manhattan, new york remedial investigation … new york remedial investigation ... report sco soil...

2011-06-21 OER Remedial Investigation Report

372 LAFAYETTE STREET

(AKA 11 GREAT JONES STREET) MANHATTAN, NEW YORK

Remedial Investigation Report

NYC BCP Site Number: 13CVCP073M

Prepared for:

Great Jones Lafayette LLC

372 Lafayette Street

Manhattan, New York

Prepared by:

ESPL Environmental Consultants Corp

2 West 32nd Street

New York, NY 10006

May 2012


2

REMEDIAL INVESTIGATION REPORT

TABLE OF CONTENTS TABLE OF CONTENTS ........................................................................................................ 4

LIST OF ACRONYMS ........................................................................................................... 5

FIGURES ................................................................................................................................. 3

LIST OF ACRONYMS ........................................................................................................... 5

CERTIFICATION ................................................................................................................... 6

EXECUTIVE SUMMARY ..................................................................................................... 7

REMEDIAL INVESTIGATION REPORT .......................................................................... 11

1.0 SITE BACKGROUND ........................................................................................... 11

1.1 SITE LOCATION AND CURRENT USAGE ................................................... 11

1.2 Proposed Redevelopment Plan ............................................................................ 11

1.3 DESCRIPTION OF SURROUNDING PROPERTY ......................................... 12

2.0 SITE HISTORY ...................................................................................................... 13

2.1 PAST USES AND OWNERSHIP ...................................................................... 13

2.2 PREVIOUS INVESTIGATIONS ....................................................................... 13

2.3 SITE INSPECTION ............................................................................................ 14

2.4 AREAS OF CONCERN...................................................................................... 14

3.0 PROJECT MANAGEMENT .................................................................................. 15

3.1 PROJECT ORGANIZATION............................................................................. 15

3.2 HEALTH AND SAFETY ................................................................................... 15

3.3 MATERIALS MANAGEMENT ........................................................................ 15

4.0 REMEDIAL INVESTIGATION ACTIVITIES ..................................................... 15

4.1 GEOPHYSICAL INVESTIGATION ................................................................. 16

4.2 BORINGS AND MONITORING WELLS......................................................... 16

4.3 SAMPLE COLLECTION AND CHEMICAL ANALYSIS ............................... 17

5.0 ENVIRONMENTAL EVALUATION ................................................................... 21

5.1 GEOLOGICAL AND HYDROGEOLOGICAL CONDITIONS ........................... 21

5.2 SOIL CHEMISTRY ........................................................................................ 21

5.5 PRIOR ACTIVITY ............................................................................................. 23

5.6 IMPEDIMENTS TO REMEDIAL ACTION ..................................................... 23


3


TABLE OF CONTENTS

FIGURES

Figure 1 - Site Location Map

Figure 2 - Redevelopment Plan

Figure 3 – Surrounding Land Usage Map

Figure 4 - Map of Areas of Concern

Figure 5 - Location of Soil Borings, Wells, Soil Vapor Samples and Groundwater Flow Direction

Figure 6 - Soil Vapor Extraction Schematic

Figure 7 - Map of Soil Chemistry Results

Figure 8 - Map of Groundwater Chemistry Results

Figure 9 - Map of Soil Vapor Chemistry Results

TABLES

Table 1 - Construction Details for Soil Borings and Monitoring Wells

Table 2 - Groundwater Level Data

Table 3 - Analytical methods summary for all media

Table 4 – Groundwater Sampling Logs

Tables 5 - 8 - Soil Analytical Data Summary (showing exceedence of Track 2 SCOs)

Tables 9 - 12 - Groundwater Analytical Data Summary (showing exceedence of New York State

Groundwater Standards)

Table 13 - Soil Vapor Analytical Data Summary (showing exceedences of NYS DOH Soil Vapor

Intrusion Guidance)


4

APPENDICES

Appendix A - Phase 1 Report

Appendix B - Phase II Report

Appendix C - Remedial Investigation Work Plan and Health and Safety Plan

Appendix D - Soil Boring Geologic Logs

Appendix E - Laboratory Data Deliverables for Soil Analytical Data

Appendix F - Laboratory Data Deliverables for Groundwater Analytical Data

Appendix G - Laboratory Data Deliverables for Soil Vapor Analytical Data


5

LIST OF ACRONYMS

Acronym Definition

AOC Area of Concern

CAMP Community Air Monitoring Plan

COC Contaminant of Concern

CPP Citizen Participation Plan

CSM Conceptual Site Model

DER-10 New York State Department of Environmental Conservation Technical Guide 10

FID Flame Ionization Detector

GPS Global Positioning System

HASP Health and Safety Plan

HAZWOPER Hazardous Waste Operations and Emergency Response

IRM Interim Remedial Measure

NAPL Non-aqueous Phase Liquid

NYC BCP New York City Brownfield Cleanup Program

NYC DOHMH New York City Department of Health and Mental Hygiene

NYC OER New York City Office of Environmental Remediation

NYS DOH ELAP

New York State Department of Health Environmental Laboratory Accreditation Program

OSHA Occupational Safety and Health Administration

PID Photoionization Detector

QEP Qualified Environmental Professional

RI Remedial Investigation

RIR Remedial Investigation Report

SCO Soil Cleanup Objective

SPEED Searchable Property Environmental Electronic Database


6

CERTIFICATION

I, Ray Kahn, am a Qualified Environmental Professional, as defined in RCNY § 43-1402(ar). I have primary

direct responsibility for implementation of the Remedial Investigation for the 372 Lafayette Street (AKA 11 Great

Jones Street) Site, (NYC BCP Site No. 13CVCP073M). I am responsible for the content of this Remedial

Investigation Report (RIR), have reviewed its contents and certify that this RIR is accurate to the best of my

knowledge and contains all available environmental information and data regarding the property.

Ray Kahn 5/30/12

Qualified Environmental Professional Date Signature


7

EXECUTIVE SUMMARY

The Remedial Investigation Report (RIR) provides sufficient information for establishment

of remedial action objectives, evaluation of remedial action alternatives, and selection of a

remedy pursuant to RCNY§ 43-1407(f). The remedial investigation (RI) described in this

document is consistent with applicable guidance.

Site Location and Current Usage

The Site is located at 372 Lafayette Street in the NoHo section in Manhattan, New York

and is identified as Block 530 and Lot 13 on the New York City Tax Map. Figure 1 shows the

Site Location Map. The Site is 3,035-square feet and is bounded by Great Jones Street to the

north, by an automobile repair facility and gasoline station to the south, Lafayette Street to the

east, and by a multiple-story residential building with ground-floor retail to the west. A map of

the site boundary is shown in Figure 1. Currently, the Site is a vacant building that was used for

the repair and maintenance of automobiles by Meineke Car Care Center and contains a one story

building, approximately 25 feet by 100 feet.

Summary of Proposed Redevelopment Plan

The proposed future use of the Site will consist of a six-story residential building with the

first floor used for retail and a cellar used for retail, mechanical and storage. Layout of the

proposed site development is presented in Figure 2. The property is located in a Manufacturing

Zoning District (M1-5B), but a zoning variance was adopted by the Board of Standards and

Appeals on April 17, 2007, printed in Bulletin No. 16, Vol. 92 so that the proposed development

would be consistent with zoning for the property.

The existing one story building will be demolished and a six story building with cellar is to

be constructed with retail and 8 residential units. The cellar will be approximately 13.5 feet

below grade and the overall building height will be approximately 82 feet. The proposed cellar

will be used to house the building’s utilities, storage and retail space, the first floor will be used

for retail and residential use, and the 2nd through 6th floors will be used for residential space. The

proposed development will cover the entire footprint of the site. The proposed redevelopment


8

plans are included in Figure 2. The excavation of the site is required in order to create the cellar

area. The excavation is not anticipated to go below the water table, since the water table is

approximately 15-20 feet below grade.

Summary of Past Uses of Site and Areas of Concern

Based on the Phase I ESA, the Site was developed prior to 1895 for residential use with a

ground-level store. From at least 1921 to 1950, the southeastern portion of the Site was used as a

gasoline station with two associated 550-gallon buried gasoline tanks. The Site was

redeveloped with the existing 1-story commercial building circa 1969 for use as a car wash and

was also used for auto repair starting around 1991. The AOCs identified for this site include:

1. Partially Exposed UST Area – A UST (500-1,000 gallon assumed capacity) was

identified during geotechnical test pits and is currently partially exposed.

2. UST/Fill Port Area – Two areas of the subject site were identified as possible

UST areas. The Sanborn maps depicted a UST in the southwest corner of the site.

Due to the presence of three abandoned fill ports located on the sidewalk of Lafayette

Street, the Phase I also indicated a potential UST in the east side of the building.

3. Lift/Bay Area – Two bays facing the Lafayette Street utilized surface mounted

lifts for automobile repairs.

4. Floor Drain Area – A portion of the floor slab of the Great Jones side of the

building was covered with a steel plate. Apparently the plate was covering a pit that

was used for draining the bay area. The pit bottom was solid and there was no

obvious drain outlet.

5. Historic Fill – historic fill was identified to approximately 16 feet bgs.

Summary of the Work Performed under the Remedial Investigation

1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e.

structures, buildings, etc.);


9

2. Installed 3 soil borings across the project Site, utilized 1 existing geotechnical test pit,

and collected seven soil samples for chemical analysis from the soil borings to

evaluate soil quality;

3. Installed two groundwater monitoring wells throughout the Site and used one existing

monitoring well adjacent to the Site to establish groundwater flow and collected three

groundwater samples for chemical analysis to evaluate groundwater quality;

4. Installed three soil vapor probes throughout the Site and collected three samples for

chemical analysis.

Summary of Environmental Findings

1. Elevation of the property ranges from 40 to 41 feet.

2. Depth to groundwater ranges from 40 to 41 feet bgs at the Site.

3. Groundwater flow is generally from east to west beneath the Site.

4. Depth to bedrock is unknown at the Site.

5. The stratigraphy of the site, from the surface down, consists of 8 to 12 feet of

heterogeneous urban fill mixed with fine to course silty sand underlain by light brown

sand.

6. Soil/fill samples collected during the RI showed no VOCs, PCBs, or pesticides at

detectable concentrations. Four SVOCs were detected slightly above Unrestricted and

Restricted Residential SCOs in one sample collected from the geotechnical test pit near

the exposed UST. These SVOCs were all PAH compounds (benzo(a)anthracene,

benzo(a)pyrene, benzo(a)fluoranthene and chrysene) and their concentrations and

distributions indicate that they are associated with historic fill material observed in

shallow soil. Five metals exceeded UUSCOs in shallow soil samples, and of these metals,

copper (max of 798 ppm), mercury (max of 1 ppm), and lead (max of 781 ppm) also

exceeded their respective RRSCOs. No SVOCs or Metals were detected above UUSCOs

within the deeper soil samples collected below the historic fill material. Overall, the

findings were consistent with observations for other historical fill sites.


10

7. Groundwater samples collected during the RI showed no VOCs, SVOCs, PCBs, or

pesticides at detectable concentrations. Dissolved metals including manganese, sodium,

iron and lead (at 0.043 ppb) were identified above NYSDEC Part 703.5 Groundwater

Quality Standards (GQS). Metals findings in groundwater are indicative of regional

groundwater impacts, rather than migration of metals from on-Site historic fill material.

The RI indicates that groundwater is not impacted by site conditions and did not reveal

any sources of contaminants onsite.

8. Soil vapor samples collected during the RI showed petroleum and chlorinated VOCs at

generally low concentrations. PCE was identified in all samples at a maximum

concentration of 41.8 ug/m3, TCE was also identified in one sample at a concentration of

3.1 ug/m3. These results for TCE and PCE are below the monitoring level ranges of the

State DOH soil vapor guidance matrix. Neither PCE nor TCE were detected within any

of the soil or groundwater samples collected at the Site, and these low levels suggest an

offsite origin.


11


1.0 SITE BACKGROUND

Great Jones Lafayette LLC has enrolled in the New York City Voluntary Cleanup Program

(NYC VCP) to investigate and remediate a 0.069-acre site located at 372 Lafayette Street (AKA

11 Great Jones Street) in NoHo section of Manhattan, New York. Residential and retail use, is

proposed for the property. The RI work was performed between March 28, 2012 and April 4,

2012. This RIR summarizes the nature and extent of contamination and provides sufficient

information for establishment of remedial action objectives, evaluation of remedial action

alternatives, and selection of a remedy that is protective of human health and the environment

consistent with the use of the property pursuant to RCNY§ 43-1407(f).

1.1 SITE LOCATION AND CURRENT USAGE

The Site is located at 372 Lafayette Street in the NoHo section of Manhattan, New York

and is identified as Block 530 and Lot 13 on the New York City Tax Map. Figure 1 shows the

Site location. The Site is 3,035-square feet and is bounded by Great Jones Street to the north, an

automobile repair facility and gasoline station to the south, Lafayette Street to the east, and a

multiple-story residential building with ground-floor retail to the west. A map of the site

boundary is shown in Figure 1. Currently, the Site is a vacant building that was used for the

repair and maintenance of automobiles by Meineke Car Care Center and contains a one story

building, approximately 25 feet by 100 feet.

1.2 Proposed Redevelopment Plan

The proposed future use of the Site will consist of a six-story residential building with the

first floor used for retail and a cellar used for retail, mechanical and storage. Layout of the

proposed site development is presented in Figure 2. The property is located in a Manufacturing

Zoning District (M1-5B), but a zoning variance was adopted by the Board of Standards and

Appeals on April 17, 2007, printed in Bulletin No. 16, Vol. 92 so that the proposed development

would be consistent with zoning for the property.


12

The proposed structure complies with all requirements for setbacks, rear yard, and side yard.

The building will also have a full sprinkler system and comply with all requirements of the New

York City Fire Department (FDNY) and the New York City Department of Buildings

(NYCDOB). The proposed cellar will be used to house the building’s utilities, storage and retail

space. The usage of the floors is as follows:

FLOOR USAGE GROSS FA

Cellar Retail

Mechanical and Storage

1,805

1,191

1st Floor Retail

Residential Unit

2,221

684

2nd – 4th Floor Residential Units 2,920 per floor

5th Floor Residential Units 2,915

6th Floor Residential Units 1,503

The existing one story building will be demolished and a six story building with cellar is to be

constructed with retail and 8 residential units. The cellar will be approximately 13.5 feet below

grade and the overall building height will be approximately 82 feet. The proposed development

will cover the entire footprint of the site. The proposed redevelopment plans are included in

Figure 2. The excavation of the site is required in order to create the cellar area. The excavation

is not anticipated to go below the water table, since the water table is approximately 40-41 feet

below grade.

1.3 DESCRIPTION OF SURROUNDING PROPERTY

The surrounding properties are residential, retail and commercial use. The buildings range

from 1 to 6 stories in height and there are several parking garages and sites that are under

construction in the area. The zoning of the surrounding area is indicated as R7-2, C6-2 and M1-

5B. There are no schools, day care facilities or hospitals within a 500 foot radius. Figure 3

shows the surrounding land usage.


13

2.0 SITE HISTORY

2.1 PAST USES AND OWNERSHIP

Based on the Phase I ESA, the Site was developed prior to 1895 for residential use with a

ground-level store. From at least 1921 to 1950, the southeastern portion of the Site was used as a

gasoline station with two associated 550-gallon buried gasoline tanks. The Site was

redeveloped with the existing 1-story commercial building circa 1969for use as a car wash and

was also used for auto repair starting around 1991.

2.2 PREVIOUS INVESTIGATIONS

Previous investigations performed at the Site include the following:

Land America Commercial Services (LAC) prepared a Phase I ESA in accordance with the

American Society of Testing Materials (ASTM) Standard E 1527 for the subject site, dated

October 2005. During the site investigation three potential fill ports were observed in the

sidewalk on Lafayette Street. These fill ports were found to be concrete filled. The NYCDOB

records include a gasoline tank permit, dated 1933. Additionally, a large rectangular metal grate

was identified in the northern garage bay within the subject site. LAC was unable to lift the

grate, due to its weight, for inspection. 55-gallon waste oil drums were observed at the site but

no disposal records were made available for inspection. Heavy staining was encountered in the

bay areas and the waste oil storage areas. A Phase II LSI was recommended based on the

findings of the Phase I ESA.

A Phase II LSI was conducted by LAC on December 6, 2005. Ground penetrating radar

(GPR) survey was conducted at the subject site and no anomalies consistent with a UST were

identified. Four (4) soil borings were advanced to various depths. SB-1 was advanced, on the

sidewalk near the fill ports that were concrete filled, to a depth of 35 feet below ground surface

(bgs). No groundwater was encountered. Borings SB-2 through SB-4 were advanced inside of

the building. SB-2 was advance to a depth of 15 bgs, and SB-3 and SB-4 was advance to 10 bgs.

No groundwater was encountered. One sample from each boring was collected and analyzed for

volatile organic compounds (VOCs), USEPA Method 8260 and semi-volatile organic

compounds (SVOCs), USEPA Method 8270.


14

2.3 SITE INSPECTION

After reviewing the previously conducted Phase I and Phase II reports, a site inspection was

performed by Ray Kahn on March 15, 2012. It was noted that several test pits had been

excavated against the north, south, east and western side of the building to approximately 20 bgs.

The test pits were shored and secured for structural evaluation and geological inspection of the

sub-surface condition. The test pit on the central east side of the site discovered a 42” diameter

UST of unknown content buried approximately 3 bgs. The UST was partially exposed, therefore

the exact length is unknown, however, the tank is assumed to have a capacity of 500-1,000

gallons.

2.4 AREAS OF CONCERN

The AOCs identified for this site include:

1. Partially Exposed UST Area – A UST (500-1,000 gallon assumed capacity) was

identified during geotechnical test pits and is currently partially exposed.

2. UST/Fill Ports Area – Two areas of the subject site were identified as possible

UST areas. The Sanborn maps depicted a UST in the southwest corner of the site.

Due to the presence of three abandoned fill ports located on the sidewalk of Lafayette

Street, the Phase I also indicated a potential UST in the east side of the building.

3. Lift/Bay Area – Two bays facing the Lafayette Street utilized surface mounted

lifts for automobile repairs.

4. Floor Drain Area – A portion of the floor slab of the Great Jones side of the

building was covered with a steel plate. Apparently the plate was covering a pit that

was used for draining the bay area. The pit bottom was solid and there was no

obvious drain outlet.

5. Historic Fill – historic fill was identified to approximately 8 to 12 feet bgs.

Phase 1 Report is presented in Appendix A. A map showing areas of concern is presented in

Figure 2.


15

3.0 PROJECT MANAGEMENT

3.1 PROJECT ORGANIZATION

The Qualified Environmental Profession (QEP) responsible for preparation of this RIR is

Ray Kahn, P.E.

3.2 HEALTH AND SAFETY

All work described in this RIR was performed in full compliance with applicable laws and

regulations, including Site and OSHA worker safety requirements and HAZWOPER

requirements.

3.3 MATERIALS MANAGEMENT

All material encountered during the RI was managed in accordance with applicable laws and

regulations.

4.0 REMEDIAL INVESTIGATION ACTIVITIES

ESPL performed the following scope of work:

1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e.

structures, buildings, etc.);

2. Installed 3 soil borings across the project Site, utilized 1 existing geotechnical test pit,

and collected seven soil samples for chemical analysis from the soil borings to

evaluate soil quality;

3. Installed two groundwater monitoring wells throughout the Site and used one existing

monitoring well adjacent to the Site to establish groundwater flow and collected three

groundwater samples for chemical analysis to evaluate groundwater quality;


16

4. Installed three soil vapor probes throughout the Site and collected three samples for

chemical analysis.

4.1 GEOPHYSICAL INVESTIGATION

A geophysical survey was conducted by Goldstar Environmental Services, Inc. (Goldstar) of

Philipsburg, New Jersey on October 28, 2005, as requested by LAC during the Phase II Limited

Site Assessment. The survey was performed on the exterior of the building, in the sidewalk area.

The interior of the building was not surveyed due to interference and access issues. The GPR

survey report is included as part of the Phase II Limited Investigation, included in the Appendix

B of this Report.

4.2 BORINGS AND MONITORING WELLS

Drilling and Soil Logging

Soil borings were installed utilizing a Geoprobe® direct-push drill rig outfitted with a

macro-core sampler and dedicated acetate liners. Soils were collected continuously from ground

surface to 20 feet bgs. Soils were field-screened for the presence of VOCs using a PID and were

visually inspected for evidence of contamination. No elevated PID readings or visual/ olfactory

evidence of contamination were identified. Drilling equipment (i.e., split spoon samplers, rods,

etc.) and non-dedicated sampling equipment was thoroughly washed with Alconox and water,

using a brush to remove particulate matter or surface film, followed by a thorough rinsing with

tap water, followed by a distilled water rinse and allowed to air dry before commencement of

drilling activities and between boring locations and sampling intervals. Soil samples at each

boring location were collected in 4’ intervals from grade to final termination depth of each

boring. Boring logs were prepared by a geotechnical engineer and are attached in Appendix D.

A map showing the location of soil borings and monitor wells is shown in Figure 5.

Groundwater Monitoring Well Construction

Permanent 1-inch diameter monitoring wells with 5-feet of screens deployed from 42 to 47

feet bgs were installed at the locations shown as MW-1 and MW-2 in Figure 5, and the casings

extended from the screen to grade. Sand pack was installed in the annular space from about one


17

foot below the bottom of the monitoring well to approximately one to three feet above the top of

the well screen. The annulus was then filled with bentonite slurry. Concrete slurry mix was used

from the top of the bentonite seal to install the flush mounted locking steel casing. Monitor well

locations are shown in Figure 5.

Survey

All sampling location measurements were taken from the south and west interior walls of the

site.

Water Level Measurement

An oil/water interface probe, cotton string and disposable bailers were used to detect the

presence of any floating products as well as water level measurement in the well. The wells

were then purged using a peristaltic pump with dedicated polyethylene tubing. Three to five well

casing volumes of standing water were removed from each well until the turbidity was cleared

prior to sample collection. Water level data is included in Table 2.

4.3 SAMPLE COLLECTION AND CHEMICAL ANALYSIS

Sampling performed as part of the field investigation was conducted for all Areas of Concern

and also considered other means for bias of sampling based on professional judgment, area

history, discolored soil, stressed vegetation, drainage patterns, field instrument measurements,

odor, or other field indicators. All media including soil, groundwater and soil vapor have been

sampled and evaluated in the RIR. Discrete (grab) samples have been used for final delineation

of the nature and extent of contamination and to determine the impact of contaminants on public

health and the environment. The sampling performed and presented in this RIR provides

sufficient basis for evaluation of remedial action alternatives, establishment of a qualitative

human health exposure assessment, and selection of a final remedy.

Soil Sampling

The soil borings were advanced to a maximum depth of 18 fbg using a track mounted

Geoprobe® system. Soil samples were collected directly from four-foot macro-core samplers.


18

The visual inspection of the samples was immediately performed and field logs were prepared.

All samples were screened using handheld MiniRAE 2000 and the readings were logged.

Discrete grab soil samples from the sampling intervals 0-2 bgs and 16-18 bgs were collected.

Samples were placed into laboratory supplied sample bottles, labeled and stored on site in a

cooler. Two soil samples from each boring were submitted to a NYSDOH ELAP-certified

laboratory for analysis. In addition, sample USTB was also collected at 6.5 feet bgs from an open

geotechnical test pit. The soil samples were analyzed for the presence of Volatile Organic

Compounds (VOC) using EPA Method 8021/8260, Semi-volatile Organic Compounds (SVOC)

using EPA Method 8270, Metals using EPA Method 6010 and Polychlorinated Biphenyls

(PCBs) using EPA Method 8082. Soil analytical results were compared to NYSDEC’s

Unrestricted Use Soil Cleanup Objectives (SCOs) and Restricted Residential Use SCOs.

Seven soil samples were collected for chemical analysis during this RI. Data on soil sample

collection for chemical analyses, including dates of collection and sample depths, is reported in

Table 5 - 8. Figure 5 shows the location of samples collected in this investigation. Laboratories

and analytical methods are shown below.

Groundwater Sampling

ESPL collected three (3) groundwater samples from borings MW-1, MW-2, and MW-3 using

a peristaltic pump on April 4, 2012. Non-dedicated sampling equipment was decontaminated

prior to the collection of each sample. Following stabilization of the field parameters,

groundwater was carefully poured from the discharge tubing into laboratory-supplied sample

containers. Groundwater sample was labeled, and analyzed for the presence of VOC, SVOC,

TAL Metals PCBs, and Pesticides. The groundwater sample analytical results were compared to

the NYSDEC Class GA Groundwater Quality Standards, Technical and Operational Guidance

Series (TOGS) 1.1.1, Ambient Water Quality Standards and Guidance Values and Groundwater

Effluent Limitations, (NYSDEC, June 1998).

Three groundwater samples were collected for chemical analysis during this RI. Groundwater

sample collection data is reported in Table 9-12. Sampling logs with information on purging and

sampling of groundwater monitor wells is included in Table 4. Figure 5 shows the location of

groundwater sampling. Laboratories and analytical methods are shown below.


19

Soil Vapor Sampling

The soil vapor probes were advanced utilizing a track mounted Geoprobe® system to a depth

of 16 feet bgs. The soil vapor probe consisted of a 21” stainless steel wire screen implant fitted with

a ¼” diameter polyethylene tubing to the surface and was sealed at grade with a cement-bentonite

mixture. A helium enriched atmosphere was created in the immediate vicinity of the area where the

probe intersects the ground surface. The tracer gas (helium) was utilized during purging and

sampling collection activities to serve as a quality assurance/quality control measure to verify the

integrity of the soil vapor probe seal, and that adequate sampling technique are being implemented.

One to three volumes (i.e., the volume of the sample probe and tube) of air was purged from the

implant using a calibrated vacuum pump. After purging, a 6-liter Summa® canister, fitted with a 2-

hour flow regulator, was attached to the surface tube of each of the four vapor implants. Prior to

initiating sample collection, sample identification, canister number, date and start time were

recorded on tags attached to each canister and in a bound field note book. Sampling then proceeded

by fully opening the flow control valve on each canister in turn. Immediately after opening the flow

control valve on a canister, the initial vacuum (inches of mercury) was recorded in the field book

and on the sample tag. When the vacuum level in the canister was between 5 and 8 inches of

mercury (approx 2 hours), the flow controller valve was closed, and the final vacuum recorded in

the field notebook and on the sample tag.

The samples were analyzed using USEPA Method TO-15 for volatile organic chemical

compounds and helium. The minimum reporting limit will be 1 microgram per cubic meter

(1mcg/m³) or less.

Three soil vapor probes were installed and three soil vapor samples were collected for

chemical analysis during this RI. Soil vapor sampling locations are shown in Figure 5. Soil vapor

sample collection data is reported in Table 13. Soil vapor sampling logs are included in

Appendix H. Methodologies used for soil vapor assessment conform to the NYS DOH Final

Guidance on Soil Vapor Intrusion, October 2006.

Chemical Analysis

Chemical analytical work presented in this RIR has been performed in the following manner:


20

Factor Description

Quality Assurance Officer The chemical analytical quality assurance is directed by Margaret

Tavares

Chemical Analytical

Laboratory

Chemical analytical laboratory(s) used in the RI is NYS ELAP

certified and were Phoenix Environmental Laboratories, Inc.

Chemical Analytical

Methods

Soil analytical methods:

TAL Metals by EPA Method 6010C (rev. 2007);

VOCs by EPA Method 8260C (rev. 2006);

SVOCs by EPA Method 8270D (rev. 2007);

Pesticides by EPA Method 8081B (rev. 2000);

PCBs by EPA Method 8082A (rev. 2000);

Groundwater analytical methods:

TAL Metals by EPA Method 6010C (rev. 2007);

VOCs by EPA Method 8260C (rev. 2006);

SVOCs by EPA Method 8270D (rev. 2007);

Pesticides by EPA Method 8081B (rev. 2000);

PCBs by EPA Method 8082A (rev. 2000);

Soil vapor analytical methods:

VOCs by TO-15 VOC parameters..

Results of Chemical Analyses

Laboratory data for soil, groundwater and soil vapor are summarized in Table 5-13,

respectively. Laboratory data deliverables for all samples evaluated in this RIR are provided in

digital form in Appendix E, F, and G.


21

5.0 ENVIRONMENTAL EVALUATION

5.1 GEOLOGICAL AND HYDROGEOLOGICAL CONDITIONS

Stratigraphy

The lithologic description of the sediments from soil borings advanced during this

investigation at the site identifies heterogeneous urban fill across most of the site mixed with fine

to coarse silty sand with rock fragments to a depth of 16 bgs. From 16-20 bgs light brown sand

is encountered.

