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MARINESHALE

PROCESSORSINc 1tALE

SERVICE

t504 3-47-1742

PLANT LOCATION

MORGAN CITY LA

504 631-3626

Ei TDAFER

DELIVERY TICKET

NOP1O4O9

--

-- --

--I

--

-S

NA ES 5$ ii HOC

Pp/j. CUSTOMER TRANSPORT jQg L113.4ATRUCKNO IRUCKNO

tin jj BARGENO FREIGHT

...-\l$.2.U iI1i.JYtJ2ttJ2_ fl_L D1 PREPAID COLLECT

5T MV NAVE

-- ACCT.COOE

ISTATEMANIFEST NO JppL

CUSTOI1ER P.0 NO WORN ORDER NO LOCATION

ESTIMATE NO OCSG NO RIG NAME WELL NO

APE NO LEASEISLOCK NO OTHER INFO

TAX EXEMPT NO DATE SHIPPED ORDERED BY

--S

SERVICE.- -- .-.. -- --

OIL BASE MUD FOR PROCESSING BBLS OBM

WATER BASE MUD FOR PROCESSING BBLS WBM

WASH WATER FOR PROCESSING BBLS WW

CLEANING SERVICE HOURS CS

BARGERENTALBARGENOS DAYS BGRE

CRANE RENTAL HOU CAREç4 3J1/B cS

21 iWbCULUL

-4

ri

Cl

D.0-

--

------S

ICNO ORNER DATE DAT

VPR SENTATIVE DATE PR EDBY

SLIDELL COPY

ADMiNISTRATIVE OFFICES P0 ROE 1E43.SL1DEILLA 704595041531-7817

GBE 44564

CONFIDENTIAL

COC

CD

cn

CDtD p2f_p

..- STATE OLI.ISIANADEPA7wp4y OF OVIRONNENTAL QUALITY

ZARDOUS WASTE DIVISION

lOX 44055

IATON ROUGE lOUISIANA 70S04 4046

Planna pt-in or rype Fm .siorild Or use On Slits 2-nttchl ryp.wnt.r FoimApptoved OM8No 20000404 .piet -31-8P

State Manifest Document Number

UNIFORM HAZAR DOUS .Gene.tc US EP ID No Manifest Page Information in the shaded areas

WASTE MANIFEST Ih ID .O .f-f at ofiS not required by Federal

.2 ueneretor erso lungAOOt as

TkPo 7H- -i Meie ifr 4i. $Y5 State Ganerators ID

Generatora Phone U2.I6 1- 2..//

urunsporier t.omçianymama US PAIU Number t.oia irsnsponer.iuEA RA 114L.Ao .7 .7 ./

.-L0.Transponers Phone

Transporter CotTipany Name iS EPA ID kumb.rState Transportes ID

F.TransportesPhonejç...453-

Dpsiated Facility Name and Site Addr.u tIS EPA ID N- tat FaciliW.ID -4

tw651Lt fc9tnc5 Cf/17- i... liiira Plnn

4Ne-r11L4 1ATht9S4Oel2.Containers 13 14

11 US DOT Description Including Piop.r Shipping Nim. Hazard Class nd 10 NumberTotal Unit

No T_YP Quantity MAc

%cl//AY/0 W4crE

-S

Additional Oasctiption for Mitensis Listed //47gg/g lr1dIIfl9 Codes for Wastes Listed/boss

Ar

.-p.- .s..i1 t4 .e._

Sp.ciaI Handling Inmructions and Mditton.l Information ..

flturpalpp.e

I.

lb -rnjr hereby dsc1ar LPIj the contents of this conslgmnt are fully ad aCcuratelY described

abOve by proper shipping nets and are clsslfiid pacted marked and labeled and are in all respeetsin pro6er condition for

transport by highway according to applicable international national arid state governmental regulattGn5

Date

Month Day YearPrinted/Typed Name Signature

$fl M11 M1 17

Cl

P4J

Ii Transporter Acknowledgement of Receipt of Mat.rials Date

18 Transporter Acknowledgement or Receipt 04 MaterialS

Printed/Typed Name1Signetur

Month Day

--

Month Day YearPrinted/Typed Name Signe4ye

Irn JNE IRiE Psso w-w iciois

Year

Date

4-------

19 Discrepancy Indication Space

GBE 44565

CONFIDENTIAL

20 Facility Owner or Operator Certification of receipt of hzrdous materials covered by this manifest except as noted in

Item 19Oat

Printed/Typed Harris Sig ure Month Day Year

7fl1LiNi S4IE P/ issosEPA Form 8700-22 3-84 O.iit-it-DtO Grm Ctnritors 2u4 itloa-DIipotar Plui-Trinspter GrId-Generator lit

DEQ FORM IW-3 9/84

-3 1.6 0100 f-iSP ST ROSE LA 044.65330w---

STATt O..J.QIIIAKA

ftPAflTNT OF VlflOKNINTAL QUALITY

W- WIAOOUS WAITI DIVIIION

$01 44664

IATON bUG tOIJISIANA 76114 4066

0J _____________

coim A44CVI4 07.1 No 2000-040- bp..4 13$

2P.9 Infoimilion in tl6 h.d.d irsi1

not r.quirad by

-f--It.w

Gin.qbtOi$ end Fd4ihfl9AOI

3tjtJj i.iBit1

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10 tIS EPIU l4 -n

Ntl1wj3ij3Lt zoc6$44 qo 51 t45P74OO4

US DOT Cf lptOflfr-cIUdfl9 POPi ShiPPL9 Hem. K.zwd CI.SL aMID Nwnb Total

last

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by Iy aordfl9 to opp1 Icible ittritbOflll rational stll 9ov6rnAIilreguat

