mt lab manual 1

76
MATERIAL TESTING LABORATORY RECORD

Upload: shamjith-km

Post on 14-Jun-2015

348 views

Category:

Engineering


4 download

DESCRIPTION

GCE Kannur

TRANSCRIPT

Page 1: Mt lab manual 1

MATERIAL TESTING

LABORATORY RECORD

Department of Civil Engineering

Govt: College of Engineering

Page 2: Mt lab manual 1

Kannur – 670 563

LABORATORY RECORD

Name : Year :

Semester :

Branch :

Roll No : Univ.Reg.No :

Certified that this is the bonafide record of the work done in the Laboratories of the

Government College of Engineering , Kannur.

By

Page 3: Mt lab manual 1

----------------------------------------------------------------------------------

Place:

Date: Staff-in-Charge

CONTENTS

Ex No. DateName of Experiments Page No. Grade Initials

1Grain size distribution of fine & coarse aggregates

2Bulk density, Voids ratio, Porosity & Specific gravity

3Bulking of sand

4Aggregate crushing value

5Aggregate impact value

6Fineness of cement

7Normal consistency of cement

8Initial &final setting time of cement

9Compressive strength of cement

10Test on timber beam

11Test on clay roofing tiles

12Compressive strength of bricks

13Rockwell hardness test

14Brinell hardness test

15 Impact test :Izod & Charpy

Page 4: Mt lab manual 1

GRAIN SIZE DISTRIBUTION OF FINE &

COARSE AGGREGATES

Experiment No: 1

Date:

AIM:

To determine the particle size distribution of fine and coarse aggregates.

GENERAL:

The aggregate most of which passes IS: 4.75 mm sieve is classified as fine

aggregate. The fine aggregates obtained from natural disintegration of rocks and

deposited by streams are known as natural sands. Fine aggregates resulting from

crushing of hard stone are known as crushed sand.

The aggregate most of which is retained on IS 4.75 mm sieve is classified as

coarse aggregate. This may be in the form of uncrushed gravel or stone resulting from

natural disintegration of rocks. Crushed gravel or stone is obtained by crushed gravel

or hard stone.

Sieve analysis is carried out for the determination of fine and coarse

aggregates by sieving or screening. Sieves of size 80 mm, 40mm, 20mm, 10 mm, 4.75

mm, 2.36 mm, 1.18 mm, 600 micron, 300 micron &150 micron confirming to IS: 460.

Page 5: Mt lab manual 1

APPARATUS:

a) Balance: -The balance shall be such that it is readable and accurate to 0.1% of

the weight of the test sample.

b) Sieves:- sieves of the sizes given in table 1 & 2 confirming to

IS: 460-1962 shall be used.

PROCEDURE:

Take2 kg of air-dry sample of the fine aggregate (3 kg of coarse aggregate) and sieve

successively on the appropriate sieves starting with the largest. Care shall be taken to

ensure that the sieves are clean before use. Each sieve shall be taken separately over a

clear tray until not more than a trace passes, but in any case for a period of not less

than 2 minutes. If a mechanical sieve shaker is used, arrange the set of sieves in the

order of their aperture sizes in such a way that the sieve having smallest opening

comes at the bottom and a minimum of 10 minutes sieving will be required. Weigh

the aggregate retained in each sieve . Draw a graph taking logarithm (Log 10 ) of

aperture size of the sieve on the X-axis and % finer on the Y-axis.

Reporting of results: -

The result shall be calculated and reported as follows

The sieve opening corresponding to 10% passing (D10) gives effective size.

The ratio of sieve opening corresponding to 60% (D60) to sieve opening

corresponding to 10% passing (D10) gives uniformity coefficient.

The sum of the cumulative % retained in each of the sieves divided by 100 gives

the fineness modulus of the aggregate.

Grading zone can be determined by plotting a graph with logarithm of aperture size

of the sieves versus % finer according to value given in table 3.

Page 6: Mt lab manual 1

OBSERVATIONS AND CALCULATIONS: -

Coarse Aggregate

Weight of coarse aggregate used for sieving = ……………Kg

IS Sieve

size

Wt.Retained

(g)

%Wt

Retained

Cumulative

%

Wt.Retained

%Wt.

passingRemarks

80 mm

40 mm

20 mm

10 mm

4.75 mm

2.36 mm

1.18 mm

600 micron

300 micron

150 micron

Residue

Check

Table: 1- sieve analysis of coarse aggregate

Fine aggregate

Weight of fine aggregate used for sieving = ………..…KgIS Sieve

size

Wt.Retained

(g)

%Wt

Retained

Cumulative %

Wt.Retained

%Wt.

passingRemarks

10 mm

4.75 mm

2.36 mm

1.18 mm

600 micron

Page 7: Mt lab manual 1

300 micron

150 micron

Residue

Check

Table: 2- sieve analysis of fine aggregate

SPECIFICATION FOR FINE AGGREGATE

(IS: 383-1970)

IS SievePercentage passingGrading zone I Grading zone II Grading zone III Grading zone IV

10 mm 100 100 100 100

4.75 mm 90-100 90-100 90-100 95-100

2.36 mm 60-95 75-100 85-100 95-100

1.18 mm 30-70 55-90 75-100 90-100

600 micron 15-34 35-59 60-79 80-100

300 micron 05-20 08-30 12-40 15-50

150 micron 00-10 00-10 00-10 00-15

Table: 3-values for grading zones

RESULTS: -

Fine aggregate Coarse aggregate

1.Effective size (D10) mm

2.Uniformity coefficient (D60/D10)

3.Fineness modulus

4.Grading zone

DISCUSSIONS: -

(Discuss about the grading curves obtained. What is the average size of Fine

aggregate and Coarse aggregate in the given sample?)

