mercontrol™ 7895 handbook mercury reduction technology · the following special equipment is...

MerControl™ 7895 HandbookMercury Reduction Technology

Table of Contents

Introduction to Nalco Water ..........................................................................................................................3

Product Description ................................................................................................................................. 4

Physical Description ....................................................................................................................................... 4

Physical Properties

Viscosity Information ............................................................................................................................... 5

Crystallization Information .................................................................................................................... 5

Material Compatibility ................................................................................................................................... 6

Storage Vessels ......................................................................................................................................... 6

Pipework ..................................................................................................................................................... 6

Pumps .......................................................................................................................................................... 6

Packaging Information ...................................................................................................................................7

Bulk Tankers ................................................................................................................................................7

Totes/IBC .....................................................................................................................................................7

Labelling ......................................................................................................................................................7

Logistics .......................................................................................................................................................7

User Guide ........................................................................................................................................................ 8

Hazards ....................................................................................................................................................... 8

Effects of Exposure

Skin Exposure................................................................................................................................... 8

Eye Contact ....................................................................................................................................... 8

Inhalation .......................................................................................................................................... 8

Ingestion ............................................................................................................................................ 8

Safe Handling ............................................................................................................................................ 8

Personal Protection ................................................................................................................................. 8

Personal Protective Equipment (PPE) ....................................................................................................... 9

Eyes .............................................................................................................................................................. 9

Body ............................................................................................................................................................. 9

Hands........................................................................................................................................................... 9

General Recommendations .......................................................................................................................... 9

Storage Facilities ...................................................................................................................................... 9

Safety and Security Measures .............................................................................................................. 10

Handling ..................................................................................................................................................... 10

Nalco Water Zero Defect Delivery Program ........................................................................................ 10-11

MerControl™ 7896 Safety Data Sheet (SDS) .................................................................................... 12-20

2 | MerControl™ 7895 Handbook — Mercury Reduction Technology

Reinventing the Way Water is ManagedNalco Water is a recognized, global leader in industrial water treatment, water

technology, expertise, and services. From the time water enters a facility until

the moment it is returned back to the environment, it’s a critical component

of our customers’ business. We use expertise and innovation to help them

manage their water and measure success one drop at a time.

Each year, through this expertise, thousands of our customers save more

than 140 billion gallons of water, the equivalent to the annual drinking needs

of more than 200 million people. Through our work, we’re not only helping

our customers preserve water, but also produce better quality products with

a lower total operating cost.

We are part of Ecolab, the global leader in water, hygiene and energy

technologies and services that protect people and vital resources. As a global

company, we are finding solutions to the world’s biggest challenges to provide

clean water, safe food, abundant energy, and healthy environments.

MerControl™ 7895 Handbook — Mercury Reduction Technology | 3

Product Description MerControl™ 7895 Technology is a coal additive used to reduce mercury emissions for coal-fired electric generating units (EGU). Specifically, MerControl 7895 is a stable, calcium bromide salt solution that increases oxidation of vapor phase mercury. It improves mercury capture efficiency of existing air quality control devices (electrostatic precipitators, fabric filters, spray dryer absorbers and w-FGD units) without adverse effects on equipment performance.

Nalco Water is the sole licensee of the application process related to bromide addition to impact coal derived flue gas mercury capture and oxidation. More specific information related to the intellectual property and patents related to this process is available from your local Nalco Water representative.

MerControl 7895 features the following:

• Provides a flexible, rapid response to fluctuations in operations and fuel quality that impact mercury emissions

• Liquid additive simplifies application, distribution, and control

• Multiple potential application points yield flexibility in the case of retrofit designs

• Can be used in conjunction with activated carbon injection (ACI) to lower carbon usage and improve fly ash quality

