pej36l~'1 p£f36~t0 · w p£f36~t0 2 x sample condition: d non-hazardous d flammable d skin...

23
POLLEN ENVIRONMENTAL, LLC. CHAIN OF CUSTODY /WORKORDER FORM 3536 International Street Fairbanks, AK 99701 (907) 479-8368 Phone (907) 452-6853 Fax jer[email protected] CLIENT INFORMATION Company: City of North Pole Address: 1 25 Snowman Lane City, State Zip: North Pole, AK 99705 Phone: 907-388-1907 Fax: 907-488-1825 Email: northpoleutilities@alaska. net Project Name: QC PFC Monitoring Sampled By: JEP Samole Identification Samole Date We ll A 10/3/2017 We ll A Dup. 10/3/2017 Field Bl ank 10/3/2017 Trio Bl ank 10/ 3/2017 Possible Hazard Identification: SamoleTime 10:05 AM 10:06 AM 10:08 AM 10:05 AM Cont act Person: Requested Analysis Paul Trissel Perservatlve Added WWTP APDES #: Pws 1D #: 31os7s repod ,:;: $ -,pec-;a / Send Results to ADEC: I ' ,J Yes D No Purchase O rder/Charge Code: . 9.0;1 - 565 Cf) u LL a.. Matrix Lab ID# Sub Lab ID# w f£F 3{ 851 2 X w P EP3t8E8 2 X w PEJ 36 l~'1 2 X w P£F36~t 0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature on arrival: oc COC Seal: Special I nstructions/QC Requirements & Comments: A " - " Rer)}/Jt / 1 'V:I M. A · ' //UT,U/'"I' l Company:f)J// {]// fAv Da1e/f!.}rqe;,r7 II OOa JN') Recei ved by: Company: 1 nqui,ed by: Company: Date & Ti me: Received by: Company: reli nquished by: Company: Date & Ti me: Received by: Company: A cc uracy, Preci s ion, and Profess ional Servi ce COC# CONP 2017 Page l of l Normal Turnaround RUSH __ day(s) Samole Comments D Intact D Broken D Absent D Intact D Broken D Absent Date & Time: Date & Time: Date & Ti me:

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Page 1: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

POLLEN ENVIRONMENTAL, LLC. CHAIN OF CUSTODY /WORKORDER FORM 3536 International Street

Fairbanks, AK 99701

(907) 479-8368 Phone (907) 452-6853 Fax

[email protected]

CLIENT INFORMATION

Company: City of North Pole

Address: 1 25 Snowman Lane

City, State Zip: North Pole, AK 99705

Phone: 907-388-1907

Fax: 907-488-1825

Email: [email protected]

Project Name: QC PFC Monitoring

Sampled By: JEP

Samole Identification Samole Date

W ell A 10/3/2017

W ell A Dup. 10/3/2017

Field Blank 10/3/2017

Trio Blank 10/3/2017

Possible Hazard Identification:

SamoleTime

10:05 AM

10:06 AM

10:08 AM

10:05 AM

Contact Person: Requested Analysis Paul Trissel

Perservatlve Added

WWTP APDES #:

Pws 1D #: 31os7s ~ repod ,:;:$ -,pec-;a/ Send Results to ADEC: I '

,J Yes D No

Purchase Order/Charge Code:

.9.0;1-565 Cf)

u LL a..

Matrix Lab ID# Sub Lab ID#

w f£F3{851 2 X

w PEP3t8E8 2 X

w PEJ36l~'1 2 X

w P£F36~t0 2 X

Sample Condition:

D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal:

Sub Lab Temoerature on arrival: oc COC Seal:

Special I nstructions/QC Requirements & Comments:

A " -" Rer)}/Jt/1'V:IM. A · '//UT,U/'"I' l

Company:f)J//{]// fAv Da1e/f!.}rqe;,r7 ~ II OOaJN') Received by: Company:

1 nqui,ed by: Company: Date & Time: Received by: Company:

relinquished by: Company: Date & Time: Received by : Company:

Accuracy, Precision, and Professional Service

COC# CONP 2017

Page l of l

□ Normal Turnaround

□ RUSH __ day(s)

Samole Comments

D Intact D Broken D Absent

D Intact D Broken D Absent

Date & Time:

Date & Time:

Date & Time:

Page 2: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

City of North Pole WTP Report Date: 11/1/2017Attn: Paul Trissel Sample Date: 10/3/2017125 Snowman Lane Sample Time: 10:05-10:08 AMNorth Pole, AK 99705 Sampled By: Jerry PollenPhone: 907-388-1907Fax: [email protected]

Project Name: CONP WTP PFC MonitoringAnalysis: PFC'SAnalysis Method: EPA 537COC#: CONP 2017Sample Matrix: Drinking WaterPWS ID#: AK2310675

Attached are the results for analysis of your samples. This sample was analyzed by

Eurofins Eaton Analytical in South Bend, IN.

