manufacturing procedure for coil mill
TRANSCRIPT
Your Trust and Success, Our Tomorrow
POSCO
Manufacturing Procedure Specification
For Hot Rolled Coil
Hot Rolled Products Technical Service Group
Document No Revision No Date Prepared by Approved by
P-MPS-H1202 0 29. Mar. 2012 Park, Yong Keun Jung, Hyo An
Steel Grade : API 5L X60MS PSL2
Project : ONGC Cluster 7
Customer : JINDAL SAW LTD.
Size (mm) : 17.50 x 1211 x C
Page 1 of 39
P-MPS-H1202 Rev. 0
PARTⅠ. General Information
1. General Item
2. Main Production Facilities
PARTⅡ. Manufacturing Procedure
1. Steel making
2. Continuous casting
3. Hot rolling
PART Ⅲ. Quality Assurance System
1. The System of Quality Planning & Quality Control
2. Identification System of Slab, Hot Coil in Manufacturing Process
3. Control of Manufacturing Process
PART Ⅳ. Quality Specification
1. Chemical Composition
2. Mechanical Property
3. Dimensional Property
C O N T E N T S
Page 2 of 39
P-MPS-H1202 Rev. 0PARTⅠ. General Information
1. General Item
1) Name : Pohang Iron & Steel Co., Ltd. (POSCO)
2) Address
- Head Office : 1, Koedong-dong, Pohang City, Kyungsangbuk-do, Korea
TEL : 054-220-0114, FAX : 054-220-6000
- Seoul Office : POSCO CENTER, 892 Daechi-4dong Kangnam-gu Seoul, Korea
TEL : 02-3457-0114, FAX : 02-3457-1999
- Pohang Works : 5, Dongchon-dong, Pohang City Kyungsangbuk-do, Korea
TEL : 054-220-0114, FAX : 054-220-6000
- Gwangyang Works : 700, Kumho-dong, Kwangyang City Chunranam-do, Korea
TEL : 061-790-0114, FAX : 061-790-7000
Page 3 of 39
P-MPS-H1202 Rev. 0
2. Main Production Facilities
Blast furnace
Iron making process by ore reduction and melting
Converter
Steel making process by removing impurities
Continuous casting
Hot rolling
Hot coil making process by rolling slabs
Roughing
Mill
Reheating
Furnace
Finishing
MillCOIL
PARTⅠ. General Information
Page 4 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
1. Steel making
1) Raw materials
- Raw materials making steel are basically Molten iron which is made by ore reduction
and melting in blast furnace process and subsidiary raw materials such as Scrap, Fe-Si,
Si-Mn, Fe-Mn, Al wire, Fe-Nb, LC Fe Mn, H C Fe Mn, etc. Ore and subsidiary raw
materials are mainly imported. These are tested at the Quality Control Laboratory for
suitability before unloading in the plant. The quality of raw materials is guaranteed by
the supplier with a test certificate.
- Quality control of molten iron used at steel making plant is to reduce impurities
involved in molten iron. Main elements affecting the quality of steel in steel making
process are P [Phosphorus], S [Sulfur], Si [Silicon] and Mn [Manganese]. Si, S and P
level of Hot metal made in blast furnace is finally reduced by hot metal pretreatment
process before Steel making process.
Generally ,the chemical composition levels of molten iron after hot metal pretreatment
are as follows:
Page 5 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
1. Steel making
Ar, N2
Refining of slags
Mn ore
Hot Metal Pretreatment
▶Scale, CaO, CaF2
mill scale
Blast furnace
Desiliconization De [S], [P]
slag removal slag removal
< Hot metal pretreatment follow >
Generally ,the chemical composition levels of molten iron after hot metal pretreatment
are as follows : C: 4.0 ~4.5%, Mn: 0.3 ~0.4%, Si: < 0.35%, P: < 0.10%, S: < 0.010%
Page 6 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
1. Steel making
Hot Matal
Flux + N2
2) Hot metal pretreatment station (HMPS)
- Before pouring hot metal steel into the converter, pretreatment will be done to control
S and P content, to meet sour service. Through this re-treatment, for CDPS(Charring
Ladle dephosphorus & desulfurizing), Na2CO3 and CaF2, etc. will be injected into
Torpedo Ladle Car through the lance while hot metal is being stirred for 50-60 minutes
and slag is removed. After CDPS, the level of S and P is : S <0.010%, P <0.030%.