• Low capital feed systems with a small footprint

PHYSICAL DESCRIPTION

Characteristic

Appearance Light yellow, amber

Odor none

Specific gravity (g/mL) 1.69

Density (lb/gal) 14.2

Viscosity @ 75ºF (cP) 8

Viscosity @ 32ºF (cP) 22

Crystallization Temperature (ºF) 1

VOC Content no data available

Freeze/Thaw recoverable


PHYSICAL PROPERTIESViscosity Information

CRYSTALLIZATION INFORMATION

CaBr2 wt% Density lb/gal Density g/ccTrue Crystallization

TemperatureºF ºC

0 8.35 1.00 32 0

10 9.10 1.09 25 -4

20 10.01 1.20 14 -10

30 11.10 1.33 -4 -20

35 11.68 1.40 -15 -26

40 12.36 1.48 -35 -37

45 13.11 1.57 -62 -52

50 13.94 1.67 -31 -35

51 14.11 1.69 -15 -26

52 14.28 1.71 1 -17

53 14.44 1.73 14 -10

0

50

100

150

200

250

0 20 40 60 80 100 120

Vis

coci

ty [c

P]

Temperature [ºF]


MATERIAL COMPATIBILITY

Compatible Not Compatible

304 SS† Polyethylene Brass

316 SS† Fiberglass (FRP) Coated Steel Drum

CPVC Polypropylene Mild Steel

Neoprene Hypalon® elastomer

Buna-N Polyurethane

† - not ideal for storage

STORAGE VESSELSStorage tanks for MerControl 7895 should be constructed from AISI 316 stainless steel or carbon steel protected by an epoxy lining. It is also possible to use FRP (Fiberglass Reinforced Plastic) tanks.

PIPEWORKStainless steel or plastic polypropylene piping can be used.

PUMPSPumps are typically constructed of 316 stainless steel contact parts.


Packaging InformationMerControl 7895 can be delivered to client facilities via bulk delivery or totes/intermediate bulk containers (IBCs).

MerControl 7895 does not contain materials regulated for transport and does not require special placard and tank labelling.

BULK TANKERSBulk deliveries can be unloaded directly into site, bulk storage tank by dedicated Nalco Water delivery specialist. These deliveries are Zero Defect Delivery by specialists trained to ensure safe, precise, and timely deliveries.

TOTES/IBCDeliveries can also be provided in 250 gallon IBCs and transported via delivery trucks. These containers have dimensions of 39” X 47” X 47” and weigh approximately 3,750 lbs..

LABELLING

LOGISTICSMerControl 7895 is manufactured in several different vendor sites and packaged at Nalco Water’s Ellwood City, PA and Freeport, TX facilities.


User GuideHAZARDSAs with all chemicals, MerControl 7895 can be hazardous if handled improperly.

Effects of ExposureSKIN EXPOSUREMerControl 7895 can irritate the skin with prolonged exposure. Wash effected area for 15 minutes with a mild soap. If symptoms persist, seek medical attention.

EYE CONTACT MerControl 7895 causes serious irritation to the eyes. Wash eyes for at least 15 minutes after exposure. If symptoms persist, seek medical attention.

INHALATION Health injuries are not known or expected under normal use.

INGESTION Swallowing MerControl 7895 may cause nausea and vomiting in addition to irritation of the mucous membranes of the gastrointestinal tract. If symptoms persist, seek medical attention.

Safe HandlingThe use of chemical gauntlets is recommended. The choice of work glove depends on work conditions and what chemicals are handled, but Nalco Water has positive experience under light handling conditions using gloves made from PVC. Leather work gloves should be avoided as they may become inflexible over time after exposure to this product. Gloves should be replaced immediately if signs of degradation are observed.

Breakthrough time not determined as preparation, consult PPE manufacturers.

PERSONAL PROTECTION Read and follow the instructions in the SDS (Safety Data Sheet) and always have it available on location. A copy of the SDS is located at the back of this handbook. Please contact a Nalco Water representative for the most current SDS.


Personal Protective Equipment (PPE)Use the correct PPE as recommended.

The following special equipment is necessary for handling MerControl 7895:

EYES Safety glasses with side shields are sufficient. However, a full face shield in combination with a chin guard may also be used in addition to safety glasses and side shields for additional protection of the eyes and face.

BODYWear standard protective clothing. Slicker suits are recommended to be worn in areas where exposure is likely.

HANDS Wear leak-proof gloves made of natural or synthetic-rubber material. Glove cuffs should be worn inside of slicker suit sleeves to prevent liquid ingress into gloves. Do not use leather gloves.

General Site RecommendationsThis guide provides some standard precautions to be taken at a MerControl 7895 installation.