Hydrogeology

A table of water level data for all monitor wells is included in Table 2. The average depth to

groundwater is 40.7 feet bgs and the range in depth is 40.33 – 41.15 feet bgs. A map of

groundwater level elevations with groundwater contours and inferred flow lines is shown in

Figure 5. Groundwater flow is from east to west.

5.2 SOIL CHEMISTRY

Soil/fill samples collected during the RI showed no VOCs, PCBs, or pesticides at detectable

concentrations. Four SVOCs were detected above Unrestricted and Restricted Residential SCOs

in one sample collected from the geotechnical test pit near the exposed UST. These SVOCs

were all PAH compounds, (benzo(a)anthracene, benzo(a)pyrene, benzo(a)fluoranthene and

chrysene) and their concentrations and distributions indicate that they are associated with historic

fill material observed in shallow soil. Five metals exceeded UUSCOs in shallow soil samples,

and of these metals, copper (max of 798 ppm), mercury (max of 1 ppm), and lead (max of 781

ppm) also exceeded their respective RRSCOs. No SVOCs or Metals were detected above

UUSCOs within the deeper soil samples collected below the historic fill material. Overall, the

findings were consistent with observations for other historical fill sites.

Data collected during the RI is sufficient to delineate the vertical and horizontal distribution

of contaminants in soil/fill at the Site. A summary table of data for chemical analyses performed


22

on soil samples is included in Table 4. Figure 7 shows the location and posts the values for

soil/fill that exceed the 6NYCRR Part 375-6.8 Track 2 Soil Cleanup Objectives.

5.3 GROUNDWATER CHEMISTRY

Groundwater samples collected during the RI showed no VOCs, SVOCs, PCBs, or pesticides

at detectable concentrations. Dissolved metals including manganese, sodium, iron and lead (at

0.043 ppb) were identified above NYSDEC Part 703.5 Groundwater Quality Standards (GQS).

Metals findings in groundwater are indicative of regional groundwater impacts, rather than

migration of metals from on-Site historic fill material. The RI indicates that groundwater is not

impacted by site conditions and did not reveal any sources of contaminants onsite.

Data collected during the RI is sufficient to delineate the distribution of contaminants in

groundwater at the Site. A summary table of data for chemical analyses performed on

groundwater samples is included in Table 9-12 Exceedence of applicable groundwater standards

are shown. Figure 8 shows the location and posts the values for groundwater that exceed the

New York State 6NYCRR Part 703.5 Class GA groundwater standards.

5.4 SOIL VAPOR CHEMISTRY

Soil vapor samples collected during the RI showed petroleum and chlorinated VOCs at

generally low concentrations. PCE was identified in all samples at a maximum concentration of

41.8 ug/m3, TCE was also identified in one sample at a concentration of 3.1 ug/m3. These results

for TCE and PCE are below the monitoring level ranges of the State DOH soil vapor guidance

matrix. Neither PCE nor TCE were detected within any of the soil or groundwater samples

collected at the Site, and these low levels suggest an offsite origin.

Data collected during the RI is sufficient to delineate the distribution of contaminants in soil

vapor at the Site. A summary table of data for chemical analyses performed on soil vapor

samples is included in Table 6. Figure 9 shows the location and posts the values for soil vapor

samples with detected concentrations.


23

5.5 PRIOR ACTIVITY

Based on an evaluation of the data and information from the RIR, disposal of significant

amounts of hazardous waste is not suspected at this site.

5.6 IMPEDIMENTS TO REMEDIAL ACTION

There are no known impediments to remedial action at this property.

ESPL Env. Consltnts. Corp. BORING LOG 2 W 32nd Street, Suite 504, New York, NY 10001 *Tel: (212) 363 3775 Sheet No. 1 of 1

BH NO. SB-1 Sampling Area:

Date: _March 27, 2012 Start Time: ___4:00_PM_ ___Time Completion: __ 6:30 PM___

Project #: 212117-2

Location: 372 Lafayette Street, New York, NY

Coordinates / Ref. Points (Datum): Concrete Slab Finished Elevation

Drilling Contractor: : Syska Inc.

Drilling Method: _Geo-probe__ Borehole Dia.: 2”

Drilling Rig: N/A Drilling Fluid Used: N/A

Driver Hammer Weight: N/A Hammer Drop: N/A

Length and Diameter Coring Device: 4 ft, 2 Inch

Driller: Todd

Sampling Interval: 4’

Total Depth Drilled (ft) 18 h

Ground Elevation: l Ground Water Level

SAMPLE /DEPTH

(ft)

Core Recovery

(ft)

PID/Field Reading

(PPM)

Sample DESCRIPTION

Y N Time

(0-4) 24” Ø Y - 4:00 PM Light brown sand with broken concrete, Backfill material (soil Sample collected for laboratory analysis)

(4-8) 30” Ø - N -- Mixed light brown sand, brick, broken concrete & fill material (8-12) 26” Ø - N -- Light brown sand, brick broken concrete (12-16) 30” Ø - N -- Light brown sand & stone fragment & rock segment (16-20) 36” Ø Y N 4:55 PM Light brown sand(soil Sample collected for laboratory analysis) Total Samples Collected: Soil/Sediment/Rock and Groundwater: __ 2__S _--___Sediment _--____Rock _--___GW __2_ __Total

Remarks/Observations: Sketch

N (SB-1) Lafayette Street

The soil boring was advanced on the path of remote fill ports

identified in phase I report and and south east of the lift.

This soil boring was converted to the Monitoring well (MW-1)

after the soil sample was collected from the bottom of the boring

at 16-18 fbfg. Soil samples for lab analysis at 0-2 & 16-20 fbfg.

Prepared By: RK Date: 3/30/2012



Date: _March 27, 2012 Start Time: ___8:00_AM_ ___Time Completion: __ 12:45 PM____

Project #: 212117-2








Driller: Todd




SAMPLE /DEPTH

(ft)

Core Recovery

(ft)

PID/Field Reading

(PPM)

Sample DESCRIPTION

Y N Time

(0-4) 24” Ø Y - 11:10 AM Light brown sand with broken concrete, asphalt & Brick (soil Sample collected for laboratory analysis)

(4-8) 24” Ø - N --- Brown sand, broken concrete & brick (8-12) 30” Ø - N -- Light brown sand & stone (12-16) 42” Ø - N -- Light brown sand & brick & concrete (16-20) 48” Ø Y N 12:00 PM Light brown sand(soil Sample collected for laboratory analysis) Total Samples Collected: Soil/Sediment/Rock and Groundwater: __ 2__S _--___Sediment _--____Rock _--___GW __2_ __Total



This soil boring was advanced near the lift area and NW of the

UST identified during the test pit excavation prior to our

investigation.

This soil boring was converted to the Monitoring well (MW-2)

after the soil sample was collected from the bottom of the boring

at 16-18 fbfg. Soil samples for lab analysis at 0-2 & 16-20 fbfg.




Date: _March 28, 2012 Start Time: ___9:00_AM_ ___Time Completion: __ 11:30 AM____

Project #: 212117-2








Driller: Todd




SAMPLE /DEPTH

(ft)

Core Recovery

(ft)

PID/Field Reading

(PPM)

Sample DESCRIPTION

Y N Time

(0-4) 24” Ø Y - 10:00 AM Light broen sand with broken concrte, Backfill material (soil Sample collected for laboratory analysis)

(4-8) 30” Ø - N -- Mixed light brown sand, brick, broken concrete & fill material (8-12) 26” Ø - N -- Light brown sand, brick broken concrete (12-16) 30” Ø - N -- Light brown sand & stone fragment & rock segment (16-20) 36” Ø Y N 10:45 AM Light brown sand(soil Sample collected for laboratory analysis) Total Samples Collected: Soil/Sediment/Rock and Groundwater: __ 2__S _--___Sediment _--____Rock _--___GW __2_ __Total



This soil boring was advanced near the floor drain area, North of

The building and the lift .

Due to refusal, this soil boring was not converted to the

Monitoring.

Two (2) soil samples were collected from this boring at

0-2 & 16-20 fbfg.


BB59635 - BB59643

Friday, April 06, 2012

Sample ID#s:

Attn: Mr. Ray KahnESPL2 West 32nd StreetSuite 504New York, NY 10001

Project ID: 212117-2

This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.

This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory. All soils and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.

Sincerely yours,

Laboratory DirectorPhyllis Shiller

If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.

NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B

NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301

587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823

Sample Information Custody Information

Matrix:

Location Code:

Rush Request:

P.O.#:

Collected by:Received by:

Analyzed by:

SOIL

ESPL

Standard

2121172

03/27/12

LB

see "By" below

RK

Laboratory Data

SB-1 (0-2)

Phoenix ID: BB59635

03/29/12

16:00

14:52

Parameter Result RL Units Date By Reference

FOR: Attn: Mr. Ray KahnESPL2 West 32nd StreetSuite 504New York, NY 10001

Analysis ReportApril 06, 2012

Time

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBB59635

Client ID:


^

4470 Aluminum 49 03/31/12 LK 6010mg/Kg< 3.3 Antimony 3.3 03/30/12 LK 6010mg/Kg2.65 Arsenic 0.65 03/30/12 LK 6010mg/Kg84.2 Barium 0.33 03/30/12 LK 6010mg/Kg0.33 Beryllium 0.26 03/30/12 LK 6010mg/Kg12800 Calcium 49 03/31/12 LK 6010mg/Kg< 0.33 Cadmium 0.33 03/30/12 LK 6010mg/Kg11.2 Chromium 0.33 03/30/12 LK 6010mg/Kg3.86 Cobalt 0.33 03/30/12 LK 6010mg/Kg32.9 Copper 0.33 03/30/12 LK 6010mg/kg8290 Iron 49 03/31/12 LK 6010mg/Kg187 Lead 0.33 03/30/12 LK 6010mg/Kg3150 Magnesium 4.9 03/30/12 LK 6010mg/Kg169 Manganese 3.3 03/31/12 LK 6010mg/Kg0.55 Mercury 0.07 04/02/12 RS SW-7471mg/Kg11.1 Nickel 0.33 03/30/12 LK 6010mg/Kg1140 Potassium 4.9 03/30/12 LK 6010mg/Kg< 1.3 Selenium 1.3 03/30/12 LK 6010mg/Kg< 0.33 Silver 0.33 03/30/12 LK 6010mg/Kg481 Sodium 4.9 03/30/12 LK 6010mg/Kg< 2.9 Thallium 2.9 03/30/12 LK 6010mg/KgCompleted Total Metals Digest 03/29/12 T SW846 - 3050

15.9 Vanadium 0.33 03/30/12 LK 6010mg/Kg178 Zinc 3.3 03/31/12 LK 6010mg/Kg91 Percent Solid 03/29/12 JL E160.3%Completed Soil Extraction for PCB 03/29/12 RB/F SW3545

Completed Soil Extraction for SVOA 03/29/12 RB/R SW3545

Completed Mercury Digestion 04/02/12 X/X SW7471

Page 1 of 41 Ver 1

SB-1 (0-2)

Phoenix I.D.: BB59635

Parameter Result RL Units Date By ReferenceTime

Client ID:212117-2Project ID:

^

Polychlorinated BiphenylsND PCB-1016 360 04/02/12 MH SW 8082ug/KgND PCB-1221 360 04/02/12 MH SW 8082ug/KgND PCB-1232 360 04/02/12 MH SW 8082ug/KgND PCB-1242 360 04/02/12 MH SW 8082ug/KgND PCB-1248 360 04/02/12 MH SW 8082ug/KgND PCB-1254 360 04/02/12 MH SW 8082ug/KgND PCB-1260 360 04/02/12 MH SW 8082ug/KgND PCB-1262 360 04/02/12 MH SW 8082ug/KgND PCB-1268 360 04/02/12 MH SW 8082ug/Kg

QA/QC Surrogates84 % DCBP 04/02/12 MH 30 - 150 %%

70 % TCMX 04/02/12 MH 30 - 150 %%

VolatilesND 1,1,1,2-Tetrachloroethane 5.5 04/02/12 H/J SW8260ug/KgND 1,1,1-Trichloroethane 5.5 04/02/12 H/J SW8260ug/KgND 1,1,2,2-Tetrachloroethane 5.5 04/02/12 H/J SW8260ug/KgND 1,1,2-Trichloroethane 5.5 04/02/12 H/J SW8260ug/KgND 1,1-Dichloroethane 5.5 04/02/12 H/J SW8260ug/KgND 1,1-Dichloroethene 5.5 04/02/12 H/J SW8260ug/KgND 1,1-Dichloropropene 5.5 04/02/12 H/J SW8260ug/KgND 1,2,3-Trichlorobenzene 5.5 04/02/12 H/J SW8260ug/Kg 1

ND 1,2,3-Trichloropropane 5.5 04/02/12 H/J SW8260ug/KgND 1,2,4-Trichlorobenzene 5.5 04/02/12 H/J SW8260ug/KgND 1,2,4-Trimethylbenzene 5.5 04/02/12 H/J SW8260ug/KgND 1,2-Dibromo-3-chloropropane 5.5 04/02/12 H/J SW8260ug/KgND 1,2-Dichlorobenzene 5.5 04/02/12 H/J SW8260ug/KgND 1,2-Dichloroethane 5.5 04/02/12 H/J SW8260ug/KgND 1,2-Dichloropropane 5.5 04/02/12 H/J SW8260ug/KgND 1,3,5-Trimethylbenzene 5.5 04/02/12 H/J SW8260ug/KgND 1,3-Dichlorobenzene 5.5 04/02/12 H/J SW8260ug/KgND 1,3-Dichloropropane 5.5 04/02/12 H/J SW8260ug/KgND 1,4-Dichlorobenzene 5.5 04/02/12 H/J SW8260ug/KgND 2,2-Dichloropropane 5.5 04/02/12 H/J SW8260ug/KgND 2-Chlorotoluene 5.5 04/02/12 H/J SW8260ug/KgND 2-Hexanone 27 04/02/12 H/J SW8260ug/KgND 2-Isopropyltoluene 5.5 04/02/12 H/J SW8260ug/Kg 1

ND 4-Chlorotoluene 5.5 04/02/12 H/J SW8260ug/KgND 4-Methyl-2-pentanone 27 04/02/12 H/J SW8260ug/KgND Acetone 27 04/02/12 H/J SW8260ug/KgND Acrylonitrile 11 04/02/12 H/J SW8260ug/KgND Benzene 5.5 04/02/12 H/J SW8260ug/KgND Bromobenzene 5.5 04/02/12 H/J SW8260ug/KgND Bromochloromethane 5.5 04/02/12 H/J SW8260ug/KgND Bromodichloromethane 5.5 04/02/12 H/J SW8260ug/KgND Bromoform 5.5 04/02/12 H/J SW8260ug/KgND Bromomethane 5.5 04/02/12 H/J SW8260ug/KgND Carbon Disulfide 5.5 04/02/12 H/J SW8260ug/KgND Carbon tetrachloride 5.5 04/02/12 H/J SW8260ug/Kg

Page 2 of 41 Ver 1

SB-1 (0-2)




^

ND Chlorobenzene 5.5 04/02/12 H/J SW8260ug/KgND Chloroethane 5.5 04/02/12 H/J SW8260ug/KgND Chloroform 5.5 04/02/12 H/J SW8260ug/KgND Chloromethane 5.5 04/02/12 H/J SW8260ug/KgND cis-1,2-Dichloroethene 5.5 04/02/12 H/J SW8260ug/KgND cis-1,3-Dichloropropene 5.5 04/02/12 H/J SW8260ug/KgND Dibromochloromethane 5.5 04/02/12 H/J SW8260ug/KgND Dibromoethane 5.5 04/02/12 H/J SW8260ug/Kg 1,1O

ND Dibromomethane 5.5 04/02/12 H/J SW8260ug/KgND Dichlorodifluoromethane 5.5 04/02/12 H/J SW8260ug/KgND Ethylbenzene 5.5 04/02/12 H/J SW8260ug/KgND Hexachlorobutadiene 5.5 04/02/12 H/J SW8260ug/Kg 1,1P

ND Isopropylbenzene 5.5 04/02/12 H/J SW8260ug/KgND m&p-Xylene 5.5 04/02/12 H/J SW8260ug/KgND Methyl Ethyl Ketone 27 04/02/12 H/J SW8260ug/KgND Methyl t-butyl ether (MTBE) 11 04/02/12 H/J SW8260ug/KgND Methylene chloride 5.5 04/02/12 H/J SW8260ug/KgND Naphthalene 5.5 04/02/12 H/J SW8260ug/KgND n-Butylbenzene 5.5 04/02/12 H/J SW8260ug/KgND n-Propylbenzene 5.5 04/02/12 H/J SW8260ug/KgND o-Xylene 5.5 04/02/12 H/J SW8260ug/KgND p-Isopropyltoluene 5.5 04/02/12 H/J SW8260ug/KgND sec-Butylbenzene 5.5 04/02/12 H/J SW8260ug/KgND Styrene 5.5 04/02/12 H/J SW8260ug/KgND tert-Butylbenzene 5.5 04/02/12 H/J SW8260ug/KgND Tetrachloroethene 5.5 04/02/12 H/J SW8260ug/KgND Tetrahydrofuran (THF) 11 04/02/12 H/J SW8260ug/Kg 1

ND Toluene 5.5 04/02/12 H/J SW8260ug/KgND Total Xylenes 5.5 04/02/12 H/J SW8260ug/KgND trans-1,2-Dichloroethene 5.5 04/02/12 H/J SW8260ug/KgND trans-1,3-Dichloropropene 5.5 04/02/12 H/J SW8260ug/KgND trans-1,4-dichloro-2-butene 11 04/02/12 H/J SW8260ug/KgND Trichloroethene 5.5 04/02/12 H/J SW8260ug/KgND Trichlorofluoromethane 5.5 04/02/12 H/J SW8260ug/KgND Trichlorotrifluoroethane 5.5 04/02/12 H/J SW8260ug/KgND Vinyl chloride 5.5 04/02/12 H/J SW8260ug/Kg

QA/QC Surrogates97 % 1,2-dichlorobenzene-d4 04/02/12 H/J 70 - 130 %%

93 % Bromofluorobenzene 04/02/12 H/J 70 - 130 %%

101 % Dibromofluoromethane 04/02/12 H/J 70 - 130 %%

97 % Toluene-d8 04/02/12 H/J 70 - 130 %%

SemivolatilesND 1,2,4,5-Tetrachlorobenzene 250 03/30/12 DD SW 8270ug/KgND 1,2,4-Trichlorobenzene 250 03/30/12 DD SW 8270ug/KgND 1,2-Dichlorobenzene 250 03/30/12 DD SW 8270ug/KgND 1,3-Dichlorobenzene 250 03/30/12 DD SW 8270ug/KgND 1,4-Dichlorobenzene 250 03/30/12 DD SW 8270ug/KgND 2,4,5-Trichlorophenol 250 03/30/12 DD SW 8270ug/KgND 2,4,6-Trichlorophenol 250 03/30/12 DD SW 8270ug/KgND 2,4-Dichlorophenol 250 03/30/12 DD SW 8270ug/Kg

Page 3 of 41 Ver 1

SB-1 (0-2)




^

ND 2,4-Dimethylphenol 250 03/30/12 DD SW 8270ug/KgND 2,4-Dinitrophenol 570 03/30/12 DD SW 8270ug/KgND 2,4-Dinitrotoluene 250 03/30/12 DD SW 8270ug/KgND 2,6-Dinitrotoluene 250 03/30/12 DD SW 8270ug/KgND 2-Chloronaphthalene 250 03/30/12 DD SW 8270ug/KgND 2-Chlorophenol 250 03/30/12 DD SW 8270ug/KgND 2-Methylnaphthalene 250 03/30/12 DD SW 8270ug/KgND 2-Methylphenol (o-cresol) 250 03/30/12 DD SW 8270ug/KgND 2-Nitroaniline 570 03/30/12 DD SW 8270ug/KgND 2-Nitrophenol 250 03/30/12 DD SW 8270ug/KgND 3&4-Methylphenol (m&p-cresol) 360 03/30/12 DD SW 8270ug/KgND 3,3'-Dichlorobenzidine 250 03/30/12 DD SW 8270ug/KgND 3-Nitroaniline 570 03/30/12 DD SW 8270ug/KgND 4,6-Dinitro-2-methylphenol 1000 03/30/12 DD SW 8270ug/KgND 4-Bromophenyl phenyl ether 360 03/30/12 DD SW 8270ug/KgND 4-Chloro-3-methylphenol 250 03/30/12 DD SW 8270ug/KgND 4-Chloroaniline 250 03/30/12 DD SW 8270ug/KgND 4-Chlorophenyl phenyl ether 250 03/30/12 DD SW 8270ug/KgND 4-Nitroaniline 570 03/30/12 DD SW 8270ug/KgND 4-Nitrophenol 1000 03/30/12 DD SW 8270ug/KgND Acenaphthene 250 03/30/12 DD SW 8270ug/KgND Acenaphthylene 250 03/30/12 DD SW 8270ug/KgND Acetophenone 250 03/30/12 DD SW 8270ug/KgND Aniline 1000 03/30/12 DD SW 8270ug/Kg 1,1O

ND Anthracene 250 03/30/12 DD SW 8270ug/KgND Azobenzene 360 03/30/12 DD SW 8270ug/Kg 1

580 Benz(a)anthracene 250 03/30/12 DD SW 8270ug/KgND Benzidine 430 03/30/12 DD SW 8270ug/Kg520 Benzo(a)pyrene 250 03/30/12 DD SW 8270ug/Kg780 Benzo(b)fluoranthene 250 03/30/12 DD SW 8270ug/KgND Benzo(ghi)perylene 250 03/30/12 DD SW 8270ug/Kg250 Benzo(k)fluoranthene 250 03/30/12 DD SW 8270ug/KgND Benzoic acid 1000 03/30/12 DD SW 8270ug/Kg 1,1O

ND Benzyl butyl phthalate 250 03/30/12 DD SW 8270ug/KgND Bis(2-chloroethoxy)methane 250 03/30/12 DD SW 8270ug/KgND Bis(2-chloroethyl)ether 360 03/30/12 DD SW 8270ug/KgND Bis(2-chloroisopropyl)ether 250 03/30/12 DD SW 8270ug/KgND Bis(2-ethylhexyl)phthalate 250 03/30/12 DD SW 8270ug/KgND Carbazole 530 03/30/12 DD SW 8270ug/Kg540 Chrysene 250 03/30/12 DD SW 8270ug/KgND Dibenz(a,h)anthracene 250 03/30/12 DD SW 8270ug/KgND Dibenzofuran 250 03/30/12 DD SW 8270ug/KgND Diethyl phthalate 250 03/30/12 DD SW 8270ug/KgND Dimethylphthalate 250 03/30/12 DD SW 8270ug/KgND Di-n-butylphthalate 250 03/30/12 DD SW 8270ug/KgND Di-n-octylphthalate 250 03/30/12 DD SW 8270ug/Kg1100 Fluoranthene 250 03/30/12 DD SW 8270ug/KgND Fluorene 250 03/30/12 DD SW 8270ug/KgND Hexachlorobenzene 250 03/30/12 DD SW 8270ug/KgND Hexachlorobutadiene 250 03/30/12 DD SW 8270ug/Kg

Page 4 of 41 Ver 1

SB-1 (0-2)




^

ND Hexachlorocyclopentadiene 250 03/30/12 DD SW 8270ug/KgND Hexachloroethane 250 03/30/12 DD SW 8270ug/KgND Indeno(1,2,3-cd)pyrene 250 03/30/12 DD SW 8270ug/KgND Isophorone 250 03/30/12 DD SW 8270ug/KgND Naphthalene 250 03/30/12 DD SW 8270ug/KgND Nitrobenzene 250 03/30/12 DD SW 8270ug/KgND N-Nitrosodimethylamine 360 03/30/12 DD SW 8270ug/KgND N-Nitrosodi-n-propylamine 250 03/30/12 DD SW 8270ug/KgND N-Nitrosodiphenylamine 360 03/30/12 DD SW 8270ug/KgND Pentachloronitrobenzene 360 03/30/12 DD SW 8270ug/KgND Pentachlorophenol 360 03/30/12 DD SW 8270ug/Kg790 Phenanthrene 250 03/30/12 DD SW 8270ug/KgND Phenol 250 03/30/12 DD SW 8270ug/Kg990 Pyrene 250 03/30/12 DD SW 8270ug/KgND Pyridine 360 03/30/12 DD SW 8270ug/Kg

QA/QC Surrogates74 % 2,4,6-Tribromophenol 03/30/12 DD 15 - 130 %%

81 % 2-Fluorobiphenyl 03/30/12 DD 15 - 130 %%

80 % 2-Fluorophenol 03/30/12 DD 15 - 130 %%

89 % Nitrobenzene-d5 03/30/12 DD 15 - 130 %%

82 % Phenol-d5 03/30/12 DD 15 - 130 %%

94 % Terphenyl-d14 03/30/12 DD 15 - 130 %%

Comments:

Phyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

April 06, 2012

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.1P = This parameter is pending certification by NY NELAC for this matrix.1O = This parameter is not certified by NY NELAC for this matrix.