Page 7 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
1. Steel making
Molten iron
Reaction on slag
2nd conbustion of CO
SRM
DegassingO2
Slag formation
dissolution of
Subsidiary
Aw materials
Oxidation on
Melting point
Scrap Melting
3) Steel Making in the LD Converter (Basic oxygen furnace)
- Steel is made in the 250~300 Ton LD Converter (Basic oxygen furnace) having top
oxygen blowing lance. This process is mainly to reduce impurities such as carbon, silicon,
phosphorus, sulfur by blowing oxygen and to make Steel having chemical compositions
required for customer by mixing Ferro alloy into hot metal. A Charge mix of 90 % Hot
metal and 10% shredded scrap is added to the converter. After the scrap is charged
through clamshell type scrap bucket, the hot metal is charged using a Pelican type ladle.
Page 8 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
1. Steel making
4) Procedure
- The scrap and hot metal are charged into the LD converter. When oxygen blowing
starts after hot metal charging into converter, Lime and dolime are added in a regulated
manner for proper slag. Using a Lance Manipulator, oxygen is continuously lanced in
the furnace at the rate of 700 ~900 ㎥/min for 16~17 minutes to reduce carbon, silicon
contents and to ensure the formation of foamy slag. Formation of foamy slag reduces
nitrogen pick-up, helps remove nitrogen/hydrogen, prevents radiation losses and
enhances the slag-metal reaction. Carbon, oxygen and temperature are checked two
times using a sub lance probe during oxygen blowing. When the level of dissolved
oxygen is reached below 900 ppm, he heat is tapped. Level of oxygen, carbon and
temperature at this moment are as follows: C:≤ 0.05 % , P:≤ 0.020% , O2: 600~ 900
ppm, Temperature : 1720 ±25 ℃. Slag -free tapping is done using a plug and slag
check ball at tap hole. During tapping, the metal is deoxidized using alloys like Fe-Al,
Fe-Si. Fe-Mn add to achieve the range of chemical composition of API Grade.
Page 9 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
1. Steel making
O2 Lance
Upper vesselO2 Blowing
(CO(g)+ ½ O2)
lower vessel
Argon gas
5) Vacuum Degassing
- Ladle is placed to the VD vessel named as RH by crane. The vessel is closed and
vacuum pumps are started. For the purpose of degassing process (H, N, etc.), operate
decreasing the pressure in the vacuum state and stirring the ladle. The same time molten
iron in VD vessel is controlled for reducing non-metallic inclusion, temp/chemical comp.
- After releasing the vacuum, cover is moved out. Steel temperature and chemistry are
checked by the final aim chemistry of API Grade. Any corrective additions required are
made. Ladle is lifted by crane for casting.
Page 10 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
1. Steel making
Ca-Si Wire
Transient
Reaction
Permanent
Reaction
SLAG
Molten Steel
Cover
Bubbling Ladle furnace
Or Powder
6) Steel refining in the Powder Injection (Ca-Si)
- Powder Injection ( capacity 250~300 Ton ) is used to refine the steel by ensuring
temperature and chemistry homogenization, alloying adjustment, removal of oxide and
alumina inclusion, desulphurization and spheroidizing of inclusion by Ca-Si powder or
wire injection. Purging with argon and Ca-Si powder or wire injection is done
continuously during the entire processing period.
