obrien & gere - technical memorandum - waste …re: waste characterization technical memorandum...

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OBRIEN G GERE

May 28, 1985

Mr. Jack BraunU.S.E.P.A.Region V, 5HE-12230 South Dearborn St.Chicago, Illinois 60604

Re: Waste CharacterizationTechnical MemorandumCliffs-Dow Disposal Site

File: 3071.001

Dear Mr. Braun:

Attached, please find our report on the nature of the waste materialspresent within the Cliffs-Dow disposal site in Marquette. This reportis being submitted as a deliverable under Tasks 2.1 through 2.3 of theEPA Work Plan, EPA 104.5 IE 7.0. We have scheduled the Waste Charac-terization and Work Plan Review Meeting to take place in Marquette onJune 4, 1985. If you have any questions or comments regarding thisreport;, please bring them to my attention prior to the meeting.

I am looking forward to our meeting and continued progress during thefield activities in June.

Very truly yours,

O'BRIEN & GERE ENGINEERS, INC.

Swiatoslav W. Kaczmar, Ph.D.Environmental Toxicologist

SWK:djb

cc: Mr. Richard Taszreak,Mr. Jerry BillsMr. William WittMr. Steven CorrellMr. William LehmanOr. Edwin TifftDr. Cornelius Murphy

C'Brien i Gero Engineers. Inc.Box .-:87 ;, / 1 304 Buckley Road ' Syracuse. NY 1 3221 / (31 5) 451 -4700B i,e Bel PA • Boston, MA / Landover. MD / New Yoik, NY / St. Louis. MO ' White Plains. NY

Chemical Characterization Memorandum

O'Brien & Gere Engineers, Inc.May 22, 1985

IntroductionDuring the period of November 26 - December 7 of 1984, a series of

exploratory borings were conducted within the boundaries of the Cliffs-Dow disposal site in Marquette, Michigan. A total of five (5) boringswere completed and sampled using split spoon sampling techniques. Theborings originated at the surface of the site and proceeded through thewaste fill until a clean sand layer was reached. The average boringdepth was 10 feet. The general locations of the borings are indicatedin Figure 1. A total of fifteen (15) samples (three from each boring)were collected from the site and submitted to the O'Brien & Gere Labo-ratory for analysis. Several of the samples were split between theRespondents' contractor (O'Brien & Gere), the Respondents' laboratory(Dow Chemical Company), the United States Environmental ProtectionAgency (USEPA) and the Michigan Department of Natural Resources (MDNR).The reader is referred to the site "Interim Technical Memorandum" for afull description of the sampling activities.

The site is reported to have been used for the disposal of wastematerials related to the production of charcoal. Hardwoods harvestedfrom Michigan's Upper Peninsula were transported to a plant located inMarquette where they underwent pyrolysis, were ground up, mixed with abinder and shaped into charcoal briquettes. Wastes which may have beengenerated by this process would include incompletely pyrolyzed woodfragments, leftover charcoal dusts, off-grade product batches, and woodtars and resins. Chemical components of these wastes were for the mostpart carbon in the form of charcoal, and may have also included thelower alcohols and aldehydes; low molecular weight aromatics such asbenzene, toluene, xylene, phenols, guaiacols; and condensed aromaticcompounds generally referred to as polynuclear aromatic hydrocarbons.1

The purpose of the sampling effort was to collect a set of samplesrepresentative of the range of materials deposited within the site andsubmit them for chemical characterization. The objective of characteri-zation of the waste material was to identify its major potentiallyhazardous components. These components would then be used as indicatorsof contamination in samples of soil and groundwater collected at off-site locations. They would also serve as parameters for field screeningof future samples.

*The Chemical Technology of Wood. Wenzl, Hermnan F., Academic Press,New York, 1970.

MethodsCharacterization of waste materials was conducted using November,

1984 USEPA Contract Laboratory Protocols (CLP) as a framework. The WorkPlan specified USEPA CLP's dated January, 1983. Those protocols havesince been superceded by protocols issued in November, 1984. It shouldbe noted that there is currently no procedure under the CLP program de-signed for the analysis of highly concentrated wastes. Nevertheless,the CLP protocols were followed with appropriate modification. Analysisof waste materials for inorganics was conducted according to CLP protocolsdated May, 1982.

The materials were initially extracted and put through the GCscreening protocol outlined in the CLP procedure for organics. Based onthe screening results, an appropriate weight of sample was subjected tofurther analyses. The analytical determinations consisted of six cate-gories: 1) Inorganics, 2) Volatiles, 3) Acid Extractables, 4) BaseNeutrals, 5) Priority Pollutant Pesticides and PCBs, and 6) 2,3,7,8-tetrachlorodibenzo-p-dioxin (2,3,7,8-TCDD).

The volatile components of the waste materials were analyzed by apacked-column gas chromatographic technique employing two detectorsconnected in series. Effluent from the gas chrcmograph eluted through aphotoionization detector connected in series to a Hall electrolyticconductivity detector. Samples which were screened and determined tocontain low level contamination were analyzed by placing 1 gram ofsample into 5 ml of pre-purged distilled water, spiked with bromochloro-methane, stripped from solution at ambient temperature by purge and traptechniques, and desorbed for gas chromatographic quantisation using thepreviously described dual detector technique. Samples identified ascontaining medium level contamination were handled by dissolving a1 gram aliquot in isopropanol, transferring and dissolving a measuredaliquot in 5 ml of purged distilled water, and analyzed by the purge andtrap gas chromatographic technique used for the low level samples.

The priority pollutant pesticide and PCB analyses were conductedaccording to the CLP protocols for organics. The sample extracts wereinjected for gas chromatographic-electron capture detection withoutfurther clean-up. Samples which could not be quantitated at a limit ofdetection of 1 mg/kg due to the presence of interferences were putthrough florisil clean-up and reinjected.

The base neutral and acid extractable fractions were spiked andanalyzed according to CLP protocols. The base neutral extracts were notcombined with the acid extractable portions, but were injected as separatesamples. Due to the concentrated nature of some of the extracts, thefinal volume of most of the extracts was set at 10 ml as opposed to the1 ml specified by the procedure. Additionally, some of the extractionswere initiated using only 0.5 g of sample.

The 2,3,7,8-TCDD analyses were performed according to current CLPprotocols for the determination of 2,3,7,8-TCDD in soils and sediments.An internal standard consisting of 50 ng of 1,2,3,4-TCDD was used tocorrect for sample recovery. Ions of nominal masses 320, 322 and 257were monitored and used as a basis for quantisation as well as identi-fication.

ResultsResults of the analyses are tabulated in Tables 1 through 6. All

results are reported on a wet weight basis. Additionally, laboratorydata reporting sheets are contained in the appendix. The tabulatedresults present only those components which were detected in the wastesamples. Results for all compounds analyzed, including those not de-tected in the mixture at method detection limits, are listed in the datasummary sheets.

Inorganics:Results of analyses of the waste materials for the presence of

hazardous substance list metals are presented in Table 1. Of themetals included in the analytical protocol, only arsenic, chromium,copper, lead, mercury, nickel and zinc were detected at levelsabove method detection limits. Of these metals, copper was foundin the greatest relative abundance with residues ranging from 7 to580 mg/kg (ppm) followed by zinc, which ranged from 6 to 440 mg/kg,lead (<1 to 110 mg/kg), chromium (<1 to 12 mg/kg), arsenic (1.3 to4.1 mg/kg) and mercury (0.13 to 2.82 mg/kg).

Volatiles:Results of the volatiles determinations are listed in Table 2.

The results indicate the major volatile components of the wastes tobe benzene, toluene, ethylbenzene and xylene. In addition, a

smaller amount of tetrachloroethene was detected in two of thesamples analyzed. The volatile component present at the highestconcentration was xylene. It was present at a level of 320 mg/kgin sample B-l"-2". This sample was a tar present at a 2-inchthickness at the top of Boring B. The volatiles were present inthe descending concentrations of xylene > ethylbenzene > toluene> benzene.

Priority Pollutant Pesticides and PCBsThere were no priority pollutant pesticides or PCBs detected

in any of the samples at a limit of detection of 1 mg/kg.

Acid Extractable Priority PollutantsTable 4 is a compilation of results of the acid extractable

priority pollutant analyses. The acid extractable componentsdetected in the waste materials were phenol, 2-methyl phenol, 4-methyl phenol and 2,4-dimethyl phenol. In general, all fourcompounds were detected in most of the samples analyzed. Phenoland 4-methyl phenol were present at higher levels than 2-methylphenol and 2,4-dimethyl phenol. The measured concentrations rangedfrom 100 ug/kg to about 900 mg/kg.

Base Neutral Extractable Priority PollutantsTable 5 lists the results of the base neutral priority pollu-

tant determinations. Components most commonly detected werenaphthalene, 2-methylnaphthalene, dibenzofuran, phenanthrene andfluorene. Small amounts of the higher molecular weight PNAs suchas benzo(a)anthracene or benzo(a)perylene were also present in someof the samples.

2,3,7,8-Tetrachlorodibenzo(p) dioxinAnalytical determinations conducted into the presence of

2,3,7,8-TCDD in the waste materials indicated the wastes to containno 2,3,7,8-TCDD at a limit of detection of 1 ug/kg. •

DiscussionResults of the waste characterizations indicate that major hazardous

substance list components of the waste materials deposited at the siteare the phenols as phenol, 2 and 4 methyl phenol and 2,4-dimethyl phenol;and base neutral extractable aromatics as naphthalene, 2-methylnaphthalene,dibenzofuran and phenanthrene. Two samples also contained the volatilearomatic compounds benzene, ethylbenzene, toluene and xylene. Thesamples which contained volatile residues were tarry in nature, whilethe remaining samples could be described as being more similar to charcoalor peat than to tars. Some samples also contained the heavy metalscopper, zinc, lead and mercury at levels higher than normally encounteredin soils. However, these levels may be typical to this mineral mining area.

The results of the characterizations identify residues consistentwith the reported source of the waste materials. Hardwood charcoalwastes typically contain substituted phenols and lower molecular weightcondensed aromatics such as naphthalene, dibenzofuran and phenanthrene.2The consistent identification of the same components in most of thesamples and the absence of waste components inconsistent with a charcoalproduction waste also rule out the site as a depository for wastes notassociated with the production of charcoal.

It can be concluded that the waste is relatively homogeneous andarose from a single process. With the exception of two small depositsof tarry material observed at boring samples B l"-2" and C 6'-8', theboring and characterization program revealed that most of the wastedeposited within the site is not a concentrated wood tar, but is com-posed of a mixture of charcoal, incompletely pyrolyzed wood fragmentsand charcoal kiln residues.

Recommendations for ScreeningThe Work Plan developed for the site specifies that samples of soil

and groundwater generated during drilling of new monitoring wells bescreened in the field for major components identified during the wastecharacterization. The components identified in the characterization arerelatively volatile, non-halogenated aromatic compounds. Althoughfavorable under certain circumstances, compound-specific screening forthe waste components identified may not be the method of choice in this

Chemical Technology of Wood

! situation. The components can be effectively sampled and detected as amixture in the vapor state by the following technique:

1) Collect approximately 15 grams of soil or water.2) Place into a 30 ml teflon-capped vial and heat in a water bath

at 40oc for 15 minutes.( 3) Shake the vial for 20 seconds, then carefully uncap and

immediately sample the headspace with a calibrated Century| organic vapor analyzer or a Photo-vac unit.l

4) Record the resultant readout from the instrument.; This technique is favored over a field gas or liquid chromatographic

technique because it samples and analyzes all volatile and semi-volatilej components in the sample headspace. It thereby allows a lower limit of1 sensitivity because it quantitates the components simultaneously. In;- this manner, all components of interest can be screened without requir-i-. ing extraction, concentration and manual quantitation. Elimination of

extraction and concentration as well as long chromatographic elution! times reduces the analysis time significantly. Turn-around time of

field screening is often a critical factor which delays drillingchedules. It is conceivable that if the laboratory is situated near thefield site, the procedure should not cause the advancement of drillingto be slowed down significantly.

r

r

Waste CharacterizationMemorandumCliffs Dow Disposal AreaMarquette, Michigan

L May 1985

O BRIEN 5 GERE

TABLE 1

Priority Pollutant Metals Detected

Sample

A-lA 6'-8'A 8'-10'B l"-2"B 2'-5'B 6'-6.5'C 4 '-6'C 6'-8'C 8'-10'D l'-3'C 3 '-4D 6'-8!

E 0 -2E 3 '-4'E 6 '-9'

% Solids

58.957.731.2

49.884.576.7—67.087.664.879.072.551.254.0

As

4.12.02.21.91.71.33.4—3.11.43.32.91.53.12.6

Cr

117865<19—8571210129

Cu

580230254300547

\

190—58520058098542357160

Pb

11075302033<147--30151090206025

Hq

1.731.520.450.152.820.130.65—0.210.250.480.410.180.730.41

Ni

15101069<116—10<124'1113713

Zn

370270803236680—601314044080160120

All results reported as mg/kg on a wet weight basis

TABLE 2

Summary of Purgeable Priority Pollutants Detected

Sample Benzene Ethyl benzene Toluene Xylenes Tetrachloroethene

A-l <10 <10 <10 <10 <10A 6'-8' <10 <10 <10 29 <10A 8'-10.' <10 <10 <10 <10 <10B l"-2" 660 83,000 16,000 320,000 <100B 2'-5' <10 <10 <10 <10 <10B 6'-6.5' <10 <10 <10 <10 <10C 4'-6' <10 <10 <10 <10 <10C 6'-8'C 8'-10' 140 3,900 3,500 10,000 490D l'-3' <10 <10 <10 18 <10D 3'-4' <10 <10 <10 <10 <10D 6'-8' <10 <10 <10 16 <10E 0 -2' <10 <10 <10 <10 <10E 3'-4' <10 <10 <10 <10 21E 6'-9' <10 <10 <10 <10 <10

All results reported as ug/kg on a wet weight basis.

TABLE 3

Priority Pollutant/PCB Summary

No priority pollutant pesticides or PCBs were detected inany sample at a method sensitivity limit of 1.0 nig/kg.

i...

TABLE 4

Summary of Acid Extractable Compounds Detected

Sample

A-lA 6'-8'A 8 '-10'B l"-2"B 2 '-5'B 6--6.51

C 4'-6'C 6'-8'C-8-10D l'-3'D 3 '-4'D 3 '-4'(Duplicate)D 3'-4'(Duplicate)D 6'-8'E 0 -2E 3'-4'E 6 '-9'

Phenol

1,2203,51012,350

ND3,300

88ND

894,000--

12,8602,875

199,300

216,500

9,33042

ND4,440

2-Methyl phenol

1,0502,9208,3403,2502,110ND804

• 540,000—3,7661,29078,300

76,930

3,19094107

3,420

4-Methyl phenol

2,2208,97019,8202,8704,250

631,070

892,000—9,4203,250

174,300

180,000

8,36051

ND10,700

2-4 Dimethyl phenol

2,0703,9309,0403,9901,300ND1,260

612,000—

2,0572,12323,500

35,330

1,890ND116

3,200


TABLE 5

Summary of Base Neutral Compounds Detected

Sample Naphthalene

A-l 6,000A G'-O' 3,450A B'-IO1 1,410B l"-2" 724,600B 2'-5' 6,410B 6'-6.5' NDC 4'-6' 1,200C G'-8' 266,000C 8'-10'D l'-3' 6,230D 3'-4' 2,150D 6'-8' 4,640E 0 -2' NDE 3'-4' 7,300E 6'-9' 4,400

flnaphthalem4,340ND1,780

501,7005,240ND892

300,000

47,9002,80010,300

1287,6603 ,800

Page 1 of 2

2 Acenaphthene1,860NDND

13,600NDNDNDND

NDNDNDNDND1,800

Dibenzofuran

4,0605.6902,50019,200

582NDND

120,000

12,800NDNDND3,5902,400

Fluoranthene

7801,280779NDNDND200ND

NDNDNDNDND420

Indcno (1,2,3) Pyrene

NDNDNDNDNDND150ND

NDNDNDNDNDND

All results reported as ug/kg on a wet weight basis,

TABLE 5

Summary of Base Neutral Compounds DetectedPage 2 of 2

Dibenz (a)Sample Anthracene

A-lA 6'-8'A 8'-10'B l"-2"B 2'-5'B 6--6.51

C 4 '-6'C 6'-8'C 8'-10'D r-31

D 3'-4'D 6'-8'E 0 -2'E 3'-4'E 6'-9'

NDNDNDNDNDND102ND—NDNDNDNDNDND

Benzo (gh1)Perylene

NDNDNDNDNDND298ND—NDNDNDNDNDND

Phena;nthrene

1,8005,340888ND

1,160NDND

112,000--ND737

4,000102

3,8801,700

Pyrene

i 810790488NDNDND193

15,600—NDND

1,130ND462520

Chrysene

850NDNDNDNDNDND

11,700—NDNDNDNDNDND

Fluorene

4,2006,3302,440ND1,200NDNDND—ND575

NDNDND3,100

Benzo (a)Anthracene

930ND454NDNDNDNDND—NDNDNDND649ND

Anthracene

4,160NDNDNDNDND829

ND--NDNDNDNDND3,200


TABLE 6

Summary of 2,3,7,8-TCDD Determinations

No 2,3,7,8-TCDD detected in any sample at a methoddetection limit of I vg/kg.

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O'Orion & Gere Engineers, Inc.fijx 4U/J / 1304 Uuvkfcfy Rj / Syracuse. NY / 13221 / (315) -151-4700

OERIEN5GEF1E

rL,PNT DOlJ

Hesiiciae/ruDPriority Pollutants

jnauo ,?O7/, OO/>St~7

DESCRIPTION C.OO ("^ donPO^(. ( L_- n ~~ 1

SAMPLE NO. o522L l DATE COLLECTED DATE REC'D. DATE ANALYSED ^7~^2-^S~

ff-BHC ^/

X-BHC

Heptachlor

<J-SHC

Aldrin

Heptachlor Epoxide

Endosulfan 1

4,4'-DDE

Dieldrin

Endrin

4,4'-DDD

|, Endosulfan II ^X' ^

4.4'-ODT !- .

Endosulfan Sulfate

Endrin Aldehyde . ' • ) . • ' . /

Chlordane 1

Toxaphene ; i1

PCB-1221 |

PCS-1232 '' ' ;. ' . . . " . . ' - - / •

PCS-1016/1242 /

pcs-1248 ; ./.,:."o^p -• •-. ^--j-;:. :-•"-- ': PCS-1254 j

PCS-1260 . - .:/ ;

Mathodology: Federal Register — 40 CFR, Part 136, DecemBer 3, 1979

Comments:

n

O'Brien 4 Gere Engineers, Inc.Box 4873 / 1304 Buckley Rd. / Syracuse, NY / 13221 / (315) -451-47CO

Authorized:

Date:

' Pesticide/PCBPriority Pollutants

CLIENT.

DESCRIPTION _ fl-2. 6 -.JOB NO. . 001. St

SAMPLE NO. ._)5Z2_S_DATE COLLECTED. .DATE HEC'D. .DATE ANALYZED ..H ~

cr-BHC

y-BHC

/J-BHC •

Heptachlor

<5-BHC

Aldrin

Heptachlor Epoxide

Endosulfan I

4,4'-DDE

Dieldrin

Endrin

4,4'-CDD

Xk. Endosulfan II

4.4'-DDT _ .

Endosulfan Sulfate

Endrin Aldehyde

Chlordane

Toxaphene - _

PCS-1221

PCB-1232_ _ _

PCS-1016/1242„ _I ___ ^^ ____, ___-_„ »———«.

PCS-1248__ ._ :'

I PCS-1254

PCS-1260

Methodology: Federal Register — 40 CFR. Part 136. December 3. 1979

Comments:

n £~T(46x, T'Cl-f

Authorized:O'Brien 4 Gere Engineers, Inc.Box 4873 / 1304 Buckley Rd. / Syracuse. NY / 13221 / (31S) 451-4700

OBniENCGERE

CLIENT.

DESCRIPTION.

Priority Pollutants

JOB NO.

SAMPLE NO..

a-BHC

y-BHC

.DATE COLLECTED.

Heptachlor

(5-BHC

Aldrin

Heptachlor Epoxide

Endosulfan t

PPb

4,4'-DDE

Dieidrin

Endrin

4.4'-DOD

... ..:.....;. _.;_...-... J. ...:-.._^,,

" ~ ' / / .' ...'-.;...__. _ .. ... ',/.. ;/...// . •ijj^-Li

.DATE ANALYZED

ppb

Endosulfan II

4.4--ODT _ ,_ ^

Endosulfan Sulfate

Endrin Aldehyde

Chlordane

Toxaphene

PCS-1221

PCB-1232_ __

PCS-1016/1242

PCS-1248_^ .

