nanomechanics instabilities and terahertz vibrations: from...
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SEM 2017 Annual Conference & Exposition SEM 2017 Annual Conference & Exposition on Experimental and Applied Mechanicson Experimental and Applied Mechanics
Indianapolis, IndianaIndianapolis, IndianaJune 12June 12--15, 201715, 2017
Nanomechanics Instabilities and TeraHertz Vibrations: From Geochemical Evolution to
Fracto-emission Seismic Precursors
Alberto Carpinteri, Oscar BorlaPolitecnico di Torino, Department of Structural, Politecnico di Torino, Department of Structural,
Geotechnical and Building EngineeringGeotechnical and Building Engineering
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(3.8 (3.8 BillionBillion yearsyears ago): ago): Fe (Fe (−−7%) + Ni 7%) + Ni ((−−0.2%) = 0.2%) = =Al=Al (+3%) + Si (+2.4%) + C (+1.8%)(+3%) + Si (+2.4%) + C (+1.8%)
(2.5 (2.5 BillionBillion yearsyears ago): ago): Fe (Fe (−−4%) + Ni 4%) + Ni ((−−0.8%) =0.8%) = =Al=Al (+1%) + Si (+2.4%) + C (+1.4%)(+1%) + Si (+2.4%) + C (+1.4%)
Tectonic plate formationTectonic plate formation
Most severe tectonic activityMost severe tectonic activity
IronIron depletiondepletion vsvs CarbonCarbon pollutionpollution
Ni (~ 0.8%) Ni (~ 0.01%)Ni (~ 1%)
Al (~ 8%)
Al (~ 4%) Al (~ 7%)
Fe (~ 8%)
Fe (~ 4%)
Fe (~ 15%)
Si(~ 24%)
Si (~ 26%)Si (~ 28%)
3.5 2.5 1.5 00.54.50
5
10
15
20
25
30
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3.8 3.8 BillionBillion yearsyears ago: ago: Ca (Ca (−−2.5%) + Mg(2.5%) + Mg(−−3.2%) = 3.2%) = = K (+1.4%) + = K (+1.4%) + NaNa (+2.1%) + O (+2.2%)(+2.1%) + O (+2.2%)
2.5 2.5 BillionBillion yearsyears ago: ago: Ca (Ca (−−1.5%) + Mg(1.5%) + Mg(−−1.5%) = 1.5%) = =K=K (+1.3%) + (+1.3%) + NaNa (+0.6%) + O (+1.1%)(+0.6%) + O (+1.1%)
Great Oxidation Event & Origin of Life
CalciumCalcium depletiondepletion vs vs OceanOcean formationformation
Na(~ 2.9%)
0
1
2
3
4
5
4.5 3.5 2.5 1.5 0.5 0
K (~ 1.5%)
K (~ 2.8%)Na(~ 2.3%)
Ca (~4.5%)
Mg(~ 2.8%)
Mg(~ 1.3%)
6
7
Mg(~ 6%)
Ca (~ 3%)
Ca (~ 7%)
8
Na(~ 0.2%)K (~ 0.08%)
Alkaline & Alkaline-Earth Elements
Na(~ 2.9%)
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Materials● Luserna stone
● Basalt
● Magnetite
● Mortar enriched with iron dioxide
● Carrara marble
● Gypsum
● Steel
ExperimentalExperimental investigationinvestigation
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Compression tests under monotonic displacement control
Cyclic loading 2 Hz
Ultrasonic vibration20 kHz
Cyclic loading 200 Hz
Uniaxil tensile tests
Different Testing Modalities in the Experimental Investigation
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Granite (Fe ∼ 1.5%)
Neutron emission from Neutron emission from cavitationcavitation in liquids in liquids and fracture in solidsand fracture in solids
Basalt (Fe ∼ 15%)
Magnetite (Fe ∼ 75%)
Marble
LIQUIDS − Cavitation
NEUTRON EMISSION
Iron chloride
SOLIDS − Fracture
101 times the Background Level
2.5 times the Background Level
up to
102 times the Background Levelup to
103 times the Background Levelup to
up to
Background Level
MATERIAL
Steel 2.5 times the Background Levelup to
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The equivalent neutron dose, at the end of the test on basaltic The equivalent neutron dose, at the end of the test on basaltic rock, was rock, was 2.62 2.62 ±± 0.53 0.53 mSv/hmSv/h (Average Background Dose = 41.95 (Average Background Dose = 41.95 ±± 0.85 0.85 nSv/hnSv/h).).
Effective Neutron DoseEffective Neutron Dose Average Background DoseAverage Background Dose≅≅5050
Cyclic Loading Experiments on Basaltic Rocks
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• Volodichev, N.N., Kuzhevskij, B.M., Nechaev, O. Yu., Panasyuk M., and Podorolsky M.I., “Lunar periodicity of the neutron radiation burst and seismic activity on the Earth”, Proc. of the 26th International Cosmic Ray Conference, Salt Lake City, 17-25 August, 1999.
