martin andersson, application specialist, foss · 2019-10-08 · martin andersson, application...
TRANSCRIPT
Martin Andersson, Application Specialist, FOSS
”We deliver rapid, reliable and dedicated analytical solutions for routine testing to allow for fast decisions on how to maximise value of production of agricultural food products”
Improved predictability and control of manufacturing processes
Safe products and compliance with regulatory requirements
Supplier Receiving points
At-line/In-line production
Quality Control Laboratories
Finished products
Payment, segregation and quality control of raw material
Customer
Customer is using the same analytical system as the supplier
• Hit the target• Understand your yield
• Traceability• Fair trade
Chemical analysis using near infrared: How?
• Spectroscopy is the study of absorption of near infrared light (energy) by molecules
• Near infrared ranges from 780 – 2500 nm• It is a part of molecular spectroscopy
where interaction between light (energy) and matter (molecules).
NIR
• Atoms vibrate with a frequency specific to the molecular bond
• When light hits the vibrating bond, it is just passing through when it does not match the frequency
• When light hits the bond with a matching frequency, the light is absorbed and the vibration intensifies
• Organic bonds absorb NIR light.
400 nm
Color & chemical compositionincluding
-OH-NH-CH
780 nm 2500 nm
T H E L U C K Y R E G I O N
1100 1300 1500 1700 1900 2100 2300 2500Wavelength / nm
Abso
rban
ce (d
ashe
d)1st
deriv
ative
(soli
d)
1100 1300 1500 1700 1900 2100 2300 2500Wavelength / nm
Abso
rban
ce (d
ashe
d)1st
deriv
ative
(soli
d)
1100 1300 1500 1700 1900 2100 2300 2500Wavelength / nm
Abso
rban
ce (d
ashe
d)1st
deriv
ative
(soli
d)
1100 1300 1500 1700 1900 2100 2300 2500Wavelength / nm
Abso
rban
ce (d
ashe
d)1st
deriv
ative
(soli
d)
Water Fat
Protein Starch
• Moisture• Protein• Water Absorbtion• Maltose• Ash• Color L (L*, a*, b*)• Rice Amylose
2019年10月7日 10
Protein
7
8
9
10
11
12
13
14
15
16
7 8 9 10 11 12 13 14 15 16
0.1
7SEP
-
0.0
2
Bias
Infra
tec
LAB
Moisture
8
9
10
11
12
13
14
15
16
8 9 10 11 12 13 14 15 16
0.1
2SEP
-
0.0
4
Bias
LAB
Infra
tec
Color Value
58
59
60
61
62
63
64
65
66
67
68
58 59 60 61 62 63 64 65 66 67 68
0.3
3SEC
0.0
1Bias
Infra
tec
LAB
Maltose
150
200
250
300
350
400
150 200 250 300 350 400
15.
5SEC
-
0.3Bias
Infra
tec
LAB
Raw material reception
production Quality Control Laboratories
Finished products
Improved control of feed manufacturing process
Safe products and compliancewith regulatory requirements
Supplier’s payment, segregationand quality control of raw material
Usually good…
But too late
Raw material reception
Quality Control Laboratories
Finished products
Safe products and compliancewith regulatory requirements
Supplier’s payment, segregationand quality control of raw material
production
Improved control of feed manufacturing process
1 2
3
1. Windows reflectance
2. Direct light
3. Powder probe
4. Lateral Transmittance
probe4
Fine sticky powdersNIR range: 1100 – 1650 nm
• Whole milk powder• Skim milk powder• Whey powder• Infant formula powder• Caseinate powder• Starch powder• Corn/wheat gluten powder
Solids on open conveyor in reflectanceNIR range: 1100 – 1650 nm
• Feed ingredients• Feed pellets• Minced meat• Pasta• Chips
For liquid & slurriesNIR range: 850 – 1050 nm
• Soy Milk• Butter• Mozzarella• WPC / MPC• Cream• Fresh Cheese• Processed Cheese• Mechanical Debone Meat• Wet Pet Food• Whole Grain• Gluten/starch slurries
Fluid PowdersNIR range: 1100 – 1650 nm
• Feed ingredients• Feed mix• Feed pellets• Soy/rape meal• Whole Wheat• Whole Corn• Flour• Cocoa liquor • Etc.
30° 45° 80°
Limit of responsibilityNote: the Kepware license will be needed with ISIscan Nova and Beckhoff
Graph view of noisy measurements with batch average as a thick red line, and moving average as thick black line.
New interface
8. Optimizing samples for reference analyses
3. Back up sample data and instrument data
2. Instrument downtime,
1. Instrument management 4. Monitoring and optimizing instrument performance
5. Securing basic Standard Operation Procedures are followed
6. Maintenance plan for your instrument
7. Calibration accuracy on your instrument
9. Documenation for audit trail?
11. ANN
10. Best possible performance for all your samples
12. Complete backup and auto-documentation
FossManager (Pro) FossAssure ProFossAssure
FREE 90 days trial
FossCalibrator (Pro)
FREE 90 days trial
”A challenge I have often encountered is that when you are working within the plant, and the instrument seems to be working OK, then everyone is happy. However, when you start getting out of spec results, you get challenged. Is it the process or the instrument? With FossAssure, we can point to and demonstrate that the instrument is not the source of the issue. It gives peace of mind because I know that someone with the right education is keeping an eye on the instruments and how they are running.”
Jennifer Robinson, VP of Corporate Quality Assurance