memorandum c c3 rn z oreviewer (if not esb) esat reviewer's name michael completion date auqust...
TRANSCRIPT
UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION 6
HOUSTON BRANCH10625FALLSTONERD.
HOUSTON, TEXAS 77099
MEMORANDUM c^ C3 rnz __ O^ CO fH
Date: August 31, 2005 co --po s <> 3
Subject: Contract Laboratory Program Data Review o "^ O
From: 71 Marvelyn Humphrey, ESAT Regional PO, 6MD-HE
To: U. Lennox, SF-LP
Site : TAR CREEK
Case#: 34211
SDG# : MF1MDO
The EPA Region 6 Houston Branch ESAT data review team hascompleted a review of the submitted Contract Laboratory Program(CLP ) data package for the referenced site. The samples analyzedand reviewed are detailed in the attached Regional data reviewreport.
The data package is acceptable for regional use. Problems, ifany, are listed in the report narrative.
If you have any questions regarding the data review report,please call me at (281) 983-2140.
Attachmentscc: M. El-Feky, Region 6 Data Coordinator
Files (2)
952827
005833
LOCKHEED MARTIN SERVICES GROUPESAT REGION 6
10625 FALLSTONE ROADHOUSTON, TEXAS 77099
MEMORANDUMI
DATE: August 30, 2005
TO: Marvelyn Humphrey, ESAT PO, Region 6 :
FROM: Tom Chiang, ESAT Program Manager, Region 6 / u—J $ n (• I / j
SUBJECT: CLP Data Review '.
REF: TDF #6-05-212A ESAT File No. 10618ESAT Contract No. 68-W-01-030
Attached is the data review summary for Case #34211SDG #MF1MDO
Site Tar Creek
COMMENTS:
I. LEVEL OF DATA REVIEW:
Modified CADRE (Computer Aided Data Review and Evaluation)review was performed for this package.
II. CONTRACTUAL ASSESSMENT OF DATA PACKAGE:
-. The laboratory was contractually compliant.
III. TECHNICAL/USABILITY ASSESSMENT OF DATA PACKAGE:
Some results have been qualified because of the significanttechnical problems addressed below.
A. Laboratory blank concentrations caused the ! j;qualification of three arsenic and two mercury results.
B. Matrix spike recoveries were outside of the QC limitsfor antimony, cadmium, lead, mercury, and zinc. ' }:! i1 Li" >
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION 6
HOUSTON BRANCH10625 FALLSTONE ROADHOUSTON, TEXAS 77099
INORGANIC REGIONAL DATA ASSESSMENT
CASE NO. 34211LABORATORY SENTINCONTRACT* 68 -W- 04 -007SDG# MF1MDOSOW# ILM05.3/Mod. 1233.0ACCT# 5302DD2GJN34SF# 302DD2CJW
SAMPLE NO. MF1MDOMF1MD1MF1MD2MF1MD3
SITE Tar CreekNO. OF SAMPLES 20MATRIX Plants
, i
1 •
REVIEWER (IF NOT ESB) ESATREVIEWER'S NAME MichaelCOMPLETION DATE Auqust 3
MF1MD5 MF1MEO MF1ME5MF1MD6 MF1ME1 MF1ME6MF1MD7 MF1ME2 MF1ME7MF1MD8 MF1ME3 MF1ME8
J. Fe'rtibta0, 2005
MF1MFOMF1MF1MF1MF2MF1MF3
DATA ASSESSMENT SUMMARY
ICP HG
1. HOLDING TIMES 0 02. CALIBRATIONS O 03 . BLANKS M M4. MATRIX SPIKES M M :
5. DUPLICATE ANALYSIS O Q6. ICP QC M7. LCS 0 08. SAMPLE VERIFICATION O O9. OTHER QC N/A N/A10. OVERALL ASSESSMENT M M
O = Data had no problems.M = Data qualified because of major or minor problems. 'Z = Data unacceptable.N/A= Not applicable
ACTION ITEMS:
AREAS OF CONCERN: Laboratory blank concentrations caused thequalification of eight aluminum, three arsenic, and two mercuryresults. Matrix spike recoveries were greater than 125 percentfor antimony and cadmium and less than 75 percent for lead1] jijmercury, and zinc. The potassium serial dilution difference wasgreater than 10 percent. 1
: j;NOTABLE PERFORMANCE: The laboratory submitted the data package 8calendar days early for the 21-day turnaround time requirement.
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COMMENTS/CLARIFICATIONSREGION 6 CLP QA REVIEW
Case 34211 SDG MF1MDO Site Tar Creek Lab SENTIN
COMMENTS: The SDG, contracted under SOW ILM05.3, consisted of 20plant samples for total metals analyses by ICP/AES and coldvapor. It was requested that the laboratory analyze the plantsamples following modified analysis request No. 1233.0. Thesampler designated sample MF1MD6 as the laboratory QC sample.The laboratory met the 21-day data package turnaround timerequirement, and the package was contractually compliant.
Per Region 6 request, the laboratory resubmitted the Forms 1, 5A,and 6 which needed correction of the reported results. Theresubmitted pages were used to replace the corresponding pages inthe package, and the resubmission cover sheets were placed at thebeginning of the package.
The target analytes of concern with the corresponding desireddetection levels in parentheses were cadmium (0.01 mg/Kg), lead(0.01 mg/Kg), and zinc (0.2 mg/Kg). The samples met the desireddetection limit criteria. All samples had results above thedesired detection limits for the analytes of concern. Thelaboratory diluted sample MF1MD2 5X because the zincconcentration was over the linear range.
Modified CADRE review was performed for this package as requestedby the TDF. Please note that the raw data were not reviewed.The laboratory contractual compliance and the technical usabilityof the sample results were primarily determined by CCS and CADRE,respectively. The reviewer performed supplemental forms checkingand applied Region 6 guidelines, where necessary, to account forknown limitations of the electronic review process. Therefore,the reviewer's final assessments may deviate from those found inthe CADRE report. The CADRE narrative was attached to thisreport as an addendum for additional information.
DATA ASSESSMENT: The QC problems affecting the sample resultsare addressed below.
• The following results above the CRQL's were qualified asestimated and biased low because of laboratory blankconcentrations: the aluminum results for samples MF1MDO,MF1MD1, MF1MD5, MF1MEO, MF1ME1, MF1ME5, MF1ME7, and MF1MF1;the arsenic results for samples MF1ME2, MF1MF2, and MF1MF3;and the mercury results for samples MF1MD2 and MF1MD3.
• Because of laboratory blank concentrations, 19 antimony, 7beryllium, 6 chromium, and 18 nickel results between theMDL's and CRQL's should be considered undetected, and thereported concentrations should be used as the quantitationlimits.