PCS-1254

PCS-1260

Mathodology: Federal Register — 40 CFR, Part 136. December 3, 1979

Comments: /

f r>t,*

C

O'Brien & Gere Engineers, Inc.Box 4373 / 1304 Buckley Rd. / Syracuse. NY / 13221 / (315) 451-4700

Authorized:.

OBRIENCGERE Priority Pollutants

DoiO 3071nwnIBTlnN ft 1 -

SAMPIPNn 3vC>227 DATE COl L FCTED

cr-BHC </.

y-BHC

0-BHC •

Heptachlor

5-BHC

Aldrin

Heptachlor Epoxide

Endosulfan 1

4,4'-DDE

Oieldrin

Endrin • . • . .

4.4'-ODD

2 "

DATE BFC'n DATE ANALYZED ^ ~ 2 ~^S

|. Endosulfan II j/. \

4.4'-DDT '. . - - . .

Endosulfan Sulfate

Endrin Aldehyde .

Chlordane

Toxaphene ; \_

PCB-1221

PCS-1232 ' \ -^.,. :-'." . - I

PCS-101 6/1 242

PCS-1248 ,; .: :'-'::':•--' •-. ^ •- ••"^IT " "•: PCS-1254 ' I

PCS-1260 - -. -: ' - ;\l/ •' .' :

Methodology: Federal Register — 40 CFR. Part 136. December 3, 1979

Comments:

O'Brien & Gers Engineers, Inc.Box 4873 / 1304 Buckley Rd. / Syracuse. NY / 13221 / (315) 451-4700

Aulrtortzed:

Oat«:

[mm OBRlENSGEnE' Pesticide/PCB

Priority Pollutants

DESCRIPTION

SAMPiPiun "3~53~S-5 OATE ro t ter

<r-BHC

X-BHC

Heptachlor

5-BHC

Aldrin

Heptachlor Epoxide

Endosulfan 1

4,4'-ODE •

Oieldrin

Endrin - .

4,4'-ODO

fb 3,'-<r'

;TFD OAT!? RPC-n. DATEANALY?pn O- ' ^V-S-^

ppb ppb

*-l 0C O Endosulfan 1 1 ^-/£>f>O

,* 4.4'-DDT ' - • - - ' . • • ".-".. /

-/V;r. Endosulfan Sulfate /

/ Endrin Aldehyde .. ^L,

I Cnlordane \

\ Toxaphene : ..^ :

\ PCB-1221

\ PCB-1232 ""_i/^-v " ' - - " . .' '

i J; ^ PC8-1016/1242 /

/ r wO~ l4t^O :- - - , * ' , " : • -*," • ' . ' , ' . . * . - " - . . - • - / -

, /- -/?_ .-: PCa-1254 ' , /jr pca-1260 - . .. ";-\.- -..': " " - " - "-•'"'•'>•' fy • . ••

Methodology: Federal Register — 40 CFR, Part 136, December 3, 1979

i * Comments:

.'/^•Jf-1, f j £<«/-

O'Brien & Gere Engineers, Inc.Box 4873 / 1304 Buckley Rd. / Syracuse, NY / 13221 / (315) 451-4700

Authorized:

Ditt:

p..

OBRlEMSGEnE' Pesticide/PCB

Priority Pollutants

CLIENT. _£. _JOB NO.

SAMPLE NO. "$£ 3-*3- / PATE COLLECTED. .DATE RECD..

ppb

.DATE ANALYZED y/O-3. /#"*?

ppb

y-BHC

Heptachlor

(5-BHCAldrin

Heptachlor Epoxide

Endosulfan I

4,4'-DDE :

Dieldrin

Endrin

4,4'-ODD

Methodology: Federal Register — 40 CFR, Part 136. December 3, 1979

Comments:

I00t>

TC rtcrcou^n

O'Brien i Gere Engineers. Inc.Box 4873 /1304 Buckley Rd. / Syracuse, NY / 13221 / (315) 451-4700

__

p.


CLIENT JOB NO. 3 C / /• f-g.'

DESCRIPTION — fe ___

SAMPLE NO. Ot? PATE COLLECTED

ppb

er-SHC

Heptachlor

5-BHC

Aldrin

Heptacnlor Epoxide

Endosulfan I

4,4'-DD£ •

Oieldrin

Endrin .

4.4'-DDD

DATE REC'D. DATE ANALYZED

ppb

Endosulfan II

Sulfate

Endrin Aldehyde .' "

Chlordane

Toxapnene • ; ;

PCS-1221

PCB-1232 >'

PC8-1016/1242

PC8-124a_^ . .

PCS-1254

PCS-1260 .

T"T7

Methodology: Federal Register — 40 CFH, Part 136, December 3, 1979

Comments:. I J S

&)£0~&J /f^t^^i^-l<r

O'Brien & Gere Engineers. Inc.Box 4873 / 1304 BucKleyRd./ Syracuse, NY/ 13221 /(315) 4S1-4700 D*i«:

rOBniENEGERE


CLIENT- OouJC- *3 - 10

-JOB NO. sn

rSAMPLE NO. . 4o23 2_ _DATE COLLECTED. .DATE RECD.- J3ATE ANALYZED

o-BHC . . . ^

y-BHC

/J-BHC

Heptachlor

<5-BHC

Aldrin

Heptachlor Epoxide

Endosulfan 1

4,4'-DOE -

Oieldrin

Endrin

4.4'-ODD J

I Endosulfan II „/

4.4--DDT '. . - . .

- Endosulfan Sulfate

. Endrin Aldehyde .."•"„.

Chlordane

Toxaphene • "

PCS-1221

PCS-1232 " ' • ^ ... " . '

PCS-1016/1242

PC8-124a- • • - . ; ./•"y-Vu; •? ; • { ' : ; ' - - r-'f

---< ; PCS-1254 ' |

pca-1260 . - . , - / • '.'-'"'i/

' I

— .

- •-— - ----- .

-...„ . .- r.: ,

Methodology: Federal Register — 40 CFH, Part 136, December 3, 1979

Comments:

<\

O'Brien 4 Gere Engineers. Inc.Box 4873 / 1304 Sucxtey Rd. / Syracuse, NY / 13221 / (315) 451-4700

Authorized:

Date:

OEniENSGERE Priority Pollutants

JOB NO. . OOI .

npsrB]PT10N Q ( - 2> ;

SAMPLE NO. 3S 1 33 DATE COLLPPTFD

0-BHC . \ x^

y-BHC

0-BHC

Heptachlor

(5-BHC '.

Aldrtn

Heptachlor Epoxida

Endosulfan 1

4.4--OOE

Dieldrin

Endrin

4.4'-DDD *

DATE RECTV DATE ANALY7FO ^~22~^^

\ Endosulfan II ^ (

4.4--DDT . . . . . . 1

Endosulfan Sulfate /

Endrin Aldehyde ' • ] . ' . 1

Chlordane /

Toxaphene . ' 1

PCS-1221 I

PCS-1232 '"__ __ .^" . " ''j_

PCB-1016/1242 j

PCS-1248 ' -J .;". :":k : ; ; • •? - • • • . •-";. -"4; "' !

-•'•> ' : PCS-1254 ' j

PCS-1260 - - , -. . "•""- «/ • . :

M«thodology: Federal Register — 40 CFH. Part 136, December 3, 1979

Comments:

TU^ /?

O'Brien 4 Gere Engineers. Inc.Box 4873 / 1304 Buckley Rd. / Syracuse. NY / 13221 / (315) 451-4700

Authorized:

Date:

Pesticide/PCB=

CLIPNT O<^ •**->

DESCRIPTION J}

S4MPIPNO ~^J> ^3>7 OATPrnlLPCTPO

ppb

<r-BHC _.; ^ ; . j£— /•_£&,

y-BHC x

" • • - - - - - • - . - - . . . ^ .. -* (

Heptachlor ^

<J-8HC \\

Aldrin \

Heptachlor Epoxide

Endosulfan 1

4,4'-DDE • • - • - " • _."-'.'

Dieldrin

Endrin • . . - . . . . --' • V^T

4,4<-DDD V

rrioniy ruiiuianio

JOB NO. 3c 7/< cs;, f"' ^i'- V

DATE nee-n DATE ANALV^PO '/-^ 3- - *f <"

_' ; Endosulfan II ^-/coc>

4.4'-DDT r . : - - . . . '

= Endosulfan Sulfate /- - - ...———— • -. ..__ ^--- -~^ r---.-.-. r- - -.---.r.. I .. - • • . -. - -

Endrin Aldehyde .'.'•-• .,.' ' \ '

Chlordane \

Toxaphene • ' " / . - \

PCS-1221 \

PCS-1232 ' "'" '^ ....'..'. '^". . '" ' '• \

PCS-1 01 6/1 242

PCS-1248 -^^-^^^-' '•-, ^:- ---•;:./ '• PCS-1254

PCS-1260 - - . ; , • - . - " '~y


Comments:

O'Brien 4 Gere Engineers, Inc.Box 4873 / 1304 Buckley Rd. / Syracuse. NY / 13221 / (315) 4S1-47CO Date:

./ y^ c r- —^ ~*J

BS OBniENSGEHE• Pesticide/PCB

Priority Pollutants

D ( - j ~ 7 f

SAMPLE NO. 35235 DATE COLLECTED . .DATE REC'D.. .DATE ANALYZED ' 2.2 ~$ S

tt-BHC

y-BHC,L

Heptachlor

<5-BHC

Aldrin

Heptachlor Epoxide

Endosulfan I

4.4'-DDE

Oieldrin

Endrin

4,4'-ODD

Endosulfan II

4.4--DDT

Endosulfan Sulfate

Endrin Aldehyde

Chlordane

Toxaphene

PCB-1221

PCB-1_232_ _'

PCS-1016/1242

PCS-1248_^ .

PCS-1254

PCB-1260

Methodology: Federal Register — 40 CFR, Part 136, December 3,. 1979

Comments:

n

O'Brien 4 Gere Engineers. Inc.Box 4873 / 1304 Buckley Hd. / Syracuse, NY / 13221 / (315) 451-4700

Authorized:

r

r

CLIENT /-"TT.VU/

DESCRIPTION & O '

SAMPLE Nn 3O i. 2> fe> DATE Cm 1 PCTPD

<r-8HC •£

y-BHC

£-8HC .' . .. -' ".''..'•_• J

Heptachlor /

<J-BHC

Aldrin \

Heptachlor Epoxide

Endosulfan 1

4,4'-DDE

Dieldrin /

Endrin . - . /

4,4'-DDD \JX

I^CTOIJUIUC/ I~\*sLJ

Priority Pollutants

JOB NO *»O7/ ( iSr/x r/ 7/

nATEHECTL DATE ANALYSED rf/^~3. /& X/ /

ppb ppb

/DCO Endosulfan II <^-/£>ce.

4.4--ODT .- •;--'• " • , I - " . . .:yf~ '>'" ' ' '"" ' """"" — — — - - - • — - - - - • , • ' - -< - , Endosulfan Sulfate /:"^'* - " . . - ; - .-- -..; ——— - _ ; - • — — — .-.J.-;.*.-.. :-. - - — — — . - . . / - - , ,.. ...,__..

Endrin Aldehyde ;. /

Chlordane 1

Toxaphene ...,„_ \

\ PCS-1221 \

PCS-1232 j'J/Li-.-^;'' . .'" . '.;. ' /

PC8-1016/1242 /

;pcs-i248 ; _ .^^ /^j^L^V ' { ' "'-L; , . . ' .-'--•.--i • 1 PCS-1254' ./

/.. ... ,-_,^T..-,_, -.tT; r.,v-__ -.,»., .„._ . ,.-r_, ..

PCB-1260 - -. ,• . - , W • • . ;

i

M«lhodology: Federal Register — 40 CFR, Part 136. December 3, 1979

Comments:

107

O'Brien & Gere Engineers, Inc.Box 4873 / 1304 BucXley Rd. / Syracuse, NY / 13221 / (315) 451-4700

Authorized:

Data:

JI - GBniENSGEnE

• Pesticide/PCBPriority Pollutants

r

/-

L.

CLIENT. .JOB NO. '"- ?.*"*/• ~- ^ '' 5~S~7

DESCRIPTION. '-<-,'

SAMPLE NO.. .DATE COLLECTED.

ppb

«r-BHC

y-8HC

Heptachlor

5-8HC

Aldrin

Heptachlor Epoxide

Endosulfan I

4,4'-DDE

Oieldrin

.DATE REC'D.. .DATE ANALYZED 1. / ,-T "T

Endrin

4.4--ODD


Comments:

Endosulfan

4.4--ODT

ppb

£ /G£>0

Endosulfan Sulfate

Endrin Aldehyde

Chlordane

Toxaphene

PCS-1221

PCB-1_232_ __"X/

PCB-1016/1242

PCS-1248 __.-> ^

PCa-1254

PCa-1260 \x

1 O'Brien & Gere Engineers, Inc.Box 4873 / 1304 Suckley Rd. / Syracuse. NY / 13221 / (315) 451-4700L

• QBRIENEGEnE• Pesticide/PCB

Priority Pollutants

TLIFNT

OESCBIPTION

SAMPLE NO ^^IX^tT

a-BHC

y-BHC

0-BHC

Heptachlor

5-BHC

Aldrin

Heptachlor Epoxide

Endosulfan 1

4,4'-DDE

Dieldrin

Endrin

4,4'-DDD

1 Jr> \-*^j JOB NO - » - - • / ) -

DATE COLL FrTFD HATE HPtrn DATE ANALY7CQ '//

ppb ppb

^-/tOO> Endosulfan II £-/Ct

^ 4,4'-DDT , - .'•- :--",. ,

/ - •. Endosulfan Sulfate /

I Endrin Aldehyde ^ ~..j_

I Cnlordane \

\ Toxaphene

\ ; PCB-1221

\ PCS-1232 '" \^ --;'" -: '

\ ."; PCS-1016/1242

PCS-1248 / v /f^i^ ^ r -Vj "-- T'~.

. . %; --";.--. i PCB-1254

\J PCS-1260 - - , • - . - . . ^y'

. ' • ?> /

/ /, ^' ^-_ / *j ^^ ^

,

•<

.

._ -.-.... .

.... ...., „-- :

Methodology: Federal Register — 40 CFR, Part 136, December 3. 1979

Comments:

-

/V A •tf^TT/'i

O'Brien 4 Gere Engineers, Inc.Box 4873 / 1304 Buckley fld. / Syracuse, NY / 13221 / (315) 451-4700

Authorized:.

Date:.

r-OBRIEiMCGEHE


fr

C

OFSPBiPTinw faUAUl<T (

SAMPI PT Nrt 75 1 S [ OATE COLLECTED

io/vrr/?c(_ I^L/>/WK

DATPRPC-n. OATP ANALY7EO V'/^P'o

ppb ppb

ff-BHC ^ IQCG Endosulfan II ^OOO

y-BHC

0-BHC , ' .

Heptachlor

5-BHC

Aldrin

Heptacnlor Epoxide

Endosulfan 1

4,4'-ODE /

Dieldrin |

Endrin _\

4.4--DOD V

4.4--ODT .'- ;- ' -> - • : - "-. _': ~-

Endosulfan Sulfate*' • • i '

Endrirr Aldehyde ; . -_ ,_ -

Chlordane

Toxaphene •

PCB-1221

PCS-1232 _'" " ^._ v^-' " . - ;.

,"; PC8-1016/1242

-PCS-124* ' :.> v-:^i;;^l- -;': •-.^"^ V^r.

-- : j PCS-1254

PCB-1260 - '-. ^^ • • . • : - \'". '• ' -" >

- ••• • - • ' •— -~

Methodology: Federal Register — 40 CFR, Pan 136. December 3. 1979

Comments:

< I OOO

O'Brien & Gere Engineers, Inc.Box 4873 / 1304 Buckley Rd. / Syracuse. NY / 13221 / (315) 451-4700

Authorized:

Date:


CLIENT NO. 3&? >, oci.sn

r

DESCRIPTION Q U f\ L ) ( t CLO A.

SAMPLE NO ~15) &£> DATE COLL PCTjm

ppb

ar-BHC ; ^

y-BHC

" /J-BHC _" : • . . ' . ' . : / : . .-•':;".

Heptachlor

<5-BHC

Aldrin

Heptachlor Epoxide

Endosulfan 1

4,4'-DDE - -V

Oieldrin

Endrin - -• - • - -•' --^

4,4'-OOD

JT/?o t_ fT^ /KuO A L/\A^KX

DATenpc-n HATP ANALYZED _4-f~))-%S

ppb

Endosulfan II

4.4--ODT ,- ' • • • - • :-.

Endosulfan Sulfate

Endrin Aldehyde V '

Chlordane

Toxaphene . -^

PCB-1221

PCB-1232 --:" ' '"''." .-... '. '\ : / " " '

j PCS-1016/1242 ^OOO JlOGOO ~ (~fO/',

r wD 1 A4*O - ^' • - -^'. - - ' . • - ' , - - - - • " - - . .

.1 PCS-1254

PCS-1260 - - - ' : . . ' - ''"•-- - . •

Methodology: Federal Hegisler — 40 CFH. Part 136. December 3, 1979

Comments:

ft T

I O'Brien & Gere Engineers. Inc.Box 4873 /1304 Buckley Rd. / Syracuse, NY / 13221 / (315) 451-4700

Authorized:.

Date:. s-f-sr


DouJDF*rm0nnN QUAL/TY Co/UT/7

PT /O/9v9n /D7~O tT"SAMPLE NO. f0062>. DATE COLLPCTPn

ppt>

o-SHC _ . :i

y-BHC

Heptachlor

5-8HC

Aldrin

Heptachlor Epoxide

Endosulfan 1

4,4'-DO£ ' • • . . . " :

Oieldrin

Endrin • --'---.

4,4'-ODD

JOB NO 3&?/.O6/,S'7

oi ^P//<u~rN .<; & ri £> t i^0-2' / LAA ff 352-lC }

"- y1

DATEBPC-n HATP ANALY2PO *f-//-£S~

ppb

Endosulfan II

4.4'-ODT , _r;_ . i-...

Endosulfan Sulfate- - ,- - - --_-..? ..-.-. ..-.-,-.-..-_ ,. -...r., ... , .. - ... ..-,., .

Endrin Aldehyde

Chlordane

Toxaphene ' ' . ' • • " ' "

PCB-1221

PCB-1232 " '-* '•;!:' '-..,:;-"' '. " -

PCB-1016/1242 <$<-{GG / lOOOO - <Q'L{

-pcB-1248 V^ ^£^.? '-' K- ' -v-^r^: "" ; -i PCS-1254

Pea-1260 -. '-.:•'.,-•... : - .l -';- . • " ' :

Methodology: Federal Register — 40 CF3. Part 136, December 3, 1979

Comments:

113

O'Brien 4 Gere Engineers. Inc.Box 4873/1304 Buckley Rd. / Syracuse. NY / 13221 / (315) 451-4700

Authorized:

Date:

s

• Pesticide/PCBPriority Pollutants

CLIENT. _JOB NO. 7X . OC!. .5DESCRIPTION C^AJT/?Q(_

f ( L-ACb ft- 352.16SAMPLE NO. S / 6 f PATE COLLECTED . .DATE RECD._ _DATE ANALYZED ~~ 1 1~

ff-BHC

X-BHC

Heptachlor

<5-BHC

Aldrin

Heptachlor Ep oxide

Endosulfan I

4,4'-DDE

Dieldrin

Endrin _

4,4'-DDD


Comments:

Endosulfan II

4.4/-ODT _•_

Endosulfan Sulfate

Endrirt Aldehyde

Chlordane

Toxaphene _

PCS-1221

PCB-1232 _;

PCB-1016/1242

ppb

'(OOO

PCB-1254

PCB-1260

uv7 o

O'Brien & Gere Engineers, Inc.Box 4873 / 1304 Buckley fld. / Syracuse, NY / 13221 / (315) 451-4700

Authorized:

Oat*:

QBFUENSGEniE LaboratoryReport

CUENT- .JOB NO.

DESCRIPTION . - "Z.

r

DATE COLLECTED. .DATE REC'D. _DATE ANALYZED

"..':'.:' ^ ,~. V ~ (

£ 6 • - f

|T./ M

iJ«t.£»j-:4A' **.-«-i :*-;-.