Pun .dff6d NqmSnaft

Mflfh Oai Vial

ic __________II

jinI0flSModQ4m6nt of R1pi 07 Mitsiliti

Prinlbd/lYpGd Uen$tur

Monih Day

_/_

GBE 44566

CONFIDENTI

GBE 44567

CONFI DENTIAL

cD

-1

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MARINE

SLIDELL COPY

.DMllSTfl.1fVE OFCf fl DO SLIIt L.A S3i-781

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1LrcopxEfl Tr7NsMITpL SHRED

OTDCLIy TO

Efe PHONE

PHONE________________

DCPtRTMENTjccounjfla__ NUMBER

O5GES

TTMTWe are cendjncj from the following Sanyo 515 Auto reCOiVU Machine

St Rose 504 465-3370

pocihlc plcac check iriinmissjori after the ltist page If younoi receiving clearly or if you have any problems with transmisiooe cal uz immediately at the following numberGBE 44568

_________ St Rose LA 504 4653360 ACcounting CONFIDENTIAL

St Rose LA 504 4653316 Data Processing

Opere tor

MAflIHE SHALE floCESSOfl iNC COIiPOnATE IIADQUAnTnsTLEPHONf $04 46S.3300flruvi wri SUIIC IO SAINT flfSr IA 700fl7 %ItMHI 01 NOW Ilfl TEr.n .lr.r..-i

/1

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55

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CO

Marine Shale Processors Inci-.

INTEROFFICE MEMO

TO George Eldredge SUBJECT Baldwin Pole PilingKOOl

iI

FROM Pbunt DATE May 24 1988

555

Please review the attached data and ccciioent realize the Material

aaraothrizatlon Data eet needs rrectlng but wented to get your centsbefore we contacted the generator As understand our guidelines for KOOl

waste streams we need the following dataz

If CCA is used in the process th we need EP lOX metals

According to the attached COS Waste tharacterizatton Data Sheet

only creosote aid PCP are used This is not stated on our data

sheet

If the sltdge cans fran pit or pond we need the GC/B analyses

Acid extractables base neutrals volatiles aid scan

Since the sludge canes fran DAF unit are the attached organics

sufficient uuitbi

we need any other certifications fran the generator

cc 8rian Recatto

GBE 44569

CONFIDENTIAL

METALS EPToxIcfty Test mg/I

Moriic Ass 5tke AgBarium Ba Copper Cu _____________

Cdmum Cd _________ Ni

chromium ci Zinc Zn _____________

Ld Pb ___________

Mercury Hg ___________ ______________

Setenhim Se ______ ________

INORCANICS mgIl or ppm

TotI CN __________ ti4ne ____________

Free CU Athesoe ___________

SiilMe ___________

Chloride

$iulfite

Sulite ______ ______ ________Si.lfate __Phosphate

Fluoit ___________ ____________ ______________

Bromine __________ _____________

Chlorine _____ _____ _______

ORGANICS Cm or ppfn

/A Orginohalide

_________Tonphne

ii

24-0

24.T.O5PPM_______ _________H/A ________ __________

Oioain LPPB See_Attachment Al

TOC ____ ____ _____

Vnlune Storage20 tOns IN _______________

iMlu IUM iaeg

1% WasiC DOT Hazrdnun ES NO

Poper DOT Shipping Hazardous vaste_i-fazrd Cac ORMEi No NA 9189

Tnrtaion qupmert Vacuum truck

II.JLardng

PHYSICAL DSRIPTIONPhyui.I Ste lxi Liquid Semi-solid Solid

P1i.ring lxi Uni-tiycr OllayCt Mvitilayet

Vcnirr XI High Medium tow

Içoldc Cranic Inorganic lxi Mixed

tiq.sI oids wi 65S13spetidcd

Solids wt .1

ltTIJ/th _____ M1 Comtent_ Wtev thy weight 35rLhIointtc

71500Type --

/p.ciric Crzvjt1r

Boiling Point Freezing PoiriI eoProisur mm Hg 24C ___________________________

II Avg Range

Total Alkilinity/Acidity SI _____________________________________

j0 Oily

ntor Gray

HAZARDOUS PROPERTiES NONE

W3IN Raacth Reactivo bpocKe

Shnck Sonsitlyc Pyrophork Polymerizabletip X1 Pcrsticlr Kcsidul ignitable

CurroSvP Toxic Vapor P.ithugcn

RiMopctl Etiological

lOther --

MARINE SI-tALL PR-.XFSSQRS INC

MATERIAI3 CHARACtkIZATION DATA SHEETMCDS Document iox 1697r

Caettoq NameBald

1988 SALES MSP CODE ___________

______ Pole Pilin Co.1 Inc lIII Baldwin Pole Piling Co Inc

FciIiiyAddress Hwy.._31 P.0._Drawer 758 .IliIr.sP.O Drawer 758

TeshnkalCnnlact Torn Hil4lllan TephonuS 205 9372141OIY 5r.t. 71p La ete_A11_.365Q7_._ c. Bay Hinette AL 36507

Title Q.inp.inyCoritcl Tom HeHillan

TeephoneNO.l 205 9372141 XT CorInierSize Bulk 4000 gallons Approx

FACility PA io ALflO 314901s501 EPA Waite No K001_Generating Proceitt Wood Preservation Sic 241

CHEMICAL COMPOSITION No Trade Name Common Named WSIC asewater treatment sludge

TotalsmuitaddupO 110% RteofC.enenflon 60 tons PsyeariQn dJ4S It In

See Attachisenth

-I

CDO .0

ca

-o-b CD-

CD

cDCD

I-

11

iiouiiOS

N/A

II

II

H/AIs

N/A

Cl

ATi.8 tQu 5040 tii hut

REQUIRED PERSONNEL PROTECTIVE

________ __________ EQUIPMENT AND PROCEDURES Neoprene gloves

________ _________ Boots Eye protection

_________ ___________ PLEASE ATTACH ALL MATERIAL SAFETY DATA SHEETS LOGISTIC

SKETCHES ANALYSIS IEPOBTSS HANDLING PRECAUTIONS ADDTIONM HAZAKO SUPPORT INFORMATION DATA COMMENTS

6TCC9tt0 daqaL CDQeJS.9SL-J 0000 I$CI 88 V.3

CLITIFICATION hereby cerIiy tht the aboe and ttachid descripion complete and accurate to the best of my knowledge and ability to

determine that no deliberate or willful omiston of composlilon or voperliex taints and that all known or suspected hazards hae been disclosed

certify that materials teiid are repeseniaihe of all he maknaiS nubjtei to the contract