Page 11 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
2. Continuous casting
LADDLETURRET
LADLE
TUNDISH
MOLD(Primarycooling)
Pinch roll
BENDING DEVICE
Secondary
cooling
Torch cutter
MOLD OSCILLATION
Reforming roll
Soft Reduction
1) Process of continuous casting
- Slabs are continuously cast in slab caster with 2 strands. The slabs can be cast on the
casting machine. Slabs can be cut to length as per requirement of Hot Strip Mill. The
process of continuous casting is as follows:
Page 12 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
2. Continuous casting
1) Procedure
- The ladle sits in the ladle turret and the turret is rotated 180 degrees to the Casting
position. Protection of liquid steel from ladle to tundish and tundish to caster mould.
Steel temperature in tundish is about 1545 °C (-15/+25 °C) To avoid any contamination
(pickup of oxygen and nitrogen) from the atmosphere, shrouding is used from ladle to
tundish and from tundish to mould. Shroud is pressed by a manipulator onto the outer-
nozzle of the ladle slide gate. Sealing is done by a gasket introduced into this joint.
Argon is also passed through this shroud. Shroud material alumina graphite between
tundish and the mould a submerged entry nozzle (SEN) of alumina graphite is used.
The SEN dips 140 mm into the liquid steel in the mould. The liquid steel in the mould is
covered with a mould powder, which prevents contact of liquid steel with air and also
provides mould lubrication.
Page 13 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
2. Continuous casting
2) Tundish preheating
- Spray mass with 60% Al2O3 is used in tundish. Appropriate preheating is essential for
trouble free casting and satisfactory quality. Too cold a tundish, cools the first incoming
liquid steel so that it freezes in the SEN nozzle or causes skulling on the outside of
submerged nozzle. Excessive tundish preheating may damage the refractory material or
melt the tundish lids so causing inclusions in slabs. Preheating is normally done for
about 2.0~3.0hrs and temperature of 1150 °C ~ 1350 °C. Liquid steel in the tundish is
covered with rice husk to prevent contact with air and temperature loss.
3) Secondary cooling
- It can be selected as per the steel grade and water flow rate varied according to the
casting speed.
4) The oscillation stroke length
- It is ± 3.5 mm. The pressure at the pinch rolls varies from 40~80 bars based on the
steel grade and section size being cast.
Page 14 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
2. Continuous casting
5) Casting speed
- Maximum casting speed is 2.2 m/min. However, actual casting speed is adjusted with
respect to quantity of molten steel being poured into mold per hour and superheat in the
tundish as per process standard.
6) Slab surface temperature at the exit end is generally 900 ~1050 °C
7) Charge No. & Slab No. are marked using a marking machine to maintain the identity
and traceability.
Page 15 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
2. Continuous casting
T 250mmSlabThickness
Center of slab width
1/2w
8) Center Segregation Evaluation Procedure
- Method: Slab macro etching Ammonium Persulphate ,(NH4)2S2O8 solution
- Density and Etching Time: 15~20%, 5 minutes
- Sampling: Samples for macro-etching shall be cut from the head of the 2nd or 3rd slab
of each strand of cast while first slab is rejected. Sampling will be per strand per casting
sequence and its position is 1/2w
Casting direction
.. .. ..
L 100mm
Page 16 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
2. Continuous casting
Classification Definition
Class1
Segregation shall be dot pattern(not continuous).
Density: 10 or less dots/100mm for dot of size 1mm≤dot≤3mm
No dots of size more than 3mm shall be identified.
Class2
Segregation shall be dot pattern(not continuous).
Density: 11 to 18dots/100mm for Dot of size 1mm≤dot<5mm, with the limitation of
maximum 5 dots/100mm for dot of size 3mm<dot<5mm.
Class3
Degregation shall be dot pattern
Density: 1) At least one dot/100mm for dot of size≥5mm or
2) 19 dots/100mm for dots of all sizes or
3) 6 dots/100mm for dots of size 3mm<dot<5mm.
Class4 Continuous black dots more than 10mm in length and more than 1mm in thickness.
Definition
Dot Clear black indications of diameter 1mm and greater.
ContinuousSome clear black indications combined with each other for the total width greater than
10mm, with no area of thickness<1mm.
Size of DotLength of clear black indication for the direction of either thickness or width whichever
is greater.
