ortho wires part iii

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(Continued) Dr.Kishor Bagalkot

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Page 1: Ortho wires part iii

(Continued)

Dr.Kishor Bagalkot

Page 2: Ortho wires part iii

Manufacture: AISI ,specially for orthodontic purposes

Various steps –

1. Melting

2. Ingot Formation

3. Rolling

4. Drawing

MANUFACTURE

Page 3: Ortho wires part iii

• Melting• Various metals of the alloy are melted

• Proportion influences the properties

• Ingot formation• Molten alloy into mold.

• Non uniform chunk of metal

• Porosities and slag.

• Grains seen in the ingot – control of mechanical properties

Steps

Page 4: Ortho wires part iii

• Porosities due to dissolved gases (produced / trapped)

• Vacuum voids due to shrinking of late cooling interior.

• Important to control microstructure at this stage – basis

of its phy properties and mechanical performance

Ingot formation

Page 5: Ortho wires part iii

Rolling –

• First mechanical process.

• Ingot reduced to thinner bars

• Finally form a wire

• Different wires from the same batch, differ in

properties

Steps

Page 6: Ortho wires part iii

• Retain their property even after rolling

• Shape & arrangement altered

• Grains get elongated, defects get rearranged

• Work hardening – structure locked up.

• Wires start to crack if rolling continued

• Annealing is done- mobile

• Cooling – structure resembles original ingot, uniform

Rolling

Page 7: Ortho wires part iii

Drawing

• More precise

• Ingot final size.

• Wire pulled through small hole in a die

• Progressively smaller diameter-uniform squeezing.

• Same pressure all around, instead of from 2 opposite

sides.

Steps

Page 8: Ortho wires part iii

• Series of dies

• Annealing at regular intervals.

• Exact number of drafts and annealing cycles

depends on the alloy (gold <carbon steel<stainless

steel)

Drawing

Page 9: Ortho wires part iii

Various alloys :

Gold

Stainless steel

Co-cr

Late 70-80’s Nitinol and TMA

Page 10: Ortho wires part iii

Variable cross section approach.

Demand for the appliance system.

• Load deflection rate.

• Resistant to permanent deformation.

• Large range of action.

Variable modulus concept.

Variable transformation temperature orthodontics

Page 11: Ortho wires part iii

Orthodontic Wires.

Titanium

Nickel-titanium alloy(NiTi)

• Nitinol

• Chinese NiTi

• Japanese NiTi

• Copper NiTi

Other Newer materials.

Page 12: Ortho wires part iii

TITANIUM

Titanium was discovered by GREGOR.

(England 1790)

Biomedical material in US military industry.

BOTHE et al implanted titanium in lab Animals.

(1940)

A light weight metal.

Atomic weight – 47.9.

Non magnetic.

Page 13: Ortho wires part iii

TITANIUM

• Corrosion resistant

• Biocompatibility

• High strength

• Ductility

Page 14: Ortho wires part iii

TITANIUM

At room temp, Ti - difficult to deform. Alpha phase – Hexagonal unit cells

Page 15: Ortho wires part iii

TITANIUM

At temp, > 16200F or 8820C - stable & easier to process.

Beta phase – Body centered cubic cells

Page 16: Ortho wires part iii

TITANIUM

Beta phase – Body centered cubic cells

• Beta II or Ormco’s TMA

- Ti - 11.5 Mo - 6 Zr - 4 Sn

• Titanium Niobium

- Ti - 13 Nb - 13 Zr

Page 17: Ortho wires part iii

Alloys with both phases

• Ti - 5 Al - 2.5Fe

• Ti - 6 Al - 4V

Page 18: Ortho wires part iii

TITANIUM

SUPERIOR CORROSION RESISTANCE

• Tio2 - Ti affinity - friction.

Titanium is not esthetic

• Laser aided depositions

• Implantation of nitrogen

• IONGUARD

Page 19: Ortho wires part iii

BETA - TITANIUM

Beta titanium was introduced by Dr. CHARLES

BURSTONE and JON GOLDBERG in the university of

CONNECTICUT ( Early 1980s )

Composition

Titanium - 73.5%

Molybdenum - 11.5%

Zirconium - 6%

Tin - 4.5 %

Page 20: Ortho wires part iii

BETA – TITANIUM(AJO Feb. 1980; Burstone and Goldberg)

- Titanium based alloy + molybdenum or columbium.

Beta stabilized titaniums

Yield strength - 1,70,000 p.s.i

Modulus of elasticity - 9,400.000 p.s.i (2 NiTi, ½ St St)

YS/E - 1.8 X 10-2 (St St - 1.1 x 10-2)

Page 21: Ortho wires part iii

BETA - TITANIUM

TEST FOR SPRING BACK TINIUS OLSEN STIFFNESS TESTER

¼ wire - 60º - 0.017’’/0.025’’

A. Straight wires

B. Wires with 35º bend

C. Wires which are overbent to 90º and then

bent back to 35º

Page 22: Ortho wires part iii

Comparison of spring back

MODE

STAINLESS STEEL

BETA TITANIUM

PERCENT INCREASE

A 16.0 32.8 105%

B 16.5

31.3 90%

C 17.5 37.3 113%

Page 23: Ortho wires part iii

BETA - TITANIUM

ADVANTAGES:

• Low stiffness

• Good formability

• High spring back

• Weldable

• Ductile

• Corrosion resistance

Page 24: Ortho wires part iii

BETA-TITANIUM

DISADVANTAGES

• High coefficient of friction.

• Esthetics.

Page 25: Ortho wires part iii

BETA - TITANIUM

Clinical Applications

Ideal edgewise arches

- Deflected twice than SS

- Range of action Initial tooth alignment or

Finishing arches

- Forces - 0.4 of SS

Eg : 0.018 x 0.025 TMA = 0.014 x 0.020 SS

- more gentle delivery of forces.

Page 26: Ortho wires part iii

BETA - TITANIUM

Clinical Applications

Ideal edgewise arches

- Full bracket engagement - 3rd order control.

- Ductility - Tie back loops or complicated bends.

Page 27: Ortho wires part iii

BETA - TITANIUM

Clinical Applications

Ideal edgewise arches

- Ductility - Tie back loops or complicated bends.

- 0.018 x .025 in .022.

Page 28: Ortho wires part iii

BETA - TITANIUM

LOOPS

‘T’ Vertical

Helical

‘L’ loop

Page 29: Ortho wires part iii

BETA TITANIUM

OPUS LOOP-0.017’’/0.025’’

Page 30: Ortho wires part iii

BETA TITANIUM

Pendulum appliance – 0.032’’

Page 31: Ortho wires part iii

BETA - TITANIUM

ROTATION INTRUSION

Page 32: Ortho wires part iii

BETA-TITANIUM

K-SIR ARCH WIRE.0.019’’/0.025’’

Page 33: Ortho wires part iii

BETA - TITANIUM

Canine root spring without helices

Closing loops

Page 34: Ortho wires part iii

BETA - TITANIUM Direct welding of auxiliaries Helical finger spring.

Page 35: Ortho wires part iii

BETA - TITANIUM

Welding of TMA wire (JCO 1987; Burstone)

What way different from St St

Page 36: Ortho wires part iii

BETA - TITANIUM

Welding of TMA wire (JCO 1987; Burstone)

5 basic principles:

1. Proper positioning

2. Minimum voltage

3. Small contact area

4. Single short pulse

5. Pressure

Page 37: Ortho wires part iii

ROCKY MOUNTAIN DIAL-A-WELD 506A

Page 38: Ortho wires part iii

1. POSITIONING

• Set down of 80%

• 25 - 60 %

After welding, one wire has "set down" into the other.

Broad, flat electrodes

Page 39: Ortho wires part iii

2. VOLTAGE Low Voltage - The parts may delaminate. Round wires - Simple to weld.

- Require lower voltages. High Voltage - Wire becomes brittle,

- Cracks

- Melting Overheating - 100% set down - Cracks

Page 40: Ortho wires part iii

3. SMALLER CONTACT AREA

- Low voltage

- Higher localized heats

- Point contact

- ‘T’ joint

Page 41: Ortho wires part iii

4. SINGLE PULSE

- Only one pulse

- Short duration.