Page 8: Mt lab manual 1

BULK DENSITY, VOID RATIO, POROSITY

AND SPECIFIC GRAVITY

Experiment No. 2

Date:

AIM:

To determine the bulk density, void ratio, porosity and specific gravity of the

given fine and coarse aggregates in loose and compact states.

GENERAL:

In estimating quantities of materials and in mix computations, when batching

is done on a volumetric basis, it is necessary to know the conditions under which the

aggregate volume is measured viz (a) loose or compact (b) dry or damp. For general

information and for comparisons of different aggregates, the standard conditions are

dry and compact. For scheduling volumetric batch quantities the unit weight in the

loose, damp state should be known.

Bulk density (unit weight) is the weight of a unit volume of aggregate, which

is usually expressed in kg. per litre.

Void ratio refers to the spaces between the aggregate particles. Numerically

this void space is the difference between the gross or overall volume of the aggregate

and the space occupies by the aggregate particles alone. Void ratio is calculated as the

ratio between the volume of voids and volume of solids.

Porosity is the ratio between the volume of voids and the total volume.

Specific gravity of aggregate is the ratio of the specific weight of aggregate

and specific weight of water.

APPARATUS:

Page 9: Mt lab manual 1

a) A balance sensitive of 0.5% of the weight of sample to be weighed.

b) A cylindrical container having sufficient capacity.

c) A tamping rod of 16 mm diameter and 60mm long rounded at one end.

d) A measuring jar.

PROCEDURE: -

Take the weight of the cylindrical container (W1). Fill water in the container up to the

brim and find the weight (W2). From these two, calculate the volume of the container

(V1). Fill the given sample of aggregate 1/3rd full in the container and give 25 strokes

with the rounded end of the tamping rod. Fill the container to overflowing by filling in

the same manner as above in two steps. Remove the surplus aggregate using the

tamping rod as a straight edge. Take the weight of the container with the aggregate

(W3). Add measured quantity of water to the aggregate in the container slowly until

the voids are completely filled with water. Note the volume of water added (V2), (To

verify the value of V2, take the weight of the container with aggregate and water and

find the weight of water added).

For loose aggregate.

Fill the container to overflowing by means of a shovel, the aggregate being

discharged from a height not exceeding 50mm above the top of the container. Level

the surface of the aggregate with a straight edge. Obtain the weight of the aggregate.

Repeat the same procedure used for compacted aggregate to ascertain the other

quantities.

Page 10: Mt lab manual 1

OBSERVATIONS AND CALCULATIONS: -

Sl.

No.Particulars

Fine aggregate Coarse aggregate

Loose Compact Loose Compact

1 Weight of Container (W1) kg

2Weight of Container +Water

(W2) kg

3Weight of Container +

Aggregate (W3) kg

4 Volume of container (V1) lit

5Volume of Water added

=Volume of voids (V2) lit

6Weight of Aggregate

(W3-W1)

7 Volume of Solids (V1-V2))

8

Bulk density =

Wt. of Aggregate

Total volume of aggregate

9Void ratio = Volume of voids

Volume of solids

10Porosity = Volume of voids

Total volume of aggregate

11

Sp. Wt. of aggregate =

Wt. of Aggregate

Volume of aggregate

12

Specific gravity =

Sp. Wt. of aggregate

Sp. Wt. of water

Page 11: Mt lab manual 1

RESULTS:

Sl

NOParameters

Fine aggregate Coarse aggregate Remarks

Loose Compact Loose Compact

1 Bulk density (kg/litre)

2 Void ratio

3 Porosity

4 Specific gravity

DISCUSSION:

(Compare the values with the usual value of the aggregates recommended for normal

concreting work)

Page 12: Mt lab manual 1

BULKING OF SAND

Experiment No: 3

Date:

AIM:

To determine the bulking characteristics of given sand.

GENERAL: -

The free moisture content of fine aggregate results in bulking of volume. Free

moisture forms a film around each particle. This film of moisture exerts surface

tension, which keeps the neighboring particles away from it. Hense no point of

contact is possible between the particles. This causes bulking of the volume .The

extent of bulking will depend upon the percentage of moisture content and particle

size of the fine aggregate. Bulking increases with the increase in moisture content up

to a certain limit and beyond that, further increase in moisture content results in the

decrease in volume.

Sand brought to work site may contain an amount of moisture, which will

cause bulking. When it is loosely filled into a measuring container, it occupies larger

volume than it would occupy if dry. Hence if sand intend to use in a concrete mix is a

measure by loose volume, it will be necessary to increase the volume of sand by

‘percentage bulking’. Otherwise the yield of concrete will be reduced and the mix

becomes deficient in sand and the aggregate is prone to segregation resulting in

honey-combing of concrete.

APPARATUS: -

Measuring jar, balance, scale and porcelain bowl.

PROCEDURE: -

Take about 200ml. of dry sand from the sample and find its weight. Add water at

2% by weight of dry sand and mix it thoroughly by hand. Pour the damp sand into the

measuring jar and consolidate it by shaking. Level the top surface using the scale.

Note its volume (V). Repeat the test with different % of water. Finally pour water into

Page 13: Mt lab manual 1

the measuring jar containing the moist sand until the water just submerge the sand

completely. Note the volume of sand (V0). Calculate the % bulking using the formula.

Percentage bulking = V- V0 × 100

V0

Draw the Percentage bulking versus moisture content curve and find the maximum

Percentage bulking and corresponding moisture content.