This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Phyllis Shiller, Laboratory Directory

Units^ = All soils and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

ND=Not detected BDL=Below Detection Level RL=Reporting Level is equivalent to NELAC LOQ (Limit of quanitation)

Page 5 of 41 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

SOIL

ESPL

Standard

2121172

03/27/12

LB

see "By" below

RK

Laboratory Data

SB-1 (16-18)

Phoenix ID: BB59636

03/29/12

16:55

14:52




Time

Date Time



SDG ID: GBB59635

Client ID:


^

5160 Aluminum 54 03/31/12 LK 6010mg/Kg< 3.6 Antimony 3.6 03/30/12 LK 6010mg/Kg< 0.72 Arsenic 0.72 03/30/12 LK 6010mg/Kg73.1 Barium 0.36 03/30/12 LK 6010mg/Kg0.32 Beryllium 0.29 03/30/12 LK 6010mg/Kg2650 Calcium 5.4 03/30/12 LK 6010mg/Kg< 0.36 Cadmium 0.36 03/30/12 LK 6010mg/Kg11.3 Chromium 0.36 03/30/12 LK 6010mg/Kg3.38 Cobalt 0.36 03/30/12 LK 6010mg/Kg10.3 Copper 0.36 03/30/12 LK 6010mg/kg8620 Iron 5.4 03/30/12 LK 6010mg/Kg50.3 Lead 0.36 03/30/12 LK 6010mg/Kg1730 Magnesium 5.4 03/30/12 LK 6010mg/Kg175 Manganese 0.36 03/30/12 LK 6010mg/Kg< 0.06 Mercury 0.06 04/02/12 RS SW-7471mg/Kg11.3 Nickel 0.36 03/30/12 LK 6010mg/Kg761 Potassium 5.4 03/30/12 LK 6010mg/Kg< 1.4 Selenium 1.4 03/30/12 LK 6010mg/Kg< 0.36 Silver 0.36 03/30/12 LK 6010mg/Kg96.0 Sodium 5.4 03/30/12 LK 6010mg/Kg< 3.2 Thallium 3.2 03/30/12 LK 6010mg/KgCompleted Total Metals Digest 03/29/12 T SW846 - 3050

14.9 Vanadium 0.36 03/30/12 LK 6010mg/Kg56.8 Zinc 0.36 03/30/12 LK 6010mg/Kg95 Percent Solid 03/29/12 JL E160.3%Completed Soil Extraction for PCB 03/29/12 RB/F SW3545



Page 6 of 41 Ver 1

SB-1 (16-18)




^



86 % TCMX 03/30/12 MH 30 - 150 %%




Page 7 of 41 Ver 1

SB-1 (16-18)




^








96 % Toluene-d8 03/31/12 H/J 70 - 130 %%


Page 8 of 41 Ver 1

SB-1 (16-18)




^



ND Benz(a)anthracene 240 03/30/12 DD SW 8270ug/KgND Benzidine 420 03/30/12 DD SW 8270ug/KgND Benzo(a)pyrene 240 03/30/12 DD SW 8270ug/KgND Benzo(b)fluoranthene 240 03/30/12 DD SW 8270ug/KgND Benzo(ghi)perylene 240 03/30/12 DD SW 8270ug/KgND Benzo(k)fluoranthene 240 03/30/12 DD SW 8270ug/KgND Benzoic acid 1000 03/30/12 DD SW 8270ug/Kg 1,1O

ND Benzyl butyl phthalate 240 03/30/12 DD SW 8270ug/KgND Bis(2-chloroethoxy)methane 240 03/30/12 DD SW 8270ug/KgND Bis(2-chloroethyl)ether 350 03/30/12 DD SW 8270ug/KgND Bis(2-chloroisopropyl)ether 240 03/30/12 DD SW 8270ug/KgND Bis(2-ethylhexyl)phthalate 240 03/30/12 DD SW 8270ug/KgND Carbazole 520 03/30/12 DD SW 8270ug/KgND Chrysene 240 03/30/12 DD SW 8270ug/KgND Dibenz(a,h)anthracene 240 03/30/12 DD SW 8270ug/KgND Dibenzofuran 240 03/30/12 DD SW 8270ug/KgND Diethyl phthalate 240 03/30/12 DD SW 8270ug/KgND Dimethylphthalate 240 03/30/12 DD SW 8270ug/KgND Di-n-butylphthalate 240 03/30/12 DD SW 8270ug/KgND Di-n-octylphthalate 240 03/30/12 DD SW 8270ug/KgND Fluoranthene 240 03/30/12 DD SW 8270ug/KgND Fluorene 240 03/30/12 DD SW 8270ug/KgND Hexachlorobenzene 240 03/30/12 DD SW 8270ug/KgND Hexachlorobutadiene 240 03/30/12 DD SW 8270ug/Kg

Page 9 of 41 Ver 1

SB-1 (16-18)




^

ND Hexachlorocyclopentadiene 240 03/30/12 DD SW 8270ug/KgND Hexachloroethane 240 03/30/12 DD SW 8270ug/KgND Indeno(1,2,3-cd)pyrene 240 03/30/12 DD SW 8270ug/KgND Isophorone 240 03/30/12 DD SW 8270ug/KgND Naphthalene 240 03/30/12 DD SW 8270ug/KgND Nitrobenzene 240 03/30/12 DD SW 8270ug/KgND N-Nitrosodimethylamine 350 03/30/12 DD SW 8270ug/KgND N-Nitrosodi-n-propylamine 240 03/30/12 DD SW 8270ug/KgND N-Nitrosodiphenylamine 350 03/30/12 DD SW 8270ug/KgND Pentachloronitrobenzene 350 03/30/12 DD SW 8270ug/KgND Pentachlorophenol 350 03/30/12 DD SW 8270ug/KgND Phenanthrene 240 03/30/12 DD SW 8270ug/KgND Phenol 240 03/30/12 DD SW 8270ug/KgND Pyrene 240 03/30/12 DD SW 8270ug/KgND Pyridine 350 03/30/12 DD SW 8270ug/Kg



79 % 2-Fluorophenol 03/30/12 DD 15 - 130 %%


79 % Phenol-d5 03/30/12 DD 15 - 130 %%

101 % Terphenyl-d14 03/30/12 DD 15 - 130 %%

Comments:



April 06, 2012






Page 10 of 41 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

SOIL

ESPL

Standard

2121172

03/27/12

LB

see "By" below

RK

Laboratory Data

SB-2 (0-2)

Phoenix ID: BB59637

03/29/12

11:10

14:52




Time

Date Time



SDG ID: GBB59635

Client ID:


^

3010 Aluminum 52 03/31/12 LK 6010mg/Kg< 3.4 Antimony 3.4 03/30/12 LK 6010mg/Kg7.69 Arsenic 0.69 03/30/12 LK 6010mg/Kg108 Barium 0.34 03/30/12 LK 6010mg/Kg< 0.28 Beryllium 0.28 03/30/12 LK 6010mg/Kg15500 Calcium 52 03/31/12 LK 6010mg/Kg0.98 Cadmium 0.34 03/30/12 LK 6010mg/Kg12.5 Chromium 0.34 03/30/12 LK 6010mg/Kg4.65 Cobalt 0.34 03/30/12 LK 6010mg/Kg76.7 Copper 0.34 03/30/12 LK 6010mg/kg15000 Iron 52 03/31/12 LK 6010mg/Kg489 Lead 3.4 03/31/12 LK 6010mg/Kg1460 Magnesium 5.2 03/30/12 LK 6010mg/Kg187 Manganese 0.34 03/30/12 LK 6010mg/Kg0.71 Mercury 0.08 04/02/12 RS SW-7471mg/Kg15.4 Nickel 0.34 03/30/12 LK 6010mg/Kg650 Potassium 5.2 03/30/12 LK 6010mg/Kg< 1.4 Selenium 1.4 03/30/12 LK 6010mg/Kg< 1 Silver 1 03/31/12 LK 6010mg/Kg196 Sodium 5.2 03/30/12 LK 6010mg/Kg< 3.1 Thallium 3.1 03/30/12 LK 6010mg/KgCompleted Total Metals Digest 03/29/12 T SW846 - 3050




Page 11 of 41 Ver 1

SB-2 (0-2)




^



74 % TCMX 03/30/12 MH 30 - 150 %%

VolatilesND 1,1,1,2-Tetrachloroethane 27 04/02/12 H/J SW8260ug/KgND 1,1,1-Trichloroethane 27 04/02/12 H/J SW8260ug/KgND 1,1,2,2-Tetrachloroethane 27 04/02/12 H/J SW8260ug/KgND 1,1,2-Trichloroethane 27 04/02/12 H/J SW8260ug/KgND 1,1-Dichloroethane 27 04/02/12 H/J SW8260ug/KgND 1,1-Dichloroethene 27 04/02/12 H/J SW8260ug/KgND 1,1-Dichloropropene 27 04/02/12 H/J SW8260ug/KgND 1,2,3-Trichlorobenzene 27 04/02/12 H/J SW8260ug/Kg 1

ND 1,2,3-Trichloropropane 27 04/02/12 H/J SW8260ug/KgND 1,2,4-Trichlorobenzene 27 04/02/12 H/J SW8260ug/KgND 1,2,4-Trimethylbenzene 27 04/02/12 H/J SW8260ug/KgND 1,2-Dibromo-3-chloropropane 27 04/02/12 H/J SW8260ug/KgND 1,2-Dichlorobenzene 27 04/02/12 H/J SW8260ug/KgND 1,2-Dichloroethane 27 04/02/12 H/J SW8260ug/KgND 1,2-Dichloropropane 27 04/02/12 H/J SW8260ug/KgND 1,3,5-Trimethylbenzene 27 04/02/12 H/J SW8260ug/KgND 1,3-Dichlorobenzene 27 04/02/12 H/J SW8260ug/KgND 1,3-Dichloropropane 27 04/02/12 H/J SW8260ug/KgND 1,4-Dichlorobenzene 27 04/02/12 H/J SW8260ug/KgND 2,2-Dichloropropane 27 04/02/12 H/J SW8260ug/KgND 2-Chlorotoluene 27 04/02/12 H/J SW8260ug/KgND 2-Hexanone 140 04/02/12 H/J SW8260ug/KgND 2-Isopropyltoluene 27 04/02/12 H/J SW8260ug/Kg 1

ND 4-Chlorotoluene 27 04/02/12 H/J SW8260ug/KgND 4-Methyl-2-pentanone 140 04/02/12 H/J SW8260ug/KgND Acetone 140 04/02/12 H/J SW8260ug/KgND Acrylonitrile 54 04/02/12 H/J SW8260ug/KgND Benzene 27 04/02/12 H/J SW8260ug/KgND Bromobenzene 27 04/02/12 H/J SW8260ug/KgND Bromochloromethane 27 04/02/12 H/J SW8260ug/KgND Bromodichloromethane 27 04/02/12 H/J SW8260ug/KgND Bromoform 27 04/02/12 H/J SW8260ug/KgND Bromomethane 27 04/02/12 H/J SW8260ug/KgND Carbon Disulfide 27 04/02/12 H/J SW8260ug/KgND Carbon tetrachloride 27 04/02/12 H/J SW8260ug/Kg

Page 12 of 41 Ver 1

SB-2 (0-2)




^

ND Chlorobenzene 27 04/02/12 H/J SW8260ug/KgND Chloroethane 27 04/02/12 H/J SW8260ug/KgND Chloroform 27 04/02/12 H/J SW8260ug/KgND Chloromethane 27 04/02/12 H/J SW8260ug/KgND cis-1,2-Dichloroethene 27 04/02/12 H/J SW8260ug/KgND cis-1,3-Dichloropropene 27 04/02/12 H/J SW8260ug/KgND Dibromochloromethane 27 04/02/12 H/J SW8260ug/KgND Dibromoethane 27 04/02/12 H/J SW8260ug/Kg 1,1O

ND Dibromomethane 27 04/02/12 H/J SW8260ug/KgND Dichlorodifluoromethane 27 04/02/12 H/J SW8260ug/KgND Ethylbenzene 27 04/02/12 H/J SW8260ug/KgND Hexachlorobutadiene 27 04/02/12 H/J SW8260ug/Kg 1,1P

ND Isopropylbenzene 27 04/02/12 H/J SW8260ug/KgND m&p-Xylene 27 04/02/12 H/J SW8260ug/KgND Methyl Ethyl Ketone 140 04/02/12 H/J SW8260ug/KgND Methyl t-butyl ether (MTBE) 54 04/02/12 H/J SW8260ug/KgND Methylene chloride 27 04/02/12 H/J SW8260ug/KgND Naphthalene 27 04/02/12 H/J SW8260ug/KgND n-Butylbenzene 27 04/02/12 H/J SW8260ug/KgND n-Propylbenzene 27 04/02/12 H/J SW8260ug/KgND o-Xylene 27 04/02/12 H/J SW8260ug/KgND p-Isopropyltoluene 27 04/02/12 H/J SW8260ug/KgND sec-Butylbenzene 27 04/02/12 H/J SW8260ug/KgND Styrene 27 04/02/12 H/J SW8260ug/KgND tert-Butylbenzene 27 04/02/12 H/J SW8260ug/KgND Tetrachloroethene 27 04/02/12 H/J SW8260ug/KgND Tetrahydrofuran (THF) 54 04/02/12 H/J SW8260ug/Kg 1

ND Toluene 27 04/02/12 H/J SW8260ug/KgND Total Xylenes 27 04/02/12 H/J SW8260ug/KgND trans-1,2-Dichloroethene 27 04/02/12 H/J SW8260ug/KgND trans-1,3-Dichloropropene 27 04/02/12 H/J SW8260ug/KgND trans-1,4-dichloro-2-butene 54 04/02/12 H/J SW8260ug/KgND Trichloroethene 27 04/02/12 H/J SW8260ug/KgND Trichlorofluoromethane 27 04/02/12 H/J SW8260ug/KgND Trichlorotrifluoroethane 27 04/02/12 H/J SW8260ug/KgND Vinyl chloride 27 04/02/12 H/J SW8260ug/Kg



21 % Dibromofluoromethane 04/02/12 H/J 70 - 130 %% 3

93 % Toluene-d8 04/02/12 H/J 70 - 130 %%


Page 13 of 41 Ver 1

SB-2 (0-2)




^



450 Benz(a)anthracene 250 03/30/12 DD SW 8270ug/KgND Benzidine 420 03/30/12 DD SW 8270ug/Kg480 Benzo(a)pyrene 250 03/30/12 DD SW 8270ug/Kg680 Benzo(b)fluoranthene 250 03/30/12 DD SW 8270ug/Kg270 Benzo(ghi)perylene 250 03/30/12 DD SW 8270ug/KgND Benzo(k)fluoranthene 250 03/30/12 DD SW 8270ug/KgND Benzoic acid 1000 03/30/12 DD SW 8270ug/Kg 1,1O


Page 14 of 41 Ver 1

SB-2 (0-2)




^

ND Hexachlorocyclopentadiene 250 03/30/12 DD SW 8270ug/KgND Hexachloroethane 250 03/30/12 DD SW 8270ug/KgND Indeno(1,2,3-cd)pyrene 250 03/30/12 DD SW 8270ug/KgND Isophorone 250 03/30/12 DD SW 8270ug/KgND Naphthalene 250 03/30/12 DD SW 8270ug/KgND Nitrobenzene 250 03/30/12 DD SW 8270ug/KgND N-Nitrosodimethylamine 350 03/30/12 DD SW 8270ug/KgND N-Nitrosodi-n-propylamine 250 03/30/12 DD SW 8270ug/KgND N-Nitrosodiphenylamine 350 03/30/12 DD SW 8270ug/KgND Pentachloronitrobenzene 350 03/30/12 DD SW 8270ug/KgND Pentachlorophenol 350 03/30/12 DD SW 8270ug/KgND Phenanthrene 250 03/30/12 DD SW 8270ug/KgND Phenol 250 03/30/12 DD SW 8270ug/Kg720 Pyrene 250 03/30/12 DD SW 8270ug/KgND Pyridine 350 03/30/12 DD SW 8270ug/Kg



74 % 2-Fluorophenol 03/30/12 DD 15 - 130 %%


76 % Phenol-d5 03/30/12 DD 15 - 130 %%

94 % Terphenyl-d14 03/30/12 DD 15 - 130 %%

Comments:Poor surrogate recovery was observed for volatiles due to matrix interference.



April 06, 2012

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.1P = This parameter is pending certification by NY NELAC for this matrix.1O = This parameter is not certified by NY NELAC for this matrix.3 = This parameter exceeds laboratory specified limits.





Page 15 of 41 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

SOIL

ESPL

Standard

2121172

03/27/12

LB

see "By" below

RK

Laboratory Data

SB-2 (16-18)

Phoenix ID: BB59638

03/29/12

12:00

14:52




Time

Date Time



SDG ID: GBB59635

Client ID:


^

3880 Aluminum 50 03/31/12 LK 6010mg/Kg< 3.3 Antimony 3.3 03/30/12 LK 6010mg/Kg< 0.67 Arsenic 0.67 03/30/12 LK 6010mg/Kg24.0 Barium 0.33 03/30/12 LK 6010mg/Kg< 0.27 Beryllium 0.27 03/30/12 LK 6010mg/Kg701 Calcium 5.0 03/30/12 LK 6010mg/Kg< 0.33 Cadmium 0.33 03/30/12 LK 6010mg/Kg6.62 Chromium 0.33 03/30/12 LK 6010mg/Kg3.07 Cobalt 0.33 03/30/12 LK 6010mg/Kg7.23 Copper 0.33 03/30/12 LK 6010mg/kg8360 Iron 5.0 03/30/12 LK 6010mg/Kg4.65 Lead 0.33 03/30/12 LK 6010mg/Kg1700 Magnesium 5.0 03/30/12 LK 6010mg/Kg157 Manganese 0.33 03/30/12 LK 6010mg/Kg< 0.06 Mercury 0.06 04/02/12 RS SW-7471mg/Kg7.62 Nickel 0.33 03/30/12 LK 6010mg/Kg588 Potassium 5.0 03/30/12 LK 6010mg/Kg< 1.3 Selenium 1.3 03/30/12 LK 6010mg/Kg< 0.33 Silver 0.33 03/30/12 LK 6010mg/Kg88.7 Sodium 5.0 03/30/12 LK 6010mg/Kg< 3.0 Thallium 3.0 03/30/12 LK 6010mg/KgCompleted Total Metals Digest 03/29/12 T SW846 - 3050




Page 16 of 41 Ver 1

SB-2 (16-18)




^



90 % TCMX 04/02/12 MH 30 - 150 %%

VolatilesND 1,1,1,2-Tetrachloroethane 5.2 04/02/12 R/J SW8260ug/KgND 1,1,1-Trichloroethane 5.2 04/02/12 R/J SW8260ug/KgND 1,1,2,2-Tetrachloroethane 5.2 04/02/12 R/J SW8260ug/KgND 1,1,2-Trichloroethane 5.2 04/02/12 R/J SW8260ug/KgND 1,1-Dichloroethane 5.2 04/02/12 R/J SW8260ug/KgND 1,1-Dichloroethene 5.2 04/02/12 R/J SW8260ug/KgND 1,1-Dichloropropene 5.2 04/02/12 R/J SW8260ug/KgND 1,2,3-Trichlorobenzene 5.2 04/02/12 R/J SW8260ug/Kg 1

ND 1,2,3-Trichloropropane 5.2 04/02/12 R/J SW8260ug/KgND 1,2,4-Trichlorobenzene 5.2 04/02/12 R/J SW8260ug/KgND 1,2,4-Trimethylbenzene 5.2 04/02/12 R/J SW8260ug/KgND 1,2-Dibromo-3-chloropropane 5.2 04/02/12 R/J SW8260ug/KgND 1,2-Dichlorobenzene 5.2 04/02/12 R/J SW8260ug/KgND 1,2-Dichloroethane 5.2 04/02/12 R/J SW8260ug/KgND 1,2-Dichloropropane 5.2 04/02/12 R/J SW8260ug/KgND 1,3,5-Trimethylbenzene 5.2 04/02/12 R/J SW8260ug/KgND 1,3-Dichlorobenzene 5.2 04/02/12 R/J SW8260ug/KgND 1,3-Dichloropropane 5.2 04/02/12 R/J SW8260ug/KgND 1,4-Dichlorobenzene 5.2 04/02/12 R/J SW8260ug/KgND 2,2-Dichloropropane 5.2 04/02/12 R/J SW8260ug/KgND 2-Chlorotoluene 5.2 04/02/12 R/J SW8260ug/KgND 2-Hexanone 26 04/02/12 R/J SW8260ug/KgND 2-Isopropyltoluene 5.2 04/02/12 R/J SW8260ug/Kg 1

ND 4-Chlorotoluene 5.2 04/02/12 R/J SW8260ug/KgND 4-Methyl-2-pentanone 26 04/02/12 R/J SW8260ug/KgND Acetone 26 04/02/12 R/J SW8260ug/KgND Acrylonitrile 10 04/02/12 R/J SW8260ug/KgND Benzene 5.2 04/02/12 R/J SW8260ug/KgND Bromobenzene 5.2 04/02/12 R/J SW8260ug/KgND Bromochloromethane 5.2 04/02/12 R/J SW8260ug/KgND Bromodichloromethane 5.2 04/02/12 R/J SW8260ug/KgND Bromoform 5.2 04/02/12 R/J SW8260ug/KgND Bromomethane 5.2 04/02/12 R/J SW8260ug/KgND Carbon Disulfide 5.2 04/02/12 R/J SW8260ug/KgND Carbon tetrachloride 5.2 04/02/12 R/J SW8260ug/Kg

Page 17 of 41 Ver 1

SB-2 (16-18)




^

ND Chlorobenzene 5.2 04/02/12 R/J SW8260ug/KgND Chloroethane 5.2 04/02/12 R/J SW8260ug/KgND Chloroform 5.2 04/02/12 R/J SW8260ug/KgND Chloromethane 5.2 04/02/12 R/J SW8260ug/KgND cis-1,2-Dichloroethene 5.2 04/02/12 R/J SW8260ug/KgND cis-1,3-Dichloropropene 5.2 04/02/12 R/J SW8260ug/KgND Dibromochloromethane 5.2 04/02/12 R/J SW8260ug/KgND Dibromoethane 5.2 04/02/12 R/J SW8260ug/Kg 1,1O

ND Dibromomethane 5.2 04/02/12 R/J SW8260ug/KgND Dichlorodifluoromethane 5.2 04/02/12 R/J SW8260ug/KgND Ethylbenzene 5.2 04/02/12 R/J SW8260ug/KgND Hexachlorobutadiene 5.2 04/02/12 R/J SW8260ug/Kg 1,1P

ND Isopropylbenzene 5.2 04/02/12 R/J SW8260ug/KgND m&p-Xylene 5.2 04/02/12 R/J SW8260ug/KgND Methyl Ethyl Ketone 26 04/02/12 R/J SW8260ug/KgND Methyl t-butyl ether (MTBE) 10 04/02/12 R/J SW8260ug/KgND Methylene chloride 5.2 04/02/12 R/J SW8260ug/KgND Naphthalene 5.2 04/02/12 R/J SW8260ug/KgND n-Butylbenzene 5.2 04/02/12 R/J SW8260ug/KgND n-Propylbenzene 5.2 04/02/12 R/J SW8260ug/KgND o-Xylene 5.2 04/02/12 R/J SW8260ug/KgND p-Isopropyltoluene 5.2 04/02/12 R/J SW8260ug/KgND sec-Butylbenzene 5.2 04/02/12 R/J SW8260ug/KgND Styrene 5.2 04/02/12 R/J SW8260ug/KgND tert-Butylbenzene 5.2 04/02/12 R/J SW8260ug/KgND Tetrachloroethene 5.2 04/02/12 R/J SW8260ug/KgND Tetrahydrofuran (THF) 10 04/02/12 R/J SW8260ug/Kg 1

ND Toluene 5.2 04/02/12 R/J SW8260ug/KgND Total Xylenes 5.2 04/02/12 R/J SW8260ug/KgND trans-1,2-Dichloroethene 5.2 04/02/12 R/J SW8260ug/KgND trans-1,3-Dichloropropene 5.2 04/02/12 R/J SW8260ug/KgND trans-1,4-dichloro-2-butene 10 04/02/12 R/J SW8260ug/KgND Trichloroethene 5.2 04/02/12 R/J SW8260ug/KgND Trichlorofluoromethane 5.2 04/02/12 R/J SW8260ug/KgND Trichlorotrifluoroethane 5.2 04/02/12 R/J SW8260ug/KgND Vinyl chloride 5.2 04/02/12 R/J SW8260ug/Kg

QA/QC Surrogates99 % 1,2-dichlorobenzene-d4 04/02/12 R/J 70 - 130 %%

103 % Bromofluorobenzene 04/02/12 R/J 70 - 130 %%

85 % Dibromofluoromethane 04/02/12 R/J 70 - 130 %%

84 % Toluene-d8 04/02/12 R/J 70 - 130 %%


Page 18 of 41 Ver 1

SB-2 (16-18)




^





Page 19 of 41 Ver 1

SB-2 (16-18)




^




80 % 2-Fluorophenol 03/30/12 DD 15 - 130 %%


80 % Phenol-d5 03/30/12 DD 15 - 130 %%

104 % Terphenyl-d14 03/30/12 DD 15 - 130 %%

Comments:



April 06, 2012






Page 20 of 41 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

SOIL

ESPL

Standard

2121172

03/28/12

LB

see "By" below

RK

Laboratory Data

SB-3 (0-2)

Phoenix ID: BB59639

03/29/12

10:00

14:52




Time

Date Time



SDG ID: GBB59635

Client ID:


^

5820 Aluminum 55 03/31/12 LK 6010mg/Kg< 3.7 Antimony 3.7 03/30/12 LK 6010mg/Kg2.77 Arsenic 0.73 03/30/12 LK 6010mg/Kg309 Barium 0.37 03/30/12 LK 6010mg/Kg0.31 Beryllium 0.29 03/30/12 LK 6010mg/Kg40800 Calcium 55 03/31/12 LK 6010mg/Kg0.39 Cadmium 0.37 03/30/12 LK 6010mg/Kg10.4 Chromium 0.37 03/30/12 LK 6010mg/Kg3.17 Cobalt 0.37 03/30/12 LK 6010mg/Kg33.3 Copper 0.37 03/30/12 LK 6010mg/kg9270 Iron 5.5 03/30/12 LK 6010mg/Kg603 Lead 3.7 03/31/12 LK 6010mg/Kg3350 Magnesium 5.5 03/30/12 LK 6010mg/Kg304 Manganese 3.7 03/31/12 LK 6010mg/Kg1.00 Mercury 0.07 04/02/12 RS SW-7471mg/Kg10.7 Nickel 0.37 03/30/12 LK 6010mg/Kg1510 Potassium 5.5 03/30/12 LK 6010mg/Kg< 1.5 Selenium 1.5 03/30/12 LK 6010mg/Kg< 0.37 Silver 0.37 03/30/12 LK 6010mg/Kg611 Sodium 5.5 03/30/12 LK 6010mg/Kg< 3.3 Thallium 3.3 03/30/12 LK 6010mg/KgCompleted Total Metals Digest 03/29/12 T SW846 - 3050




Page 21 of 41 Ver 1

SB-3 (0-2)




^



90 % TCMX 03/30/12 MH 30 - 150 %%




Page 22 of 41 Ver 1

SB-3 (0-2)




^








95 % Toluene-d8 04/02/12 H/J 70 - 130 %%


Page 23 of 41 Ver 1

SB-3 (0-2)




^



460 Benz(a)anthracene 260 03/30/12 DD SW 8270ug/KgND Benzidine 440 03/30/12 DD SW 8270ug/Kg460 Benzo(a)pyrene 260 03/30/12 DD SW 8270ug/Kg650 Benzo(b)fluoranthene 260 03/30/12 DD SW 8270ug/KgND Benzo(ghi)perylene 260 03/30/12 DD SW 8270ug/KgND Benzo(k)fluoranthene 260 03/30/12 DD SW 8270ug/KgND Benzoic acid 1100 03/30/12 DD SW 8270ug/Kg 1,1O


Page 24 of 41 Ver 1

SB-3 (0-2)




^

ND Hexachlorocyclopentadiene 260 03/30/12 DD SW 8270ug/KgND Hexachloroethane 260 03/30/12 DD SW 8270ug/KgND Indeno(1,2,3-cd)pyrene 260 03/30/12 DD SW 8270ug/KgND Isophorone 260 03/30/12 DD SW 8270ug/KgND Naphthalene 260 03/30/12 DD SW 8270ug/KgND Nitrobenzene 260 03/30/12 DD SW 8270ug/KgND N-Nitrosodimethylamine 360 03/30/12 DD SW 8270ug/KgND N-Nitrosodi-n-propylamine 260 03/30/12 DD SW 8270ug/KgND N-Nitrosodiphenylamine 360 03/30/12 DD SW 8270ug/KgND Pentachloronitrobenzene 360 03/30/12 DD SW 8270ug/KgND Pentachlorophenol 360 03/30/12 DD SW 8270ug/Kg260 Phenanthrene 260 03/30/12 DD SW 8270ug/KgND Phenol 260 03/30/12 DD SW 8270ug/Kg730 Pyrene 260 03/30/12 DD SW 8270ug/KgND Pyridine 360 03/30/12 DD SW 8270ug/Kg



84 % 2-Fluorophenol 03/30/12 DD 15 - 130 %%


84 % Phenol-d5 03/30/12 DD 15 - 130 %%

103 % Terphenyl-d14 03/30/12 DD 15 - 130 %%

Comments:



April 06, 2012






Page 25 of 41 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

SOIL

ESPL

Standard

2121172

03/28/12

LB

see "By" below

RK

Laboratory Data

SB-3 (16-18)

Phoenix ID: BB59640

03/29/12

10:45

14:52




Time

Date Time



SDG ID: GBB59635

Client ID:


^

6170 Aluminum 56 03/31/12 LK 6010mg/Kg< 3.7 Antimony 3.7 03/30/12 LK 6010mg/Kg< 0.74 Arsenic 0.74 03/30/12 LK 6010mg/Kg36.6 Barium 0.37 03/30/12 LK 6010mg/Kg0.41 Beryllium 0.30 03/30/12 LK 6010mg/Kg1290 Calcium 5.6 03/30/12 LK 6010mg/Kg< 0.37 Cadmium 0.37 03/30/12 LK 6010mg/Kg13.6 Chromium 0.37 03/30/12 LK 6010mg/Kg5.05 Cobalt 0.37 03/30/12 LK 6010mg/Kg8.98 Copper 0.37 03/30/12 LK 6010mg/kg12100 Iron 56 03/31/12 LK 6010mg/Kg4.61 Lead 0.37 03/30/12 LK 6010mg/Kg2100 Magnesium 5.6 03/30/12 LK 6010mg/Kg377 Manganese 3.7 03/31/12 LK 6010mg/Kg< 0.08 Mercury 0.08 04/02/12 RS SW-7471mg/Kg15.4 Nickel 0.37 03/30/12 LK 6010mg/Kg1210 Potassium 5.6 03/30/12 LK 6010mg/Kg< 1.5 Selenium 1.5 03/30/12 LK 6010mg/Kg< 0.37 Silver 0.37 03/30/12 LK 6010mg/Kg85.5 Sodium 5.6 03/30/12 LK 6010mg/Kg< 3.3 Thallium 3.3 03/30/12 LK 6010mg/KgCompleted Total Metals Digest 03/29/12 T SW846 - 3050




Page 26 of 41 Ver 1

SB-3 (16-18)




^



92 % TCMX 03/30/12 MH 30 - 150 %%




Page 27 of 41 Ver 1

SB-3 (16-18)




^








100 % Toluene-d8 04/03/12 R/J 70 - 130 %%


Page 28 of 41 Ver 1

SB-3 (16-18)




^





Page 29 of 41 Ver 1

SB-3 (16-18)




^




74 % 2-Fluorophenol 03/30/12 DD 15 - 130 %%


75 % Phenol-d5 03/30/12 DD 15 - 130 %%

95 % Terphenyl-d14 03/30/12 DD 15 - 130 %%

Comments:



April 06, 2012






Page 30 of 41 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

SOIL

ESPL

Standard

2121172

03/28/12

LB

see "By" below

RK

Laboratory Data

USTB

Phoenix ID: BB59641

03/29/12

12:00

14:52




Time

Date Time



SDG ID: GBB59635

Client ID:


