resource… · 1 icp test report certification packet company name : littelfuse, inc. product...
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![Page 1: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/1.jpg)
1
ICP Test Report Certification Packet
Company name : Littelfuse, Inc.
Product Series: FUSE - BF1 58V
Product #: 142.5631.xxx Series
Issue Date: August 22, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the FUSE - BF1 58V RoHS-Compliant series products
manufactured by Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:.
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2
Table 1: List of Raw Materials covered by this report
Total Parts Raw Material Part Number Raw Material Description Page(s)
1 353.2131.4300 Housing - orange 3-11
2 353.2131.4400 Housing – Light green 12-20
3 353.2131.4500 Housing - red 21-29
4 353.2131.4600 Housing - yellow 30-38
5 353.2130.4700 Housing - brown 39-47
6 353.2131.4800 Housing – white 48-56
7 353.2131.5100 Housing – blue 57-65
8 353.2131.5125 Housing – pink 66-74
9 353.2131.5150 Housing – gray 75-83
10 353.1119.4043 Band CuZn (base) 84-86
11 353.1119.4043 Band CuZn (plating) 84-86
12 353.1126.4043 Band Cu Fe2P (base) 87-89
13 353.1126.4043 Band Cu Fe2P (plating) 87-89
14 355.1115.2053 Band Cu-ETP 90-94
15 355.1115.3053 Band Cu-ETP 95-99
16 325.2131.0001 Housing – natural 100-108
17 353.2131.5200/ 325.7692.0810 Housing – violet 109-117
18 353.2140.1000 BF1 Clear Cover 118-126
19 353.1590.0001 Solder 127-131
Form 585-047 Rev. A 2/21/06
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Test Report Number : TWNC00241666
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : HOUSING ORANGE Part Number : 353.2131.4300 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 4: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/4.jpg)
Number : TWNC00241666
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Orange Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 17 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 59154 Iodine (I) ND
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Number : TWNC00241666
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Orange Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 6: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/6.jpg)
Number : TWNC00241666
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
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Number : TWNC00241666
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 8: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/8.jpg)
Number : TWNC00241666
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
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Number : TWNC00241666
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 10: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/10.jpg)
Number : TWNC00241666
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 11: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/11.jpg)
Number : TWNC00241666
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 12: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/12.jpg)
Test Report Number : TWNC00241667
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : HOUSING LIGHT GREEN Part Number : 353.2131.4400 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 13: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/13.jpg)
Number : TWNC00241667
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Green Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 12 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 55286 Iodine (I) ND
![Page 14: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/14.jpg)
Number : TWNC00241667
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Green Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 15: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/15.jpg)
Number : TWNC00241667
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 16: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/16.jpg)
Number : TWNC00241667
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 17: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/17.jpg)
Number : TWNC00241667
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 18: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/18.jpg)
Number : TWNC00241667
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 19: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/19.jpg)
Number : TWNC00241667
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 20: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/20.jpg)
Number : TWNC00241667
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 21: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/21.jpg)
Test Report Number : TWNC00241664
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : HOUSING RED Part Number : 353.2131.4500 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 22: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/22.jpg)
Number : TWNC00241664
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Red Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 7 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 55745 Iodine (I) ND
![Page 23: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/23.jpg)
Number : TWNC00241664
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Red Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 24: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/24.jpg)
Number : TWNC00241664
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 25: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/25.jpg)
Number : TWNC00241664
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 26: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/26.jpg)
Number : TWNC00241664
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 27: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/27.jpg)
Number : TWNC00241664
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 28: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/28.jpg)
Number : TWNC00241664
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 29: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/29.jpg)
Number : TWNC00241664
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 30: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/30.jpg)
Test Report Number : TWNC00258321
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : May 29, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : YELLOW BOTTOM HOUSING Part Number : 353.2131.4600 Date Sample Received : May 17, 2012 Date Test Started : May 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 31: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/31.jpg)
Number : TWNC00258321
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Yellow Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 15 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) 403 Chlorine (Cl) 139 Bromine (Br) 22339 Iodine (I) ND
Z
![Page 32: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/32.jpg)
Number : TWNC00258321
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Yellow Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : May 17, 2012 Test Period : May 19, 2012 To May 28, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
Z
![Page 33: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/33.jpg)
Number : TWNC00258321
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.