O.I

J . x

1 ."2

Methodology: Federal Register — 40 CFR, Part 136, December 3,1979

Com ii wn tn

O'Brien & Gera Engineers, Inc.Box 4873 / 1304 Buckley Rd. / Syracuse, NY / 13221 / (315) 451-4700

Units: mg/t (ppm) unless otherwise noted

Author!; Ml'-/ /

•mm OBniENCGERE PurgeablePriority Pollutants

CLIENT-

DESCRIPTION ._ CooC P>- I_JOB NO.

SAMPLE NO. 3-5 2 2 L| OA7g COLLECTED . _DATEHEC-D.- _DATE ANALYZED

cI ^(000

ppbChloromethane ^ j Q

Bromomethane

Oichlorodifluoromethane

Vinyl chloride

Chloroethane

Methylene chloride

Trichlorofluoromethane

1,1-Dichloroethene

1,1 -Dichloroethane

t-1,2-Dichloroethene

Chloroform

1,2-Dichloroethane

1,1,1-Trichloroethane

Carbon tetrachloride

Bromodichloromethane

Methodology: Federal Register — 40 CFH, Part 136, Decembers, 1979

Comments:

1,2-Dichloropropane

t-1,3-Dichloropropene

Trichloroethene

Benzene

Dibromochloromethane

1,1,2-Trich loroethane

c-1,3-Dichloropropene

2-Chloroethylvinyl ether

Bromoform

1,1,2,2-Tetrachloroethane

Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

ppb

<\0

\

C'3r:sr> i Gsre5ox 4373

E"Cir=9rs. Ire.- 5uc:<:ev Sc. .:

c^

OBniENGGErtE PurgeablePriority Pollutants

r•in

CL!ENT_ _JOB NO.

cL

DESCRIPTION .

SAMPLE NO.. ^522-5 .DATE COLLECTED.

ppb

_DATE REC'D.. _DATE ANALYZED

Chloromethane

Bromomethane

Dichlorodifluoromethane

Vinyl chloride

Chloroethane

Methylene chloride


• 1,1-Dichloroethene

1.1-Oichloroethane


Chloroform

1.2-Dichloroethane





Comments:

50/7/I06A

1,2-Dichloropropane


Trichloroethene

Benzene



c-1,3-Dichloropropene-


Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

ppb

O'Erisn i Gere Hrgiraers. inc.Box 4573 . 13C-i 2uc:<ley inc. / Syracuse. NY

Aurhorized:

1 OBniENGGERE PurgeablePriority Pollutants

CLIENT-

DESCRIPTION .

-JOB NO. .137/. C&/.S/7

Ci[.

L :

ppb

coco

SAMPLE NO. 3527.C> DATE

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane



Bromodichloromethane xMethodology: Federal Register — 40 CFR, Part 136, December 3. 1979

Comments:

E REC'D.. .DATS ANALYZED

1,2-Dichloropropane


Trichloroethene

Benzene





Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

T

C S.'ign i G-sre E^cineers. .'re.Box *373 :3C-i 5 Jc:<iey P.c. S>-ac j ac

A-j::-orizec!:

r

r

OBniENSGERE

CLIENT.

DESCRIPTION /- 2.

PurgeablePriority Pollutants

_JOS NO.

SAMPLE NO. .35127 .DATE COLLECTED. _DATE REC'D.. .DATE ANALYZED

J '.

GI.

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane



BromodichloromethaneT


Comments:

1,2-Dich loropropane


Trichloroethene

Benzene



c-1.3-Dichloropropene


Bromoform

1,1,2.2-Tetrachloroethane

Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

L 320 coo

t: ^i

iI C'anert i Qere E.'g.'nsers. :nc

3cx 45~3 . 130-t Suckisv ,-•.;.

OBniENCGEREPurgeable

Priority PollutantsCLIENT.

DESCRIPTION

_JOB N JV 7

SAMPLE NO. .3-5^ ?2 S PATF COLLECTED ___________DATE HEC'D.. _DATE ANALYZED

L

ppb

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1 -Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane


Carbon tetrachlorideI

Bromodichloromethane J/YMethodology: Federal Register — 40 CFR, Part 136, December 3, 1979

Comments:

1,2-Dichloropropane


Trichloroethene

Benzene





Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

537,

C'Srien 3. Gsre Engineers, ire.Sox 4373, 13C4 3ucx'ev Re. S/ 'ac. jse. '-iV • 3'5'j -51-iTCO

QBRIENSGEREPurgeable

Priority PollutantsCLIENT- KJ .JOB NO. 3f37t .OCf.-S I?

DESCRIPTION

SAMPLE NO. 2>5 22- jf HAT? COLLECTED .

ppb

/^

v--CCCGO

-^l O

.DATE REC'D.. _DATE ANALYZED

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane

t-1 ,2-Dichloroethene

Chloroform

1.2-Dichloroethane



Bromodichloromethane .i/


Comments:

1,2-Dichloropropane


Trichloroethene

Benzene





Bromoform


Tetrachloroethene

• Toluene

Chlorobenzene

Ethylbenzene

ppb

O'5r:en 4 Gere £rc;ree.rs. ir.c.Box 4873 12C4 =Jc,<i2y .=.c S--.-2c.se.

r

r,r

P

c:L

mm QBRIENCGERE PurgeablePriority Pollutants

CLIENT. Pop .JOB NO.

DESCaiPTION C

SAMPLE NO. nATg COLLECTED . _DATE FIEC'D.. .DATE ANALYZED

ppb

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane

1,1,1 -Trichloroethane




Comments:

ppb

1,2-Dichloropropane


Trichloroethene

Benzene





Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

N/CO

L:

O'Brien i Gsre Engireers. Ire.Box 4S73 / 13C4 Buckiey Re. S/'2C'JS9. NY

pOBRIENSGERE Purgeable

Priority Pollutants

CLIENT. _JOB NO.

DESCRIPTION

P

LCi.

SAMPLE NO. . "3J—

ppb

_DATE REC'D.. _DATE ANALYZHD

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform /j

1.2-Dichloroethane !



Bromodichloromethane V


Comments:

1,2-Dichloropropane


Trichloroethene

Benzene - ~~~





Bromoform

1.1,2,2-Tetrachloroethane

Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

ppb

«?(0

3500

77

C 3nen a Gere Engireers. Ire.Box 4373 13C4 aJcKley r.c. Syracuse. .NY

CLL

\mm QBRHENSGERE

CLIENT. CotJ


____JOB NO. 307' 06 > Si"1

DESCRIPTION o

SAMPLE NO. PATE COLLECTED . _DATH HEC'D.. .DATE ANALYZED

ppbQChloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane

1.1,1-Trichloroethane /

Carbon tetrachloride /

Bromodichloromethane 4

Methodology: Federal Register — 40 CFR, Part 136, December 3,

Comments:

1979

1,2-Dichloropropane


Trichloroethene

Benzene





Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

ppb

V

O'3rien & Gere Epcinaers. Inc.Box 4573 . 1304 aJckley Pd. Syracuse. NY 1222'

p.fi

C

L

CLIENT.

QBRIENCGER1E

06 *O

PurgeablePriority Pollutants____JOB NO. 3<T7I .COL 5 i~7

DESCHIPTION . D

SAMPLE NO. _JlS-2 iA__DATE COLLHCTHD . .DATE HEC'O.. _DATH ANALYZED

ppb

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride

TrichloroflUoromethane

1,1-Dichloroethene I

1.1-Dichloroethane }1

t-1,2-Dichloroethene ;I

Chloroform {• !

1.2-Dichloroethane

1,1,1-Trichloroethane •

Carbon tetrachloride :<Bromodichloromethane Y


Comments:

1,2-Dichloropropane


Trichloroethene

Benzene



" c-1.3-Dichloropropene


Bromoform

1.1,2.2-Tetrachloroethane

Tetrachloroethene

Toluene

Ghlorobenzene

Ethyfbenzene

ppb

to

(

3ox

.p.f;

rQBRIENGGERE

„__D


oot J/7

n ppb

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride

. Trichlorofluoromethane

1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane !i1,1,1-Trichloroethane j

Carbon tetrachloride <\

Bromodichloromethane jVMethodology: Federal Register — 40 CFR, Part 136, December 3, 1979

Comments:

i

1,2-Oichloropropane


Trichloroethene

Benzene





Bromoform


Tetrachloroethene

Toluene

Chiorobenzene

Ethylbenzene

ppb

V

/6

L[>i ;

OBniENSGERE

CLIENT. DoiO


NO.DESCRIPTION 0-1'

SAMPLE NO. Par- COLLECTED . _DAT= REC'D.. .DATE ANALYZED

0'.£

f ;

PRO

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride

Trichlorofluoromethane ' ^-l(J

1,1-Dichloroethene I\

1.1-Dichloroethane '.!


Chloroform s

1.2-Dichloroethane ;



Bromodichloromethane /


Comments:

1,2-Dichloropropane


Trichloroethene

Benzene



c-i ,3-Dichloropropene


Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

ppb

L

r,:C

<—',

OBFHENSGEnEPurgeabie

Priority PollutantsCLIENT. _JOS NO.

DESCRIPTION

SAMPLE NO. 35 Z DATE COLLECTED .

ppb

.DATE REC'D.. _DATS ANALYZED

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane

1,1,1 -Trichloroethanei

Carbon tetrachloride ii

Bromodichloromethane -J


Comments:

1,2-Dichloropropane


Trichloroethene

Benzene

Oibromochloromethane


c-1,3-Dichloropropene '


Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

~2L/~oS

ppb

O'Srien i Gere3ox 4373 "SC-i

eers. Ire.A-'-or!;

OBRIENSGEnEPurgeable

Priority PollutantsCLIENT. _JOB NO.

DESCRIPTION

SAMPLE NO.. .DATE COLLECTED. _DATE RECD. .DATE ANALYZED •> 2 •-!-?.<'ppb

Chloromethane y / n

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane



Bromodichloromethane '/


Comments:

1,2-Oichloropropane


Trichloroethene

Benzene





Bromoform


Tetrach loroethene

Toluene

Chlorobenzene

Ethylbenzene

O'Brien i Gere Engineers. !rc.Box -18T3 •' 13CJ 3uck:ev Re. Svrs

Authorizoo:

IT

uCLIENT-

QBRIENSGERE

OOP


NO. 3071 CO/ 5/7DESCRIPTION _

SAMPLE NO.. .DATE COLLECTED. _DATE REC'D.- _DATE ANALYZED '<? V '

ppbChloromethane

Bromomethane


Vinyl chloride - — —

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane Ii

1,1,1-Trichloroethane IiCarbon tetrachloride j

Bromodichloromethane '>.


Comments:

ppb

1,2-Dichloropropane


Trichloroethene

Benzene





Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethyl benzene

O'Bnen i Gere Engineers. Inc.Box 4373 13C4 3uc!<!ev R<j. Svracjss. NY

A-rhorizad:.

Ifr QBRIENCGERE


CLIENT. JOB NO.

DESCRIPTION . i Y

r.D'L

SAMPLE NO.. -DATE COLLECTED.

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Oichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane




ppb

V

_DATE REC'D.. _DATE ANALYZED V" 2*7 '

1,2-Oichloropropane


Tcichloroethene

Benzene

Dlbromochloromethane




Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

ppb

< (GO


OBRIENSGEREPurgeabie

Priority PollutantsCL1ENT_

DESCRIPTION.

.JOB NO. 3671 • CO I.AT ^ ICO

f- SAMPLE NO.. .DATE COLLECTED . .DATE RECD.- DATE ANALYZED V'

ppbChloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane


Chloroform

1.2-Dichloroethane

1.1,1 -Trichloroethane




Comments:

/ISO =

1,2-Oichloropropane

t-1,3-Oichloropropene

Trichloroethene

Benzene





Bromoform


Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

ppb

73*7*

123%

C'Brien i Gsre Ergireers. Ire.Box 4873 . 13C-1 Stick lay =i. ' S/rn -se. .NY • '222'. ( 2 ' s i -5'--i

QBniENSGEREPurgeable

Priority Pollutantsn IFNT

DESCRIPTION

SAMPLE NO. _Z

L^KJ

QU0U TV/ j /

Oo -b 5" PATC COLL = CTED

C&rJTSLQ L Z)^/}£> / 357^2 J

DATC P1PC-D

ppb

joa NO L5OV/ . O^-V* C ? ' /

^ , /^ THrf <0 P

DAT? ANALY7Pn T • 2^/ ' ¥5)

ppb

7

Chloromethane

Bromomethane

Oichlorodifluoromethane

Vinyl chloride

Chloroethane

Methylene chloride


1.1-Dichloroethene

1.1-Dichloroethane

t-1 ,2-Dichloroethene

Chloroform

1.2-Dichloroethane

1.1,1-Trichloroethane



Methodology: Federal Register — 40 CFR, Part 136, December 3.

Comment*:

1979

1,2-Dichloropropane


Trichloroethene

Benzene





Bromoform

1,1,2.2-Tetrachloroethane

Tetrachloroethene

Joluene

Chlorobenzene

Ethylbenzene

No/V

/See

,r

L O'Brisn i Gere Engineers. ;rc.5ox -373 12C-J 3uc.<:ev nc. £v.-ac-jse. NY

Frr

QBRHENSGEREPurgeable

Priority Pollutants

DESCRIPTION

SAMPLE NO ~? LjS tfS

ftutf L-irr/ ' ( u\&-#i DATE COLLECTED

C6AJ77?6i_ OupL- 3S237 }y

DATC RPC-n

fC«977- 01-

DATE ANALY7FD *7 ~ 2 H * OO

ppb

Chloromethane

Bromomethane


Vinyl chloride

Chloroethane

Methylene chloride


1,1-Dichloroethene

1.1-Dichloroethane

t-1,2-Dichloroethene '

Chloroform

1.2-Dichloroethane





Comments:

1,2-Dichloropropane


Trichloroethene

Benzene

Oibromochloromethane


c-1,3-Dich loropropene


Bromoform

1,1,2.2-Tetrachloroethan

Tetrachloroethene

Toluene

Chlorobenzene

Ethylbenzene

ppb

L O'Bnen A Gere Encinsers. Inc.Box -1673 13C4 BiTckley Re. Syracuse. NY . T322"

.iu:!:oriiad:

"5'' -51--TCO

/>. 0. Box 818. Alexandria. Virginia 22313 703/557-2«90

Organics Analysis Data Sheet(Page 2)

r

Semivolatile Compounds

Concentration: Low Medium (Circle One)

Date Analy;

Conc/Dil F«

- CASNumber

•^v)

U

I

1

J-75-9108-95-262-53-31 i ; -Ad.495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9

N-NitrosoaimethylaminePhenolAnilinebis(-2-Chloroethvl)Ether2'Chloroohenol1 . 3-Oichlorobenzene1. A.QicfilorobenzeneBenzyl Alconol1. 2-Oichlorobenrene2-Metnvlohenolbis(2-CfiloroisODrODY')Ether

106-44-5 |4-Metnv!phenol62 1 -64-7 | N-Nitroso-Di-n-ProDylamme67-72-1 JHexacM'oroethane

L98-95-38-59-1

88-75-5105-57-9

NitrobenzeneIsoBhoror.e2-Nitrosnenol2. 4-Dime:hvl3henol

•65-85-0 Senioic Acid111-91-1 bis(-2-CMIoroe:hoxvtMethane

rarf-

'FjuâJ l/&iw(.&- 10/yiJ

ug/lorug/Kg CAS(Circle One) Number

/<2JO

to5O

*3 at 2o

2.0^0

120-83-2 2. 4-Dicnloro3nenoi ' |120-82-1 1. 2. 4.7ncMiorooenzene91-20-3 Nasnthaiene105-47-8 1 4-C.uiioro3niUneS7-63-359-50-791-57-6

Hexacniorcsutaoiene4-Chlo-c-3-Me!.ivl3n9noi2-We:r.vir.a3".tr.ai»ne |

77-47-4 | Mexadvcrocvclooeniac'iene63-05-2 2. 4 o-TncnioroonenciS5-S5-4 '2. 4. S-Tncnioroon-nol

9 1 - 5 3 - 7 iZ-CniorcnacnoaieneS3-74.4 2-Nnroanilme

131-11-3 Qimetnvi Pntnaiaie203-95-8 | Acenao^t^vicne99-C9-2 3-Nnroanilme

83-32-91-25-500-C2-732-£4-921-14.2

605-20-2 "84-65-2-005-72-385-73-700-C1-6 '

534-52-185-3C-6i01-55-3118-74-137-85-5S5-01-8120- 12 -734-74-2205-44-052-87-5129-00-0S5-65-791-54.;55 -==-3117-E1-7

Acenasntnene2. 4-Dini:ro3neno!4-Ni:ro=henciDibenzofuraa2. 4-Dint:rotofL-sne2. 6-Dini:ro:3i'-ene

ug/lorug/Kg(Circle One)

Die;hvi3!-.:ha!8:s |4-Chloro3iisny!-ohenvle:nerriuorene4-tNitroaniline4. 6-Dinitro-2-.V.e!nvl3heno!.N'-Ni:r2soicne.-iv!amine (1 !4-Bro.-nc=nenv;-Dnenyle:rierHexacniorocenzene

,

•

|

PsntachlorcsnenolPnenantnreneAninraceneDi-n-3u:vlDh:hs!a:erluoranrhens •BsnzidmePyrene

au!viDenrv:=n:r,alats3. 3"-0'cnicrc3er.z>ainesenâiAnt.irscensb.s(2-=:nvip.exv:!Pr.;nalaie

213-C-9 jCi-.rvsene1 17-54-0 |Di-n-Oc:vi Pht.-.aiate |205-53-2 |5enzo(3i?iuc:ra.i:nene:07-C3-950-j:-5193-25-553-70-3191 -14.;

3en:-<*!=iu=ra-:.ienesenzcca yreneInCff^c'. 1 2. 3-Ci!^vêre

0-5en::a n;An:-iraceie3en:r(c ^ .-iP- i-n-

(l]-C«nno: De sesaraied Irom CicnenY'a""1"'1*

Form I 4/S4

P. 0 Bo* 818. "Alexandria. Virginia 22313 703/557-2-S&0



Concentration:c"~Tow~~ Medium (Circle One)

A'£'-*•

.

- CASNumber

H'1

'

i

i

1-75-9108-95-262-53-31 1 1 .44-4

95-57-8541-73-1106-46-7100-51-695-50-195-48-7

Date Analy

Conc/Dil F«

N-NitrosodimethvlaminePhenolAnilinebis(-2-Ch!oroetnvllether2-Chloroohenol1. 3-Dichiorobenzene1 . 4-Dichloro'benzeneSenzvl Alcohol1 . 2-Dichlorobenzene2-Metnvtorienol

39538-32-9 | bis(2-chloroisoorooYUEther106-44-5521-64-767-72-198-95-3'3-59-1

88-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-837-63-359-50-7

4-MetnvlDnenofN-Nitroso-Di-n-PrcDvlammehexachloroethaneNitrobenzeneISODhorone2-NitroohenoI2. A-Oimemylsnenol3e".zoic Acidbisf-2-Chloroe:hoxv)Methane2. 4-Dicnloroonenol1 . 2. 4-TnchloroDenzeneNaonthaiene4-CnioroaniiineHexacnlorcsutaoiene4-Chloro-3-Methvionenol

91-57-6 2-Me:rwina3n;nai-ne77-47-433-05-2S5-95--91-58-733-74-4131 -11 -3208-95-899-09-2

Hexacniorocvciooentadiene2. 4 6-Tncnioroonenol2. 4. 5-Tnc.iioroon<nol2-Chiorona=ntâiene2-NnfoaniimeDimeinvi Phjha'ateAcenaohtriviene3-Nitroanitme

red-,r,nr. lV/\fr$ 4tM*S

ug/lorug/Kg CAS(Circle Onel Number-

?>SIO

'Lt'C+O

'gyô

3 *f 3'O

S3-32-91-28-500-02-732-6i-921-1--2

Acenacntrie2. 4-Dimtro4-NitroohenDibenzofura2. 4-Dinitro

506-20-2 " I 2. 5-Dinitro54-65-27005-72-3S5-73-700-01-5

53i-=2-165-30-6101-55-3118-74.1

Diethytanth4-Chloroo!"><rluorene4-N'itroanili-. 6-OmitroN-Nitrssoci4-aromoonHexachloro

37-35-5 |?entachlorc35-01-5120-12-7

PhenantnreAnthracene

34-74-2 |Di-n-3u:viD205-14-0 rluoranther52-87-5 |3enzidine1 29-00-0 | Pvrsne35-6S-7 3u:yiSerr%-!SI -34.'. . |3. 3'-Oicnio55-55-3 5en:oo)An1 1 7-S'! -7 3iSi'2-£tnvlr

21S-C1-S Cîrysene: 17-54-0 (D'-n-Octvi205-53-2 Benzooirlt207-C3-9 |3er.;oUi='u50-32-5 |3enzoia!sv193-29-5 [Incsnoil 253-70-3 |3'2»r.::a r>191-24-2 3-->;rfc h

(1)-Cannc: se se;araied Irom

ug/l orug/Kg(Circle One)

4/S4

P. O. Bo* 818. Alexandria. Virginia 22313 703/557-2*90



Concentration: Low Medium (Circle One) A

Date Extracted/Prepared: ________________

Date Analyzed: —

Conc/Dil Factor:

U

E

CASNumber

ug/I or ug/Kg(Circle One)

CASNumber

ug/1 orug/Kg(Circle One)

''*^?-75-9

)

*

.08-95-262-53-3\ \ \ .££..£

95-57-8541-73-1106-46-7100-51-695-50-195-48-739633-32-9106-4Z-5621-64-767-72-198-95-3^•8-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-387-63-359-50-791-57-577-47-4

N-Ni!rosodimethylaminePhenolAnilinebis(-2-Chlcroetrwl)E:her2-Chloroohenol1. 3-Dichlorobenzene1 . 4-DichlorobenzeneBenrvl Alcohol1. 2-Oichlorobenzene2-Metriylohenolbis<2-cMloroisoDroDYMEther4-Metrivior.enolN-Nitroso-Di-n-ProoylarnineHexachloroethaneNitrobenzeneIsoohorone.2-Nitroohendl| 2. 4.DirneiMYlsneno!

