n/a matrix: derivative certificate · 1,1-dichloroethene 1 ppm 8 pass nd 1,2-dichloroethane 0.18...
TRANSCRIPT
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/24/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCrystalline Solid
N/AMatrix: Derivative
Certificateof Analysis
Sample:DA00214012-001Harvest/Lot ID: N/A
Seed to Sale #n/aBatch Date :N/A
Batch#: 8049619.002Sample Size Received: 29 gram
Retail Product Size: 120Ordered : 02/13/20Sampled : 02/13/20
Completed: 03/24/20 Expires: 03/24/21Sampling Method: SOP Client Method
Mar 24, 2020 | Origin Labs Inc2102 Buisness Center Drive,.,Irvine,92612,California
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesNOT TESTED
CANNABINOID RESULTS
Total THC
0.133%Total CBD
95.590%Total Cannabinoids
97.720%
CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA
0.705% ND 0.583% 0.125% ND 0.584% ND ND95.590% 0.133% ND
7.050mg/g ND
5.830mg/g
1.250mg/g ND
5.840mg/g ND ND
955.900mg/g
1.330mg/g ND
LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :1224 0.1003g 02/14/20 11:02:12 965
Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 02/17/20 11:22:57Analytical Batch -DA010244POT Instrument Used : DA-LC-003 Batch Date : 02/14/20 09:31:17
Reagent Dilution Consums. ID
123019.R09 400 181205SFN-BX-1025849C4-849AK840C6-840H
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSED
Analyzed By Weight Extraction date LOD(ppm) Extracted By584 1g 02/14/20 584
Analysis Method -SOP.T.40.013 Batch Date : 02/14/20 11:49:39Analytical Batch -DA010267FIL Reviewed On - 02/14/20 13:33:01Instrument Used :
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
TEST 1) Raw Material Test
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/24/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCrystalline Solid
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrigin Labs Inc
2102 Buisness Center Drive,.Irvine,92612,CaliforniaTelephone: 9494560124Email: [email protected]
Sample : DA00214012-001Harvest/LOT ID: N/ABatch# : 8049619.002Sampled : 02/13/20Ordered : 02/13/20
Sample Size Received : 29 gramCompleted : 03/24/20Expires: 03/24/21Sample Method : SOP Client Method
Page 2 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultDIMETHOATE 0.01 ppm 0.1 NDCYPERMETHRIN 0.05 ppm 1 NDCYFLUTHRIN 0.05 ppm 1 NDCHLORFENAPYR 0.01 ppm 0.1 NDMETHYL PARATHION 0.005 ppm 0.1 NDCAPTAN 0.07 ppm 3 NDABAMECTIN B1A 0.02 ppm 0.3 NDACEPHATE 0.001 ppm 3 NDDICHLORVOS 0.05 ppm 0.1 NDDIMETHOMORPH 0.005 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDALDICARB 0.02 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDETOXAZOLE 0.01 ppm 1.5 NDBIFENAZATE 0.01 ppm 3 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDFENPYROXIMATE 0.01 ppm 2 NDCARBARYL 0.01 ppm 0.5 NDFIPRONIL 0.02 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.01 ppm 3 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDCHLORMEQUAT CHLORIDE 0.05 ppm 3 NDIMIDACLOPRID 0.01 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.01 ppm 2 NDCLOFENTEZINE 0.01 ppm 0.5 NDMETALAXYL 0.01 ppm 3 NDCOUMAPHOS 0.005 ppm 0.1 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 ND
Pesticides LOD Units Action Level ResultDAMINOZIDE 0.02 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.01 ppm 0.5 NDOXAMYL 0.01 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.01 ppm 3 NDPRALLETHRIN 0.05 ppm 0.4 NDPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.01 ppm 1 NDPYRIDABEN 0.01 ppm 3 NDSPINETORAM 0.01 PPM 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.02 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.01 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0.1 ppm 20 ND
TOTAL PERMETHRIN 1 ppm 1 NDTOTAL SPINOSAD 1 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By56 1.0258g 02/14/20 01:02:02 1082
Analysis Method - SOP.T.30.065, SOP.T.40.065,SOP.T40.060, SOP.T.40.070 and SOP.T.40.090 ,SOP.T.30.065, SOP.T.40.065, SOP.T40.060 andSOP.T.40.090Analytical Batch - DA010261PES Reviewed On- 02/14/20 13:33:01Instrument Used : LCMS E-SHI-039Batch Date : 02/14/20 11:47:17