STORAGE FACILITIESThe following is a general guide for choosing and supervising a storage area for MerControl 7895. Note that all local laws and regulations and codes must be strictly followed; the precautions listed below are in addition to those specified in local codes and site-specific instructions.

If required by local regulations, dikes should enclose the worksite to protect the area from external flooding and to minimize the potential dispersal of MerControl 7895 in those cases. The minimum diked volume should be equivalent to the largest storage tank plus 10%.

The diked area can have a sewer connection if equipped with a quick closing device to prevent the ingress of MerControl 7895 into the sewer system in case of emergency.

Provide an adequately sized sump in the diked area for collecting MerControl 7895 spills and pumping away collected contaminated rain water or firefighting water.

Minimize areas where MerControl 7895 liquid can accumulate, such as pits or confined spaces.


SAFETY AND SECURITY MEASURESAreas used for MerControl 7895 use or storage should be secured to prevent unauthorized access. The area should have adequate lighting to ensure proper visibility.

Non-freeze safety showers and eyewash fountains should be located in MerControl 7895 usage areas. These showers should be marked clearly and with unobstructed access within 30 meters or 10 seconds walking distance from any location in the storage area. Provide an alternate supply of clean water.

Provide telephone/communications for accident reporting that is clearly available and easily accessible in the event of an emergency.

HANDLING All management and operating personnel involved in the use or handling of MerControl 7895 should undergo safety training in addition to the specific task training.

Only experienced, well-trained operators should be allowed to receive and handle MerControl 7895 receptacles.

Any handling of MerControl 7895 should be done with a high standard of housekeeping and personal hygiene. Ensure that road and rail vehicles cannot be moved during a transfer operation.

Nalco Water Zero Defect Delivery ProgramThese are the eight steps Nalco Water uses to ensure correct and safe deliveries.

1. RIGHT PRODUCTDuring the delivery, any time chemicals are transferred - Checks are made against the delivery documentation, the tanker information, and the bulk tank. Any discrepancy must be resolved before any further steps are taken.

2. RIGHT QUANTITYBulk tanks will only be filled to 90% of capacity. If additional chemical remains in tanker, it may not be used to fill other tanks or IBCs without dispatch approval.

3. RIGHT TANKBulk tank numbers and fill lines must match bill of lading (BOL) information.

4. RIGHT TIMEDeliveries must be checked against the requested delivery times and dates specified on the BOL.


5. RIGHT SAFETY PROCEDURESThe delivery specialist must wear, at minimum; hard hat, face shield, chemical goggles, steel toed shoes, long pants, long-sleeved shirt, chemical gloves, and apron. Specific chemicals and/or site location may require additonal PPE. Any hazardous material deliveries will require additional PPE. Hazard survey will take place before work begins. Additionally, safety showers and eye washes will be identified before working.

6. RIGHT SECURITY PROCEDURESVehicles will be secured when stopped, including removal of keys. The tractor will be disabled when not in service.

7. NO CONTAMINATIONBefore initially accepting chemical, trailer compartments will be cleaned and washed properly. Clean hoses, pumps and fittings will be used for every single chemical transfer. Once at the delivery site, a Zero Defect Delivery checklist will be performed to ensure the right product is unloaded in the right tank.

8. NO SPILLSBefore delivery, all fill lines and all connections must be secured and sight glass/level gauge verified. Buckets and spill pads will be used under connections. During the delivery, the delivery specialist will check for leaks and monitor tank level. After the delivery, lines will be removed carefully and bled prior to disconnecting.

Nalco Water views a single drop of chemical to be a spill. Our delivery specialists are trained and used specifically because of their adherence to our Zero Defect Delivery program.


SAFETY DATA SHEET

MERCONTROL® 7895

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Section: 1. PRODUCT AND COMPANY IDENTIFICATION Product name : MERCONTROL® 7895

Other means of identification : Not applicable.

Recommended use : Mercury Control

Restrictions on use : Refer to available product literature or ask your local Sales Representative for restrictions on use and dose limits.