RESULT:-

1. Maximum percentage of bulking =

2. Moisture content at maximum bulking =

DISCUSSION: -

Page 14: Mt lab manual 1

OBSERVATION :-

Sl.noPercentage

moisture

Volume of

Water added

(ml)

Volume of

Moist sand

(Vml)

Percentage bulking

= V- V0 × 100

V0

Remarks

1 2

2 4

3 6

4 8

5 10

6 15

7 20

8 25

9 30

Page 15: Mt lab manual 1

AGGREGATE CRUSHING VALUE

Experiment No: 4

Date:

AIM:-

To determine the aggregate crushing value of the given coarse aggregate.

GENERAL: -

The aggregate crushing value gives a relative measure of the resistance of an

aggregate to crushing under a gradually applied compressive load. Crushing value is

defined as the ratio of fines passing a standard sieve produced by crushing under

standard condition to the weight of coarse aggregate expressed as a percentage.

Aggregate crushing values as determined by the IS code method shall not

exceed 30 for aggregate to be used for making concrete for wearing surface such as

roads and runways and 45 for uses other than wearing surface.

APPARATUS: -

An open-ended 150mm cylindrical cell with appropriate base plate and metal

tamping rod 16mm diameter 45cm long rounded at one end. A balance of capacity

5kg, IS sieves 12.5mm, 10mm and 2.36mm, compression testing machine capable of

applying a load of 40T and which can be operated to give a uniform rate of loading so

that a maximum load of 40T is reached in 10 minutes.

PROCEDURE: -

Take required quantity of aggregate passing on a 12.5mm sieve and retained

on a 10mm sieve. When aggregate of the required size is not available, test may be

conducted on the available sample, the specifications for cylinder and sieve separating

the fines may be taken from IS: 2386-1963. The aggregate should be in a saturated

surface dry condition. Fill the test sample of aggregates in the cylinder in thirds, each

part being subjected to 25 strokes from the tamping rod. Take the weight of the test

Page 16: Mt lab manual 1

sample (A) after leveling the surface of the aggregate and insert the plunger sot that at

rests horizontally on the surface of the aggregates. Place the apparatus with the test

sample and the plunger between the platens of the testing machine and apply the load

fairly at uniform rate so that the total load of 40T reaches in 10 minutes.

Release the load and remove the material from the cylinder and sieve it

through 2.36mm sieve. Collect and weigh the fraction passing the sieve (B).

Aggregate crushing value can be calculated as (B/A) x 100.

OBSERVATIONS AND CALCULATIONS:-

Weight of dry sample passing through IS 12.5mm sieve and retained on

IS: 10mm sieve (A) =

Weight of aggregate passing through the IS 2.36mm

Sieve after the test (B) =

Aggregate crushing value =

RESULT: -Aggregate crushing value for standard size aggregate =

DISCUSSION: -(Discussion the suitability of aggregate for construction)

Page 17: Mt lab manual 1

AGGREGATE IMPACT VALUE

Experiment No: 5

Date:

AIM: -

To determine the impact value of the given aggregates.

GENERAL:-

The property of a material to resist impact is known as toughness. Due to

movement of vehicles on the road aggregates are subjected to impact resulting in their

breaking down into smaller pieces. The aggregates should therefore have sufficient

toughness to resist their disintegration due to impact. This characteristic is measured

by impact value test. The aggregate impact value is a measure of resistance to sudden

impact or shock, which may differ from its resistance to gradually applied

compressive load.

APPARATUS: -

The apparatus of the aggregate impact value test as per IS: 2386 (Part IV)

1963 consists of:

(i) A testing machine weighing 45 to 60 kg and having a metal base with a

plane lower surface of not less than 30cm in diameter. It is supported

on level and plane concrete floor of minimum 450mm thickness. The

machine should also have provisions for fixing its base.

(ii) A cylindrical steel cup of internal diameter 102mm, depth 50mm and

minimum thickness 6.3mm.

(iii) A metal hammer weighing 13.5 to 14 kg the lower end is cylindrical in

shape, is 50mm long, 100mm in diameter with a 2mm chamfer at the

lower edge and case hardened. The hammer should slide freely

between vertical guides and be concentric with the cup. The free fall of

the hammer should be within 380+ 5mm

(iv) A cylindrical metal measure having internal diameter of 75mm and

depth 50mm for measuring aggregates.

Page 18: Mt lab manual 1

(v) Tamping rod 10mm in diameter and 230mm long rounded at one end.

(vi) A balance of capacity not less than 500g readable and accurate up to

0.1g.

PROCEDURE:-

Take 300g dried aggregate which passes through 12.5mm IS: sieve and

retained in 10mm IS: sieve. Pour the aggregate to fill about 1/3 depth of measuring

cylinder and give 25 blows using the rounded end of the tamping rod. Add two more

layers in similar manner to fill the mould completely. Strike of the surplus aggregates

and takes the weight of aggregates to nearest grams (W1). Fix the cup firmly in

position on the base of machine and place whole of the test sample in it and compact

by giving 25 gentle strokes with tamping rod. Raise the hammer until its lower face is

380mm above the surface of the aggregate sample in the cup and allow it to fall freely

on the aggregate sample. Give 15 such blows at an interval of not less than 1 second

between successive falls. Remove the crushed aggregates from the cup and sieve it

through 2.36 mm IS: sieve until no further significant amount passes in one minute.

Weigh the fraction passing the sieve to an accuracy of 1g (W2). Also weigh the

fraction retained in the sieve. Aggregate impact value can be calculated as aggregate

impact value = (W2/W1) x 100 and should be expressed as a nearest whole number.

The following precautions should be taken while conducting the test.

(i) The plunger should be placed centrally so that it falls directly on the

aggregate sample and does not touch the walls of the cylinder in the

order to ensure that the entire load is transmitted on to the aggregates.

(ii) In the operation of sieving the aggregates through 2.36mm IS sieve,

the sum of the weights of the fraction retained and passing the sieve

should not differ from the original weight of the specimen by more

than 1g.