3«nzoic ACIC&is(-2-ChioroeT^oxviMe:hane2. 4-Dicnioroonenol1. 2. 4-TnchlorooenzeneNaontnaiene4-C.i'oroaniimeHexacnlorcsutaaiene4-ChIoro-3-Me'.nviortenot2-Me;nyinaonTnaieneHexacniorocvciooentacjiene

33-05-2 2. 4 6-Tnc.-iio.'3onenol95-95-4 2. 4. 5-TriC.*>IOrODn'!riOl

9 1 - 5 8 - 7 | 2 -CiiioronacruMaiene33-74-4 1 2-Nnroanilme131 -11 -3 | DimeTnvi P^iihalate203-95-8 AcenaoM:nviene93-09-2 1 3-Nuroanidne

/23S-0

&310

"\1szo

foVo

83-32-951-28-51 00-02-7132-64-g•,21-1-1.2605-20-2 '54-66-27005-72-385-73-7100-01-653-4-52-185-30-6101-55-3118-74-137-36-555-01 -3120-12-7 !34.74-2205-i^-OS2-37-5129-00-0E5-63-791-94.155-55-2117-81-7zia-oi-s1 1 7-34-02C5-9S-2207-03-950-32-c1S3-35-553-70-31S1-24-2

AcenacnTnene2. 4-Dim:ro5Heno!4-NitroonenolDibenzofuran2. 4-Dini:ro*oluene2. 6-DinitrotaiueneDie:hy!oh;rialate4-ChloroDhenyl-Dnenvletnerrluorene

4-N'itroaniline4. 6-Dinitro-2-MeT:">yi3henoiN-Nitrosodiohenylamine (1 )4-3romoDnenvl-£jhenvie:,lerHexacnlcroaenrenePeniacMioroshenolPnsnantfireneAnthraceneDi-n-Butvi2htha!a:erluoraniheneHeniidinePyrene

SutyiterrvJcnthalate3. S'-Oicnioroaenzisine55n:o<3>An;nraceneDis(2-£:nvlnexvl).=r.:na:3i»C.~.rysene

|Di.n-Oc*vi PhtnaJateseniooiriuorantnene3enio(itlsluoran:.ieneBeniofaPyreneineenoil. 2. 3-c2!?vcene0'5enr!a n)AnTnra;»ne

3eT:r(c H iiPervie.'*"

.•

1

.a: 3e seoaraied from

Poin\ I 4/Si

P.O. So* 818. Alexandria. Virginia 22313 703/557-2150

jttt^to tcp/4i«uf



Concentration: (Z&S&7 Medium (Circle One)

Date Extracted/Prepared: •____________________

Date Analyzed: ————————————————————

35227-

Conc/Dil Factor:

0• CAS

./-dumberug/I or ug/Kg

(Circle One).2-75-9108-95-262-53-31 VI .44-4

95-57-8541-73-1106-46-7100-51-695-50-195-48-739S38-32-9106-4i-S621-64.767-72-1^3-95-3/8-55-188-75-5105-67-965-85-01U-91-1120-83-2120-82-191-20-3106-47-387-63-359-50-791-57-677-47-.:83-05-295-95-491-58-783-74-i

131 -11 -3203-95-899-09-2

N-NitrosodimcthvlammePhenolAnilinebis(-2-Chioroetfivl)=!her2-Chloroohenol1, 3-Dichlorobenzene1 . 4-DichlorobenzeneBenzyl Alcohol1 . 2-Oichlorobenzene2-MethylDhenolbis(2-chloroisooroDYl)Ether4-MetriylphenolN-Nuroso-Di-n-ProoylamiheHexachioroeihaneNitrobenzeneIsoohorone2-Ni:roshenol2. 4-DimethylohenolBenzoic Acidbis(-2-ChlorosThoxvlMe:hane2. 4-Oicnloroohenol

I 1. 2. 4-Tnc^loroDenzeneNaphthaleneA-ChloroanilmeHexachlorcDutaaienei-Chloro-3-We'.hvlohenol2-Me;."iyina3."it,-.3ieneMe«achiorocvciooenia(3iene2. 4 6-Tncr>ioroonenol2. 4. S-TncrnofOonenoi2-Ch'orcnac^ihaiene2 -NuroaniimeDimethyl PhthaiateAcenaohtnviene3-f«'>troaniline

32SO

•£g3o

3ffO

PI*"? txhtC&J^

CASNumber

ug/I orug/Xg(Circle One)

83-32-951-25-51OO-C2-7 |132-6-i-9*,21-1-i-2605-20-2 " \84-65-27005-72-385-72-7100 -01 -553-t-=2-185-3C-5101-55-3118-74-'.37-85-585-01-8: 20-1 2-7S4-7i-2206-1 .092-87-5129 -CO-065-65-791-54--,55-55-2117-51-721 5-0- =1 17-Si-r205-55-:207-C5-350-32-c193-35-553-70-2191-2--2

Acenasninene2. 4-Oini:ro3fiencI4-Ni:roohenolOibenzofuran2. 4-Dinitrotoluene |2. 6-Oini:roto!ueneDiethybhtrialaie4-Chloroo.uienvl-Dhenvle:r:e.'rl'JO'Sne '

4-Nitroaniline4, S-Oinitro-2-MetnybhenoiN-Niirssoosnenvlamme (1!4-Bromo3henvl-Dfierivle:Me''HexacnloraoenienePsn;ac~ioro3henol |Pr.ena.-.tnreneAotnraceneOi-n-BjtviDhtnalateriuoranTheneSeniidme3vreneSu'.vl&anrvlDntnaiate3. 3'-0'cnicro3enncmeSenroolAntnracensS'S!2-E:nvlnexvl)Pr.:r.3laj«Cnrysene

|0.-n-0r:vi ?h:nata:sasnzooiriuora/v.nene3en;o<n)::luoranjnene

IBenicKai'yrene

Infisnoil . 2. 3-C2!?vreie

3'0e>".:!a h)An;nrac«ie1 Benzene h ilPerviene

nr.;: 35 sasaraied from

;~r~ pro.Box 818. Alexandria. Virginia 22313 703/557-2*90


^ (T/

, „ Semivolatile Compounds K> J- ~

... feh ff^*** " Concentration: Low Medium (Circle One)

, L.L.Date Analy

Conc/Dil F,

. CASNumber

-" t

fî)

(L...

r

i! . •

ri

i

i _

~""-75*9.08-95-262-53-31 i 1 .4 .495-57-85*1.73-1106-45-7100-51-695-50-195-43-7

N-Nitrosodimetrtvl3minePhenolAnilinebis(-2-Chloroethvl)£tner2-Chloroohenol1. 3-Oichlorobenzene1. 4,-DichlorobenzeneBenrvl Alconol1. 2-Oichlorobeniene2-MetMvlohenol

39638-32-9 bis(2-chtorotsoDrooYl)Ether106-".-5 4-MetnvlDhenol621 -S—-7 N-Nitroso-Di-n-ProDvlamine67-72-198-95-3

"""'9-59-1dS-75-5105-57-9

•65-85-01 1 1-91-1120-83-2120-82-191-20-3106 -47- 887-63-3£9-50-7

HexachioroethaneNitrobenzene 1Isosnorone2-Nitroohenol2. 4-DimeihYlDnenolBenzoic AcidSisf-2-C^loroe:"0)cvtMe:hane2. 4-Dicnloroorienol1.2. 4-Tnc^loroDenzeneNacntr.a'ene4-CnicroanihneHexacnlorcsuiacsiene

| 4-Chloro-3-iMe!rivloner.ol91-57-6 2-Me:nviriaDn;r;3iene77-47-4 HexacnlorocvcioDentad.ene83-05-2 2. 4 o-Tncniorooneno!55-S5-4 2. 4. S-TriC-'llOrOO'ifnOl

91-58-7 2-Chiorona=ninaicneS3-74-- 2-Nnroamline

1 3 1 - 1 1 - 3 0'ifietnvi P^nhaiaie203-95-8 Acenaoîivien-99-09-2 j-'-'itroamline

?pd-

af.,nr- f^ll/ (rtlu^Z. (AfcJ

ug/I orug/Kg CAS .(Circle One) Number

,3 3 os

«^l/c>

^^ô

/3â

|

83-32-951-28-5

00-02-7132-64-9121-14-2606-20-2 "84-65-27005-72-38 6-73 -.7100-01-6534-52-185-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2203-4-i-O92-87-5129-00-085-63-791-94-1

AcenannTMe2. 4-Dini:ro4-Nitroohen

Dibenzofura2. 4-Dini:ro2. 6-OinitroDiethybhtn4-Chloroo.Triuorene4-Nitroanili4. 6-DinitroN-NitrssoCi4-Bromoon

HexacnloroPsn;ac lorcPhenan;nreAnihracenepi-n-5utvlo|.=iuoran:ner1 3en:idine|3vrene|Butviber.rv!|3. 3'-0«cnlo

55-55-3 |5en:aa)An1 17-81 -7 |Disi2-E:nvir218-01-9 |C:-.rvse.-ie117-5.1-0 p.-n-Or.vif205-9S-2 |5enzo(3)?lu207-06-9 |3enzw^)=tu50-32-8 (SenzaaPv193-39-553-70-3191-24-2

jinsenoi i 2iDioer.zfa r>(5e~:r(c *

(1 )-Canno: 3e separated from <

ug/Iorug/Kg(Circle One)

4/84

T P.O.Box 81 8. 703/557-2490




Date Extracted/Prepared: ——————————————

Date Analyzed: __

fle^ ti^<h&4^* f >6 f o - 6 5~

Conc/Dil Factor:

- CASNumber

ug/l or ug/Kg(Circle One)

CASNumber

orug/Kg(Circle One)

"2-75-9108-95-262-53-31 1 1 .44.4

95-57-8 '•541-73-T106-4S-7100-51-695-50-195-^3-739638-32-9106-4i-5621-64-767-72-198-95-3?8-59-183-75-5105-67-9

•65-85-0111-91-1120-33-21 20-82-- 191-20-3106-47-887-63-359-50-791 -57 -677-47--83-05-2S5-S5-491-58-738-74..:131 -11 -3203-95-693-09-2

N-NiirosodimcthviaminePnenolAnilineDis(-2-CMoroethvllEther2-CMoroohenol1. 3-Dicnloro&enzene1. 4-DichlorobenzeneBenrvl Alcohol1. 2-Diciilorobenrene2-Methvlohenolbis(2-chlorotsoDroDyl)£ther4-Methvlor.enolN-Nitroso-Di-n-ProDvlammeHexachloroeihaneNitrobenzeneIsoDnorone2-Nitrosh»noI2. 4-Di."ne:hylahenolBer.zoic Acidtjis(-2-Chloroe:hoxv)Methane2. 4-Dicnlor3onenol1. 2. 4-Tnc*iloroDen2eneNaontnaienei-CnioroanilineHexac.i!or;sijtaaiene4-CMocc-3-Me:rivion9r,o!2-M«:r.vir.a3n:r.ai«neHexac~:cro:vclooentadiene2. 4 6-TncniO.'03nenol

2. 4. 5-Tncnlor03n»nol

2-Chiofcnacrijiaieê2 -NifoaîimeO'rnefrwi PMthaiateAcenaor.tiwiene3-N'iir3aniiine

S-F

- ^J

S3-32-951-2B-510C-C2-7132-64-9121 -14-2505-20-2 "34-65-27005-72-385-72-7IOO-Ct-6534.52--.85-3C-5101-55-311 8 -/A.-,37-35-585-01 -3120-12-734-74-2205-44 -c92-37-5129-OO-0S5-55-7Sl-ai-',55-55-3T17-S1-72 1 3 - C - - 51 1 7-5i-C205-r5-2-07-CH-550-3:-£• S3-2r-553-70-3191-24-2

Acenasnrnene2. 4-Dini:rooheno!4-Ni:ro3heno!Oib«niofuran2. 4-Dinitro:oluene2. 6-Oini»ro:olueneDiethviahthalate4-Chloroonsnv'-Dhenvle;riefriuorene4-Nitroaniline4. 6-Dinirro-2-f.'etnvbhenoiN-NitrosoCicnenylarnme fl)4-Sromoonenvl-phenvle:ner

Hexacr.icrosenjenePentac.MoroshenofPhenantnrencAnthraceneDi-n-Survb^thalaterluoranthensosnjidioePvrene5utviSenrv!sn:fialats3. 3'-0'cnioroDenname| SenrKalAninraceneD'Si2-E:nvir.exv!lP.i:na!at«

jC.Vvsene|3i-n-Cc:vi PhtnaiatesenicOiriuaranêne

|3en:?(<i?iuor3ri;nene|3en:>a!svreneiniencil 2. 3-csi'veneOiOec;!a MlAntnracene

3ei:o<c i il?»rvlene

,•

1

I

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L

"P.O. Box 818. Alexandra. Virginia 22313 703/557-2450




:f; •

- CAS" /"""lumber

r1

i,iii

ii..L

\

L

d2-75-9108-25-262-53-3111-44-4

95-57-8541-73-1106-4S-7100-51-695-50-195-48-739638-32-9

Date Analy:

Conc/Dil Pi

•

N-NitrosodimethvlaminePhenolAnilinebis(-2-Cnloroetrwl)=:ner2-Chloroohenol1. 3-Dichlorcaenzene1. 4-DichlorcbenzeneSenzvl Alconol1 . 2-Dichlorobenjene

1 2-Metnvlohenol' ais(2-cnloroiso3rc3YDEtner

106-4A-5. 4-Metnvlonenol621-64-767-72-1'18-95-373-59-188-75-5105-67-955-85-0

[ N-Nitroso-Di-n-PrcovlamtneI Hexacnioroethane! Nitrobenzeneisopnorone

| 2-Nitro3nenol

| 2. 4-OimethviDhenolI Senzorc Ac:a

111-91-1 1 3.sf-2-Oloroe^0xv)Methane120-83-2120-82-1

| 2. A-Dicnlorcsnenol| 1. 2. 4-Tric^loro3enzene

91-20-3 | NaontnaleneYC/b -1.V& ' t-rrtioroaninne37-63-3 | Hexacniorss'jtaaisne

-pd- ,~i~r 8 Jfi-ft** - >A '•• L\r\nr- r > Stf O-Jf \S<7 \A34\\t_ - ft) ^l 1

ug/lorug/Kg CAS(Circle One) Number

JT^V• io^-O

/2-<c>

59-50-7 | 4-Chloro-3-Metnvi3r.er.oi |91-57-6 1 2-Mernvina3~t!".a'ens |77-47-4 | Mexachioro;vciooentafliene63-06-2S5-95-4

|2. 4 o-Tncnioroon.nol

| 2. 4. 5-TricnloroonenOl

9 1 - 5 8 - 7 |2-Chiorcna=.-ur>aiene

aa-74.i | 2-Nifoanilme131-11-3 1 Dimethyl Phtnaiate208-95-3 I Acenaontrwien?99-C9-2 1 3-Wuroanilme

3-32-9 Acena3~:ne1 -2S-5 | 2. 4-Dini:.-s00-02-732-64-92-.-".4-206-20-2 '4-65-2005-72-25-72-700-01 -634-52-15-3C-601-55-2 '18-74.17-35-55-01-5

4-Ni:ro3.ierDibenzofura2. 4-Dini:ro2. 6-Oini:rcDierfwis.-.in4-ChlcrcsMrluorens4-Nitroanili4. 6-Om,:roN-Nnr=sc-=i4-3romo3'"iHexacnicroPeniacniorcPhenanr-.r-

20-12-7 Anthracene84-74-2^06 -4-1-0c2-87-5

29-00-085-6S-791-34-:

Oi-n-5u:viDPluorantnerSenzio.naPyrene3u!Yl3er.:v.3. 3"-0'C-.c

55-£ = -2 5en:»3;ArT,7-£1-7 |o.s<2-E:r'v!

:i6-C'-= Cnrvsene117-34.; pi-n-0r:vi205-95-1 5enzcXC.-'i207-C3-5 |3en:?(*;=.i5C-32-E |3enzo-'a =v193-3 = - =53-70-3

Inti-no'.: :Di=e<-.;!a <•

191-I4-; iBenics's -.

(l)-CJ-iRS: 5e sesaratea lro-^>

ug/I or ug/Kg(Circle One]

L 4 /£i

P 0. BoYaia. Alexandria. Virginia 22313 703/557-2490

{Zc

Iin


Semivolatile CompoundsConcentration: ^^) Medium (Circle One)

Date Extracted/Prepared: _____________

Date Analyzed: _

Conc/Dil Factor:

n1

L

fI

•

CAS • ug/lorug/Kgdumber . (Circle One)

2-75-9108-95-262-53-31 1 1 .44.495-57-8541-73-1106-46-7100-51-695-50-195-48-739633-32-9

N-NurosodimethylaminePhenolAnilinebisl-2-ChloroeihvDEtrier2-ChloroorienolT. 3-Dichlorobenzene1. 4-DichiorobenzeneBenrvl Alcohol1. 2-Dichlorobenzene2-MethylDhenolbis(2-chloroisoDroDyl)Etrier

106-44-5 |4-Metnvlohenol621-64-767-72-1

^8-95-38-59-1

83-75-5105-67-9

•65-85-0

N-Nitroso-Di-n-PropylamineHexacftloroethaneNitrobenzeneIsosnorone2-NitroDhenol2. 4-Dime:rivi3henolSsnioic Acid

111-91-1 ' b.sf-2-ChioroethoxvlMe!hane120-33-2 2. 4-DicnlorDDnenol120-82-191-20-3106-47-887-63-359-50-791-57-677-47-463-05-2S5-S5-4

1. 2. 4-TncMoroDenzsneNaontnalens4-ChioroanilineHexacniorosutaaiene4-Chlo.'o-3-MetnvlDnsnol2-Me:nvinaon;n3ieneHexacniorocvciooentadiene2. 4 6-7ncnloroon«nol2. 4. 5-Tncrilor03r»*riOl

9 1 - 5 8 - 7 1 2-Oioi-onacnjnaiene33-74~i 2-Nifoariii,ne131-11 -3 Dimethyl Phihaiate208-95-8 Acenao^tnvieneCA-C,°-'' 1 •> .'.Vf'iVaTWrlTi-t

^>9v,«>0<i>

S*f 6,03d

&<? 2 . O&&

^'2,0^0

•

\

CASNumber

og/Iorug/Kg(Circle One)

83-22-9 |51-28-5 J100-C2-7 j132-64-9 |121-14.2 |606-20-2 " 184-65-2 I70C5-72-3 185-73-7 -|100-01-6 |534-52-185-30-6101-55-3118-74-137-36-535-01-3120-12-734-74-2206-4-1-092-87-51 29-00-085-63-791-94.-,55-55-3117-S1-7213-01-=117.54.:205-55-:207-06-550-32-5•'93-35-553-70-3 '191-24-:

Acenasntnene2. 4-Dini:roerienol4-Ni:ro3henolOibenzofuran2. 4-Dtni:ro:oluene2. 5-Diri:ro:oiuer.eOiethybrstria.'ate4-Chloroorienvl-orienvletnerriyorene4-NitroaniIine4. S-Otnnro-2-Metrivbheno;N-Nnrosocicnenylamme (1 14-3romoonenvi-5rienvle:rie''HexacniorocenzenePsntaciilorosnenolP.-.enantnreneAntnrareneDi-n-5u:vioh;r.ala:e

|=luoran:h«neI Senztdine| ?vene1 5u-:yl&er.r>-!sn:naiate|3. j'-D'cniorosenzicine5en:a3)An;nracene

I D-s(2 • E:nvinexv:)?.-.:na:aisC-.rysene

D-n-Octvi Phtr.aiate5?^zo(Diîuo.'3n;nene3enim(-iu3r3n:neie5enzoi3:=Y''erie

jinssnoii 2. 3-cs'3ve-eO'ênrla n!An;nrac»ne

BsiIC^'C K ilr»rvi«.1»

•

•

j 1

disênyiamme

L

I "Tb. Bo.