^

5500 Aluminum 67 03/31/12 LK 6010mg/Kg< 4.5 Antimony 4.5 03/30/12 LK 6010mg/Kg15.0 Arsenic 0.89 03/30/12 LK 6010mg/Kg165 Barium 0.45 03/30/12 LK 6010mg/Kg0.40 Beryllium 0.36 03/30/12 LK 6010mg/Kg11300 Calcium 6.7 03/30/12 LK 6010mg/Kg0.59 Cadmium 0.45 03/30/12 LK 6010mg/Kg19.8 Chromium 0.45 03/30/12 LK 6010mg/Kg5.58 Cobalt 0.45 03/30/12 LK 6010mg/Kg798 Copper 4.5 03/31/12 LK 6010mg/kg16800 Iron 67 03/31/12 LK 6010mg/Kg781 Lead 4.5 03/31/12 LK 6010mg/Kg2500 Magnesium 6.7 03/30/12 LK 6010mg/Kg291 Manganese 4.5 03/31/12 LK 6010mg/Kg0.73 Mercury 0.09 04/02/12 RS SW-7471mg/Kg21.9 Nickel 0.45 03/30/12 LK 6010mg/Kg976 Potassium 6.7 03/30/12 LK 6010mg/Kg< 1.8 Selenium 1.8 03/30/12 LK 6010mg/Kg< 9 Silver 9 03/31/12 LK 6010mg/Kg685 Sodium 6.7 03/30/12 LK 6010mg/Kg< 4.0 Thallium 4.0 03/30/12 LK 6010mg/KgCompleted Total Metals Digest 03/29/12 T SW846 - 3050




Page 31 of 41 Ver 1

USTB




^



72 % TCMX 03/30/12 MH 30 - 150 %%




Page 32 of 41 Ver 1

USTB




^








93 % Toluene-d8 04/03/12 R/J 70 - 130 %%


Page 33 of 41 Ver 1

USTB




^



1200 Benz(a)anthracene 300 03/30/12 DD SW 8270ug/KgND Benzidine 510 03/30/12 DD SW 8270ug/Kg1200 Benzo(a)pyrene 300 03/30/12 DD SW 8270ug/Kg1600 Benzo(b)fluoranthene 300 03/30/12 DD SW 8270ug/Kg520 Benzo(ghi)perylene 300 03/30/12 DD SW 8270ug/Kg530 Benzo(k)fluoranthene 300 03/30/12 DD SW 8270ug/KgND Benzoic acid 1200 03/30/12 DD SW 8270ug/Kg 1,1O


Page 34 of 41 Ver 1

USTB




^

ND Hexachlorocyclopentadiene 300 03/30/12 DD SW 8270ug/KgND Hexachloroethane 300 03/30/12 DD SW 8270ug/Kg470 Indeno(1,2,3-cd)pyrene 300 03/30/12 DD SW 8270ug/KgND Isophorone 300 03/30/12 DD SW 8270ug/KgND Naphthalene 300 03/30/12 DD SW 8270ug/KgND Nitrobenzene 300 03/30/12 DD SW 8270ug/KgND N-Nitrosodimethylamine 420 03/30/12 DD SW 8270ug/KgND N-Nitrosodi-n-propylamine 300 03/30/12 DD SW 8270ug/KgND N-Nitrosodiphenylamine 420 03/30/12 DD SW 8270ug/KgND Pentachloronitrobenzene 420 03/30/12 DD SW 8270ug/KgND Pentachlorophenol 420 03/30/12 DD SW 8270ug/KgND Phenanthrene 300 03/30/12 DD SW 8270ug/KgND Phenol 300 03/30/12 DD SW 8270ug/Kg1700 Pyrene 300 03/30/12 DD SW 8270ug/KgND Pyridine 420 03/30/12 DD SW 8270ug/Kg



79 % 2-Fluorophenol 03/30/12 DD 15 - 130 %%


80 % Phenol-d5 03/30/12 DD 15 - 130 %%

100 % Terphenyl-d14 03/30/12 DD 15 - 130 %%

Comments:



April 06, 2012






Page 35 of 41 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

WATER

ESPL

Standard

2121172

03/27/12

LB

see "By" below

RK

Laboratory Data

BLANK FIELD

Phoenix ID: BB59642

03/29/12

11:40

14:52




Time

Date Time



SDG ID: GBB59635

Client ID:


VolatilesND 1,1,1,2-Tetrachloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1,1-Trichloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1,2,2-Tetrachloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1,2-Trichloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1-Dichloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1-Dichloroethene 5.0 03/30/12 H/J SW8260ug/LND 1,1-Dichloropropene 5.0 03/30/12 H/J SW8260ug/LND 1,2,3-Trichlorobenzene 5.0 03/30/12 H/J SW8260ug/LND 1,2,3-Trichloropropane 5.0 03/30/12 H/J SW8260ug/LND 1,2,4-Trichlorobenzene 5.0 03/30/12 H/J SW8260ug/L 1,1P

ND 1,2,4-Trimethylbenzene 5.0 03/30/12 H/J SW8260ug/LND 1,2-Dibromo-3-chloropropane 5.0 03/30/12 H/J SW8260ug/LND 1,2-Dichlorobenzene 5.0 03/30/12 H/J SW8260ug/LND 1,2-Dichloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,2-Dichloropropane 5.0 03/30/12 H/J SW8260ug/LND 1,3,5-Trimethylbenzene 5.0 03/30/12 H/J SW8260ug/LND 1,3-Dichlorobenzene 5.0 03/30/12 H/J SW8260ug/LND 1,3-Dichloropropane 5.0 03/30/12 H/J SW8260ug/LND 1,4-Dichlorobenzene 5.0 03/30/12 H/J SW8260ug/LND 2,2-Dichloropropane 5.0 03/30/12 H/J SW8260ug/LND 2-Chlorotoluene 5.0 03/30/12 H/J SW8260ug/LND 2-Hexanone 25 03/30/12 H/J SW8260ug/LND 2-Isopropyltoluene 5.0 03/30/12 H/J SW8260ug/L 1

ND 4-Chlorotoluene 5.0 03/30/12 H/J SW8260ug/LND 4-Methyl-2-pentanone 25 03/30/12 H/J SW8260ug/LND Acetone 50 03/30/12 H/J SW8260ug/L

Page 36 of 41 Ver 1

BLANK FIELD




ND Acrylonitrile 10 03/30/12 H/J SW8260ug/LND Benzene 5.0 03/30/12 H/J SW8260ug/LND Bromobenzene 5.0 03/30/12 H/J SW8260ug/L 1,1O

ND Bromochloromethane 5.0 03/30/12 H/J SW8260ug/LND Bromodichloromethane 5.0 03/30/12 H/J SW8260ug/LND Bromoform 5.0 03/30/12 H/J SW8260ug/LND Bromomethane 5.0 03/30/12 H/J SW8260ug/LND Carbon Disulfide 5.0 03/30/12 H/J SW8260ug/LND Carbon tetrachloride 5.0 03/30/12 H/J SW8260ug/LND Chlorobenzene 5.0 03/30/12 H/J SW8260ug/LND Chloroethane 5.0 03/30/12 H/J SW8260ug/LND Chloroform 5.0 03/30/12 H/J SW8260ug/LND Chloromethane 5.0 03/30/12 H/J SW8260ug/LND cis-1,2-Dichloroethene 5.0 03/30/12 H/J SW8260ug/LND cis-1,3-Dichloropropene 5.0 03/30/12 H/J SW8260ug/LND Dibromochloromethane 5.0 03/30/12 H/J SW8260ug/LND Dibromoethane 5.0 03/30/12 H/J SW8260ug/LND Dibromomethane 5.0 03/30/12 H/J SW8260ug/LND Dichlorodifluoromethane 5.0 03/30/12 H/J SW8260ug/LND Ethylbenzene 5.0 03/30/12 H/J SW8260ug/LND Hexachlorobutadiene 5.0 03/30/12 H/J SW8260ug/LND Isopropylbenzene 5.0 03/30/12 H/J SW8260ug/LND m&p-Xylene 5.0 03/30/12 H/J SW8260ug/LND Methyl Ethyl Ketone 60 03/30/12 H/J SW8260ug/LND Methyl t-butyl ether (MTBE) 10 03/30/12 H/J SW8260ug/LND Methylene chloride 5.0 03/30/12 H/J SW8260ug/LND Naphthalene 5.0 03/30/12 H/J SW8260ug/L 1,1P

ND n-Butylbenzene 5.0 03/30/12 H/J SW8260ug/LND n-Propylbenzene 5.0 03/30/12 H/J SW8260ug/LND o-Xylene 5.0 03/30/12 H/J SW8260ug/LND p-Isopropyltoluene 5.0 03/30/12 H/J SW8260ug/LND sec-Butylbenzene 5.0 03/30/12 H/J SW8260ug/LND Styrene 5.0 03/30/12 H/J SW8260ug/LND tert-Butylbenzene 5.0 03/30/12 H/J SW8260ug/LND Tetrachloroethene 5.0 03/30/12 H/J SW8260ug/LND Tetrahydrofuran (THF) 10 03/30/12 H/J SW8260ug/L 1

ND Toluene 5.0 03/30/12 H/J SW8260ug/LND Total Xylenes 5.0 03/30/12 H/J SW8260ug/LND trans-1,2-Dichloroethene 5.0 03/30/12 H/J SW8260ug/LND trans-1,3-Dichloropropene 5.0 03/30/12 H/J SW8260ug/LND trans-1,4-dichloro-2-butene 10 03/30/12 H/J SW8260ug/LND Trichloroethene 5.0 03/30/12 H/J SW8260ug/LND Trichlorofluoromethane 5.0 03/30/12 H/J SW8260ug/LND Trichlorotrifluoroethane 5.0 03/30/12 H/J SW8260ug/L 1

ND Vinyl chloride 5.0 03/30/12 H/J SW8260ug/L




101 % Toluene-d8 03/30/12 H/J 70 - 130 %%

Page 37 of 41 Ver 1

BLANK FIELD




Comments:FIELD BLANK INCLUDED



April 06, 2012





Page 38 of 41 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

WATER

ESPL

Standard

2121172

03/27/12

LB

see "By" below

RK

Laboratory Data

BLANK TRIP

Phoenix ID: BB59643

03/29/12

0:00

14:52




Time

Date Time



SDG ID: GBB59635

Client ID:


VolatilesND 1,1,1,2-Tetrachloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1,1-Trichloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1,2,2-Tetrachloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1,2-Trichloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1-Dichloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,1-Dichloroethene 5.0 03/30/12 H/J SW8260ug/LND 1,1-Dichloropropene 5.0 03/30/12 H/J SW8260ug/LND 1,2,3-Trichlorobenzene 5.0 03/30/12 H/J SW8260ug/LND 1,2,3-Trichloropropane 5.0 03/30/12 H/J SW8260ug/LND 1,2,4-Trichlorobenzene 5.0 03/30/12 H/J SW8260ug/L 1,1P

ND 1,2,4-Trimethylbenzene 5.0 03/30/12 H/J SW8260ug/LND 1,2-Dibromo-3-chloropropane 5.0 03/30/12 H/J SW8260ug/LND 1,2-Dichlorobenzene 5.0 03/30/12 H/J SW8260ug/LND 1,2-Dichloroethane 5.0 03/30/12 H/J SW8260ug/LND 1,2-Dichloropropane 5.0 03/30/12 H/J SW8260ug/LND 1,3,5-Trimethylbenzene 5.0 03/30/12 H/J SW8260ug/LND 1,3-Dichlorobenzene 5.0 03/30/12 H/J SW8260ug/LND 1,3-Dichloropropane 5.0 03/30/12 H/J SW8260ug/LND 1,4-Dichlorobenzene 5.0 03/30/12 H/J SW8260ug/LND 2,2-Dichloropropane 5.0 03/30/12 H/J SW8260ug/LND 2-Chlorotoluene 5.0 03/30/12 H/J SW8260ug/LND 2-Hexanone 25 03/30/12 H/J SW8260ug/LND 2-Isopropyltoluene 5.0 03/30/12 H/J SW8260ug/L 1

ND 4-Chlorotoluene 5.0 03/30/12 H/J SW8260ug/LND 4-Methyl-2-pentanone 25 03/30/12 H/J SW8260ug/LND Acetone 50 03/30/12 H/J SW8260ug/L

Page 39 of 41 Ver 1

BLANK TRIP




ND Acrylonitrile 10 03/30/12 H/J SW8260ug/LND Benzene 5.0 03/30/12 H/J SW8260ug/LND Bromobenzene 5.0 03/30/12 H/J SW8260ug/L 1,1O

ND Bromochloromethane 5.0 03/30/12 H/J SW8260ug/LND Bromodichloromethane 5.0 03/30/12 H/J SW8260ug/LND Bromoform 5.0 03/30/12 H/J SW8260ug/LND Bromomethane 5.0 03/30/12 H/J SW8260ug/LND Carbon Disulfide 5.0 03/30/12 H/J SW8260ug/LND Carbon tetrachloride 5.0 03/30/12 H/J SW8260ug/LND Chlorobenzene 5.0 03/30/12 H/J SW8260ug/LND Chloroethane 5.0 03/30/12 H/J SW8260ug/LND Chloroform 5.0 03/30/12 H/J SW8260ug/LND Chloromethane 5.0 03/30/12 H/J SW8260ug/LND cis-1,2-Dichloroethene 5.0 03/30/12 H/J SW8260ug/LND cis-1,3-Dichloropropene 5.0 03/30/12 H/J SW8260ug/LND Dibromochloromethane 5.0 03/30/12 H/J SW8260ug/LND Dibromoethane 5.0 03/30/12 H/J SW8260ug/LND Dibromomethane 5.0 03/30/12 H/J SW8260ug/LND Dichlorodifluoromethane 5.0 03/30/12 H/J SW8260ug/LND Ethylbenzene 5.0 03/30/12 H/J SW8260ug/LND Hexachlorobutadiene 5.0 03/30/12 H/J SW8260ug/LND Isopropylbenzene 5.0 03/30/12 H/J SW8260ug/LND m&p-Xylene 5.0 03/30/12 H/J SW8260ug/LND Methyl Ethyl Ketone 60 03/30/12 H/J SW8260ug/LND Methyl t-butyl ether (MTBE) 10 03/30/12 H/J SW8260ug/LND Methylene chloride 5.0 03/30/12 H/J SW8260ug/LND Naphthalene 5.0 03/30/12 H/J SW8260ug/L 1,1P

ND n-Butylbenzene 5.0 03/30/12 H/J SW8260ug/LND n-Propylbenzene 5.0 03/30/12 H/J SW8260ug/LND o-Xylene 5.0 03/30/12 H/J SW8260ug/LND p-Isopropyltoluene 5.0 03/30/12 H/J SW8260ug/LND sec-Butylbenzene 5.0 03/30/12 H/J SW8260ug/LND Styrene 5.0 03/30/12 H/J SW8260ug/LND tert-Butylbenzene 5.0 03/30/12 H/J SW8260ug/LND Tetrachloroethene 5.0 03/30/12 H/J SW8260ug/LND Tetrahydrofuran (THF) 10 03/30/12 H/J SW8260ug/L 1

ND Toluene 5.0 03/30/12 H/J SW8260ug/LND Total Xylenes 5.0 03/30/12 H/J SW8260ug/LND trans-1,2-Dichloroethene 5.0 03/30/12 H/J SW8260ug/LND trans-1,3-Dichloropropene 5.0 03/30/12 H/J SW8260ug/LND trans-1,4-dichloro-2-butene 10 03/30/12 H/J SW8260ug/LND Trichloroethene 5.0 03/30/12 H/J SW8260ug/LND Trichlorofluoromethane 5.0 03/30/12 H/J SW8260ug/LND Trichlorotrifluoroethane 5.0 03/30/12 H/J SW8260ug/L 1

ND Vinyl chloride 5.0 03/30/12 H/J SW8260ug/L




102 % Toluene-d8 03/30/12 H/J 70 - 130 %%

Page 40 of 41 Ver 1

BLANK TRIP




Comments:TRIP BLANK INCLUDED



April 06, 2012





Page 41 of 41 Ver 1

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

QA/QC ReportApril 06, 2012



SDG I.D.: GBB59635

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

SampleResult

DupResult

QA/QC Batch 197317, QC Sample No: BB59621 (BB59635, BB59636, BB59637, BB59638, BB59639, BB59640, BB59641)

ICP Metals - SoilNC NCAluminum BDL NC1013.70 104 2.9 75 - 125 3013700 13200

74.9 79.1Antimony BDL 5.5116NC 114 1.7 m75 - 125 30<3.7 <3.8

83.5 88.7Arsenic BDL 6.085.1NC 87.3 2.6 75 - 125 30<0.74 <0.75

92.8 97.4Barium BDL 4.889.78.60 88.1 1.8 75 - 125 3062.6 68.2

84.3 90.8Beryllium BDL 7.489.2NC 89.4 0.2 75 - 125 300.38 0.41

82.2 87.3Cadmium BDL 6.086.1NC 85.3 0.9 75 - 125 30<0.37 <0.38

>130 >130Calcium BDL NC87.04.90 88.7 1.9 m75 - 125 30461 439

89.5 92.0Chromium BDL 2.892.52.60 93.9 1.5 75 - 125 3039.3 38.3

84.0 89.4Cobalt BDL 6.287.72.90 87.9 0.2 75 - 125 308.96 9.22

88.5 93.7Copper BDL 5.790.30.60 90.2 0.1 75 - 125 3063.5 63.9

NC NCIron BDL NC1023.10 108 5.7 75 - 125 3019100 19700

83.4 89.0Lead BDL 6.587.30.20 88.9 1.8 75 - 125 305.07 5.06

NC NCMagnesium BDL NC90.58.50 90.6 0.1 75 - 125 306500 5970

98.4 108Manganese BDL 9.391.13.40 92.0 1.0 75 - 125 30232 240

83.4 89.4Nickel BDL 6.987.54.80 86.3 1.4 75 - 125 3014.3 15.0

81.9 81.4Potassium BDL 0.697.82.60 100 2.2 75 - 125 302330 2270

80.2 85.2Selenium BDL 6.082.1NC 83.1 1.2 75 - 125 30<1.5 <1.5

85.3 88.6Silver BDL 3.886.5NC 84.8 2.0 75 - 125 30<0.37 <0.38

127 >130Sodium BDL NC94.78.30 112 16.7 m75 - 125 30106 97.6

82.1 86.8Thallium BDL 5.687.6NC 88.3 0.8 75 - 125 30<3.3 <3.4

90.9 96.1Vanadium BDL 5.61004.20 103 3.0 75 - 125 3040.0 41.7

87.6 91.0Zinc BDL 3.886.03.40 85.7 0.3 75 - 125 3041.8 40.4

QA/QC Batch 197441, QC Sample No: BB60419 (BB59635, BB59636, BB59637, BB59638, BB59639, BB59640, BB59641)117 107Mercury - Soil BDL 8.9113NC 110 2.7 70 - 130 30<0.07 <0.07

m = This parameter is outside laboratory ms/msd specified recovery limits.

Page 1 of 9

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBB59635

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

QA/QC Batch 197562, QC Sample No: BB58060 (BB59635, BB59637, BB59638, BB59639)

Volatiles - Soil125 1191,1,1,2-Tetrachloroethane ND 4.9115 123 6.7 70 - 130 30

93 1001,1,1-Trichloroethane ND 7.3113 110 2.7 70 - 130 30

114 1051,1,2,2-Tetrachloroethane ND 8.2107 120 11.5 70 - 130 30


93 1101,1-Dichloroethane ND 16.7112 101 10.3 70 - 130 30

92 861,1-Dichloroethene ND 6.7102 107 4.8 70 - 130 30

101 961,1-Dichloropropene ND 5.1110 94 15.7 70 - 130 30

113 991,2,3-Trichlorobenzene ND 13.2107 121 12.3 70 - 130 30

113 1071,2,3-Trichloropropane ND 5.5105 119 12.5 70 - 130 30


111 1021,2,4-Trimethylbenzene ND 8.5115 120 4.3 70 - 130 30

107 1011,2-Dibromo-3-chloropropane ND 5.899 120 19.2 70 - 130 30

102 961,2-Dichlorobenzene ND 6.1102 107 4.8 70 - 130 30


108 1051,2-Dichloropropane ND 2.8104 105 1.0 70 - 130 30






102 962-Chlorotoluene ND 6.1107 108 0.9 70 - 130 30

71 622-Hexanone ND 13.591 104 13.3 m70 - 130 30

106 1002-Isopropyltoluene ND 5.8109 113 3.6 70 - 130 30


94 874-Methyl-2-pentanone ND 7.791 107 16.2 70 - 130 30

79 66Acetone ND 17.988 109 21.3 m70 - 130 30

88 104Acrylonitrile ND 16.7103 97 6.0 70 - 130 30

107 102Benzene ND 4.8103 107 3.8 70 - 130 30

106 103Bromobenzene ND 2.9103 108 4.7 70 - 130 30

96 116Bromochloromethane ND 18.9111 98 12.4 70 - 130 30

110 110Bromodichloromethane ND 0.0107 108 0.9 70 - 130 30

103 108Bromoform ND 4.799 104 4.9 70 - 130 30

90 93Bromomethane ND 3.399 92 7.3 70 - 130 30

89 84Carbon Disulfide ND 5.896 104 8.0 70 - 130 30

86 98Carbon tetrachloride ND 13.0115 105 9.1 70 - 130 30

107 106Chlorobenzene ND 0.9104 109 4.7 70 - 130 30

95 96Chloroethane ND 1.0110 97 12.6 70 - 130 30

98 109Chloroform ND 10.6113 105 7.3 70 - 130 30

92 88Chloromethane ND 4.496 99 3.1 70 - 130 30

94 113cis-1,2-Dichloroethene ND 18.4113 98 14.2 70 - 130 30

109 106cis-1,3-Dichloropropene ND 2.8103 105 1.9 70 - 130 30

Page 2 of 9

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB59635

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

112 107Dibromochloromethane ND 4.6104 113 8.3 70 - 130 30

108 110Dibromoethane ND 1.8102 107 4.8 70 - 130 30

109 107Dibromomethane ND 1.9104 106 1.9 70 - 130 30

65 81Dichlorodifluoromethane ND 21.997 84 14.4 m70 - 130 30

103 104Ethylbenzene ND 1.0108 112 3.6 70 - 130 30

94 84Hexachlorobutadiene ND 11.2109 110 0.9 70 - 130 30

110 105Isopropylbenzene ND 4.7118 121 2.5 70 - 130 30

106 104m&p-Xylene ND 1.9111 114 2.7 70 - 130 30

75 73Methyl ethyl ketone ND 2.790 84 6.9 70 - 130 30

106 98Methyl t-butyl ether (MTBE) ND 7.888 96 8.7 70 - 130 30

104 102Methylene chloride ND 1.9100 106 5.8 70 - 130 30

116 101Naphthalene ND 13.899 121 20.0 70 - 130 30

93 87n-Butylbenzene ND 6.7115 116 0.9 70 - 130 30

96 91n-Propylbenzene ND 5.3109 109 0.0 70 - 130 30

113 113o-Xylene ND 0.0113 116 2.6 70 - 130 30

104 98p-Isopropyltoluene ND 5.9116 118 1.7 70 - 130 30

102 98sec-Butylbenzene ND 4.0115 116 0.9 70 - 130 30

90 98Styrene ND 8.593 94 1.1 70 - 130 30

102 99tert-Butylbenzene ND 3.0110 110 0.0 70 - 130 30

100 92Tetrachloroethene ND 8.3109 115 5.4 70 - 130 30

86 99Tetrahydrofuran (THF) ND 14.199 92 7.3 70 - 130 30

104 105Toluene ND 1.0106 107 0.9 70 - 130 30

98 95trans-1,2-Dichloroethene ND 3.1102 110 7.5 70 - 130 30

112 109trans-1,3-Dichloropropene ND 2.7104 107 2.8 70 - 130 30

119 114trans-1,4-dichloro-2-butene ND 4.3115 129 11.5 70 - 130 30

102 99Trichloroethene ND 3.0105 108 2.8 70 - 130 30

99 95Trichlorofluoromethane ND 4.1125 132 5.4 l70 - 130 30

88 80Trichlorotrifluoroethane ND 9.5103 112 8.4 70 - 130 30

87 87Vinyl chloride ND 0.0101 104 2.9 70 - 130 30

97 94% 1,2-dichlorobenzene-d4 95 3.196 98 2.1 70 - 130 30

98 101% Bromofluorobenzene 94 3.099 98 1.0 70 - 130 30

87 103% Dibromofluoromethane 85 16.8109 89 20.2 70 - 130 30

97 99% Toluene-d8 94 2.097 95 2.1 70 - 130 30

A blank MS/MSD was analyzed with this batch.