Reagent Dilution Consums. ID020320.25 10 846C7-8323021420.R02021420.R03
Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparationfor Pesticides Analysis via LCMSMS and SOP.T40.060 Procedure for Pesticide Quantification Using LCMS).Volatile Pesticides may be tested with GCMSMS under SOP.T.40.070 and SOP.T.40.090. * Pesticide screen isperformed using GC-MS which can screen down to below single digit ppb concentrations for regulatedPesticides. Currently we analyze for 2 Volatile Pesticides. (Method: SOP.T.30.060 Sample Preparation forPesticides Analysis via LCMSMS and SOP.T.40.090 Volatile Pesticides Analysis by GC-MS/MS
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/24/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCrystalline Solid
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrigin Labs Inc
2102 Buisness Center Drive,.Irvine,92612,CaliforniaTelephone: 9494560124Email: [email protected]
Sample : DA00214012-001Harvest/LOT ID: N/ABatch# : 8049619.002Sampled : 02/13/20Ordered : 02/13/20
Sample Size Received : 29 gramCompleted : 03/24/20Expires: 03/24/21Sample Method : SOP Client Method
Page 3 of 4
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
1,1-DICHLOROETHENE 1 ppm 8 PASS ND
1,2-DICHLOROETHANE 0.18 ppm 2 PASS ND
2-PROPANOL 45 ppm 500 PASS ND
ACETONE 67.5 ppm 750 PASS ND
ACETONITRILE 5.4 ppm 60 PASS ND
BENZENE 0.09 ppm 1 PASS ND
BUTANES (N-BUTANE) 96 ppm 5000 PASS ND
CHLOROFORM 0.18 ppm 2 PASS ND
DICHLOROMETHANE 3.75 ppm 125 PASS ND
ETHANOL 90 ppm 5000 PASS ND
ETHYL ACETATE 36 ppm 400 PASS ND
ETHYL ETHER 45 ppm 500 PASS ND
ETHYLENE OXIDE 0.6 ppm 5 PASS ND
HEPTANE 45 ppm 5000 PASS ND
METHANOL 22.5 ppm 250 PASS ND
N-HEXANE 4.5 ppm 250 PASS ND
PENTANES (N-PENTANE) 67.5 ppm 750 PASS ND
PROPANE 120 ppm 5000 PASS ND
TOLUENE 13.5 ppm 150 PASS ND
TOTAL XYLENES 13.5 ppm 150 PASS ND
TRICHLOROETHYLENE 2.25 ppm 25 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0265g 02/14/20 02:02:52 850
Analysis Method -SOP.T.40.032Analytical Batch -DA010276SOL Reviewed On - 02/17/20 14:51:28Instrument Used : Headspace GCMSBatch Date : 02/14/20 14:34:18
Reagent Dilution Consums. ID
1 00268767161040-124152436
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.30.032 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/24/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCrystalline Solid
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrigin Labs Inc
2102 Buisness Center Drive,.Irvine,92612,CaliforniaTelephone: 9494560124Email: [email protected]
Sample : DA00214012-001Harvest/LOT ID: N/ABatch# : 8049619.002Sampled : 02/13/20Ordered : 02/13/20
Sample Size Received : 29 gramCompleted : 03/24/20Expires: 03/24/21Sample Method : SOP Client Method
Page 4 of 4
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA010262 | Reviewed On - 02/17/20 17:12:31Instrument Used : LCMS E-SHI-039Batch Date : 02/14/20 11:47:23
Analyzed by Weight Extraction date Extracted By56 1g NA NA
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Microbials PASSED
Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Analysis Method -SOP.T.40.043Analytical Batch -DA010247MIC | Reviewed On - 02/17/20 15:07:16Instrument Used : PathogenDX PCR_Array Scanner,PathogenDX PCR_119Batch Date : 02/14/20 10:15:00
Analyzed by Weight Extraction date Extracted By513 1.0431g 02/14/20 10:02:16 1082
Reagent Dilution Consums. ID
021320.R13 181019-274
121619.08 SG298A
Reagent Consums. ID020420.371020420.377122719.60122719.65122719.66013120.63013120.66013120.301122719.21122719.85
918C4923C4-923AK929C6-929H50AX262191932323819111190611634
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR)method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as acrude lysate which avoids purification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli,Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus isdetected in 1g of a sample, the sample fails the microbiological-impurity testing.