(iii) The tamping is to be done properly by gently dropping the tamping rod

and not by hammering action. Also the tamping should be uniform

over the surface of the aggregate taking care that the tamping rod does

not frequently strike against the walls of the mould.

Page 19: Mt lab manual 1

OBSERVATIONS AND CALCULATIONS:-

Total weight of dry sample (W1) =

Weight of portion passing IS 2.36mm sieve (W2) =

Aggregate impact value = (W2/W1) X100

RESULT: -

Aggregate impact value =

DISCUSSION: -

(Discuss the suitability of the aggregate for road construction)

Page 20: Mt lab manual 1

FINENESS OF CEMENT

Experiment No:-6

Date:

AIM :

To determine the Fineness of cement by dry sieving

GENERAL:

Fines of cement has significant role on the rate of hydration and on the rate of

evolution of heat. Cement which is more finely ground hardened more rapidly and has

a higher rate of heat evolution at early ages. Greater finesses improves the

cohesiveness of concrete mix and quality of water rising to the surface of concrete

known as bleeding, is reduced.

Shrinkage cracking is related to the rate of development of strength of concrete. In

general, cement which gains more strength rapidly are more subjected to cracking.

Increasing the fineness of any particular cement, raises its rate of development of

strength and so indirectly increases the risk of shrinkage crack formation.

APPARATUS :

IS 90 micron sieve, weighing balance with a sensitivity of 0.1 gm.

PROCEDURE :

Weigh 100gm. of given sample of cement. Place it on a standard IS 90 micron

sieve. Breaking down any air set lumps in the cement sample with finger.

Continuously sieve the sample with a gently wrist motion for a period of, rotating the

sieve continuously throughout the sieving. Weigh the residue after 15 minutes of

sieving. Repeat the procedure for two more such samples.

OBSERVATION AND CALCULATIONS:

Weight of cement taken =

Weight of residue after 15 minutes of sieving =

RESULTS :

Fineness of cement of dry sieving =

Page 21: Mt lab manual 1

DISCUSSION :

(Discuss the quality of the given sample of cement by comparing with IS specifications.)

Page 22: Mt lab manual 1

OBSERVATIONS:-

Sl no

Type of

cement

Wt. of cement

W1 (g)

Wt of residue

W2 (g)

% Wt.of

residue

W2 X 100

W1

Average % of

residue

IS specification

Remarks

1

2

3

Page 23: Mt lab manual 1

NORMAL CONSISTENCY OF CEMENT

Experiment No:7

Date:

AIM:-

To determine the normal consistency of the given sample of cement.

GENERAL:-

Since different batches of cement differ in fineness, pastes with the same

water content may differ in consistency when first mixed. For this reason the

consistency of the paste is standardized by varying the water content until the paste

has a given resistance to penetration when it is first mixed.

Consistency is a state of flow and varies with the amount of water added to the

given quantity of cement. More water increases the plasticity of the mortar to flow

whereas reducing its quantity in the paste makes it hard and stiff. The normal

consistency of a cement paste is defined as that consistency which will permit the

Vicat plunger to penetrate to a point 5 to 7 mm from the bottom of Vicat mould when

the cement paste is tested. The value of the amount of water required to prepare a

paste of normal consistency is necessary for conducting other tests such as tensile test,

soundness test, setting time test and compressive strength test.

APPARATUS:-

Vicat’s apparatus with Vicat’s plunger, weighing balance, stop watch,

measuring jar, glass plates and porcelain bowl.

PROCEDURE:-

Take 400g of cement and break air set lumps of cement if any by hand. Add

water about 20 percentage by weight of cement. Start a stopwatch when water is

added to the dry cement. Prepare the cement paste such that the gauging time is not

less than 3 minutes nor greater than 5 minutes. The gauging time is counted from the

time of adding water to the dry cement until commencing to fill the mould. Fill the

mould completely and during filling shake the mould slightly to expel air. After filling

level the surface of the mould. Place the mould with the test block with non-porous

plate under the plunger. Lower the plunger gently to touch the surface of the test

Page 24: Mt lab manual 1

block and release it quickly. Note the reading on the scale. Prepare the trial pastes

with varying percentages of water until the amount of water necessary for making up

the normal consistency as defined is found.

RESULT:

Normal consistency of cement =

DISCUSSION:

Page 25: Mt lab manual 1

OBSERVATIONS:

Sl

no

Percentage of

Water added (%)

Quantity of

Water (cc)

Plunger

Reading (mm)

Page 26: Mt lab manual 1

INITIAL AND FINAL SETTING TIME OF CEMENT

Experiment No.8

Date:

AIM:

To determine the initial and final setting time of cement.

GAENERAL:

It is essential that cement set neither too rapidly nor too slowly. In the first

case there might be insufficient time to transport and place the concrete before it

becomes too rigid. In the second case too long a setting time tends to slow up the

work unduly and it might postpone the actual use of structure because of inadequate

strength at the desired age. As per IS: 4081-1968 the setting time of cements when

tested by Vicat apparatus are as follows.

Particulars

Ordinary Portland

cement

Rapid hardening

cement

Low heat

cement

1. Initial setting time

in minutes (not

less than)

30 30 60

2. Final setting time

in minutes (not

greater than )

600 600 600

APPARATUS: Vicat’s apparatus with needles, weighing balance, stopwatch,

measuring jar, porcelain bowl.

PROCEDURE:

Take 400gm. of cement and prepare a neat cement past with 0.85 times of

water required for normal consistency. The preparation of test block for the test is

same as that for the normal consistency test. Start a stopwatch when water is added to

the dry cement. Place the test block confined in the mould and resting on the non-

Page 27: Mt lab manual 1

porous plate below the needle of the Vicat apparatus. Lower the needle gently to

touch the surface of the test block and release quickly. In the beginning the needle

completely pierces the test block. Repeat this procedure until the needle pierces the

block by 5 ± 0.5mm measured from the bottom of the mould. The period elapsing

between the time when water is added to the cement and the time at which the needle

fails to pierce the test block by 5 ± 0.5mm is the initial setting time.