Comment:

QA/QC Batch 197630, QC Sample No: BB58377 (BB59640, BB59641)
















Page 3 of 9

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB59635

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits







53 622-Hexanone ND 15.764 81 23.4 l,m70 - 130 30




<40 <40Acetone ND NC67 92 31.4 l,m,r70 - 130 30


105 105Benzene ND 0.0108 108 0.0 70 - 130 30

101 102Bromobenzene ND 1.0106 106 0.0 70 - 130 30



92 97Bromoform ND 5.3101 106 4.8 70 - 130 30

74 74Bromomethane ND 0.0112 110 1.8 70 - 130 30




<40 <40Chloroethane ND NC104 107 2.8 m70 - 130 30

110 105Chloroform ND 4.7112 110 1.8 70 - 130 30







115 113Dichlorodifluoromethane ND 1.898 94 4.2 70 - 130 30

107 106Ethylbenzene ND 0.9110 108 1.8 70 - 130 30



107 106m&p-Xylene ND 0.9109 105 3.7 70 - 130 30

50 56Methyl ethyl ketone ND 11.369 95 31.7 l,m,r70 - 130 30



118 97Naphthalene ND 19.5120 99 19.2 70 - 130 30



108 106o-Xylene ND 1.9108 105 2.8 70 - 130 30



107 109Styrene ND 1.9106 107 0.9 70 - 130 30




108 105Toluene ND 2.8109 108 0.9 70 - 130 30





57 <40Trichlorofluoromethane ND NC120 122 1.7 m70 - 130 30

Page 4 of 9

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB59635

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits






102 101% Toluene-d8 100 1.0100 100 0.0 70 - 130 30

QA/QC Batch 197472, QC Sample No: BB58767 (BB59636)



128 1311,1,2,2-Tetrachloroethane ND 2.3106 108 1.9 m70 - 130 30



















<40 <402-Hexanone ND NC77 85 9.9 m70 - 130 30




<40 <40Acetone ND NC74 92 21.7 m70 - 130 30


105 103Benzene ND 1.9101 101 0.0 70 - 130 30

114 109Bromobenzene ND 4.5115 111 3.5 70 - 130 30



108 104Bromoform ND 3.8109 103 5.7 70 - 130 30

107 91Bromomethane ND 16.294 85 10.1 70 - 130 30




118 99Chloroethane ND 17.5106 99 6.8 70 - 130 30

112 95Chloroform ND 16.4114 98 15.1 70 - 130 30







Page 5 of 9

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB59635

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits


111 101Ethylbenzene ND 9.4102 98 4.0 70 - 130 30


136 129Isopropylbenzene ND 5.3119 116 2.6 m70 - 130 30

108 102m&p-Xylene ND 5.7102 100 2.0 70 - 130 30

40 42Methyl ethyl ketone ND 4.985 76 11.2 m70 - 130 30



51 55Naphthalene ND 7.5104 119 13.5 m70 - 130 30



116 109o-Xylene ND 6.2111 106 4.6 70 - 130 30



66 59Styrene ND 11.297 92 5.3 m70 - 130 30




104 98Toluene ND 5.9101 98 3.0 70 - 130 30





106 102Trichlorofluoromethane ND 3.8108 108 0.0 70 - 130 30






99 98% Toluene-d8 94 1.0101 97 4.0 70 - 130 30


Polychlorinated Biphenyls - Soil102 91PCB-1016 ND 11.476 82 7.6 40 - 140 30

PCB-1221 ND 40 - 140 30

PCB-1232 ND 40 - 140 30

PCB-1242 ND 40 - 140 30

PCB-1248 ND 40 - 140 30

PCB-1254 ND 40 - 140 30

111 102PCB-1260 ND 8.577 92 17.8 40 - 140 30

PCB-1262 ND 40 - 140 30

PCB-1268 ND 40 - 140 30

103 94% DCBP (Surrogate Rec) 72 9.166 69 4.4 30 - 150 30

80 74% TCMX (Surrogate Rec) 73 7.877 81 5.1 30 - 150 30


Semivolatiles - Soil59 601,2,4,5-Tetrachlorobenzene ND 1.756 57 1.8 30 - 130 30





85 842,4,5-Trichlorophenol ND 1.280 79 1.3 30 - 130 30

89 902,4,6-Trichlorophenol ND 1.181 81 0.0 30 - 130 30

Page 6 of 9

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB59635

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

87 882,4-Dichlorophenol ND 1.182 82 0.0 30 - 130 30

48 482,4-Dimethylphenol ND 0.039 39 0.0 30 - 130 30

9.2 102,4-Dinitrophenol ND 8.333 12 93.3 l,m,r30 - 130 30

88 892,4-Dinitrotoluene ND 1.182 85 3.6 30 - 130 30

84 852,6-Dinitrotoluene ND 1.281 84 3.6 30 - 130 30

81 832-Chloronaphthalene ND 2.475 75 0.0 30 - 130 30

78 802-Chlorophenol ND 2.572 73 1.4 30 - 130 30

NC NC2-Methylnaphthalene ND NC72 73 1.4 30 - 130 30

87 882-Methylphenol (o-cresol) ND 1.168 69 1.5 30 - 130 30

>130 >1302-Nitroaniline ND NC>150 >150 NC l,m30 - 130 30

79 802-Nitrophenol ND 1.375 77 2.6 30 - 130 30

78 783&4-Methylphenol (m&p-cresol) ND 0.072 73 1.4 30 - 130 30

78 843,3'-Dichlorobenzidine ND 7.482 82 0.0 30 - 130 30

88 913-Nitroaniline ND 3.483 85 2.4 30 - 130 30

26 214,6-Dinitro-2-methylphenol ND 21.375 62 19.0 m30 - 130 30

85 874-Bromophenyl phenyl ether ND 2.379 80 1.3 30 - 130 30

87 894-Chloro-3-methylphenol ND 2.383 84 1.2 30 - 130 30

37 494-Chloroaniline ND 27.954 53 1.9 30 - 130 30

82 844-Chlorophenyl phenyl ether ND 2.479 79 0.0 30 - 130 30

88 914-Nitroaniline ND 3.483 85 2.4 30 - 130 30

99 984-Nitrophenol ND 1.087 88 1.1 30 - 130 30

55 56Acenaphthene ND 1.875 75 0.0 30 - 130 30

NC NCAcenaphthylene ND NC73 74 1.4 30 - 130 30

56 57Acetophenone ND 1.848 49 2.1 30 - 130 30

19 46Aniline ND 83.151 52 1.9 m,r30 - 130 30

NC NCAnthracene ND NC76 76 0.0 30 - 130 30

48 47Azobenzene ND 2.149 49 0.0 30 - 130 30

NC NCBenz(a)anthracene ND NC79 80 1.3 30 - 130 30

<5 <5Benzidine ND NC69 72 4.3 m30 - 130 30

NC NCBenzo(a)pyrene ND NC77 77 0.0 30 - 130 30

NC NCBenzo(b)fluoranthene ND NC82 80 2.5 30 - 130 30

NC NCBenzo(ghi)perylene ND NC83 81 2.4 30 - 130 30

50 66Benzo(k)fluoranthene ND 27.682 79 3.7 30 - 130 30

107 105Benzyl butyl phthalate ND 1.980 80 0.0 30 - 130 30

80 81Bis(2-chloroethoxy)methane ND 1.273 75 2.7 30 - 130 30

106 74Bis(2-chloroethyl)ether ND 35.664 65 1.6 r30 - 130 30

77 79Bis(2-chloroisopropyl)ether ND 2.671 73 2.8 30 - 130 30

130 100Bis(2-ethylhexyl)phthalate ND 26.174 71 4.1 30 - 130 30

78 81Carbazole ND 3.8109 110 0.9 30 - 130 30

NC NCChrysene ND NC79 80 1.3 30 - 130 30

53 50Dibenz(a,h)anthracene ND 5.884 84 0.0 30 - 130 30

55 64Dibenzofuran ND 15.175 75 0.0 30 - 130 30

80 82Diethyl phthalate ND 2.579 79 0.0 30 - 130 30

81 83Dimethylphthalate ND 2.478 78 0.0 30 - 130 30

78 79Di-n-butylphthalate ND 1.376 76 0.0 30 - 130 30

107 108Di-n-octylphthalate ND 0.979 79 0.0 30 - 130 30

NC NCFluoranthene ND NC79 80 1.3 30 - 130 30

NC NCFluorene ND NC78 78 0.0 30 - 130 30

80 81Hexachlorobenzene ND 1.279 79 0.0 30 - 130 30


5.6 4.6Hexachlorocyclopentadiene ND 19.654 58 7.1 m30 - 130 30

80 76Hexachloroethane ND 5.166 67 1.5 30 - 130 30

28 24Indeno(1,2,3-cd)pyrene ND 15.484 83 1.2 m30 - 130 30

Page 7 of 9

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB59635

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

66 66Isophorone ND 0.059 61 3.3 30 - 130 30

NC NCNaphthalene ND NC73 74 1.4 30 - 130 30

81 84Nitrobenzene ND 3.673 75 2.7 30 - 130 30

69 72N-Nitrosodimethylamine ND 4.363 65 3.1 30 - 130 30

77 79N-Nitrosodi-n-propylamine ND 2.674 76 2.7 30 - 130 30

96 98N-Nitrosodiphenylamine ND 2.187 87 0.0 30 - 130 30

98 98Pentachloronitrobenzene ND 0.0108 108 0.0 30 - 130 30

97 92Pentachlorophenol ND 5.370 67 4.4 30 - 130 30

NC NCPhenanthrene ND NC80 80 0.0 30 - 130 30

99 97Phenol ND 2.078 79 1.3 30 - 130 30

NC NCPyrene ND NC81 81 0.0 30 - 130 30

43 50Pyridine ND 15.134 36 5.7 30 - 130 30

85 89% 2,4,6-Tribromophenol 80 4.681 82 1.2 15 - 130 30

74 77% 2-Fluorobiphenyl 71 4.070 71 1.4 30 - 130 30

78 81% 2-Fluorophenol 73 3.872 73 1.4 15 - 130 30

76 79% Nitrobenzene-d5 74 3.970 73 4.2 30 - 130 30

75 78% Phenol-d5 72 3.971 73 2.8 15 - 130 30

93 95% Terphenyl-d14 93 2.193 94 1.1 30 - 130 30


Volatiles - Water93 911,1,1,2-Tetrachloroethane ND 2.2103 102 1.0 70 - 130 30





















64 642-Hexanone ND 0.073 71 2.8 m70 - 130 30




<40 44Acetone ND NC52 52 0.0 l,m70 - 130 30


99 95Benzene ND 4.1109 107 1.9 70 - 130 30

88 83Bromobenzene ND 5.8101 98 3.0 70 - 130 30



101 98Bromoform ND 3.0117 112 4.4 70 - 130 30

Page 8 of 9

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB59635

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

120 115Bromomethane ND 4.3127 128 0.8 70 - 130 30




107 106Chloroethane ND 0.9112 112 0.0 70 - 130 30

102 100Chloroform ND 2.0111 108 2.7 70 - 130 30








95 92Ethylbenzene ND 3.2106 106 0.0 70 - 130 30



99 95m&p-Xylene ND 4.1111 108 2.7 70 - 130 30

65 65Methyl ethyl ketone ND 0.067 63 6.2 l,m70 - 130 30



107 102Naphthalene ND 4.8117 119 1.7 70 - 130 30



100 95o-Xylene ND 5.1109 107 1.9 70 - 130 30



113 108Styrene ND 4.5126 123 2.4 70 - 130 30




98 94Toluene ND 4.2109 107 1.9 70 - 130 30











102 100% Toluene-d8 101 2.0101 102 1.0 70 - 130 30

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.

MS - Matrix SpikePhyllis Shiller, Laboratory Director


April 06, 2012MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate

NC - No Criteria

Page 9 of 9

Sample Criteria Exceedences ReportFriday, April 06, 2012 Page 1 of 1

Acode Phoenix AnalyteFactoredCriteriaResult RLCriteria NameSampNo LocCode

AnalysisUnitsST State Category

CriteriaUnits

GBB59635Requested Criteria: 375NR, 375RSFactored

RLCriteria

PB-SM Lead 400489 3.4 mg/KgBB59637 ESPL NY 375-6.8 Metals Residentialmg/kg 400

HG-SM Mercury 0.811.00 0.07 mg/KgBB59639 ESPL NY 375-6.8 Metals Residentialmg/kg 0.81PB-SM Lead 400603 3.7 mg/KgBB59639 ESPL NY 375-6.8 Metals Residentialmg/kg 400

$8270-SMR Benz(a)anthracene 10001200 300 ug/KgBB59641 ESPL NY 375-6.8 Semivolatiles Residentialmg/kg 1000$8270-SMR Chrysene 10001100 300 ug/KgBB59641 ESPL NY 375-6.8 Semivolatiles Residentialmg/kg 1000$8270-SMR Benzo(b)fluoranthene 10001600 300 ug/KgBB59641 ESPL NY 375-6.8 Semivolatiles Residentialmg/kg 1000$8270-SMR Benzo(a)pyrene 10001200 300 ug/KgBB59641 ESPL NY 375-6.8 Semivolatiles Commercialmg/kg 1000$8270-SMR Benzo(a)pyrene 10001200 300 ug/KgBB59641 ESPL NY 375-6.8 Semivolatiles Residentialmg/kg 1000CU-SM Copper 270798 4.5 mg/kgBB59641 ESPL NY 375-6.8 Metals Commercialmg/kg 270CU-SM Copper 270798 4.5 mg/kgBB59641 ESPL NY 375-6.8 Metals Residentialmg/kg 270PB-SM Lead 400781 4.5 mg/KgBB59641 ESPL NY 375-6.8 Metals Residentialmg/kg 400

Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.

BB62841 - BB62845

Thursday, April 12, 2012

Sample ID#s:






Sincerely yours,







Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

ESPL

72 Hour

212117-2

04/04/12

SW

see "By" below

Laboratory Data

MW-1

Phoenix ID: BB62841

04/05/12

10:15

16:35




Time

Date Time



SDG ID: GBB62841

Client ID:


130 Aluminum 0.10 04/09/12 LK 6010mg/L5.05 Aluminum (Dissolved) 0.01 04/06/12 EK 6010mg/L< 0.005 Antimony (Dissolved) 0.005 04/06/12 EK 6010mg/L< 0.005 Antimony 0.005 04/07/12 LK 6010mg/L0.026 Arsenic 0.004 04/07/12 LK 6010mg/L< 0.004 Arsenic (Dissolved) 0.004 04/06/12 EK 6010mg/L4.57 Barium 0.002 04/07/12 LK 6010mg/L0.450 Barium (Dissolved) 0.002 04/06/12 EK 6010mg/L0.011 Beryllium 0.001 04/07/12 LK 6010mg/L< 0.001 Beryllium (Dissolved) 0.001 04/06/12 EK 6010mg/L124 Calcium 0.010 04/07/12 LK 6010mg/L0.003 Cadmium 0.001 04/07/12 LK 6010mg/L90.0 Calcium (Dissolved) 0.01 04/06/12 EK 6010mg/L< 0.001 Cadmium (Dissolved) 0.001 04/06/12 EK 6010mg/L0.423 Chromium 0.001 04/07/12 LK 6010mg/L0.022 Chromium (Dissolved) 0.001 04/06/12 EK 6010mg/L0.178 Cobalt 0.002 04/07/12 LK 6010mg/L0.446 Copper 0.005 04/07/12 LK 6010mg/L0.012 Cobalt (Dissolved) 0.001 04/06/12 EK 6010mg/L0.043 Copper (Dissolved) 0.005 04/06/12 EK 6010mg/LCompleted Dissolved Metals Preparation 04/05/12 AG SW846-3005

8.23 Iron (Dissolved) 0.011 04/06/12 EK 6010mg/L210 Iron 0.10 04/09/12 LK 6010mg/L0.043 Lead (Dissolved) 0.002 04/06/12 EK 6010mg/L0.492 Lead 0.002 04/07/12 LK 6010mg/L33.1 Magnesium (Dissolved) 0.01 04/06/12 EK 6010mg/L2.26 Manganese (Dissolved) 0.011 04/09/12 LK 6010mg/L89.0 Magnesium 0.10 04/09/12 LK 6010mg/L

Page 1 of 24 Ver 1

MW-1




15.3 Manganese 0.010 04/09/12 LK 6010mg/L< 0.0002 Mercury (Dissolved) 0.0002 04/06/12 RS 7470/E245.1mg/L< 0.0002 Mercury 0.0002 04/06/12 RS 7470/E245.1mg/L0.039 Nickel (Dissolved) 0.001 04/06/12 EK 6010mg/L0.836 Nickel 0.001 04/07/12 LK 6010mg/L16.8 Potassium (Dissolved) 0.1 04/06/12 EK 6010mg/L42.1 Potassium 0.1 04/07/12 LK 6010mg/L< 0.011 Selenium (Dissolved) 0.011 04/09/12 LK 6010mg/L< 0.010 Selenium 0.010 04/07/12 LK 6010mg/L< 0.001 Silver 0.001 04/09/12 LK 6010mg/L< 0.001 Silver (Dissolved) 0.001 04/06/12 EK 6010mg/L37.8 Sodium (Dissolved) 0.11 04/06/12 EK 6010mg/L30.1 Sodium 0.1 04/07/12 LK 6010mg/L< 0.002 Thallium (Dissolved) 0.002 04/09/12 RS 7010/279.2mg/L< 0.002 Thallium 0.002 04/09/12 RS SW7010/200.9mg/LCompleted Total Metals Digestion 04/05/12 AG

0.015 Vanadium (Dissolved) 0.002 04/06/12 EK 6010mg/L0.227 Vanadium 0.002 04/07/12 LK 6010mg/L0.186 Zinc (Dissolved) 0.002 04/06/12 EK 6010mg/L1.81 Zinc 0.002 04/07/12 LK 6010mg/LCompleted Filtration 04/05/12 AG 0.45um Filter

Completed Dissolved Mercury Digestion 04/06/12 X/X SW7470

Completed Mercury Digestion 04/06/12 X/X 7471/245.1

Completed PCB Extraction 04/06/12 L SW3510C

Completed Extraction for Pest (2 Liter) 04/06/12 L SW3510

Completed Semi-Volatile Extraction 04/05/12 F/K SW3520

Polychlorinated BiphenylsND PCB-1016 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1221 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1232 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1242 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1248 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1254 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1260 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1262 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1268 0.09 04/10/12 MH 608/ 8082ug/L


70 % TCMX 04/10/12 MH 30 - 150 %%

PesticidesND 4,4' -DDD 0.01 04/10/12 MR SW8081ug/LND* 4,4' -DDE 0.07 04/10/12 MR SW8081ug/LND 4,4' -DDT 0.01 04/10/12 MR SW8081ug/LND a-BHC 0.01 04/10/12 MR SW8081ug/LND Alachlor 0.1 04/10/12 MR SW8081ug/L 1

ND Aldrin 0.003 04/10/12 MR SW8081ug/LND b-BHC 0.04 04/10/12 MR SW8081ug/LND Chlordane 0.05 04/10/12 MR SW8081ug/LND d-BHC 0.04 04/10/12 MR SW8081ug/L

Page 2 of 24 Ver 1

MW-1




ND Dieldrin 0.004 04/10/12 MR SW8081ug/LND Endosulfan I 0.1 04/10/12 MR SW8081ug/LND Endosulfan II 0.1 04/10/12 MR SW8081ug/LND Endosulfan Sulfate 0.1 04/10/12 MR SW8081ug/LND Endrin 0.01 04/10/12 MR SW8081ug/LND Endrin Aldehyde 0.1 04/10/12 MR SW8081ug/LND Endrin ketone 0.1 04/10/12 MR SW8081ug/LND g-BHC (Lindane) 0.05 04/10/12 MR SW8081ug/LND Heptachlor 0.01 04/10/12 MR SW8081ug/LND Heptachlor epoxide 0.01 04/10/12 MR SW8081ug/LND Methoxychlor 0.2 04/10/12 MR SW8081ug/LND Toxaphene 1.0 04/10/12 MR SW8081ug/L

QA/QC Surrogates44 %DCBP (Surrogate Rec) 04/10/12 MR 30 - 150 %%

75 %TCMX (Surrogate Rec) 04/10/12 MR 30 - 150 %%

VolatilesND 1,1,1,2-Tetrachloroethane 1.0 04/09/12 H/T SW8260ug/LND 1,1,1-Trichloroethane 1.0 04/09/12 H/T SW8260ug/LND 1,1,2,2-Tetrachloroethane 0.50 04/09/12 H/T SW8260ug/LND 1,1,2-Trichloroethane 1.0 04/09/12 H/T SW8260ug/LND 1,1-Dichloroethane 1.0 04/09/12 H/T SW8260ug/LND 1,1-Dichloroethene 1.0 04/09/12 H/T SW8260ug/LND 1,1-Dichloropropene 1.0 04/09/12 H/T SW8260ug/LND 1,2,3-Trichlorobenzene 1.0 04/09/12 H/T SW8260ug/LND 1,2,3-Trichloropropane 1.0 04/09/12 H/T SW8260ug/LND 1,2,4-Trichlorobenzene 1.0 04/09/12 H/T SW8260ug/L 1,1P

ND 1,2,4-Trimethylbenzene 1.0 04/09/12 H/T SW8260ug/LND 1,2-Dibromo-3-chloropropane 1.0 04/09/12 H/T SW8260ug/LND 1,2-Dichlorobenzene 1.0 04/09/12 H/T SW8260ug/LND 1,2-Dichloroethane 0.60 04/09/12 H/T SW8260ug/LND 1,2-Dichloropropane 1.0 04/09/12 H/T SW8260ug/LND 1,3,5-Trimethylbenzene 1.0 04/09/12 H/T SW8260ug/LND 1,3-Dichlorobenzene 1.0 04/09/12 H/T SW8260ug/LND 1,3-Dichloropropane 1.0 04/09/12 H/T SW8260ug/LND 1,4-Dichlorobenzene 1.0 04/09/12 H/T SW8260ug/LND 2,2-Dichloropropane 1.0 04/09/12 H/T SW8260ug/LND 2-Chlorotoluene 1.0 04/09/12 H/T SW8260ug/LND 2-Hexanone 5.0 04/09/12 H/T SW8260ug/LND 2-Isopropyltoluene 1.0 04/09/12 H/T SW8260ug/L 1

ND 4-Chlorotoluene 1.0 04/09/12 H/T SW8260ug/LND 4-Methyl-2-pentanone 5.0 04/09/12 H/T SW8260ug/LND Acetone 25 04/09/12 H/T SW8260ug/LND Acrylonitrile 5.0 04/09/12 H/T SW8260ug/LND Benzene 0.70 04/09/12 H/T SW8260ug/LND Bromobenzene 1.0 04/09/12 H/T SW8260ug/L 1,1O

ND Bromochloromethane 1.0 04/09/12 H/T SW8260ug/LND Bromodichloromethane 0.50 04/09/12 H/T SW8260ug/LND Bromoform 1.0 04/09/12 H/T SW8260ug/LND Bromomethane 1.0 04/09/12 H/T SW8260ug/LND Carbon Disulfide 5.0 04/09/12 H/T SW8260ug/L

Page 3 of 24 Ver 1

MW-1




ND Carbon tetrachloride 1.0 04/09/12 H/T SW8260ug/LND Chlorobenzene 1.0 04/09/12 H/T SW8260ug/LND Chloroethane 1.0 04/09/12 H/T SW8260ug/LND Chloroform 1.0 04/09/12 H/T SW8260ug/LND Chloromethane 1.0 04/09/12 H/T SW8260ug/LND cis-1,2-Dichloroethene 1.0 04/09/12 H/T SW8260ug/LND cis-1,3-Dichloropropene 0.50 04/09/12 H/T SW8260ug/LND Dibromochloromethane 0.50 04/09/12 H/T SW8260ug/LND Dibromoethane 1.0 04/09/12 H/T SW8260ug/LND Dibromomethane 1.0 04/09/12 H/T SW8260ug/LND Dichlorodifluoromethane 1.0 04/09/12 H/T SW8260ug/LND Ethylbenzene 1.0 04/09/12 H/T SW8260ug/LND Hexachlorobutadiene 0.40 04/09/12 H/T SW8260ug/LND Isopropylbenzene 1.0 04/09/12 H/T SW8260ug/LND m&p-Xylene 1.0 04/09/12 H/T SW8260ug/LND Methyl ethyl ketone 5.0 04/09/12 H/T SW8260ug/LND Methyl t-butyl ether (MTBE) 1.0 04/09/12 H/T SW8260ug/LND Methylene chloride 1.0 04/09/12 H/T SW8260ug/LND Naphthalene 1.0 04/09/12 H/T SW8260ug/L 1,1P

ND n-Butylbenzene 1.0 04/09/12 H/T SW8260ug/LND n-Propylbenzene 1.0 04/09/12 H/T SW8260ug/LND o-Xylene 1.0 04/09/12 H/T SW8260ug/LND p-Isopropyltoluene 1.0 04/09/12 H/T SW8260ug/LND sec-Butylbenzene 1.0 04/09/12 H/T SW8260ug/LND Styrene 1.0 04/09/12 H/T SW8260ug/LND tert-Butylbenzene 1.0 04/09/12 H/T SW8260ug/LND Tetrachloroethene 1.0 04/09/12 H/T SW8260ug/LND Tetrahydrofuran (THF) 5.0 04/09/12 H/T SW8260ug/L 1

ND Toluene 1.0 04/09/12 H/T SW8260ug/LND Total Xylenes 1.0 04/09/12 H/T SW8260ug/LND trans-1,2-Dichloroethene 1.0 04/09/12 H/T SW8260ug/LND trans-1,3-Dichloropropene 0.50 04/09/12 H/T SW8260ug/LND trans-1,4-dichloro-2-butene 5.0 04/09/12 H/T SW8260ug/LND Trichloroethene 1.0 04/09/12 H/T SW8260ug/LND Trichlorofluoromethane 1.0 04/09/12 H/T SW8260ug/LND Trichlorotrifluoroethane 1.0 04/09/12 H/T SW8260ug/L 1

ND Vinyl chloride 1.0 04/09/12 H/T SW8260ug/L

QA/QC Surrogates98 % 1,2-dichlorobenzene-d4 04/09/12 H/T 70 - 130 %%

89 % Bromofluorobenzene 04/09/12 H/T 70 - 130 %%

102 % Dibromofluoromethane 04/09/12 H/T 70 - 130 %%

101 % Toluene-d8 04/09/12 H/T 70 - 130 %%

SemivolatilesND 1,2,4-Trichlorobenzene 5.0 04/07/12 DD SW8270ug/LND 1,2-Dichlorobenzene 5.0 04/07/12 DD SW8270ug/LND 1,3-Dichlorobenzene 5.0 04/07/12 DD SW8270ug/LND 1,4-Dichlorobenzene 5.0 04/07/12 DD SW8270ug/LND 2,4,5-Trichlorophenol 10 04/07/12 DD SW8270ug/LND 2,4,6-Trichlorophenol 10 04/07/12 DD SW8270ug/LND 2,4-Dichlorophenol 10 04/07/12 DD SW8270ug/L

Page 4 of 24 Ver 1

MW-1




ND 2,4-Dimethylphenol 10 04/07/12 DD SW8270ug/LND 2,4-Dinitrophenol 50 04/07/12 DD SW8270ug/LND 2,4-Dinitrotoluene 5.0 04/07/12 DD SW8270ug/LND 2,6-Dinitrotoluene 5.0 04/07/12 DD SW8270ug/LND 2-Chloronaphthalene 5.0 04/07/12 DD SW8270ug/LND 2-Chlorophenol 10 04/07/12 DD SW8270ug/LND 2-Methylnaphthalene 5.0 04/07/12 DD SW8270ug/LND 2-Methylphenol (o-cresol) 10 04/07/12 DD SW8270ug/LND 2-Nitroaniline 50 04/07/12 DD SW8270ug/LND 2-Nitrophenol 10 04/07/12 DD SW8270ug/LND 3&4-Methylphenol (m&p-cresol) 10 04/07/12 DD SW8270ug/LND 3,3'-Dichlorobenzidine 50 04/07/12 DD SW8270ug/LND 3-Nitroaniline 50 04/07/12 DD SW8270ug/LND 4,6-Dinitro-2-methylphenol 50 04/07/12 DD SW8270ug/LND 4-Bromophenyl phenyl ether 5.0 04/07/12 DD SW8270ug/LND 4-Chloro-3-methylphenol 20 04/07/12 DD SW8270ug/LND 4-Chloroaniline 20 04/07/12 DD SW8270ug/LND 4-Chlorophenyl phenyl ether 5.0 04/07/12 DD SW8270ug/LND 4-Nitroaniline 20 04/07/12 DD SW8270ug/LND 4-Nitrophenol 50 04/07/12 DD SW8270ug/LND Acetophenone 5.0 04/07/12 DD SW8270ug/LND Aniline 10 04/07/12 DD SW8270ug/L 1,1O

ND Anthracene 5.0 04/07/12 DD SW8270ug/LND Azobenzene 5.0 04/07/12 DD SW8270ug/L 1

ND Benzidine 50 04/07/12 DD SW8270ug/LND Benzoic acid 50 04/07/12 DD SW8270ug/L 1,1P

ND Benzyl butyl phthalate 5.0 04/07/12 DD SW8270ug/LND Bis(2-chloroethoxy)methane 5.0 04/07/12 DD SW8270ug/LND Bis(2-chloroethyl)ether 5.0 04/07/12 DD SW8270ug/LND Bis(2-chloroisopropyl)ether 5.0 04/07/12 DD SW8270ug/LND Carbazole 5.0 04/07/12 DD SW8270ug/LND Dibenzofuran 5.0 04/07/12 DD SW8270ug/LND Diethyl phthalate 5.0 04/07/12 DD SW8270ug/LND Dimethylphthalate 5.0 04/07/12 DD SW8270ug/LND Di-n-butylphthalate 5.0 04/07/12 DD SW8270ug/LND Di-n-octylphthalate 5.0 04/07/12 DD SW8270ug/LND Fluoranthene 5.0 04/07/12 DD SW8270ug/LND Fluorene 5.0 04/07/12 DD SW8270ug/LND Hexachlorobutadiene 5.0 04/07/12 DD SW8270ug/LND Hexachlorocyclopentadiene 5.0 04/07/12 DD SW8270ug/LND Isophorone 5.0 04/07/12 DD SW8270ug/LND Naphthalene 5.0 04/07/12 DD SW8270ug/LND Nitrobenzene 5.0 04/07/12 DD SW8270ug/LND N-Nitrosodimethylamine 5.0 04/07/12 DD SW8270ug/LND N-Nitrosodi-n-propylamine 5.0 04/07/12 DD SW8270ug/LND N-Nitrosodiphenylamine 5.0 04/07/12 DD SW8270ug/LND Phenol 10 04/07/12 DD SW8270ug/LND Pyrene 5.0 04/07/12 DD SW8270ug/LND Pyridine 5.0 04/07/12 DD SW8270ug/L

QA/QC Surrogates

Page 5 of 24 Ver 1

MW-1




107 % 2,4,6-Tribromophenol 04/07/12 DD 15 - 130 %%


72 % 2-Fluorophenol 04/07/12 DD 15 - 130 %%


74 % Phenol-d5 04/07/12 DD 15 - 130 %%

100 % Terphenyl-d14 04/07/12 DD 15 - 130 %%

SemivolatilesND 1,2,4,5-Tetrachlorobenzene 1.6 04/06/12 DD SW8270 (SIM)ug/LND Acenaphthene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Acenaphthylene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Benz(a)anthracene 0.040 04/06/12 DD SW8270 (SIM)ug/LND Benzo(a)pyrene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Benzo(b)fluoranthene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Benzo(ghi)perylene 3.0 04/06/12 DD SW8270 (SIM)ug/LND Benzo(k)fluoranthene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Bis(2-ethylhexyl)phthalate 1.6 04/06/12 DD SW8270 (SIM)ug/LND Chrysene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Dibenz(a,h)anthracene 0.010 04/06/12 DD SW8270 (SIM)ug/LND Hexachlorobenzene 0.060 04/06/12 DD SW8270 (SIM)ug/LND Hexachloroethane 2.4 04/06/12 DD SW8270 (SIM)ug/LND Indeno(1,2,3-cd)pyrene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Pentachloronitrobenzene 0.10 04/06/12 DD SW8270 (SIM)ug/L 1,1O

ND Pentachlorophenol 0.80 04/06/12 DD SW8270 (SIM)ug/L0.08 Phenanthrene 0.050 04/06/12 DD SW8270 (SIM)ug/L



72 % 2-Fluorophenol 04/06/12 DD 15 - 130 %%


74 % Phenol-d5 04/06/12 DD 15 - 130 %%

100 % Terphenyl-d14 04/06/12 DD 15 - 130 %%

Comments:

* For Pesticides, due to matrix interference from non target compounds in the sample, an elevated RL was reported.