Heavy Metals PASSED
Reagent Dilution021320.R12021220.R17021220.R15021020.R10012920.R03020520.R01
50
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 ppm ND 1.5CADMIUM 0.02 ppm ND 0.5LEAD 0.02 ppm ND 0.5MERCURY 0.02 ppm ND 3
Analyzed by Weight Extraction date Extracted By53 0.2621g 02/14/20 01:02:46 457
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA010237HEA | Reviewed On - 02/17/20 14:46:32Instrument Used : ICPMS-2030 BBatch Date : 02/14/20 08:32:51
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.
Pharma Natural 14500 NW 60th Ave. Building 7F
Miami Lakes. Fl 33014 USA www.pharmanatural.com
P a g e 1 | 1
Test Certificate
QC Chemistry Laboratory
Product Description: Full spectrum CBD Liquid capsules
Client: Pharma Natural for Origin Labs, Inc.
Serving Size 1 capsule Reference #: 0064
Sample ID: BK2374 Lot #: 9344
Expiration date: 03/2023
Date received: 03/16/2020 Date completed: 03/16/2020
Chemical Analysis
Analysis Result Units Specifications Test Method
Cannabidiol CBD 32.90 mg/cap 23.4 – 34.9 HPLC, USP <621>, STP 001
Tested by: _____________________________ Date: ______________________ Yusel Espinosa - Analyst
Approved by: _____________________________ Date: ______________________ Rosa Lidia Solis – QC Manager
TEST 2) In-House Lab Test (Post-Formulation)
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/25/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCBD Capsules
N/AMatrix: Derivative
Certificateof Analysis
Sample:DA00318004-001Harvest/Lot ID: Lot#C000206336
Seed to Sale #N/ABatch Date :N/ABatch#: BK2374
Sample Size Received: 60Retail Product Size: 60
Ordered : 03/16/20Sampled : 03/16/20
Completed: 03/24/20 Expires: 03/24/21Sampling Method: SOP Client Method
Mar 24, 2020 | Origin Labs Inc2102 Buisness Center Drive,.,Irvine,92612,California
PASSEDPage 1 of 5
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
0.012%Total CBD
6.435%Total Cannabinoids
6.583%
CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA
0.054% ND 0.041% ND ND 0.042% ND ND 6.435% 0.012% ND
0.540mg/g ND
0.410mg/g ND ND
0.420mg/g ND ND
64.349mg/g
0.120mg/g ND
LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :1224 1.5036g 03/20/20 11:03:48 965
Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 03/23/20 10:14:30Analytical Batch -DA011096POT Instrument Used : DA-LC-003 Batch Date : 03/20/20 08:48:17
Reagent Dilution Consums. ID
022820.05 400 180111280653964914C4-914AK929C6-929H
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSED
Analyzed By Weight Extraction date LOD(ppm) Extracted By584 1g 03/18/20 584
Analysis Method -SOP.T.40.013 Batch Date : 03/18/20 09:47:32Analytical Batch -DA011054FIL Reviewed On - 03/18/20 11:31:48Instrument Used : Filth/Foreign Material Microscope
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
TEST 3) Third Party Post-Test
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/25/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCBD Capsules
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrigin Labs Inc
2102 Buisness Center Drive,.Irvine,92612,CaliforniaTelephone: 9494560124Email: [email protected]
Sample : DA00318004-001Harvest/LOT ID: Lot#C000206336Batch# : BK2374Sampled : 03/16/20Ordered : 03/16/20
Sample Size Received : 60Completed : 03/24/20Expires: 03/24/21Sample Method : SOP Client Method
Page 2 of 5
Terpenes TESTEDTerpenes LOD Units Result (%)
ALPHA-CEDRENE 0.007 % NDALPHA-HUMULENE 0.007 % 0.023ALPHA-PINENE 0.007 % NDALPHA-TERPINENE 0.007 % NDBETA-MYRCENE 0.007 % NDBETA-PINENE 0.007 % NDBORNEOL 0.013 % NDCAMPHENE 0.007 % NDCAMPHOR 0.013 % NDCARYOPHYLLENEOXIDE
0.007 % ND