For determining the final setting time, replace the needle of Vicat apparatus by

the needle with an annular attachment. The cement is considered finally set when

upon applying the final setting needle gently to the surface of the test block, the

needle makes an impression thereon, while the attachment fails to do so. The period

elapsing between the time when water id added to the cement and the time at which

the needle make an impression on the surface of the test block while the attachment

fails to do so shall be the final setting time. In the event of a scum forming on the

surface of the test block, use underside of the test block for the determination of final

setting time.

RESULT:

Initial setting time of the given sample =

Final setting time of the given sample =

DISCUSSION:

(Discuss the quality of the given sample of cement comparing with IS

specifications)

Page 28: Mt lab manual 1

OBSERVATIONS:

INITIAL SETTING TIME OF CEMENT

Type of cement =

Weight of cement =

Quality of water added =

Sl. No Time Reading(mm) Remarks

Page 29: Mt lab manual 1

COMPRESSIVE STRENGTH OF CEMENT

EXPERIMENT. NO.9

Date :

AIM :

To determine the compressive strength of given sample of cement.

GENERAL :

The mechanical strength of hardened cement is the property of material that is

needed in the structural designs. The strength of cement is usually determined from

tests on mortar made with cement. The compressive strength of cement is determined

as represented by compressive strength tests on mortar cubes prepared by standard

method.

APPARATUS :

Moulds for the cube specimens of 50 cm2 face area, vibrating machine,

compression testing machine, apparatus for gauging and mixing mortar etc.

PROCEDURE :

The test specimen shall be in the form of cubes having of face area equal to 50

cm2 made of cement mortar 1:3 .In assembling the mould ready for use, cover the joint

between the halves of the mould and between the contact surface of the bottom of the

mould and base plate with a thin film of petroleum jelly, in order to ensure that no

water escapes during vibration. Coat the interior faces of the mould with thin coat of

mineral oil. Place the assembled mould on the table of the vibration machine and

firmly hold it in position by means of suitable clamp.

The material for each cube shall be cement W1 =200 gm

P +3

Standard sand W2 =3W1= 600 gm, water = 4 (W1+W2) g, where p is the 100 Percentage of water for standard consistency.

Place the mixture of cement and standard sand in a non-porous plate. Mix dry

with a trowel for one minute and add the required quantity of water and mix until the

Page 30: Mt lab manual 1

mixture is of uniform colour. The mixing time should not exceed 4 minutes and

should not be less than 3 minutes.

Immediately after mixing the mortar fill it in the cube mould and rod 20 times

with a rod in three layers. Place the remaining quantity of mortar in the hopper of the

cube moulds and pressed it again and then compact the mortar by vibration. The

period of vibration shall be 2 minutes at the specified rate of 12000+ 400 vibrations

per minutes. At the end of the vibration remove the mould together with the base plate

from the machine and finish the top surface of the cube in the mould by smoothing the

surface with the blade of the trowel.

Keep the filled mould at a temperature of 27 + 20C in an atmosphere of at least

90% relative humidity for 24 hrs. At the end of the period remove them from the

moulds and immediately submerge in fresh water and keep there until taken out just

prior to testing.

TESTING OF MORTAR CUBES

Test 3 cubes for compressive strength at the period mentioned in the IS

specification. The cubes are tested on their sides without any packing. The load shall

be readily and uniformly applied at the rate of 350kg / cm2 / min.

OBSERVATION AND CALCULATIONS

Weight of cement for one cube = 200g

Weight of sand = 600g

Weight of water for one cube =

Area of the cube face =

RESULT:

The average value of compressive strength of cement sand mortar cubes at

(i) 3days =

(ii) 7days =

DISCUSSION:

(Discuss (i) standard sand (ii) the quality of the given sample of cement)

Page 31: Mt lab manual 1

OBSERVATIONS:-

Sample

noAt 3 days age At 7 days age

LoadCompressive

Strength

Average

Compressive

Strength

LoadCompressive

Strength

Average

Compressive

Strength

(N) (N/mm2) (N/mm2) (N) (N/mm2) (N/mm2)

1

2

3

Page 32: Mt lab manual 1

TEST ON TIMBER BEAM

Experiment No:-10

Date:

AIM :

To determine the following properties of the timber specimen by conducting static

bending test.

1) Fibre stress at limit of proportionality

2) Modulus of rupture.

3) Modulus of elasticity

4) Elastic resilience.

GENERAL :

Standard size of specimen is 5 x 5 x 75 cm with 70 cm span. Where a standard

specimen cannot be obtain the dimensions of the test specimen shall be such as to

make the span l = 14 times the depth. Central deflections shall be measured at load

intervals of 50 kg.

EQUIPMENT :

30T U. T. M,Scale.

PROCEDURE :

Measure the size of the specimen and fix the span. Assuming the

maximum fibre stress ‘f ‘ (say 1000 kg / cm2) calculate the maximum central (W) the

specimen can carry.

M = wl = f Z, hence W = 4 f Z

4 l

where M is Maximum B.M

Z is the section modulus = bd 2 where ‘b ‘and ‘d ‘ are the breadth and

6

depth of the specimen.

Page 33: Mt lab manual 1

Select a suitable loading range and adjust the machine for that range. Mount

the beam supports over the cross head at correct span and place the specimen, fix the

special loading device to the cylinder device at top. Start the motor and slowly open

the inlet valve until the ram is floated. Adjust the pointer to the zero reading, raise the

cross head the central loading device just touches the top of the beam

specimen .Adjust the deflection dial to zero reading. Now slowly load the specimen

opening the inlet value and note deflections corresponding to the load increments until

the specimen fails. Also note the maximum load .Now draw load deflection curve.