T-

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C

Box 818. Alexandria. Virjmia 22313 703/557-2490

Organics Analysis Data Sheet



Date Extracted/Prepared:

CAS

zed- .....

?rrnr- ?~~4 S


1 Z 8&O

3^66

~ ytjlo

lo^l

;,/ (jjt^t_ -

CASNumber

83-32-9 I31-28-500-02-7 |32-64-921 -'.4-2

S05-20-2 "54-65-27005-72-385-73-700-01-6

534-52-185-30-5.01-55-311 8-74.1E7-36-565-01 -a120-12-784-74-2205-i4-QS2-87-5129-00-0S5-68-791-34.'.55-55-2117-31-721 5-01 -r117-54-0205-95-2207-05-950-32-5193-39-553-70-3191-24 -2

' fO A^f

Acenasiinene2. 4.0ini:ro=nencl4-Nitro3ner.o!Dtbenrofuran2. 4-Dini:ro:oIuene2. S-DinitrotOl'jer.e

Disthybhjhaiate4-ChloroD.kienv!-ohenvletharriuorene .

4-Nurcaniline4, 6-Dtnitro-2-f«'«etnvl5henolN *NiTr3SOCf£it€nvl3rninG (1)** * 3 f o rn o D ft & n v 1 * c rt s n v 1 c t 6 fHexacnlcrossnienePentachloroshsnolSu

i AninraceneiOi-n-5u:vbh:.ia!a!erluoraniMeneoenria'me?vrene

5L!!Yi5enrv:=r!;nal3:e3. 3'-0.cnioro5er-.ii(j.ne5en:K3iAn;nracene

|D'S<2-E:nvir-.exvi]=-:n3iateCnryseoe3.-o-Cc:vi Pn:.~,a:aieSer-.zooiriuorantnene3enia<)riu3ra.n;nene5en:cxaPvrene

|lns«no!l. 2. 3-C=!=vrer»e

1 Doer.;: a niAni-i-ac-ne5ei:o<c ^ i>s»rv'*ne


*

*

(l-)-Canne: 3e separates frofn CiC^

4/84

?7O. Box 818. AleMncna. Virginia 22313 703/557-2490

r Organics Analysis Data Sheet(Page 2)

r;rr


Concentration: \Lows) Medium (Circle One)

Date Extracted/Prepared:,£'-«'

CAS

;C

zed' .,....,_>— -

actor- , ' A£


ef 3 Jo

^3 i*fo

~g3&O

/8^O

V(jJ (/<*&**_

CASNumber

83-32-951-28-500-02-7

132-64-9•21-14-2606-20-2 "84-66-27005-72-385-73-7100-01-5534-52-185-30-6101-55-3118-74-157-86-585-01-3120-12-784-74-2205-44-092-87-5129-00-0S5-6S-791-94-;55-55-3117-51 -721 8-01 •=117-54-0205-99-2207-06-350-32-c-.93-39-553-70-2191-24-2

- i#JlJt


Acenasf.tnene2. 4-Oini:rcahenol4-NitroDhenolDibeniofuran2. --Dinitrotoluene2. 5-DinitrotolueneDiethvbnthalate4-ChloroDnenvl-ofienvletherrluorene *4-NitroaniIine4. 5-Dmitro-2-MetriYlDher,oiN-NitrosociohenvIamine fll4.3rorr!3onenvi-ohenYletr)erHexacnicrosenrenePentacMoroohenolPhenanthreneAnthraceneDi-n-Butviohthalate

(FluorantMeneSeniidinePyrene

ButviDenrv-iontnalate3. j'-O'cn.oroseniiome3en:3<3)An;nraceneSisi2-E:nvinexv!)Pr.:n3iateChrvsene

|Di-n-Oc:vi P^.tnaiai"senzooiriusramnene

|3enz3t»i=iuoran;nene|3enz»a!svrene(indenoil 2. 3-cii?vren«(Dioeczia ilAntnracene3ei!«c h ,»5»rv!ene |

(l)-Cannc; 5e sesaratea Irom

Form I 4/gi

L.........Organics Analysis Data Sheet

(Page 2)

Semivolatile Compounds_,.^-i

Concentration:^—-Eoy— Medium (Circle One)

Date Extracted/Prepared: ______________

Date Analyzed: _______

Conc/Dil Factor:

mberug/l orug/Kg

(Circle One)CASNumber

r

L"

L

C

62-75-S |106-95-262-53-31 1 1 -AA-4.

55-57.8 I541.73-1106-AS-7100-51-695-50-195-48-735633-22-9106-^t-S621-6-i-7

1*7.72-1J-S5-3

78-5S-138-75-5105-67-965-35-0111-91-1120-S3-2120-82-191-20-3105-^7-337-63-359-50-7Si-57-577"i7~i83-06-2S5-55--9 1 - 5 8 - 7aS-7A-i131-11-3203-S5-S99-C9-2

N-NurosodimethviarninePhenolAniline |bis(-2-Chloroe;hvnHther 12-Chloroohenol I1. 3-Dicftlorobenzene1. A-DichlorobenreneBenzvl Alcohol I1 . 2-Dichlorobenzgne I2-Meihvlohenol Ibtsf2-cMloroisoorooyf)Etrier4-MetnvlDhenolN-Nitroso-Di-n-ProoylammeHexacnloroeihaneNitrobenzeneisoohorone

( 2-Nitroonenol1 2. £-Dimethyl3henolI Ber.zoic AcidI S>s(-2-C^iloroe:noxv>WeThane| 2. i-Dicnloroonenol '| 1. 2. -Tncfilorooenzene| Nasntr.aiens| A-Cnioroaniime| Hexacnlorcsutaoiene| --Chlo'o-3-MetnvlcnenoiI 2-MenvinaD!-.ir-.3tene| ^exacnicrocvciODeniadiensI 2 «i o-~f icnioroonenol| 2. *. 5-Tf icnioro3n*nol

t 2-Cniofona:noaleneI 2 -Nitroarnhne1 Dimtrnvi Pninalate1 A;enaon;nvien;1 3-Uitroanilme

^2^

efH

* ^1

1I1

ug/! orug/Kg(Circle One)

63-22-5 15',-2S-5 |10O-C2-7132-ci-r121-'.i-25C5-::-2 " J5-i-6=-27005-72-335-72-71CO-C1-553i-:2--,SS-SC-c1C1-55-3118 -74-;37-35-535-Oi-e*.20- '.2-7S-i-7^-2205-iiOS2-37-51 29-X-OS5-6E-791-5--*.55-==-;: 17-s'-72-5- : - -=' i / •;•—-«"" 5.ii. ~

207-CE-S50-31-cTS3-3r-5£3-70-2isi-:--2

Acenas .tnene |

2. £-Dini;rc9heno! I4-Ni:rosnenolOibenzofuran2. £Oini:ro:oluene2. 6-Dini:rctolueneDietnvlsr.thaJate--ChioroD."i«nvl-ohenvle:nsrrluoreneA-NitroanilineA. 5-Oini:ro-2-iV4ethvlDhenolN-Niussocisnenvlarnine (1 )4-5rono3.ienvl-Bhenvle:nerHexacnicrooenrenePentacnlorosneno!PnenantnreneAnthracsnaOi-n-5urvlohtnala:erluorantneneSennoine| ?vren«3u!Yiw5rr>-!on;halat83. 3'-3>cniofoDen:iS!ne

|3en:5<3iAn:nraceneJD'S(2-E:nvinexvlp.-;:na;aje(C^rvse^S

|Di-n-Cc:vi Phrnalats1 5en:o(ri "uor3n:nene|3en;?i«;::iuora!-.:nene|5enio.'3!5vfene(Incenc-.l. 2. 3-ci!?ve-ieO'Secna MAninrac-ieSen;?;? ^ i'??rvien»

,•

1

1f11

ro'n> I </£.:

T

3. Bo* 81 3, Alexandria. Virginia 22313 703/557-2490


Semivotatile Compounds


Date Extracted/Prepared: ———;———————————

Date Analyzed: _______

Conc/Di! Factor:

(I£

CAS ug/l orug/Kg(Circle One)

CASNumber

ug/I orug/Kg(Circle One)

L

C

^•75-9108-95-262-53-31 1 1 .44.4

95-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-1-<l-95-3.d-59-183-75-5105-67-965-85-0111-91-1120-83-2120-82-131-20-3105-47-887-65-353-50-791-57-677-47-453-05-2S5-95-451 -58 -783-74.41 3 1 - 1 1 - 3208-96-899-09-2

N-NurosodimethvlaminePhenolAnilinebis(-2-Chloroethvl)Ether2-Chloroohenol1 . 3-Oichlorobenzene1 . 4-DichlorobenzeneSenzvl Alconol1. 2-Dichlorobenzene2-Meihvlo^enolbis(2-chloroisooropYnEther4-MetfivbnenolN-Niuoso-Di-n-ProDvlamineHexacnioroethaneNitrobenzeneIsoohorone2-Nitroohenol2. 4-DimethylphenolBer.ioic Acidbis(-2-Chloroe:noxvlWeihane2. 4-Dicnioroonenol1. 2. 4-TncMloroo«nzeneNaontnaien"4-CnioroanihneHexacnioroDutaaiene4-Chloro-3-Me:nvl3henol2-Me:nv"naon:r-.ai9neHexacntorocvciooentadiene2 4 6-"ncriloroon9nol2. 4. 5-TricrilorODr>9nol

2-Chioronac?it^aiene2-NnroanilmeDimetnvi PiithaiaieAcenao^t.iviene3-N'itroamline

/*9-

lib

53-32-951-2S-5100-C2-7132-64-S121-'4.2605-20-284-55-27005-72-285-72-7100 -01 -5534-52-'8S-3C-510T-55-3US -74-'.87-35-585-01-5'.2C-: 2 -784-74-2205-44-092-87-5129-00-085-65-791-34-;55-55-2117-51-7-* • r* *•* • •*. t a-\. •:1 1 7-5-- C205-sr-I207-C5-550-32-=lS3-2r -553-7C-3'91-24-2

Acena=!-.:ne.ie2. 4-Dini;ro3nenol4.Ni:roDfienolDsDenzofuran2. 4-Dini:ro;oluene2. 5-Oinitro!oiueneO'ethvls.-.thalats4-Chlo.'00'"ienv-'-ohenvletnerPi-jflrene '4-Nitroaniline4. 5-Oinitro-2-WetnylDhenolN-N;trosc-2iorienvlamine (')4-£ro.Tioonenvl-phenvle:fier|Hexacr.isrosenzenePenracniocosnenol?r.enar,inreneArnnracanaOi-n-Sjrvbntnalaterluoran:Men»SeniidmePvrens5u:Yi3err\'!ontha!ats3. 3'-0'C.iioroSennGine5en:>3iAn;nracene

|D'5i2-5:riv!nexv!)Pr.:.-ia!a:eC~'VSSH8

|~,.n-0c:vi Pfntnalates9r.;D»3iriuoran;nene

| 59'MOi*i"|uoraninene|59p;D.alS>vren9|ln-eiO:l 2. 3-CS!=vrene

|0'29".Sa nlAntnracsne

i3s~:>'c ^ ii?»rvie."»9

.-.c: 3s se;ai-aiea I

4/Si

, Bo* 818. Alexancria. Virginia 22313 703/557-2490

r,rE

Organics Analysis Data Sheet(Page21

Semivolatile CompoundsConcentration: Low Medium (Circle One)

Date Extracted/Prepared: —————————————

Date Analyzed: —————

Conc/Dil Factor:

Iit CAS ug/l or ug/Kg

(Circle One)

L

>2-75-9108-95-262-53-3111,44.4

95-57-8•541-73-1106-46-7100-51-695-50-195-48-73S533-32-9106-44-5621-64-767-72-193-95-373-59-133-75-5105-67-9

•65-85-0• 111-91-1

120-83-2120-82-131-20-3105-47-887-53-359-50-7SI-57-677-47-433-05-2S5-S5-491-58-783-74.4131-11-3203-95-899-C9'2

N'-NitrosodimeiiiylaminePhenolAnilinebis(-2-Chloroethvl)E:her2-Chloroohenol1. 3-Dichlorooenzene1 . 4-DichlorobenzeneSenrvt Alcohol1. 2-Dichlorobenzene2-WejnyiDnenolbis(2-chloroisooroovU£tne''4-MeinylonenblN-Nitroso-Di-n-ProDvlamineHexac.iioroeihaneNitrobenzeneIsoshorone2-Nitranhsnci2. 4.Qimethyl3henolSer.roic Acic!bist-2-CîloroeTôxy (Methane2. 4-DicnlorsDnenol1 . 2. 4-7nc!iloroD9n2eneNasnsnaiene4-CnioroanilmeHexacnlorocutaaiene4-Chio*o-3-Ma;rivionenoi2-Me:.ivir,aDn;r.a.ienei-iexac-lococvciODeniadiene2 4 5-7nc."iioroonenoi2. 4. 5-Tricnioraon«nOl

2-ChiO'ona:^tâi»ne2 -Niiroanilme

Dimetnvi Pntna'ateAcenao-^t^viene3-N'u.'oanilme

9 Y**

JVZO

VO?-O^

^J.00

1

CASNumber


83-32-951-2S-S100-C2-7132-64-91 21-'. 4-2606-20-2 "84-65-27005-72-386-73-7100-01-6534-52--.85-3C-6101-55-311 8-74. •,87-85-5£5-01-3'.20-12-7S4-74-2206-44-092-87-5129-00-055-65-7SI-Si-156-55-3 •117-31-72 18-01 -9l 17-5^-0205-59-2:07-C8-950-32-5193-35-553-70-3191-24-2

Acenaantnene2. 4-Dini:roanenol4-Nitro3heriolDibenzofuran2. 4-Dinitrotoluene2. 6-Dimiroioluer.eOiethvbhthalats4-Criloroohsnvl-ohenvletriarrluorene4-Nitroaniline4. 6-Oinitro-2-We:nvl3her,olN-NiirosoCiahenvlamme (1 )4.3romoDhenvl-prienvle:Me!'HexacniorooenrenePentacMorocnar.olPhenantfireneAnthraceneOi-n-BuTvbhihalaterluorantheneSeniidinepyrene5utviSsnrv!Dn;.-iala:s3. 3'-Oicnioro3eniicine5*n;o<3)An;nracen»

|Bis(2-Etnvlhexv:]P.-itr.aiaiejCrsrysene|Q.-n-Oc:vi ?h:.-.aia:sJ5enio(3i?iuo--an:ner>e|3enro(<i=luora''.:!iene|3enioiai:svre"ellnCeoot'i 2. 3-cS!?v'e?*.e|0>0enr(a hlAntnracenei3e".:?!c i iiPervie.i?

#

•

(l)-Canno: De sesarated Irom

Fofii I 4/£i

H.!(i

P.0.8o*8ia. Alexancna. Virginia 22313 703/557-249O

n•p

L

IL.

L




Date Analyzed: ____________________

Conc/Dil Factor:

CAS ug/l or ug/Kg(Circle One)

.2-75.910B-95-262-53-31 1 1 .44.4

95-57-8541-73-1106-45-7100-51-6 -95-50-195-48-739638-32-9106-44.5621-64-767-72-1"S-95-3/8-59-188-75-5105-67-9

•65-35-011 1-91-1120-83-2120-82-191-20-3105-47-337-63-359-50-791-57-677-47-.:63-06-295-95--91-58-733-7d.c131-11 -3208-95-399-C9-2

N-NitrosodimethylammePhenolAniline&is(-2-Chloroethvl)E:her2-Cnloroohenol1. 3-Dichlorobenzene1 . 4-Dichlorobenzene3enzvl Alcohol1. 2-DichIorobenzene2-Methvtohenolbisf2-ctiloroisooroovl)£ther4-MetnvlphenolN-Nitroso-Oi-n-ProDylsmineHexachloroethaneNitrobenzeneIsoahorone2-Nitroahenol2. 4-DimethylDhenolSer.roic Acrdbis(-2-Chioroe:.ioxvtMethane2. 4-DicnloroDnenol1. 2. 4-TncMorooenzeneNaantnaiene4-ChioroaniimeHexacnlorcsutaoiene4-Cl".lorc-3-.V.s:nvioMenol2-Ms:nyir,aor'.;r.aieneHexachiorocvclcoentaoiene2. +• 6-7ricriloroonenoi

2. 4. 5-Tncnior03n«nol

2 •Chioronac.'Mâiene2 -Niiroamlme

Ormetnvi PhthaiateAcenaohtriviene3-Nitroanil.r.e

•z*?r"

/Z fO

^^sx?

2./Z3

CASNumber

ug/Iorug/Kg(Circle One]

83-32-951-28-5100-02-7132-64-9'.21-14.2505-20-2 "64.66-2 i7005-72-3 |86-73-7100-01-653-1-52-185-30-6101-55-3118-74.',87-86-535-01-5120-12-7BA.7f.-2206-44-052-87-51 29-00-085-68-7S 1-54-155-55-3117-81-721S-0-.-51 1 7-5--C205-95-2:o7-oe-950-32-5193-3?- =53-70-3191-24-2

Acenas^:ner>»2. A-Oinitrosnene!i-NitroohenoiOibenrofuran2. ~-Dini:ro:ofuene2. S-Dinitro'.oi'jeneOiethybMthaiarc |--Cfiloroorienv.'-cnenvleinerriuorene '•i-Nitroani'ine•i. 6-Oinitro-2-.V.etivl5r>eroiN-Nitrosocicnenvlamine fl)-•3ro."no2nenvi-ohanvle:rie''Hexacnlcrossr'.ienePentacfiioroDnanolpr.enantnrene

I Anthracene|0i-n-5utvi3hrr.a!a:eIrluoranthenssenridine3vrene

1 3utvlSen^-!sn:na:at9|3. j'-Oicnicrcserîicine

Senzs-aiAninracerie|D'S!2-E:nvine«vii?-.:."ia!a:eCnrvsene

|Di-p-Cr:vl ?!-.:.-.a;a:=5e^zo<D!=iu5ân:nene3enioi*!-iuo''a";~ene

|3er.i»a!=yreê|inieictl. 2. j-cr^veêiD'oeniia MA-.:nra;»n»Ee'rr'c "i i!=»r.i»-»

Ol-Canno: Se separates from

Form I 4/Si

P. o".~Boa 818. "Alexanoria. Virginia 22313 703/557-2*90



Date Analy

Conc/Dil F.. -t

• CASNumber

"— '

[1.

[..

;:

i.Lf "

LIti1

^•75-9108-95-262-53-31U-44-4

95-57-8541-73-1106-46-7100-51-695-50-195-43-73S538-32-9106-4^-5621-64-767-72-198-95-3>8-59-l

N-Nitrosodim«thvlaminePhenolAniline5is(-2-Cl"»loroetrivllErner2-Chloroohenol1. 3-Dichlorobenzene1, A-DichlorobenzeneBenrvl Alcohol1. 2-Dichloro&en:ene2-MethylD'ienoIBisf2-chloroisoorcayl}Etrter•4-MetMvlpnenolN-Nitroso-Di-n-ProDylamineHexacMoroethaneNitrobenzeneisoonorone

88-75-5 1 2-Niirochenol105-67-9 2. 4-DimethylDrierio!