• The pre-digestion matrix spike recovery for mercury was lessthan 75 percent, and a post-digestion spike analysis was notrequired. Because of this deficiency, the mercury resultswere qualified as estimated and biased low.
• Nineteen antimony results and all cadmium, lead, and zincresults were qualified as estimated because the pre-digestion matrix spike recoveries were greater than 125
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INORGANIC QA REVIEWCONTINUATION PAGE
Case 34211 SDG MF1MDO Site Tar Creek Lab SENTIN
Percent for antimony and cadmium and less than 75 percentor lead and zinc. These results were not qualified'asbiased high or low because the post-digestion matrix spikerecoveries for antimony, cadmium, lead, and zinc were|withinthe QC limits.
• The potassium results were qualified as estimated becausethe potassium serial dilution percent difference was 'greaterthan 10 percent. These results were also qualified as,biased low because the serial dilution result indicate'd thatmatrix interferences suppressed the signal for potassium.
The technical usability of all reported results is indicated inthe Data Summary Table (DST). An Evidence Audit was conductedfor the Complete Sample Delivery Group File (CSF), and theresults were recorded in the Evidence Inventory Checklist.
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HEADER DEFINITIONS FOR INORGANIC EXCEL DST
CASE: Case NumberSDG: SDG NumberEPASAMP: EPA Sample NumberLABID: Laboratory Sample IDMATRIX: Sample MatrixQCCODE: Sample QC CodeSMPQUAL: Sample QualifierANDATE: Sample Analysis DateANTIME: Sample Analysis TimeCASNUM: Analyte CAS NumberANALYTE: Analyte NameCONG: Analyte ConcentrationUNITS: Concentration UnitsADJCRQL: Adjusted Contract Required Quantitation Limit ValueLABQUAL: Laboratory QualifierSMPDATE: Sampling DateVALDQAL: Region 6 Inorganic Data Validation Qualifier (see
Inorganic Data Qualifier Definitions on the next page)PRPDATE: Sample Preparation DateLRDATE: Laboratory Receipt DateLEVEL: Sample LevelPERSOLD: Sample Percent SolidsSMPWTVL: Sample Weight (Soil Samples)/Initial Sample Volume
(Water Samples)FINLVOL: Final Sample VolumeMETHOD: Method of AnalysisSTATLOC: Station Location
Disclaimer: ESAT verified the accuracy of the informationreported in the Excel DST only for the followingdata fields: CASE, SDG, EPASAMP, MATRIX, ANALYTE,CONG, UNITS, ADJCRQL, VALDQAL, and PERSOLD. Thedata qualifiers in the VALDQAL column indicate thetechnical usability of the reported results.
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INORGANIC DATA QUALIFIER DEFINITIONS
The following definitions provide brief explanations of the ESAT-Region 6 qualifiers assigned to results in the inorganic datareview process.
U Not detected at the laboratory reported quantitation limit.
L Reported concentration is between the MDL and the CRQL.
J Result is estimated because of outlying quality controlparameters such as matrix spike, serial dilution, etc., orthe result is below the CRQL.
R Result is unusable.
F A possibility of a false negative exists.
UC Reported concentration should be used as a raisedquantitation limit because of blank effects and/orlaboratory or field contamination.
A High bias. Actual concentration may be lower than theconcentration reported.
v Low bias. Actual concentration may be higher than theconcentration reported.
W The result should be used with caution. The result wasreported on a dry weight basis although the sample did notconform to the EPA Office of Water definition of a soilsample because of its high water content (>70% moisture).
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CASE SDG EPASAMP34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MDO34211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD134211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MO2
LABID MATRIX QCCODE13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13561 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13562 S13563 S13563 S13563 S13563 S13563 S13563 S13563 S13563 S13SS3 S13563 S13563 S13563 S13563 S13563 S13563 S13563 S13563 S13563 S13563 S
ANDATE ANTIME07/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107(04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/07/2005 23:3307/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5107/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/07/2005 23:3507/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607/04/2005 17:5607(04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/07/2005 23:3707/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907104(2005 «:19
CASNUM ANALYTE CONC7429905 ALUMINUM 34.27440360 ANTIMONY 0.757440382 ARSENIC 0.317440393 BARIUM 1.37440417 BERYLLIUM 0.507440439 CADMIUM 68.97440702 CALCIUM 63407440473 CHROMIUM 0.437440484 COBALT 0.487440508 COPPER 10.27439896 IRON 1047439921 LEAD 20.97439954 MAGNESIUM 7297439965 MANGANESE 50.97439976 MERCURY 0.107440020 NICKEL 2.47440097 POTASSIUM 91807782492 SELENIUM 0.967440224 SILVER 0.187440235 SODIUM 17407440280 THALLIUM 2.57440622 VANADIUM 0.127440666 ZINC 7847429905 ALUMINUM 33.17440360 ANTIMONY 6.07440382 ARSENIC 0.317440393 BARIUM 1.57440417 BERYLLIUM 0.507440439 CADMIUM 73.67440702 CALCIUM 76507440473 CHROMIUM 0.197440484 COBALT 0.427440508 COPPER 827439896 IRON 69.47439921 LEAD 6.67439954 MAGNESIUM 6627439965 MANGANESE 58.27439976 MERCURY 0.107440020 NICKEL 1.97440097 POTASSIUM 97807782492 SELENIUM 1.07440224 SILVER 1.07440235 SODIUM 20607440280 THALLIUM 2.57440622 VANADIUM 5.07440566 ZINC 9217429905 ALUMINUM 9957440360 ANTIMONY 0.847440382 ARSENIC 4.47440393 BARIUM 10.07440417 BERYLLIUM 0.257440439 CADMIUM 1297440702 CALCIUM 144007440473 CHROMIUM 5.B7440484 COBALT 3.47440508 COPPER 1267439896 IRON 50607439921 LEAD 27507439954 MAGNESIUM 23607439965 MANGANESE 1177439976 MERCURY 0.167440020 NICKEL 35.77440097 POTASSIUM 12207782492 SELENIUM 0.357440224 SILVER 1.0
VALDQALJv
ULJLJLJ
UJ
ULJLJ
J
UJvULJ
JvULJ
ULJJJv
UULJ
UJ
ULJLJ
J
UJvULJ
JvLJ
U
UU
J
ULJ
LJULJ
J
LJ
J
Jv
JvLJ
U
UNITS ADJCRQLMG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0
SMPDATE PRPDATE LRDAT6 LEVEL06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/06/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/26/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW0604/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/06/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/06/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW0604/2005 07/01/2005 06/28/2005 LOW
PERSOLD100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0
SMPWTVL1.001.001.001.001.001.001.001.001.001.001.001.001.001.000.201.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.000.201.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.000.201.001.001.001.00
FINLVOL100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100
METHODppppppppppppppcvppppppppppppppppppppppcv
-ppppppppppppppppppppppcvpppp
STATLOCTC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-B1O-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29ATC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29BTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29C
ige7oM7
005840
34211 MF1MDO MF1MD234211 MR1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD234211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1M0334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD334211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MDS34211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD534211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDQ MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD634211 MF1MDO MF1MD6
13563 S13563 S13563 S13563 S13564 S13S64 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13564 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13565 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S13566 S