Client Sample ID: Eurofins Eaton Analytical ID:Well A PEF36857Well A Dup. PEF36858 3793430Field Blank* PEF36859 3793431Travel Blank PEF36860 3793432

*PFC reagent water added to Field Blank bottle at the time and location of Well A sample collection.

Comments: Well A sample result for PFHxS is 1.9ng/L. This result is slightly below the laboratories detection limit of 2.0ng/L, so the report indicates the result is <2.0ng/L. This is being addressed due to the detection of 2.0ng/L of PFHxS in the Well A Dup. sample.

Jerry PollenPollen Environmental, LLC - Fairbanks

CERTIFICATE OF ANALYSIS

Pollen Env ID:3793429

Pollen Environmental, LLC

Page 3: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

LABORATORY REPORT

This report may not be reproduced, except in full, without written approval from EEA.

If you have any questions concerning this report, please do not hesitate to call us at (800) 332-4345 or (574) 233-4777.

Page 1 of 21

=::: e u rofi n s I Eaton Analytical

Page 4: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

 

Revision date:  08/28/2017  

STATE CERTIFICATION LIST

State Certification State Certification Alabama 40700 Missouri 880 Alaska IN00035 Montana CERT0026 Arizona AZ0432 Nebraska NE-OS-05-04

Arkansas IN00035 Nevada IN00035 California 2920 New Hampshire* 2124 Colorado IN035 New Jersey* IN598

Colorado Radiochemistry IN035 New Mexico IN00035 Connecticut PH-0132 New York* 11398 Delaware IN035 North Carolina 18700 Florida* E87775 North Dakota R-035 Georgia 929 Ohio 87775 Hawaii IN035 Oklahoma D9508 Idaho IN00035 Oregon (Primary AB)* 4074-001

Illinois* 200001 Pennsylvania* 68-00466 Illinois Microbiology 17767 Puerto Rico IN00035

Illinois Radiochemistry IN00035 Rhode Island LAO00343 Indiana Chemistry C-71-01 South Carolina 95005

Indiana Microbiology M-76-07 South Dakota IN00035 Iowa 098 Tennessee TN02973

Kansas* E-10233 Texas* T104704187-15-8Kentucky 90056 Texas/TCEQ TX207

Louisiana* LA170006 Utah* IN00035 Maine IN00035 Vermont VT-8775

Maryland 209 Virginia* 460275 Massachusetts M-IN035 Washington C837

Michigan 9926 West Virginia 9927 C Minnesota* 018-999-338 Wisconsin 999766900 Mississippi IN035 Wyoming IN035

EPA IN00035 *NELAP/TNI Recognized Accreditation Bodies

Page 2 of 21

·=- eurofins I t Analytical -:.• Ea on

Page 5: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

Laboratory Report

Client:

Attn:

Report:

Priority:

Status:

PWS ID:

Pollen Environmental LLC

Jerry Pollen

3536 International Avenue

399812

AK2310675

Standard Written

Final

IN00035Alaska Lab ID #

Fairbanks, AK 99701

110 South Hill Street

South Bend, IN 46617

Tel: (574) 233-4777

Fax: (574) 233-8207

1 800 332 4345

*NR = The chlorine demand was not performed for this

analytical sample, at the request of the client.

EEA

ID #

Client ID Method Collected

Date / Time

Collected

By:

Received

Date / Time

3793429 PEF36857 Well A 537 10/03/17 10:05 Client 10/05/17 08:30

3793430 PEF36858 Well A Dup. 537 10/03/17 10:06 Client 10/05/17 08:30

3793431 PEF36859 FTB 537 10/03/17 10:08 Client 10/05/17 08:30

3793432 PEF36860 LTB-09/13/17 537 10/03/17 10:05 EEA 10/05/17 08:30

Sample Information

Report Summary

Note: This report was amended on 10/20/2017 to report additional compounds at the request of the client.

Note: This report was further amended on 11/01/17 to report field blank and lab blank results, at the request of the client.

Detailed quantitative results are presented on the following pages. The results presented relate only to the samples provided for

analysis.

We appreciate the opportunity to provide you with this analysis. If you have any questions concerning this report, please do not

hesitate to call Traci Chlebowski at (574) 233-4777.

Note: This report may not be reproduced, except in full, without written approval from EEA.

Client Name:

Report #:

Pollen Environmental LLC

399812

Authorized Signature Title Date

11/01/2017

Page 1 of 4

Page 3 of 21

=:~ eurofins I Eaton Analytical

Page 6: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

Client Name: Report #: 399812Pollen Environmental LLC

Sampling Point: PWS ID:PEF36857 Well A AK2310675

EEA Methods

Analyte

ID #

Analyte Method Reg

Limit

MRL† Result Units Preparation

Date

Analyzed

Date

EEA

ID #

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorobutanesulfonic acid (PFBS)375-73-5

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorodecanoic acid (PFDA)335-76-2

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluoroheptanoic acid (PFHpA)375-85-9

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorohexanesulfonic acid (PFHxS)355-46-4

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorohexanoic acid (PFHxA)307-24-4

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorolauric acid (PFDoA)307-55-1