•65-85-0 3enzoic Acii1 1 1-91-1 |ais(-2-Chioroe:noxv)Me:fiane120-83-2120-82-191-20-3105-47-887-63-3

2. 4-Oicnloroofienol1. 2. 4-TnchlorooenzeneNaontnalene4-C."iioroanilineHexacnlorosucaaiene

59-50-7 A-Chloro-3-Me:rivio«enoi91-57-6 2-Metnv»na3!".:r.aiene77--i7-~ HexacMcrocvciooeniafliene63-05-2 2. 4 6-TncnioroonenoiS5-55-4 2. 4. 5.TncnioroD"»noi9 1 - 5 8 - 7 2 -Cfiioconacntriaiene33.7^.^ 2 -Nucoaniline131-H-3 Oimethvi Phtha'aie203-95-8 Acenao^tnviene99-C9-2 3-Nuroaniiir.e

red- . ,.,,....,„„.,, .. , „,nnr. T^âJ Uf6&+~Jl ~ M*d[


/ f f. 3^

75,3<>^>

V9V, 3a0

21,5-60

CASNumber

83-32-951-28-500-02-732-64-921-1A-2

606-20-2 *64-66-27005-72-386-73-700-01-6

534-52-185-30-6101-55-3118-74-187-86-585^)1-8120-12-784-74-2206-14-0S2-87-51 29-00-065-65-791-94.155-55-3117-81-7213-01-9

Acenasnrne2. A-Dinitro4-Nitrooîen

Dibenzofura2. 4-Dinitro-2. 6-DinitroOiethybhth4-ChloroDh

rluorene4-Nitroanili4. 6-DinitrcN-NiKOSOCP

4-8fornoonHexacnioroPentac.MorcPhenantnreAntnraceneD'-n-3uTvbriuorantnerSenndinePvreneSutyi&enry!3. 3'-D'cnicSenjwaiAnois(2-E:rivtrCîrvsene

M 7-54-C |D.-n-0=:vi205-S5-2207-06-950-32-81S3-39-S53-70-3191-24-2

5en:o(Dirivj3en:o(*)=iu5enio«aiavIndenoil 2D'Oen::a r\3sn;c>(c "i

(l]-Cannot 5e seoa'aied from


OiOMenyUmine

L 4/34

T~ P.O. 6ox818. Aleiancna. Virsmia 22313 703/557-2490

rrcPci.

i

i

c




Date Extracted/Prepared: ———;___________

Date Analyzed: _——i————————————————

•b -3 -y '

Conc/Dil Factor:

CASNumber


*^-75-9,05-95-262-53-31 1 1 -tt-.4

95-57-8541-73-1106-46-7100-51-695-50-195-43-739538-32-9106-A4-5621-64-767-72-193-95-3'"V59-1oS-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-387-63-359-50-791-57-677-47-4

63-05-255-95-491-58-7aa-74.4131 -11 -3203-95-899-C9-2

N-NiirosodirnethylaminePhenolAnilinebis(-2-ChloroethvllEtner2-ChloroohenoI1, 3-Dichlorobenzene1. A-DicMorobenzeneBenzyl Alcohol1. 2-Dichlorobenzene2-Meihvlohenolbis(2-c.fc>loroisoDrcpyl)Ether4-MethvbhenolN-Nitrcso-Oi-n-ProDvlammeHexacnioroethaneNitrobenzeneIsoonorone2-Nitronhenol2. 4.Dime:fiylphenol3enzo»c AcidSis(-2-CMioroe!hoxv)Me?hane2. A-Dicnioroorienol1. 2, 4-TncîlorooenzeneNaonjnaiens4-ChioroanilmeHexacrHorcsutatiiene4.Chloô-3-Wetnvlonenoi2-We:nyina3ntnaieneMexacnicrocvciooentadiene2. 4 o-'ncriloroonenol2. 4. 5-TncMOCODn*nol

2-Chiofonacritriaiene2 -NuroamlmeOimetnvi Pfiiha'aieAcenaomnviene3-N'nroaniiine

-LK.,^*

K.130

r8* QGO

_?r,33<>

CASNumber

ug/l or ug/Kg(Circle One!

S3-32-951-28-510C-C2-7132-6^-9121-1 4-2S06-20-2 *84-66-27005-72-385-73-7100-01-6534-52-135-30-6101-55-3118-74-187-35-5S5-01-3120-12-784-74-2205-44 -092-87-5129-00-085-65-791-94.;56-55-3117-81-7218-01-5117-54-0205-99-2:07-C6-950-32-8193-35-553-70-3191-24-2

Acenas-.:r>ene2. 4-Oim:rca-fcienol4-Ni:ros">enolDi&enzofuran2. --Dini;rc:oluene2. 6-Oim:ro!oi'jeneDierhvlshtnalate4-Chloroohsnvl-ohenvletrierriuorene4-Nitroaniline4. 6-Dirnrro-2-MetnybhenoiN-Nitrosoccrtenvlamine (1 )4-Brornooh»nvl-phenvle:nerHexacr.ioroSenienePeniacMoroDheno!PnenantnreneAnthraceneOi-n-5u:vbhiha!aierluorantnene3snzidinePyreneButyiserrN-ionthaiata

|3. 3"-Dicr,ioroSe.".2iaine|5€n:>.3:An:nracen»|Dis(2-E:nvir-,exv!)?n:nalateC?".rvss"e

p.-n-Cc:vi Phtnaiat-5e.ij3<r:?iu3ran:nerie3er.;^*j:!uor3n;nene3en:Dia.'avrer<eIncsnc:' 2. 3-ci!3vreê3oen;:a fiiAn;nracerie3e^.;c>''c ^ 'l?»rvien»

,•

{1 l-Cannot 5e sesaratefl (ro^ ai

4/Si

r.r - - ; f Organics Analysis Data Sheet

{Page 2)

r Semivolatile CompoundsConcentration: /Low ) Medium (Circle One)Date Extracted/Prepared: _____________Date Analyzed: _Conc/Dil Factor:

-•>£ASf umber~i

-•

--

^

*-*.-

r "••L_

1

i .

• ug/1 or ug/Kg; (Circle One)

62-75-9 JN-Nnrosodimetr»ylamme108-95-2 |62-53-3 --:,|111-A4-4 *

95-57-8541-73-1106-46-7 j100-51-695-50-195-&S -739633-32-9106-4Z-5521-64-7,67-72-1

8-95-3

PhenolAnilinebisf-2-ChloroetnvnEtner2-Chloroohenol1 . 3-Dichlorobenzene I1. A-Dichlorobenzene 1Senzvl Alcohol1. 2-Dichlorcben-ene2-Mejnvlohenol | -bis.'2-chloroisoBroDyl)£ther

| A-Meir.vlohenol| N-Nijroso-Di-n-Proovlamme |Hexacnioroethane INitrobenzene

78-59-1 Iscohorone88-75-5105-67-965-85-0111-91-1120-83-2120-32-191-20-3

2-NiTroohenol2. 4-Di.T»ethyl3henolSenioic Acidbisf-2-CîoroeôxvlMeThane2. A-Dicnloroonenol '•1. 2. 4-7ncliloroDen2sneNasr.;r.aiane

105-47-3 4-Chioroamiine£7-68-3 Hexacnioroautaoien*59-50-7 4-Chlcro-3".Me!:wlon9noi91-57-6 2-Me:nvma3n;naiene77-^.7-4 "lexacJiicrocvciosentacJiene83-06-2S5-S5-491-58-7£3-74-4

2 4 5-~f icniorosnenol2. 4. 5-Tnc."ilOf03"enol

2 •CMofonac.'itnaiene2 -Nuroaniline

i3 i- l " i -3 DiTi»tnvi Pmnaiaie203-95-3 A:eriao."i:nviene93-C9-2 2-^nroaniline

*

iooo

^3ô\11

1

CASNumber


83-32-9 I51-28-5 11OO-C2-7132-64-9•;2l-*4.2505-2C-2 "_J84-65-270O5-72-386-72-7100-C1-5534-E2-'.85-3C-5101-55-3118-74-*,87-8=-=35-01-e120-12-784-74-2206-4-t-O92-87-51 29-CC-O35-65-791-54.;55-=:-211 7-=' -72:8-:-.-s1 1 7-ji. 2205-sr-2207-C3-350-32-=•93-2r-553-70-31S1-2--2

Acenas .tnen* |2. A-Dim:rc3heno! |4-NitroDênolDibenzofuran2. 4-Oins:ro:oluene2. 6-D'mi:rc!oiuer.eDie:hv!s.-.:hala:e4-ChlBroonenvi-ohenvle:nerrluorens4-Niuoaniline

4. S-Dmi:ro-2-f''etnybhenolN-Niussocisnenvtamtne (1)4-8romo3'ienvl-Dnenyle:r>erHexacnisrooenrenePeniscrtiorosnenolPhenantnreneAmnraiene

Di-n-5uTvbh:hala:ertuorantnene|3enridine| Pyr eneSuiyica.-.rfisntnalate3. 3'-3'cmorobenriiSine

j3enrs.-a;An;nracene

o«s<2-s:.ivir>exv!)?:".:natai»Cnr%-s«ne

jDi-n-Or.vi Phtnalate|senio<3i-'uof3n:nene|3e".r:M<;-iuoran;.''>eneIBeniD-'a^vfsneInsenoil 2. 3-ci'?vene

O'Denra niAntnraceneloe'rr-'; K i'~«rvie^*

/<T6£>

<-t(^0

*

^t'ôo •

l?80<1/6<)

IgQ

<r/o

!w3"50

om dignenYUrnme

roi n\ I

_r~—-_

P.O. Box 818. Alexanana. Virginia 22313 703/557-2490

rr

n


_ . -7 Semivolatile Compoundsc fa i /*Concentration: <£sv? Medium (Circle One)


Date Analyzed: —————————————————————

[ 3^2-5"

: A

Conc/Dil Factor:

CASNumber


>75-9108-95-262-53-31 1 1 .44-4

95-57-8541-73-1106-45-7100-51-695-50-195-43-739638-32-9106-44-5621-64-767-72-198-S5-3"S-59-133-75-5105-87-965-85-0111-91-1120-83-2120-32-191-20-3105-47-837-63-359-50-791-57-677-47-433-06-295-95-491-58-733-74-4131-11-3203-95-399-C9-2

N-NitrosodimethylaminePhenolAnilineDis(-2-Chloroethvl)E:her2-Chlorool">enol :—• •1. 3-Dichlorobenzene1 . 4-DichlorobenzeneBenzyl Alcohol1. 2-Oichlorobenzene2-Methylohenolbis(2-chloroisoDroDY')Ether4-MethylphenolN-Nitroso-Oi-n-?rooylamineHexachloroethaneNitrobenzeneIsoohorone2-Nitroonenol2. 4-DirnerhylDnenolBenzoic Acidbis(-2-C>Moroe:noxv)Methane2. 4-Otcnloroonenol1 . 2. 4-Tnc!iiorooenzene

1 Naontnaiene4-ChloroaniimeHexachlocccutaaiene4.Chlor0.3-MetnvlDnenol

|2-Metnvtnaai;r.aieneHexacMorocvciODentadiene2. 4 6-Tncriloroonenol

2. 4. 5-Tncrilorooi"»*i"»Ol

2-Chlor0na;.niM3iene2-NnfoamimeOimetnviPhthaiaie

lAcenaorx-wieneI 3-'Ji«roaniline

-

3Y>"D

CAS.Number


83-32-951-28-5100-02-7132-64-S121-14-2605-20-2 '84-66-27005-72-386-73-7100-01-6534-52-'.85-30-6101-55-3118-74-137-86-585-01-8120-12-784-74-2205-4-i-OS2-87-5129-0-0-085-68-791-94-155-55-3117-81-7218-01-S117-34-0205-9S-2:07-C3-950-32-5193-39-553-70-3191-24-:

Acenaontnene2. 4-Diniuoghenol4-NrtroohenolOibenzofuran2. 4-Dinitrotolu«n«2. 6-DinitrotolueneDiethylpnthalate4*ChlotODhenyl-onenvletnerrluorene4-Nitroaniline4, S-Oinitro-2-MetnvlphenolN-Nnrcsociohenylamtne (1 )4-8romODhenyl-pnenvle:herHcxacnlorob«n;enePentacMloroortenolPhenanthreneAnthraceneDi-n-ButvtohthalateriuorantneneBeniidinePvrene3utv'&enr>'lsntnaJate3. S'-O'cniorobenjiome3en:a3iAn;nracen«Dis(2-£:nvinexvl)Pr::natate

[ChryseneDi-n-0c:vl PhtnaJateaenio<S)rluorantnene3enio<i<)sluor3rt:r>eneseniotalPyreneIndenod 2. 3-c3!?ve^e0'Deiiia hlAi:rirac»ne

l3eni?(o h ilPerviene

A.&*0

^riO

«

6 3 3 o •

5T3VO

I3.&

Wo

: 3e sesarated (rom

Form I 4/SC

So*aia. Alexandria. Virginia 22313 703/557-2*90


— ..X- •-

"2.

rr~t -

(-•L,

•"'-.

(

r)1..1 :

i

-fyU>000 >.

_ —————— ——— '—' ————

UjJJS^k^

CAS

J2-75-9108-95-262-53-31 1 1 .44-4

95-57-8541-73-1 i106-46-7100-51-695-50-195-43-7

t&wJ. cî<" Concentrati

Date Extrac

Date Analy,

Conc/Dil F«

N-NitrosodimethylaminePhenolAnilinebisf-2-CriloroethvHE:her2-CMoroohenol1. 3-Dichlorobenzene1 . 4-Oichlorobenzene

Semivolati

on: Low

ted/Prepared:

red-

e Compounds

Medium (Circle One)

,-

actor:

ug/l orug/Kg CAS(Circle One) Number

Senryl Alcohol |1 . 2-Dichlorobenzene2-Methybhenol

39633-32-9 j bis(2-ch[oroisoDropyl)Etrter106-44-5621-64-767-72-1,98-95-378-59-188-75-5105-67-965-85-0111.91-1120-83-2120-82-191-20-3

4-MetrtylDhenolN-Nitroso-Di-n-PrcoylammeHexacrtioroetnaneNitrobenzeneIsoohorone2-Nitroohenol2. 4-Oimetnyi3henoISer.zoic AcidSis(-2-CMoroeThoxv)Me;hane2. 4.DicnloroDnenol1 . 2. 4-Trichlorooenz8n»Naonthaiene

1 05*^7 -3 £-C^lo*Q3nihne87-63-359-50-791-57-6

Hexachlorcoutaaiene

•>

/ V/o

—-C^'oô-3 - Wstn vbns not2 *^«1e*nvfna Dntns'enc

77-47-4 Hexacniororvclooentadiene83-06-295-95-4

2. 4 6-Tncriioroonenol2. 4. 5-Tncniaroon»iol

9 1 - 5 8 - 7 I 2 -Cf Qfcnacntâiene33-74.4 :.Nnroanilme131-11-3 Dimethyl Pht'iaiate203-95-3 Acenaonnviene99-09-2 3-%'nroaniime

IT-SO

83-32-91-28-500-02-732-64-921-14-2

506-20-2 "84-66-27005-72-385-73-700-01-6

534-52-185-30-6101-55-3118-74-1S7-85-535-01-8-.20-12-734-74-2205-44-092-87-5

Acenaontne2. 4.Dini:ro4-Ni:roDhenDibenrofura2. 4-Dinhro2. 6-DinitroOie:hybhth4-Chlorooh<riuorene4-Nitroanili4. 5-OmitroN-Nitrosodi4-3ro.TiODnHexachioroPentacrtlorcPhenantnreAntnracsnsOi-n-5utvlDFluoranther3enzidine

1 29-00-0 |3vreneS5-65-791-94-'.

3utvlSenr\-!3. 3'-0'cnic

55-55-3 5sn:»alAn117-S: -7 Dis;2--=:nvir218-01-9 ICiryseneM 7-84-0 p.-n-0c:vl205-99-2 senzooirii.:07-C3-9 |3en;r<<j?i(j50-32-5 |3enzo<aPv193-39-5 |lncenod.253-70-3 jOioeoiia n.191-24-2 |3en;?<c hi

(IJ-Canno: 5e sesaratea from

i -Z"


4/8-1

. P . O . Box 818. Alexandria. Virginia 22313 703/557-2450


Semivolatile CompoundsConcentration: Low fftfediurrp" (Circle One)


Date Analyzed: .—————

Conc/Dil Factor:

CASNumber


L

L_

,

'

1

12-75.9108-95-262-53-31 1 1 -44-4.

95-57-85*1-73-1

N-NitrosodimethylammePhenolAnilinebis(-2-Chloroethvn=!ner2-Chloroohenol1. 3-Dichlorobenzene

106-^6-7 1 1. 4-Dicnlorobenzene100-51-695-50-195-A8-739633-32-9106-44-5621-64-767-72-193-95-378-59-183-75-5105-67-9

•65-85-0111-91-1120-83-2120-82-191-20-3106-47-3S7-6S-359-50-7 .91-57-677-47-4

Benrvl Alcohol1 . 2-OicNorobenzene2-MethylohenolbiS(2-cr»loroisODrooyl)Ether4-MetnvionenolN-Nitroso-Di-n-PrcovlamineHexachioroethaneNitrobenzeneIsopnorone2-NiTrosnenol2. A-DimeihylphenolSenzoic Acid&'S(-2-Chloroe:noxv)Methane2. A-Dicnloroonenol1. 2. 4-TnchloroDenzeneNaonmaiene4-CrtioroamimeHe'xacn!orccut30ien«4-Chloro-3-.*/e:nviDênoi2-Me:nviria3''.:r-.3ieneHexacniorocvciooeniaaiene

83-06-2 2. «i o-'fcriioroonenoi55-55-4 2. <i. 5-Tfcniofoo"e«oi9 1 - 5 6 - 7 j 2-CMorona=.-unaiene93-74-4 2-Nttroanilme

1 3 1 - 1 1 - 3 Dimetnvi Phthaiate208-55.899-05-2

Acenaoritrwiene3-Mttroanilir.e

-

IZl&o

SOIÔQ

CASNumber


83-22-551-2E-510C-C2-7132-64-512* -"4-2505-20-2 *54-56-27005-72-385-72-71OO-C-.-553--52-135-3C-6'.01-55-3< « Q •* * «. i C-/*-- »

57-3=.=85-01-5-.20-12-734-74-2205-4-i-O52-87-512S-OO-0B5-6S-79'. -54.:E 5 - 5 5 - 31 f,7-c1-7«. i C -<w ' • »

i * / -5~ *C:o5-s5-:207 -CH- 55C-32-E1=3-3 = - =53-70- ji9i-S4.:

Acenaontrtene2. 4-Oini:rcDrienot4-NitroanenolOibenzofuran2. A-Dinitro:oluene2. 6-OinitrotoiueneDietnylpnthalate-•Chloroohenv'-orienvletrierriuorene4-Nitroaniline4. 6-Dmitro-2-Met!"ivl3her\olN-NitrasociDnenylarnine (1)4-3romoo."ienvi-phenyle:herHexacnlorosenzenePenta:riioroorienolPhenantnreneAntnraceneOi-n-SjTvl2î:.*ialaierluorantheneSeozidme?vreneSutyibenrvionthalate3. 3'-OicnioroDenzicme5en;a3)Ar\;.iracene

| Bisi2 -E:nv(neivl|Pri:r.a!ais(Cnrvsene|3'-r>-0c:vi ?h:naia:»5enio\3!riuorantnene

|3eai?<«)::i-jarari;rieneSenioiai'vreneInceôil 2. 3-cs!?v«-er>eD'Benr!a niAntnraceie3e~ir^c " ii'srviene

yjô^

19. TOO

••

(1 )-Canr,s: se sesaâted Irom

4/8-

P. 0.60x813. Alexanoha. Virginia 22313 703/557-2450



Concentration: ( LoyJ' Medium (Circle One)


Date Analyzed: ______________,————;——

Conc/Dil Factor:

CASNumber

ug/l or<ug/K

c

L

/•K2-75-9

y

I

;

.08-95-262-53-31 1 1 -4Z.4

95-57-8541-73-1106-46-7100-51-695-50-195-43-739638-32-9106-44-5621-64-767-72-198-95-3^8-59-1jS-75-5105-67-965-85-0111-91-1

N-NitrosodimethvlaminePhenolAnilinebis(-2-Chlcroethvl)£:her2-Chloroohenol1 . 3-Oicnlorooenzene1 . A-OicnlorobenreneBenzyl Alcohol1. 2-Oichlorobenzene2-Meihvlohenolbis(2-cMloroisoDropyl)Ether4-MethvlohenolN-Nitroso-Di-n-?rcovlammeHexachioroethaneNitrobenzeneIsoonorone2-Niuochenol2. 4-Di.TiethvlphenolSenzoic Acidbisf-2-C^loroe:hoxy)Methane