07/04/2005 18:1907/04/2005 18:1907/04/2005 18:1907/05/2005 21:1307/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/07/2005 23:3907/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:2407/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/07/2005 23:4607/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 18:3007/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/07/2005 23:2607/04/2005 17:2807/04/2005 17:28
7440235744028074406227440666742990574403607440382744039374404177440439744070274404737440484744050874398967439921743995474399657439976744002074400977782492744022474402357440280744062274406667429905744036074403827440393744041774404397440702744047374404847440508743989674399217439954743996574399767440020744009777824927440224744023574402807440622744066674299057440360744038274403937440417744043974407027440473744048474405087439896743992174399547439965743997674400207440097
SODIUMTHALLIUMVANADIUMZINCALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMVANADIUMZINCALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMVANADIUMZINCALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKELPOTASSIUM
643002.55.1287002240.98
1.65.10.059235163002.51.810529502510130038.1
0.12
14.243401.41.0167002.51.3672032.20.56
0.392.40.50
18.0
107000.305.06.675.610.9
169075.8
0.100.45
199000.961.07622.50.12
32648.50.83
0.433.30.5013.9
125000.340.0976.989.9
9.91950
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22200
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MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 30.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG7KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MS/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500
06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/06/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/06/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06728/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06O8/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/06/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW
100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0
1.001.00
1.001.001.00
1.001.00
1.00
1.00
1.001.001.00
1.001.00
1.001.001.001.00
0.20
1.00
1.00
1.001.001.00
1.00
1.001.00
1.001.00
1.001.001.001.00
1.00
1.001.00
1.00
1.001.001.00
1.000.201.00
1.001.00
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100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100
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TC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29CTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-29DTC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30ATC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30BTC4-BIO-30B
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005841
34211 MF1MDO MF1MD6 13566 S34211 MF1MDO MF1MD6 13566 S34211 MF1MDO MF1MD6 13566 S34211 MF1MDO MF1MD6 13566 S34211 MF1MDO MF1MD6 13566 S34211 MF1MDO MF1MD6 13566 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD7 13567 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MD8 13568 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MOO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S34211 MF1MDO MF1MEO 13569 S
07/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 17:2807/04/2005 175807/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 16:3507/04/2005 18:3507/07/2005 23:4807/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:3507/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/07/2005 23:5007/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4107/04/2005 18:4707/04/2005 18:4707/04/2005 16:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/04/2005 18:4707/07/2005 23:52
7782492 SELENIUM 1.07440224 SILVER 0.247440235 SODIUM 8257440280 THALLIUM 2.57440622 VANADIUM 0.157440666 ZINC 3557429905 ALUMINUM 70.17440360 ANTIMONY 0.817440382 ARSENIC 0.577440393 BARIUM 1.37440417 BERYLLIUM 0.0207440439 CADMIUM 41.47440702 CALCIUM 49907440473 CHROMIUM 1.17440484 COBALT 0.377440508 COPPER 17.47439896 IRON 496
7439921 LEAD 2117439954 MAGNESIUM 6677439965 MANGANESE 33.27439976 MERCURY 0.107440020 NICKEL 1.57440097 POTASSIUM 112007782492 SELENIUM 1.07440224 SILVER 0.197440235 SODIUM 33207440280 THALLIUM 2.57440622 VANADIUM 0.477440666 ZINC 14807429905 ALUMINUM 52.17440360 ANTIMONY 0.597440382 ARSENIC 0.487440393 BARIUM 0.837440417 BERYLLIUM 0.507440439 CADMIUM 57.37440702 CALCIUM 41507440473 CHROMIUM 0.927440484 COBALT 0.397440508 COPPER 20.57439896 IRON 3297439921 LEAD 2057439954 MAGNESIUM 3327439965 MANGANESE 14.97439976 MERCURY 0.107440020 NICKEL 1.97440097 POTASSIUM 108007782492 SELENIUM 1.17440224 SILVER 1.07440235 SODIUM 37207440280 THALLIUM 2.57440622 VANADIUM 0.277440666 ZINC 16407429905 ALUMINUM 37.17440360 ANTIMONY 0.427440382 ARSENIC 0.267440393 BARIUM 2.77440417 BERYLLIUM 0.507440439 CADMIUM 11.67440702 CALCIUM 117007440473 CHROMIUM 0.417440484 COBALT 5.07440508 COPPER 5.77439896 IRON 67.17439921 LEAD 11.87439954 MAGNESIUM 15307439965 MANGANESE 72.77439976 MERCURY 0.10
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MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10
06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/06/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 05/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/06/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/06/2005 05/28/2005 LOW
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1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.000.201.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.000.201.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.000.20
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005843
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07/04/2005 19:3707/07/2005 23:5807/04(2005 19:3707/04/2005 19:3707/04/2005 19:3707/04/2005 19:3707/04/2005 19:3707/04/2005 19:3707/04/2005 19:3707/04/2005 19:3707/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/08/2005 0:0107/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4307/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/08/2005 0:0307/04/2005 19:4807(04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807/04/2005 19:4807(04/2005 19:5407/04/2005 19:5407/04/2005 19:5407/04/2005 19:5407/04/2005 19:5407/04/2005 19:5407/04/2005 19:5407/04/2005 19:5407/04/2005 19:5407(04/2005 19:5407/04/2005 19:54
7439965 MANGANESE 61.17439976 MERCURY 0.107440020 NICKEL 1.77440097 POTASSIUM 108007762492 SELENIUM 0.867440224 SILVER 1.07440235 SODIUM 34407440280 THALLIUM 2.57440622 VANADIUM 0.477440666 ZINC 15607429905 ALUMINUM 20.77440360 ANTIMONY 0.647440382 ARSENIC 0.217440393 BARIUM 1.97440417 BERYLLIUM 0.507440439 CADMIUM 0.217440702 CALCIUM 113007440473 CHROMIUM 0.467440484 COBALT 0.0967440508 COPPER 2.77439896 IRON 26.67439921 LEAD 2.07439954 MAGNESIUM 4117439965 MANGANESE 1557439976 MERCURY 0.107440020 NICKEL 0.537440097 POTASSIUM 98007782492 SELENIUM 1.17440224 SILVER 1 .07440235 SODIUM 12507440280 THALLIUM 2.57440622 VANADIUM 5.07440666 ZINC 1397429905 ALUMINUM 18.67440360 ANTIMONY 0.567440382 ARSENIC 1.07440393 BARIUM 1.57440417 BERYLLIUM 0.507440439 CADMIUM 0.147440702 CALCIUM 74507440473 CHROMIUM 0.417440484 COBALT 5.07440508 COPPER 2.77439896 IRON 33.97439921 LEAD 1.97439954 MAGNESIUM 4957439965 MANGANESE 1517439976 MERCURY 0.107440020 NICKEL 0.467440097 POTASSIUM 96807782492 SELENIUM 1.17440224 SILVER 1.07440235 SODIUM 9477440280 THALLIUM 2.57440622 VANADIUM 5.07440666 ZINC 84.47429905 ALUMINUM 45.67440360 ANTIMONY 0.397440382 ARSENIC 0.267440393 BARIUM 1.17440417 BERYLLIUM 0.507440439 CADMIUM 2.67440702 CALCIUM 52707440473 CHROMIUM 0.637440484 COBALT 0.447440508 COPPER 5.07439896 IRON 718
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MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0