Company : Nalco Company 1601 W. Diehl Road Naperville, Illinois 60563-1198 USA TEL: (630)305-1000

Emergency telephone number

: (800) 424-9300 (24 Hours) CHEMTREC

Issuing date : 11/18/2014

Section: 2. HAZARDS IDENTIFICATION

GHS Classification

Skin irritation : Category 2 Eye irritation : Category 2A

GHS Label element

Hazard pictograms :

Signal Word : Warning

Hazard Statements : Causes skin irritation.

Causes serious eye irritation.

Precautionary Statements : Prevention: Wash skin thoroughly after handling. Wear eye protection/face protection. Wear protective gloves. Response: IF ON SKIN: Wash with plenty of soap and water. IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. If skin irritation occurs: Get medical advice/attention. If eye irritation persists: Get medical advice/ attention. Take off contaminated clothing and wash before reuse.

Other hazards : None known. Section: 3. COMPOSITION/INFORMATION ON INGREDIENTS


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Pure substance/mixture : Mixture

Chemical Name CAS-No. Concentration: (%) Calcium Bromide 7789-41-5 30 - 60 Section: 4. FIRST AID MEASURES In case of eye contact : Rinse immediately with plenty of water, also under the eyelids.

Remove contact lenses, if present and easy to do. Continue rinsing. Get medical attention if symptoms occur.

In case of skin contact : Wash off immediately with plenty of water. Use a mild soap if available. Get medical attention if irritation develops and persists.

If swallowed : Rinse mouth. Get medical attention if symptoms occur.

If inhaled : Get medical attention if symptoms occur.

Protection of first-aiders : In event of emergency assess the danger before taking action. Do not put yourself at risk of injury. If in doubt, contact emergency responders.Use personal protective equipment as required.

Notes to physician : Treat symptomatically.

Most important symptoms and effects, both acute and delayed

: See Section 11 for more detailed information on health effects and symptoms.

Section: 5. FIREFIGHTING MEASURES Suitable extinguishing media : Use extinguishing measures that are appropriate to local

circumstances and the surrounding environment. Unsuitable extinguishing media

: None known.

Specific hazards during firefighting

: Not flammable or combustible.

Hazardous combustion products

: Carbon oxides

Special protective equipment for firefighters

: Use personal protective equipment.

Specific extinguishing methods

: Fire residues and contaminated fire extinguishing water must be disposed of in accordance with local regulations. In the event of fire and/or explosion do not breathe fumes.

Section: 6. ACCIDENTAL RELEASE MEASURES Personal precautions, protective equipment and emergency procedures

: Ensure clean-up is conducted by trained personnel only. Refer to protective measures listed in sections 7 and 8.

Environmental precautions : Do not allow contact with soil, surface or ground water.


SAFETY DATA SHEET

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Methods and materials for containment and cleaning up

: Stop leak if safe to do so. Contain spillage, and then collect with non-combustible absorbent material, (e.g. sand, earth, diatomaceous earth, vermiculite) and place in container for disposal according to local / national regulations (see section 13). For large spills, dike spilled material or otherwise contain material to ensure runoff does not reach a waterway. Flush away traces with water.

Section: 7. HANDLING AND STORAGE Advice on safe handling : Avoid contact with skin and eyes. Wash hands thoroughly after

handling. Use only with adequate ventilation.

Conditions for safe storage : Keep out of reach of children. Keep container tightly closed. Store in suitable labeled containers.

Suitable material : The following compatibility data is suggested based on similar product data and/or industry experience: Shipping and long term storage compatibility with construction materials can vary; we therefore recommend that compatibility is tested prior to use.

Unsuitable material : not determined Section: 8. EXPOSURE CONTROLS/PERSONAL PROTECTION

Components with workplace control parameters

Contains no substances with occupational exposure limit values. Engineering measures : Good general ventilation should be sufficient to control worker

exposure to airborne contaminants. Personal protective equipment Eye protection : Safety glasses with side-shields

Hand protection : Wear the following personal protective equipment:

Standard glove type. Gloves should be discarded and replaced if there is any indication of degradation or chemical breakthrough.

Skin protection : Wear suitable protective clothing.

Respiratory protection : No personal respiratory protective equipment normally required.

Hygiene measures : Handle in accordance with good industrial hygiene and safety practice. Remove and wash contaminated clothing before re-use. Wash face, hands and any exposed skin thoroughly after handling.