Neutron emission from earthquakesNeutron emission from earthquakes
• Sigaeva, E., Nechaev, O., Panasyuk, M., Bruns, A., Vladimirsky, B. and Kuzmin Yu., “Thermal neutrons’ observationsbefore the Sumatra earthquake”, Geophysical Research Abstracts, 8: 00435 (2006).
• Sobolev, G.A., Shestopalov, I.P., Kharin, E.P. “Implications of Solar Flares for the Seismic Activity of the Earth”. Izvestiya, Phys. Solid Earth 34: 603-607 (1998).
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Neutron flux up to 100 cm–2 s–1 (103 times the background level) was detected in correspondence to earthquakes with a magnitude of the 4th degree in Richter Scale (Volodichev N.N., et al. (1999)).
Seismic activity and neutron flux measurements in the period 1975-1987, Kola Peninsula, Russia (Sobolev et al. 1998).
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Earthquake Preparation ZoneEarthquake Preparation Zone
R =100.433M+0.60 km (*)
(*) Dobrovolsky I. P., Zubkov S. I., Miachkin V. I., (1979) "Estimation of the size of earthquake preparation zones" Pure and Applied Geophysics Volume 117, Issue 5, pp 1025-1044.
● Sumatra 2004 (M = 9.2)
● Chile 2010 (M = 8.8)
● Japan 2011 (M = 9.0)
L’Aquila Earthquake 2009
R
Earthquake preparation zoneEarthquake preparation zone
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Monitoring of a gMonitoring of a gypsumypsum mine in mine in MurisengoMurisengo ((ItalyItaly))
The mine is structured in five levels and a pillar located at about 100 meters below the ground level has been subjected to a multi-parameter monitoring since July 1st , 2013.
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f (Hertz)
λ (Metre)
1012 109 106 103 100
10310010 −610 −9 10 −3
HumansInsectsProteins Bacteria Earthquakes
wave velocity = λ × f ≈ 103 m s–1
Wavelength Wavelength vsvs FrequencyFrequency
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Energy vs Energy vs FrequencyFrequency
VibrationalVibrational Energy Energy vsvs VibrationalVibrational FrequencyFrequencyin the in the AtomicAtomic Lattice Lattice
E = h × f
0.025 eV = (4.13 ×10–15) eVs × (6.05 × 1012) s–1
(1) (1) TeraHertzTeraHertz phononsphonons presentpresent anan energyenergy equivalentequivalent toto thatthat of of thermalthermal neutronsneutrons
(2) TeraHertz phonons present a frequency equivalent to the (2) TeraHertz phonons present a frequency equivalent to the Debye frequency (atomic lattice resonance at 4.79 THz Debye frequency (atomic lattice resonance at 4.79 THz forfor CaCa, , 6.24 6.24 THzTHz forfor U, and 7.77 U, and 7.77 THzTHz forfor FeFe))
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FractoFracto--emissions measurementemissions measurement
Acoustic Emission(kHz – MHz)
PZT TRANSDUCER
Electromagnetic Emission(MHz – GHz)
TELESCOPIC ANTENNA
Neutron Emission(GHz – THz)
NEUTRON DETECTOR
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Seismic activity: July 1st, 2013 – December 31, 2015, within a distance ≤ 100 km
MURISENGO
242 earthquakes with a magnitude ≥ 1.8 (Richter)
31 seismic swarms (epicentre magnitude 2.5 – 4.7)
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EARTHQUAKE MULTI-MODAL ANALYSIS (First Sem. 2015)
0 15 30 45 60 75 90 105 120 135 150 165 1800,01,5
2,0
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5,0FIRST SEMESTER - YEAR 2015
Mag
nitu
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Days
EarthquakesEp
icen
tre
Mag
nitu
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AE MULTI-MODAL ANALYSIS (First Sem. 2015)
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100FIRST SEMESTER - YEAR 2015
Aco
ustic
Em
issi
on R
ate
(AE/
day)
Days
Acoustic Emission Rate
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EME MULTI-MODAL ANALYSIS (First Sem. 2015)
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E M
ON
ITO
RIN
G
FIRST SEMESTER - YEAR 2015El
ectr
omag
netic
Em
issi
on R
ate
(EM
/day
)
Days
EM Emission Rate
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NE MULTI-MODAL ANALYSIS (First Sem. 2015)
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3
4
5
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7
8FIRST SEMESTER - YEAR 2015
Neu
tron
Flu
x (X
103 c
m−2
day
−1)
Days
NEUTRON FLUX
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AE vs EARTHQUAKES (Second sem. 2013)