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluoromyristic acid (PFTA)376-06-7

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorononanoic acid (PFNA)375-95-1

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorooctane sulfonate (PFOS)1763-23-1

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorotridecanoic acid (PFTrDA)72629-94-8

379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluoroundecanoic acid (PFUnA)2058-94-8

Sampling Point: PWS ID:PEF36858 Well A Dup. AK2310675

EEA Methods

Analyte

ID #

Analyte Method Reg

Limit

MRL† Result Units Preparation

Date

Analyzed

Date

EEA

ID #

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorobutanesulfonic acid (PFBS)375-73-5

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorodecanoic acid (PFDA)335-76-2

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluoroheptanoic acid (PFHpA)375-85-9

379343010/11/17 01:2710/10/17 08:00ng/L2.02.0---537Perfluorohexanesulfonic acid (PFHxS)355-46-4

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorohexanoic acid (PFHxA)307-24-4

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorolauric acid (PFDoA)307-55-1

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluoromyristic acid (PFTA)376-06-7

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorononanoic acid (PFNA)375-95-1

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorooctane sulfonate (PFOS)1763-23-1

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorotridecanoic acid (PFTrDA)72629-94-8

379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluoroundecanoic acid (PFUnA)2058-94-8

Page 2 of 4Page 4 of 21

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Client Name: Report #: 399812Pollen Environmental LLC

Sampling Point: PWS ID:PEF36859 FTB AK2310675

EEA Methods

Analyte

ID #

Analyte Method Reg

Limit

MRL† Result Units Preparation

Date

Analyzed

Date

EEA

ID #

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorobutanesulfonic acid (PFBS)375-73-5

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorodecanoic acid (PFDA)335-76-2

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluoroheptanoic acid (PFHpA)375-85-9

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorohexanesulfonic acid (PFHxS)355-46-4

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorohexanoic acid (PFHxA)307-24-4

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorolauric acid (PFDoA)307-55-1

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluoromyristic acid (PFTA)376-06-7

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorononanoic acid (PFNA)375-95-1

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorooctane sulfonate (PFOS)1763-23-1

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorotridecanoic acid (PFTrDA)72629-94-8

379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluoroundecanoic acid (PFUnA)2058-94-8

Sampling Point: PWS ID:PEF36860 LTB-09/13/17 Not Supplied

EEA Methods

Analyte

ID #

Analyte Method Reg

Limit

MRL† Result Units Preparation

Date

Analyzed

Date

EEA

ID #

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorobutanesulfonic acid (PFBS)375-73-5

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorodecanoic acid (PFDA)335-76-2

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluoroheptanoic acid (PFHpA)375-85-9

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorohexanesulfonic acid (PFHxS)355-46-4

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorohexanoic acid (PFHxA)307-24-4

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorolauric acid (PFDoA)307-55-1

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluoromyristic acid (PFTA)376-06-7

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorononanoic acid (PFNA)375-95-1

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorooctane sulfonate (PFOS)1763-23-1

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorotridecanoic acid (PFTrDA)72629-94-8

379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluoroundecanoic acid (PFUnA)2058-94-8

Reg Limit Type:

Symbol:

MCL SMCL AL

* ^ !

† EEA has demonstrated it can achieve these report limits in reagent water, but can not document them in all sample matrices.

Page 3 of 4Page 5 of 21

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Client Name: Report #: 399812Pollen Environmental LLC

Lab Definitions

Continuing Calibration Check Standard (CCC) / Continuing Calibration Verification (CCV) / Initial Calibration

Verification Standard (ICV) / Initial Performance Check (IPC) - is a standard containing one or more of the target

analytes that is prepared from the same standards used to calibrate the instrument. This standard is used to verify

the calibration curve at the beginning of each analytical sequence, and may also be analyzed throughout and at the

end of the sequence. The concentration of continuing standards may be varied, when prescribed by the reference

method, so that the range of the calibration curve is verified on a regular basis. CCL, CCM, and CCH are the CCC

standards at low, mid, and high concentration levels, respectively.

Internal Standards (IS) - are pure compounds with properties similar to the analytes of interest, which are added to

field samples or extracts, calibration standards, and quality control standards at a known concentration. They are

used to measure the relative responses of the analytes of interest and surrogates in the sample, calibration standard

or quality control standard.

Laboratory Duplicate (LD) - is a field sample aliquot taken from the same sample container in the laboratory and

analyzed separately using identical procedures. Analysis of laboratory duplicates provides a measure of the

precision of the laboratory procedures.

Laboratory Fortified Blank (LFB) / Laboratory Control Sample (LCS) - is an aliquot of reagent water to which

known concentrations of the analytes of interest are added. The LFB is analyzed exactly the same as the field

samples. LFBs are used to determine whether the method is in control. FBL, FBM, and FBH are the LFB samples at

low, mid, and high concentration levels, respectively.

Laboratory Method Blank (LMB) / Laboratory Reagent Blank (LRB) - is a sample of reagent water included in the

sample batch analyzed in the same way as the associated field samples. The LMB is used to determine if method

analytes or other background contamination have been introduced during the preparation or analytical procedure.