9) Center Segregation Classification level allowed for API Steels : Class 1, Class 2
Page 17 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
3. Hot rolling
#1 #2 #3
F1 ~ F7E/H C.S FSB
RHF
VSB
R2R1
Lamnar flow
#1 #2Thickness gauge
D.C
Shape Meter
1) General Process
2) Reheating Furnace
- Three walking beam reheating furnaces are used to reheat the slab for rolling. The
slabs are heated at a temperature of 1100 ~ 1290 ºC. The heating time is 3 to 4 hours
with a soaking time of 20~80 minutes. Slab of maximum 12.0 m length can be charged
into furnace.
- Slabs are charged in the furnace as the schedule given by the Production Process
Control Department. A coil number is assigned to each slab scheduled to be rolled.
- Uniform slab heating and soaking within a preset is automatically accomplished.
Page 18 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
3. Hot rolling
3) Roughing Mill
- The roughing mill consists of 2 Hi one stand and 4 Hi one stand reversing mills with
edger for width control and descaling facility on entry and exit sides of the mill. In this
process, slab is made into rolling materials (bar) with proper shape, thickness and width.
In the entry and exit area of the roughing mill, the edger rolls the bar in crosswise
direction using the automatic width control (AWC) system.
- Primary scale is completely removed by using vertical scale breaker (VSB) and
hydraulic descaler of 100~150 kg/cm2. The descaling unit is always maintained for the
best performance.
- Required dimensions are obtained by ensuring proper edger operation and by giving
6~10 number of passes ( R1: 3 ~ 5, R2: 3 ~5 passes )
Page 19 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
3. Hot rolling
4) Finishing Mill
- The finishing mill consists of 4 Hi- 7 stands in tandem & equipped with Hydraulic
Automatic Gauge control, work roll bending and work roll pair crossing systems.
- The finishing scale breaker (FSB) and the crop shear operations are ensured at the
seven stand finishing mill.
- A Quick Roll change system is used for changing the work rolls after every optimum
rolling schedule depending on the thickness and size rolled.
- In finishing mill, Strip thickness and width are controlled according to specified
standards and rolled for top surface and shape quality using finishing temperature at
target ±40 ℃ for API Grade application. The pair cross mill and on-line grinder (ORG)
control the shape and crown of the strip, improving both the productivity and quality.
Page 20 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
3. Hot rolling
5) Cooling & Coiling
- The finishing mill, the strip passes to the run-out table where it is then coiled. While
being rolled along the table, the strip is sprayed with water to cool it to the proper
temperature to have a good mechanical property. For API Grade Coiling temperature
is target ±40℃.
- A hydraulic Automatic Gauge Control (AGC) is used to control the gauge of the Hot
Rolled Coil being manufactured.
- Coil numbers on the strip are marked on each coil.
- Delivery condition is thermomechanically controlled rolling(TMCP) and accelerated
cooling
Page 21 of 39
P-MPS-H1202 Rev. 0PARTⅡ. Manufacturing Procedure
3. Hot rolling
6) Inspection and testing
- An X-ray thickness gauge and width gauge checked the dimensions of each coil during
rolling. However, to counter check the dimensions of these coils, one in every ten coils is
measured manually for dimensions. Also, the coils are inspected for any surface.
- Sample drawn from the coil is tested at the Products Inspection Section of Quality
Technology Department, as per sampling plan. 1 coil is tested per heat per size rolled.
- If the test coil does not conform to the specification, the retest carried out on two more
coils from the same heat. If the retest conform to the specified requirement, the heat (or
lot) except the first failed one can be accepted. If the result of the retest fail, all coils in
the heat (or lot) is rejected
- A mill certificate is issued for the coils conforming to the specification and hands over
to the customer.
- All slabs are inspected and All coils are inspected by SDD (Surface Defects Detector)
- Mill Test Certificate shall be issued according to EN 10204. 3.1
Page 22 of 39
P-MPS-H1202 Rev. 0PARTⅢ. Quality Assurance System
1. The System of Quality Planning & Quality Control
Dept .