5. PRESSURE

Page 42: Ortho wires part iii

Improper Welding

Low voltage - The parts may delaminate

High voltage - Wire become brittle

Cracks

Melting

Page 43: Ortho wires part iii

CLINICAL APPLICATIONS

PASSIVE APPLICATIONS:

- Stops

- Tie back hooks

Page 44: Ortho wires part iii

CLINICAL APPLICATIONS

ACTIVE APPLICATIONS

- Without loss of spring back

Page 45: Ortho wires part iii

CLINICAL APPLICATIONS

To gain space in the

anterior segment

Page 46: Ortho wires part iii

CLINICAL IMPLICATIONS

ROTATIONAL

CORRECTION

Page 47: Ortho wires part iii

CLINICAL IMPLICATIONS

TO INCLUDE SECOND MOLARS

Page 48: Ortho wires part iii

Composite continuous arch with

posterior segment of .021"

x .025" TMA and anterior

segment of .016" round TMA to

facilitate alignment.

Composite continuous arch wire:

Page 49: Ortho wires part iii

ALPHA TITANIUM (AJO March 1989; A.J.Wilcock)

Dr.Begg and Prof. Greenwood (1954)

0.018 Titanium wire

- Too soft

- Alpha stabilized by the addition of O2

Page 50: Ortho wires part iii

ALPHA TITANIUM

TITANIUM - 90%

ALUMINIUM - 6%

VANADIUM - 4%

Close packed hexagonal lattice

ALPHA stabilizing elements–Aluminum, Gallium,

Germanium, Carbon, Oxygen and Nitrogen

‘NEAR ALPHA ALLOY’

- WILCOCK company

Page 51: Ortho wires part iii

ALPHA – BETA PHASE

Page 52: Ortho wires part iii

ALPHA TITANIUM

PROPERTIES: Heat treated to improve strength.

Satisfactory creep properties - Finishing & braking arches.

Wire becomes hard in the oral environment due to hydrogen absorption.

TITANIUM HYDRIDE Less ductile – one slip plane

Nickel free

Page 53: Ortho wires part iii

Clinical Applications:

BEGG-II STAGE

• Combination wire

• 0.022x0.018-ant

• 0.018-post

• BRAKING MECH

Page 54: Ortho wires part iii

Clinical Implications:

• BEGG-Finishing stage

• Rectangular wires

• 0.022’’x0.018-ribbon

• 0.020’’x0.020’’-square

Page 55: Ortho wires part iii

TITANIUM-NIOBIUM

A new finishing wire alloy M. Dalstra et al

Nickel free Titanium alloy

(SYBRON DENTAL SPECIALITIES CALIFORNIA)

Ti - 74%

Nb - 13%

Zr - 13%

Page 56: Ortho wires part iii

TITANIUM-NIOBIUM PROPERTIES

• Easy to bend, formability is less than TMA

• When lower forces are used than TMA

• Stiffness - ¼ of St St,

- ¾ of TMA

Page 57: Ortho wires part iii

TITANIUM-NIOBIUM

PROPERTIES

• Load deflection rate is lower than TMA

• Yield strength is lower than St St

Page 58: Ortho wires part iii

TITANIUM-NIOBIUM ADVANTAGES:

• Used when lower forces than TMA.

• No leaching of nickel

CLINICAL APPLICATIONS:

• Finishing wire with multiple bends

• Fixed retainers ( Biocompatible )

Page 59: Ortho wires part iii

TIMOLIUM WIRES

- Research lab, TP orthodontics.

- New and improved titanium alloy.

Composition:

Ti - 82%

Mo - 15%

Nb - 3%

- Breakage resistance.

- Compressive strength.

Page 60: Ortho wires part iii

TIMOLIUM WIRES

- Yield strength.

- Optimum delivered force.

- Friction

- Formability

Page 61: Ortho wires part iii

BETA –III WIRES

Introduced by RAVINDRA NANDA• Bendable

• High force

• Low deflection rate

• Co-efficient of friction is more

• Nickel free titanium wire with memory

• Ideal for multilooping, cantilever, utility arches

- Finishing stages where tip & torque corrections done during initial stages.

Page 62: Ortho wires part iii

A comparative study of metallurgical and working properties of two

new titanium based alloy wires (TiMolium and Beta III ) with the

earlier introduced titanium wires ( TMA ), and also alpha titanium

wires. - Jiku

Abraham

TiMolium - T.P.Orthodontics

Beta III - Ortho organizers

TMA - Ormco corp.

Alpha Titanium - A.J. WILLCOCK

Page 63: Ortho wires part iii

Straight rectangular wires

GROUP I

- 4 wires in 16”x 22” dimension

GROUP II

- 4 wires in 17”x 25” dimension

GROUP III

- 4 wires in 19”x 25” dimension

Page 64: Ortho wires part iii

Properties studied are

1. Yield, tensile strength & elastic modulus

2. Maximum load via 3-point bending test

3. Frictional resistance

4. Welding characteristics

5. Stress relaxation

6. Working range / spring back

7. Surface topography

8. Micro hardness

9. Elemental analysis

Page 65: Ortho wires part iii

INSTRON MODEL NO.1193

Expr.setup for yield strength & ultimate tensile strength

Page 66: Ortho wires part iii

Manufacturers claim that:

• Timolium is superior to TMA wires in the following:

1. Friction and surface smoothness.

2. Compressive strength.

3. Yield strength & breakage resistance.

• Beta III is bendable, high force low deflection, nickel free

arch wire with memory.

Page 67: Ortho wires part iii

Results of the study showed that The coefficient of friction, surface smoothness, yield strength

& ultimate tensile strength of TiMolium was superior to that

of TMA.

However TMA has low load deflection rate and

high spring back than TiMolium .

Yield strength of Beta III was lower than TMA and TiMolium

Formability is good but resiliency is low.

Page 68: Ortho wires part iii

CLINICAL APPLICATIONS OF THIS STUDY

1. Correction of crowding or alignment of teeth -

TMA > Beta III

2. Intrusion -

TMA shows a better stress relaxation

TMA > TiMolium .

Page 69: Ortho wires part iii

3. Space closure

• Sliding mechanics -

TiMolium shows lowest values of coefficient of

friction in both static as well as kinetic friction.

TiMolium > Alpha titanium

• Frictionless mechanics –

Formability - Beta III > TMA > TiMolium

Resilience - TiMolium > TMA > Beta III

Page 70: Ortho wires part iii

WELDABILITY

TiMolium > Beta III

FINISHING STAGES

Incomplete tip, torque correction.

Beta III > TMA > TiMolium.

Page 71: Ortho wires part iii

NICKEL-TITANIUM ALLOYS

CONVENTIONAL - NITINOL

SUPERELASTIC

• Pseudoelastic-Japanese NiTi

• Thermo elastic-Cu NiTi.

Page 72: Ortho wires part iii

NICKEL-TITANIUM ALLOYS

2 forms of NiTi alloys

1. Martensite – Face centered (close packed

hexagonal).

2. Austenite – Body centered cubic/tetragonal

lattice.

Page 73: Ortho wires part iii

NICKEL-TITANIUM ALLOYS

Steel : temp. – FCC st - Austenite - C at the center of unit cell.

temp. – BCC st. – Ferritic – Fe at the center of unit cell.

rapid temp. – BCT st.– Martensite – C trapped in the unit cell.

Martensite – hard, strong, brittle.

NiTi : temp. –FCC st - Austenite

temp. - BCC st - Martensite

Martensite – Soft.

Page 74: Ortho wires part iii

NICKEL-TITANIUM

TRANSITION TEMPERATURE RANGE

Martensitic transformation – Range.

TTR > body temp - Austenitic - Rigid.

TTR< body temp - Martensitic - Elastic.

Austenite wires - 2% of the strain range.

Martensitic wires - 8%.