06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/0672005 06/28/2005 LOW06724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 0672672005 LOW05724/2005 07/01/2005 06/28/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06/24/2005 07(01/2005 06/28/2005 LOW06724/2005 07/01/2005 06728/2005 LOW06/24/2005 07/01/2005 06/28/2005 LOW06724/2005 07/01/2005 06/2672005 LOW06725/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06725/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06125/2005 07/01/2005 06728/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06728/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06728/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06(25/2005 07/01/2005 06/28/2005 LOW06725/2005 07/06/2005 06/2672005 LOW06725/2005 07/01/2005 06728/2005 LOW06725/2005 07/01/2005 06/28/2005 LOW06725/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06725/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06728/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06725/2005 07/01/2005 06728/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01(2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01(2005 06/2672005 LOW06/25/2005 07/01(2005 06/28(2005 LOW06/25/2005 07/06/2005 06728/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01(2005 06/28/2005 LOW06/25/2005 07/01/2005 06728/2005 LOW06725/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25(2005 07(01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28(2005 LOW06/25(2005 07/01/2005 06/28(2005 LOW06/25/2005 07/01/2005 06/2872005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06725/2005 07/01/2005 06/28/2005 LOW06725/2005 07/01/2005 06/28/2005 LOW
100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0
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TC4-BIO-30ITC4-BIO-30ITC4-BIO-30ITC4-BIO-30ITC4-BIO-30ITC4-BIO-3QITC4-BIO-30ITC4-BIO-30ITC4-BIO-30ITC4-BIO-30ITC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-B1O-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31ATC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31BTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4rBIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31C
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07/04/200507/04/200507/04/200507/08/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/08/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/08/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/200507/04/2005
19:5419:5419:540:11
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19:5919:5919:5919:5919:5919:5919:5919:5920:0520:0520:0520:0520:0520:0520:0520:0520:0520:0520:0520:0520:0520:050:16
20:0520:0520:0520:0520:0520:0520:0520:0520:1120:1120:1120:1120:1120:1120:1120:1120:11
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81.51100
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5001.05.0
06/25/2005 i06/25/2005 i06/25/200506/25/2005 i06/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/251200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/2 5/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/2 5/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/200506/25/2005
07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/06/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/06/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/06/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/200S 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/2872005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW07/01/2005 06/28/2005 LOW
100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0
1.001.001.000.201.001.001.001.001.00
1.001.00
1.00
1.001.00
1.001.00
1.001.00
1.00
1.001.001.001.00
1.00
1.00
1.000.20
1.001.00
1.00
1.00
1.001.001.001.00
1.001.00
1.00
1.001.001.00
1.001.00
1.00
1.00
1.00
1.001.00
1.000.20
1.00
1.001.00
1.00
1.00
1.00
1.001.00
1.00
1.001.00
1.001.00
1.00
1.00
1.00
1.00
100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100
100100100100
pppcvppppppppppppppppppppppcvppppppppppppppppppppppcvppppppppppppppppp
TC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31CTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31 DTC4-BIO-31DTC4-BIO-31 DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-31DTC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32ATC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32B
Page 12 of 17
005845
34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 1357B S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF1 13578 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF2 13579 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 '13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S34211 MF1MDO MF1MF3 13580 S
07/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/08/2005 0:1807/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/04/2005 20:1107/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/08/2005 0:2007/04/2005 20:3307/04/2005 20:33Q7(04f2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3307/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/08/2005 0:2207/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:3907/04/2005 20:39
7440508 COPPER 6.67439896 IRON 65.17439921 LEAD 4.27439954 MAGNESIUM 10207439965 MANGANESE 20.07439976 MERCURY 0.107440020 NICKEL 0.247440097 POTASSIUM 153007782492 SELENIUM 1.07440224 SILVER 0.197440235 SODIUM 4457440280 THALLIUM 2.57440622 VANADIUM 0.117440666 ZINC 1897429905 ALUMINUM 1947440360 ANTIMONY 0.717440382 ARSENIC 1.47440393 BARIUM 6.77440417 BERYLLIUM 0.0727440439 CADMIUM 25.47440702 CALCIUM 177007440473 CHROMIUM 3.07440484 COBALT 0.517440508 COPPER 41.67439896 IRON 18007439921 LEAD 3557439954 MAGNESIUM 37807439965 MANGANESE 54.77439976 MERCURY 0.0307440020 NICKEL 4.07440097 POTASSIUM 63607782432 SELENIUM 0.937440224 SILVER 1.07440235 SODIUM 43207440280 THALLIUM 2.57440622 VANADIUM 1.67440666 ZINC 19607429905 ALUMINUM 1337440360 ANTIMONY 0.467440382 ARSENIC 1.17440393 BARIUM 4.97440417 BERYLLIUM 0.0477440439 CADMIUM 23.57440702 CALCIUM 116007440473 CHROMIUM 1.97440484 COBALT 0.367440508 COPPER 30.17439896 IRON 11307439921 LEAD 2297439954 MAGNESIUM 22607439965 MANGANESE 34.67439976 MERCURY 0.107440020 NICKEL 2.47440097 POTASSIUM 67807782492 SELENIUM 1.07440224 SILVER 1.07440235 SODIUM 29607440280 THALLIUM 2.57440622 VANADIUM 0.997440666 ZINC 1340
J
UJvULJ
JvLJUU
ULJJ
ULJJvLJ
ULJJ
U
J
UvULJ
JvU
U
ULJJ
ULJJvLJ
ULJJ
LJ
J
UJvULJ
JvU
U
ULJJ
MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0MG/KG 20.0MG/KG 6.0MG/KG 1.0MG/KG 20.0MG/KG 0.50MG/KG 0.50MG/KG 500MG/KG 1.0MG/KG 5.0MG/KG 2.5MG/KG 10.0MG/KG 1.0MG/KG 500MG/KG 1.5MG/KG 0.10MG/KG 4.0MG/KG 500MG/KG 3.5MG/KG 1.0MG/KG 500MG/KG 2.5MG/KG 5.0MG/KG 6.0
06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/06/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06728/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 0672872005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/2672005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/06/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/2872005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/2672005 LOW06/25/2005 07/01/2005 06728/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/06/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW06/25/2005 07/01/2005 06/28/2005 LOW
100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0100.0
1.00
1.00
1.00
1.00
1.00
0.20
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.001.00
1.00
1.00
0.20
1.00
1.001.00
1.001.00
1.00
1.001.00
1.00
1.001.00
1.00
1.00
1.001.00
1.00
1.00
1.001.00
1.00
1.00
1.00
0.20
1.00
1.00
1.00
1.001.001.00
1.00
1.00
100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100
pppppcvppppppppppppppppppppppcvppppppppppppppppppppppcvpppppppp
TC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-328TC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32BTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32CTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32DTC4-BIO-32D
Page 13 of 17
005846
INORGANIC/ORGANIC COMPLETE SDG FILE (CSF) INVENTORY CHECKLIST
Case No. 34211 SDG No. MF1MDO SDG Nos. To Follow SAS No. Date Rec 07/11/05
EPA Lab ID: SENTIN
Lab Location: Huntsville, AL
Region: 6 Audit No.: 34211/MF1MDO
Resubmitted CSF? Yes No X
Box No(s): 1
COMMENTS:
Over for additional comments.