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Earthquakes distribution
Aco
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ate
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Days
AE distribution
Epic
entr
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6,5FIRST SEMESTER - YEAR 2014
Aco
ustic
Em
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ate
(AE/
day)
Days
AE distribution
Mag
nitu
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Earthquakes distribution
Epic
entr
eM
agni
tude
AE vs EARTHQUAKES (First sem. 2014)
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180 195 210 225 240 255 270 285 300 315 330 345 3600,01,5
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agni
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Earthquakes distribution
SECOND SEMESTER - YEAR 2014
Aco
ustic
Em
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ate
(AE/
day)
AE distribution
Epic
entr
eM
agni
tude
AE vs EARTHQUAKES (Second sem. 2014)
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0 15 30 45 60 75 90 105 120 135 150 165 1800,01,5
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140FIRST SEMESTER - YEAR 2015
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Earthquakes distribution
Aco
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Em
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ate
(AE/
day)
AE distribution
Epic
entr
eM
agni
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AE vs EARTHQUAKES (First sem. 2015)
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180 195 210 225 240 255 270 285 300 315 330 345 3600,02,0
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240M
agni
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Earthquakes distribution
SECOND SEMESTER - YEAR 2015
Aco
ustic
Em
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ate
(AE/
day)
AE distribution
Epic
entr
eM
agni
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AE vs EARTHQUAKES (Second sem. 2015)
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O E
ME
MO
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ING
FIRST SEMESTER - YEAR 2015
Elec
trom
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tic E
mis
sion
Rat
e (E
M/d
ay) EM distribution
Epic
entr
eM
agni
tude
EME vs EARTHQUAKES (First sem. 2015)
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180 195 210 225 240 255 270 285 300 315 330 345 3600,0
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20SECOND SEMESTER - YEAR 2015
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trom
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tic E
mis
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Rat
e (E
M/d
ay)
EM distribution
Epic
entr
eM
agni
tude
EME vs EARTHQUAKES (Second sem. 2015)
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180 195 210 225 240 255 270 285 300 315 330 345 3600,0
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SECOND SEMESTER - YEAR 2013
Mag
nitu
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Earthquakes distribution
Neu
tron
Flu
x (X
103 c
m−2
day
−1)
Days
Neutron distribution
Epic
entr
eM
agni
tude
NE vs EARTHQUAKES (Second sem. 2013)
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6,5
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8
25
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40M
agni
tude
Earthquakes distribution
FIRST SEMESTER - YEAR 2014
Neu
tron
Flu
x (X
103 c
m−2
day
−1)
Days
Neutron distribution
Epic
entr
eM
agni
tude
NE vs EARTHQUAKES (First sem. 2014)
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180 195 210 225 240 255 270 285 300 315 330 345 3600,01,5
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12M
agni
tude
Earthquakes distribution
SECOND SEMESTER - YEAR 2014
Neu
tron
Flu
x (X
103 c
m−2
day
−1)
Days
Neutron distribution
Epic
entr
eM
agni
tude
NE vs EARTHQUAKES (Second sem. 2014)
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0 15 30 45 60 75 90 105 120 135 150 165 1800,01,5
2,0
2,5
3,0
3,5
4,0
4,5
5,0
5,5
6,0
6,5
0 15 30 45 60 75 90 105 120 135 150 165 1800,03
4
5
6
7
8
9
10M
agni
tude
Days
Earthquakes distribution
FIRST SEMESTER - YEAR 2015
Neu
tron
Flu
x (X
103 c
m−2
day
−1)
Neutron distribution
Epic
entr
eM
agni
tude