May 23 1988 CNFRATORSSICNATURIr_

GBE 44570CONFIDENTIAL

-i1

gR.JlbVIc

vIIkcNI.1IuI\I

IM

ATTACHMENT

BALDWIN POLE AND PILING COMPANY INC

BAY IIINETTE ALABAMA

1001 WASTE COMPOSITION

representative snpie of the 1O0 wst been an1yzed for

the compounds shown .s b.si f..r itng of thim waste ouhdIn EPA 40 CF z-t 261 Aoend vopy of tj na1ysi is

qnolosd -ypi.o O5t1on ot this 1001 is ts 1oflows

cco-i

ca

-0

r1

Pheno

2-Chicroohenc1

24 Dim9thyiphenol

p-choro-n-crso.I

Trich oroheno1

Tetr.h loreohqnol

Pentehiorooheno1

Prnitrophno1

Nphths1enAcenthsj.inAcenttththne

Phenan

Anthrsaenw

Csrbzoje

Fluortrnthene

Benzo pvrneChrygne

.05 ppm

2.08 ppm

.05 P91

64 ppm

.05 ppm

30 ppm

1526 ppm

231 ppM

2212 Pr.05 pp.05

277 pp659 ppm

.05 ppm

1799 p9t

.05 ppm

305

7211.35 ppm or

Cl

-0

Water

Petroleum 0isWood Zuqrm tnd Other Extrctjvee

Tot.51

3550c

14k

dOL aISdSIJ 0000 tOI 88. .IJ

GBE 44571

coNF1DTIMJ

cD

Co

cD

rt

.-CDCD

gj

-1/

ATTACHMENT PAGE

BALDWIN POLE PILING CONPANY INC

K002 WA5TE COflPOITION

Thie waste contains pentach1orc.hono1 and therefore. coulci

contain the dioxin cont inan.s of pentachiorophenol in trace

quantities This is not restricted dioxin waste The

fo1lowini sunrory of tyic content of pentachiorophenol

and the toxicity equiiaiency tors wiLt show that sxected

content of all isOrs of the thcxrs is til1 below pert per

billion

IN IN TEQHNZCAL PENTACHLQRppJ4ENOL

COMPOUND TYPICAL TOXICITY EQUIVALENT

ANALYI5 EQUIVALENCY TOXICITY

FACTOR

Tetravhlorodibenodioine

Tetrachlorodihenzofurans

Perthlorodibenoxins

Pontachiored ib.nzournc

Hexachlorodihenzc.don

Hexachlorodthenzofuronu oi

Heptschlorodibenzodiocina 75 ppm

I-

I-

Heptach lorodi benzofuran ppI .001

.2 tipb

Sppb.04 60 pph

.01 ppb

.001.0000l 75 ppb

using .001

DbTotal 255 ppb

the expectedAt 1500 ppm pentachloropheno concentration

eauivalent dioxin content would be

CO

0-

GBE 44572

CONFI DENTIAL

dqeJ. o9 eeoo 88 ..cw

GBE 44573

daq.J. so ScjSIz ztcT 88. LJill

TLPi-AC.LLIiAH G3

.ijtiiI..

Gviicor

Oer Ir iruTh r.ui -i eivd 222-S2icw1n ir-- II .jtjonz9 t..-.--.--.

jr b1 tt lrh9

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Z4 46

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-isl-lrf TFTMENT3LUCCE

rn

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CO

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GBE 44574

CONFIDENTIAL

6IEt--t0 dcjq.j 0000 CtZCI 88 I-1

OWNERS CERTIFICATION

OF DIOXIN CONTENT

CDCO

rP

Bed uron tte xected dion coJtputtion6 Iound in

Attchrent ccompetnyinq the we hrcterizotjon date

rtfy th th w.te no xoected to contain iore then

ppb of tetradiocin equiv1ont.

Z1- ii4L _____ _____Thom Mi11n Preaidrit DatB1dwin Po Pilin9 Conpdny Inc

Cl

GBE 44575

CONFIDENTIAL

-j

I-

VOUuC1 Coot

ssço NVMOR

CD

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cI\uA rtrii.vrunz flATA

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___flROWNINO.FERRIS INDUSTRIES

I.tPOIlTANT PLCASE RrAf I5TIwCTIONsflroR COMrUTING TillS fORM

GENERAL INFORMATION

Ceneraio Baldwin Pole ond Piling Ccnertor t4o ALDO3140SOjcompany Inc

$tte Regslolion t4o--

Generating Facility Compltc Jd tailinR Address Drawer 738 Bay Minetto AL 36507Address 1.307 Atr Highwyoy Hthettei.L

di AIhorized Conipany resenIaLi Thomns ...MeMillan ThIe ircside_.._____________Phone Nurnb ..A05937-2l41 Atr Uours Phone Number 71 33Emergency Cont Mcjfllan Thl. rciid.en.L..__ rhone....2ai372l41_General Desclpion of The tAstc Mastewter trcatnöst_sludçe from wood preiarving prses

Jng creosQ.t.Jtnd/or pentaehlorophno1.hi Process Cerserating Wood preservation sIC Zk91WASTE PROPERTIES 25

Pi-rysital State Solid Po%kr Uctukl xJ Semi.solid sludge or

MiturcQcscriViscosity 310w Medium HIgh

PhaseVLsyers x3 S111 Hhl.ynrI Midtit.vred

Percenig lun ttli tnycr 1of ________ Middle _________1 ____________ Oottom

Oensiry_ 8.0lxi thtigal Lbs.4tJ.3 gicc Other_

dl Odor JNcrrre tJMild or Srong iou._coa1 Tarlrurpentineci Vapor Pressure in mm ol Hf Not tested Kaio_tbe Low Colors. 4fly Bron_gi pi-i....... Approx th Solubility ii0O ________________________________