ORIGINALS
CUSTODY SEALS1 . Present on package?
2. Intact upon receipt?
FORM DC-2
3. Numbering scheme accurate?
4. Are enclosed documents listed?
5. Are listed documents enclosed?
FORM DC-1
6. Present?
7. Complete?
8. Accurate?
CHAIN-OF-CUSTODYRECORD(s)
9. Signed?
10. Dated?
TRAFFIC REPORT(s)PACKING LIST(s)
11. Signed?
12. Dated?
AIRBILLS/AIRBILL STICKER
13. Present?
14. Signed?
15. Dated?
SAMPLE TAGS
16. Does DC-1 list tags as being included?
1 7. Present?
OTHER DOCUMENTS18. Complete?
19. Legible?
20. Original?
20a. If "NO", does the copy indicatewhere original documents are located?
YES
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
NO
X
N/A
Auditedb*:
Audited by:
Audited by:
Signature
Michael J. Fertitta/ESAT Data Reviewer
Printed Name/Title
Date 08/26/05
Date
Date
DC-2
Page 14 of 17
005847
*»HHM obtHA contract Laboratory Program Case NO-, ,34211. DT^gr L«l J^
Region:
Project Code:
Account Code:
.CERCLIS ID:
Spill ID:
Site Name/State
Project Leader:
Action:
Sampling Co:
INORGANICSAMPLE No.
MF1MC3
MF1MC5
MF1MC6
MF1MC7
MF1MC8
MF1MDO
MF1MD1
MF1MD2
MF1MD3
MF1MD5
MF1MD6
Inorganic Traffic
6
OKD980629844
Tar Creek OU4 Plants/OK
SCOTT IRVINGOther
CH2M HILL
MATRIX/ CONC/SAMPLER TYPE
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Report & Chain of Custody Record DAS No /rte^tso**'^ •>. rXicJ2>\Q/'(L\ G2_ N^ ' \~~l^*-5-{J
ANALYSIS/TURNAROUND
TM (21)
TM (21)
TM (21)
TM (21)
TM (21)
TM(21)
TM (21)
TM (21)
TM(21)
TM(21)
TM (21)
Date Shipped: 06/27/2005 Chain Of Custody Record Sampler _Sigiature: /^ / ^
rarrior Namo- F°dEv / *! V""'*
AlrhHI: fUfildlRRMRR Relinquished By (Date /Time) Received Byx^ ' ^(bate/Time)s — "^ ^- — /
Shipped to: Sentinel Inc. 1 f ) /~\ X^^ 0/7^7/^-^ / S- DID116 Washington Street, / * < _ ) * ' & < 1 i \JNE 2
Huntsville AL 35801(256) 534-9800 3
4
TAGNoJ STATION SAMPLE COLLECT ORGANIC QCPRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. TYPe
6350944,6424096(2) TC4-BIO-27D 5:06/24/2005 10:57
6350946(1) TC4-BIO-28A 5:06/24/2005 14:18
6350947(1) TC4-BIO-28B 3:06/24/2005 14:22
6350948(1) TC4-BIO-28C 5:06/24/2005 14:28
6350949(1) TC4-BIO-28D 5:06/24/2005 14:30 - 1
6350951 (1) TC4-BIO-29A S: 06/24/2005 14:44 -- ^
6350952(1) TC4-BIO-29B 5:06/24/2005 14:50 - '
6350953(1) TC4-BIO-29C 5:06/24/2005 14:55 - ^V^
6350954(1) TC4-B1O-29D 5:06/24/2005 15:00 - i
6350956(1) TC4-BIO-30A 5:06/24/2005 15:10
6350957,6424095(2) TC4-BIO-30B 5:06/24/2005 15:21
Shipment for CaseComplete? N
Analysis Key:
Samplo(s) to be used for laboratory QC:
MF1MC3, MF1MD6
Additional Sampler Slgnature(s):-| j -,
^^" (lJ^<^^-sfc<^-^ /~"^Concentration: L = Low, M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G
Chain of Custody Seal Number:
Shipment Iced?
TM - CLP I AL I otal Metals + Hg
TR Number: 6-564209055-062405-0001PR provides preliminary results. Requests for preliminary results will Increase analytical costs.
Send Copy to: Sample Management Office. 2000 Edmund Halley Dr., Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222 F2V5.1.043 Page 2 of 3
005848
^j^ , . ^..»uv.i. i-ciuui QI.UI y rruyram Case No: ./34211 ["^
* Inorganic Traffic Report & Chain of Custody Record DAS No j£2§C^^^\^n -in T\ ^x
Region:
Project Code:
Account Code:
CERCLIS ID:cn;|1 in-opni IL>.
Site Name/State
Project Leader:
Action:
Sampling Co:
INORGANICSAMPLE No.