Page 75: Ortho wires part iii

NICKEL-TITANIUM

HYSTERESIS

• The transformation at different temperatures.

• The difference between cooling and heating.

• The range for most binary alloys is 400 – 600

Page 76: Ortho wires part iii

PROPERTY AUSTENITE MARTENSITE

YIELD STRENGTH 560 MPa 100 MPa

ELASTIC MODULUS 75 GPa 28 GPa

NICKEL-TITANIUM

Page 77: Ortho wires part iii

NICKEL-TITANIUM Martensitic transformation of

NiTi

FIDUCIARY LINE

Page 78: Ortho wires part iii

Phase Transformation

Page 79: Ortho wires part iii

MARTENSITIC TRANSFORMATION

ADDDITIONS and IMPURITIES

• + n of 3rd metal - TTR -200ºC

- Narrow the hysteresis.

- More accurate response.

• Thermally activated alloys contain third metal (Cu,Co)

• Small amounts of Al, Zr, Cr, or Fe will improve the

strength of the martensitic form

Page 80: Ortho wires part iii

NITINOL

Laboratory and clinical Analysis Of Nitinol Wire

- G F. Andreasen, R E. Morrow ( AJO Feb 1978 )

Introduction of stainless steel wire appliances.

(1930- 1940) Nitinol ( Early 1960s) - William.F.Buehler, a research

metallurgist at the Naval Ordnance Lab in Silver Springs, Maryland

(Now called the Naval Surface Weapons Center ).

Page 81: Ortho wires part iii

NITINOL

Ni - Nickel

Ti - Titanium

Nol - Naval ordnance laboratory

Clinical use of Nitinol wire started in May 1972

by G.F.ANDREASEN et al.

Page 82: Ortho wires part iii

- Marketed as Nitinol by Unitek corp.

- Developed for the space programme.

- Useful because of its exceptional springiness.

Shape memory and

Super elasticity

NITINOL

Page 83: Ortho wires part iii

NITINOL

SHAPE MEMORY WIRE

The characteristic of being able to return to a previously

manufactured shape when it is heated to a TTR.

Ability of the material to remember its original shape after being plastically deformed while in the martensitic form.

ELASTIC ORTHODONTIC WIRE

An outstanding elasticity which is useful for

orthodontic applications compared with st st.

Page 84: Ortho wires part iii

NITINOL

In orthodontic applications

1. Requires fewer arch wire changes.

2. Requires less chair time.

3. Shortens the time required to accomplish the

rotations and leveling

4. Produces less patient discomfort.

Page 85: Ortho wires part iii

NITINOL

PHYSICAL PROPERTIES

Material property Nitinol Stainless steel

Alloy Nickel, Titanium Iron, Chrome,Nickel

Ultimate strength 230,000 to 250,000 p.s.i 280,000 to 300,000 p.s.i

Modulus of elasticity 4.8 x106 p.s.i 28.5 x 106 p.s.i

Page 86: Ortho wires part iii

NITINOL

BEND TEST

Acc to ADA Specification no.32 on orthodontic wires. TOST

Page 87: Ortho wires part iii

NITINOL

Page 88: Ortho wires part iii

NITINOL

TORSION TEST

A comparison between nitinol and stainless steel wires.

0 90 180 270 360 450 540 630 720

Torque Angle

Page 89: Ortho wires part iii

NITINOL

STORED ENERGY COMPARISONS

Stored energy of Nitinol wire is significantly greater than an equivalent SS wire.this comparison was based upon the wires being bent 90 degrees

Page 90: Ortho wires part iii

NITINOL

SPRING RATE

• Max F – both wires – full recovery without any permanent set.

Page 91: Ortho wires part iii

NITINOL

CLINICAL APPLICATIONS

Class I ,II,III malocclusions in both extraction and non

extraction cases

Page 92: Ortho wires part iii

NITINOL Primary criterion – Amount of malalignment from the

ideal arch form.

More the deflection – more the benefit.

Page 93: Ortho wires part iii

NITINOL

Imp benefits - a rectangular wire is inserted early in the

treatment.

Simultaneous rotation, leveling, tipping and torquing

can be accomplished earlier with a resilient rectangular

wire,

Cross bite correction

Uprighting impacted canines

Opening the bite

Page 94: Ortho wires part iii

NITINOL

Torquing auxiliary in uprighting impacted canine.

Page 95: Ortho wires part iii

NITINOL

Sectional arch wire

Page 96: Ortho wires part iii

NITINOL

LIMITATIONS 1.Can`t be bent with sharp – cornered instruments.

2.It will readily break when bent over a sharp edge.

3.The bending of loops or omega bends are not

recommended. ( especially closing loops ).

4.Can`t be soldered or welded to itself without annealing

the wire.

Page 97: Ortho wires part iii

NITINOL

5. Bending of tie-back hooks entails a high risk of

failure.

6. Cinch – backs.

- Annealing - Dark blue color flame.

- Cherry red flame – brittle.

Page 98: Ortho wires part iii

(Continued)

Dr.Kishor Bagalkot

Page 99: Ortho wires part iii

1970 – Nitinol – Martensitic.

Late 1980s – Austenitic – Superelasticity.

Page 100: Ortho wires part iii

Phase - Transformation

AUSTENITE PHASE

MARTENSITE PHASE

• Martensite start(MS)

• Martensite finish(MF)

• Austenite start(AS)

• Austenite finish(AF)

Page 101: Ortho wires part iii

Hysteresis A-B

(Ela

stic

D o

f A p

hase

. )(Transfn to M)

(Transfn completed.)

(E D of M structure)

(P D)

Page 102: Ortho wires part iii

Hysteresis A-B

If stress released before reaching permanent deformation.

Elastic unloading of M

(Reverse transformation)(A Structure restored.)

(Elastic unloading of A)

Page 103: Ortho wires part iii

Hysteresis A-B Elastic unloading of M

(Reverse transformation)(A Structure restored.)

(Elastic unloading of A)(Ela

stic

D o

f A p

hase

)(Transfn to M)

(Transfn completed.)

(E D of M structure)

(P D)

Page 104: Ortho wires part iii

-Unloading curve differs from

the loading curve.

-The reversibility has an

energy loss.

-The force delivered - not the same as the force applied.

-Remarkable effect.

Hysteresis

Page 105: Ortho wires part iii

NICKEL-TITANIUM ALLOYS

CONVENTIONAL - NITINOL

SUPERELASTIC

• Chinese NiTi

• Pseudoelastic-Japanese NiTi

• Thermo elastic-Cu NiTi.

Page 106: Ortho wires part iii

NICKEL-TITANIUM ALLOYS

A certain shape is set at elevated temperatures (above the

TTR).When the alloy is cooled below the TTR, it can be

plastically deformed but when it is heated again the original

shape is restored.

Ex: An orthodontic arch form.

By lowering the temperature the alloy is transformed into

martensite and becomes pliable and easily deformed.

THERMOELASTICITY

SHAPE MEMORY

Page 107: Ortho wires part iii

-High modulus alloy st st.

ELASTICITY AND SUPERELASTICITY:

-Effective strain Range cor to optm force zone.

-Force rapidly s as the teeth move.

Page 108: Ortho wires part iii

Low EM. Alloy:

- Effective Strain Range – Larger.

- Nitinol, Braided wires.

Page 109: Ortho wires part iii

SUPERELASTIC NITI

Eff. Strain Range cor to opt F zone

during Deactivation – more.

Small strain ranges

cor to other zones.

Page 110: Ortho wires part iii

To remove small strain ranges -

Super position - over bending

Force guided activation -

overactivation

Page 111: Ortho wires part iii

AJO 2001 - Olivier Nicolay – Pseudoelasticity and

thermoelasticity of nickel titanium alloys

Austenitic & Martensitic

Smart materials

- Reorganization of molecules

without change in the atomic compn to

meet the environmental

condn

Page 112: Ortho wires part iii

Pseudoelasticity

-For most NiTi

- A phase (prevalent) + small (M) + intermediate R phase.