Determine the slope of the straight line portion of the graph (P1)

RESULT :

1. Fibre stress at limit of proportionality =

2. Modulus of rupture =

3. Modulus of elasticity , =

4. Elastic resilience, =

DISCUSSION :

(Discuss the quality of the given timber.)

Page 34: Mt lab manual 1

OBSERVATIOS :

Load, kg

Central

deflection,mm

1. Span of the test specimen l (mm) =

2. Breadth of the test specimen b (mm) =

3. Depth of the test specimen d (mm) =

4. section modulus = bd 2 (mm3) =

6

5. Moment of inertia I = bd 3 (mm4) =

12

6. Load at limit of proportionality P (N) =

7.Maximum load P1(N) =

8. Fibre stress at limit of proportionality = Pl (N/mm2) =

4Z

9. Equivalent Fibre stress at Maximum

load = = P 1 l (N/mm2) =

4Z

10. Modulus of elasticity , =P1l3/48I∆ (N/mm2) =

11. Elastic resilience = work to limit of proportionalty/volume

(Nmm / mm3) =

Page 35: Mt lab manual 1
Page 36: Mt lab manual 1

TEST ON CLAY ROOFING TILES

Experiment No:-11

Date:

AIM :

To determine the following properties of clay roofing tiles

(i) water absorption percentage (ii) permeability (iii) breaking load.

GENERAL :

The roofing tiles shall be made from suitable clay of even texture and shall be

well burnt .They shall be free from irregularities such as twists,bends,cracks and

laminations. The roofing tiles shall be free from impurities such as particles of stone,

lime or other foreign materials visible to naked eye or on the fractured face of tile.

When struck the tile shall give a ringing sound and when broken the fracture shall be

clean and sharp at the edges. The average weight of six tiles shall not be less than 2Kg

and not more than3Kg. The strength requirements of roofing tiles as per IS654-1992

are (1) water absorption (2) permeability (3) breaking load.

APPARATUS :

Tile flexure strength testing machine. weighing balance,eletric oven.

PROCEDURE :

(1) water absorption Test:

Dry six tiles by placing in the oven at 1050C to 1100C till they attain

constant weight and them cool and weigh (A) Immerse the dry specimen in

clean water at 240C to 300C for 24 hrs .Take out the specimens wipe off the

surface water and weigh the specimens (B)

The % water absorption = (B-A ) x100

A The average % water absorption of six tiles can be taken as the % water absorption

Page 37: Mt lab manual 1

(2) Permeability test :

This test can be conducted at 27+/-20C and relative humidity of 65+/-5%.The

tile shall be fitted at the bottom of the trough and the space between the sides of the

trough plugged water tight with a suitable materials like wax or bitumen.

Pour water into the mould so that it stands over the lowest tile surface

to a height of 5cm and keep it for a period of six hours. After the period

the bottom of the tile shall be carefully examined to see whether the water

has seeped through the tiles.

(3) Breaking load.

Test six tiles after soaking them in water at 27+/-20C for 24hrs

in the wet condition. Support the tile evenly flat wise as the bearer set

with a span of 25cm and resting on the bottom surface. Apply the load

with the direction of the load perpendicular to the span at a uniform

rate of 450 to 550 N/min.Take the individual bearing load of each of

the six tiles separately in the wet condition and calculate the average

value .

PRINCIPLES OF TILE TESTING MACHINE :

Loding roller Upper lever

R

D E F

G C

Lower lever

W

DE = 15 cm EF =7.5 cm AC = 7.5 cm BC =22.5 cm

Lower arm

R

G A C B

7.5 cm 22.5 cm W

Page 38: Mt lab manual 1

Taking moments at A

W(7.5+22.5)– (P x 7.5) =

W = 7.5 P

30

P = 30W ……(1)

7.5

Upper lever R

D C F

P

15 cm 7.5 cm

Taking moments at F

R x 7.5 - P (15 + 7.5 ) = 0

7.5 R = 22.5 x 30W

7.5

R = 22.5 x 30 = 12 W

7.5 x 7.5

ie R = 12W

Page 39: Mt lab manual 1

RESULTS :

Sl

no

Identificat

-ion mark

Length

(cm)

Width

(cm)

Dry

wt.

(Kg)

%Water

absorptionBreaking

load(KN)

Permeabi-

lity

Classificatio

n as per IS:

654-1992

DISCUSSION :

(Discuss specifications of M P roofing tiles as per IS 654-1962 like sample size,

criteria for conformity etc.)

OBSERVATIONS AND CALCULATIONS :

Page 40: Mt lab manual 1

Water absorption test :

Sl

noIdentification

mark

Length

(cm)

Width

(cm)

Dry

wt.

(Kg)

Wet

wt.

(Kg)

%Water

absorption

Average

%Water

absorption

Classification

as per IS:

654-1992

Breaking load test :

Sl no

Identification mark

Length

(cm)

Width

(cm)

Dry wt.

(Kg)

Breaking load

(KN)

Average breaking

load (KN)

Classification as per

IS 654-1992

COMPRESSIVE STRENGTH OF BRICKS

Page 41: Mt lab manual 1

EXPERIMENT NO.12

Date :

AIM

To determine the compressive strength of the given sample of brick.

GENERAL :

Bricks are generally subjected to compression and rarely to tension. The usual

crushing strength of common hand moulded well burnt bricks is about 5 to 10 N/mm2

varying according to the nature of preparation of the clay.

APPARATUS:

A compression testing machine.

