material characterization at desy - amap gmbh€¦ · desy spin-offs as suppliers 4 start-ups – 4...

Sabine JaehmlichAMAP ColloquiumAachen, 3 rd May 2018

Material characterization at DESYBest practice , benefits and access .

DESY Today .

Presentation Title | Firstname Lastname | <program short term> | <research unit short term>

2

2018

PETRA III

XFEL

FLASH I+II

DESY. The most brilliant X -ray light worldwide.ZEU

• over 400 Mio. € investments p.a. in/around Hamburg in recent years

• over 400 Mio. € investments p.a. in/around Hamburg in recent years

• ca. 220 Mio. € base budget + 100 Mio. € third party funding

• ca. 220 Mio. € base budget + 100 Mio. € third party funding

• more then 3.000 users per year from 45 countries

• more then 3.000 users per year from 45 countries

• 2.378 employees• 2.378 employees

Source: EMBL.

PETRA III Beamlines .19 beamlines for multidisciplinary research.

P01 DynamicsP02 Hard X-Ray Diffraction BeamlineP03 MINAXSP04 XUV BeamlineP05 Imaging BeamlineP06 Hard X-Ray Micro/Nano-ProbeP07 High Energy Materials ScienceP08 HighRes DiffractionP09 Resonant Scattering and DiffractionP10 Coherence ApplicationsP11 Bio-Imaging and DiffractionP12 BioSAXSP13 Macromolecular Crystallography IP14 Macromolecular Crystallography IIP22 HAXPESP23 In-situ and Nano DiffractionP24 Chemical CrystallographyP64 Advanced XAFSP65 Applied XAFS

Synchrotron research is part of our lives .

Ice cream texture

PHARMA & COSMETICSFOOD INDUSTRY Suntan cream

Adhesives for nappies

MATERIALS SCIENCE

New Pharmaceuticals

BIOTECHNOLOGY

CHEMICAL INDUSTRY

Dye

… and can improve our future .

AUTOMOTIVE & AEROSPACE

New alloys & stress tests

CHEMISTRYCharacterization & performance

of coatings, paintings & new materials

ENERGY & CATALYSIS

Analysis of trace elements in fuels & catalysis performance

Why not a home source? .

What makes synchrotrons special .and home sources can not achieve.

• Flux

• Collimation

• Absorption

• Which instrument fit my needs?

• Market prospection

� 19 state-of-the art stations available

� Scientific consultancy services

• Purchase and maintenance

• Upgrading & Deprecation costs� Upgrading & New Construction

� Hundreds of million investment

• From minutes to hours� From seconds to few minutes

Synchrotron radiation is time-cost effective .Outsourcing of R&D

Home source Synchrotron facilities

Synchrotron radiation is a non-destructive method

Enabling Innovation together with the Industry

Enables

Supplies

Industrial Suppliers

DESY Spin-offs as Suppliers4 Start-ups – 4 new Suppliers

Invention by a Scientists at DESY

evaluating the technology

founding a company (eventually)

supplying DESY with their products

• ideas developed by DESY or with DESY scientist can lead to new companies

• the products then produced by these companies often are needed by DESY

• new supplies come up, but not only for DESY, but also for other institutes

• all of our four spin-offs now supply DESY (and many others) with their products

Partner to the Industry .

Med Tech

Complex Materials

Chemical industry

Pharma

Optics

Accelerator Technology Automotive

Aerospace

Which Industry?

Drug Design Medical

Imaging

Customized Magnetic Sensors

3D - Printing

Quality Testings

Protein Crystallography

DetectorDevelopment

Residual Stress Testing

MTCA.4

High Precision X-Ray Mirrors

Partner to the Industry .Two Access Modes

Methodorientated request

SCIENCE

Challengeorientated

request

INDUSTRY

Data Management

Prototypes:

Design & Construction

Problem Solver:

ScientistsEngineers

Technicians Technologies Nano-Science:

Structural AnalysesMaterial Characteristics

Nano-ProcessesDrug-Design

Perfect Ecosystem for Enterprises .

Life Science

NanoTech

LaserTech

New Materials

Cooperation with industry : Magneto SensorsGeneral Application

Elec. resistance sensors Sensors for micro-position detection and control

sensitec.com

3D Magnetometer

Read head in hard disc drivers Angle sensors for automotive application (motors control / ABS units)

NXP.com www.buonenotizie.ittheconversation.com

� Different measurement possibilities like angle, lengt h, position, speed, magneitc field, current, …

The Technology .Thin film deposition in oblique incidence (OID)

Validation for industrial production

� Helmholtz Validation Project funded by the Helmholtz Association (HVF-0059)

� Budget 1,8 Mio. EUR, 02/2017 – 07/2019

� OID tuning of GMR and TMR sensors

� Validation of 200 mm wafer deposition

� Micro structuring and stress tests

� Integration into ASIC

� Goal: Within 2 years - building of an industrial-size UHV deposition test chamber and fabrication of OID-based superior (speed) sensors for automotive applications on 200 mm wafers.

HVF-project

Lab Size Industry Size

contacts

sensors

The NanoLab .Access and Usage

Implementation of

� nano characterization techniques

(atomic scale structure and chemistry)

� nano structuring techniques

� nano synthesis techniques

� Development of well defined sample transfer protocols between

NanoLab and beamlines (nano-PS)

Open for industrial users

Techniques .

� UHV sample preparation chamber with LEED / AES

� XPS, FT-IR

Spectroscopy & Growth (H. Noei)

� Reflectometer

� Six circle diffractometer

X-ray diffraction (V. Vonk)

Microscopy & Structuring (T. Keller)

� AFM, STM, optical

� SEM + FIB + Lithography (CHyN)

Magnetic Characterization (R. Röhlsberger)

� Physical properties measurement system

� Kerr Microscope

Use Cases from the NanoLabOperando Studies at the Atomic Scale

� UHV, Gas pressures > 1bar, RT- 800°C

� Catalytic flow conditions, operando studies

„You follow the oxidationprocess at the surface“

Use Cases from the NanoLabOxidation of Alloys (Scenarios)

Questions of interest:

� detailed atomic structure and chemical composition of oxide layer

� transport processes (segregation), rate limiting steps

� interfacial structure / epitaxy

� kinetic behavior (T, p(O2))

Use Cases from the NanoLabOxidation of Alloys (Scenarios)

LEED pattern at 78 eV (300 K)

Use Cases from the NanoLabEdges and corners increase efficiency of catalytic converters

Reference:Identification of a catalytically highly active surface phase for CO oxidation over PtRh nanoparticles under operando reaction conditions; U. Hejral, D. Franz, S. Volkov, S. Francoual, J. Strempfer, and A. Stierle; Physical Review Letters, 2018; DOI: 10.1103/PhysRevLett.120.126101

� Platinum-rhodium nanoparticles

� Insitu/in operando measurements(working conditions automotive)

� Different gasous conditions

� PETRA III on P09 (Resonant Scattering and Diffraction beamline)

� Higher effectivity at edges

� Catalytic converters increaseefficiency

See you in Hamburg .Thank you for your attention.

Accelerators | Photon Science | Particle Physics

Deutsches Elektronen-SynchrotronA Research Center of the Helmholtz-Association

Dr. Sabine JaehmlichIndustry Relations Manager

material characterization at desy - amap gmbh€¦ · desy spin-offs as suppliers 4 start-ups – 4...

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