-On stress appln deflection - Stress Induced Martensite

Stress Induced Martensite (SIM)

-Unstable – On removal of stress.

-Partially compensates for the lack of thermally induced Martensite

-Contributes to the superelastic behavior of A – NiTi.

-This localized stressed related superelastic phenomenon

Page 113: Ortho wires part iii

CHINESE NITI WIRE

CHINESE NiTi wire - A new orthodontic wire

- C. J. BURSTONE ( AJO JUNE

1985)

New NiTi by Dr.Tien Hua Cheng and associates at

the General Research Institute for non Ferrous

Metals, in Beijing, China.

Page 114: Ortho wires part iii

CHINESE NITI WIRE

Austenitic parent phase + Little work hardened

Chinese NiTi wire has much lower transitional

temperature than NiTi wire.

Page 115: Ortho wires part iii

CHINESE NITI WIRE

CANTILEVER APPARATUS

0.016 SS, Nitinol and A-NiTi

were submitted to a flexural test

STIFFNESS

SPRINGBACK

MAXIMUM MOMENT

Angular deflection measured by

protractor.

Page 116: Ortho wires part iii

Bending moment Vs.Deflection

Arch Wire - Same force

- “Unique and Extremely desirable”.

CHINESE NITI WIRE

SPRING BACK

For 80º activation

SS - 16º

Nitinol - 52º

Chinese NiTi - 73º

Page 117: Ortho wires part iii

CHINESE NITI WIRE

STIFFNESS

Activation and reactivation curves.

Unloading curves change at different

activation.

Page 118: Ortho wires part iii

CHINESE NITI WIRE

THE MAXIMUM MOMENT

WIRE MOMENT SPRING BACK % RECOVERY

SS 3,067 16 20

NITINOL 2,112 52 65

NITI 1,233 73 91

Page 119: Ortho wires part iii

CHINESE NITI WIRE

TEMPERATURE DEPENDENT CHANGES

temp. - stiffness

- reduced spring back

Page 120: Ortho wires part iii

CHINESE NITI WIRE

TIME DEPENDANT CHANGESThe wires remained tied between 3 brackets for periods of 1 minute,1 hour and 72 hours.

Increased range of action –

large deflection.

Deformation - 4.4 st.st.

- 1.6 nitinol

Page 121: Ortho wires part iii

CHINESE NITI WIRE

1. Applicable in situations where large deflections are

required.

2. When tooth are badly malpositoned.

3. Niti wire deformation is not time dependent

CLINICAL SIGNIFICANCE

Page 122: Ortho wires part iii

JAPANESE NITI

The super - elastic property of the Japanese NiTi alloy wire

for use in orthodontics.

- Fujio Miura et al ( AJODO July 1986 )

In 1978 Furukawa electric co.ltd of Japan produced a new

type of alloy

1. High spring back.

2. Shape memory.

3. Super elasticity.

Page 123: Ortho wires part iii

JAPANESE NITI

1. Examination of mechanical property of the wire.

1. Tensile test

2. Bending test

TESTS

Page 124: Ortho wires part iii

JAPANESE NITI

Co-Cr-Ni, Nitinol ,

Ss and Japanese NiTi.

0.016 wire

Superelasticity.

1. Tensile test

Page 125: Ortho wires part iii

JAPANESE NITI

Page 126: Ortho wires part iii

JAPANESE NITI

Bending test

Different 0.016 wires

Page 127: Ortho wires part iii

CLINICAL IMPLICATIONS

Alignment of badly malposed teeth

Distalize the molar

Expansion of arch

Gain/Close the space

Periodontally compromised pts

Page 128: Ortho wires part iii

CLINICAL APPLICATIONS

INITIAL

TWO MONTHS LATER

Page 129: Ortho wires part iii

CLINICAL APPLICATIONS

Page 130: Ortho wires part iii

CLINICAL APPLICATION

The concept of NiTi coil springs was suggested in 1975.

1. Open coil springs.

2. Closed coil springs.

NITI COIL SPRINGS

Page 131: Ortho wires part iii

CLINICAL APPLICATION

Tensile and comp properties studied

- Japanese NiTi coil springs

- Desirable spring back and superelastic properties than st.st.

- Diameter of wire - SE

- Decreased lumen of the coil – increased SE

- Increased TTR – decreased SE

FACTORS THAT AFFECT THE MECHANICAL PROPERTIES OF SPRINGS.

AJO 1988, Fujio Miura

Page 132: Ortho wires part iii

CLINICAL APPLICATION

Closed coil spring

After 5 months

Page 133: Ortho wires part iii

CLINICAL APPLICATION

Open coil spring

After 3 months

Page 134: Ortho wires part iii

CLINICAL APPLICATION

Partially Impacted

second molar

Modified lingual arch &

NiTi coil spring.

Closed coil spring

After 3 months

Page 135: Ortho wires part iii

CLINICAL APPLICATION

Page 136: Ortho wires part iii

CLINICAL APPLICATIONS

MOLAR DISTALIZATION WITH SUPER ELASTIC NiTi

WIRE. - R.LOCATLLI et al ( JCO 1992 MAY ) .

After 4 months

Page 137: Ortho wires part iii

CLINICAL APPLICATION

NICKEL TITANIUM DOUBLE

LOOP SYSTEM- GIANCOTTI ( JCO APRIL 1998 )

After second molar erupts

80g Neosentalloy arch wire

2 sectional arch wires

Page 138: Ortho wires part iii

NICKEL TITANIUM PALATAL EXPANDER

Tandem loop, nickel titanium , temperature activated palatal

expander.

- Light continuous pressure on the mid palatal suture .

( Simultaneous uprighting , rotating , and distalising the

maxillary first molars )

NICKEL TITANIUM PALATAL EXPANDER

W.V.ARNDT ( JCO 1993

Page 139: Ortho wires part iii

NICKEL TITANIUM PALATAL EXPANDER

Disadvantages of conventional expansion.

-Intermittent force

-Inability to correct rotations.

-Arndt and Rickets – Uni/bilateral MLgl rotations

of molars.

Page 140: Ortho wires part iii

NICKEL TITANIUM PALATAL EXPANDER

Page 141: Ortho wires part iii

NICKEL TITANIUM PALATAL EXPANDER

A consequence of nickel titanium’ s shape memory and transition temperature effects.

The nickel titanium expander has a transition temperature of 940 F.

Below TTR – Metal is flexible

Above TTR – Metal stiffen

THE ACTION OF THE APPLIANCE

Page 142: Ortho wires part iii

BELOW 200 C AT TTR

Page 143: Ortho wires part iii

Passiveappliance

Initial activation

After expansion

Page 144: Ortho wires part iii

8 intermolar widths 26-47mm

180-300gms

Amount of expansion + 3mm over correction.

Freeze gel packs in the expander kit.

Page 145: Ortho wires part iii

AJO 2001, Christopher Ciambotti -- Comparison

Both – D Alv expn

Crossbite correction.

Tipping of molars.

More reliable widening

Page 146: Ortho wires part iii

Comparison:

1. Palatal width change - RPE group is 28 %

- In NiTi group 16 %.

2. Buccal tipping of the alveolar process - RPE group – 5.080.

- NiTi group – 6.610

3. Molar rotation - RPE group 1.580

- NiTi group 26.610

Page 147: Ortho wires part iii

4. Radiographic evidence shows that mid palatal

suture separation is less obvious in the NiTi group

than RPE group.

5. No correlation between age and amount of dento-

alveolar expansion.

6. RPE appliance widened the palate more reliably,

NiTi appliance tipped the molars buccally.

Page 148: Ortho wires part iii

CLINICAL APPLICATION

INDIVIDUALISED PRESURGICAL ARCH FORMS

- Fujio MIURA et al JCO Sept. 1990.

Page 149: Ortho wires part iii

CLINICAL APPLICATION

Page 150: Ortho wires part iii

CLINICAL APPLICATION

Page 151: Ortho wires part iii

Clinical Application

Arch wires that have

MEMORIZED

various tooth

movement.

