mse$307$materials$ characterization$iimse307.cankaya.edu.tr/uploads/files/mse 307_introduction...mse...

INTRODUCTION

Assist. Prof. Dr. İlkay KALAY Materials Science and Engineering Department

Çankaya University

MSE 307 MATERIALS CHARACTERIZATION II

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INSTRUCTOR Assist. Prof. Dr. İlkay Kalay Materials Science and Engineering Department Office: N-‐B11 E-‐mail: [email protected] Office Hours: Wednesday 9:20-‐11:10* *Use e-‐mails as much as possible out of office hours TAs Ezgi Butev Office: N-‐C09 E-‐mail: [email protected] Emre Yilmaz Office: N-‐C08 E-‐mail: [email protected]

MSE 307 Materials Characterization II

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CLASS SCHEDULE Lecture: Tuesday 14:20-‐17:10

3 hours of lecture

2 hours of laboratory

4 credits


Laboratory: SecZon 1: Thursday, 09:20-‐11:10 SecZon 2: Thursday, 15:20-‐17:10 SecZon 3: Friday, 15:20-‐17:10

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COURSE GRADING

Midterm I 20 Midterm II 25 Laboratory 10 Quiz 10 Term Paper 5 Final ExaminaUon 30 TOTAL 100 % AVendance: Minimum of 70 % a`endance in class is mandatory. LECTURE NOTES PPTs, handouts and etc. Check course website (h9p://mse307.cankaya.edu.tr/) frequently!!!



!""#$ %&'()*$+&,"-".$

!" No Laboratory"

#" Production and Detection of X-rays, Continuous and Characteristics Spectra, Filtering of X-rays"

$" Elemental Analysis by EDX by X-ray Fluoresence"

%"No Laboratory Preliminary Report 1 (Elemental Analysis by EDX) must be submitted to your lab assistant by October 20."

&" Stereographic Projection"

'" Exercises on Stereographic Projection "

(" Spreadsheet analysis of X-ray diffraction (Reciprocal Lattice) You can bring your own laptops-notebooks

)" Qualitative Phase Analysis

*"Cell Size Determination Report 2 (Qualitative Phase Analysis by XRD) must be submitted to your lab assistant by before the lab session."

!+"Determination of Crystal Structure Report 3 (Cell Size Determination using XRD) must be submitted to your lab assistant by before the lab session."

!!"Exercises on Structure Factor Calculation Report 4 (Determination of Crystal Structure) must be submitted to your lab assistant by before the lab session.$

!#" Quantitative Phase Analysis"

!$" ,-./0"12345"6/7348"must be submitted to your lab assistant.

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Please noUce: For any type of plagiarism (i.e. copy and paste from your friends, internet, textbooks, research papers, encyclopaedia, etc. and/or using graphs, data, figures, etc. without ciUng the reference) you will lose half of your grade. ATTENDANCE: Class parZcipaZon will be added as bonus. (70% a`endance is highly recommended) Students will a`end only one assigned group for the lab sessions. You are not allowed to miss more than 1 lab session throughout the semester, otherwise you will get “N.A.” as your course grade. Please try to be in class on Zme….. Please put your cell phone on silence in the classroom …


“Elements of X-‐ray DiffracUon” by B.D. Cullity and Stock S.R. , Pearson EducaZon, 2003. (ISBN-‐13:9780131788183)

Text Book

Laboratory Manual and Workbook, 2008, Ç. Özgit.


“Structure of Materials: An IntroducUon to Crystallography, DiffracUon and Symmetry” by Marc de Graef and Michael McHenry, Cambridge University Press, 2007. (ISBN-‐13:9780521651516)

Reference Books


“Fundamentals of Powder DiffracUon and Structural CharacterizaUon of Materials” by V.K. Pecharsky and P.Y. Zavalij, Springer Press, 2008. (ISBN-‐13:978-‐0387095783)

Reference Books


ProperZes of X-‐rays and electron beams. Spectroscopy. Fundamentals of crystallography. DiffracZon, direcZon of diffracted beam; diffracZon under non-‐ideal condiZons, crystal structure determinaZon. IntensiZes of diffracted beam. Precise parameter measurement. Phase diagram determinaZon. Order-‐disorder transiZons. CharacterizaZon of amorphous materials. Design of material characterizaZon procedures.

Course Highlights:


mse$307$materials$ characterization$iimse307.cankaya.edu.tr/uploads/files/mse 307_introduction...mse...

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