Section: 9. PHYSICAL AND CHEMICAL PROPERTIES Appearance : Liquid

Colour : Light yellow Amber

Odour : no data available

Flash point : does not flash

pH : 7.5


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Odour Threshold : no data available

Melting point/freezing point : no data available

Initial boiling point and boiling range

: 127.7 °C

Evaporation rate : no data available

Flammability (solid, gas) : no data available

Upper explosion limit : no data available

Lower explosion limit : no data available

Vapour pressure : Not applicable.

Relative vapour density : no data available

Relative density : 1.69

Density : 14 lb/gal

Water solubility : completely soluble

Solubility in other solvents : no data available

Partition coefficient: n-octanol/water

: no data available

Auto-ignition temperature : no data available

Thermal decomposition temperature

: no data available

Viscosity, dynamic : no data available

Viscosity, kinematic : no data available

VOC : no data available

Section: 10. STABILITY AND REACTIVITY Chemical stability : Stable under normal conditions.

Possibility of hazardous reactions

: No dangerous reaction known under conditions of normal use.

Conditions to avoid : None known.

Incompatible materials : Strong acids Strong oxidizing agents

Hazardous decomposition products

: Hydrogen bromide Bromine

Section: 11. TOXICOLOGICAL INFORMATION Information on likely routes of exposure

: Inhalation, Eye contact, Skin contact

Potential Health Effects Eyes : Causes serious eye irritation.

Skin : Causes skin irritation.

Ingestion : Health injuries are not known or expected under normal use.


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Inhalation : Health injuries are not known or expected under normal use.

Chronic Exposure : Health injuries are not known or expected under normal use.

Experience with human exposure Eye contact : Redness, Pain, Irritation

Skin contact : Redness, Irritation

Ingestion : No symptoms known or expected.

Inhalation : No symptoms known or expected.

Toxicity Product

Acute oral toxicity : rat: 2,210 mg/kg Test substance: Active Substance

Acute inhalation toxicity : no data available

Acute dermal toxicity : no data available

Skin corrosion/irritation : Result: Skin irritation

Serious eye damage/eye irritation

: Result: Eye irritation

Respiratory or skin sensitization

: no data available

Carcinogenicity : no data available

Reproductive effects : no data available

Germ cell mutagenicity : no data available

Teratogenicity : no data available

STOT - single exposure : no data available

STOT - repeated exposure : no data available

Aspiration toxicity : no data available

Section: 12. ECOLOGICAL INFORMATION Ecotoxicity

Environmental Effects : This product has no known ecotoxicological effects.

Product

Toxicity to fish : LC50 Guppy: 538 mg/l Exposure time: 96 hrs


SAFETY DATA SHEET

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Test substance: Similar Product

LC50 Rainbow Trout: > 1,000 mg/l Exposure time: 96 hrs Test substance: Similar Product

LC50 Fathead Minnow: > 1,000 mg/l Exposure time: 96 hrs Test substance: Similar Product

LC50 Inland Silverside: > 5,000.000 mg/l Exposure time: 96 hrs Test substance: Similar Product

Product

Toxicity to daphnia and other aquatic invertebrates

: LC50 Daphnia magna: > 1,000 mg/l Exposure time: 48 hrs Test substance: Similar Product

LC50 Mysid Shrimp (Mysidopsis bahia): 1,827.000 mg/l Exposure time: 96 hrs Test substance: Similar Product

Persistence and degradability

Greater than 95% of this product consists of inorganic substances for which a biodegradation value is not applicable. Mobility The environmental fate was estimated using a level III fugacity model embedded in the EPI (estimation program interface) Suite TM, provided by the US EPA. The model assumes a steady state condition between the total input and output. The level III model does not require equilibrium between the defined media. The information provided is intended to give the user a general estimate of the environmental fate of this product under the defined conditions of the models. If released into the environment this material is expected to distribute to the air, water and soil/sediment in the approximate respective percentages; Air : <5% Water : 30 - 50% Soil : 50 - 70% Bioaccumulative potential This preparation or material is not expected to bioaccumulate. Other information no data available Section: 13. DISPOSAL CONSIDERATIONS


SAFETY DATA SHEET

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If this product becomes a waste, it is not a hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA) 40 CFR 261, since it does not have the characteristics of Subpart C, nor is it listed under Subpart D. Disposal methods : Where possible recycling is preferred to disposal or

incineration. If recycling is not practicable, dispose of in compliance with local regulations. Dispose of wastes in an approved waste disposal facility.