Page 152: Ortho wires part iii

CLINICAL APPLICATION

Before surgery After surgery

Page 153: Ortho wires part iii

CLINICAL APPLICATION

Provides 3 dimensional control Effective in surgical orthodontic cases Eliminates need to change arch wires frequently

DISADVANTAGES Bracket friction will be more when large wires are used

ADVANTAGES

Page 154: Ortho wires part iii

Superelasticity –Llight constant force levels

Shape memory – Easy arch wire placement

REFRIGERENT SPRAY – ENDO ICE

CLINICAL APPLICATION

BIOEFFICIENT THERAPY

ANTHONY.D.VIAZIS ( JCO Sept 1995 )

Page 155: Ortho wires part iii

CLINICAL APPLICATION

Page 156: Ortho wires part iii

CLINICAL APPLICATION

3-micron nitrogen coating that is produced by ion

bombardment of the wire surface.

Reduce

1.Friction

2. Breakage

3.Release of nickel into the mouth .

BIOFORCE IONGUARD WIRES

Page 157: Ortho wires part iii

COPPER NiTi

VARIABLE TRANSFORMATION TEMPERATURE

ORTHODONTICS

- ROHIT C. L. SACHDEVA.

“Variable cross sectional orthodontics”.

“Variable modulus concept”

- BURSTONE

Page 158: Ortho wires part iii

COPPER NiTi

• Introduced by Rohit sachdeva

• It has the advantage of generating more constant

forces than any other super elastic nickel titanium

alloys.

• More resistant to deformation.

• Smaller mechanical hysteresis

Page 159: Ortho wires part iii

COPPER NiTi

QUATERNARY METAL – Nickel, Titanium, Copper,

Chromium.

Copper enhances thermal reactive properties and creates a

consistent unloading force.

CLASSIFICATION

Type I Af – 150 c

Type II Af - 270 c

Type III Af - 350c

Type IV Af - 400c

Page 160: Ortho wires part iii

COPPER NiTi

1. Smaller loading force for the same degree of deformation. (20%

less )

2. Reduced hysteresis makes to exert consistent tooth movement and

reduced trauma.

ADVANTAGES OF COPPER NiTi ALLOYS OVER

OTHER NiTi WIRES

Page 161: Ortho wires part iii

DIRECT ELECTIC RESISTANCE HEAT TREATMENT METHOD (DERHT)

ARCHMATE

Page 162: Ortho wires part iii

DIRECT ELECTIC RESISTANCE HEAT TREATMENT METHOD (DERHT)

Page 163: Ortho wires part iii

DIRECT ELECTIC RESISTANCE HEAT TREATMENT METHOD (DERHT)

Page 164: Ortho wires part iii

COMPOSITE WIRES

The future of orthodontic materials ROBERT.P.KUSY (AJODO Jan 1998)

• Metals

• Polymers

• Ceramics

Advantages are realised

Disadvantages are minimised

Page 165: Ortho wires part iii

METAL-CERAMIC

METAL- POLYMER

CERAMIC- COMPOSITE

POLYMERS

METALS

CERAMICS

SEMICONDUCTORS

Page 166: Ortho wires part iii

COMPOSITE WIRES

In orthodontics

Composite prototypes of arch wires, ligatures,

Brackets - S-2 glass fibers ( ceramic )

- Acrylic resins ( polymer )

Esthetically pleasing because they tend to transmit the

colour of host teeth Strong & Springy.

Page 167: Ortho wires part iii

COMPOSITE WIRES

The process of manufacturing components of

continuous lengths & a constant cross sectional shape

Eg; Arch wires

Bundles of continuous fibers are impregnated with a

polymeric resin pulled through a sizing die

Then passed through a curing die that imparts a

precise shape ( Electro magnetic radiation )

PULTRUSION

Page 168: Ortho wires part iii

Comparison of unidirectional fiber reinforced polymeric composites to NITI alloys in bending

Page 169: Ortho wires part iii

COMPOSITE WIRES

Patients with allergic reactions with nickel

Esthetic than previous wires

Better strength & springiness

DISADVANTAGES

Shape can not be changed

ADVANTAGES

Page 170: Ortho wires part iii

COMPOSITE WIRESOPTIFLEX WIRES

A composite ceramic fiber-plastic-nylon ( ORMCO )

Dr.TALASS

Page 171: Ortho wires part iii

COMPOSITE WIRES

A. Silicon dioxide core - ForceB. Silicon resin middle

layer - Protection from moistureC. Nylon layer - Prevents from damage

Structure – Clear optical fiber made of 3 Layers

Page 172: Ortho wires part iii

COMPOSITE WIRES

The wire can be ROUND or RECTANGULAR

• Wide range of action

• Light continuous force

• Sharp bend must be avoided

• Highly resilient - Effective in the alignment of

crowded teeth

Page 173: Ortho wires part iii

References :•Proffit W R; Contemporary Orthodontics,Ed.2,Mosby YearBook Inc.,St.Louis,U.S.A.,1993.

•Graber T M & Vanarsdall R L;Orthodontics,Current Principles & Techniques,Ed.3,Mosby Inc,St.Louis,U.S.A.2000.

•Ralph W P;Skinner’s science of dental materials;Ed.9,

W B Saunders Company,1992

•Robert P.Kusy;A review of contemporary arch wires;Their properties and characteristics’ Angle Orthod,1997;67(3);197-208

Page 174: Ortho wires part iii

References :

Charles J Burstone&AJ Goldberg;Beta Titanium;A new orthodontic alloy;AMJ Orthod 1980;77:121-132.

Wilcock AJ;Applied materials engineering for orthodontic wires; Aust Orthod J,1989;11(1);22-29

Andreasen GF& Marrow RE;Laboratory &clinical analysis of nitinol wire;AMJ Orthod 1978;73;142-151

Charles J Burstone,Qin&Morton;Chinese Niti wire;A new orthodontic alloy;AMJ Orthod 1985;87;445-451

Fujio Miura,Mogi,Ohura&Hamanaka;The super-elastic property of the Japanese NiTi alloy wire for use in orthodontics;AMJ Orthod Dentofac Orthop,1986;90;1-10

Page 175: Ortho wires part iii

References:

Rohit sachdeva;Orthodontics for the next

millenium;chapter-Biomechanical consideration in the

selection of NiTi alloys in orthodontics and variable

transformation temperature orthodontics with copper-

NiTi,1997;Ormco,227-247

A comparative study of metallurgical & working properties

of two new Titanium based alloy wires(TiMolium &Beta

III)with the earlier introduced titanium wires(TMA),and

also Alpha Titanium wires

-Dr. Jiku Abraham

Page 176: Ortho wires part iii

Clinical Insights on Copper NiTi

Charles R.Sager – A.Clinical Comment

- 35º - 17 x 25 or 19 x 25 – Initial A/w.

- Dead soft in hand, Resilient M. temp.

- Easy to place crimpable hooks

- For elastics or

- For ant. H.G.

Page 177: Ortho wires part iii

Clinical Insights on Copper NiTi

Charles R.Sager – A.Clinical Comment

- Ethyl chloride sprayed on cotton applicator.

- Bend back / Cinch back – flame the wire.

- Rect . A/W – Very early in treatment

Page 178: Ortho wires part iii

Allen Polland – Australia.

- 35º - 16 x 22 – for minimum crowding, non extraction.

- Triplex spray – for engaging the wire.

- No pain.

- H.G. – C1 pull H.G. for correction of class II molar relation

- Rectangular wire – to limit the lingual collapse of lower

anterior.

- Disadvantage – no transverse and vertical control.

Page 179: Ortho wires part iii

Randall C. Moles

Patient + doctor – time = Copper NiTi

- Temp – at which the wire will deliver its optimum

force level.

- 35º copper NiTi - initial phase 19 x 25.

Page 180: Ortho wires part iii

(Continued)

Dr.Kishor Bagalkot

Page 181: Ortho wires part iii

- Amount of force delivered by the wires to the D Alv

st. in the deactivation phase.

- Light forces - More physiologic.

- Literature about the delivery of forces - Large

variations.