PROCEDURE :

Take 5 bricks, remove unevenness observed in the bed face to provide two

smooth parallel faces by grinding. Immerse the bricks in water at room temperature

for 24 hours. Take out the specimen from water and drain out any surplus moisture at

room temperature. Fill the frog (if provided) and all voids in the bed face flush with

cement mortar. Remove and wipe out any traces of moisture.

Place the specimen with flat faces horizontal and mortar filled face facing

upwards between two 3-plywood sheet each of 3 mm thickness and carefully cantered

between plates of the testing machine. Apply an axial load at a uniform rate 14 N/mm2

Per minute till failure and note the maximum load at failure.

RESULT:

Average compressive strength of brick =

DISCUSSION :

(Discussion the quality of the given sample of bricks).

OBSERVATIONS & CALCULATIONS

Page 42: Mt lab manual 1

Brick No Dimensions of the brick

(LxBxD ) mm

Average area of the bed face

mm2

Maximum load at

failure(N)

Compressive strength(N/mm2 )

1

2

3

4

5

Maximum Load of failure

Compressive strength = _________________________

Average area of the bed face

IS Classification of Bricks:-

Page 43: Mt lab manual 1
Page 44: Mt lab manual 1

ROCKWELL HARDNESS TEST

EXPERIMENT NO:13

Date :

AIM :

To study the Lucknik hardness testing machine and to find the Rockwell

hardness number of the materials of the given specimens.

GENERAL:

The test consists in forcing an indenter of standard type (cone or ball) into the

surface of the test piece in two operations and measuring the permanent increase of

the depth of indentation “e” of this indenter under specified conditions. The unit of

measurement of “e” is 0.002 mm from which a number known as the Rockwell

hardness is deduced.

The load and the indenter to be used for a particular test is decided from an

approximate relative hardness of the different materials. In general for hard materials

diamond cone indenter is used and for soft materials steel ball indenter is used.

Sl

no

Material Indenter Total load Scale symbol Scale

1 Very hard and thin Diamond cone 60 A Black

2 Very hard Diamond cone 150 C Black

3 Soft Steel ball

1.5875mm.dia.

100 B Red

4 Soft and thin Steel ball

1.5875mm.dia

60 F Red

Usually C and B are used. HRC;used for very hard materials.

F0 = ,Preliminary load = 10 kgf

Page 45: Mt lab manual 1

F1 =Additional load 140 Kgf.

F1 = F0 + F1 =150 kgf

e = Permanent increase of depth of indentation under the preliminary load after

removal of additional load. This is expressed in units of 0.002 mm

HRC =Rockwell hardness C =100-e

Range of the scale is 0 to 100 and block scale is to be used.

HRB used for soft materials. The ball inter has to be used.

F = F0 + F1 = 10 +90 = 100 kgf

HRB =Rockwell hardness B =130-e

Range of the scale is 30 to 130

ep =Depth of indentation due to F0

ea =Increase in depth of indentation due to F1

Test requirements:-

Page 46: Mt lab manual 1

1.The surface of the test piece shall be smooth and even and free from oxide

Scales and foreign matter.

2. The thickness of the test piece shall be at least 8 times the permanent

increase of depth “e”

3. The distance between centres of two adjacent impressions shall be at least 4

times the diameter of indentation and the distance from the center of the

indentation to the side of the test piece shall be at least 2.5 times the

diameter of indentation.

4.The dial of the indicator shall be set at initial position and the load increased

without sudden shock within 2 to 8 seconds.,

EQUIPMENT:

Lucknik hardness testing machine

PROCEDURE

Put the required weight on the pan. Insert the indenter and fasten with a screw.

Place the specimen on the object table and turn the wheel to raise the elevation screw

until specimen touches the indenter. Turn the wheel slowly to make the indenter

penetrate the specimen until the small pointer of the dial indicator is on the red dash.

Now the specimen is subjected to the preliminary load of 10kgf.Bring the big pointer

to read zero for C scale (black) or 30 of B-scale (red). Press the releasing device to

increase the load from F0 to F1 inducing a further driving of indenter into the

specimen.

Keep the load stationary for 4 to 6 seconds for hard materials and 6 to 8

seconds for soft materials. Release the load by turning the crank in the reverse

direction. The reading corresponds to the position of the big pointer gives the

hardness number directly (black scale HRC and red scale HRB).

Page 47: Mt lab manual 1

OBSERVATION:

Material Indenter Load(kgf) HRC Mean HRC HRB Mean

HRB

RESULT:

Rockwell hardness no. of ( ì )

( ì ì)

( ììì )

(ìv)

Page 48: Mt lab manual 1

BRINELL HARDNESS TEST

EXPERIMENT NO: 14

Date :

AIM :

To study the Brinell hardness testing machine and to find the Brinell hardness

number of the material of the specimen supplied.

GENERAL: -

The test consisting in forcing a steel ball of diamater “D” under a load “F” into

the test piece and measuring the diameter of the indentation left in the surface “d”.

The Brinell hardness is obtained by dividing the test load F in kgf.by the curved

surface area of indentation in square mm.

Total loadHBS or HBW =

Surface area of indentation

F

= ╥ Dh where “h” is the depth of indentation in mm.

F =

╥D [D─√ D2─d2] 2

2 F =

╥D [D─√D2─d2 ]

HBS =Brinell hardness in case where a steel ball is used for materials whose HB is

not exceeding 450.

HBW = Brinell hardness in case where as hard metal ball is used for materials whose

HB is not exceeding 650

Example :- 160 HBS 10/3000/15 = Brinell hardness of 160 determined with a steel

ball of 10 mm diameter and with a test force of 3000 kgs. Applied for 15 seconds.