Disposal considerations : Dispose of as unused product. Empty containers should be

taken to an approved waste handling site for recycling or disposal. Do not re-use empty containers.

Section: 14. TRANSPORT INFORMATION The shipper/consignor/sender is responsible to ensure that the packaging, labeling, and markings are in compliance with the selected mode of transport. Land transport (DOT) Proper shipping name : PRODUCT IS NOT REGULATED DURING

TRANSPORTATION Air transport (IATA) Proper shipping name : PRODUCT IS NOT REGULATED DURING

TRANSPORTATION Sea transport (IMDG/IMO) Proper shipping name : PRODUCT IS NOT REGULATED DURING

TRANSPORTATION Section: 15. REGULATORY INFORMATION

EPCRA - Emergency Planning and Community Right-to-Know Act

CERCLA Reportable Quantity This material does not contain any components with a CERCLA RQ.

SARA 304 Extremely Hazardous Substances Reportable Quantity This material does not contain any components with a section 304 EHS RQ. SARA 311/312 Hazards

: Acute Health Hazard

SARA 302

: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302.

SARA 313

: This material does not contain any chemical components with known CAS numbers that exceed the threshold (De Minimis) reporting levels established by SARA Title III, Section 313.

California Prop 65 This product does not contain any chemicals known to State of California to cause cancer, birth defects, or any other reproductive harm.


SAFETY DATA SHEET

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INTERNATIONAL CHEMICAL CONTROL LAWS : TOXIC SUBSTANCES CONTROL ACT (TSCA) The substances in this preparation are included on or exempted from the TSCA 8(b) Inventory (40 CFR 710) CANADIAN ENVIRONMENTAL PROTECTION ACT (CEPA) The substances in this preparation are listed on the Domestic Substances List (DSL), are exempt, or have been reported in accordance with the New Substances Notification Regulations. AUSTRALIA All substances in this product comply with the National Industrial Chemicals Notification & Assessment Scheme (NICNAS). CHINA All substances in this product comply with the Provisions on the Environmental Administration of New Chemical Substances and are listed on or exempt from the Inventory of Existing Chemical Substances China (IECSC). EUROPE The substances in this preparation have been reviewed for compliance with the EINECS or ELINCS inventories. JAPAN All substances in this product comply with the Law Regulating the Manufacture and Importation Of Chemical Substances and are listed on the Existing and New Chemical Substances list (ENCS). KOREA All substances in this product comply with the Toxic Chemical Control Law (TCCL) and are listed on the Existing Chemicals List (ECL) NEW ZEALAND All substances in this product comply with the Hazardous Substances and New Organisms (HSNO) Act 1996,and are listed on or are exempt from the New Zealand Inventory of Chemicals. PHILIPPINES All substances in this product comply with the Republic Act 6969 (RA 6969) and are listed on the Philippines Inventory of Chemicals & Chemical Substances (PICCS). Section: 16. OTHER INFORMATION

NFPA: HMIS III:

Revision Date : 11/18/2014 Version Number : 1.1

Flammability

Hea

lth

Instability

2 0

0

FLAMMABILITY

PHYSICAL HAZARD

HEALTH

0

0

2

Special hazard.

0 = not significant, 1 =Slight, 2 = Moderate, 3 = High 4 = Extreme, * = Chronic


SAFETY DATA SHEET

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Prepared By : Regulatory Affairs

REVISED INFORMATION: Significant changes to regulatory or health information for this revision is indicated by a bar in the left-hand margin of the SDS. The information provided in this Safety Data Sheet is correct to the best of our knowledge, information and belief at the date of its publication. The information given is designed only as a guidance for safe handling, use, processing, storage, transportation, disposal and release and is not to be considered a warranty or quality specification. The information relates only to the specific material designated and may not be valid for such material used in combination with any other materials or in any process, unless specified in the text. For additional copies of an MSDS visit www.nalco.com and request access.


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