Pseudoelasticity and thermoelasticity of NiTi

alloys: A clinically oriented review – Margherita

Santoro, Olivier F Nicolay. (AJO 2001)

Page 182: Ortho wires part iii

-Variations in forces delivered

- Non uniform methods of measuring i.e, N, cN, Pa.

-Alloy compn, CS, No of strands in the wire.

-In the early expts, uniaxial tensile tests for comparing

mechanical properties.

- Stretch of > 8% to see the SE properties.

Page 183: Ortho wires part iii

- Using cantilever configuration.

- Bending moments in gm/mm.

- Deflection in degrees.

- ADA approved method – Sp No. 32.

Flexural Tests:

Page 184: Ortho wires part iii

- May simulate SE behavior even for non SE alloy.

For reliable and valuable data, expts that simulate as

closely as possible IOl setting.

-3 bracket bending tests.

- Useful results for clinical needs.

- Unilateral bending tests.

Page 185: Ortho wires part iii

3 Bracket Bending Test

Page 186: Ortho wires part iii

3 Point Bending Test

Page 187: Ortho wires part iii

-Thermostats and insulated chambers.

-Alt approach – expts at room temp.

-Wires with TTR at oral temp. – partially M.

Tests at room temp. – as SE wires & low forces.

Temperature Settings:

Page 188: Ortho wires part iii

-An ideal arch wire – differential forces to the arch

segments.

-70gms – 80gms in the incisor area

-Gradually increase towards post. Segments upto 300gms

How heavy are the deactivation forces

Page 189: Ortho wires part iii
Page 190: Ortho wires part iii

- Small diameter multistranded st.st.

- SE wires

- Forces < 100gm

Page 191: Ortho wires part iii

Force delivery characteristics of some of the commercially available NiTi alloys*

Page 192: Ortho wires part iii

Force delivery characteristics of some of the

commercially available NiTi alloys

Page 193: Ortho wires part iii

0.016 x 0.022

600

500

400

300

200

100

NiTiNitinol SE Nitinol Classic 27ºC Cu Niti 35º C Cu Niti 40ºC Cu Niti Sentalloy(H) Neo Sentalloy

300 gms

215 gms

137 gms80 gms

87 gms

313 gms

293 gms

143 gms

Page 194: Ortho wires part iii

Two primary considerations.

1. An appropriate stress related TTR cor. to the

oral temp.

2. A physiologic force to the teeth and pdm.

How to choose a NiTi wire?

Page 195: Ortho wires part iii

- At least 2mm of deflection.

- Severe dental crowding.

- Not in very mild crowding.

- Pdly compromised patient.

How to choose a NiTi wire?

Page 196: Ortho wires part iii
Page 197: Ortho wires part iii

- The stress value Fairly constant

- Heat Rx with Nitrate Salt Bath – dramatic changes in these properties.

- It might be possible to bend the wire in to the other configurations and still be able to control the amount of force.

Japanese NiTiWire use of DE RHT method - Fujio

Minra Masakuni Mogi & Yoshiaki Ohura –EJO 1988

- Subject of basic research – Tokyo university – 1978.

- Spring back

- Shape memory

- SE

Page 198: Ortho wires part iii

Controlling the amount of force with SE

Material – 5 difnt diameters of Jap NiTi alloy wire

014,016,018,020 & 022.

Wires – Other wires

St.St., Co-Cr Ni, Work hardened NiTi

2 Parts Bending the A/W

Page 199: Ortho wires part iii

- Electric power supply – a transformer, timer, meter, foot switch.

- A pair of electric pliers.

- An electric arch holder.

Heating equipment ARCHMATE

Page 200: Ortho wires part iii

- A 6cm straight wire – curved

- Current – Wire – Memorized the new shape.

- A longer Rx time – less current

- The small wire – less current

Methods findings – Bending the A/W

Graph – Reln betn length of time & Amperage of Current

when wire bent for 90°

Page 201: Ortho wires part iii

- Jap NiTi – bent with DERHT rebounded to original 90° indicating pt deformn of 0° degree.

- i.e. On heat Rx – No change in spring back properly

- St. St. & Co-Cr Ni – Rebound 50°

- Work hardened NiTi - 75°

Testing the Mechl properties of wires

-A cantilever straightening test.

- Wires – Rebent - 90° to 0°

Page 202: Ortho wires part iii

3.5Amps – Arch holder – Ant. Segment – 45 mins

3.5 Amp – Pm segment + Ant segment 15mins.

i.e. A-A1 – 60 mins. Ends / Molars segments – Not heat

treated.

Controlling the Amount of force

Page 203: Ortho wires part iii

- Only desired secn of wire – heat treated.

2. Bending

- Pliers and finger cold hardening process

- Difficult for NiTi wire,

- Special pliers – loose spring back property

- DERHT does not diminish mech1 property

Discussion –

1. DERHT Method

- Utilizes electric resistance of wire to generate

Page 204: Ortho wires part iii

016” utility wire with electric pliers

Page 205: Ortho wires part iii
Page 206: Ortho wires part iii

Pseudoelasticity and Thermoelasticity of NiTi

alloys: A Clinically Oriented Review – Margherita

Santoro, Olivier F Nicolay. (AJO 2001)

- Data available in the literature - TTR S of alloys.

- Thermomechl behavior – Correln betn TTR and Oral temp.

- Buehler – 1960

- NiTi orthodontic alloy – Andreasen

Page 207: Ortho wires part iii

- Claims

- Difnt parameters and Exptl settings to analyze difnt

compns and properties.

- Improvements

Page 208: Ortho wires part iii

Thermoelasticity and Shape memory effect:

An ideal NiTi – Stable at mouth.

- Formable at room temp.

Most Recent Techno – Advances – SE NiTi s

SE NiTi

A - Phase

M - Phase

‘R’ - Phase

Mechl Properties and composition of NiTi alloys

Page 209: Ortho wires part iii

- Molecular arrangement - modified

- No change in atomic compn

- Transformn Diffusionless

- Smart Material

Temp variations Crystal St. Deformns

Mechl Properties and composition of NiTi alloys

Page 210: Ortho wires part iii

- Crystal st of alloy confirmed by

- Radiographic diffracn

- Difntial scanning calorimetry

- Each NiTi alloy specific TTR

Mechl Properties and composition of NiTi alloys

Page 211: Ortho wires part iii

Resistivity of SE NiTi to Temp

-Both A and M difnt amount of resistance to passage of

electric currents.

Mechl Properties and composition of NiTi alloys

Page 212: Ortho wires part iii

- At higher temp > Af wire remains in Austenitic

phase.

- Shape memory - Wire in A – Phase able to memorize a

PREFORMED shape.

Mechl Properties and composition of NiTi alloys

- Low temp. M.; Temp A

Page 213: Ortho wires part iii

Every time Temp > Af Arch form.

Technically One way shape Memory Effect.

Eg – CuNiTi 40º

At room temp. M or mixed phase sharp bends.

Wire Hot water Temp > Af i e 40ºc Original arch form.

- Temp M pliable and easily deformed.

Page 214: Ortho wires part iii

- When Completely austenitic Above Af Stress strain

curve follows Regular pattern of other alloys such as St.St. ie

Lack of plateau.

A - NiTi More Elastic than other Alloys.

Not SE (In absence of Stress)

- Af.< Oral Temp, wire primarily A – IOly and Fully M – EOly

Page 215: Ortho wires part iii

Objectives of Research New Alloy like CuNiTi.

TTR cor to oral Temp and Reach Af above Oral

Temp.

In phase transition, both A and M – NiTi will be stiffer

than SE wire

-NiTi absorbs Deflecn stresses.

ME low more stiffer.

Page 216: Ortho wires part iii

- When only moderate deflection in required A NiTi

deliver biologically acceptable force.

- Low forces of NiTi Hypothetical

- Need to be compared with force delivery of other alloys

through proper expts.

- The performance of any NiTi – Composition and

Manufacturing procedures.

Page 217: Ortho wires part iii

A + (Small M) + R Phase Grain St.