50 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 34: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/34.jpg)
Number : TWNC00258321
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 35: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/35.jpg)
Number : TWNC00258321
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 36: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/36.jpg)
Number : TWNC00258321
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 37: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/37.jpg)
Number : TWNC00258321
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 38: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/38.jpg)
Number : TWNC00258321
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 39: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/39.jpg)
Test Report Number : TWNC00241665
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : HOUSING BROWN Part Number : 353.2131.4700 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 40: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/40.jpg)
Number : TWNC00241665
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Brown Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 17 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 54767 Iodine (I) ND
![Page 41: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/41.jpg)
Number : TWNC00241665
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Brown Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 42: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/42.jpg)
Number : TWNC00241665
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 43: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/43.jpg)
Number : TWNC00241665
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 44: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/44.jpg)
Number : TWNC00241665
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 45: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/45.jpg)
Number : TWNC00241665
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 46: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/46.jpg)
Number : TWNC00241665
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 47: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/47.jpg)
Number : TWNC00241665
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 48: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/48.jpg)
Test Report Number : TWNC00258324
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : May 29, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : WHITE BOTTOM HOUSING Part Number : 353.2131.4800 Date Sample Received : May 17, 2012 Date Test Started : May 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 49: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/49.jpg)
Number : TWNC00258324
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item White Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 15 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) 248 Chlorine (Cl) 149 Bromine (Br) 25496 Iodine (I) ND
Z
![Page 50: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/50.jpg)
Number : TWNC00258324
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item White Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : May 17, 2012 Test Period : May 19, 2012 To May 28, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
Z
![Page 51: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/51.jpg)
Number : TWNC00258324
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.
50 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 52: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/52.jpg)
Number : TWNC00258324
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 53: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/53.jpg)
Number : TWNC00258324
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 54: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/54.jpg)
Number : TWNC00258324
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 55: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/55.jpg)
Number : TWNC00258324
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 56: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/56.jpg)
Number : TWNC00258324
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 57: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/57.jpg)
Test Report Number : TWNC00234713S1
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Dec 15, 2011 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
This is to supersede report NO. TWNC00234713 dated Dec 02, 2011
Sample Description:
One (1) group of submitted samples said to be : Part Description : BOTTOM HOUSING BLUE Part Number : 353.2131.5100 Date Sample Received : Nov 28, 2011 Date Test Started : Nov 29, 2011
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 58: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/58.jpg)
Number : TWNC00234713S1
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Blue Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 22 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
![Page 59: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/59.jpg)
Number : TWNC00234713S1
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Blue Plastic
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 50000 Iodine (I) ND
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Nov 28, 2011 Test Period : Nov 29, 2011 To Dec 02, 2011
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 60: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/60.jpg)
Number : TWNC00234713S1
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography
50 ppm
Phthalates
With reference to EN14372:2004, by solvent extraction and determined by GC-MSD
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 61: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/61.jpg)
Number : TWNC00234713S1
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 62: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/62.jpg)
Number : TWNC00234713S1
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the flask at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 63: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/63.jpg)
Number : TWNC00234713S1
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 64: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/64.jpg)
Number : TWNC00234713S1
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 65: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/65.jpg)
Number : TWNC00234713S1
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 66: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/66.jpg)
Test Report Number : TWNC00241669
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : HOUSING PINK Part Number : 353.2131.5125 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 67: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/67.jpg)
Number : TWNC00241669
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Pink Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 16 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 54183 Iodine (I) ND
![Page 68: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/68.jpg)
Number : TWNC00241669
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Pink Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 69: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/69.jpg)
Number : TWNC00241669
