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Page 1: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

Page 2: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

X

Z Y

Comparison of shear strength tests

A4PB Asymmetrical four-point bending test (ASTM C1469)

TC Torsion cylinder

TT Torsion Tube

TS Torsion square

THG Torsion hour-glass

DN Double notched ASTM C1292-00 & C1425-99

SLO single lap off

set ASTM D905-03

DLO Double-lap offset

SL Single lap offset

BT Brazilian test ASTM B 898

Page 3: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

X

Z Y

Comparison of shear strength tests

A4PB Asymmetrical four-point bending test (ASTM C1469)

TC Torsion cylinder

TT Torsion Tube

TS Torsion square

THG Torsion hour-glass

DN Double notched ASTM

C1292-00 & C1425-99

SLO Single lap off set

DLO Double-lap offset

SL Single lap offset

BT Brazilian test

4 3

18

10

10 φ 10

10

φo 10

φi 8 10

5

25

12 5

10

3

5

10

10 6

10

5

6

φ 15

3

15

15

4 4

30

ASTM B 898

A4PB Asymmetrical four-point bending test (ASTM C1469)

Page 4: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

X

Z Y

Comparison of shear strength tests

A4PB Asymmetrical four-point bending test (ASTM C1469)

TC Torsion cylinder

TT Torsion Tube

TS Torsion square

THG Torsion hour-glass

DN Double notched ASTM

C1292-00 & C1425-99

SLO Single lap off set

DLO Double-lap offset

SL Single lap offset

BT Brazilian test

4 3

18

10

10 φ 10

10

φo 10

φi 8 10

5

25

12 5

10

3

5

10

10 6

10

5

6

φ 15

3

15

15

4 4

30

ASTM B 898

the adhesive is a “ model” joining material to obtain a large number of joined samples in reasonable time

SiC , Al2O3, C/C joined by an adhesive (epoxy resin - Araldite AV 119)

A4PB Asymmetrical four-point bending test (ASTM C1469)

Page 5: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

4P- Asy: Notches needed, not suitable for strong joints, pure shear

•different tests give different results on identical samples

•PROs and CONs of each test for a specific joint must be evaluated

Single lap (SL): Critical alignment joint/fixtures Not suitable for strong joints

Double notched (DN) : Critical role of notches

Single lap off set (SLO): Critical role of lateral fixtures

Double lap off set (DLO) Underestimated values

B 898: Huge amount of material needed

Brazilian: Shear value not straightforward

•M. Ferraris et al., Composites: Part B 41 (2010) 182–191 •A. Ventrella et al., J Mater Sci (2010) 45:4401–4405 •E. Martin et al., submitted to Materials Characterization (2010)

Page 6: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

C/C test efficiency %

Ceramics test efficiency

% DN 16,29 ± 3,30

(33,02 ± 4,98 *) 80%

TS

Not suitable 0% Not suitable 0%

TC

19.7± 5.4 70% 53,7±9.4 80%

BT 32±2.6

B898 22,2±6.67

SL 18.3 ± 1.9 (10.45± 2.68 *)

55% 45,8 ±3,5 25 %

SLO 20.4±2.0 (28,00±2,15*)

80 % 52.3± 6 75%

DLO 12.2 ± 0.9 85% 29.4± 7.6

70%

test efficiency % (number of samples broken inside the joint /

total number of prepared samples, %)

( *) = misplaced notches for DN, misaligned fixtures for SL, fixture-sample friction for SLO

C/C

Multiplicative factor

Ceramics

TC 19.7± 5.4 x 2.5 ~ 53,7±9.4

SL 18.3 ± 1.9 x 2.5 ~ 45,8 ±3,5

SLO

20.4±2.0 x 2.6 ~

52.3± 6

DLO

12.2 ± 0.9

x 2.4 ~ 29.4± 7.6

Page 7: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

ASTM F734-95(2006) and

F1362-97(2003)

Torsion Test

Test rig for the torsion test

Page 8: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M. Ferraris torsion tests for joined CMC and ceramics:

Page 9: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

Torsion Tests on epoxy joined SiC tubes

Page 10: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

Torsion Tests on epoxy joined SiC hour glasses

Page 11: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

Page 12: M.Ferraris-35th ICACC Daytona Beach , FL · 2018-01-28 · M.Ferraris-35th ICACC Daytona Beach , FL X . Z . Y . Comparison of shear strength tests . A4PB . Asymmetrical four-point

M.Ferraris-35th ICACC Daytona Beach , FL

X

Z Y

Concluding remarks:

A4PB Asymmetrical four-point bending test (ASTM C1469)

TC Torsion cylinder

TT Torsion Tube

TS Torsion square

THG Torsion hour-glass

DN Double notched ASTM

C1292-00 & C1425-99

SLO Single lap off set

DLO Double-lap offset

SL Single lap offset

BT Brazilian test

4 3

18

10

10 φ 10

10

φo 10

φi 8 10

5

25

12 5

10

3

5

10

10 6

10

5

6

15

15

4 4

30

ASTM B 898

φ 15

3