To activate SE properties quantities of M

On Stress appn Deflection (SIM) formed

Local M. Transformation Even rest of wire remains A

Pseudoelasticity

These areas wire will be SE till the tooth moves.

– When Af below oral temp.; A phase intra orally

Page 218: Ortho wires part iii

This property Pseudoelasticity.

A localized stress related SE phenomenon

- SIM formation possible only. Af slightly lower than oral

temp.

- If Af considerably lower than oral temp – more Austenitic

and Too much energy required for maintaining (SIM).

- SIM Compensates for TIM and contributes to SE properties.

Only in cases of very severe crowding

An A – NiTi behaves SE lically.

Page 219: Ortho wires part iii

-Pseudo and thermoelasticsity not always present

-Advertisement Confusing/misleading

-Attempt to simplify the clinical choice

Review of Available Alloys

Page 220: Ortho wires part iii

NiTi : Generally classified - SE

- Non SE

SE Pseudoelastic Chinese NiTi

Japanese NiTi

Thermoelastic - Copper NiTi

Review of Available Alloys

Page 221: Ortho wires part iii

Review of Available Alloys

- Heat treatment and pressure variations

- Modifications of atomic compn eg. CuNiTi

Tech Advancements - TTR at sp temp. 27º,35º,40º C

Page 222: Ortho wires part iii

1. TTR betn room and body temp - M active alloys

2. TTR below oral temp – A active alloys

3. TTR close to body temp – on insertion, shape memory

Review of Available Alloys

Water’s review – 1992 – three groups based on their TTRs

Page 223: Ortho wires part iii

Review of Available Alloys

Phase I Au & St.St.

Phase II Stabilized eg. Work hardened Nitinol

Phase III SE – A, Active Austinitic, TTR < oral temp,

predominantly A at room temp.

Phase IV Thermodynamic.

Phase V Graded thermodynamic

Recently Evans and Durning – 5 groups

Page 224: Ortho wires part iii

Review of Available Alloys:

- TTR close or cor to oral temp.- working range at room temp - On temp both SIM & TIM Austinite

-Wires Af above 37ºC i.e. CuNiTi 40ºC

-Austinite forms only when the temp above 40ºC

- Hot rinses to force

- Cold rinses to discomfort

Phase V Graded thermodynamic

Phase IV Thermodynamic - Active Martensitic

Page 225: Ortho wires part iii

- TTR close or slightly below oral temp. to allow SIM

formn

TTRs of available alloys

- Several expts – to verify TTR values

Page 226: Ortho wires part iii

2. Complexity of Manufacturing procedures.

- Wires of lllr compn difnt TTRs

- Expt1 findings Not comparable

- Some manufactures don’t provide accurate

informns of TTR

Variations in TTRs

1. IO1 temp wide fluctuations – Appx – 35º - 37º expt1

settings.

TTRs of available alloys

Page 227: Ortho wires part iii

-Most alloys TTR betn 17º & 32ºC

-Practically unable to exhibit – SE behavior during clinical

applicns

-CuNiTi s 27 & 35º Af active Austenite

- CuNiTi 40ºC Truly SE at oral temp.

Yoneyama, Doi and Hanamaka – used differential scanning

claorimetory

TTRs of available alloys

Page 228: Ortho wires part iii

-Formn of SIM Shift of TTR towards higher temp.

-On stress apln maintains Martensitic phase.

Higher energy to reconvert SIM A

Clinically stress related TTR/Stress related Af

-Actual temp at which thermoactive wires activated.

-Necessity of studying TTR in +nce of stress.

Stress related TTRs

Page 229: Ortho wires part iii

Coluzzi et al :

When No Deflecn NeoSentalloy – Af - 28ºC

On Loading Af - ed proportionally to 34ºC

Leone’s unloaded 20ºC

on loading 35ºC

- Deflecn device loading of 2

- At 5ºC all alloys M 2.38mm of PDn

- At 37ºC all alloys A 0.08mm of PDn

Mullins, Bagby & Norman – N.Sentalloy – F100, 200, 300

& bioforce sentalloy

Page 230: Ortho wires part iii

– Compared thermodynamic properties of active arch Nitinol

Heat activated Nitinol and Neosentalloy.

Expt setup Variation of cantiliver bend test in temp

controlled environments.

Bishara et al

Page 231: Ortho wires part iii

-30º and 40º bends in straight wire segments

-Samples Immersed in H2O

-100% Recovery of original shape.

-All alloys TTR an average betn 21-28ºC

All Samples TTR below oral temp.

Page 232: Ortho wires part iii

Santoro & Beshers.

Neosentalloy

27º Se CuNi & Thermoactive 35 & 40º CuNiTi

Active Arch Nitinol.

-Thermoactive NiTi alloys also studied under stress.

Page 233: Ortho wires part iii

Neosentalloy Stress related Af - 28ºC

27º SeE CuNiTi Stress related Af - 32ºC

Both Mainly Austenitic Ioly even +nce of Delfect.

35º CuNiTi – Stress related Af 39ºC

40º CuNiTi

Expt1 Setting Crowded lower incisors.

Page 234: Ortho wires part iii

In summary – 2 fundamental properties to select a NiTi wire.

1. A proper stress related TIR cor to or slightly below oral temp.

2. A Low deactivation force to the dentoalv. St.

Page 235: Ortho wires part iii

• Light forces - bone hyaline

• Limit undermined resorption

• More physiologic tooth movt.

• A review of literature large variations in study designs

Part II Deactivation forces:

• Amount of force delivered by wires to dentoalv. St. in

Deactivation force.

Page 236: Ortho wires part iii

• Forces may be given in cN, N, or expressed as strengths in parcals

• In clinical practice, forces in gms/ounces.

• Parameter commonly used force delivery – Stiffness values i.e. force required to obtain a deflecn in the wire below the yield point.

• Does not give useful informn about amount of force to D.Alv. st.

Part II Deactivation forces:

• Methods used to measure force not uniform.

Page 237: Ortho wires part iii

• Alloy compn

• CS

• No of strands of wire used in the expt

         Specific expts to obtain direct clinical data

Force delivery influenced by

Page 238: Ortho wires part iii

Wire attached at one end & stretched.

A stretch of more than 8% to see SE expression

Forces - not usually observed in clinical aplns

Generally produce values of ME which are

significantly lower than those obtained by deflecn

tests.

In early expts, - uniaxial tensile tests – most acceptable

for comparing mechl properties of difnt alloys.

Page 239: Ortho wires part iii

• Forces evaluated on bending moments

• Expressed in gms/mms.

• Delfecn – measured in degrees.

Flexural tests using cantilever configurn

• Cantilever tests -ADA approved

• ADA Sp No. 32

• A single direcn deformn by unilat1 bending.

• May simulate SE behavior (even if alloys is not SE)

Page 240: Ortho wires part iii

• Wire slides unrestrained over the supp device

• Fricn the loading force SE behavior

• Non restrained - No considn of fricn by ligations.

Does not reproduce the clinical constraint.

To obtain reliable & valuable data.

• Free end principle

Page 241: Ortho wires part iii

• Consistent method of ligation of wire

• IB distance

• Type of Bracket used

• Length of wire specimen.

Expts simulate IO clinical setting.

Page 242: Ortho wires part iii

- Used in recent lab expts on A-NiTi

- Common finding – High stiffness if wire is deflected less than 2mm.

- Because of lack of formn of SIM

ANiTi presents 0.28 Stiffness for small deflecns

Nitinol presents 0.20 – stiffness for small deflecns

3 Bracket B.Test – Partially restrained model

Page 243: Ortho wires part iii

Threshold of 2mm – minimum activation of SE – A NiTi

Stress strain curves for St.St. Nitinol & NiTi -

Page 244: Ortho wires part iii

- Consistent +nce of Martensite – Lowering deactivn force.

- Martensite – Low stiffness phase – ME 2000000psi

- Austenite – higher stiffness phase – ME – 8000000psi

- The relative concn of two phases - Resultant stiffness &

amount force delivered.  