FlHP Point 150 Eqr Qpcn Cup xl Closed Cup

REACTIVITY

Hbdrophorc \t kd No Auiopotymorizable Yes bo No Shock Sensiti Yes lou NoAcid Reacit 11 No Alkalinc Re.ictivv Yes 101 to Pyrophorie NoEkpIO$ht bs kd No Thermally Scnsitivr bs No

THIS WASTE CONTAINS

Npt dioxin wasteBiological Matedals Yes CV NO Pathogcis Yes PU$ No Pesticides

dological Agents Yes 3cj NO Dioxtng Ycg 1tS Oils

Fret Cyanide sls lc No Free Sulfide fX$ No Fr AmmoniaRadioactive Materials No liquids Yes No Absorbents

OSHA Substances cI Yes No PCOs circle one fl

if vs speciFy type fit pplichh aut cOnCcnltion in th ste composition Secdon

COMPLETE WASTE COMPOSITION

ORGANIC ________See Attachment

I$Dol Yet

rosIns

pcaq No

JNo

k3 No

No

INORGANIC

ft this waste Hazardous Vaste as dclncd by regulations or tho U.S rwironmentiI Proecdon Agency pursunl to 40 CFR 261 or the RetoureCozsseryaiion and Recovery Act_Xea

--It ths 1lrduut tIr us tt1iitI Silo ti 1nc.I ReguItun_ YPS

Is tample included lxi bs Nr

Anlicipatcd b7urnc _____6p Gallons Tn5 Cubic YircJ Other _______Per Day %.bck Month x3 Yeç or Other __________________________________________

be Iransporied in fxJ fltifl CtCO.f\K Drums l1x/siu

8d

GBE 44576

CONFIDENTIAL

6EC9tt0 daq.J. SSdSI.J 0000 CtCT 89.

1/

cDCD

-1CD1

3-4k

CD

CDCD

J/2

St ose Louisiana P1X No 504 4653319

TLEcXPIER TRP1NSMIP1L SHEEr

-j- FkfME

ENVIRONMENTALLY SAFE

TO ____ _______

MBER OF inc1ud1rg this transmittal shtLetter

Legal

Cl

-D

If pssible please check transmission after the last page If you are nOtreceiving clearly or if you have any prthlns with transnission plEasecall us isrnedlately at the following ntzrber

___________ St ibse Louisiana 504 4653302

/43TItE sNr

Jack tint

TEYNICAL N7F

MARIHE SHALE PROCESSORS INC CORPORATE HLDOUARTCR$

110 JAMES DRIVE WEST SUITE 120 SAINT ROSE LA 70087 Suburb of New Oiears

6WYttU dCJLIJJ. UU dtII Ud.

GBE 44577

CONFIDENTIAL

cJ

INTEROFFICE MEMO

Marine Shale Processors Inc

George Eldreige Baldwin Pole Piling

KOOl

Jak Mount May 24 1988

TO

FROM

SUBJECT

DATE

CDco

Co3b

CD

CDCD.-p

CI

Cl

Please review the attached data and catroent realize the Material

Characterization Data Sheet needs correcting but wanted to get your ctinents

before we contactel the generator understaM our guidelinee for KOOl

waste streams we need the followirq data

If CC. is used in the process then we need EP lOX metals

According to the attached C006 Waste Characterization Data Sheet

only creosote aid rc are used This is not stated on our data

sheet

If the sl3ge ccms from pit or pond we need the X/B analyses

Acid extractables base neutrals volatiles and PC scan

Since the sluige canes fran DAP unit are the attached organics

euff to tent

we neal any Other certifications from the generator

cc 8rlan RecattO

Thankat

GBE 44578

SQ6MARINE SHAUROqESSORS INC

MATERA1S CHARACIIZATION DATA SHEETMCDSDocumen pç nox u51r KF

1988 SMESO4t MSP CODE ___________

Baldwin Pole _PiljCo.h Inc ii Baldwin Pole Piling Co Inc

FacslityAddres Hwy.iI P.0._Drawer 758 _________________________________City S1 7p

technical Contact Tom MHU1an ____________________________________PreehtnP ______________________________

______ ____________ EXT _______ _________________________________________

Title

TepPporreNO.I 205 _9372141FiC.l.ty PA ID AL0 3490I

2__.cD -i

CD

-eCDCDCl CO

CD

\V

-1

-I

1-

-p

CHEMICAL COMPOSITION Na Trade Nero

Totilt mutt add up to IOC%

Aklrp..s P.O Drawer 758

iy..I.iti 7r Bay Hinette AL 36507

TOtIIOOUI 205 9372141

Crtnpnv Contact Ton MeMillan

ConlanerSize Bulk 4000 a1long ApproxPA Wapte No 1001

Censtating Prtt Mond Preservat ion_S ic249lCompon ame of watte atewater treatment sludge

Rate of C.eneruttnn 60 _tQfl PER yearKlp...nt itj..4.i iT... ii.v

see Attachtoent

N/A

Ii

-S

I.

METALS EP Toxkity Test mg/I

Asonc As 9k Silver AgBarium Ba Copoer Cu ______________

Cadmium Cd NrdeI _____________

Chromium fcr Zinc IZo ______________

Lead Pb __________ __________ _____________

Mercury HISelenium Se _____ _______INORCANICS mg/i or ppm

ToiICN _______ rnn _________Free CN ________ Athsto __________Sulfide

OsoqideII

Bisulfite______________ ____________________

Sulfite ___________ ___________ ______________

Sulfate __PStosphte _______ ________Fluorine ___________ ___________ ______________