MF1M07
MF1MD8
MF1MEO
MF1ME1
MF1ME2
MF1ME3
6
'
OKD980629844
Tar Creek OU4 Plants/OK
SCOTT IRVINGOther
CH2M HILL
MATRIX/ CONG/SAMPLER TYPE
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Vegetation/ UGJennifer Luffy
Date Shipped:
Carrier Name:
Airbill:
Shipped to:
06/27/2005
FedEx
846141880988
Sentinel Inc.116 Washington Street,NEHuntsville AL 35801(256) 534-9800
Chain of Custody Record
Relinquished By (Date / Time)
1 L l/~-\\s^~ &/'£~)fo5/ /s
2
3
4
Sampler ^^~\ -~ ^Signature: £ ) ^ ( ^
Received By f (Bate /Time)
/ 5 ' OT^
ANALYSIS/ TAG No./ STATION SAMPLE COLLECT ORGANIC QCTURNAROUND PRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. Type
TM(21) 6350958(1)
TM(21) 6350959(1)
TM (21) 6350961 (1)
TM(21) 6350962(1)
TM(21) 6350963(1)
TM(21) 6350964(1)
TC4-BIO-30C S: 06/24/2005 15:14
TC4-BIO-30D S: 06/24/2005 15:26
TC4-BIO-30F 5:06/24/2005 15:10 Field Duplicate
TC4-BIO-30G 5:06/24/2005 15:21 Field Duplicate
TC4-BIO-30H 5:06/24/2005 15:14 Field Duplicate C_^ )
TC4-BIO-30I S: 06/24/2005 15:26 Field Duplicate Ov-?
Shipment for CaseComplete? N
Analysis Key:
Sample(s) to bo used for laboratory QC:
MF1MC3.MF1MD6
Additional Sampler Slgnature(s):^-, /' /•' /
"T^" /^?^=^~~x/fc2^-<^-__- Cii /'~^c_-x:
Concentration: L = Low, M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G
Chain of Custody Seal Number:
Shipment Iced?
TM - CLP TAL 'I otal Metals + Hg ' ~ . . .—
TR Number: 6-564209055-062405-0001PRprovides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr., Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222 F2V5.1.043 Page 3 of 3
005849
VS%? """" h*J-li l-^''t-'" M "-»-»>IU dCL L
"""" Inorganic Traffic
Region: 5
Project Code:
Account Code:
CERCLIS ID: OKD980629844
Spill ID:
Site Name/State: Tar Creek OU4 Plants/OK
Project Leader-. SCOTT IRVING
Action: Other
Sampling Co: CH2M HILL
INORGANIC MATRIX/ CONC/SAMPLE No. SAMPLER TYPE
MF1ME5 Vegetation/ L/GJennifer Luffy
MF1ME6 Vegetation/ UGJennifer Luffy
MF1ME7 Vegetation/ UGJennifer Luffy
MF1ME8 Vegetation/ L/GJennifer Luffy
MF1MFO Vegetation/ U'GJennifer Luffy
MF1MF1 Vegetation/ UGJennifer Luffy
MF1MF2 Vegetation/ UGJennifer Luffy
MF1MF3 Vegetation/ UGJennifer Luffy
MF1MF5 Vegetation/ U'GJennifer Luffy
MF1MF6 Vegetation/ U'GJennifer Luffy
MF1MF7 Vegetation/ L/GJennifer Luffy
auoidcory programReport & Chain of Custody Record
ANALYSIS;TURNAROUND
TM (21)
TM(21)
TM(21)
TM(21)
TM(21)
TM(21)
TM (21)
TM(21)
TM(21)
TM(21)
TM (21)
Date Shipped: 06/27/2005 Chain of CustodyHarrier Name- PorjPv
Airhill- ««^iflAn«7A Relinquished By
Shipped to: Sentinel Inc. 1 / ) ~^ \,116 Washington Street, A' ^ /)NE 2 ^Huntsville AL 35801(256) 534-9800 3
4
TAG NoJ STATION SAMPLE
Case No: f~j - i. 34211 ,. 1"")/ / o *~i f~; c^Onb . r<
iuL*\frfy\ (^ AJt> • I *2-*?>3 • 0Record Sampler ^_^ _
Signature: / J \^^
(Date /Time) Received By ,/ ''(DaW/Time)
-^~ £/lT?fd5, /J-Oc)
COLLECT ORGANIC QCPRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. Type
6350966(1) TC4-B1O-31A 5:06/25/2005
6350967(1) TC4-BIO-31B 5:06/25/2005
6350968(1) TC4-BIO-31C 5:06/25/2005
6350969(1) TC4-BIO-31D 5:06/25/2005
6350971 (1) TC4-BIO-32A S: 06/25/2005
6350972(1) TC4-BIO-32B 5:06/25/2005
6350973(1) TC4-BIO-32C 5:06/25/2005
6350974(1) TC4-BIO-32D 5:06/25/2005
6350976(1) TC4-BIO-33A 5:06/25/2005
6350977 (1) TC4-BIO-33B 5: 06/25/2005
6350978(1) TC4-BIO-33C 5:06/25/2005
9:44
9:45
9:48r^-
9:51 - v ./O
10:02 - p-
*•
10:10 - ,0
^
10:15 - ^
£^-10:20
10:35
10:48
10:55
Shipment for CaseComplete? N
Analysis Key:
Samplo(s) to bo used (or laboratory QC:
MF1MG5
Additional Sampler Signaturo(s):
Y? ' • ^L>^/ -X^-V— K- —-<-«_ / ^-t f l * .
Concentration: L = Low, M = Low/Medium. H = High ""7?ypc/Des!gnate: Composite = C. Grab = G
Chain of Custody Seal Number:
Shipment Iced7
TM = CLP "I AL '1 otal Metals -t- Hg
TR Number: 6-564209055-062605-0001PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr., Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222 F2V5.1.043 Page 1 of 3
005850
ADDENDUM
CADRE NARRATIVE
005851
Date: 8/25/2005
Lab ID: SENTINFile Name: MF1MDO
Qualification: Calibrations
No defects found.
Wincadre3.1.3.2
Data Review Results
Page: 1
Case No.: 34211SDGNo.: MF1MDO
Method: ILM05Criteria: ILM05
Flag :REG6ILM5Defects: R6INORO
Protocol: INORG
005852
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Page:
Lab ID: SENTIN
File Name: MF1MDO
Qualification: CRPL/CROL Standard
No defects found.
Case No.: 34211
SDGNo.: MF1MDO
Method: ILM05
Criteria: ILM05
Flag :REG6ILM5
Defects: R6FNORG
Protocol: INORG
005853
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Lab ID: SENTIN
File Name: MF1MDO
Qualification: Duplicates
No defects found.
