

Channel: BCurrent Time: Feb 28, 2001 17:38:06Method: c:\mti\ezchrom\2 00\rnethods\raymark. File : c:\mti\ezchrom\200\chrom\16115A.l Data file creation time: Feb 28, -2001 17:35:49 Instrument ID: 02402283 Column Type: 8m PPQ Carrier Gas: He Column Head Pressure: 16.7 psi Column Temperature: 44 C Instrument Gain: LOW Sample Time: 30 seconds Inject Time: 80 milliseconds Run Time: 100 seconds

T J

J 3

m200h mgc analytical report, volume 2 of …1 28.380 30.300 37.34 bv 0 179645376 21.257 i 2 37.340...

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