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 70: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/70.jpg)
Number : TWNC00241669
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 71: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/71.jpg)
Number : TWNC00241669
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 72: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/72.jpg)
Number : TWNC00241669
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 73: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/73.jpg)
Number : TWNC00241669
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 74: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/74.jpg)
Number : TWNC00241669
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 75: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/75.jpg)
Test Report Number : TWNC00241668
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : HOUSING GRAY Part Number : 353.2131.5150 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 76: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/76.jpg)
Number : TWNC00241668
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Grey Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 19 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 59698 Iodine (I) ND
![Page 77: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/77.jpg)
Number : TWNC00241668
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Grey Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 78: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/78.jpg)
Number : TWNC00241668
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 79: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/79.jpg)
Number : TWNC00241668
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 80: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/80.jpg)
Number : TWNC00241668
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 81: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/81.jpg)
Number : TWNC00241668
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 82: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/82.jpg)
Number : TWNC00241668
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 83: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/83.jpg)
Number : TWNC00241668
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 84: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/84.jpg)
Report No.: MX11-0928-03 Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com
TEST REPORT
APPLICANT Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila Ing. María Valdez SAMPLE DESCRIPTION
One (1) group of submitted samples said to be : Sample Description NP Item No. 3) Element Sn Plated Copper N/P 353.1119.4043 Country of Origin NP Buyer's Name NP Supplier's Name NP Date sample received 2011-05-05 Testing period 2011-05-09 to 2011-05-13 ******************************************************************************************** TEST CONDUCTED
As requested by the applicant, for details please refer to attached pages. ********************************************************************************************
CONCLUSION
Sample Number Testing item Conclusion Failed component Failed result
3 (Base)
Element Sn Plated Copper N/P 353.1119.4043
Pass See Result summary
--- ---
3 (Plated)
Element Sn Plated Copper N/P 353.1119.4043
Pass See Result summary
--- ---
********************************************************************************************
TEST CONDUCTED
Samples:
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Report No.: MX11-0928-03 Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com
3) Base Element Sn Plated Copper N/P 353.1119.4043 3) Plated Element Sn Plated Copper N/P 353.1119.4043 TEST RESULT SUMMARY FOR RoHS DIRECTIVE :
TESTING ITEM Ω RESULT (ppm)
Limit (3) Base
(3) Plated
Cadmium (Cd) content ND ND 0,01% (100 ppm)
Lead (Pb) content 36,10 148,1 0,1% (1000 ppm)
Mercury (Hg) content ND ND 0,1% (1000 ppm)
Chromium (VI) (Cr6+) ND ND 0,1% (1000 ppm)
ppm = parts per million based on dry weight of sample. µg/cm2 = microgram per square centimeter. mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter. < = less than. ND = Not detected. The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.
Prepared and checked by: For Intertek Laboratory Manager
The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).
NOTE : DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.
# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-03 WERE TESTED SEPARATED. Test method:
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Report No.: MX11-0928-03 Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com
Sample Number Testing item Ω Testing method
Quality control Batch:
Analysis Date:
Analyzed By:
Reporting limit ppm
3 Chromium VI (Cr6+) content
With reference to USEPA 3060, by EPA 7196
QHU2010-61p73 2011-05-13 MELA 20,0
Sample Number Testing item Ω Testing method
Quality control Batch:
Analysis Date:
Analyzed By:
Reporting limit ppm
3 (Base) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 5,0 3 (Plated) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 50,0
Sample Number Testing item Ω Testing method
Quality control Batch:
Analysis Date:
Analyzed By:
Reporting limit ppm
3 (Base) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 2,0 3 (Plated) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 20,0
Sample Number Testing item Ω Testing method
Quality control Batch:
Analysis Date:
Analyzed By:
Reporting limit ppm
3 (Base) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 0,25 3 (Plated) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 2,5
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Report No.: MX11-0928-05 Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com
TEST REPORT
APPLICANT Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila Ing. María Valdez SAMPLE DESCRIPTION
One (1) group of submitted samples said to be : Sample Description NP Item No. 5) N/P 353.1126.4043 Country of Origin NP Buyer's Name NP Supplier's Name NP Date sample received 2011-05-05 Testing period 2011-05-09 to 2011-05-13 ******************************************************************************************** TEST CONDUCTED
As requested by the applicant, for details please refer to attached pages. ********************************************************************************************
CONCLUSION
Sample Number Testing item Conclusion Failed component Failed result
5 (Base)
N/P 353.1126.4043 Pass
See Result summary --- ---
5 (Plated)
N/P 353.1126.4043 Pass
See Result summary --- ---
********************************************************************************************
TEST CONDUCTED
Samples:
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Report No.: MX11-0928-05 Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com
5) Base N/P 353.1126.4043 5) Plated N/P 353.1126.4043 TEST RESULT SUMMARY FOR RoHS DIRECTIVE :
TESTING ITEM Ω RESULT (ppm)
Limit (5) Base
(5) Plated
Cadmium (Cd) content ND ND 0,01% (100 ppm)
Lead (Pb) content 61,51 ND 0,1% (1000 ppm)
Mercury (Hg) content ND ND 0,1% (1000 ppm)
Chromium (VI) (Cr6+) ND ND 0,1% (1000 ppm)
ppm = parts per million based on dry weight of sample. µg/cm2 = microgram per square centimeter. mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter. < = less than. ND = Not detected. The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.