Activity
Marketing
Division
Quality
Service
Department
Production
Process
Control
Dept
Plant(Mill) Quality Technology Dept Maintenance,
Electrical
Control
Supporting
Dept.
Testing
Service Sec
(Chemical
test)
Product
Inspection
Sec
(Material Test)
Quality
Improvement
Department
Plan
Do
Check
Action
Customer’s
information
Contract
Quality
Inspection
Standard
Corrective
Action
Order
Sheet
Quality
Design
Manufacturing
Review
Trial
Production
Inquiry
Production
Planning
Manufacturing Specification
Marking
Test & ExaminationQuality
Improvement
Quality
Control
Committee
Quality
System
Control of
Operating
Measuring
& Testing
Equipment
Reject
Accept
Page 23 of 39
P-MPS-H1202 Rev. 0PARTⅢ. Quality Assurance System
2. Identification System of Slab, Hot Coil in Manufacturing Process
Iron
Marking
Hot Metal
Pretreatment
Oxygen
BlowingBubbling
Powder
Injection
Vacuum
Degassing
Continuous
Casting
Torch
Cutting
Cold Charge
Rolling Slab
Scarfing
(Cutting)
ReheatingHot Charge
Rolling Slab
Hot Direct
Rolling Slab
Converter
R H
P I
Steel making practice No
Order NoHeat No Slab No
Rolling program No
Hot Rolling No
Order. No Sequence No Heat No
Steelmaking Plant Code
1st Cut Piece No
In Strand
Sequence No
Month Code
Descaling Rolling Water Cooling Air Coiling
Skin Pass
Rolling
Dividing
Rolling
Packing &
Marking
Mill Code
Hot Coil No(Casting program No)
Page 24 of 39
P-MPS-H1202 Rev. 0PARTⅢ. Quality Assurance System
3. Control of Manufacturing Process
Process Process Simbol Equipment Control Item Record
Hot Metal
PretreatmentLance, Slag Skimmer Desulfurizing
Data Base
Hot Metal Input Lance, Crane Mix Ratio, Input Time
Oxygen BlowingConverter,
Temperature CheckerTemperature, Blowing Time
Bubbling(LF or RH) B/B Stand (LF, RH) Temperature, Time
Continuous CastingTundish, Temperature
Auto CheckerTemperature
1st Cooling Mould, MLACCasting Speed, Cooling
Condition
2nd Cooling Foot Roll, SegmentRoll Gap,Cooling Condition
Torch Cutting Torch Cutting Machine SLAB Profile
Slab Finishing Deburrer, Scarfer Defect. Scarfing Method
Slab Reheating FurnaceReheating Time,
Temperature
Descaling DescalerWater Pressure, Water
Amount
Page 25 of 39
P-MPS-H1202 Rev. 0PARTⅢ. Quality Assurance System
3. Control of Manufacturing Process
Process Process Simbol Equipment Control Item Record
Rough Mill Roughing MillPass Schedule,
Temperature
Data Base
Finish MillFinishing Mill,
r-Ray Gauge
Temperature, Profile,
Thickness, Width
Water Cooling Laminar Flow Cooling Pattern
Coiling Down Coiler Coiling Temperature
Inspection &
Material Test
Auto Material Tester
Ruler
Defect,
Mechanical Properties
RecoilingSkin Pass Mill,
Dividing Mill, Gauge
Profile, Defect,
Thickness, Width
Weighing Weigher Weight
Banding Machine,
Label Printer
Parking Pattern,
Marking ItemPacking & Marking
Storage Crane Storage Condition
: Manufacturing : Inspection, Judging : Weighing
Page 26 of 39
P-MPS-H1202 Rev. 0PART Ⅳ. Quality Specification
1. Chemical Composition
1) Test Frequency: Ladle analysis : One sample per heat
Product analysis : Two samples from different coils per heat
2) CE (IIW) = C+ Mn/6 + (Cr+Mo+V)/5 + (Cu+Ni)/15 (API 5L 44th Ed. 9.2.5)
3) CE (Pcm) = C+Si/30+Mn/20+Cu/20+Ni/60+Cr/20+Mo/15+V/10+5B (API 5L 44th Ed. 9.2.4)
4) The soluble aluminium to nitrogen, Al/N shall be at least 2:1
5) Ca/S ratio shall be minimum 2.0 and maximum 3.0. However, there is no restriction on
maximum value of Ca/S ratio in case S<0.0015% and maximum value of Ca is 50 ppm.