April 12, 2012



Reviewed and Released by: Johanna Harrington, Project Manage


Page 6 of 24 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

ESPL

72 Hour

212117-2

04/04/12

SW

see "By" below

Laboratory Data

MW-2

Phoenix ID: BB62842

04/05/12

12:40

16:35




Time

Date Time



SDG ID: GBB62841

Client ID:


1.02 Aluminum (Dissolved) 0.01 04/06/12 EK 6010mg/L< 0.005 Antimony (Dissolved) 0.005 04/09/12 EK 6010mg/L< 0.004 Arsenic (Dissolved) 0.004 04/06/12 EK 6010mg/L0.073 Barium (Dissolved) 0.002 04/06/12 EK 6010mg/L< 0.001 Beryllium (Dissolved) 0.001 04/06/12 EK 6010mg/L24.4 Calcium (Dissolved) 0.01 04/06/12 EK 6010mg/L< 0.001 Cadmium (Dissolved) 0.001 04/06/12 EK 6010mg/L0.004 Chromium (Dissolved) 0.001 04/06/12 EK 6010mg/L0.001 Cobalt (Dissolved) 0.001 04/06/12 EK 6010mg/L0.018 Copper (Dissolved) 0.005 04/06/12 EK 6010mg/LCompleted Dissolved Metals Preparation 04/05/12 AG SW846-3005

0.935 Iron (Dissolved) 0.011 04/06/12 EK 6010mg/L0.005 Lead (Dissolved) 0.002 04/06/12 EK 6010mg/L6.71 Magnesium (Dissolved) 0.01 04/06/12 EK 6010mg/L1.24 Manganese (Dissolved) 0.001 04/06/12 EK 6010mg/L< 0.0002 Mercury (Dissolved) 0.0002 04/06/12 RS 7470/E245.1mg/L0.008 Nickel (Dissolved) 0.001 04/06/12 EK 6010mg/L5.0 Potassium (Dissolved) 0.1 04/06/12 EK 6010mg/L< 0.011 Selenium (Dissolved) 0.011 04/06/12 EK 6010mg/L< 0.001 Silver (Dissolved) 0.001 04/06/12 EK 6010mg/L78.5 Sodium (Dissolved) 1.1 04/09/12 EK 6010mg/L< 0.002 Thallium (Dissolved) 0.002 04/09/12 RS 7010/279.2mg/L0.002 Vanadium (Dissolved) 0.002 04/06/12 EK 6010mg/L0.024 Zinc (Dissolved) 0.002 04/06/12 EK 6010mg/LCompleted Filtration 04/05/12 AG 0.45um Filter



Page 7 of 24 Ver 1

MW-2







ND Bromochloromethane 1.0 04/06/12 H/T SW8260ug/LND Bromodichloromethane 0.50 04/06/12 H/T SW8260ug/LND Bromoform 1.0 04/06/12 H/T SW8260ug/LND Bromomethane 1.0 04/06/12 H/T SW8260ug/LND Carbon Disulfide 5.0 04/06/12 H/T SW8260ug/LND Carbon tetrachloride 1.0 04/06/12 H/T SW8260ug/LND Chlorobenzene 1.0 04/06/12 H/T SW8260ug/LND Chloroethane 1.0 04/06/12 H/T SW8260ug/LND Chloroform 1.0 04/06/12 H/T SW8260ug/LND Chloromethane 1.0 04/06/12 H/T SW8260ug/LND cis-1,2-Dichloroethene 1.0 04/06/12 H/T SW8260ug/LND cis-1,3-Dichloropropene 0.50 04/06/12 H/T SW8260ug/LND Dibromochloromethane 0.50 04/06/12 H/T SW8260ug/LND Dibromoethane 1.0 04/06/12 H/T SW8260ug/LND Dibromomethane 1.0 04/06/12 H/T SW8260ug/LND Dichlorodifluoromethane 1.0 04/06/12 H/T SW8260ug/LND Ethylbenzene 1.0 04/06/12 H/T SW8260ug/LND Hexachlorobutadiene 0.40 04/06/12 H/T SW8260ug/LND Isopropylbenzene 1.0 04/06/12 H/T SW8260ug/LND m&p-Xylene 1.0 04/06/12 H/T SW8260ug/L

Page 8 of 24 Ver 1

MW-2




9.1 Methyl ethyl ketone 5.0 04/06/12 H/T SW8260ug/LND Methyl t-butyl ether (MTBE) 1.0 04/06/12 H/T SW8260ug/LND Methylene chloride 1.0 04/06/12 H/T SW8260ug/LND Naphthalene 1.0 04/06/12 H/T SW8260ug/L 1,1P







100 % Toluene-d8 04/06/12 H/T 70 - 130 %%

SemivolatilesND 1,2,4-Trichlorobenzene 6.3 04/07/12 DD SW8270ug/LND 1,2-Dichlorobenzene 6.3 04/07/12 DD SW8270ug/LND 1,3-Dichlorobenzene 6.3 04/07/12 DD SW8270ug/LND 1,4-Dichlorobenzene 6.3 04/07/12 DD SW8270ug/LND 2,4,5-Trichlorophenol 13 04/07/12 DD SW8270ug/LND 2,4,6-Trichlorophenol 13 04/07/12 DD SW8270ug/LND 2,4-Dichlorophenol 13 04/07/12 DD SW8270ug/LND 2,4-Dimethylphenol 13 04/07/12 DD SW8270ug/LND 2,4-Dinitrophenol 63 04/07/12 DD SW8270ug/LND 2,4-Dinitrotoluene 6.3 04/07/12 DD SW8270ug/LND 2,6-Dinitrotoluene 6.3 04/07/12 DD SW8270ug/LND 2-Chloronaphthalene 6.3 04/07/12 DD SW8270ug/LND 2-Chlorophenol 13 04/07/12 DD SW8270ug/LND 2-Methylnaphthalene 6.3 04/07/12 DD SW8270ug/LND 2-Methylphenol (o-cresol) 13 04/07/12 DD SW8270ug/LND 2-Nitroaniline 63 04/07/12 DD SW8270ug/LND 2-Nitrophenol 13 04/07/12 DD SW8270ug/LND 3&4-Methylphenol (m&p-cresol) 13 04/07/12 DD SW8270ug/LND 3,3'-Dichlorobenzidine 63 04/07/12 DD SW8270ug/LND 3-Nitroaniline 63 04/07/12 DD SW8270ug/LND 4,6-Dinitro-2-methylphenol 63 04/07/12 DD SW8270ug/LND 4-Bromophenyl phenyl ether 6.3 04/07/12 DD SW8270ug/L

Page 9 of 24 Ver 1

MW-2




ND 4-Chloro-3-methylphenol 25 04/07/12 DD SW8270ug/LND 4-Chloroaniline 25 04/07/12 DD SW8270ug/LND 4-Chlorophenyl phenyl ether 6.3 04/07/12 DD SW8270ug/LND 4-Nitroaniline 25 04/07/12 DD SW8270ug/LND 4-Nitrophenol 63 04/07/12 DD SW8270ug/LND Acetophenone 6.3 04/07/12 DD SW8270ug/LND Aniline 13 04/07/12 DD SW8270ug/L 1,1O






46 % 2-Fluorophenol 04/07/12 DD 15 - 130 %%


51 % Phenol-d5 04/07/12 DD 15 - 130 %%

117 % Terphenyl-d14 04/07/12 DD 15 - 130 %%

SemivolatilesND 1,2,4,5-Tetrachlorobenzene 2.0 04/06/12 DD SW8270 (SIM)ug/LND Acenaphthene 0.063 04/06/12 DD SW8270 (SIM)ug/L0.075 Acenaphthylene 0.063 04/06/12 DD SW8270 (SIM)ug/LND Benz(a)anthracene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Benzo(a)pyrene 0.063 04/06/12 DD SW8270 (SIM)ug/LND Benzo(b)fluoranthene 0.063 04/06/12 DD SW8270 (SIM)ug/LND Benzo(ghi)perylene 3.8 04/06/12 DD SW8270 (SIM)ug/LND Benzo(k)fluoranthene 0.063 04/06/12 DD SW8270 (SIM)ug/L

Page 10 of 24 Ver 1

MW-2




ND Bis(2-ethylhexyl)phthalate 2.0 04/06/12 DD SW8270 (SIM)ug/LND Chrysene 0.063 04/06/12 DD SW8270 (SIM)ug/LND Dibenz(a,h)anthracene 0.013 04/06/12 DD SW8270 (SIM)ug/LND Hexachlorobenzene 0.075 04/06/12 DD SW8270 (SIM)ug/LND Hexachloroethane 3.0 04/06/12 DD SW8270 (SIM)ug/LND Indeno(1,2,3-cd)pyrene 0.063 04/06/12 DD SW8270 (SIM)ug/LND Pentachloronitrobenzene 0.13 04/06/12 DD SW8270 (SIM)ug/L 1,1O

ND Pentachlorophenol 1.0 04/06/12 DD SW8270 (SIM)ug/L0.063 Phenanthrene 0.063 04/06/12 DD SW8270 (SIM)ug/L



46 % 2-Fluorophenol 04/06/12 DD 15 - 130 %%


51 % Phenol-d5 04/06/12 DD 15 - 130 %%

117 % Terphenyl-d14 04/06/12 DD 15 - 130 %%

Comments:



April 12, 2012





Page 11 of 24 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

ESPL

72 Hour

212117-2

04/04/12

SW

see "By" below

Laboratory Data

MW-3

Phoenix ID: BB62843

04/05/12

15:25

16:35




Time

Date Time



SDG ID: GBB62841

Client ID:


14.1 Aluminum 0.010 04/07/12 LK 6010mg/L1.25 Aluminum (Dissolved) 0.01 04/06/12 EK 6010mg/L< 0.005 Antimony (Dissolved) 0.005 04/06/12 EK 6010mg/L< 0.005 Antimony 0.005 04/07/12 LK 6010mg/L0.004 Arsenic 0.004 04/07/12 LK 6010mg/L< 0.004 Arsenic (Dissolved) 0.004 04/06/12 EK 6010mg/L0.411 Barium 0.002 04/07/12 LK 6010mg/L0.182 Barium (Dissolved) 0.002 04/06/12 EK 6010mg/L0.001 Beryllium 0.001 04/07/12 LK 6010mg/L< 0.001 Beryllium (Dissolved) 0.001 04/06/12 EK 6010mg/L44.9 Calcium 0.010 04/07/12 LK 6010mg/L< 0.001 Cadmium 0.001 04/07/12 LK 6010mg/L44.0 Calcium (Dissolved) 0.01 04/06/12 EK 6010mg/L< 0.001 Cadmium (Dissolved) 0.001 04/06/12 EK 6010mg/L0.043 Chromium 0.001 04/07/12 LK 6010mg/L0.008 Chromium (Dissolved) 0.001 04/06/12 EK 6010mg/L0.017 Cobalt 0.002 04/07/12 LK 6010mg/L0.065 Copper 0.005 04/07/12 LK 6010mg/L0.002 Cobalt (Dissolved) 0.001 04/06/12 EK 6010mg/L0.018 Copper (Dissolved) 0.005 04/06/12 EK 6010mg/LCompleted Dissolved Metals Preparation 04/05/12 AG SW846-3005

1.65 Iron (Dissolved) 0.011 04/06/12 EK 6010mg/L19.7 Iron 0.010 04/07/12 LK 6010mg/L0.007 Lead (Dissolved) 0.002 04/06/12 EK 6010mg/L0.039 Lead 0.002 04/07/12 LK 6010mg/L12.7 Magnesium (Dissolved) 0.01 04/06/12 EK 6010mg/L0.415 Manganese (Dissolved) 0.001 04/06/12 EK 6010mg/L18.7 Magnesium 0.01 04/07/12 LK 6010mg/L

Page 12 of 24 Ver 1

MW-3




2.65 Manganese 0.010 04/09/12 EK 6010mg/L< 0.0002 Mercury (Dissolved) 0.0002 04/06/12 RS 7470/E245.1mg/L0.0009 Mercury 0.0002 04/06/12 RS 7470/E245.1mg/L0.017 Nickel (Dissolved) 0.001 04/06/12 EK 6010mg/L0.118 Nickel 0.001 04/07/12 LK 6010mg/L10.8 Potassium (Dissolved) 0.1 04/06/12 EK 6010mg/L14.1 Potassium 0.1 04/07/12 LK 6010mg/L< 0.011 Selenium (Dissolved) 0.011 04/06/12 EK 6010mg/L< 0.010 Selenium 0.010 04/07/12 LK 6010mg/L< 0.001 Silver 0.001 04/07/12 LK 6010mg/L< 0.001 Silver (Dissolved) 0.001 04/06/12 EK 6010mg/L139 Sodium (Dissolved) 1.1 04/09/12 EK 6010mg/L131 Sodium 1.0 04/09/12 EK 6010mg/L< 0.002 Thallium (Dissolved) 0.002 04/09/12 RS 7010/279.2mg/L< 0.002 Thallium 0.002 04/09/12 RS SW7010/200.9mg/LCompleted Total Metals Digestion 04/05/12 AG

0.005 Vanadium (Dissolved) 0.002 04/06/12 EK 6010mg/L0.033 Vanadium 0.002 04/07/12 LK 6010mg/L0.020 Zinc (Dissolved) 0.002 04/06/12 EK 6010mg/L0.100 Zinc 0.002 04/07/12 LK 6010mg/LCompleted Filtration 04/05/12 AG 0.45um Filter






Polychlorinated BiphenylsND PCB-1016 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1221 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1232 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1242 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1248 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1254 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1260 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1262 0.09 04/10/12 MH 608/ 8082ug/LND PCB-1268 0.09 04/10/12 MH 608/ 8082ug/L


67 % TCMX 04/10/12 MH 30 - 150 %%

PesticidesND 4,4' -DDD 0.01 04/10/12 MR SW8081ug/LND 4,4' -DDE 0.01 04/10/12 MR SW8081ug/LND 4,4' -DDT 0.01 04/10/12 MR SW8081ug/LND a-BHC 0.01 04/10/12 MR SW8081ug/LND Alachlor 0.5 04/10/12 MR SW8081ug/L 1

ND Aldrin 0.01 04/10/12 MR SW8081ug/LND b-BHC 0.01 04/10/12 MR SW8081ug/LND Chlordane 0.05 04/10/12 MR SW8081ug/LND d-BHC 0.04 04/10/12 MR SW8081ug/L

Page 13 of 24 Ver 1

MW-3




ND Dieldrin 0.004 04/10/12 MR SW8081ug/LND Endosulfan I 0.1 04/10/12 MR SW8081ug/LND Endosulfan II 0.1 04/10/12 MR SW8081ug/LND Endosulfan Sulfate 0.1 04/10/12 MR SW8081ug/LND Endrin 0.01 04/10/12 MR SW8081ug/LND Endrin Aldehyde 5 04/10/12 MR SW8081ug/LND Endrin ketone 5 04/10/12 MR SW8081ug/LND g-BHC (Lindane) 0.05 04/10/12 MR SW8081ug/LND Heptachlor 0.01 04/10/12 MR SW8081ug/LND Heptachlor epoxide 0.01 04/10/12 MR SW8081ug/LND Methoxychlor 35 04/10/12 MR SW8081ug/LND Toxaphene 1.0 04/10/12 MR SW8081ug/L






ND Bromochloromethane 1.0 04/06/12 H/T SW8260ug/LND Bromodichloromethane 0.50 04/06/12 H/T SW8260ug/LND Bromoform 1.0 04/06/12 H/T SW8260ug/LND Bromomethane 1.0 04/06/12 H/T SW8260ug/LND Carbon Disulfide 5.0 04/06/12 H/T SW8260ug/L

Page 14 of 24 Ver 1

MW-3




ND Carbon tetrachloride 1.0 04/06/12 H/T SW8260ug/LND Chlorobenzene 1.0 04/06/12 H/T SW8260ug/LND Chloroethane 1.0 04/06/12 H/T SW8260ug/L1.4 Chloroform 1.0 04/06/12 H/T SW8260ug/LND Chloromethane 1.0 04/06/12 H/T SW8260ug/LND cis-1,2-Dichloroethene 1.0 04/06/12 H/T SW8260ug/LND cis-1,3-Dichloropropene 0.50 04/06/12 H/T SW8260ug/LND Dibromochloromethane 0.50 04/06/12 H/T SW8260ug/LND Dibromoethane 1.0 04/06/12 H/T SW8260ug/LND Dibromomethane 1.0 04/06/12 H/T SW8260ug/LND Dichlorodifluoromethane 1.0 04/06/12 H/T SW8260ug/LND Ethylbenzene 1.0 04/06/12 H/T SW8260ug/LND Hexachlorobutadiene 0.40 04/06/12 H/T SW8260ug/LND Isopropylbenzene 1.0 04/06/12 H/T SW8260ug/LND m&p-Xylene 1.0 04/06/12 H/T SW8260ug/LND Methyl ethyl ketone 5.0 04/06/12 H/T SW8260ug/LND Methyl t-butyl ether (MTBE) 1.0 04/06/12 H/T SW8260ug/LND Methylene chloride 1.0 04/06/12 H/T SW8260ug/LND Naphthalene 1.0 04/06/12 H/T SW8260ug/L 1,1P







101 % Toluene-d8 04/06/12 H/T 70 - 130 %%

SemivolatilesND 1,2,4-Trichlorobenzene 5.0 04/07/12 DD SW8270ug/LND 1,2-Dichlorobenzene 5.0 04/07/12 DD SW8270ug/LND 1,3-Dichlorobenzene 5.0 04/07/12 DD SW8270ug/LND 1,4-Dichlorobenzene 5.0 04/07/12 DD SW8270ug/LND 2,4,5-Trichlorophenol 10 04/07/12 DD SW8270ug/LND 2,4,6-Trichlorophenol 10 04/07/12 DD SW8270ug/LND 2,4-Dichlorophenol 10 04/07/12 DD SW8270ug/L

Page 15 of 24 Ver 1

MW-3




ND 2,4-Dimethylphenol 10 04/07/12 DD SW8270ug/LND 2,4-Dinitrophenol 50 04/07/12 DD SW8270ug/LND 2,4-Dinitrotoluene 5.0 04/07/12 DD SW8270ug/LND 2,6-Dinitrotoluene 5.0 04/07/12 DD SW8270ug/LND 2-Chloronaphthalene 5.0 04/07/12 DD SW8270ug/LND 2-Chlorophenol 10 04/07/12 DD SW8270ug/LND 2-Methylnaphthalene 5.0 04/07/12 DD SW8270ug/LND 2-Methylphenol (o-cresol) 10 04/07/12 DD SW8270ug/LND 2-Nitroaniline 50 04/07/12 DD SW8270ug/LND 2-Nitrophenol 10 04/07/12 DD SW8270ug/LND 3&4-Methylphenol (m&p-cresol) 10 04/07/12 DD SW8270ug/LND 3,3'-Dichlorobenzidine 50 04/07/12 DD SW8270ug/LND 3-Nitroaniline 50 04/07/12 DD SW8270ug/LND 4,6-Dinitro-2-methylphenol 50 04/07/12 DD SW8270ug/LND 4-Bromophenyl phenyl ether 5.0 04/07/12 DD SW8270ug/LND 4-Chloro-3-methylphenol 20 04/07/12 DD SW8270ug/LND 4-Chloroaniline 20 04/07/12 DD SW8270ug/LND 4-Chlorophenyl phenyl ether 5.0 04/07/12 DD SW8270ug/LND 4-Nitroaniline 20 04/07/12 DD SW8270ug/LND 4-Nitrophenol 50 04/07/12 DD SW8270ug/LND Acetophenone 5.0 04/07/12 DD SW8270ug/LND Aniline 10 04/07/12 DD SW8270ug/L 1,1O




QA/QC Surrogates

Page 16 of 24 Ver 1

MW-3




78 % 2,4,6-Tribromophenol 04/07/12 DD 15 - 130 %%


57 % 2-Fluorophenol 04/07/12 DD 15 - 130 %%


<5 % Phenol-d5 04/07/12 DD 15 - 130 %% 3

21 % Terphenyl-d14 04/07/12 DD 15 - 130 %%

SemivolatilesND 1,2,4,5-Tetrachlorobenzene 1.6 04/06/12 DD SW8270 (SIM)ug/LND Acenaphthene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Acenaphthylene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Benz(a)anthracene 0.040 04/06/12 DD SW8270 (SIM)ug/LND Benzo(a)pyrene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Benzo(b)fluoranthene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Benzo(ghi)perylene 3.0 04/06/12 DD SW8270 (SIM)ug/LND Benzo(k)fluoranthene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Bis(2-ethylhexyl)phthalate 1.6 04/06/12 DD SW8270 (SIM)ug/LND Chrysene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Dibenz(a,h)anthracene 0.010 04/06/12 DD SW8270 (SIM)ug/LND Hexachlorobenzene 0.060 04/06/12 DD SW8270 (SIM)ug/LND Hexachloroethane 2.4 04/06/12 DD SW8270 (SIM)ug/LND Indeno(1,2,3-cd)pyrene 0.050 04/06/12 DD SW8270 (SIM)ug/LND Pentachloronitrobenzene 0.10 04/06/12 DD SW8270 (SIM)ug/L 1,1O

2.4 Pentachlorophenol 0.80 04/06/12 DD SW8270 (SIM)ug/LND Phenanthrene 0.050 04/06/12 DD SW8270 (SIM)ug/L



57 % 2-Fluorophenol 04/06/12 DD 15 - 130 %%


<5 % Phenol-d5 04/06/12 DD 15 - 130 %% 3

21 % Terphenyl-d14 04/06/12 DD 15 - 130 %%

Page 17 of 24 Ver 1

MW-3




Comments:

* Poor surrogate recovery was observed for semivolatiles. The other surrogates associated with this sample were within QA/QC criteria. No further action was necessary.

* For Pesticides, due to matrix interference from non target compounds in the sample, an elevated RL was reported.



April 12, 2012

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.1P = This parameter is pending certification by NY NELAC for this matrix.1O = This parameter is not certified by NY NELAC for this matrix.3 = This parameter exceeds laboratory specified limits.




Page 18 of 24 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

ESPL

72 Hour

212117-2

04/04/12

SW

see "By" below

Laboratory Data

F BLANK

Phoenix ID: BB62844

04/05/12

12:55

16:35




Time

Date Time



SDG ID: GBB62841

Client ID:




ND 4-Chlorotoluene 1.0 04/06/12 H/T SW8260ug/LND 4-Methyl-2-pentanone 5.0 04/06/12 H/T SW8260ug/LND Acetone 25 04/06/12 H/T SW8260ug/L

Page 19 of 24 Ver 1

F BLANK




ND Acrylonitrile 5.0 04/06/12 H/T SW8260ug/LND Benzene 0.70 04/06/12 H/T SW8260ug/LND Bromobenzene 1.0 04/06/12 H/T SW8260ug/L 1,1O

ND Bromochloromethane 1.0 04/06/12 H/T SW8260ug/LND Bromodichloromethane 0.50 04/06/12 H/T SW8260ug/LND Bromoform 1.0 04/06/12 H/T SW8260ug/LND Bromomethane 1.0 04/06/12 H/T SW8260ug/LND Carbon Disulfide 5.0 04/06/12 H/T SW8260ug/LND Carbon tetrachloride 1.0 04/06/12 H/T SW8260ug/LND Chlorobenzene 1.0 04/06/12 H/T SW8260ug/LND Chloroethane 1.0 04/06/12 H/T SW8260ug/LND Chloroform 1.0 04/06/12 H/T SW8260ug/LND Chloromethane 1.0 04/06/12 H/T SW8260ug/LND cis-1,2-Dichloroethene 1.0 04/06/12 H/T SW8260ug/LND cis-1,3-Dichloropropene 0.50 04/06/12 H/T SW8260ug/LND Dibromochloromethane 0.50 04/06/12 H/T SW8260ug/LND Dibromoethane 1.0 04/06/12 H/T SW8260ug/LND Dibromomethane 1.0 04/06/12 H/T SW8260ug/LND Dichlorodifluoromethane 1.0 04/06/12 H/T SW8260ug/LND Ethylbenzene 1.0 04/06/12 H/T SW8260ug/LND Hexachlorobutadiene 0.40 04/06/12 H/T SW8260ug/LND Isopropylbenzene 1.0 04/06/12 H/T SW8260ug/LND m&p-Xylene 1.0 04/06/12 H/T SW8260ug/LND Methyl ethyl ketone 5.0 04/06/12 H/T SW8260ug/LND Methyl t-butyl ether (MTBE) 1.0 04/06/12 H/T SW8260ug/LND Methylene chloride 1.0 04/06/12 H/T SW8260ug/LND Naphthalene 1.0 04/06/12 H/T SW8260ug/L 1,1P







99 % Toluene-d8 04/06/12 H/T 70 - 130 %%

Page 20 of 24 Ver 1

F BLANK




Comments:



April 12, 2012





Page 21 of 24 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

ESPL

72 Hour

212117-2

04/04/12

SW

see "By" below

Laboratory Data

TRIP BLANK

Phoenix ID: BB62845

04/05/12

0:00

16:35




Time

Date Time



SDG ID: GBB62841

Client ID:




ND 4-Chlorotoluene 1.0 04/06/12 H/T SW8260ug/LND 4-Methyl-2-pentanone 5.0 04/06/12 H/T SW8260ug/LND Acetone 25 04/06/12 H/T SW8260ug/L

Page 22 of 24 Ver 1

TRIP BLANK




ND Acrylonitrile 5.0 04/06/12 H/T SW8260ug/LND Benzene 0.70 04/06/12 H/T SW8260ug/LND Bromobenzene 1.0 04/06/12 H/T SW8260ug/L 1,1O

ND Bromochloromethane 1.0 04/06/12 H/T SW8260ug/LND Bromodichloromethane 0.50 04/06/12 H/T SW8260ug/LND Bromoform 1.0 04/06/12 H/T SW8260ug/LND Bromomethane 1.0 04/06/12 H/T SW8260ug/LND Carbon Disulfide 5.0 04/06/12 H/T SW8260ug/LND Carbon tetrachloride 1.0 04/06/12 H/T SW8260ug/LND Chlorobenzene 1.0 04/06/12 H/T SW8260ug/LND Chloroethane 1.0 04/06/12 H/T SW8260ug/LND Chloroform 1.0 04/06/12 H/T SW8260ug/LND Chloromethane 1.0 04/06/12 H/T SW8260ug/LND cis-1,2-Dichloroethene 1.0 04/06/12 H/T SW8260ug/LND cis-1,3-Dichloropropene 0.50 04/06/12 H/T SW8260ug/LND Dibromochloromethane 0.50 04/06/12 H/T SW8260ug/LND Dibromoethane 1.0 04/06/12 H/T SW8260ug/LND Dibromomethane 1.0 04/06/12 H/T SW8260ug/LND Dichlorodifluoromethane 1.0 04/06/12 H/T SW8260ug/LND Ethylbenzene 1.0 04/06/12 H/T SW8260ug/LND Hexachlorobutadiene 0.40 04/06/12 H/T SW8260ug/LND Isopropylbenzene 1.0 04/06/12 H/T SW8260ug/LND m&p-Xylene 1.0 04/06/12 H/T SW8260ug/LND Methyl ethyl ketone 5.0 04/06/12 H/T SW8260ug/LND Methyl t-butyl ether (MTBE) 1.0 04/06/12 H/T SW8260ug/LND Methylene chloride 1.0 04/06/12 H/T SW8260ug/LND Naphthalene 1.0 04/06/12 H/T SW8260ug/L 1,1P







98 % Toluene-d8 04/06/12 H/T 70 - 130 %%

Page 23 of 24 Ver 1

TRIP BLANK




Comments:



April 12, 2012





Page 24 of 24 Ver 1

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBB62841

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

SampleResult

DupResult

QA/QC Batch 197600, QC Sample No: BB60961 (BB62841, BB62843)112 105Thallium - Water BDL 6.5110NC 115 4.4 75 - 125 20<0.001 <0.001


ICP Metals - Aqueous98.8 97.8Aluminum 0.011 1.099.2NC 100 0.8 75 - 125 200.022 0.023