Bromine __________ __________ _____________

Chlorine ______ ______ _______

ORCANICS or ppmEndrin /A N/A

M.thoxychtOr Meicaptans

Thaiphen

24.0

24.T.O5PPH_______ _________

PCBs NLk_ ________Dioxin IPPB See Attachment_kl

TOC ____ ____ _____

Volume in Storage..20 tOflS IN ________________

iQ.U itMal ptpp...n Si. .i4 f.cti

t.WacteOOTHazarps iXitS NOProper DOT Shipping Name Hazardous vast e_liQutd NOS

I4azard Class ORMEIQN0 NA 9189

trantporlation Equipment Vacuum truck

Plotarding

PHYSICAL DkCRIPTIONPhycirit St.re IX liquid Semi-toM Solid

PheayNirn IX Uni-Liycr Orlayer Muttilayer

Vitcoiry IXI 1-righ Medium Low

ly1ii.iifSol.rh Organic Inorganic XI Mixed

1.lSoIdsti65Z_SspendedSolidrwt

Hflilh _______ Ash Content Wr by weight 35Z

d1tt1PninI 7150Type

Crav.ty1.1

tint Iirrg Point Cl Freezing Point

Vapor ProCure mm Hg 24C _________________________

T1 Avg .5 Range in

Total AtkIlinitylAcidity

Odor

Gray

HAZARDOUS PROPERTIES NONWtlar Reactivt Reactive Explosive

Shod Scncitiv Pymphorit ISifymerizable

R.trlrutc-thp 1X1 Pesticide kesiduals IMtibe

C.srrotiv Toxic Vapor P.tihugen

Rioiogic.t Etiotogicat

Other

REQUIRED PERSONNEL PROTECTIVE

EQUIPMENT AND PROCEDURES Neoprene .gloves

Boots Eye protection

N/A

Cl

s_V..

_________ ___________ PLEASE ATTACH ALL MATERIAL SAFETY DATA SHEETS LOGISTIC

SKETCHES ANALYSIS REPORTS HANDUNG PRECMJTIONS ADDITIONAL HAZARD SUPPORT INFORMATION DATA COMMENTS

CERTIFICATION hereby certify thilt the above and attached descrirriion LompTec and accurate to the be-ct of my knowledge and ability to

detemrire that no deliberate or willful omhton of composition or prnpPilx exists and that all known or suspected hazards have b. disclosed

rtify that the marriaIs teited are reprawntath-r of all th makrijlt subvçt to the contract

PATI May 23 1988___ GENERATORS SIGNATUREr

IOtsaC4.ittsrFtt4h GBE 44579

CONFIDENTIAL

Water

P9troleuM OiWOQd uqar and Other Extractjve

Total

14k

OO

GBE 44580CONFIDENTIAL

ATTACHMENT

SALDWIN POLE AND PILING COIIPANY INC

SAY NINETTE ALABAHA

KOOl WASTE C0NPOfITX0N

-I

cD

Cb

rP

representat.iv9 sample of the KOQI waste has been analyzed for

the cotoonds shown as basis for iistina of this waste as found

in EPA 40 CF Part Aooend copy of this analysis is

enclosed T- Si10fl c.t this KOOl is as foJjows

Phenr..

2-Chlr.rohQnol

24 Dimethyiphenol

p-choro-rt-crQsol

orooh enol

TetrahloreQhenoi

Pent-ach iorohenol

Paranitrophenol

Naphthalene

Ac en .h

Acenh-hnePhenantr.n

Anthracen

Cerbzo.te

Fluorenthen

Benzo is pvrene

Ch ry en

WI

.05

.05

64

.05

30

52231

2212

.05

.05

277

659

.05

799

.05

_3057.211 .35

ppm

DOn

ppm

ppm

ppm

00Th

Ow

ppm

ppm

Ppm

P1i

ppm

ppm

ppm

Ppm

PPM

ppm or

Cl

CCOC.b.CcCo1

ATTACHMENT PAGE-7

BALDWIN POLE PILING COMPANY INC D-KOOl WA5TE COMPOSITION

LOrlI.E3I

CD

Thie waste contains pentechlovo9honol and therefore could

contain the dioxin cont inans pentachiorophenol in trace

quantities This is not restricted dioxin waste The

fo1iowinc suio1y of tyica1 ...-ri ccnt-ent of pentechlorophenol

and the toxicity eauiveiency itor Wi1 show that eeected

content oI all isoners ox the d3cxrs is still below pert per

billion

IP-tIECHNICAL PENTACHLOROPfENOL

COMPOUND TYPICAL TOXICITY EQUIVALENT

AMLYI5 EQUIVALENCY TOXICITY

FACTOR

Tetrachlorc.dxbenzodjoxjrie U.fl

Ttrachlorodihenzofuraris N.D --

Pentachlorodienzc.toxins .2 .O ppb

Pentach1erodiI.enofurnc opb

Hexachorothhenzc.th.oxxns .04 60 phHexachlorodibenzofurene ppi .01 30 pbHeptachlerodibenzodloxins 75 ppm .OO1-.00001 75 ppb

using .001

H.ptachlorodibenzofuren .003 75 oob

Total 255 ppb

At 1500 ppm pentachloropheno concntretion the expected

equivalent dioxin content would he _______

GBE 44581CONFIDENTIAL

aTcCcte dqCDJ aSdSL-J 0000 3ZT 88

I-

ear lr

Tl jI ri rivd 222iw1r -- I. æI rptioni9 i...--

If bf fltct 1rh 1i.tn4rIjs

XLLI4rQ

cD

rt

0_

i-i ti .ii1Si

fz

TLPr4r-ASCA31iiAC1

33

eni

-.0

GBE 44582

CONFIDENTIAL

II

CDCD

co CD

Co

ct CO

GDCD

TQ I-i t-I

FRc1 .r

Phno12-Ch1ororri

Trh1.tc1c

ran trren

49n aDhtr1n9

Phenan threethracc.n

1ovn trr3enzo fiu%hrue

46

rT

-i

4-r-io

I\VI

IN3 cMFANif .--i--- LA4LZ

.iii.ijp TATMENT

Ac-

rn

05

12.0505

05

GBE 44583

CONFIDENTI

CD

.0

-I

HI

qu

1/

OWNERS CERTIFICATION

OF DIOXIN CONTENT

ed upon te ctioxji-i CQpiputtjon found in

Attchent ocomnyinq th ohrcteriztjon detcertty tht thiG w.t8te not xpectd to contain more than