ITEM C Si Mn P S Nb V
Range ≦ 0.08 0.15~0.35 ≦ 1.45 ≦ 0.015 ≦ 0.002 ≦ 0.05 ≦ 0.08
ITEM Ni Cr Cu Mo Ti Al N
Range ≦ 0.30 ≦ 0.30 0.05~0.35 ≦ 0.08 ≦ 0.06 0.01~0.06 ≦ 0.01
ITEM B Nb+V Nb+V+Ti Cu+Ni Cr+Mo CE Pcm
Range ≦0.0005 ≦ 0.1 ≦ 0.12 ≦ 0.40 ≦ 0.25 ≦ 0.19
Page 27 of 39
P-MPS-H1202 Rev. 0PART Ⅳ. Quality Specification
2. Mechanical Property * All mechanical properties will be guaranteed in coil condition only
1) Tensile Properties (ASTM A370/API 5L)
- Test Frequency : One sample per heat
- Sampling : Rolling tail of the coil and ¼ width
- Direction : Transverse direction
- Value : Table A (→)
※ Longitudinal test result will be submitted by separate sheet for information only.
2) Bending Test (ASTM A370/API 5L)
- Test Frequency : One sample per heat
- Sampling : Rolling tail of the coil and ¼ width
- Direction : Transverse direction
- Specimen when bent on a jig of radius 2 times the thickness shall be free from any cracks
YP (MPa) 415-540 Mpa
TS (MPa) 540-750 Mpa
YR 0.90 maximum
EL (%) 30% min on 2” gauge length
[ Table A ]
Page 28 of 39
P-MPS-H1202 Rev. 0PART Ⅳ. Quality Specification
2. Mechanical Property * All mechanical properties will be guaranteed in coil condition only
3) Hardness Test (ASTM A370)
- Test Frequency : One sample per heat
- Sampling : Rolling tail of the coil and ¼ width
- Direction : Transverse direction
- Value : 210 HV 10 maximum
4) Charpy V-notch Impact Test (ASTM A370/API 5L)
- Test Frequency : One set per heat
- Sampling : Rolling tail of the coil and ¼ width
- Direction : Transverse direction
- Value : Table B (→)
- Temperature : 0℃
- Full size specimen
Enegry
(J)
Individual absorbed energy = 100 Joules min
Average absorbed energy = 100 Joules min
Shear Area
(%)
Shear fracture area per specimen = 85% min
Average Shear fracture area = 85% min
[ Table B ]
Page 29 of 39
P-MPS-H1202 Rev. 0PART Ⅳ. Quality Specification
2. Mechanical Property * All mechanical properties will be guaranteed in coil condition only
5) DWTT Test ( API RP 5L3)
- Test Frequency : One set per heat
- Sampling : Rolling tail of the coil and ¼ width
- Direction : Transverse direction
- Value : Table C (→)
- Temperature : 0℃
6) HIC Test
- Test Frequency : One set per heat
- Sampling : Rolling tail of the coil and ¼ width
- Method : NACE TM 0284-2003 Solution A
- Immersion Period : 96 hours
- Temperature : 25 +/- 3℃
- Value : CSR ≤ 1%
Shear Area
(%)
Shear fracture area per specimen = 85% min
Average Shear fracture area = 85% min
[ Table B ]
Page 30 of 39
P-MPS-H1202 Rev. 0PART Ⅳ. Quality Specification
2. Mechanical Property * All mechanical properties will be guaranteed in coil condition only
7) Four Point Bend Test
- For point bend test specimen preparation & size shall be as per ASTM G39 except that the
thickness shall be minimum 5mm. One set of the three specimens from the steel coil shall be
taken transverse to the direction of rolling.