103 102Antimony BDL 1.0102NC 100 2.0 75 - 125 20<0.005 <0.005

102 101Arsenic BDL 1.0101NC 99.9 1.1 75 - 125 20<0.004 <0.004

103 103Barium BDL 0.0104NC 102 1.9 75 - 125 20<0.002 <0.002

103 102Beryllium BDL 1.0103NC 101 2.0 75 - 125 20<0.001 <0.001

103 101Cadmium BDL 2.0102NC 101 1.0 75 - 125 20<0.001 <0.001

102 97.3Calcium BDL 4.71030.60 101 2.0 75 - 125 203.20 3.18

102 101Chromium BDL 1.0103NC 101 2.0 75 - 125 20<0.001 <0.001

105 103Cobalt BDL 1.9104NC 103 1.0 75 - 125 20<0.002 <0.002

105 103Copper BDL 1.9104NC 102 1.9 75 - 125 20<0.005 <0.005

101 99.6Iron BDL 1.4101NC 99.3 1.7 75 - 125 20<0.010 <0.010

103 102Lead BDL 1.0103NC 101 2.0 75 - 125 20<0.002 <0.002

104 103Magnesium BDL 1.01030 102 1.0 75 - 125 200.82 0.82

102 101Manganese BDL 1.0102NC 100 2.0 75 - 125 20<0.001 <0.001

102 101Nickel BDL 1.0103NC 100 3.0 75 - 125 20<0.001 <0.001

108 104Potassium BDL 3.81070 103 3.8 75 - 125 200.5 0.5

98.1 97.9Selenium BDL 0.298.1NC 96.5 1.6 75 - 125 20<0.010 <0.010

99.0 97.8Silver BDL 1.298.8NC 97.0 1.8 75 - 125 20<0.001 <0.001

NC NCSodium BDL NC1111.10 105 5.6 75 - 125 209.2 9.3

102 100Vanadium BDL 2.0102NC 100 2.0 75 - 125 20<0.002 <0.002

106 105Zinc BDL 0.9105NC 103 1.9 75 - 125 20<0.01 0.009

QA/QC Batch 197764, QC Sample No: BB62580 (BB62841, BB62842, BB62843)

ICP Metals - Dissolved95.3 95.3Aluminum BDL 0.091.5NC 94.1 2.8 75 - 125 200.007 <0.01

96.5 96.5Antimony BDL 0.091.1NC 94.6 3.8 75 - 125 20<0.005 <0.005

94.7 94.6Arsenic BDL 0.189.5NC 92.8 3.6 75 - 125 20<0.004 <0.004

96.6 96.1Barium BDL 0.593.02.20 96.1 3.3 75 - 125 200.046 0.045

95.8 95.8Beryllium BDL 0.093.2NC 95.3 2.2 75 - 125 20<0.004 <0.001

92.4 93.1Cadmium BDL 0.889.2NC 91.9 3.0 75 - 125 20<0.001 <0.001

NC NCCalcium BDL NC92.00 94.5 2.7 75 - 125 2020.2 20.2

96.9 96.9Chromium BDL 0.093.2NC 96.0 3.0 75 - 125 20<0.001 <0.001

96.2 96.5Cobalt BDL 0.392.3NC 95.1 3.0 75 - 125 20<0.004 0.003

99.8 99.7Copper BDL 0.194.0NC 96.9 3.0 75 - 125 20<0.005 <0.005

93.2 93.8Iron BDL 0.689.71.00 92.5 3.1 75 - 125 200.206 0.204

96.8 97.4Lead BDL 0.694.0NC 96.6 2.7 75 - 125 20<0.002 <0.002

NC NCMagnesium BDL NC91.50.70 94.0 2.7 75 - 125 205.41 5.37

95.3 95.3Manganese BDL 0.092.30.80 95.0 2.9 75 - 125 200.264 0.262

97.9 97.9Nickel BDL 0.094.60 97.5 3.0 75 - 125 200.005 0.005

Page 1 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB62841

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

SampleResult

DupResult

102 111Potassium BDL 8.599.52.20 100 0.5 75 - 125 204.4 4.5

89.0 88.4Selenium BDL 0.783.2NC 86.6 4.0 75 - 125 20<0.011 <0.011

83.6 83.5Silver BDL 0.191.1NC 93.9 3.0 75 - 125 20<0.001 <0.001

NC NCSodium BDL NC1040.20 102 1.9 75 - 125 2047.2 47.3

95.8 95.9Vanadium BDL 0.191.8NC 94.6 3.0 75 - 125 20<0.002 <0.002

101 101Zinc BDL 0.096.75.70 99.5 2.9 75 - 125 200.018 0.017

QA/QC Batch 197805, QC Sample No: BB62834 (BB62841, BB62842, BB62843)97.8 103Mercury - Water BDL 5.2107NC 103 3.8 70 - 130 20<0.0002 <0.0002

Page 2 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBB62841

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits


Pesticides - Ground Water4,4' -DDD ND 87 83 4.7 40 - 140 20

4,4' -DDE ND 86 81 6.0 40 - 140 20

4,4' -DDT ND 92 87 5.6 40 - 140 20

a-BHC ND 83 77 7.5 40 - 140 20

a-Chlordane ND 83 78 6.2 40 - 140 20

Alachlor ND N/A N/A NC 40 - 140 20

Aldrin ND 77 72 6.7 40 - 140 20

b-BHC ND 83 78 6.2 40 - 140 20

Chlordane ND N/A N/A NC 40 - 140 20

d-BHC ND 83 78 6.2 40 - 140 20

Dieldrin ND 83 79 4.9 40 - 140 20

Endosulfan I ND 84 78 7.4 40 - 140 20

Endosulfan II ND 86 81 6.0 40 - 140 20

Endosulfan sulfate ND 84 80 4.9 40 - 140 20

Endrin ND 82 78 5.0 40 - 140 20

Endrin aldehyde ND 83 76 8.8 40 - 140 20

Endrin ketone ND 90 85 5.7 40 - 140 20

g-BHC ND 80 76 5.1 40 - 140 20

g-Chlordane ND 80 75 6.5 40 - 140 20

Heptachlor ND 90 84 6.9 40 - 140 20

Heptachlor epoxide ND 79 74 6.5 40 - 140 20

Methoxychlor ND 102 96 6.1 40 - 140 20

Toxaphene ND N/A N/A NC 40 - 140 20

% DCBP 88 93 88 5.5 30 - 150 20

% TCMX 69 80 75 6.5 30 - 150 20


Polychlorinated Biphenyls - Ground Water83 83PCB-1016 ND 0.081 81 0.0 40 - 140 20

PCB-1221 ND 40 - 140 20

PCB-1232 ND 40 - 140 20

PCB-1242 ND 40 - 140 20

PCB-1248 ND 40 - 140 20

PCB-1254 ND 40 - 140 20

82 82PCB-1260 ND 0.076 77 1.3 40 - 140 20

PCB-1262 ND 40 - 140 20

PCB-1268 ND 40 - 140 20

84 86% DCBP (Surrogate Rec) 91 2.485 86 1.2 30 - 150 20

80 77% TCMX (Surrogate Rec) 74 3.878 77 1.3 30 - 150 20

Page 3 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB62841

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits


Semivolatiles - Ground Water1,2,4,5-Tetrachlorobenzene ND 54 58 7.1 30 - 130 20

1,2,4-Trichlorobenzene ND 68 74 8.5 30 - 130 20

1,2-Dichlorobenzene ND 70 77 9.5 30 - 130 20



2,4,5-Trichlorophenol ND 83 84 1.2 30 - 130 20

2,4,6-Trichlorophenol ND 87 88 1.1 30 - 130 20

2,4-Dichlorophenol ND 81 86 6.0 30 - 130 20

2,4-Dimethylphenol ND 40 43 7.2 30 - 130 20

2,4-Dinitrophenol ND 61 33 59.6 r30 - 130 20

2,4-Dinitrotoluene ND 88 89 1.1 30 - 130 20

2,6-Dinitrotoluene ND 83 85 2.4 30 - 130 20

2-Chloronaphthalene ND 77 82 6.3 30 - 130 20

2-Chlorophenol ND 69 75 8.3 30 - 130 20

2-Methylnaphthalene ND 73 78 6.6 30 - 130 20

2-Methylphenol (o-cresol) ND 76 90 16.9 30 - 130 20

2-Nitroaniline ND >150 >150 NC l30 - 130 20

2-Nitrophenol ND 76 80 5.1 30 - 130 20

3&4-Methylphenol (m&p-cresol) ND 74 79 6.5 30 - 130 20

3,3'-Dichlorobenzidine ND N/A N/A NC 30 - 130 20

3-Nitroaniline ND 87 88 1.1 30 - 130 20

4,6-Dinitro-2-methylphenol ND 89 74 18.4 30 - 130 20

4-Bromophenyl phenyl ether ND 80 83 3.7 30 - 130 20

4-Chloro-3-methylphenol ND 85 88 3.5 30 - 130 20

4-Chloroaniline ND 69 75 8.3 30 - 130 20

4-Chlorophenyl phenyl ether ND 85 89 4.6 30 - 130 20

4-Nitroaniline ND 87 88 1.1 30 - 130 20

4-Nitrophenol ND 74 59 22.6 r30 - 130 20

Acenaphthene ND 78 84 7.4 30 - 130 20

Acenaphthylene ND 77 82 6.3 30 - 130 20

Acetophenone ND 51 55 7.5 30 - 130 20

Aniline ND N/A N/A NC 30 - 130 20

Anthracene ND 84 88 4.7 30 - 130 20

Azobenzene ND 55 58 5.3 30 - 130 20

Benz(a)anthracene ND 103 103 0.0 30 - 130 20

Benzidine ND N/A N/A NC 30 - 130 20

Benzo(a)pyrene ND 86 86 0.0 30 - 130 20

Benzo(b)fluoranthene ND 90 90 0.0 30 - 130 20

Benzo(ghi)perylene ND 88 85 3.5 30 - 130 20

Benzo(k)fluoranthene ND 100 91 9.4 30 - 130 20

Benzoic acid ND N/A N/A NC 30 - 130 20

Benzyl butyl phthalate ND 89 89 0.0 30 - 130 20

Bis(2-chloroethoxy)methane ND 75 81 7.7 30 - 130 20

Bis(2-chloroethyl)ether ND 62 67 7.8 30 - 130 20

Bis(2-chloroisopropyl)ether ND 77 84 8.7 30 - 130 20

Bis(2-ethylhexyl)phthalate ND 103 106 2.9 30 - 130 20

Carbazole ND >150 >150 NC l30 - 130 20

Chrysene ND 93 93 0.0 30 - 130 20

Dibenz(a,h)anthracene ND 90 95 5.4 30 - 130 20

Dibenzofuran ND 79 84 6.1 30 - 130 20

Page 4 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB62841

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

Diethyl phthalate ND 89 93 4.4 30 - 130 20

Dimethylphthalate ND 83 87 4.7 30 - 130 20

Di-n-butylphthalate ND 99 102 3.0 30 - 130 20

Di-n-octylphthalate ND 97 98 1.0 30 - 130 20

Fluoranthene ND 94 95 1.1 30 - 130 20

Fluorene ND 86 90 4.5 30 - 130 20

Hexachlorobenzene ND 83 88 5.8 30 - 130 20

Hexachlorobutadiene ND 71 77 8.1 30 - 130 20

Hexachlorocyclopentadiene ND 25 22 12.8 l30 - 130 20

Hexachloroethane ND 69 77 11.0 30 - 130 20

Indeno(1,2,3-cd)pyrene ND 90 94 4.3 30 - 130 20

Isophorone ND 61 65 6.3 30 - 130 20

Naphthalene ND 77 83 7.5 30 - 130 20

Nitrobenzene ND 75 80 6.5 30 - 130 20

N-Nitrosodimethylamine ND 58 58 0.0 30 - 130 20

N-Nitrosodi-n-propylamine ND 79 84 6.1 30 - 130 20

N-Nitrosodiphenylamine ND 95 98 3.1 30 - 130 20

Pentachloronitrobenzene ND 120 126 4.9 30 - 130 20

Pentachlorophenol ND 52 23 77.3 l,r30 - 130 20

Phenanthrene ND 88 93 5.5 30 - 130 20

Phenol ND 78 79 1.3 30 - 130 20

Pyrene ND 96 97 1.0 30 - 130 20

Pyridine ND 13 <5 NC l30 - 130 20

% 2,4,6-Tribromophenol 95 89 93 4.4 15 - 130 20

% 2-Fluorobiphenyl 70 69 76 9.7 30 - 130 20

% 2-Fluorophenol 71 59 64 8.1 15 - 130 20

% Nitrobenzene-d5 76 70 77 9.5 30 - 130 20

% Phenol-d5 19 62 65 4.7 15 - 130 20

% Terphenyl-d14 87 104 107 2.8 30 - 130 20


Volatiles - Ground Water126 1281,1,1,2-Tetrachloroethane ND 1.6120 119 0.8 70 - 130 30





















Page 5 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB62841

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

92 1002-Hexanone ND 8.389 89 0.0 70 - 130 30




101 102Acetone ND 1.089 89 0.0 70 - 130 30


100 102Benzene ND 2.092 93 1.1 70 - 130 30

95 100Bromobenzene ND 5.193 93 0.0 70 - 130 30



137 132Bromoform ND 3.7124 117 5.8 m70 - 130 30

89 101Bromomethane ND 12.699 100 1.0 70 - 130 30

108 113Carbon Disulfide ND 4.5139 139 0.0 l70 - 130 30



99 103Chloroethane ND 4.088 84 4.7 70 - 130 30

104 102Chloroform ND 1.995 95 0.0 70 - 130 30








116 115Ethylbenzene ND 0.9103 104 1.0 70 - 130 30



111 111m&p-Xylene ND 0.0102 101 1.0 70 - 130 30




72 92Naphthalene ND 24.481 91 11.6 70 - 130 30



110 108o-Xylene ND 1.8103 100 3.0 70 - 130 30



116 108Styrene ND 7.199 94 5.2 70 - 130 30




101 102Toluene ND 1.094 95 1.1 70 - 130 30











97 96% Toluene-d8 98 1.096 96 0.0 70 - 130 30

Page 6 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB62841

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

QA/QC Batch 197934, QC Sample No: BB62844 (BB62842, BB62843, BB62844, BB62845)

Volatiles - Ground Water114 1131,1,1,2-Tetrachloroethane ND 0.9130 117 10.5 70 - 130 30





















90 892-Hexanone ND 1.195 85 11.1 70 - 130 30




100 109Acetone ND 8.6115 111 3.5 70 - 130 30


97 96Benzene ND 1.0108 98 9.7 70 - 130 30

93 92Bromobenzene ND 1.198 93 5.2 70 - 130 30



115 107Bromoform ND 7.2131 95 31.9 l,r70 - 130 30

96 99Bromomethane ND 3.1112 93 18.5 70 - 130 30

101 99Carbon Disulfide ND 2.0>150 135 NC l70 - 130 30



94 93Chloroethane ND 1.1106 87 19.7 70 - 130 30

100 96Chloroform ND 4.1109 99 9.6 70 - 130 30







96 98Dichlorodifluoromethane ND 2.1113 76 39.2 r70 - 130 30

102 99Ethylbenzene ND 3.0121 106 13.2 70 - 130 30



102 99m&p-Xylene ND 3.0114 99 14.1 70 - 130 30


Page 7 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB62841

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits



70 84Naphthalene ND 18.281 87 7.1 70 - 130 30



102 97o-Xylene ND 5.0115 96 18.0 70 - 130 30



95 90Styrene ND 5.4115 87 27.7 70 - 130 30




99 97Toluene ND 2.0107 99 7.8 70 - 130 30











98 99% Toluene-d8 99 1.097 98 1.0 70 - 130 30

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.





NC - No Criteria

Page 8 of 8

Sample Criteria Exceedences ReportThursday, April 12, 2012 Page 1 of 6



CriteriaUnits

GBB62841Requested Criteria: 375, GWFactored

RLCriteria

$8260GWR Dibromoethane 0.0006ND 1.0 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0006$8260GWR 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8260GWR 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8270-SIMFSR Phenol 1ND 10 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1$8270-SIMFSR Phenol 1ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Bis(2-chloroethyl)ether 1ND 5.0 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Aniline 5ND 10 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR Aniline 5ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2-Chlorophenol 1ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2-Methylphenol (o-cresol) 5ND 10 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Methylphenol (o-cresol) 1ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Nitrobenzene 0.4ND 5.0 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.4$8270-SIMFSR 2-Nitrophenol 5ND 10 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Nitrophenol 1ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4-Dimethylphenol 1ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4-Dimethylphenol 5ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dichlorophenol 1ND 10 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1$8270-SIMFSR 2,4-Dichlorophenol 5ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dichlorophenol 1ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 4-Chloroaniline 5ND 20 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Chloroaniline 5ND 20 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 4-Chloro-3-methylphenol 5ND 20 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Chloro-3-methylphenol 1ND 20 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4,6-Trichlorophenol 1ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4,5-Trichlorophenol 1ND 10 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1$8270-SIMFSR 2,4,5-Trichlorophenol 1ND 10 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 4-Nitroaniline 5ND 20 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 3-Nitroaniline 5ND 50 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 3-Nitroaniline 5ND 50 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dinitrophenol 5ND 50 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2,4-Dinitrophenol 1ND 50 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4-Dinitrophenol 5ND 50 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 4-Nitrophenol 5ND 50 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Nitrophenol 1ND 50 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2-Nitroaniline 5ND 50 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Nitroaniline 5ND 50 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 4,6-Dinitro-2-methylphenol 1ND 50 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Benzidine 5ND 50 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 3,3'-Dichlorobenzidine 5ND 50 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMR Hexachlorobenzene 0.04ND 0.060 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04




CriteriaUnits


RLCriteria

$8270-SIMR Benz(a)anthracene 0.002ND 0.040 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benz(a)anthracene 0.002ND 0.040 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Chrysene 0.002ND 0.050 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Chrysene 0.002ND 0.050 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(b)fluoranthene 0.002ND 0.050 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benzo(b)fluoranthene 0.002ND 0.050 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(k)fluoranthene 0.002ND 0.050 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benzo(k)fluoranthene 0.002ND 0.050 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(a)pyrene 0.002ND 0.050 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.050 ug/LBB62841 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.050 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$PESTGAW 4,4' -DDE 0.01ND* 0.07 ug/LBB62841 ESPL NY Tagm - Pest/herb/pcbs Groundwater Standardsug/L 0.01$PESTGAW Toxaphene 0.06ND 1.0 ug/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.06AL-WM Aluminum 0.1130 0.10 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1AS-WM Arsenic 0.0250.026 0.004 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.025BA-WM Barium 14.57 0.002 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 1BE-WM Beryllium 0.0030.011 0.001 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.003CR-WM Chromium 0.050.423 0.001 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.05CU-WM Copper 0.20.446 0.005 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.2D-AL Aluminum (Dissolved) 0.15.05 0.01 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1D-FE Iron (Dissolved) 0.38.23 0.011 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3D-MN Manganese (Dissolved) 0.32.26 0.011 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3D-NA Sodium (Dissolved) 2037.8 0.11 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 20D-PB Lead (Dissolved) 0.0250.043 0.002 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.025D-SB Antimony (Dissolved) 0.003BDL 0.005 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.003D-SE Selenium (Dissolved) 0.01BDL 0.011 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.01D-TL Thallium (Dissolved) 0.0005BDL 0.002 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0005FE-WM Iron 0.3210 0.10 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3MG-WM Magnesium 3589.0 0.10 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 35MN-WM Manganese 0.315.3 0.010 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3NA-WM Sodium 2030.1 0.1 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 20NI-WM Nickel 0.10.836 0.001 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1PB-WM Lead 0.0250.492 0.002 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.025SB-WM Antimony 0.003BDL 0.005 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.003TL-WM Thallium 0.0005BDL 0.002 mg/LBB62841 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0005

$8260GWR Dibromoethane 0.0006ND 1.0 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0006$8260GWR 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8260GWR 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8270-SIMFSR Phenol 1ND 13 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1




CriteriaUnits


RLCriteria

$8270-SIMFSR Phenol 1ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Bis(2-chloroethyl)ether 1ND 6.3 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Aniline 5ND 13 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR Aniline 5ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2-Chlorophenol 1ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2-Methylphenol (o-cresol) 5ND 13 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Methylphenol (o-cresol) 1ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Nitrobenzene 5ND 6.3 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR Nitrobenzene 0.4ND 6.3 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.4$8270-SIMFSR 2-Nitrophenol 5ND 13 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Nitrophenol 1ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4-Dimethylphenol 1ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4-Dimethylphenol 5ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR Bis(2-chloroethoxy)methane 5ND 6.3 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dichlorophenol 1ND 13 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1$8270-SIMFSR 2,4-Dichlorophenol 5ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dichlorophenol 1ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 4-Chloroaniline 5ND 25 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Chloroaniline 5ND 25 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 4-Chloro-3-methylphenol 5ND 25 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Chloro-3-methylphenol 1ND 25 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Hexachlorocyclopentadiene 5ND 6.3 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4,6-Trichlorophenol 1ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4,5-Trichlorophenol 1ND 13 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1$8270-SIMFSR 2,4,5-Trichlorophenol 1ND 13 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 4-Nitroaniline 5ND 25 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,6-Dinitrotoluene 5ND 6.3 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2,6-Dinitrotoluene 5ND 6.3 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 3-Nitroaniline 5ND 63 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 3-Nitroaniline 5ND 63 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dinitrophenol 5ND 63 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2,4-Dinitrophenol 5ND 63 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dinitrophenol 1ND 63 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Dibenzofuran 5ND 6.3 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2,4-Dinitrotoluene 5ND 6.3 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 4-Nitrophenol 5ND 63 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Nitrophenol 1ND 63 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2-Nitroaniline 5ND 63 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Nitroaniline 5ND 63 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 4,6-Dinitro-2-methylphenol 1ND 63 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 1




CriteriaUnits


RLCriteria

$8270-SIMFSR Azobenzene 5ND 6.3 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR Benzidine 5ND 63 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 3,3'-Dichlorobenzidine 5ND 63 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMR Hexachlorobenzene 0.04ND 0.075 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8270-SIMR Benz(a)anthracene 0.002ND 0.050 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benz(a)anthracene 0.002ND 0.050 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Chrysene 0.002ND 0.063 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Chrysene 0.002ND 0.063 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(b)fluoranthene 0.002ND 0.063 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benzo(b)fluoranthene 0.002ND 0.063 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(k)fluoranthene 0.002ND 0.063 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benzo(k)fluoranthene 0.002ND 0.063 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(a)pyrene 0.002ND 0.063 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.063 ug/LBB62842 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.063 ug/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002D-AL Aluminum (Dissolved) 0.11.02 0.01 mg/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1D-FE Iron (Dissolved) 0.30.935 0.011 mg/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3D-MN Manganese (Dissolved) 0.31.24 0.001 mg/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3D-NA Sodium (Dissolved) 2078.5 1.1 mg/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 20D-SB Antimony (Dissolved) 0.003BDL 0.005 mg/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.003D-SE Selenium (Dissolved) 0.01BDL 0.011 mg/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.01D-TL Thallium (Dissolved) 0.0005BDL 0.002 mg/LBB62842 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0005

$8260GWR Dibromoethane 0.0006ND 1.0 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0006$8260GWR 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8260GWR 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8270-SIMFSR Phenol 1ND 10 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1$8270-SIMFSR Phenol 1ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Bis(2-chloroethyl)ether 1ND 5.0 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Aniline 5ND 10 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR Aniline 5ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2-Chlorophenol 1ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2-Methylphenol (o-cresol) 5ND 10 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Methylphenol (o-cresol) 1ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Nitrobenzene 0.4ND 5.0 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.4$8270-SIMFSR 2-Nitrophenol 5ND 10 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Nitrophenol 1ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4-Dimethylphenol 5ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dimethylphenol 1ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4-Dichlorophenol 1ND 10 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1




CriteriaUnits


RLCriteria

$8270-SIMFSR 2,4-Dichlorophenol 5ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dichlorophenol 1ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 4-Chloroaniline 5ND 20 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Chloroaniline 5ND 20 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 4-Chloro-3-methylphenol 5ND 20 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Chloro-3-methylphenol 1ND 20 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4,6-Trichlorophenol 1ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2,4,5-Trichlorophenol 1ND 10 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1$8270-SIMFSR 2,4,5-Trichlorophenol 1ND 10 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 4-Nitroaniline 5ND 20 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 3-Nitroaniline 5ND 50 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 3-Nitroaniline 5ND 50 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dinitrophenol 5ND 50 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2,4-Dinitrophenol 5ND 50 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 2,4-Dinitrophenol 1ND 50 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 4-Nitrophenol 5ND 50 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 4-Nitrophenol 1ND 50 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR 2-Nitroaniline 5ND 50 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 5$8270-SIMFSR 2-Nitroaniline 5ND 50 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 4,6-Dinitro-2-methylphenol 1ND 50 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMFSR Benzidine 5ND 50 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMFSR 3,3'-Dichlorobenzidine 5ND 50 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 5$8270-SIMR Hexachlorobenzene 0.04ND 0.060 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8270-SIMR Pentachlorophenol 12.4 0.80 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 1$8270-SIMR Pentachlorophenol 12.4 0.80 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 1$8270-SIMR Benz(a)anthracene 0.002ND 0.040 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benz(a)anthracene 0.002ND 0.040 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Chrysene 0.002ND 0.050 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Chrysene 0.002ND 0.050 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(b)fluoranthene 0.002ND 0.050 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benzo(b)fluoranthene 0.002ND 0.050 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(k)fluoranthene 0.002ND 0.050 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Benzo(k)fluoranthene 0.002ND 0.050 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$8270-SIMR Benzo(a)pyrene 0.002ND 0.050 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.050 ug/LBB62843 ESPL NY Tagm - Semi-volatiles Groundwater Standardsug/L 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.050 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.002$PESTGAW Toxaphene 0.06ND 1.0 ug/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.06AL-WM Aluminum 0.114.1 0.010 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1D-AL Aluminum (Dissolved) 0.11.25 0.01 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1D-FE Iron (Dissolved) 0.31.65 0.011 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3




CriteriaUnits


RLCriteria

D-MN Manganese (Dissolved) 0.30.415 0.001 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3D-NA Sodium (Dissolved) 20139 1.1 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 20D-SB Antimony (Dissolved) 0.003BDL 0.005 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.003D-SE Selenium (Dissolved) 0.01BDL 0.011 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.01D-TL Thallium (Dissolved) 0.0005BDL 0.002 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0005FE-WM Iron 0.319.7 0.010 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3HG-WM Mercury 0.00070.0009 0.0002 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0007MN-WM Manganese 0.32.65 0.010 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3NA-WM Sodium 20131 1.0 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 20NI-WM Nickel 0.10.118 0.001 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1PB-WM Lead 0.0250.039 0.002 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.025SB-WM Antimony 0.003BDL 0.005 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.003TL-WM Thallium 0.0005BDL 0.002 mg/LBB62843 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0005

$8260GWR Dibromoethane 0.0006ND 1.0 ug/LBB62844 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0006$8260GWR 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBB62844 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8260GWR 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBB62844 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04

$8260GWR Dibromoethane 0.0006ND 1.0 ug/LBB62845 ESPL NY Togs - Water Quality GA Criteriaug/L 0.0006$8260GWR 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBB62845 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04$8260GWR 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBB62845 ESPL NY Togs - Water Quality GA Criteriaug/L 0.04


BB74626

Tuesday, May 01, 2012

Sample ID#s:






Sincerely yours,







Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

GROUND WATER

ESPL

Standard

212117-2

04/19/12

LB

see "By" below

RK

Laboratory Data

MW-2

Phoenix ID: BB74626

04/19/12

8:00

17:10



Analysis ReportMay 01, 2012

Time

Date Time



SDG ID: GBB74626

Client ID:


5.86 Aluminum 0.010 04/21/12 LK 6010mg/L7.16 Aluminum (Dissolved) 0.01 04/22/12 LK 6010mg/L< 0.003 Antimony (Dissolved) 0.003 04/22/12 LK 6010mg/L< 0.003 Antimony 0.003 04/24/12 TH 6010mg/L< 0.004 Arsenic 0.004 04/21/12 LK 6010mg/L< 0.004 Arsenic (Dissolved) 0.004 04/22/12 LK 6010mg/L0.132 Barium 0.002 04/21/12 LK 6010mg/L0.130 Barium (Dissolved) 0.002 04/22/12 LK 6010mg/L< 0.001 Beryllium 0.001 04/21/12 LK 6010mg/L< 0.001 Beryllium (Dissolved) 0.001 04/22/12 LK 6010mg/L33.5 Calcium 0.010 04/21/12 LK 6010mg/L< 0.001 Cadmium 0.001 04/21/12 LK 6010mg/L28.2 Calcium (Dissolved) 0.01 04/22/12 LK 6010mg/L< 0.001 Cadmium (Dissolved) 0.001 04/22/12 LK 6010mg/L0.023 Chromium 0.001 04/21/12 LK 6010mg/L0.026 Chromium (Dissolved) 0.001 04/22/12 LK 6010mg/L0.004 Cobalt 0.002 04/21/12 LK 6010mg/L0.043 Copper 0.005 04/21/12 LK 6010mg/L0.004 Cobalt (Dissolved) 0.001 04/22/12 LK 6010mg/L0.027 Copper (Dissolved) 0.005 04/22/12 LK 6010mg/LCompleted Dissolved Metals Preparation 04/19/12 AG SW846-3005