ppb of tetrAdioxin equivalent-

7Z- 174i44kLThoo8 cMillan resldrt Date

Baldwin Po1 Pilini Copcny Inc

rT

lj

II

GBE 44584CON Fl DENTIAL

Is thu waste Hardotj Vastc as dcncd by tegutations of the U.S Environmental ProlecIion Agency puisuant to CFR 261 of the ResourceCowvation and Rccovry A_.Xe8

lhi 1Iwduus Wils tlc1iuI Ip SLtle l.nal ReguTtkm_._.. YsIt indudedf lxi \.i

AntiCipated \blurne Gallons lx Tent Cubic Mrds Other _____________________________Pet Day %clc Month xJ Year or Other __________

be Irnsponed in xl fliD CCO.fYK Drums Iypc/siz

v%c ft Cl lAuAC 1Cl/ATOtt nATA

Ii.i

BROWNING.FERRIS INDUSTRIESbIIwAiCOrI

IMPOItTANr RrAn_INSTISUCTIONS nro1 COMPLETING TIHS fORM

IRODuCI Coot

SO NUMOR

kLVILWU UY

--

CDO

-o

cD

CD

r$

cI

Liquid

VSC0Si1y Low

Midiilavred

Semf.solid sludge or

Medium

GENERAL INFORMATION

Ceneratos Name B1dwin Pole and Piling Cenrotor No ALD03140501Company Inc

State Registration NoCeneratins Fa.iUiy Compteto Address Draver 758 8ayL_5p7

g_Address 1307 Atmpr IihtaJ3py Minetta...J.L

dI Authorized Company Repr cniatie 6JcMi11an Tltle ....1rcsidett.._..._Phoae Number 1059372141 Aner Hours Phone Number 2f.IS7 7133Emergency Con i_I 3QIS jcllillan TIIIC PrcIid.en.t...._L_ Phon.2Q5372141__ConoraI DescrIption of The W.aste Wastewater treatnsonL.s1ude from wood prarvfng prorcsejjng creoorjs.ndJpr pentachiorophenol

hI ProIts Cenerating ase Wood presvptfpn SIC 2_49fl

WASTE PROPERTIES QD 25C

Physkal State Sold

MiXtUrCDeSCIbC

Phases/Lpyrs Srq 8hIaraI

Percentage lurn C.cIi 1aer lop Middle flonom

Oentiry_ 8.0 Ix LhsJgtI Lbs./ytf.3 gicc Other_

dl Oen None lJ Mild or Srong Describe Coal Tar/Turpentinepor Pressure in mm of Hg Not tested om_to.be low Coor. lyBrosçs_pH__ Approx Solubilay J10OFIh Point 150 Egt

Ixj.F Ix Ctosed Cup

REACTIVITY

Hdrophoric \ts kid No Aucopolymerizabk ts No Shodc Sensitive Yes Kxl NoAcid Reacth 3i4 No AlkaIin Reactive Yes oI No Pyrophoric Yes c4 Noptotht No Thermally Sentitkv No

THIS S.STE CONTAINS

Npt dioxin wasteBolo5cl Materials Yes No Pathogens YCS JO No/ Pstiidcs

Etiologicat Agcnii Yes k4 No Dioxins YCS Oils

Free Cinde \bs No Free Sulfide Yes No FrCO AmmoniaRadioactive Materials Yes No trce Liquids bYes No Absorbents

OSHA Sibstances Yes No PCO5 circle one It

If vs specify type lit applicabli and concentration in tIre w.wc composition Section

COMPLETE WASTE COMPOSITION

ORGANIC INORCANI

Ix High

iO Cup

See Attachment

Yes

Do Yes

JYCsYes

poq No

JNo

No

NoCl

--

--

GBE 44585CONFIDENTIAL

6TC69Vt0Q da9Di O954 0000 tZT 88

A4

__._ENVIRONMENTALLY SAFE

CD

-o3-bCD

CD

CD

0.

r$

CD

St Rose Louisiana FAX No 504 46533

TE TRNSMIP11L SIEEr

5-2q-

ALbw PLINEI

TO ________________RARDrNG

N11BER OF FNES including this transmittal s1eet

______ legal

If ixssible please check transmission after the last page If you are not

receiving clearly or if you have any problns with transnission pleasecall us iirrtediately at the follciing nurer