The LMB is analyzed exactly the same as the field samples.

Laboratory Trip Blank (LTB) / Field Reagent Blank (FRB) - is a sample of laboratory reagent water placed in a

sample container in the laboratory and treated as a field sample, including storage, preservation, and all analytical

procedures. The FRB/LTB container follows the collection bottles to and from the collection site, but the FRB/LTB is

not opened at any time during the trip. The FRB/LTB is primarily a travel blank used to verify that the samples were

not contaminated during shipment.

Matrix Spike Duplicate Sample (MSD) / Laboratory Fortified Sample Matrix Duplicate (LFSMD) - is a sample

aliquot taken from the same field sample source as the Matrix Spike Sample to which known quantities of the

analytes of interest are added in the laboratory. The MSD is analyzed exactly the same as the field samples.

Analysis of the MSD provides a measure of the precision of the laboratory procedures in a specific matrix. SDL,

SDM, and SDH / LFSMDL, LFSMDM, and LFSMDH are the MSD or LFSMD at low, mid, and high concentration

levels, respectively.

Matrix Spike Sample (MS) / Laboratory Fortified Sample Matrix (LFSM) - is a sample aliquot taken from field

sample source to which known quantities of the analytes of interest are added in the laboratory. The MS is analyzed

exactly the same as the field samples. The purpose is to demonstrate recovery of the analytes from a sample matrix

to determine if the specific matrix contributes bias to the analytical results. MSL, MSM, and MSH / LFSML, LFSMM,

and LFSMH are the MS or LFSM at low, mid, and high concentration levels, respectively.

Quality Control Standard (QCS) / Second Source Calibration Verification (SSCV) - is a solution containing

known concentrations of the analytes of interest prepared from a source different from the source of the calibration

standards. The solution is obtained from a second manufacturer or lot if the lot can be demonstrated by the

manufacturer as prepared independently from other lots. The QCS sample is analyzed using the same procedures

as field samples. The QCS is used as a check on the calibration standards used in the method on a routine basis.

Reporting Limit Check (RLC) / Initial Calibration Check Standard (ICCS) - is a procedural standard that is

analyzed each day to evaluate instrument performance at or below the minimum reporting limit (MRL).

Surrogate Standard (SS) / Surrogate Analyte (SUR) - is a pure compound with properties similar to the analytes of

interest, which is highly unlikely to be found in any field sample, that is added to the field samples, calibration

standards, blanks and quality control standards before sample preparation. The SS is used to evaluate the efficiency

of the sample preparation process.

Page 4 of 4Page 6 of 21

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Page 7 of 21

p~C,{ S5 io-511 CN:[l(?:x)

I ~

1e 10-s,1

POLLEN ENVIRONMENTAL, LLC. 3 0°!2//--

CHAIN OF CUSTODY /WORKORDER FORM 3536 International Street

Fairbanks, AK 99701

(907) 479-8368 Phone (907) 452-6853 Fax

[email protected]

CLIENT INFORMATION

Company: City of North Pole

Address: 125 Snowman Lane

City, State Zip: North Pole, AK 99705

Phone: 907-388- 1907

Fax: 907-488-1825

Email: [email protected]

Project Name: QC PFC Monitoring

Sampled By : JEP

Samole,Identification Samole Date"

Well A 10/3/2017

Well A Dup. 10/3/2017

Field Blank 10/3/2017

Trip Blank 10/3/2017

,,

Possible Hazard Identification:

Samole Tim•

10:05 AM

10:06 AM

10:08 AM

10:05 AM

Contact Person:

Paul Trissel

WWTP APDES # :

pws m # : 31061s ,, report Gr:f 5pin"al Send Results to ADEC: I I

,J Yes D No

Purchase Order/Charge Code:

;J.O;'l-565

Matrix_ Lab ID# Sub Lab ID#

w lJEf 3fi!fl m~ l-/;z.q 7lf3t8E8 - 430 w

w ff3tl §1 L/3) w P€F36~to .y 43~

-3 J<lO/<pc# CONP 2017

Requested Analysis

Page 1 of 1

Perservatlve Added

D Normal Turnaround

~ . C

D RUSH --day(s) 'ii C 0 u 0 {,/) L u . .,, E LL ,

Cl.. z Samole.Comments

2 X (_t z) Ct A0 2 X {e 0 ' 2 X(r,

,-2 X{.J /,) r-:t 1, 7 ·- I -, l ,"l I

Sample Condit ion:

D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: •c (. g•c COC Seal: D I ntact D Broken D Absent

Sub Lab Temoerature on arrival: COC Seal: K intact D Broken D Absent

Special Instructions/QC Requirements &. Comments:

A ,.. A

Re'.Wl&!, TJ,tf f//4 A • 11//U ffl' {

Company:f,J // et/ &n/ Daj!J~irct-f1 ~ iJ DOa;vJ Re~ D--- Com~~ Dit)2;'"J1 OR~ Rfjfnqul,ed by: Company: Date & Time: Recel~ y: l) Company : Date & Time:

r elinquished by: Company: Date & Time: Received by: Company: Date & Time:

Accuracy, Precision, and Professional Service

Page 10: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

Eurofins Eaton Analytical

Run LogRun ID: 235318 Method: 537

Sample SiteSample IdType Instrument ID Calibration FileAnalysis DateMatrix

CCL 3796119 FL 101017M537b-FL-PFC12.mdb10/10/2017 18:28OS

LRB 3796102 FL 101017M537b-FL-PFC12.mdb10/10/2017 19:01RW

FBL 3796103 FL 101017M537b-FL-PFC12.mdb10/10/2017 19:18RW

CCM 3796121 FL 101017M537b-FL-PFC12.mdb10/10/2017 22:39OS

FS 3793429 PEF36857 Well A FL 101017M537b-FL-PFC12.mdb10/11/2017 00:53DW

FD 3796105 PEF36857 Well A FL 101017M537b-FL-PFC12.mdb10/11/2017 01:10DW

FS 3793430 PEF36858 Well A Dup. FL 101017M537b-FL-PFC12.mdb10/11/2017 01:27DW

CCH 3796122 FL 101017M537b-FL-PFC12.mdb10/11/2017 02:34OS

0.00

Page 1 of 5 EEA Run ID 235318 / EEA Report # 399812

Page 8 of 21

=::: e u rof i n s I Eaton Analytical

Page 11: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

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N/A

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0ng/L

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3796119

---

---

---

50 -

150

100

1807790

09/2

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017 1

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8

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104

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3796119

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---

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70 -

130

97

100

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110/1

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017 1

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8

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SS

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2537

N/A

CC

L50.1

889

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3796119

---

---

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130

100

50.0

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8

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Perf

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nesu

lfonic

aci

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2.0

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892

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3796119

---

---

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50 -

150

104

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8

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2.0

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102

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2.0

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321

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3796119

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107

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aci

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106

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3796119

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102

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2.0

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3796119

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3796119

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53796102

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104

1807790

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50 -

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105

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---

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93

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---

---

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50 -

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106

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2537

N/A

FB

L95.4

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3796103

---

---

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70 -

130

95

100

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L49.0

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---

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98

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Page 9 of 21

~ ~ ~

D D D D

□□□□--□□--□--□ □--□ □--□--□□--□--□

Page 12: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

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3796103

---

---

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0ng/L

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3796121

---

---

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50 -

150

100

1863950

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344

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---

---

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70 -

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99

100

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luoro

undeca

noic

aci

d (

PF

UnA

)537

2.0

FS

2.0

ng/L

0.9

3793430

PE

F36858 W

ell

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up.

---

---

---

---

<

10/1

0/2

017 0

8:0

010/1

1/2

017 0

1:2

7

Tru

e

IS-P

FO

A-1

3C

2537

N/A

CC

H1744740.0

0ng/L

1.0

3796122

---

---

---

50 -

150

100

1744740

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

IS-P

FO

S-1

3C

4537

N/A

CC

H306487.0

0ng/L

1.0

3796122

---

---

---

50 -

150

100

306487

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

SS

-PF

DA

-13C

2537

N/A

CC

H97.8

339

ng/L

1.0

3796122

---

---

---

70 -

130

98

100

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

SS

-PF

HxA

-13C

2537

N/A

CC

H50.3

025

ng/L

1.0

3796122

---

---

---

70 -

130

101

50.0

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

Perf

luoro

buta

nesu

lfonic

aci

d (

PF

BS

)537

2.0

CC

H196.8

460

ng/L

1.0

3796122

---

---

---

70 -

130

98

200

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

Perf

luoro

deca

noic

aci

d (

PF

DA

)537

2.0

CC

H196.3

350

ng/L

1.0

3796122

---

---

---

70 -

130

98

200

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

Perf

luoro

hepta

noic

aci

d (

PF

HpA

)537

2.0

CC

H203.4

180

ng/L

1.0

3796122

---

---

---

70 -

130

102

200

09/2

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017 1

4:3

110/1

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017 0

2:3

4

Tru

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luoro

hexa

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lfonic

aci

d (

PF

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2.0

CC

H201.6

560

ng/L

1.0

3796122

---

---

---

70 -

130

101

200

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

Perf

luoro

hexa

noic

aci

d (

PF

HxA

)537

2.0

CC

H203.1

960

ng/L

1.0

3796122

---

---

---

70 -

130

102

200

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

Perf

luoro

lauric

aci

d (

PF

DoA

)537

2.0

CC

H198.3

530

ng/L

1.0

3796122

---

---

---

70 -

130

99

200

09/2

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017 1

4:3

110/1

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017 0

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Page 11 of 21

D ~

□ DJ D D D

JJDI

JJD

_ DJ __ DD_ -□--□ DODD □□□□--□□--□--□ □--

Page 14: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

Sam

ple

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aci

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2.0

CC

H203.8

160

ng/L

1.0

3796122

---

---

---

70 -

130

102

200

09/2

7/2

017 1

4:3

110/1

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017 0

2:3

4

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aci

d (

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)537

2.0

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H201.6

340

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1.0

3796122

---

---

---

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200

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017 1

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2.0

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H200.5

660

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---

---

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017 1

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110/1

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aci

d (

PF

OA

)537

2.0

CC

H201.7

170

ng/L

1.0

3796122

---

---

---

70 -

130

101

200

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

Perf

luoro

trid

eca

noic

aci

d (

PF

TrD

A)