7.75 Iron (Dissolved) 0.011 04/22/12 LK 6010mg/L7.62 Iron 0.010 04/21/12 LK 6010mg/L0.038 Lead (Dissolved) 0.002 04/22/12 LK 6010mg/L0.110 Lead 0.002 04/21/12 LK 6010mg/L8.74 Magnesium (Dissolved) 0.01 04/22/12 LK 6010mg/L1.30 Manganese (Dissolved) 0.001 04/22/12 LK 6010mg/L10.5 Magnesium 0.01 04/21/12 LK 6010mg/L

Page 1 of 3 Ver 1

MW-2




0.794 Manganese 0.001 04/21/12 LK 6010mg/L< 0.0002 Mercury (Dissolved) 0.0002 04/20/12 JA 7470/E245.1mg/L< 0.0002 Mercury 0.0002 04/20/12 JA 7470/E245.1mg/L0.029 Nickel (Dissolved) 0.001 04/22/12 LK 6010mg/L0.035 Nickel 0.001 04/21/12 LK 6010mg/L7.6 Potassium (Dissolved) 0.1 04/22/12 LK 6010mg/L6.6 Potassium 0.1 04/21/12 LK 6010mg/L< 0.010 Selenium (Dissolved) 0.010 04/22/12 LK 6010mg/L< 0.010 Selenium 0.010 04/24/12 TH 6010mg/L< 0.001 Silver 0.001 04/21/12 LK 6010mg/L< 0.001 Silver (Dissolved) 0.001 04/22/12 LK 6010mg/L84.8 Sodium (Dissolved) 1.1 04/24/12 LK 6010mg/L79.2 Sodium 1.0 04/24/12 LK 6010mg/L< 0.0005 Thallium (Dissolved) 0.0005 04/23/12 TH 7010/279.2mg/L< 0.0005 Thallium 0.0005 04/23/12 TH SW7010/200.9mg/LCompleted Total Metals Digestion 04/20/12 AG

0.013 Vanadium (Dissolved) 0.002 04/22/12 LK 6010mg/L0.012 Vanadium 0.002 04/21/12 LK 6010mg/L0.038 Zinc (Dissolved) 0.002 04/22/12 LK 6010mg/L0.055 Zinc 0.002 04/21/12 LK 6010mg/LCompleted Dissolved Mercury Digestion 04/20/12 X/X SW7470




Polychlorinated BiphenylsND PCB-1016 0.05 04/25/12 KCA 608/ 8082ug/LND PCB-1221 0.05 04/25/12 KCA 608/ 8082ug/LND PCB-1232 0.05 04/25/12 KCA 608/ 8082ug/LND PCB-1242 0.05 04/25/12 KCA 608/ 8082ug/LND PCB-1248 0.05 04/25/12 KCA 608/ 8082ug/LND PCB-1254 0.05 04/25/12 KCA 608/ 8082ug/LND PCB-1260 0.05 04/25/12 KCA 608/ 8082ug/LND PCB-1262 0.05 04/25/12 KCA 608/ 8082ug/LND PCB-1268 0.05 04/25/12 KCA 608/ 8082ug/L

QA/QC Surrogates63 % DCBP 04/25/12 KCA 30 - 150 %%

79 % TCMX 04/25/12 KCA 30 - 150 %%

PesticidesND 4,4' -DDD 0.01 04/23/12 MR SW8081ug/LND 4,4' -DDE 0.01 04/23/12 MR SW8081ug/LND 4,4' -DDT 0.01 04/23/12 MR SW8081ug/LND a-BHC 0.01 04/23/12 MR SW8081ug/LND Alachlor 0.5 04/23/12 MR SW8081ug/L 1

ND Aldrin 0.01 04/23/12 MR SW8081ug/LND b-BHC 0.01 04/23/12 MR SW8081ug/LND Chlordane 0.05 04/23/12 MR SW8081ug/LND d-BHC 0.04 04/23/12 MR SW8081ug/LND Dieldrin 0.004 04/23/12 MR SW8081ug/LND Endosulfan I 0.1 04/23/12 MR SW8081ug/L

Page 2 of 3 Ver 1

MW-2




ND Endosulfan II 0.1 04/23/12 MR SW8081ug/LND Endosulfan Sulfate 0.1 04/23/12 MR SW8081ug/LND Endrin 0.01 04/23/12 MR SW8081ug/LND Endrin Aldehyde 5 04/23/12 MR SW8081ug/LND Endrin ketone 5 04/23/12 MR SW8081ug/LND g-BHC (Lindane) 0.05 04/23/12 MR SW8081ug/LND Heptachlor 0.01 04/23/12 MR SW8081ug/LND Heptachlor epoxide 0.01 04/23/12 MR SW8081ug/LND Methoxychlor 35 04/23/12 MR SW8081ug/LND Toxaphene 0.06 04/23/12 MR SW8081ug/L



Comments:



May 01, 2012

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.


Reviewed and Released by: Johanna Harrington, Project Manager


Page 3 of 3 Ver 1

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

QA/QC ReportMay 01, 2012



SDG I.D.: GBB74626

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

SampleResult

DupResult

QA/QC Batch 198681, QC Sample No: BB73699 (BB74626)102 102Thallium - Water BDL 0.0103NC 103 0.0 75 - 125 20<0.001 <0.001


ICP Metals - Aqueous95.8 98.2Aluminum 0.023 2.595.6NC 98.4 2.9 75 - 125 20<0.010 <0.010

102 104Antimony BDL 1.9102NC 106 3.8 75 - 125 200.005 0.006

100 103Arsenic BDL 3.0101NC 104 2.9 75 - 125 20<0.004 <0.004

98.6 101Barium BDL 2.498.7NC 101 2.3 75 - 125 20<0.002 <0.002

101 105Beryllium BDL 3.9101NC 105 3.9 75 - 125 20<0.001 <0.001

105 108Cadmium BDL 2.8105NC 108 2.8 75 - 125 20<0.001 <0.001

102 104Calcium BDL 1.9102NC 105 2.9 75 - 125 200.042 0.047

102 105Chromium BDL 2.9102NC 105 2.9 75 - 125 20<0.001 <0.001

103 106Cobalt BDL 2.9103NC 106 2.9 75 - 125 20<0.002 <0.002

104 108Copper BDL 3.8104NC 108 3.8 75 - 125 20<0.005 <0.005

99.7 102Iron BDL 2.399.3NC 103 3.7 75 - 125 200.016 0.014

103 106Lead BDL 2.9104NC 106 1.9 75 - 125 20<0.002 0.002

106 108Magnesium BDL 1.9105NC 108 2.8 75 - 125 20<0.01 <0.01

101 104Manganese BDL 2.9102NC 104 1.9 75 - 125 20<0.002 <0.001

101 104Nickel BDL 2.9101NC 104 2.9 75 - 125 20<0.002 <0.001

97.4 100Potassium BDL 2.696.7NC 98.2 1.5 75 - 125 20<0.1 <0.1

95.4 98.5Selenium BDL 3.297.5NC 100 2.5 75 - 125 20<0.010 <0.010

99.9 103Silver BDL 3.1100NC 103 3.0 75 - 125 20<0.002 <0.001

103 107Sodium BDL 3.8102NC 104 1.9 75 - 125 200.32 0.3

101 103Vanadium BDL 2.0100NC 103 3.0 75 - 125 20<0.002 <0.002

103 106Zinc BDL 2.9103NC 106 2.9 75 - 125 20<0.002 <0.002

QA/QC Batch 198800, QC Sample No: BB74630 (BB74626)92.9 95.4Mercury - Water BDL 2.791.5NC 91.4 0.1 70 - 130 20<0.0002 <0.0002


ICP Metals - Dissolved99.4 99.9Aluminum BDL 0.593.2NC 98.6 5.6 75 - 125 200.037 0.04

102 102Antimony BDL 0.095.6NC 101 5.5 75 - 125 200.005 0.006

99.3 99.7Arsenic BDL 0.492.2NC 97.5 5.6 75 - 125 20<0.004 <0.004

101 101Barium BDL 0.094.1NC 99.5 5.6 75 - 125 200.006 0.006

105 105Beryllium BDL 0.097.6NC 103 5.4 75 - 125 20<0.004 <0.001

104 104Cadmium BDL 0.097.0NC 103 6.0 75 - 125 20<0.001 <0.001

NC NCCalcium BDL NC96.62.00 102 5.4 75 - 125 206.00 5.88

102 102Chromium BDL 0.094.8NC 100 5.3 75 - 125 20<0.001 <0.001

103 104Cobalt BDL 1.096.0NC 102 6.1 75 - 125 20<0.004 <0.001

108 109Copper BDL 0.999.8NC 106 6.0 75 - 125 20<0.005 <0.005

99.5 100Iron BDL 0.593.2NC 98.7 5.7 75 - 125 200.042 0.039

100 101Lead BDL 1.093.5NC 98.6 5.3 75 - 125 20<0.002 <0.002

93.0 93.8Magnesium BDL 0.91001.40 105 4.9 75 - 125 202.10 2.07

Page 1 of 3

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBB74626

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits

SampleResult

DupResult

101 102Manganese BDL 1.094.50 100 5.7 75 - 125 200.009 0.009

102 103Nickel BDL 1.095.2NC 101 5.9 75 - 125 20<0.001 <0.001

105 108Potassium BDL 2.897.70 100 2.3 75 - 125 201.0 1.0

95.5 96.0Selenium BDL 0.589.0NC 94.3 5.8 75 - 125 20<0.011 <0.011

85.2 86.1Silver BDL 1.194.6NC 100 5.5 75 - 125 20<0.001 <0.001

NC NCSodium BDL NC96.80.60 99.1 2.3 75 - 125 206.45 6.49

101 102Vanadium BDL 1.094.4NC 99.6 5.4 75 - 125 20<0.002 <0.002

101 102Zinc BDL 1.094.0NC 99.5 5.7 75 - 125 200.006 0.006

Page 2 of 3

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

QA/QC ReportMay 01, 2012



SDG I.D.: GBB74626

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPDLimits


Pesticides - Ground Water4,4' -DDD ND 98 91 7.4 40 - 140 20

4,4' -DDE ND 89 85 4.6 40 - 140 20

4,4' -DDT ND 88 84 4.7 40 - 140 20

a-BHC ND 79 78 1.3 40 - 140 20

a-Chlordane ND 84 82 2.4 40 - 140 20

Alachlor ND N/A N/A NC 40 - 140 20

Aldrin ND 75 73 2.7 40 - 140 20

b-BHC ND 83 81 2.4 40 - 140 20

Chlordane ND N/A N/A NC 40 - 140 20

d-BHC ND 82 81 1.2 40 - 140 20

Dieldrin ND 88 86 2.3 40 - 140 20

Endosulfan I ND 81 80 1.2 40 - 140 20

Endosulfan II ND 94 89 5.5 40 - 140 20

Endosulfan sulfate ND 86 85 1.2 40 - 140 20

Endrin ND 90 88 2.2 40 - 140 20

Endrin aldehyde ND 96 93 3.2 40 - 140 20

Endrin ketone ND 92 90 2.2 40 - 140 20

g-BHC ND 81 80 1.2 40 - 140 20

g-Chlordane ND 83 81 2.4 40 - 140 20

Heptachlor ND 90 88 2.2 40 - 140 20

Heptachlor epoxide ND 82 79 3.7 40 - 140 20

Methoxychlor ND 108 108 0.0 40 - 140 20

Toxaphene ND N/A N/A NC 40 - 140 20

% DCBP 88 93 90 3.3 30 - 150 20

% TCMX 74 83 78 6.2 30 - 150 20



May 01, 2012MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No CriteriaIntf - Interference

Page 3 of 3

Sample Criteria Exceedences ReportTuesday, May 01, 2012 Page 1 of 1



CriteriaUnits

GBB74626Requested Criteria: GWFactored

RLCriteria

AL-WM Aluminum 0.15.86 0.010 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1D-AL Aluminum (Dissolved) 0.17.16 0.01 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 0.1D-FE Iron (Dissolved) 0.37.75 0.011 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3D-MN Manganese (Dissolved) 0.31.30 0.001 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3D-NA Sodium (Dissolved) 2084.8 1.1 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 20D-PB Lead (Dissolved) 0.0250.038 0.002 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 0.025FE-WM Iron 0.37.62 0.010 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3MN-WM Manganese 0.30.794 0.001 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 0.3NA-WM Sodium 2079.2 1.0 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 20PB-WM Lead 0.0250.110 0.002 mg/LBB74626 ESPL NY Togs - Water Quality GA Criteriaug/L 0.025


BB60083 - BB60085

Wednesday, April 04, 2012

Sample ID#s:






Sincerely yours,







Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

AIR

ESPL

72 Hour

212117-2

03/28/12

LB

see "By" below

Laboratory Data

SV-2

Phoenix ID: BB60083

03/30/12

9:30

11:04

Parameter Result RL Result RL By Reference



Date

Date Time



SDG ID: GBB60083

Client ID:


ppbv ug/m3ppbv ug/m3^

Volatiles (TO15)ND 1,1,1,2-Tetrachloroethane 0.146 1.0 KCA TO15ND 04/02/12 1

ND 1,1,1-Trichloroethane 0.183 1.0 KCA TO15ND 04/02/12

ND 1,1,2,2-Tetrachloroethane 0.146 1.0 KCA TO15ND 04/02/12


ND 1,1-Dichloroethane 0.247 1.0 KCA TO15ND 04/02/12

ND 1,1-Dichloroethene 0.252 1.0 KCA TO15ND 04/02/12

ND 1,2,4-Trichlorobenzene 0.135 1.0 KCA TO15ND 04/02/12

8.92 1,2,4-Trimethylbenzene 0.204 1.0 KCA TO1543.8 04/02/12

ND 1,2-Dibromoethane(EDB) 0.130 1.0 KCA TO15ND 04/02/12

ND 1,2-Dichlorobenzene 0.166 1.0 KCA TO15ND 04/02/12


ND 1,2-dichloropropane 0.216 1.0 KCA TO15ND 04/02/12

ND 1,2-Dichlorotetrafluoroethane 0.143 1.0 KCA TO15ND 04/02/12


ND 1,3-Butadiene 0.452 1.0 KCA TO15ND 04/02/12


0.39 1,4-Dichlorobenzene 0.166 1.0 KCA TO152.34 04/02/12

ND 1,4-Dioxane 0.278 1.0 KCA TO15ND 04/02/12

ND 2-Hexanone(MBK) 0.244 1.0 KCA TO15ND 04/02/12 1

2.13 4-Ethyltoluene 0.204 1.0 KCA TO1510.5 04/02/12 1

0.45 4-Isopropyltoluene 0.182 1.0 KCA TO152.47 04/02/12 1

2.07 4-Methyl-2-pentanone(MIBK) 0.244 1.0 KCA TO158.47 04/02/12

6.08 Acetone 0.421 1.0 KCA TO1514.4 04/02/12

ND Acrylonitrile 0.461 1.0 KCA TO15ND 04/02/12

0.47 Benzene 0.313 1.0 KCA TO151.50 04/02/12

ND Benzyl chloride 0.193 1.0 KCA TO15ND 04/02/12 1

Page 1 of 9 Ver 1

SV-2


Parameter Result RL Result RL By ReferenceDate


ppbv ug/m3ppbv ug/m3

ND Bromodichloromethane 0.149 1.0 KCA TO15ND 04/02/12

ND Bromoform 0.097 1.0 KCA TO15ND 04/02/12

ND Bromomethane 0.258 1.0 KCA TO15ND 04/02/12

ND Carbon Disulfide 0.321 1.0 KCA TO15ND 04/02/12

0.07 Carbon Tetrachloride 0.040 0.25 KCA TO150.440 04/02/12

ND Chlorobenzene 0.217 1.0 KCA TO15ND 04/02/12

ND Chloroethane 0.379 1.0 KCA TO15ND 04/02/12

ND Chloroform 0.205 1.0 KCA TO15ND 04/02/12

ND Chloromethane 0.484 1.0 KCA TO15ND 04/02/12

ND Cis-1,2-Dichloroethene 0.252 1.0 KCA TO15ND 04/02/12

ND cis-1,3-Dichloropropene 0.220 1.0 KCA TO15ND 04/02/12 1

1.27 Cyclohexane 0.291 1.0 KCA TO154.37 04/02/12

ND Dibromochloromethane 0.117 1.0 KCA TO15ND 04/02/12

0.59 Dichlorodifluoromethane 0.202 1.0 KCA TO152.92 04/02/12

4.38 Ethanol 0.531 1.0 KCA TO158.25 04/02/12 1

1.92 Ethyl acetate 0.278 1.0 KCA TO156.91 04/02/12 1

3.4 Ethylbenzene 0.230 1.0 KCA TO1514.8 04/02/12

0.67 Heptane 0.244 1.0 KCA TO152.74 04/02/12

ND Hexachlorobutadiene 0.094 1.0 KCA TO15ND 04/02/12

0.35 Hexane 0.284 1.0 KCA TO151.23 04/02/12

8.54 Isopropylalcohol 0.407 1.0 KCA TO1521.0 04/02/12

0.45 Isopropylbenzene 0.204 1.0 KCA TO152.21 04/02/12

11.7 m,p-Xylene 0.230 1.0 KCA TO1550.8 04/02/12

0.76 Methyl Ethyl Ketone 0.339 1.0 KCA TO152.24 04/02/12

ND Methyl tert-butyl ether(MTBE) 0.278 1.0 KCA TO15ND 04/02/12

ND Methylene Chloride 0.288 1.0 KCA TO15ND 04/02/12

0.96 n-Butylbenzene 0.182 1.0 KCA TO155.27 04/02/12 1

5.81 o-Xylene 0.230 1.0 KCA TO1525.2 04/02/12

ND Propylene 0.581 1.0 KCA TO15ND 04/02/12 1

0.3 sec-Butylbenzene 0.182 1.0 KCA TO151.64 04/02/12 1

ND Styrene 0.235 1.0 KCA TO15ND 04/02/12

6.17 Tetrachloroethene 0.037 0.25 KCA TO1541.8 04/02/12

ND Tetrahydrofuran 0.339 1.0 KCA TO15ND 04/02/12 1

39.4 Toluene 0.266 1.0 KCA TO15148 04/02/12

ND Trans-1,2-Dichloroethene 0.252 1.0 KCA TO15ND 04/02/12

ND trans-1,3-Dichloropropene 0.220 1.0 KCA TO15ND 04/02/12

ND Trichloroethene 0.047 0.25 KCA TO15ND 04/02/12

0.27 Trichlorofluoromethane 0.178 1.0 KCA TO151.52 04/02/12

ND Trichlorotrifluoroethane 0.130 1.0 KCA TO15ND 04/02/12

ND Vinyl Chloride 0.098 0.25 KCA TO15ND 04/02/12

QA/QC Surrogates107 % Bromofluorobenzene % % KCA 70 - 130 %107 04/02/12

Page 2 of 9 Ver 1

SV-2





Comments:



April 04, 2012

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters.


Reviewed and Released by: Greg Lawrence, Assistant Lab Directo


Page 3 of 9 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

AIR

ESPL

72 Hour

212117-2

03/28/12

LB

see "By" below

Laboratory Data

SV-1

Phoenix ID: BB60084

03/30/12

10:50

11:04




Date

Date Time



SDG ID: GBB60083

Client ID:

























5.65 Acetone 0.421 1.0 KCA TO1513.4 04/02/12


0.47 Benzene 0.313 1.0 KCA TO151.50 04/02/12


Page 4 of 9 Ver 1

SV-1








0.43 Carbon Disulfide 0.321 1.0 KCA TO151.34 04/02/12




ND Chloroform 0.205 1.0 KCA TO15ND 04/02/12




2.16 Cyclohexane 0.291 1.0 KCA TO157.43 04/02/12



10.4 Ethanol 0.531 1.0 KCA TO1519.6 04/02/12 1



0.76 Heptane 0.244 1.0 KCA TO153.11 04/02/12


0.42 Hexane 0.284 1.0 KCA TO151.48 04/02/12



12.2 m,p-Xylene 0.230 1.0 KCA TO1552.9 04/02/12



ND Methylene Chloride 0.288 1.0 KCA TO15ND 04/02/12


6.04 o-Xylene 0.230 1.0 KCA TO1526.2 04/02/12


0.29 sec-Butylbenzene 0.182 1.0 KCA TO151.59 04/02/12 1




37.4 Toluene 0.266 1.0 KCA TO15141 04/02/12








Page 5 of 9 Ver 1

SV-1





Comments:



April 04, 2012





Page 6 of 9 Ver 1


Matrix:

Location Code:

Rush Request:

P.O.#:


Analyzed by:

AIR

ESPL

72 Hour

212117-2

03/28/12

LB

see "By" below

Laboratory Data

SV-3

Phoenix ID: BB60085

03/30/12

1:15

11:04




Date

Date Time



SDG ID: GBB60083

Client ID:



















0.51 1,4-Dichlorobenzene 0.166 1.0 KCA TO153.06 04/02/12






10.2 Acetone 0.421 1.0 KCA TO1524.2 04/02/12


0.56 Benzene 0.313 1.0 KCA TO151.79 04/02/12


Page 7 of 9 Ver 1

SV-3








ND Carbon Disulfide 0.321 1.0 KCA TO15ND 04/02/12




0.32 Chloroform 0.205 1.0 KCA TO151.56 04/02/12




5 Cyclohexane 0.291 1.0 KCA TO1517.2 04/02/12



13.1 Ethanol 0.531 1.0 KCA TO1524.7 04/02/12 1



0.68 Heptane 0.244 1.0 KCA TO152.78 04/02/12


1.48 Hexane 0.284 1.0 KCA TO155.21 04/02/12



8.09 m,p-Xylene 0.230 1.0 KCA TO1535.1 04/02/12



0.99 Methylene Chloride 0.288 1.0 KCA TO153.44 04/02/12


3.95 o-Xylene 0.230 1.0 KCA TO1517.1 04/02/12


ND sec-Butylbenzene 0.182 1.0 KCA TO15ND 04/02/12 1




17.1 Toluene 0.266 1.0 KCA TO1564.4 04/02/12








Page 8 of 9 Ver 1

SV-3





Comments:



April 04, 2012





Page 9 of 9 Ver 1

QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD




SDG I.D.: GBB60083

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPDLimits

Blankug/m3


VolatilesND ND1,1,1,2-Tetrachloroethane ND NC114 ND ND 70 - 130 20ND

ND ND1,1,1-Trichloroethane ND NC108 ND ND 70 - 130 20ND

ND ND1,1,2,2-Tetrachloroethane ND NC104 ND ND 70 - 130 20ND

ND ND1,1,2-Trichloroethane ND NC95 ND ND 70 - 130 20ND

ND ND1,1-Dichloroethane ND NC104 ND ND 70 - 130 20ND

ND ND1,1-Dichloroethene ND NC106 ND ND 70 - 130 20ND

ND ND1,2,4-Trichlorobenzene ND NC118 ND ND 70 - 130 20ND

0.30 0.361,2,4-Trimethylbenzene ND 18.2101 1.47 1.77 70 - 130 20ND

ND ND1,2-Dibromoethane(EDB) ND NC97 ND ND 70 - 130 20ND

ND ND1,2-Dichlorobenzene ND NC90 ND ND 70 - 130 20ND

ND ND1,2-Dichloroethane ND NC107 ND ND 70 - 130 20ND

ND ND1,2-dichloropropane ND NC94 ND ND 70 - 130 20ND

ND ND1,2-Dichlorotetrafluoroethane ND NC99 ND ND 70 - 130 20ND

ND ND1,3,5-Trimethylbenzene ND NC103 ND ND 70 - 130 20ND

ND ND1,3-Butadiene ND NC101 ND ND 70 - 130 20ND



ND ND1,4-Dioxane ND NC85 ND ND 70 - 130 20ND

ND ND2-Hexanone(MBK) ND NC88 ND ND 70 - 130 20ND

ND ND4-Ethyltoluene ND NC106 ND ND 70 - 130 20ND

ND ND4-Isopropyltoluene ND NC112 ND ND 70 - 130 20ND

ND ND4-Methyl-2-pentanone(MIBK) ND NC92 ND ND 70 - 130 20ND

10.1 8.44Acetone ND 17.998 24.0 20.0 70 - 130 20ND

ND NDAcrylonitrile ND NC100 ND ND 70 - 130 20ND

0.35 0.35Benzene ND 0.099 1.12 1.12 70 - 130 20ND

ND NDBenzyl chloride ND NC93 ND ND 70 - 130 20ND

ND NDBromodichloromethane ND NC101 ND ND 70 - 130 20ND

ND NDBromoform ND NC105 ND ND 70 - 130 20ND

ND NDBromomethane ND NC101 ND ND 70 - 130 20ND

ND NDCarbon Disulfide ND NC118 ND ND 70 - 130 20ND

0.08 0.08Carbon Tetrachloride ND 0.0105 0.503 0.503 70 - 130 20ND

ND NDChlorobenzene ND NC103 ND ND 70 - 130 20ND

ND NDChloroethane ND NC100 ND ND 70 - 130 20ND

ND NDChloroform ND NC107 ND ND 70 - 130 20ND

ND NDChloromethane ND NC99 ND ND 70 - 130 20ND

ND NDCis-1,2-Dichloroethene ND NC99 ND ND 70 - 130 20ND

ND NDcis-1,3-Dichloropropene ND NC93 ND ND 70 - 130 20ND

ND NDCyclohexane ND NC103 ND ND 70 - 130 20ND

ND NDDibromochloromethane ND NC100 ND ND 70 - 130 20ND

0.57 0.69Dichlorodifluoromethane ND 19.0112 2.82 3.41 70 - 130 20ND

159 147Ethanol ND 7.8100 299 277 70 - 130 20ND

Page 1 of 2

QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD

SDG I.D.: GBB60083

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPDLimits

Blankug/m3

0.39 0.37Ethyl acetate ND 5.3109 1.40 1.33 70 - 130 20ND

ND 0.24Ethylbenzene ND NC106 ND 1.04 70 - 130 20ND

ND NDHeptane ND NC94 ND ND 70 - 130 20ND

ND NDHexachlorobutadiene ND NC116 ND ND 70 - 130 20ND

0.40 0.33Hexane ND 19.2101 1.41 1.16 70 - 130 20ND

5.11 4.91Isopropylalcohol ND 4.076 12.6 12.1 70 - 130 20ND

ND NDIsopropylbenzene ND NC110 ND ND 70 - 130 20ND

0.84 0.86m,p-Xylene ND 2.4107 3.64 3.73 70 - 130 20ND

0.75 NDMethyl Ethyl Ketone ND NC106 2.21 ND 70 - 130 20ND

ND NDMethyl tert-butyl ether(MTBE) ND NC107 ND ND 70 - 130 20ND

0.82 0.35Methylene Chloride ND 80.3105 2.85 1.22 70 - 130 20ND

ND NDn-Butylbenzene ND NC116 ND ND 70 - 130 20ND

0.29 0.32o-Xylene ND 9.8107 1.26 1.39 70 - 130 20ND

ND NDPropylene ND NC102 ND ND 70 - 130 20ND

ND 0.30sec-Butylbenzene ND NC134 ND 1.64 l70 - 130 20ND

ND NDStyrene ND NC103 ND ND 70 - 130 20ND

0.20 0.21Tetrachloroethene ND 4.995 1.36 1.42 70 - 130 20ND

ND NDTetrahydrofuran ND NC120 ND ND 70 - 130 20ND

1.76 1.56Toluene ND 12.091 6.63 5.88 70 - 130 20ND

ND NDTrans-1,2-Dichloroethene ND NC112 ND ND 70 - 130 20ND

ND NDtrans-1,3-Dichloropropene ND NC93 ND ND 70 - 130 20ND

0.21 0.20Trichloroethene ND 4.989 1.13 1.07 70 - 130 20ND

0.27 0.23Trichlorofluoromethane ND 16.0109 1.52 1.29 70 - 130 20ND

ND NDTrichlorotrifluoroethane ND NC108 ND ND 70 - 130 20ND

ND NDVinyl Chloride ND NC100 ND ND 70 - 130 20ND

104 105% Bromofluorobenzene 115 1.0101 104 105 70 - 130 20115

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.





NC - No Criteria

Page 2 of 2

manhattan, new york remedial investigation … new york remedial investigation ... report sco soil...

Documents