NE vs EARTHQUAKES (First sem. 2015)
![Page 32: Nanomechanics Instabilities and TeraHertz Vibrations: From ...staff.polito.it/alberto.carpinteri/piezonuclear reactions conference/Carpinteri... · SEM 2017 Annual Conference & Exposition](https://reader033.vdocument.in/reader033/viewer/2022041421/5e1f09a03c5626446e15ed1e/html5/thumbnails/32.jpg)
180 195 210 225 240 255 270 285 300 315 330 345 3600,02,0
2,5
3,0
3,5
4,0
4,5
5,0
5,5
6,0
6,5
180 195 210 225 240 255 270 285 300 315 330 345 3603
4
5
6
7
8
36
37
38
Mag
nitu
de
Days
Earthquakes distribution
SECOND SEMESTER - YEAR 2015
Neu
tron
Flu
x (X
103 c
m−2
day
−1)
Neutron distribution
Epic
entr
eM
agni
tude
NE vs EARTHQUAKES (Second sem. 2015)
![Page 33: Nanomechanics Instabilities and TeraHertz Vibrations: From ...staff.polito.it/alberto.carpinteri/piezonuclear reactions conference/Carpinteri... · SEM 2017 Annual Conference & Exposition](https://reader033.vdocument.in/reader033/viewer/2022041421/5e1f09a03c5626446e15ed1e/html5/thumbnails/33.jpg)
80 85 90 95 100 105 110 115 120 125 1300,0
2,0
2,5
3,0
3,5
4,0
80 85 90 95 100 105 110 115 120 125 13005101520253035404550556065
April 11, 2015 - Earthquake M=3.2
Mag
nitu
de
Days
Earthquakes distribution
Aco
ustic
Em
issi
on R
ate
(AE/
day)
AE distribution
Epic
entr
eM
agni
tude
Shifting of the three Shifting of the three fractofracto--emissionsemissions
![Page 34: Nanomechanics Instabilities and TeraHertz Vibrations: From ...staff.polito.it/alberto.carpinteri/piezonuclear reactions conference/Carpinteri... · SEM 2017 Annual Conference & Exposition](https://reader033.vdocument.in/reader033/viewer/2022041421/5e1f09a03c5626446e15ed1e/html5/thumbnails/34.jpg)
80 85 90 95 100 105 110 115 120 125 1300
1
2
3
4
5
6
7
80 85 90 95 100 105 110 115 120 125 1300,01,5
2,0
2,5
3,0
3,5
4,0
El
ectro
mag
netic
Em
issi
on R
ate
(EM
/day
) EME distribution
April 11, 2015 - Earthquake M=3.2 M
agni
tude
Days
Earthquakes distribution
Epic
entr
eM
agni
tude
![Page 35: Nanomechanics Instabilities and TeraHertz Vibrations: From ...staff.polito.it/alberto.carpinteri/piezonuclear reactions conference/Carpinteri... · SEM 2017 Annual Conference & Exposition](https://reader033.vdocument.in/reader033/viewer/2022041421/5e1f09a03c5626446e15ed1e/html5/thumbnails/35.jpg)
80 85 90 95 100 105 110 115 120 125 1300,01,5
2,0
2,5
3,0
3,5
4,0
80 85 90 95 100 105 110 115 120 125 1300
3
4
5
6
7
8April 11, 2015 - Earthquake M=3.2
Mag
nitu
de
Days
Earthquakes distribution
N
eutr
on F
lux
(X 1
03 cm
−2 d
ay−1
)
NE distribution
Epic
entr
eM
agni
tude
![Page 36: Nanomechanics Instabilities and TeraHertz Vibrations: From ...staff.polito.it/alberto.carpinteri/piezonuclear reactions conference/Carpinteri... · SEM 2017 Annual Conference & Exposition](https://reader033.vdocument.in/reader033/viewer/2022041421/5e1f09a03c5626446e15ed1e/html5/thumbnails/36.jpg)
0 1 2 3 4 5 6 7 8 9 1010
100
1000
10000 AE Rate vs. MagnitudeA
cous
tic E
mis
sion
Rat
e (A
E/da
y)
Local Magnitude in Murisengo
FractoFracto--emissionemission peak peak intensityintensity vsvsearthquakeearthquake locallocal magnitudemagnitude
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0 1 2 3 4 5 6 7 8 9 101
10
100EME Rate vs. Magnitude
Elec
trom
agne
tic E
mis
sion
Rat
e (E
ME/
day)
Local Magnitude in Murisengo
![Page 38: Nanomechanics Instabilities and TeraHertz Vibrations: From ...staff.polito.it/alberto.carpinteri/piezonuclear reactions conference/Carpinteri... · SEM 2017 Annual Conference & Exposition](https://reader033.vdocument.in/reader033/viewer/2022041421/5e1f09a03c5626446e15ed1e/html5/thumbnails/38.jpg)
0 1 2 3 4 5 6 7 8 9 1010-510-410-310-210-1100101102103104105106107108109
10101011
Earthquake Magnitude 4.8Garfagnana(Local Magnitude) in Bettola 2.6)
Earthquake Magnitude 4.7Mentone(Local Magnitude) in Murisengo 2.3)
Earthquake Magnitude 9(1010 n cm−2s−1)
Earthquake Magnitude 4(Pamir)
Neutron Fluence Rate vs. MagnitudeN
eutr
on F
luen
ce R
ate
(cm
−2s−1
)
Local Magnitude in Murisengo
![Page 39: Nanomechanics Instabilities and TeraHertz Vibrations: From ...staff.polito.it/alberto.carpinteri/piezonuclear reactions conference/Carpinteri... · SEM 2017 Annual Conference & Exposition](https://reader033.vdocument.in/reader033/viewer/2022041421/5e1f09a03c5626446e15ed1e/html5/thumbnails/39.jpg)