537

2.0

CC

H200.9

130

ng/L

1.0

3796122

---

---

---

70 -

130

100

200

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

Tru

e

Perf

luoro

undeca

noic

aci

d (

PF

UnA

)537

2.0

CC

H198.8

460

ng/L

1.0

3796122

---

---

---

70 -

130

99

200

09/2

7/2

017 1

4:3

110/1

1/2

017 0

2:3

4

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Page 12 of 21

D

□ DJ

JJDI

JJD

- DJ - - DD -

Page 15: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

Eurofins Eaton Analytical

Run LogRun ID: 235533 Method: 537

Sample SiteSample IdType Instrument ID Calibration FileAnalysis DateMatrix

CCL 3796835 FL 101117M537b-FL-PFC12.mdb10/11/2017 19:03OS

UQCSM 3796834 FL 101117M537b-FL-PFC12.mdb10/11/2017 19:20OS

LRB 3796817 FL 101117M537b-FL-PFC12.mdb10/11/2017 19:37RW

FBM 3796818 FL 101117M537b-FL-PFC12.mdb10/11/2017 20:11RW

0.00

Page 1 of 3 EEA Run ID 235533 / EEA Report # 399812

Page 13 of 21

=::: e u rof i n s I Eaton Analytical

Page 16: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

QC

Su

mm

ary

Re

po

rt

EE

A

ID #

RP

DU

nit

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arg

et

Am

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nt

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%

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very

Resu

lt

Fla

g

MR

LE

xtr

acte

dA

naly

zed

Tru

e

IS-P

FO

A-1

3C

2537

N/A

CC

L1765390.0

0ng/L

1.0

3796835

---

---

---

50 -

150

100

1765390

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

IS-P

FO

S-1

3C

4537

N/A

CC

L313002.0

0ng/L

1.0

3796835

---

---

---

50 -

150

100

313002

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

SS

-PF

DA

-13C

2537

N/A

CC

L95.5

705

ng/L

1.0

3796835

---

---

---

70 -

130

96

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

SS

-PF

HxA

-13C

2537

N/A

CC

L48.9

792

ng/L

1.0

3796835

---

---

---

70 -

130

98

50.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

buta

nesu

lfonic

aci

d (

PF

BS

)537

2.0

CC

L2.0

286

ng/L

1.0

3796835

---

---

---

50 -

150

101

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

deca

noic

aci

d (

PF

DA

)537

2.0

CC

L2.0

933

ng/L

1.0

3796835

---

---

---

50 -

150

105

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

hepta

noic

aci

d (

PF

HpA

)537

2.0

CC

L2.0

415

ng/L

1.0

3796835

---

---

---

50 -

150

102

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

hexa

nesu

lfonic

aci

d (

PF

HxS

)537

2.0

CC

L1.9

971

ng/L

1.0

3796835

---

---

---

50 -

150

100

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

hexa

noic

aci

d (

PF

HxA

)537

2.0

CC

L2.1

359

ng/L

1.0

3796835

---

---

---

50 -

150

107

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

lauric

aci

d (

PF

DoA

)537

2.0

CC

L2.1

000

ng/L

1.0

3796835

---

---

---

50 -

150

105

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

myr

istic

aci

d (

PF

TA

)537

2.0

CC

L2.0

378

ng/L

1.0

3796835

---

---

---

50 -

150

102

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

nonanoic

aci

d (

PF

NA

)537

2.0

CC

L2.0

415

ng/L

1.0

3796835

---

---

---

50 -

150

102

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

oct

ane s

ulfo

nate

(P

FO

S)

537

2.0

CC

L2.0

850

ng/L

1.0

3796835

---

---

---

50 -

150

104

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

oct

anoic

aci

d (

PF

OA

)537

2.0

CC

L2.0

989

ng/L

1.0

3796835

---

---

---

50 -

150

105

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

trid

eca

noic

aci

d (

PF

TrD

A)