120-83-2 | 2. 4.Dicnloro3nenol120-82-1 1. 2. 4-Tnchlorooenzene91-20-3 (Naontnaiene106-47-3 4-Cnioroaniime87-63-3 Hexacr.iorosutaaiene59-50-7 1 4-Chlo'o-3-Me:rivlohenol91 -57-6 | 2-Me:nvma3-.:naiene77-47-i Hexac^icrocvciooentadiene38-05-2 2. 4 6-TdcriioroonenolS5-95-4 2. 4, 5-~ricr\!oroor>'!i-iol9 1 - 5 8 - 7 2-CMofonac.nt."iaiene33-74-i 1 2-Nnroariiline131-11-3 | Dimemvi Pnthalate203-95-399-09-2

AcenasMnviene3-^'it'oaniline

-

<V/0

S-Z.HS

CASNumber

CM.ug/i orug/Kg

(Circle One)63-32-951-28-5100-02-7132-6-1-9121 -'.4-2606-20-2 '84-65-27005-72-3S6-73-7100-01-6534-52-185-30-6101-55-3118-74.137-85-555-01-8120-12-784-74-2205-J-i-OS2-87-5129-00-0S5-63-791-94-155-55-31 17-31-721 3-0" -S117-34-0205-55-2207-08-950-32-S193-39-553-70-3191-24-2

Acenasntnene2. 4-Oinitrcshenol4-Niuoohenol

Dibsniofuran2. 4-Oinitro:oluene2, S-OinitrotoiueneDiethvbhthalate4-Chloroohsnvl-orienvleTfierrluorene

4-N'itroaniline4. 6-Oinitro-2-Mei.lvlDhenolN-Nitrosocisrienvlamine (1)4-Sronooreftvl-Dnenvle:rierHexacniorosenienePeniacMorcsnenoiPnenantnreneAnthraceneOi-n-Sutvb^:^ala!erluoranthereSenridinePyrene3 uiY'Ser.rYlsntnaiate3. 3"-0'C."iicrobenricine3enraaiAn:nraceneDis(2-E:nvi":exvll.:>n;nalaisCirvseneOi-n-0c:vi Phtnaiate5enio<0)riuora.->;nene

|3enjc>(»)=i'_3!'3n;Mene(Beriooi'yrenemsanoil 2. 3-css?veneD'Denita ntintriraceieBenrc'i" h n??rvlen»

iioo

Sf£-

•

/a->* '

l li,o

1

(l)-Carinc: Se seaaraied from eiS'

6/84

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pir

L

flu





Date Analyzed: _____________________

Conc/Dil Factor:

CASNumber

ug/I ____(Circle Oriel"

";2-75-910B-95-262-53-31 1 1 .44-4

95-57-8541-73-1106-46-7100-51-655-50-195-48-73S638-32-9106-44-5 •621-64-767-72-198-95-3>8-59-188-75-5105-67-955-85-0111-91-1120-83-2120-82-191-20-3106-47-387-68-359-50-791-57-677-47-488-06-295-S5-4S l - 5 8 - 788-74.4131 -11 -3208-95-399-09-2

N-NitrosodimethylammePhenolAnilinebis(-2-Chloroethvl)Ether2-Chloroohenol1. 3-Oichlorobenrene1 . 4-OichlorobenreneBenzvl Alcohol1. 2-Dichlorobenzene2-Methylohenolbis(2-cnloroisoorouyl)Ether4-MeinylDhenolN-Niiroso-Oi-n-proDvlammeHexacnloroethaneNitrobenzeneIsosnorone2-Nitroorienoi2. 4-OimethylDhenolSenzoic AcidDis(-2-Cnloroeth0xv)Methane2. 4-Dicnloroonenol1. 2. 4.Tnc!"ilorooenzeneNaonmaiene4-ChioroanilmeHexacniorooutaaiene4-Chloro-3-Wetnvionenol2-Me:nvmaorur-.3ieneHexacniofocvctooentadiene2. 4 o-Tricnloroonenol

2. 4. 5-TncfiloroonAnol

2-Chioronacntnaiene2 -Nitrpamlirie

| D"Ti*Tr<vi Pntha'atfAcsna=ntnviene3-Nnroaniline

KiO

'

!

i

i1

!

:

1i

'•-'.

i1

CASNumber


83-32-951-28-5100-02-7132-64-3121-14-2605-20-2 "84-65-27005-72-386-73-7100-01-5 •534-52-186-30-6101-55-3118-74-187-85-585^)1-8120-12-784-74-2206-44-092-87-5129-OCOS5-6S-791-94-:56-55-31.17-81-7218-01-=1 17-34-2205-55-I207-CE-950-32-s1 9 3 - 2 S - 553-70-3191-24-2

Acenaontnene2. 4-Oinitroohenol4-NitroahenolDibenzofuran2. 4-Dinitrotoluene2. 6-OinitrotolueneDie:hybhtha!ate4-Chloroohenyl-ohenvletnerrluorene4-Nitroaniline4. 6-Omitro-2-Metrivl3henciN-Nitrosociohenylamme (1)4-Bromoonenyl-pfienyle:MerHexacnlorosenzenePentachloroohenolPhenanrhreneAnthraceneOi-n-5utybhthalaterluorantneneSenzidinePvreneButylbenrytonthalate3. 3'-Oicnlorooenziame3enio<a)AninraceneoiSi'2-E:nvinexvl)Pn:na:ate

|Chrysene|0i-n-0ctvi Phtnalate5enzo<D)rluor3ninene3en:o(<)?iuorantheneBenjoialPyreneIndenoi 1 . 2. 3-cii?vrene0<&enz!a hiAntnraceneBenzene K ilPervlene

\.'/^

it

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V_4/84

"p. 6. Bo* 818. Alexanaria. Virginia 22313 703/557-2*90


Semivolatile CompoundsConcentration: ^Cgv^ Medium (Circle One)


Date Analyzed: ————————————————————

35230

- C

Conc/Dil Factor:

CASNumber


CASNumber

ug/1 orug/Kg. (Circle One)

/

i1.0

T75-9.08-95-262-53-31 1 1 .i4-495-57-8•541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44.5621-64-767-72-198-95-3>e-59-id8-75-5105-67-9

•65-85-0

N-NiuosodimethylammePhenolAnilinebis(-2-Chloroeinvl)Ether2-CWoroohenol1. 3-Dichlorobenzene1. 4-DichlorobenzeneBenzyl Alcohol1 . 2-Oichlorobenzene2-MethvloHenolbis(2-cnloroisooi'ooyl)Ether4-MetnvlonenolN-NiTroso-Di-n-ProDvlamineHexachioroethaneNitrobenzeneIsopnorone2-Nitroonenol2. 4.DifT>etnvlDhenol3enzoic Acid

1 1 1-91-1 |bis(-2-Chloroe:!-ioxy)MeTMane120-83-2 | 2. 4-Dicnloroonenol1 20-82- 1 1 1 . 2. 4-7nchloroD«nzene91-20-3 Naomnaiens105-47-8 1 4-Cnioroanilme87-68-3 | Hexacniorosutaaiene59-50-7 4-Chlofo-3-Me'.nvloner.oi91-57-6 2-M«:nvinaon;r.aiene77-47-4

83-05-255-95-49 1 - 5 8 - 783-74-i131-11-3208-95-899-09-2

HexacMorocvciooentaOiene2.4 5-Tncmoroonenoi2. 4. S-Tncnioroon-nol

2-Chioronacnnatene2 -NitroanilmeOim«tnvi P^tnaiateAcenaontnviene3-N'nroanihne

-

/Pcjo

S*5?^

83-32-951-2B-5100-02-7132-64-9121-14-2506-20-2 "SA-65-27005-72-386-73-7100-01-6534-52-'.85-30-6101-55-3na-7^-'i87-85-585-01-8120-12-78i-74-2206-i-i-O92-87-51 29-00-0S5-68-791-9-i-l55-55-3117-21.7216-0'. -9H7-S--0205-59-2207-CS-950-32-c193-39-553-70-319'. -24-2

Acenacntnene2. 4-Oinnroohenol4-NitroDhenolDibenrofuran2. 4-Dinitro:oluene2. 6-OinitrotolueneOiethvbhtiiaiate4-ChlofODhenvl-Dnenvle:nerriuorene4-NitroaniIine4. 6-Dinitro-2-MetriYbnenclN-Niirc-soeiDhenvlamine (')-•BroiDODnenvl-pherivlet^ei'HexacniorooenrenePsntachloroohenolPnenanrnreneAntnracsneDi-n-5utvbh;halaieFluorantheneSenzidinePyreneSutvl&er.rvlontnalats3. S'-O'cnioro&enzicme5en;o.;3)An;nracene

|&iSi'2-E:nvlnexvi)P^tn3:ateCnrysene

|Di-n-Oc:vl Phtnaiaiesenzooiriuorarv.nene

|3enjo(M-iuor3o;nerie|5enz«a>svrene(incenoii 2. 3-c3!?vre"eiD'Oenr.a hiAn;nraceieiBenzc^o h ilP»rvlen«

t

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r

f;nO


Semivolatile Compounds^ --——— -Nj

Concentration: Low ClMediurrj-y (Circle One)


Date Analyzed: ______

3523

Conc/Dil Factor:

CASNumber

ug/l(CircTe One)[_.'

;Et

)/•*

'

\

^

•"S- 7-5-9.08-95-262-53-31 1 1 .44.4

95-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5521-64-767-72-1 j98-95-3^8-59-138-75-5105-57-9

•65-85-0111-91-1120-83-2120-82-191-20-3106-47-837-63-359-50-791-57-677-47-483-06-2S5-S5-49 1 - 5 8 - 738-74.4131-11-3208-95-899-09-2

N-Nitrosodimethy!ammePhenolAnilinebis(-2-Chloroetnvl)Ether2-Chloroohenol1 , 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzy< Alcohol1. 2-Oichlorobenzene2-Methylohenolbis(2-chloroisooroDyl)Ether4-MetnvlphenolN-Nitroso-Di-h-ProoylammeHexacnloroethaneNitrobenzeneIsoohorone2-Nitroohenol2. 4-DimeihylohenolSenzoic Acido.s(-2-Chioroei.n0xv)Metnane2. 4-DicnloroDnenol1. 2. 4-7richlorooenzeneNaontnalens4-ChioroaniiineHexacnlorcoutaoiene4.Chloro-3-Metnvlsnenol2-Me:nvinasrw.aieneHexacnic-ocvciooentadiene2. 4 5-Tncriio'oorienol2. 4. S-Tricnioroonenoi

i 2-Chiorona:.-n->aiene2-NnroanilmeOirnptnvi P ritâiateAcenao^t^viene3-Nnroanil.ne

-

7.(C< o4^

300^0^*0

CASNumber


83-32-951-2S-5100-02-7 j132-64-9121-14-2606-20-2 "8-1-65-27005-72-386-73-7100-01-6534-52-185-30-6101-55-3118-74-187-35-535-01-3 -120-12-784-74-2206-44-052-87-5129-00-085-68-791-94.',55-55-3117-S1-7218-01.-9117-54.0205-9S-;207-08-950-32-8193-39-553-70-3191-24-2

Acenasntnene2. 4-Oim:roohenoi4-NitroDnenolDibenzofuran2. 4-Dini:ro:oluene2. 6-DinitrotoiueneDieihybrsthalate•i-ChlofOSdenvl-ohenvletherrluorena•i-Nitroaniline•i. 6-Dinitro-2-.V.etnvlsher,olN-NitrosoCionenvlamme (1)•i-Sromoonenvl-ohenvleTfie-HexachlorooenienePantachloroshenolPnenantnreneAnthracsn-Di-n-Burvtoht-haiaterluoran;neneoenjidmePvrene3utvl5snrv!3n:n3late3. 3'-DicnlarooenzicineSenrwasAninracene5is(2'£:rivihexvl!?~:rialaisC^rvsene

pi-n-OcTv! Phrr.asate5enio<Di?iuG.'3n;ncne

1 3enrM*!5'uoi'an;êne5enro( a Gyrene

(infisnoil 2. 3-c5!av'eêl0'5en:!a h)Anf>rac»neiBenir'c ^ iP-rviene

Z^fjOW

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1 1 OO<3

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r


j _ - -, _ -,

(Lz\/fV4<~^~Semivolatile Compounds


\ '-3

Date Analy:

Conc/Dil Ft

.»— .

.

' CASNumber

' '

/

(•

[.

12-75-9108-95-262-53-31 1 1 .44-4

95-57-8541-73-V106-45-7100-51-695-50-195-43-739638-32-3106-44-5621-64-767-72-198-95-3'78-59-188-75-5105-67-9

•65-85-0111-91-1120-83-2120-82-191-20-3106-47-887-63-3

N-Nitrosodime'thylammePhenol :Anilinebisf-2-ChlordetrwMEther2-Chloroohenol1. 3-Dichlorofaenzene1 . A-OichlorobenzeneBenrvl Alcohol1 . 2-Dichlorbbenzene2-Methylohenolbis(2-chloroisooro3yl)£ther4-MetfiylohenolN-Nitroso-Di-n-PrcoylamineHexacfiloroethaneNitrobenzeneIsobnorone2-Nitroonenol2. 4-Dimethyl3henol3»nzoic Acidbis(-2-CMioroe!noxvlMethane2. 4-Dicnloraonenof1. 2. 4-TnchlorooenzeneNaoninaiene4-ChioroanilmeHexacniorcDutaaiene

59-50-7 4-Chioro-3-Me:rv/iohSnol31-57-6 2-Me:nvmaan:r.3iene77-47-4 Hexacnicrocvciooentadiene83-06-2 2. 4 5-Tncîo.'oonenoiS5-S5-4 2. 4. 5-TfiCMOrODnenol

91 ' 58 -7 2 •C'TO'onac^"âiene33-74.- 2-N'Uoaniline131-11-3 Dimetrivi Pntnaiate208-96-3 Acenaoînviene99-09-2 3-Niuoaniiine

-prf-

irtnr- _. __ ..__ _

f=>A<

-

6Z3o

^9-i^jO

cJ jVK^^f V-6-**-

CASNumber3-32-91-28-500-02-732-64-921-14-206-20-2 '4-66-2005-72-35-73-700-01 -634-52-15-30-601-55-318-74-17-85-55-01-820-12-7

Acenagntne2. 4-Oini:ro4-NiuoohenDibenzofura2. 4-Dinitro2. 6-DinitroDiethylohtri4-Chloroahrluorene4-Nitroanili4. 6-OinitroN-Nitrosoci4-aromooh

PentachiorcPhenantnreAnthracsn*

84-74-2 JDi-n-Sutvl:205-4-1.092-87-51 29-00-085-63-791-54-1

riuorantfieSenzidinePyrene3utylber.r,3. 3'-D>cni

55-55-3 |5an;aaiAr117-81-7 Dis(2-E:."ivi21S-C-S (Cnrysene117-54-C (Di-n-Ocivi205-9S-2 |5enio(3J?i207-06-9 |3ei".ro(<l=ii50-32-5 laenroja^v193-39-5 indenod. ;53-70-3 |D-ben:!a f191-24-2 (3en:!Nc h

(l)-Canno: 3e sesaraiea Irom

L


aiofenyiamme

Fo>ni I 4/S4

. O Box 81 a! Alexandria. Virginia 22313 703/557-2490

nOrganics Analysis Data Sheet

(Page 2)

' ^—4 ——— """"T0 .-71 O Ju L / ^ ' ^ ê^ (t C^^^X^M^Hf

_ V ' Concentrati

Date Extrac-.'

Date Analy.

' ' Conc/Dil F«

•-•

• ;' CAS

Number

D*i

->

\ ,.

\ \i....

L'\

\

r

^t-75-3 '.J8-95-262-53-31 11 -4A-4

95-57-8541-73-1106-46-7100-51-695-50-195-43-739638-32-9106-44.-5621-64-767-72-198-95-3N8-59-1o3-75-5105-67-965-85-0

N-NitrosodirnethylammePhenolAnilinebis(-2-Chloroethvl1Ether2-CMoroohenol1. 3-Oichlorobenzene1. 4,-DicniorobenzeneBenzyl Alconol1. 2-Diciilorobenzene2-MsihylDhenolbis(2-chloroiso3f03yl)Ether4-MetnvlohenolN-Nnroso-Di-n-ProoylamineHexac.'iloroethaneNiirobenzeneIsosnorone2-Nitrocnenol2. 4-OimethylohenolBer.zoic Acid

1 1 1 -91-1 orsl-2-ChloroeThoxytMethane

Semivolati

an-jr LovT") "

ted/Prepared

rpd-

i— > ~ *e Compounds

Medium (Circle One)

sctor: nr — / O i \ ) \l£~" jL/ V51— \ ^ JV10 M" \J^-^*-^~~^ —

ug/l orug/Kg CAS(Circle One) Number •

*

120-83-2 2. 4-Oicnloroonenol - |120-82-1 1 . 2. 4-Tncnlorooenzene91-20-3 Naonjnaiene105-47-3 4-C."iioroaniime87-63-3 | Hexacnlorosutaoiene59-50-7 4-Chioro-3-Me'..ivl3henol91-57-6 2-M5:nv<na3n:r-.oiene77-47-4 . | Hexacniorocvciooentadiene53-05-2 2. 4 6-~ricr\ioroanenol95-95-4 | 2. 4. S-Tncniofosnenoi3 1 - 5 8 - 7C3-74-4

131-11-3208-95-899-09-2

2-CMoronacntâiene2.Nltroan.lmeD'Tiatnvi PhthaiaifAcenaontriviene3-Nnroan.l.ne

£.1 S^>

_2 Joci

63-32-951-25-500-C2-732-S4-921-14-2

506-20-2 "34-55-27005-72-335-73-71OO-01 -6534-52-135-30-5 .'.01-55-3118-74-;37-35-535-01-3120-12-7

Acenaontnene2. 4-Oini:ro3henol4-NitroofienolOibenzofuran2. 4-Dini:rotoluene2. S-Dinitro!olueneDiethybhthalate4-Chloro3henyl-chenvFiuorene4-Nitroaniline4. 6-Omi:ro-2-Methyl3N-.NurosotfionenvIamn4-3rorno3nenyl-orienvHexacnioroaenzenePentacMoroohenolPhenantnreneAnthracene

34-74-2 |Qi-n-Butvloh:ha!ate205-^4-0 |riuoran;nene92-87-5129-CO-O55-55-7

SenzidinePvrene3utyiaenrv!3ntriaiate

91 -=4. ; -|3. 3'-0'cniorooenzi(3in(55-55-3 5en:cv,3lAn;nracene' 1 7-31 -7 &isi2-£:nvlnexvl)?~;na218-C1-3 |CnrYsene1 '7-34-C |D.-n-Oc:vi ?!i:naia:e205-55-2 5enzcXS!riuoran:nene207-CS-s SenicXul'iuorantriene50-32-c (39nzoiaisvrene193-39-553-70-2191 -24-2

Indsncil 2. 3-C2!?vre

O'Denzia filAntnracen

3?":cô n i)?»rvien5

(1 1-Canr.s: Se sesarated from ciofenviamif

= ICyV^


TT;

r;r,

D*0

:Dr!:

1 •(,'•

G

< -

•i \u.