St Jse Louisiana 504 4653302

/43B

cn

.0

TINE SENF

Jack Mxint

TEQiNICAL ANACF.R

MARINE SHALE PROCESSORS INC CORPORATE HEADQUARTERS

110 JAMES OFWE WEST SUiTE 120 SAINT ROSE LA 70087 Suburb of New Orleans

thj JlJJ IjwjLj utt

GBE 44586

CONFIDENTIAL

cc Brian Recatto

TO

FROM

Marine Shale Processors Inc

INTEROFFICE MEMO

George Eldredqe SUBJECT I3aldwin Pole PiIinKOOl

Jk Mount DATE MaY 24 1988

CD

rt

_cDcLCo

CD

CD

rf

CI

_1

--

Li OX

rq

Please review the attached data and cTInent realize the Material

Characterization Data Sheet needs oorrectir but wanted to get your cornients

betore we contacted the generator As understand our guidelines for KOOl

waste atreants we need the following data

If CCA is used in the process then we need EP lOX metals

According to the attached CDCS Waste iaracterization Data Sheet

only creosote and are used This is not stated on our data

sheet

If the sludge comes from pit or pond we need the CX/tE analyses

Acid extraclables base neutrals volat iles and scan

Since the sludge comes fran DF urit are the attached organ ics

cuff icient

Do we neal any other certifications from the generator

Cl

-L

Thanksl

GBE 44587

CONFIDENTIAL

MCOS Document

C.mroq Nrne .-.- ____--

F.icityAddres Hwy jI P.O._D4Wer 758

Cty c.vp

TePinicl Cnslact Torn MMtl.lan

Ttle Pr.c1dsWJ --

Teepsorr p.O 205 .93Z2141 XT _______

Facdly EPA ID ALDO 3l49OO1

CHFLMICAL COMPOSITION NnTrade Nami

Tolalt muSt add up to IflO

METALS EP Toxkity Test mg/I

Arsec As MABarium 8a ___________

C3dmium CdI

Clvornum ccitI

MrcwyHg4

SelenwmSej

INORCANICS mg/i or

To1aICN N/

FreeCH _______Sulfide

--

Coode

8iwIte

SuIfte ___________

Sulfate ______________

PNosphte

Fluoine

Bromine __________

Csorrnv ________

____ .4

.4

.4

.4

.4

ORGANICS or ppmErsdn WA

Organohaltde

thoeychlor Mercaptans ____________

Tosaphene

2.4-0 _______ _______ ________2.4.-T

P1tnocs ___ 051 PH ___________N/A _______ _________1PPB See Attachent_AJ

HAZARDOUS PROPERTIES

Wss.r Reacte Reacriy

Swck SnnsiUvv Pyrriphorit

q.çft5p Pesticidc Kc.stduh

CurosIv Tosic Vapor

Rntnçtt lioosit al

Other

NONE

Esplosse

Polymetizabe

liabe

.rihvgen

I/

rir 1CMARINE SHALE fROESSORS INC

MATERIALS CHARACttIZATION DATA SHEETP.O BOX I597r 11

MA 41988 SALES ________RalIwn Pi P41in2 Co. Inc Baldwin Pole Piling Co Inc

\d.lrts P.O Drawer 758

See Attachment

CDCO

CO

CO

CD 0-CD

CD.-F

CD

I.

IM

I.

.1

Lead Pb

15 Bay Hinette AL 36507--

Tcrfrore 205 9372141

Comp.isv Contact Tom MeMillan

Cone Sze- _Bulk 4000 gallons ApproxEPS Waste No K001

Ceneatg Wood Preservat ion_S Ic _2491Cormon _Wa ewate.rtratment slsi4e

Rue ofCnpratinn 60 tons PER yearMe U- tTEt ICVJ

V4IunC Storage20 tOflS

__________________am Cs- 5s .d sse

Is W.soe DOT HMardous XI YES NO

Pope DOT Shipping NarTeHazardous waste_34QuLd NOS

rdclasc ORMEIDN0 NA 9189

Trzmposlaton EQupmeetVacuum truck

PHYSICAL DSRIPTIONPhciaI SlzJe IX Ltqud Semi-solid Solid

Ps1aenng IXI Uni- Bitayer Multilaver

Xi High Cdium Low

y. .t Solids Oranc rn-nrgan XI Mscd

Iul Solids ssl .4 65Z_Suspended Solids 4.41

_______ .4 Ash CotersI .4 WaIP hit weight ISI.ashPoniF 7150_Type

6pc.rdc Cravity1.1

Itoling oint Freezing Po fr _____________

Pressure mm Kg 24O _____________________________

Avg .5 Range in

Total AIkaliltyIACsdtly 1% __________________________________________

Odor Oily

otor Gray --

Slier Ag

Copper Cu

Zinc Zn

ppm

Icpds

Asbestos

N/A

It

N/A

N/A

PCBs

ICC

REQUIRED PERSONNEL PROTECTIVE

EQUIPMENT AND PROCEDURES Neoprene gloves

Boots Eye protection

PLEASE A1TACH ALL MATERIAL SAFETY DATA SHEETS LOGISTIC

SKETCHES ANALYSIS REPORTS HANDLING PRECAUTIONS AUDITIONAI HAZARD SUPPORT INFORMATION DATA COMMENTS

CERTIFICATION heehy cey ibM tbp .boc-e .nr4 attached destrptrs is cornteC arid acctjrale tO Lh best of my knwIrefge rd ibfity to

detnmir thaI no etberaie or llfu omscors of composioc frnpert.ssnsus and that Lro.s nor stispected hazards have been dscosed

Ceitty that the maerah tested art repPSelrIatnre of all the mat.rjS ubjtI is r1e cytracl

DATT May 23 1988 CNFRATORSSIGNATURI

.sSf01tr4oH.rtiII GBE 44588CONFI DENTIAL

cIcJqDmJ mrscsci ItT -cl.i

Phen

2- Ch r. rio24 Jirnthyiheno1

-ch oro-M-cresoL

Trchc.rothenc1

Ttrs.h orohnc.i

PQflt.etCh iorochQnoi

Psrsnit rophnc

Nsphthaien

Ace net

Ace net fl

Phcnsn

Ant hretoene

Ben vro.n

Chrysene

.05

.05

Ed

.O30

232212

.05

O5

277

.01799

.05

305

7.211 .35

ppn

p911

ppm

ppM

ppm

ppM

PP

Ppm

pm

ppm or

ATTACHMENT

MLDWIN POLE AN PILING COMPANY INC

BAY IINETTE ALABAMA

KOOl WASTE C0MPOSITr0N

representttve rli5 of the NCO wtB hets been sr1yzsd orthe coNouflçs houn ets et bsis T..r istina of thig sste es found