537

2.0

CC

L2.0

233

ng/L

1.0

3796835

---

---

---

50 -

150

101

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Tru

e

Perf

luoro

undeca

noic

aci

d (

PF

UnA

)537

2.0

CC

L2.0

212

ng/L

1.0

3796835

---

---

---

50 -

150

101

2.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:0

3

Fals

e

IS-P

FO

A-1

3C

2537

N/A

UQ

CS

M1711970.0

0ng/L

1.0

3796834

---

---

---

50 -

150

97

1765390

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

IS-P

FO

S-1

3C

4537

N/A

UQ

CS

M305262.0

0ng/L

1.0

3796834

---

---

---

50 -

150

98

313002

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

SS

-PF

DA

-13C

2537

N/A

UQ

CS

M99.7

112

ng/L

1.0

3796834

---

---

---

70 -

130

100

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

SS

-PF

HxA

-13C

2537

N/A

UQ

CS

M50.5

456

ng/L

1.0

3796834

---

---

---

70 -

130

101

50.0

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

buta

nesu

lfonic

aci

d (

PF

BS

)537

2.0

UQ

CS

M95.1

907

ng/L

1.0

3796834

---

---

---

70 -

130

95

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

deca

noic

aci

d (

PF

DA

)537

2.0

UQ

CS

M84.4

468

ng/L

1.0

3796834

---

---

---

70 -

130

84

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

hepta

noic

aci

d (

PF

HpA

)537

2.0

UQ

CS

M91.4

448

ng/L

1.0

3796834

---

---

---

70 -

130

91

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

hexa

nesu

lfonic

aci

d (

PF

HxS

)537

2.0

UQ

CS

M92.8

937

ng/L

1.0

3796834

---

---

---

70 -

130

93

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

hexa

noic

aci

d (

PF

HxA

)537

2.0

UQ

CS

M94.3

009

ng/L

1.0

3796834

---

---

---

70 -

130

94

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

lauric

aci

d (

PF

DoA

)537

2.0

UQ

CS

M94.9

277

ng/L

1.0

3796834

---

---

---

70 -

130

95

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

myr

istic

aci

d (

PF

TA

)537

2.0

UQ

CS

M94.8

577

ng/L

1.0

3796834

---

---

---

70 -

130

95

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

nonanoic

aci

d (

PF

NA

)537

2.0

UQ

CS

M96.8

010

ng/L

1.0

3796834

---

---

---

70 -

130

97

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

oct

ane s

ulfo

nate

(P

FO

S)

537

2.0

UQ

CS

M92.4

556

ng/L

1.0

3796834

---

---

---

70 -

130

92

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

oct

anoic

aci

d (

PF

OA

)537

2.0

UQ

CS

M93.8

446

ng/L

1.0

3796834

---

---

---

70 -

130

94

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

trid

eca

noic

aci

d (

PF

TrD

A)

537

2.0

UQ

CS

M95.7

611

ng/L

1.0

3796834

---

---

---

70 -

130

96

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Fals

e

Perf

luoro

undeca

noic

aci

d (

PF

UnA

)537

2.0

UQ

CS

M92.8

426

ng/L

1.0

3796834

---

---

---

70 -

130

93

100

10/1

1/2

017 1

2:4

010/1

1/2

017 1

9:2

0

Tru

e

IS-P

FO

A-1

3C

2537

N/A

LR

B1747310.0

0ng/L

1.0

3796817

---

---

---

50 -

150

99

1765390

10/1

1/2

017 0

8:2

010/1

1/2

017 1

9:3

7

Tru

e

IS-P

FO

S-1

3C

4537

N/A

LR

B316177.0

0ng/L

1.0

3796817

---

---

---

50 -

150

101

313002

10/1

1/2

017 0

8:2

010/1

1/2

017 1

9:3

7

Tru

e

SS

-PF

DA

-13C

2537

N/A

LR

B94.0

317

ng/L

1.0

3796817

---

---

---

70 -

130

94

100

10/1

1/2

017 0

8:2

010/1

1/2

017 1

9:3

7

Tru

e

SS

-PF

HxA

-13C

2537

N/A

LR

B47.8

147

ng/L

1.0

3796817

---

---

---

70 -

130

96

50.0

10/1

1/2

017 0

8:2

010/1

1/2

017 1

9:3

7

Tru

e

Perf

luoro

buta

nesu

lfonic

aci

d (

PF

BS

)537

2.0

LR

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Page 14 of 21

~

D DJ D DJ

□--□--□□--□--□ DODD □□□□--□□--□

Page 17: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

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Page 15 of 21

D

□ DJ

JJDI

JJD

_ DJ __ DD_ -□--□ DODD DOD

Page 18: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

Eurofins Eaton Analytical

Run LogRun ID: 235682 Method: 537

Sample SiteSample IdType Instrument ID Calibration FileAnalysis DateMatrix

CCL 3804256 FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 19:34OS

LRB 3804246 FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 20:08RW

FBM 3804247 FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 20:41RW

FTB 3793431 PEF36859 FTB FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 20:58RW

LTB 3793432 PEF36860 LTB-09/13/17 FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 21:15RW

CCM 3804257 FL 102017M537b-FL-PFC-Ext.mdb10/21/2017 00:53OS

0.00

Page 1 of 4 EEA Run ID 235682 / EEA Report # 399812

Page 16 of 21

=::: e u rof i n s I Eaton Analytical

Page 19: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

QC

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CC

L783896.0

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50 -

150

100

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3804246

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---

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---

---

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70 -

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---

---

---

70 -

130

90

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Page 17 of 21

~ ~

D D D DJ

□□□□--□□--□--□ □--□ □--□--□□--□--□

Page 20: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

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12

Page 18 of 21

~ l R DD D D DJ D

JODI

JD□

-□□--□□- -□--□ DODD □--□--□□--□--□ DOD

Page 21: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

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0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