Prepared and checked by: For Intertek Laboratory Manager
The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).
NOTE : DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.
# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-05 WERE TESTED SEPARATED. Test method:
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Report No.: MX11-0928-05 Date:2011-06-16
It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing
Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).
1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8
Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo
C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com
Sample Number Testing item Ω Testing method
Quality control Batch:
Analysis Date:
Analyzed By:
Reporting limit ppm
5 Chromium VI (Cr6+) content
With reference to USEPA 3060, by EPA 7196
QHU2010-61p73 2011-05-13 MELA 20,0
Sample Number Testing item Ω Testing method
Quality control Batch:
Analysis Date:
Analyzed By:
Reporting limit ppm
5 (Base) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 5,0 5 (Plated) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 41,67
Sample Number Testing item Ω Testing method
Quality control Batch:
Analysis Date:
Analyzed By:
Reporting limit ppm
5 (Base) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 2,0 5 (Plated) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 16,7
Sample Number Testing item Ω Testing method
Quality control Batch:
Analysis Date:
Analyzed By:
Reporting limit ppm
5 (Base) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 0,25 5 (Plated) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 2,5
![Page 90: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/90.jpg)
Test Report Number : TWNC00258877
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : May 28, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : TIN PLATED COPPER STRIP Part Number : 355.1115.2053 Date Sample Received : May 22, 2012 Date Test Started : May 23, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 91: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/91.jpg)
Number : TWNC00258877
Test Conducted
Page 2 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item (1) (2)
Heavy Metal
Cadmium (Cd) content ND ND Lead (Pb) content ND 344 Mercury (Hg) content ND ND
Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (<0.02)
Negative (<0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation
was not found at the time of Test.
Tested Components (1) Silvery Plating Layer (2) Coppery Metal Base Material
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : May 22, 2012 Test Period : May 23, 2012 To May 28, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 92: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/92.jpg)
Number : TWNC00258877
Test Conducted
Page 3 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.
0.02 mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 93: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/93.jpg)
Number : TWNC00258877
Test Conducted
Page 4 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
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Number : TWNC00258877
Test Conducted
Page 5 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 95: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/95.jpg)
Test Report Number : TWNC00258878
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : May 28, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : Sn PLATED COPPER STRIP Part Number : 355.1115.3053 Date Sample Received : May 22, 2012 Date Test Started : May 23, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 96: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/96.jpg)
Number : TWNC00258878
Test Conducted
Page 2 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item (1) (2)
Heavy Metal
Cadmium (Cd) content ND ND Lead (Pb) content ND 211 Mercury (Hg) content ND ND
Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (<0.02)
Negative (<0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation
was not found at the time of Test.
Tested Components (1) Silvery Plating Layer (2) Coppery Metal Base Material
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : May 22, 2012 Test Period : May 23, 2012 To May 28, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 97: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/97.jpg)
Number : TWNC00258878
Test Conducted
Page 3 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.
0.02 mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 98: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/98.jpg)
Number : TWNC00258878
Test Conducted
Page 4 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
![Page 99: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/99.jpg)
Number : TWNC00258878
Test Conducted
Page 5 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 100: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/100.jpg)
Test Report Number : TWNC00241458
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : COLORANT NATURAL Part Number : 325.2131.0001 Date Sample Received : Jan 19, 2012 Date Test Started : Jan 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 101: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/101.jpg)
Number : TWNC00241458
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item White Plastic Pellet
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 20 Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) 290 Chlorine (Cl) 86 Bromine (Br) 33550 Iodine (I) ND
![Page 102: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/102.jpg)
Number : TWNC00241458
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item White Plastic Pellet
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Jan 19, 2012 Test Period : Jan 19, 2012 To Feb 01, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 103: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/103.jpg)
Number : TWNC00241458
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 104: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/104.jpg)
Number : TWNC00241458
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 105: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/105.jpg)
Number : TWNC00241458
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 106: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/106.jpg)
Number : TWNC00241458
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 107: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/107.jpg)
Number : TWNC00241458
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 108: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/108.jpg)
Number : TWNC00241458
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 109: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/109.jpg)
Test Report Number : TWNC00242056
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : Feb 03, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : COLORANT VIOLET Part Number : 325.7692.0810 Date Sample Received : Feb 01, 2012 Date Test Started : Feb 01, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 110: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/110.jpg)
Number : TWNC00242056