in EPA 40 .rt \eri oy of this sns.ysi .s

enc1osd Th otT this KOOl is ets fUows

1010

10

3-4CD

CO

.i

.g -4i

-p

Cl

Water

Pqtrmsum Oi..s

Zuetrs nd Cir Extretctvos

Tots

35

50

1O0II

GBE 44589

CONFIDENTIAL

------ --

ATTACHMENT PACE

BALDWIN POLE PILING COMPANY INC

1001 WA5TE COMPOSITION

This wsto eontsins psntschoi-c.hQnol end therefore CoUld

contain the dioxin cc.ntninens of rent hiorophenol in trece

quentities This is net rest tictd dioxin weste The

fo11owini surrory oC content of pentechlorophenol

end the tc.xi.ity euiveiCncv ctr wiLt show thet expected

content of ii isonr of the ti1l below pz-t erbillion

PXIN IN TEQHNICAL PENTACHLOROPHENOL

COMPOUND TYPICAL TOXICITY EQUIVALENT

ANALYI5 EQUIVALENCY TOXICITY

FACTOR

-I

ococa

cb1

CD

r4 CD

CD CD

-CD

rf

rt

cI

IrP

-t

ii

-I

Tetrech1orc.dibenodi.oxjns

Tetrechlorodibenzofurens N.D

Pent hlorin.oirjs .2

Penteeh1orodibenzofurns

Hexehorohenzc.deyns -io .04

Hexechlorodtheofuren .01

Heptschlorodibenzothoxin8 porn .0O1-.00001

L151fl9 00t

Xeptachlorodibenzofuren ppt QO

60

75

pph

pb

the expectdAt 1500 otm penteehioropheno ccncentretion

ouive.ent dioxin content c.u1d be ______

Tote 255 ppb

EEttO doqL Oe4SSLi I3O tI /L-J

GBE 44590CONFIDENTIAL

NO

TIC

EIf

the

filmIm

age

isIe

ss

cle

ar

than

this

notic

eit

isdue

toth

e

quality

of

the

docu

ment

bein

gfilm

ed

__________

.I

._p

-1jj

I1.t

1L

.J

IZ..

.1

tIp.1

._

sii

ls

.1.1

.IIc.

1-.-

II

X.iJ

ijT

If2

1I-.I

HM

sDo

7l

13-I

IDc-n

c-n

N$P

Pro

do.d

byM

P9/9

3

___

LCC.0

ti

4-III

..-

.8

4.

Ill

_y

.4

CL

II

IL

Ct

11

Co CO

CO1

cD

I3

Phri

Tr

Nhth

Anthrcc.r

r1ucy.nrr..B9flQCbruier..

LN3 C.-1PA

TT1iE7LCc

rn

ii

.-

0..Dfit

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CI

GBE 44592CONFIDENTIAL

.t9tto daqJ SdSL-I 0000 EtEt 88 .l

Co

cD

cb T-

Ci

1M

Cl

.0

-I

OWNERS CERTIFICATION

OF DIOXIN CONTENT

od upon te xctd dion ouv.nt comouttion found

Attchnt cow.pnyinq the rcteriztjon dt sheetcertxy th.t thi w.te no -xo.ted to contain ore thn

ppb of tetz-.diocin eaujv1ent

A. ii4Thom ci11n Preidnt bate

Blctwin Po Puma Ccony Inc

dG 0000 ct

-4

GBE 44593

CONFIDENTIAL

I-i

this waste Hazardous se ts defined by tegutitkns of the U.S Erwronrnenta Procctior Agency pursuant to 40 CF 2t of the ResojceConservation and Recocry

th iirtkit tk th1nI Silc ti 1it.I ci tn _......_Ies

Is sample included xl \i.s Ni

Antcipat4 \bume 60GIIons Ix ns Cefic Yirc1s Otbr _________________________________

Per Day YearS Other

he It OrleJ in lxi fiiU CtCO-P_______________________________ GBE 44594

CONFIDENTIAL

CJ-il -t F2

DMOWNING.FERRIS INoiSIfliEs

tv\cvr \rir

v.ç .tiu

A\/ ___KtVLsVtJ Ii

DII W51 COfri.IPOUY\Nl PLCASE RIAO INSTIUCTIO-.S nuoc COMIIETING THIS rOitM

CO

9Irt

cD

GENERAl INFORMATiON

Cerierators Nnc Daidwin Pole and Piling PA CCcrtor No ALDl4O5oionspany Inc

State Restation NoCeneatrng Facl.sy Compete Athfress-_J gdress Drawer 758 flay Minett AL 36507

Street Address L3OlAtrnore

Avthozed Company Rcpr crslaIi fltotnas .4illan Titic ..Jrcsidett --Phn Numbt .2059372141 .\ft Iforjrs Phonc Nvmbc 2133fi Emergency Co cI_ThQs Jjdfliflpn Thic. rhone..2Q.1937214l__._

Ceiat Oscipion of The Waste iajer treatment s2udie forn wood preerving proe..se8jng creo-- __________________________

hi Poces Cenearing W.we ..Wood Preservation LC._2L91

WA5T PROPERTIES 25C

PhysiaI Sut SOlidlirp.iicl lxi Semi-sIid hedge or

MistuDihViscosity Low Mcdum tx1 H5h

bI Phases/ayirs x1 Silr IIil.tyrr-iI iiitvrcd

Percentage Iurr .iOI U-yvr Top -- MiIrIl _________ __________ flortom

Density 8.0 ix Lbs/gal tIid/d.3 glee OtherOot None xl Mild or Strong OCSCfibC Coal Tar/Turpentine

ci Vapor Pressure in mm of Hg Not tested 1nosjn be low Coots OJ Broi.npH__ Aporox thi Sotubitity t/i0O 5-1201 _.-FIh Point 150 Est XJ Open Cup xl Cosd Cup

REACTIVITY

Hrophoric \s kd No Arnopolymerizabk Yes bci NoAcid Rtis Yes c4 AIkalin R.ictiv No

Yes kx No ThmtIly Seniiti.r Yes No

THIS WASTE CONTAINS

Not dioxin wasteBiological Materials Yes No Pathoens Yes No. Peticidcs

Etiological Agents Yes No Dioxin fx Yos OUsFree CYanide Yes .c4 No fr Sulfide Yes fX No Fc AmmoniaRidiativ Materials Yes No Iree Liquids Fx No Absorbents

051-IA Subssjras PCOs Cirsc oneif vs specify type if

itpj calil and COnCCnIraIO in ih visc COrIlpOSIIiCIn Section

COMPLETE WASTE COMPOSITION

ORGANIC

See Attachment

tx

Shock Senilive

Pyrophodç

Yes

JYes

ex No

Yes

ix Yes

Yes

JYe

No

JNo

No

No

Cl

INORGANIC