Case No.: 34211
SDGNo.: MFIMDOMethod: ILM05
Criteria: ILM05
Flag :REG6ILM5
Defects: R6INORG
Protocol: INORG
005854
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Lab ID: SENTIN
File Name: MF1MDO
Qualification: Holding Time
Case No.: 34211
SDGNo.: MF1MDO
Method: ILM05
Criteria: ILM05
Flag :REG6ILM5
Defects: R6INORG
Protocol: INORG
DC-10 The following inorganic soil samples were reviewed for holding time violations using criteriadeveloped for water samples.
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD6D, MF1MD6S, MF1MD7,
MFIMD8, MF1MEO, MF1ME1, MF1ME2, MF1ME3, MF1ME5,MF1ME6, MF1ME7, MF1ME8,
MF1MFO, MF1MF1, MF1MF2, MF1MF3
005855
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Lab ID: SENTIN
File Name: MF1MDOCase No.: 34211SDGNo.: MF1MDO
Method: 1LM05Criteria: ILM05
Flag .-REG6ILM5
Defects: R6INORG
Qualification: Interference Check Sample Protocol: INORG
DC-6 The following inorganic samples have elements other than Al, Ca, Fe, and Mg at concentrationshigher than 10 mg/L that may cause potential interference. Use professional judgement
to qualify sample data.
MF1MDOPotassium, Sodium
MF1MD1
Potassium, Sodium
MF1MD2Lead, Potassium, Sodium, Zinc
MF1MD3Lead, Potassium, Sodium, Zinc
MF1MD5
Potassium
MF1MD6
Potassium
MF1MD7Potassium, Sodium, Zinc
MF1MD8Potassium, Sodium, Zinc
MF1MEOPotassium
MF1ME1Potassium
MF1ME2
Potassium, Sodium, Zinc
MF1ME3
Potassium, Sodium, Zinc
MF1 IVIES
Potassium, Sodium
MF1ME6Potassium
005856
Date: 8/25/2005 Wincadre 3.1.3.2
Data Review Results
Page:
Lab ID: SENTIN
File Name: MF1MDO
Case No.: 34211
SDGNo.: MF1MDO
Method: ILM05
Criteria: ILM05
Flag :REG6ILM5
Defects: R6INORG
MF1ME7
Potassium, Sodium
MF1ME8
Potassium, Sodium, Zinc
MF1MFO
Potassium
MF1MF1
Potassium
MF1MF2
Potassium, Sodium, Zinc
MF1MF3
Potassium, Sodium, Zinc
005857
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Lab ID: SENTIN
File Name: MF1MDOCase No.: 34211SDONo.: MF1MDO
Method: ILM05Criteria: ILM05
Page:
Flag :REG6ILM5
Defects: R6INORG
Qualification: Laboratory Blanks Protocol: 1NORG
DC-15 The following inorganic samples are associated with an ICB concentration which is lessthan or equal to the CRQL. Detected sample result is also less than or equal to the CRQL.Hits are qualified "U". Sample result is raised to the CRQL if "Raise to detection limit"
option is selected by the validator.
Beryllium
MF1MD2, MF1MD3, MF1MD7, MF1ME2, MF1ME8, MF1MF2, MF1MF3
DC-18 The following inorganic samples are associated with a CCB concentration which is less thanor equal to the CRQL Sample result is also less than or equal to the CRQL. Hits are
qualified "U". Sample result is raised to the CRQL if "Raise to detection limit" option
is selected by the validator.
Beryllium
MF1MD2, MF1MD3, MF1MD7, MF1ME2, MF1ME8, MF1MF2, MF1MF3
Chromium
MF1MDO, MF1MD1, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO
DC-19 The following inorganic samples are associated with a CCB concentration which is less thanor equal to the CRQL. Sample result is greater than the CRQL. Use professional judgement
to qualify data.
ChromiumMF1MD2, MF1MD3
Zinc
MF1MD2, MF1MD3, MF1MD5, MF1MD7, MF1MD8, MF1MEO, MF1ME1, MF1ME2, MF1ME3,
MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1
DC-21 The following inorganic samples are associated with an ICB analyte with negative concentrationwhose absolute value is greater than or equal to the method detection limit (MDL) but lessthan or equal to the CRQL. Use professional judgement to qualify sample data.
Mercury
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,MF1MF2, MF1MF3
ZincMF1MDO, MF1MD1, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO, MF1ME1,MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1, MF1MF2,
MF1MF3
DC-22 The following inorganic samples are associated with a CCB analyte with negative concentrationwhose absolute value is greater than or equal to the method detection limit (MDL) but less
than or equal to the CRQL. Use professional judgement to qualify sample data.
Aluminum
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
005858
Date: 8/25/2005 Wincadre 3.1.3.2
Data Review Results
Lab ID: SENTIN Case No.: 34211 Method: ILM05 Flag :REG6ILM5
File Name: MF1MDO SDGNo.: MF1MDO Criteria: ILM05 Defects: R6INORG
Mercury
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
Zinc
MF1MDO, MF1MD1, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO, MF1ME1,
MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1, MF1MF2,
MF1MF3
005859
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Lab ID: SENTIN
File Name: MF1MDOCase No.: 34211
SDGNo.: MF1MDO
Qualification: Laboratory Control Sample
No defects found.
Method: 1LM05Criteria: ILM05
Page:
Flag :REG6ILM5Defects: R6INORG
Protocol: INORG
005860
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Page: 10
Lab ID: SENTINFile Name: MF1MDO
Case No.: 34211SDGNo.: MF1MDO
Method: ILM05
Criteria: ILM05
Flag :REG6ILM5
Defects: R6FNORG
Qualification: Matrix Spikes Protocol: INORG
DC-5 The following inorganic samples are associated with a matrix spike recovery which is outsideprimary low criteria. Post-digest spike sample was either not required or it was required
but not analyzed. Hits are qualified "J-" and non-detects are qualified "UJ-".
Mercury
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
DC-8 The following inorganic samples are associated with a matrix spike recovery outside primaryhigh criteria. However, post-digest spike percent recovery was less than or equal to the
high limit. Detects are flagged "J" and non-detects are not flagged.
Antimony
MF1MDO, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO, MF1ME1,
MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1, MF1MF2,
MF1MF3
Cadmium
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
DC-11 The following inorganic samples are associated with a matrix spike recovery which is outsideprimary low criteria. However, post-digest spike percent recovery was more than or equal
to the low limit. Detects are flagged "J".
Lead
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,MF1MF2, MF1MF3
Zinc
MF1MDO, MFIMD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
005861
Date: 8/25/2005 Wincadre 3.1.3.2
Data Review Results
Lab ID: SENTIN Case No.: 34211 Method: ILM05 Flag :REG6ILM5
File Name: MF1MDO SDONo.: MF1MDO Criteria: ILM05 Defects: R6INORG
Qualification: Sample Result Verification Protocol: 1NORG
DC-5 The following inorganic samples have analyte concentrations reported below the quantitation
limit (CRQL). All results below the CRQL are qualified"LJ".