CEDROL 0.007 % NDALPHA-BISABOLOL 0.007 % 0.041SABINENE 0.007 % NDSABINENE HYDRATE 0.007 % NDTERPINEOL 0.007 % NDTERPINOLENE 0.007 % NDBETA-CARYOPHYLLENE 0.007 % 0.087TRANS-NEROLIDOL 0.007 % NDVALENCENE 0.007 % NDPULEGONE 0.007 % NDALPHA-PHELLANDRENE 0.007 % NDOCIMENE 0.007 % NDNEROL 0.007 % NDLINALOOL 0.007 % NDLIMONENE 0.007 % NDGUAIOL 0.007 % 0.027GERANYL ACETATE 0.007 % NDGERANIOL 0.007 % NDGAMMA-TERPINENE 0.007 % NDFENCHONE 0.007 % NDFARNESENE 0.007 % 0.148
Terpenes LOD Units Result (%)
EUCALYPTOL 0.007 % NDISOBORNEOL 0.007 % NDHEXAHYDROTHYMOL 0.007 % NDFENCHYL ALCOHOL 0.007 % ND3-CARENE 0.007 % NDCIS-NEROLIDOL 0.007 % NDISOPULEGOL 0.007 % ND
Terpenes TESTED
Analyzed by Weight Extraction date Extracted By1351 0.9849g 03/18/20 10:03:54 1351
Analysis Method -SOP.T.40.090Analytical Batch -DA011038TER Reviewed On - 03/19/20 08:35:42Instrument Used : GA-Triple Quad GCMS TerpBatch Date : 03/18/20 08:31:00
Reagent Dilution Consums. ID
021420.10 10 180111012120.R13 280653964
Terpenoid profile screening is performed using GC-MS with Liquid Injection(Gas Chromatography – Mass Spectrometer) which can screen 38 terpenesusing Method SOP.T.40.091 Terpenoid Analysis Via GC/MS.
Total 0.33
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/25/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCBD Capsules
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrigin Labs Inc
2102 Buisness Center Drive,.Irvine,92612,CaliforniaTelephone: 9494560124Email: [email protected]
Sample : DA00318004-001Harvest/LOT ID: Lot#C000206336Batch# : BK2374Sampled : 03/16/20Ordered : 03/16/20
Sample Size Received : 60Completed : 03/24/20Expires: 03/24/21Sample Method : SOP Client Method
Page 3 of 5
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.02 ppm 0.3 NDACEPHATE 0.001 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.02 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCAPTAN 0.07 ppm 3 NDCARBARYL 0.01 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.01 ppm 3 NDCHLORFENAPYR 0.01 ppm 0.1 NDCHLORMEQUAT CHLORIDE 0.05 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.01 ppm 0.5 NDCOUMAPHOS 0.005 ppm 0.1 NDCYFLUTHRIN 0.05 ppm 1 NDCYPERMETHRIN 0.05 ppm 1 NDDAMINOZIDE 0.02 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.05 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.005 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.02 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.01 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.01 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 ND
Pesticides LOD Units Action Level ResultMETHOMYL 0.01 ppm 0.1 NDMETHYL PARATHION 0.005 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.01 ppm 0.5 NDOXAMYL 0.01 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.01 ppm 3 NDPRALLETHRIN 0.05 ppm 0.4 NDPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.01 ppm 1 NDPYRIDABEN 0.01 ppm 3 NDSPINETORAM 0.01 PPM 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.02 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.01 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0 ppm 20 ND
TOTAL PERMETHRIN 1 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 1.0563g 03/18/20 12:03:13 1082
Analysis Method - SOP.T.30.065, SOP.T.40.065,SOP.T40.060, SOP.T.40.070 and SOP.T.40.090 ,SOP.T.30.065, SOP.T.40.065, SOP.T40.060 andSOP.T.40.090Analytical Batch - DA011047PES Reviewed On- 03/18/20 11:31:48Instrument Used : DA-LCMS-001_DERBatch Date : 03/18/20 09:34:02
Reagent Dilution Consums. ID10
Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparationfor Pesticides Analysis via LCMSMS and SOP.T40.060 Procedure for Pesticide Quantification Using LCMS).Volatile Pesticides may be tested with GCMSMS under SOP.T.40.070 and SOP.T.40.090. * Pesticide screen isperformed using GC-MS which can screen down to below single digit ppb concentrations for regulatedPesticides. Currently we analyze for 2 Volatile Pesticides. (Method: SOP.T.30.060 Sample Preparation forPesticides Analysis via LCMSMS and SOP.T.40.090 Volatile Pesticides Analysis by GC-MS/MS