- Specimen shall be bent using four point loading Jigs to reach a stress level of 72% SMYS
and then immersed in a NACE solution as per standard TM 0177-2005 for aperiod of 96 hrs
with the inner surface/root in tension.
- Reference purpose only for three heats.
8) Ferrite Grain Size (ASTM E112)
- ASTM No.7 or finer
Page 31 of 39
P-MPS-H1202 Rev. 0PART Ⅳ. Quality Specification
3. Dimensional Property
1) Thickness
- +0.25mm to +1.0mm
2) Width
- -0mm to +20mm
3) Camber
- 20mm max in 10M
4) Telescopicity
- 50mm max
5) Other
- Value : As per API 5L 44th Ed.
Page 32 of 39
P-MPS-H1202 Rev. 0
APPENDIX –1
Apparatus for the Determination of Chemical Analysis and Mechanical Test
Page 33 of 39
P-MPS-H1202 Rev. 0
o Chemical Analyzer
Apparatus Type Quantity MakerElements to be
Determined
C,S DeterminatorC,S-244C,S-444
1 LECO C,S
N,O DeterminatorT/C-136T/C-436
1 LECO N,O
H-Determinator RH-402 1 LECO H2
C-Determinator IR-412 1 LECO C
S-DeterminatorIR-232IR-432
1 LECO S
Automic AbsorptionSpectrometer
PERKIN-5000 1 PERKINELMER
Al,Mn,Pb,Zn,Mo,Na,K,Si,Ni,Cu,B,Cr,Ti,Ag,Ca,
Mg,Co,Cd,V,Fe,Sn,Bi,Cs,Sb,Pd,Se,Hg,Hs,Ta,Zr,Ga,RB
SpectrometerUV150-02
1 SHIMADZU CORP
P,S,Mn,Si,Ni,Cr,Mo,V,Cu,Sb,Co,Nb,Ti,Al,Sn,Mg,B,Zr,Pb,As,Zn,Ca,Ta,Ce,Fe,W,Bi,Ag,
Cd,Ba,Te,Se,La,Pd
Vacuum EmissionSpectrometer
GVM-1016 1 SHIMADZU CORP C,Si,Mn,P,S
X-Ray FluorescenceSIMULTIX-6BRIGAKU-3530VXQ-150A(S)
1
RIGAKURIGACU
SHIMADZU CORP
Fe,Si,Ca,Al,P,S
ICP Spectrometer ICPV-1015 1 SHIMADZU CORP
Fe,P,S,Mn,Si,Ni,Cr,Mo,V,Cu,Sb,Co,Nb,Ti,Al,S
n,Mg,B,Zr,Pb,As,Zn,Ca,Ta,Ce,Fe,W,Bi,Ag,Cd,
Ba,Te,Se,La,Pd
Page 34 of 39
P-MPS-H1202 Rev. 0
o Mechanical tester
Apparatus Type Quantity MakerElements to be
Determined
Tensile TestingUniversalTestingMachine
4Zuick,
ShimadzuCorp
TS, YS, EL, YR, n
Bend TestingHydraulicBendingMachine
1Korea
HydraulicCorp
Bending Property
Impact TestingCharpy V
Notch ImpackMachine
2 KawadezAbsorbed Energy,% of Shear Area
Hardness Test
VickersBrinell
RockwellShore
8 Matsuzawa HV, HrB, HB, HRc, HS
MicrostructuralAnalysis
SEMEPMAOptical
113
PhillisCAN
NipponFGS, AGS other
DWTT TestSeries 3120 1 MAEGAWA % of Shear Area
HIC Test NACE TM 02844
(7 Vessel)Sungwha Plant
BLISTER, CLR,CSR, CTR, ETC
SSCC
Tensile Test 14Ea Sunwha PlantStree : TimeTo Failure
Four PointBent Tester
40Ea Sungwha Plant Streres To Failure
Page 35 of 39
P-MPS-H1202 Rev. 0
APPENDIX 2
Manufacturing Flow Chart and Process Parameters
Page 36 of 39
P-MPS-H1202 Rev. 0
Manufacturing Process Flow Chart of Gwangyang Works
#1 Blast furnace
De - S
Convert
HSM #3
Continuous casting
#1,#2,#3,#4 M/C of
#1 plant
(Hot Metal Pretretment)
(Steel refining in Ladle furnace)
LF (Ca-Si Treatment)
YES
N ≤ 50ppm
RHNO
(Casting into Slab atContinuous caster)
#2 Blast furnace
De–S
Convert
HSM #3 Continuous casting