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Purple Plastic Pellet
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND
![Page 111: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/111.jpg)
Number : TWNC00242056
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Purple Plastic Pellet
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : Feb 01, 2012 Test Period : Feb 01, 2012 To Feb 03, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
![Page 112: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/112.jpg)
Number : TWNC00242056
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID
10 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
![Page 113: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/113.jpg)
Number : TWNC00242056
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
![Page 114: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/114.jpg)
Number : TWNC00242056
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
![Page 115: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/115.jpg)
Number : TWNC00242056
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 116: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/116.jpg)
Number : TWNC00242056
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 117: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/117.jpg)
Number : TWNC00242056
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 118: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/118.jpg)
Test Report Number : TWNC00258320
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : May 29, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : BF1 CLEAR COVER Part Number : 353.2140.1000 Date Sample Received : May 17, 2012 Date Test Started : May 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 119: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/119.jpg)
Number : TWNC00258320
Test Conducted
Page 2 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Clear Orange Plastic
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
Halogen Content Fluorine (F) ND Chlorine (Cl) 1768 Bromine (Br) ND Iodine (I) ND
Z
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Number : TWNC00258320
Test Conducted
Page 3 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Clear Orange Plastic
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : May 17, 2012 Test Period : May 19, 2012 To May 28, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
Z
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Number : TWNC00258320
Test Conducted
Page 4 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.
50 ppm
Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.
50 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.
10 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
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Number : TWNC00258320
Test Conducted
Page 5 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008
Remarks: *1: List of Appropriate Acid:
Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
Sample preparation
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Weigh sample and add organic solvent
By Soxhlet extraction or Solvent extraction
Concentrate the extract and make upwith organic solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
By spot test
Get 50cm2 sample
By boiling water extraction
Metal Polymers / electronics
Negative *2
Confirm the tested samples are totally dissolved
Take sample and immerse into Aqua Regia, start to strip plating layer
Stop the stripping procedure upon color change completely
Take the Aqua solution as plating component and stripped body as substrate component
For non-metal part For metal part
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Number : TWNC00258320
Test Conducted
Page 6 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test for Halogen Content Reference Standard:EN 14582
Add absorbent in a combustion flask & place weighed sample in equipment
Fill oxygen into calorimetric bomb
Ignite then leave the bomb at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by ion chromatography
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Number : TWNC00258320
Test Conducted
Page 7 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
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Number : TWNC00258320
Test Conducted
Page 8 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
![Page 126: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/126.jpg)
Number : TWNC00258320
Test Conducted
Page 9 of 9 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo
![Page 127: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/127.jpg)
Test Report Number : TWNC00258319
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Applicant: Littelfuse, S.A. de C.V. Date : May 29, 2012 Blvd. Fausto Z. Martinez #1800
Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico
Sample Description:
One (1) group of submitted samples said to be : Part Description : SOLDER DIN Part Number : 353.1590.0001 Date Sample Received : May 17, 2012 Date Test Started : May 19, 2012
Test Conducted :
As requested by the applicant, for details please refer to attached pages.
![Page 128: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It](https://reader033.vdocument.in/reader033/viewer/2022060607/605df4e1efdd9c0e8e39659b/html5/thumbnails/128.jpg)
Number : TWNC00258319
Test Conducted
Page 2 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅰ) Test Result Summary : Result (ppm)
Test Item Silvery Metal
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)
Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation
was not found at the time of Test.
Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen
Date Sample Received : May 17, 2012 Test Period : May 19, 2012 To May 28, 2012
(Ⅱ) RoHS Requirement:
Restricted Substances Limits
Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
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Number : TWNC00258319
Test Conducted
Page 3 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅲ) Test Method: Test Item Test Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.
0.02 mg/kg with 50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
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Number : TWNC00258319
Test Conducted
Page 4 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008
Remarks: *1: List Of Appropriate Acid:
Material Acid Added For Digestion
Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
End of Report
Sampling/grinding or cutting
For different material, digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline solution
Definite temp. extraction
Make up with deionized water and add diphenyl-carbazide solution
Cool and filter the extract
Cr6+
Analyzed by UV-VIS
By spot test
Get 50cm2 sample
Boiling water extraction
Metal Polymers / Electronics
Negative*2 Confirm the tested samples are totally dissolved
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Number : TWNC00258319
Test Conducted
Page 5 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.
全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓
Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401
Photo