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/25/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCBD Capsules
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrigin Labs Inc
2102 Buisness Center Drive,.Irvine,92612,CaliforniaTelephone: 9494560124Email: [email protected]
Sample : DA00318004-001Harvest/LOT ID: Lot#C000206336Batch# : BK2374Sampled : 03/16/20Ordered : 03/16/20
Sample Size Received : 60Completed : 03/24/20Expires: 03/24/21Sample Method : SOP Client Method
Page 4 of 5
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
1,1-DICHLOROETHENE 1 ppm 8 PASS ND
1,2-DICHLOROETHANE 0.18 ppm 2 PASS ND
2-PROPANOL 45 ppm 500 PASS ND
ACETONE 67.5 ppm 750 PASS ND
ACETONITRILE 5.4 ppm 60 PASS ND
BENZENE 0.09 ppm 1 PASS ND
BUTANES (N-BUTANE) 96 ppm 5000 PASS ND
CHLOROFORM 0.18 ppm 2 PASS ND
DICHLOROMETHANE 3.75 ppm 125 PASS ND
ETHANOL 90 ppm 5000 PASS ND
ETHYL ACETATE 36 ppm 400 PASS ND
ETHYL ETHER 45 ppm 500 PASS ND
ETHYLENE OXIDE 0.6 ppm 5 PASS ND
HEPTANE 45 ppm 5000 PASS ND
METHANOL 22.5 ppm 250 PASS ND
N-HEXANE 4.5 ppm 250 PASS ND
PENTANES (N-PENTANE) 67.5 ppm 750 PASS ND
PROPANE 120 ppm 5000 PASS ND
TOLUENE 13.5 ppm 150 PASS ND
TOTAL XYLENES 13.5 ppm 150 PASS ND
TRICHLOROETHYLENE 2.25 ppm 25 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0265g 03/18/20 03:03:10 850
Analysis Method -SOP.T.40.032Analytical Batch -DA011062SOL Reviewed On - 03/20/20 11:37:51Instrument Used : Headspace GCMSBatch Date : 03/18/20 13:21:22
Reagent Dilution Consums. ID
1
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.30.032 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
03/25/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsCBD Capsules
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrigin Labs Inc
2102 Buisness Center Drive,.Irvine,92612,CaliforniaTelephone: 9494560124Email: [email protected]
Sample : DA00318004-001Harvest/LOT ID: Lot#C000206336Batch# : BK2374Sampled : 03/16/20Ordered : 03/16/20
Sample Size Received : 60Completed : 03/24/20Expires: 03/24/21Sample Method : SOP Client Method
Page 5 of 5
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA011048MYC | Reviewed On - 03/20/20 16:34:21Instrument Used : DA-LCMS-001_DERBatch Date : 03/18/20 09:34:54
Analyzed by Weight Extraction date Extracted By585 1g 03/20/20 04:03:18 585
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Microbials PASSED
Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Analysis Method -SOP.T.40.043Analytical Batch -DA011125MIC | Reviewed On - 03/24/20 16:05:43Instrument Used : PathogenDX PCR_Array Scanner,PathogenDX PCR_DA-013Batch Date : 03/23/20 08:57:33
Analyzed by Weight Extraction date Extracted By513 1.0118g 03/23/20 09:03:33 513
Reagent Dilution Consums. ID
121619.17 4603475C
929C6-929H
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR)method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as acrude lysate which avoids purification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli,Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus isdetected in 1g of a sample, the sample fails the microbiological-impurity testing.
Heavy Metals PASSED
Reagent Reagent Dilution031720.R07031720.R08031720.R02031720.R03031820.R03031820.R02
031820.R01031020.R02111319.02
50
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 ppm ND 1.5CADMIUM 0.02 ppm ND 0.5LEAD 0.02 ppm ND 0.5MERCURY 0.02 ppm ND 3
Analyzed by Weight Extraction date Extracted By457 0.2790g 03/18/20 10:03:09 457
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA011041HEA | Reviewed On - 03/19/20 10:09:46Instrument Used : ICPMS-2030Batch Date : 03/18/20 08:39:21
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.