 

On Stress:

A – SIM – Pseudoelasticity

Page 245: Ortho wires part iii

• Initial activn force – 3 times more than Nitinol.

• Once SIM forms – Hzl plateau appears.

• Alloy absorbs any additional load and releases it.

• Linear region cor to deactn plateau lower than the activn

phase.

• SE compounds – high stiffness initially when deflecn minm.

Page 246: Ortho wires part iii

Nakano et al – 16 x 22 Nitinol SE – 3pt BT at 37

Segner & Ibe, Oltjen – 16 x 22 Nitinol SE – 3 brackets BT at 35

Other authors – Nitinol SE – 79.6 9/mm at room temp.

Dift. Expt1 settings – Results

Nitinol SE, Nitinol classic

Page 247: Ortho wires part iii

• Control of temp – Thermostats & Insulated chambers.

• Numerous expts – done at room temp.

• Wires – TTR at O1 temp – partially Martensitic

• When Tests conducted at room temp – performs as SE

• At oral temp- M A.

• Highest temp at which SIM can form – Md.

• In active A-NiTi – Md > Af

Temperature settings

Page 248: Ortho wires part iii

-   In active Martensitic wire – TTR at oral temp so that amount of M – constantly available.

-   Tonners & Waters – Plateau with of temp.

-   Sentalloy light 0.016 – 20 cN at 35C – 62 cN at 50C

-   Sentalloy heavy .016 - .77 cN at 35C, 108 cN at 50C

-   Ormco NiTi – 102 cN at 35 - 112 cN at 50C

-  Af – located slightly below oral temp.

Temperature settings

Authors confirmed• temp - SIM

• SE wires at least 2mm of deflecn.

Page 249: Ortho wires part iii

• How heavy are the deactn forces.

• Depends on Ratio betn Magnitude of force & affected Root Bone surface.

• An ideal A/W – differential forces.

• Forces < 100gm – by small multistranded st.st.

Stress strain values –

Page 250: Ortho wires part iii

• Manufacturing process• Difnt expt1 settings.

Variability of E properties -

16x22 sentalloy medium – 3BBT – 695 gm/mm if – for clinical appln

- To maintain 100gm force - .016 round wire. - 73gm in 3 PBT

Eg. 1. Sentalloy

16x22 sentalloy medium – 3 PBT 193gm /mm

Page 251: Ortho wires part iii

- 3 PBT at 37C – 143gm/mm force

- 3 BBT – 36gm

2. For Neosentalloy –

16 x 22 wire type F240

Page 252: Ortho wires part iii

- Light forces – range of or below 100 gm/mm 3 BBT at oral temp. 37° C.

27 ° SE CuNiTi – 137 gm/mm

Small diameter round wire.

Cu NiTi – 16 x 22 35° & 45° C

Page 253: Ortho wires part iii

Multibraided strand NiTi wire – 17 x 25 – 12.4gm/mm.

Classic Multi stranded St.St. – 17 x 25 - 170.7 gm/mm.

0175 – st.st in 6 strand – 43.1 gm/mm.

Lab tests – st. st 4 to 5 times more stiffer than SE NiTi.

Multi stranded St St Vs. Nickel Titanium

Oltjen et al – 3 BBT at room temp.

A NiTi 17x25 – 2mm deflecn – 18gm/mm.

Page 254: Ortho wires part iii

- Multi stranded st.st, Nitinol & Chinese NiTi – compared to

test degree of pt deformation.

- > 50% of Braided st. st – pth deformed.

- 3 PBT – 4mm deflecn - at 2mm - Braided wire – moderate

plastic deformn.

- Exceptional spring back and

- R to pt deformn – over a longer period.

Advantage of SE wire

Page 255: Ortho wires part iii

- Range of force by multist st.st. – Acceptable.

SE. NiTi – Elective choice

1. Moderate crowding

2. Arch form & torque control require in initial stages.

Acc to data – minm crowding – A multistr. St.St. wire.

- i.e. Less force + Torque control required.

lar Cu NiTi 40°C

In cases of severe crowding & Pdl compromised pts

Page 256: Ortho wires part iii

- Miura – immersed several SE NiTi wires – in Nitrate

Salt bath at difnt temps.

- Bending Test for testing mechl properties.

Jap NiTi - 500° C for 20 mins

Force – 300 – 50 gm

i.e. A higher temp Rx – Complete loss of SE properties.

Graded Thermodynamic NiTi

Page 257: Ortho wires part iii

- Heat Rx of selected secns of A/W by means of difnt currents, delivered by electric pliers.

- Modified values of deactivn forces by varying the amount of Austenite in the alloy.

- After heating ant segment 60 mins – force – 80gms

- lllr procedures – Bioforce wires – selective force.

- Evans & Durning – Classified – Phase V or Graded Thermodynamic NiTi.

A few years later,

- DERHT – Direct Electric Resistance Heat Treatment.

Page 258: Ortho wires part iii

Filleul & Jordan

- Used differential scanning calorimetry.

- Teq – that measures Euthalpy of phase transition .

Torsional Behavior

- Rect NiTi wires – Early Torque control during the aligning.

Page 259: Ortho wires part iii

At 22°C, 39° & 44°C

N.S.F100 - 22°C – SE plateau – 910gm/mm Torque

At higher temp – No plateau – wires – Austenite

Filleul & Jordan

- 17 x 25 - Neo sentalloys F100,

35° Cu NiTi

40° Cu NiTi

Page 260: Ortho wires part iii

19 x 25 st.st – 30° degree twist – 3000gm/mm

Deactivn of SE NiTi – Definitely Lower than St.St.

Temp - Torquing forces of NiTi.

CuNiTi - 35° & 40° - Equivalent torsional behavior

21.7°C – SE plateau – 560gm/mm torque

39° C – SE plateau – 1190gm/mm torque

44° C – SE plateau – 1400 gm/mm torque.

Page 261: Ortho wires part iii

- Temp - force by 85%

- Force variations – Transient

For All Cu NiTis & Neo Sentalloys –

- 20° constant twist - 37°C – 1000gm/mm

Meling & Odegaard

- Temp - Torsional force

Page 262: Ortho wires part iii

- Rate of tooth movt – light cont forces – double.

- Histologically – Normal oblasts, oclasts in Plig of rats when SE NiTi.

- When work hardened alloy – hyalinizn - no of cells.

Clinical Trials:

- Randomized clinical trials

- Faster tooth movt.

- Less pt discomfort

Acc to Expt1 data obtained on rats.

By Warita Et al

Page 263: Ortho wires part iii

Jones & Richmond –

Triple strand .015 St.St. = 0.014 sentalloy

West et al :

- 015 multist st.st. Vs. 014 A-NiTi

- 6 weeks clinical trial

- SE wires showed better performance only in lower incisors

OBrien et al

- No difference in rate of tooth movt. betn. Austenite & work hardened alloy

Page 264: Ortho wires part iii

Reitan & Storey – Definite Reln betn amount of force &

pain.

Jones & Chan – recorded pain & discomfort

- 014 Heavy sentalloy

- 015 multistranded st.st.

Minm discomfort – by pt.

Page 265: Ortho wires part iii

1. More pain after A/W insertion than that of Xn

2. No difference betn A/W

3. No difference degree of crowding

4. Significant coreln betn age and level of pain

- Pain reported by pt –

Page 266: Ortho wires part iii

1. An appropriate stress – related TTR cor to oral temp.

2. A physiologic force.

Considerations for choosing NiTi

Page 267: Ortho wires part iii

1. Type of loading

- lllr to oral condn/clinical appln. - 3

BBT – most consistent device.

2. Amount of loading

- At least 2mm deflect – SIM formation

- Below 2mm – higher force – more A

- Severe dental crowding

- Deflecn – Localized SIM

Expts to study NiTi

Page 268: Ortho wires part iii

- No need of SE wire

- A small diameter work hardened alloy or

- Multistranded round st.st. wire

In pdly compromised pts – force level > 100gm

- controlled force levels

Mild Crowding

Page 269: Ortho wires part iii