Page 49: Mt lab manual 1

Test requirement:-

1. The surface of the test piece shall be sufficiently smooth and even.

2. The thickness of test piece shall not be less than 8times the depth

of indentation h .

3. The distance of centre of indentation from the edge of test piece shall be at

least 2.5 times the diameter of the indentation and the distance between center

of two adjacent indentation shall be at least 4 times the diameter of

indentation.

4. The test load is attained without shock or vibration. The test load shall be

Maintained for 10 or 15 seconds.

5. It is desirable that the diameter “d” of the indentation should range between

0.25D and 0.05 D

The ratio of F/ D2 shall be chosen according to the material.

Material F/D2

Mild steel 30

Brass 10 or 15

Copper 10

EQUIPMENTS:

Brinell hardness testing machine, traveling microscope.

PROCEDURE :

Page 50: Mt lab manual 1

Considering the material of the specimen and the size of the ball indenter

select a suitable load and suspend weights on the yoke tray accordingly. Insert the

steel ball indenter in position and place the specimen on the work table. Raise the

specimen by turning the hand wheel until the contact with the steel ball is obtained.

Close the valve and smoothly pump oil without causing any shock using the hand

lever until the desire load is obtained. Maintaine the load for specified time (10 to 15

seconds)for steel and 30 ±2 seconds for light metals. Then slowly open the valve there

by raleasing the oil pressure and the load. Lower the specimen by turning the hand

wheel.

Remove the specimen and measure the diameter of indentation in two perpendicular

directions (d1and d2 ).The average of d1and d2 is the diameter of indentation

“d”.Calculate HBS using the formula.

RESULT :-

Brinell Hardness no of ( ì )

( ì ì)

Page 51: Mt lab manual 1

OBSERVATION :

Materials Load(kgf

)

D(mm) Dia of indentation d(mm) HBS Mean

HBSd1(mm) d2(mm)

Page 52: Mt lab manual 1

IMPACT TESTS: IZOD, CHARPY

Experiment No:-15

Date:

AIM :

a) To draw calibration curves for the machine used.

b) To find the impact values (izod and charpy) of the materials of the

standard specimens.

EXPERIMENT:

Avery impact testing machine, setting gauges.

GENERAL:

For deciding the suitability of material, which is expected to resist repeated

shocks, the ordinary static tensile test is not formed satisfactory. Testing machines

have been decided so that a specimen can be subjected to shock load. The energy

required to break the specimen is taken as a measure of the resistance of the

material against shock loading. The property of a material relating to the work

required to cause rupture has been termed as “toughness”.

AVERY IMPACT TESTING MACHINE:

The machine consists of a pendulum with a hammer having a striker at the

end. The length of the pendulum is 0.825m with a hammer weight of 22.05kg for

izod and 20.996kg for charpy along with its accessories. The machine has two

capacity ranges 0 to 164 J for izod test (cantilever test) and 0 to 300 J for charpy

test(beam test). Two control levers are fitted one for releasing the pendulum and

other for clamping the specimen. The angle of raise of pendulum after impact is

read from the dial. A stop is fitted to support the pendulum in the rest portion.

Two ratchets fitted to the pendulum lock at the 164 J or 300 J height

which ever is selected.

Page 53: Mt lab manual 1

PROCEDURE:

a) Calibration curves:-

Initial energy E1 = Wh1

= W( L- LcosΦ1) –––––––– (1)

Final energy E2 = Wh2

= W( L- LcosΦ) –––––––– (2)

Loss of energy or impact value = EL = E1 - E2 = WL ( cosΦ- cosΦ1)

L = 0.825m

W=22.057 Kg for Izod and 20.996 Kg for charpy

Φ1 = 85.35° for Izod

Φ1= 140° for Chatpy

E1 = 164J for izod test and 300J for charpy test. Substitute the

corresponding values in eqn: (1) and find Φ1. To find a relation between

ELand Φ1. Substitute for W.Land Φ1.for varying values of Φ1,calculate the

corresponding values of EL and draw a curve of EL Vs Φ which is the

calibration curve. Now during a test if the pointer indicates an angle of Φ2

after impact ,the corresponding impact value can be read from the

calibration curve.

Φ1

Φ

L L

L

h1

h2

W W

W

Page 54: Mt lab manual 1

B (1) Cantilever test (izod and charpy)

Fit the striker with the horizontal face in the striker

position. the appropriate grips are positioned .after inserting the test piece with the

notch to the right, set the specimen for the correct height with the setting gauge and

lock the grips with the right hand lever, with the safety lever in the izod position ,raise

the pendulum to 164J position. Rotate the maximum pointer anticlockwise until it

contacts the fixed pointer attached to the pendulum. Release the pendulum by the left

hand lever.After the pendulum has passed the test piece it will carry the maximum

pointer and leave it indicating the angle of raise of pendulum after impact. Arrest the

pendulum by catching the handle with the right hand. after pulling the pendulum back

raise the stop to allow the top of the pendulum to rest on it. Repeat the test by using

the remaining two notches of the specimen. Take the average of these three values as

the impact value of the specimen.

2) Beam test (charpy test):

In this case fit with the striker with the central vertical

edge in the striking position. Position and lock the anvil. Place the test piece across

the anvil with the notch to the left locating it centrally with the centering gauge with

the safety lever in the charpy position raise the pendulum to the 300J position and

release. Read the values indicated in the dial.

RESULT :

a) calibration curves were drawn.

b) Impact value of the materials of standard specimen (mild steel)

1. By izod test =

2. By charpy test =

DISCUSSION:

Page 55: Mt lab manual 1

OBSERVTION:

Calibration curve Test Result

Φ EL(kgm) EL(kgm) Angle Φ2 EL (J)Mean

EL (J)

0 Izod

10

20

30

40

50

60

70 Charpy

80

90

100

110

120

130

140