#1,#2,#3,#4 M/C of
#2 plant
(Hot Metal Pretretment)
(Steel refining in Ladle furnace)
LF (Ca-Si Treatment)
YES
N ≤ 50ppm
RHNO
(Casting into Slab atContinuous caster)
N ≤ 120ppmYES
De-PNO
Page 37 of 39
P-MPS-H1202 Rev. 0
Manufacturing Process Flow Chart and Important Process Parameters which are checked
①
PROCESS STAGE PARAMETERS BEING CHECKED EQUIPMENT USED FREQUENCY OF CHECK
Thermocouple probe,
Slag Skimmer
One per torpedo ladle car
Thermocouple probe, Vaccum
Emission Spectrometer
Minimum one per heat
Thermocouple probe, Vaccum
Emission Spectrometer, o2/N2/H2
Analysis(Determinator. Leco)
Minimum two per heat
Thermocouple probe, Vaccum
Emission Spectrometer, o2/N2/H2
Analysis(Determinator. Leco)
Vaccum level constantly is
controled by computer.
hemistry and o2 three per heat
Thermocouple probe and other
Parameters by continuos
Monitoring computer
Temperature 3~4 per heat.
Other parameters. Continuous
Monitor by computer
Raw Materials
Steel Making in LD
Steel refining in
Ladle furnace
Steel refining in
Vaccum degassing
Casting into Slab at
Continuous caster
Molten iron chemical testing,
Slag removing
Temperature and soluble oxygen
Measurement, chemical analysis
of bath sample
Steel chemistry and temperature,
Homogenization through argon
gas injection
Vaccum level, treatment time
and treatment temperature.
Chemistry and dissolved oxygen
Tundish Temperature, casting
speed, osillation frequency of
mould.
Primary and secondary cooling,
mould powder
Page 38 of 39
P-MPS-H1202 Rev. 0
Slab inspection and
Conditioning
Slab dimentions. S-print and
Surface condition (defects)S-print lab equiped with sample
Preparation equipments and
machine / hand scarfer
S-print : One per heat
Scarfing : Slabs selected
By Quality Evaluation
system
Reheating furnace Temperature profile in SRF,
Reheating rate, soaking time
and temperature
By computer
* ACC : Automatic Combution
Control
Continuous Controling By
ACC, AI(Artificial
Intelligence)
Rolling in Hot strip mill Width, thickness, shape control,
Finishing and coiling temperatures,
Descaling, Weghing and marking
Automatic X-Gauge,
Temperature probe Shape and
Size controled by computer
(ASC, AWC, AGC system)
Automatic X-ray Gauge
Control, continuous full
length FT & CT monitoring
of all coils
Final testing and
inspectionVisual inspection oncoil, Testing
for mechanical properties ( tensile,
bend, Charpy impact test)
Tesile tester, Bend tester,
Impact tester, Microscope,
Image analyzer
Visual inspection : All coils
Mechanical props : 1
sample/thickness/heat
Product chemistry analysis
: one per heat
Packing / Marking As per customer’s specification
or POSCO standardEvery coils
①
Page 39 of 39
P-MPS-H1202 Rev. 0
APPENDIX 3
Packing / Marking
BAND
BUCKLE
Gwangyang Works