MF1MDO
Aluminum, Antimony, Arsenic, Barium, Chromium, Cobalt, Magnesium, Nickel,
Selenium, Silver, Vanadium
MF1MD1
Aluminum, Arsenic, Barium, Chromium, Cobalt, Magnesium, Nickel, Selenium
MF1MD2
Antimony, Barium, Beryllium, Cobalt, Selenium, Vanadium
MF1MD3
Antimony, Arsenic, Barium, Beryllium, Cobalt, Selenium, Vanadium
MF1MD5
Aluminum, Antimony, Arsenic, Barium, Chromium, Nickel, Selenium, Sodium,
Vanadium
MF1MD6
Antimony, Arsenic, Barium, Chromium, Cobalt, Nickel, Selenium, Silver,
Sodium, Vanadium
MF1MD6D
Antimony, Arsenic, Barium, Chromium, Nickel, Selenium, Silver, Sodium,
Vanadium
MF1MD7
Antimony, Arsenic, Barium, Beryllium, Chromium, Cobalt, Magnesium, Nickel,
Selenium, Silver, Vanadium
MF1MD8
Antimony, Arsenic, Barium, Chromium, Cobalt, Magnesium, Nickel, Selenium,
Vanadium
MF1MEO
Aluminum, Antimony, Arsenic, Barium, Chromium, Nickel, Selenium, Sodium,
Vanadium
MF1ME1
Antimony, Arsenic, Barium, Chromium, Cobalt, Nickel, Selenium, Silver,
Sodium, Vanadium
MF1ME2
Antimony, Arsenic, Barium, Beryllium, Cobalt, Nickel, Selenium, Silver,
Vanadium
005862
Date: 8/25/2005 Wincadre 3.1.3.2 Page: 12
Data Review Results
Lab ID: SENT1N Case No.: 34211 Method: ILM05 Flag :REG6ILM5File Name: MF1MDO SDG No.: MF1MDO Criteria: ILM05 Defects: R6INORG
MF1ME3Antimony, Arsenic, Barium, Chromium, Cobalt, Magnesium, Nickel, Selenium,Vanadium
MF1ME5
Aluminum, Antimony, Arsenic, Barium, Cadmium, Chromium, Cobalt, Copper,
Magnesium, Nickel, Selenium
MF1ME6Aluminum, Antimony, Barium, Cadmium, Chromium, Copper, Lead, Magnesium,
Nickel, Selenium, Sodium
MF1ME7
Antimony, Arsenic, Barium, Chromium, Cobalt, Mercury, Nickel, Silver,Vanadium
MF1ME8Antimony, Arsenic, Barium, Beryllium, Chromium, Cobalt, Nickel, Selenium,Vanadium
MF1MFO
Antimony, Arsenic, Barium, Chromium, Magnesium, Nickel, Selenium, Sodium,Vanadium
MF1MF1Aluminum, Antimony, Barium, Chromium, Nickel, Selenium, Silver, Sodium,Vanadium
MF1MF2Antimony, Arsenic, Barium, Beryllium, Cobalt, Mercury, Nickel, Selenium,Vanadium
MF1MF3Antimony, Arsenic, Barium, Beryllium, Chromium, Cobalt, Nickel, Selenium,Vanadium
005863
Date: 8/25/2005
Lab ID: SENTIN
File Name: MF1MDO
Wincadre3.1.3.2
Data Review Results
Case No.: 34211
SDGNo.: MF1MDO
Method: ILM05
Criteria: ILM05
Page: 13
Flag :REG6ILM5
Defects: R6INORG
Qualification: Serial Dilution Protocol: 1NORG
DC-4 The following inorganic samples are associated with an ICP serial dilution percent difference
which is not in criteria. The serial dilution result is greater than the sample result,
indicating a potential negative interference. Hits and non-detects are not qualified.
Aluminum
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
Nickel
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
Potassium
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
Sodium
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD7, MF1MD8, MF1MEO,
MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO, MF1MF1,
MF1MF2, MF1MF3
005864
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Lab ID: SENTIN
File Name: MF1MDO
Qualification: CADRE Reserved
Case No.: 34211
SDGNo.: MF1MDO
Method: ILM05
Criteria: ILM05
Page: 14
Flag :REO6ILM5
Defects: R6INORG
Protocol: INORG
DC-2 Verification of non-detected results and assignment of "U" qualifier when the reported
value is less than detection limit.
MF1MDO, MF1MD1, MF1MD2, MF1MD3, MF1MD5, MF1MD6, MF1MD6D, MF1MD7, MF1MD8,
MF1MEO, MF1ME1, MF1ME2, MF1ME3, MF1ME5, MF1ME6, MF1ME7, MF1ME8, MF1MFO,
MF1MF1, MF1MF2, MF1MF3, PBS
005865
Date: 8/25/2005 Wincadre3.1.3.2
Data Review Results
Page: 15
Lab ID: SENTIN
File Name: MF1MDO
Case No.: 34211
SDGNo.: MF1MDO
Method: ILM05
Criteria: ILM05
Flag :REG6ILM5
Defects: R6INORG
Data Review Criteria Set Options:
Detection LimitPEST pel D expanded criteria
Use MDL
Holding Time
Region 3 PAH option
Region 3 PCB option
Expanded criteriaInorganic missing pH option
CalibrationsRRF expanded criteria
VOA/BNA PctD expanded criteria
VOA/BNA PelRSD expanded criteria
Use mean RRFUse VOA/BNA dual purpose standard option
Use in i l i a l I N D A / I N D B pel resolution
Use continuing INDA/INDB pel resolution
Use PEST low concentration option
PEST low concentration PclRSD expanded criteriaUse DMC/SMC/SuiTOgale oplion
Use INORG extreme high pet recovery
Matrix Spikes
Use PEST low concentration rules
DMC/SMC/SurrogatesRegion 3 validation rules
Check di lu t ion tacior
Use advisory surrogatesUse low concentration rules
Use BNA low concentration expanded criteria
CADRE association rules
IPC/TuneExpanded criteria
System PerformanceUse i n i l i a l PEM pel resolution
Use cont inuing PEM pet resolution
CRDUCRQL Standards
Region 2 validation rulesRegion 3 validation rules
LCS
Pet rec expanded criteria
Duplicates
RPD and AD expanded criteria
Furnace AA QCPet R expanded upper criteria
Corr coef expanded criteria
BlanksRaise lo detection l imil
Use VOA storage/insl blanks
Use low concentration rules
Field QCCombine method/field blanksCRDL contamination criteria
005866