C•Li

[ •1.

nvironmtfVal Protection Agency. CLP Sample Mar. 0. Bo* Slfiy AleWtoria. Virginia 22313 703/55

•M5^ °'

3~* n s\ *, Concentrat.ft D ~V 0 lÂP^j^m^Y ^' Date Extrac

~ IT 1 9 f?*/V ' • vffy DateAnaly

Conc/Dil F,

CAS""ûmberJ2-75-9108-95-262-53-31 1 1 -A4-495-57-8541-73-1105-46-7100-51-695-50-195-48-739538-32-9

• 105-44-5621-64-757-72-1 .^-95-3 •/3-59-138-75-5105-57-965-85-0111-91-1

N-Nitrosodime;hvlarninePnenolAniline •bis(-2-Chloroetrivl)Sther2-Chloroohenol1. 3-Dichlorobenzene1, 4-DicnlorobenzeneSenzvl Alconol1. 2-Dichlorobenjene

ia;ement OHice.7-2490

ganics Ana(Ps

Semivolati

on: /Cow j)

ted/Prepared,-PH-

lysis Data Sheetige2)

e Compounds ^

Medium (Circle One)

,_t_r. i_L/yûJr \SoJu^/»J*<L' 1 J\fJ^~

ug/1 o(ug/Kg^> CAS(Circle One) Numb«r

2-Metnylohenoi 1biS(2-cnloroisooropyl)E:rier |4-Metnylohenol | "N-Nitroso-Di-n-Prooylamme |HexachloroerrianeNitrobenzeneisoanorone2-Nitraonenol2. 4-Dime!hyi3rienolBenzoic Acidbis(-2-CMoro*!hoxvlMe:hane

120-83-2 2. 4-Oicnloroonenol120-82-1 1. 2. 4.7ricMorooenzene91-20-3 Naon;naien« ^(f^fO106-47-3 4-Crtioroaniime87-53-3 Hexacniorccutaaiene59-50-791-57-6

4.Chloro-3-Metnvt3nenol2-Me:nvina3n:r.3tene

77-47-4 Mesacntorocvciooentaêne33-05-2 2. 4 6-Tncnioroonenol

)Q5OO

S5-95-4 2. 4. 5-TnCilOfOO.-i»no: |

91 -58-7 2-Chioronacn;naiene38-74-4 2 -Nitroaniime131-11-3 Oimetflvi PMtna'ais209-95-8 Acenaorv.ivieneS9-C9-2 3-Nnroanilme

83-32-91-28-500-02-732-64-921-14-2

606-20-2 '84-65-27005-72-386-73-7

00-01 -6534-52-185-30-601-55-318-74-1

87-86-585-01-8120-12-784-74-2206-44-092-87-5129-00-085-68-791.54-155-55-3117-81-7218-01-9117-34-0205-9S-2207-08-950-32-6•193-39-553-70-3191-24-2

Acenaomne2. 4-Dinitro4-Ni:reorienDibenzofura2. 4-Dinitro2. 6-OinitroDiethylphth4-ChloroohFluorene4-Nitroanili4. 6-OmitroN-Nitrosodi4-BromoonHexacnloroPentacnlorcPhenantnreAntnraceneDi-n-Butylorluorantrier3enzidinePyreneButyl&enry3. 3'-OtcnicSenzooiAndis«2-£:nyifCnryseneOi-n-0c:ylBenzcxairk

BenzcxaiPyIndeno* 1. 2DiOenzia hBenzo<a. n

(l)-Cannc: Qe separated Irom

Sample Numoar

4/84

' cov'-'on •lema.F'Otec.io , . i. *, P.O. Box 818, Alexandria. Virginia 22313 703/557-2*90


Semivolatile Compounds - »"Concentration: Low Medium (Circle One)

Date Extracted/Prepared: ———;—————:————

Date Analyzed: ______________________

Sample Numoer

Conc/Dil Factor:T>vC^J -= (D/v^

CASNumber

ug/l orujg/KsT(Circlel ^

CASNumber

ug/lorug/Kg(Circle Onal

I•\r

:./

i

'

I

- •

\

i-

^

--

\

^2-75-9108-95-262-53-3111-44-4

95-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-3'8-59-168-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-63-359-50-791-57-677-47-488-06-295-95-49 1 - 5 8 - 788-74-4131-11 -3208-96-899-09-2

^-NitrosodimethylaminePhenolAnilinebis(-2-Chloroethvl)Ether2-Chloroohenol1. 3-Oichlorobenzene1. 4-OichlorobenzeneBenzyl Alcohol1. 2-Dichlorobenzene2-Methylohenolbis(2-chloroisoDropyl)Ether4-MethylphenolN-Nitroso-Di-n-ProoylamineHexachloroetharieNitrobenzeneIsophorone2-Nitrophenol2. 4-OimethylphenolBenzoic Acidbis(-2-Chloroe!hoxv)Methane2. 4-Dicnloropnenol1 . 2. 4-TnchiorooenzeneNaphthalene4-ChioroanilmeHexachlorooutaaiene4-Chloro-3-Methvlphenol2-MetnyinaohtnaleneHexachiorocvciooentadiene2. 4 6-Tricnlorooneno!2. 4. 5-Tnchloropnenol

2 -Chioronacnthaiene2 -NuroanilmeOimetnvi PhthaiateAcenaohtnviene3-Nnroanilme

-

7Z8

83-32-951-28-5100 -02.- 7132 -64.9121-1 4-2606-20-2 '84-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-3120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-31 17-81-7218-01-91 17-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2

Acenaphtriene2. 4-Dinitropnenol4-NitroohenolDibenzofuran2. 4-Dinitrotoluene2. 6-DinitrotolueneDiethylohthalate4-Chlorophenyl-phenyletherFluorene4-Nitroaniline4. 6-Dmitro-2-MethylphenolN-Nitroso<!iohenylamine (1 )4-Bromophenvl-phenyleTherHexachiorooenzenePentachloroohenolPhenaninreneAnthraceneOi-n-ButvlohthalaterluorantfieneBenzidinePyreneautyi&enrviDninalaTe3. 3'-Oicnloroi3enziairie3en:o(3)Antnracene6is(2-£:nvihexvllPntnaiateChryseneOi-n-Ocwl PhtnalateSenzcXSlrluorantneneBenzol klPluorantheneBenzcXalPyreneIndenod. 2. 3-cd)?vreneOibenzia hlAntnraceneBenzcXo n ilPen/iene

.•

IOL

(l)-Cannoi t>e seoaraied from

Form I C/S-iI

f " f'O. Bo» 818. Alexanaria. Virginia 22313 703/557-2490•; • .


5,i>

F;n

/o

pi. /

Semivolatile CompoundsConcentration: Low feTediufn) (Circle One)

Date Extracted/Prepared: ———:———————————

Date Analyzed: .———————————————————

Conc/Dil Factor:

CAS ug/I orug/Kg(Circle One)

Lrr.hi

i:Vi <

i •.i

CV '

U

1 •L-

1 '

^2-75-S1 0S-9.5-262-53-31 1 t -4^-4

95-57-85*1-73-1106-46-7100-51-695-50-195-43-739538-32-9105-44-5621-64-767-72-198-95-378-59-188-75-5105-67-9

N-NurosodimethylaminePhenolAnilinebis(-2-Chloroetnvl)Etner2-Crtloroohenol1. 3-Dicfiloroben:ene1. 4-OichlorobenzeneBenzyl AlcoholV. 2-Oichlorobenzsne2-MeinylDhenolbis(2-chloroisooropyl)Etner4-MetnvlonenolN-Nitroso-Di-n-?roDvlammeHexac.MoroethaneNitrobenzeneIsooriorone

2-Nitrooheriol2. 4-Dimethyl5henol

65-35-0 1 Berszoic Acid111-91-1 I t3is(-2-CMoroe:hoxv)Metfiane120-83-2 | 2. 4.Dicnloroonenol120-82-1 1. 2. 4-Trichlorooenzene91-20-3 Naomnaiene105-47-8 A-Cnioraaniime87-63-3 Hexacalorooutaaiene59-50-7 • 4.Chloro-3-.Mstnvlo«er,olS 1-57-6 | 2-Ms:~vinaontr.aiene77-47-4 HexachiorocvciooentacJieneS3-06-2 2. 4 6-TncniorocnenoiS5-95-4 2. &. 5-TncrilorODn»nol

3 1 - 5 8 - 7 . 2-Chioronac.it^3iene33-74.4 2-Nitroanihne

131-11-3 O'Tietrivi Pnthaiaie203-96-3 Acenaonirwiene93-C9-2 3-f.'iuoaniiine

-

T-,3**

'1&6&

CAS 'Number


83-32-951-28-5100-C2-7132-64-r121-1^-2506-20-2 *84-65-27005-72-385-73-7100 -01 -6534-52-185-30-6101-55-3118-74--.87-35-5£5-01-5120-12-784-74-2206-44-C92-87-5129-00-035-68-791-94--.55-55-3117-81-2" 8-0" -r1 1 7-5^-C

205-9=-;:07-C5-=50-32-5193-3 = - =53-70-2191-24.;

Acenacnrrvene2. A-Oini;ros.-,enc!4-Ni:ro3henclDibenzofuran2. 4-DmitroTolusne2. 6-Dimtrotc!uer.eDie:hybhtnal3:s4-Chloroohenv-!-pnenvie;nerPluorene4-Nitroaniline4. 6-Oinitro-2-i'-'e:r.vbhenoiN'-NiT.'0-Scxicne.nvi3mine (J )4-3rornoDnenvi-s.ienvle:.K.erHexacnioroser.renePentac^lorosfienoiPhena.-.tnreneAnthraceneDi-n-5jtvbh:f.a!a:srluorarstnene3enzicS:ne

|?vren»1 3uf.vlSsnz>'l3r.:na;a:e|3. 3'-0'C.iioro3enzicine|3enzw3iAn;nracer.e|S'S(2-E:nylnexv!|?-.:naiats|C^rvse."-eDi-n-0::vi ?h:nata:e3enzotD)r!uora.i:nene

|3en:n<!-iuora!-.:-ene1 3enzoia!svrene|!nc»no(l. 2. 3-C2!?vre-.e

|DiDen;!a MAn:iracenel3enzc>fc i iiPerviene

3>S10

•

•

3$$0

462.

6V^

(1 l-Canrc: 3e sesarated from

?otni I

P.O.Box 818. Alexandria. Virginia 22313 703/557-2*50

1

M


Semivolatile CompoundsConcentration: (J-ow^ Medium (Circle One)


CASnber

70H-

arror 'J*


«

y-to°

3?0^

n a.U-&JO/**ji ^

CASNumber

53-32-951-2S-500-C2-7

132-ci-S.21 -••4-2506-23-2Si-65-27005-72-386-72-7100-C1-553-4-5 2 •'.85-30-6101-55-3118-7.1.137-35-585-01-3120-12-78i-7i-2206-^-092-37-5129 -CO-035-63-791-5-.'.55-=£-311 7-5* -7213-C-.- =\ 17.=--:2C5-rr-2207-C=-350-32-S1S3-25-553-70-31S1-2- -2

• \()fp>*-jp

Acena-ntnene2. A-DiniTroshenoIA-NitroonenolDibenzofuran2. 4-Dini:ro;oluene2. 6-Oini:ro:olueneOiethvb-thalatei-ChloroDnenvl-phenvletnerriuorene•i-Nitroaniline4. 6-Dinitro-2-Methyl3henoiN-Nitrasofiicnenylarnine (1 )A-3ro.-noDnenyl-ohenvle:.ierHexacniorosenrenePentacnioroonenolPhenantnreneAninraceneOi-n-5utvlohthala:erluoran:neneSenzidinePyrene3utyl£er.r\-ionthalate3. 3'Oicnioro&ensia:ne3enrw3lAn:nracenebis<2-£:nvmexvl|Pr.;na:aTe

|Cnrysene

|Di-n-Or:vi Pht.iaiateD6n20^3ir*iuor3ntnci*3€^v»^(*-ip*ûor3njricn*3enzcxa)=vreneIneenoil 2. 3-c2!?veêOibeciia niAninracene3enz«= ^ .iP-rvien*


1 f7)&

3.*id£>

,3iov "

' 1 T-OO3ô^

Sô

S <?-o

01-Cinr.s: J» separated Irom dio-">enylamine

foin\ I



Concentration:,' LowJ Medium (Circle One)

-j ^

fe K)

cr;_.•\}

! •• - : '

\ . . /

L'

riL

i 'L

I .i,' \

(L

i\

•\

Date Analyz

Conc/Dil Fa

CAS iM~>«pber, .75-9.103-95-262-53-31 1 1 -44,495-57-8541-73-1*,t/o-*o--/ '100-51-695-50-195-43-739633-32-9106-4A-5621-64-767-72-1

N-NitrosodimetnylammePhenolAnilineois(-2-Chloroe:r»vllEtner2-Chloroohenol1 . 3-Oichlorobenzene~\ . t-I/itfriiordoenzeneBenzvl Alcohol1 . 2-DichIorobenjene2-Metfivloênolbis'2-cnloroiso3rooYOEtr>er

|4-Metnylsrenol! N-Nitroso-D-rn-ProDylamineHexacnlorosthane

' "95-3 (Nitrobenzene/.j-59-i llsoanorone88-75-5 1 2-N«rosr>enol105-67-965-85-0111-91-1

| 2. 4-DimethylshenolBe^zoic AsuJ&isf-2-CîOfoe;noxvtWe!hane

oH-

lO/W

jg/l or ug/Kg(Circle One!

C,i'f

*

120*83-2 1 2- 4-DicnloroonenoI '• |120-82-1 | 1. 2. 4-7nchlorooenzene91-20-3 |N33n:naien-105-47-387-63-3

4-ChioroaniiineH*xacnlorsautaoiene

59-50-7 1 4-Chloro-3-Me!nviB"eriolS'i -57-6 | 2-M«::ivinasnt~3tene77-^:7.4 | -lezacMlcrocvclODeniadiene83-05-2 | 2 4 o-TricniorcsnenolS5-S5-4 | 2. 4. 5-~r>C-"ilOr03ri»nol

9 1 - 5 8 - 7 J2-Chiofonacninaienea5-74.z 1 2-Nuroanidne131-11-3 ( Dimernv! Pnihalaie203-95-5 j A;ena3rt:nviene93-C9-2 1 3-N'nroaniline

^^fc-/7?33^^

j;

CASNumber

33-32-9 | Acenac!-.tr>e31-2E-5!00-C2-7132-6-4-ri21-'4-2

2. 4-Oim:rc4-NitroDnenDibenzefura2. A-Dinttro

506-20-2 " 1 2. 6-Dim:rcBi- -7 '|7005-72-2 |86-72-7

00-C1 -5534-52-185-30-6101-55-3•S18.74-*,57-35-535-01-E'.20- :2 -734-74-2206-i-t-O92-37-5' 29-CC-OE5-6S-7 • •91-54.-.5o-5;-2n7-s<-72:s-:-..=117.5^-:

"DieThv'.s.-.T.11

4-Chlorosrirluorene4-NitroaniI4. 6-Dini:rcN-Nnrescc4-3roTio3hHexacnioroPsntzchlorPhenan:nr(AntnracervDi-n-5utvl:rluorantneSenzidinePyreneSutyioerrv3. 3"-OicniSenrocaiArD'Sl2-E:nviCrirvse^spi-n-0::vi

205-rr-I J5en;o(5)ri207-C5-5 |3er.rs«;=n50-32 -E |5enioia-*v••S3-2r-553-70-2

IneertCil . IO'&er.r'.a c

191-14-1 3enr~; h

(l)-Cin.-s: s» seaaraied Iro-Ti

ug/1orug/Kg(Circle One!

disênyijmine

ro»n» I

-1 *"" J~ — -^*-~

inP. 0. Box 818. Alexanorla. Virginia 22313 703/557-2490

B


Semivolatile CompoundsConcentration: /Low) Medium (Circle One)


Date Analyzed: —————————————————————

Conc/Dil Factor:

CAS ug/I orug/Kg(Circle One)

CASNumber

ug/1orug/Kg(Circle One)

o2-75-9108-95-262-S3-31 1 1 .A4..A

95-57-8-541-73-1106-4S-7100-51-695-50-195-48-739638-32-9105 -44.. 5621-64-767-72-1N3-95-3

. 78-59-133-75-5105-67-9

•65-85-0111.91-1120-83-2120-82-1

N-NurosoGirnetriYlaminePhenolAniline&is(-2-Chloroetrivl)Ether2-CM6roorienol1 . 3-Dichlorobenz8ne1 . A-DichlorobenzeneBenryl Alconol1. 2-Oichlorobenzene2-MetriylDhenolbis(2-cnioroisoDrooyl)Ether4-MetnvlphenolN-Nitroso-Di-n-PrcDvlamineHexacMIoroethareNitrobenzeneIsosnorone2-Niuoonenol2. 4-Dtmethyl3henolBenzoic Acidbis(-2-CMoro«TnoxvlMeThane2. 4-Dicnlofoonenol1. 2. 4-Tnchlorooenzene

91-20-3 | Naontnaiene106-47-887-63-3=9-50-7SI -57-677-47-4

33-06-255-95-491-58 -7S3-74-4J 3 1 - 1 1 - 3203-95-3S9-C9-2

4-CnioroanilineHexacnlorosutaaiene4-Chlo.'0-3-Wetnvlonenol2-Metnvtnaon;naieneHexacnlorocvdooentadiene2. 4 5-Tncriio'oonenoi2. 4. 5-TficrilorO3n»nol

2 -Chiorona-ninaiene2-Nnroanilme

Dirnetnvl Phtha'a'?Acenao^'iviene3-Nitroaniline

-

.

83-32-951-28-5100-02-7132-64-9121-14-2606-20-2 '84-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-36-585-01-8120-12-784-74-2206-i-:.oS2-87-5129-00-085-68-7S1-94.',55-55-3117-81-7213-0'. -S117-54-0205-SS-2207-06-950-32-5193-29-5 •53-70-3191-24-2

Acenacnrnene2. 4-DinurcDHeno'4-Ni:roohenolDibenzofuran2. 4-Dirntrotoluene2. 6-DinitrotoiueneDiethytohthalate4-Chloroohenvt-onenvietnerrluorene

4-Niiroaniline4. S-Oinitro-2-MetnYlDher.olN-NiTfosodicnenyiamme (1)4-BromoDrienvl-oiienvle:r.erHexacnloro&enienePentactilorosbeno!PhenantnreneAnthracsrisDi-n-SuTvlDhthala:e

IrluorantheneBenzidinePvrsne3u:v'&enrvl3ntriaia!S

|3. 3'-0"cniofo5enncine5enzo(3lAn:nraceneDis;2-E:nvinenvll?-:.i3i3isC^ryss-^s

|3i-n-0c:vi ?h:r,a:ate5enjoO)riu3'an;r>ene

|3en:?(^i?iuoran:neneIBenicxalPvreneIncenoi 2. 3-ci:3vene3'2enr!a hlAn;r»racei«

IBen'^c f» i)?»rvie^»

.•

Ol-Canno: be separated from

Form I

.[".._—.... .—~1 ' P.O. Box 818. Alexandria.

»

if--. - •;

:r\ ;

i(

Virginia 22313 703/557-2450

Organics Analysts Data Sheet(Page 2)


Concentration: f' LowJ) Medium (Circle One)

Date Extracted/Prepared: —\—;——————————

Date Analyzed: —

op

Conc/Dil Factor:

nCASNumber

ug/i orug/Kg(Circle One)

iL

L

ii .

\

32-75-910S-95-262-53-31 1 1 .US..A

95-57-8541-73-1106-46-7100-51-695-50-195-48-7

N-NitrosodimetnylammePhenolAnilinebis(-2-Chloroetnyl)Ether2-Chloroohenot1. 3-Dichlorobenzene1 . 4-OichlorobenzeneBenzvl Alconol1. 2-Dichlorobenz»ne2-Methvlohenol

39638-32-9 | bisf2-chloroisoorcDV')Etner106-4i-5 1 4-Metnvlonenol62 1 -64-7 | N-Nitroso-Oi-n-ProDylamine67-72-198-95-378-59-188-75-5105-67-965-85-011 1-91-1

HexachloroethaneNitrobenzeneIsosnorone2-Nitroonenol2. 4-OimethylDhenolSer.zoic Acidbist-2-CîoroeTnoxvtMethane

120-83-2 | 2. 4-Dicnlor-onenol120-82-1 | 1. 2. 4-Tncfilorooenzene91-20-3 |Naon:nalene106-47-887-68-359-50-7

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/V3o4-CMioroaniime |Hexacnloro-utaoiene |4-Chioro-3-Metr.vlisr>enol |

91-57-6 |2-Me:-.vinaD~.;r.aiene77-47-4 HexacnicrocvciooentadieneS3-05-2 2. 4 o-Tncnio.'oonenol55-95-4 2. 4. S-Tncniofoonenoi9 1 - 5 8 - 7 2-Cnioronacntnaiene38-74-i 2 -Nuroaniiine131-11-3 Oimetnvi Phihalaie203-95-8 AcenaoMnvieneS9-09-2 3-Nuroaniime

CASNumber


83-22-S5 ',-25-5100-02-7132-5-1-9121 -14-2606-20-2 "S^-65-270C5-72-336-73-7100-01-6534-52-185-30-5101-55-3118-74-1S7-55-5S5-01-H',20-12-7Si-74-2205-i-i-OS2-S7-5' 29-CC-O85-63-7Sl-ri--.55-55-3T. 7-21.721S-0-91-.7-5-.C235-s5-2207-OH-95C-22-H•• 53-3 = -553-70-319 -.-24-2

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4-Nitroaniline4. 6-Dirn:ro-2-iV.einvIonenoiN-Niuosoci;nenviamme (1)4.Bro.Tso3ne.-.vi-Dânvle:ne!>

HexacnicrosenienePeniacniorcshanolPhenanr-.re-êAnTr.racsneDi-n-Sutv lo~.tr; siateFluoranine~eSeniidmePvreneSutvl&er^Y^-tâiat"3. 3"-Oic~!crcoenncine35n;oi3iAn:-iracene&is(2-E:r.vir.exv:]Pr.:.->a!atsC*"..'vS5ne

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