-70 -

130

105

100

10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

SS

-PF

HxA

-13C

2537

N/A

LT

B44.5

144

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

-70 -

130

99

50.0

10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

buta

nesu

lfonic

aci

d (

PF

BS

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

deca

noic

aci

d (

PF

DA

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

hepta

noic

aci

d (

PF

HpA

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

hexa

nesu

lfonic

aci

d (

PF

HxS

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

hexa

noic

aci

d (

PF

HxA

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

lauric

aci

d (

PF

DoA

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

myr

istic

aci

d (

PF

TA

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

nonanoic

aci

d (

PF

NA

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

oct

ane s

ulfo

nate

(P

FO

S)

537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

oct

anoic

aci

d (

PF

OA

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

trid

eca

noic

aci

d (

PF

TrD

A)

537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Fals

e

Perf

luoro

undeca

noic

aci

d (

PF

UnA

)537

2.0

LT

B2.0

ng/L

0.9

3793432

PE

F36860 L

TB

-09/1

3/1

7--

---

---

---

-

<10/1

1/2

017 0

8:2

010/2

0/2

017 2

1:1

5

Tru

e

IS-N

MeF

OS

AA

-d3

537

N/A

CC

M818341.0

0ng/L

1.0

3804257

---

---

---

50 -

150

100

818341

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

IS-P

FO

A-1

3C

2537

N/A

CC

M1768840.0

0ng/L

1.0

3804257

---

---

---

50 -

150

100

1768840

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

IS-P

FO

S-1

3C

4537

N/A

CC

M313944.0

0ng/L

1.0

3804257

---

---

---

50 -

150

100

313944

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

IS-G

enX

-13C

3537

N/A

CC

M7563.0

4ng/L

1.0

3804257

---

---

---

50 -

150

100

7563.0

4

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

SS

-NE

tFO

SA

A-d

5537

N/A

CC

M201.8

620

ng/L

1.0

3804257

---

---

---

70 -

130

101

200

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

SS

-PF

DA

-13C

2537

N/A

CC

M98.3

485

ng/L

1.0

3804257

---

---

---

70 -

130

98

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

SS

-PF

HxA

-13C

2537

N/A

CC

M48.6

021

ng/L

1.0

3804257

---

---

---

70 -

130

97

50.0

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

buta

nesu

lfonic

aci

d (

PF

BS

)537

2.0

CC

M97.6

198

ng/L

1.0

3804257

---

---

---

70 -

130

98

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

deca

noic

aci

d (

PF

DA

)537

2.0

CC

M97.8

170

ng/L

1.0

3804257

---

---

---

70 -

130

98

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

hepta

noic

aci

d (

PF

HpA

)537

2.0

CC

M96.5

528

ng/L

1.0

3804257

---

---

---

70 -

130

97

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

hexa

nesu

lfonic

aci

d (

PF

HxS

)537

2.0

CC

M97.5

045

ng/L

1.0

3804257

---

---

---

70 -

130

98

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

hexa

noic

aci

d (

PF

HxA

)537

2.0

CC

M96.6

162

ng/L

1.0

3804257

---

---

---

70 -

130

97

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

lauric

aci

d (

PF

DoA

)537

2.0

CC

M96.2

915

ng/L

1.0

3804257

---

---

---

70 -

130

96

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

myr

istic

aci

d (

PF

TA

)537

2.0

CC

M98.5

777

ng/L

1.0

3804257

---

---

---

70 -

130

99

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

nonanoic

aci

d (

PF

NA

)537

2.0

CC

M99.4

858

ng/L

1.0

3804257

---

---

---

70 -

130

99

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

oct

ane s

ulfo

nate

(P

FO

S)

537

2.0

CC

M98.1

474

ng/L

1.0

3804257

---

---

---

70 -

130

98

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

oct

anoic

aci

d (

PF

OA

)537

2.0

CC

M98.4

584

ng/L

1.0

3804257

---

---

---

70 -

130

98

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

trid

eca

noic

aci

d (

PF

TrD

A)

537

2.0

CC

M99.0

507

ng/L

1.0

3804257

---

---

---

70 -

130

99

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

3

Tru

e

Perf

luoro

undeca

noic

aci

d (

PF

UnA

)537

2.0

CC

M97.6

129

ng/L

1.0

3804257

---

---

---

70 -

130

98

100

10/2

0/2

017 1

4:1

310/2

1/2

017 0

0:5

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Page 19 of 21

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-□□--□□- -□--□ □--□ □--□--□□--□-

Page 22: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

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Page 20 of 21

Page 23: PEJ36l~'1 P£F36~t0 · w P£F36~t0 2 X Sample Condition: D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal: Sub Lab Temoerature

END OF REPORT

Page 21 of 21