phase ii environmental assessment
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P. O. Box 295
2561 Stouffville Road, Suite 202
Gormley, Ontario
L0H 1G0
Telephone (905) 887-6661
BARENCO INC.
Phase IIEnvironmental Assessment
Thirteen Properties, High Park Project
Toronto, Ontario
March 5, 2008
Daniels HR Corporation20 Queen Street West
Suite 3400
Toronto, Ontario
M5H 3R3
For
07126
ENVIRONMENTAL ENGINEERING AND SITE REMEDIATION SERVICES
.
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any decision made or any action taken based on this report or the work referredto in this report.
The investigation undertaken by Barenco Inc. with respect to this report andany conclusions or recommendations made in this report reflect Barenco Inc.'sjudgement based on the site conditions observed at the time of the siteinspection on the date(s) set out in this report and on information available atthe time of preparation of this report. This report has been prepared for specificapplication to this site and it is based, in part, upon visual observatiou of, thesite, subsurface investigation at discrete locations and depths, and specificanalysis of specific chemical parameters and materials during a specific timeinterval, all as described in this report. Unless otherwise stated, the findingscannot be extended to previous or future site conditions, portions of the sitewhich were unavailable for direct investigation, subsurface locations whichwere not investigated directly, or chemical parameters, materials or analysiswhich were not addressed. Substances other than those addressed by theinvestigation described in this report may exist within the site, substancesaddressed by the investigation may exist in areas of the site not investigated andconcentrations of substances addressed which are different than those reportedmay exist in areas other than the locations from which the samples were taken.
If site conditions or applicable standards change or if any additional informationbecomes available at a future date, modifications to the findings, conclusionsand recommendations in this report may be necessary.
Other than by Daniels HR Corporation, copying or distribution of this report orthe use of or reliance on the information contained herein, in whole or in part, isnot permitted without the express written permission of Barenco Inc. Nothingin this report is intended to constitute or provide a legal opinion.
Respectfully submitted,BARENCO INC.
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/I Jim Phimister, P .Eng, !.. '-
Principal, Hydrogeologist
March 5, 20088
Phase II Environmental AssessmentThirteen Properties, High Park Project, Toronto, Ontario
FIGURES
SITE
SITE
SITE
SITE
1FIGURE
SCALE: NOTES:
SOURCE:
DRAWN BY
07126-LOCALITY
C.D. V.K.
CHECKED BY
BARENCO JOB #: 07126 DATE: DECEMBER 2007
N
THIRTEEN PROPERTIES,HIGH PARK PROJECTTORONTO, ONTARIO
1:25000
LOCALITY PLAN
MAPART PUBLISHING 2005
SITE
SITE
SITE
SITE
SITE
2FIGURE
SCALE: SOURCE:
DRAWN BY
07126-SITE PLAN1-JAN08
M.A. B.C.
CHECKED BY
BARENCO JOB #: 07126 DATE: JANUARY 2008
N
THIRTEEN PROPERTIES,HIGH PARK PROJECTTORONTO, ONTARIO
SITE PLANCITY OF TORONTO PLANFIELD OBSERVATIONS BYBARENCO STAFF
SITE
0 20m
( APPROXIMATE)
10TEST HOLE WITHMONITOR DRILLEDIN JANUARY 2008
TEST HOLE DRILLED IN DECEMBER 2007
LEGEND:
BLOOR STREET WEST
PA
CIF
IC A
VE
NU
E
OA
KM
OU
NT
RO
AD
8
6
10
12
14
184418461848185018521854
35
37
GARAGE
SHED
TH106
TH101
TH104
TH105
TH102
TH103
FORMER USTEXCAVATION
TH3
TABLES
Table 1
SITE ENVIRONMENTAL SETTING DATA
Site Location: Thirteen Properties, High Park Project, Toronto, Ontario Date: January 24, 2008
NATIVE SOIL
Silty sandType:(select range)Hydraulic Conductivity
> 10-3 cm/s: Estimated to be 10-5 cm/s<10-3 to >10-6 cm/s:
< 10-6 cm/s: Estimated to be less than 50% Soil Particles < 75 Microns:
GROUND WATER
Approximately 15.6 to 15.9 metres below gradeDepth to Water Table: Measured from onsite monitorsEstimated or Measured: SouthDirection of Flow: Estimated based on topographyEstimated or Measured:
MUNICIPAL SERVICES
YesPiped Water: NoGround Water Source: NADistance to Well: Yes - Lake OntarioSurface Water Source: YesSanitary Sewer: YesStorm Sewer:
PRIVATE SERVICES
NADistance to Nearest Well: NAApproximate Depth of Well: NoPrivate Sanitary Sewage:
SURFACE WATER
Lake OntarioName of water body: Approximately 2 kilometres to the southDistance from site: UnknownElevation drop from site: NoDirect Drainage from site:
07126 BARENCO INC.
Table 2
DARCY'S LAW CALCULATIONS
Site Location: Thirteen Properties, High Park Project, Toronto, Ontario Date: January 24, 2008 v=ki/n
1.00E-07Permeability k (m/sec) =1.00E-05(cm/sec) =
0.010Gradient i (m/m) =2.50E-09Velocity v (m/sec) =0.4Porosity* n =8.20E-09(feet/sec) =7.08E-04(feet/day) =
0.259(feet/year) =0.079(metres/year) = * (from Freeze & Cherry, 1979)
Hydraulic conductivity for silty sandbased on published valuesGradient estimated based on slope of land
07126 BARENCO INC.
Table 3
SOIL CHEMICAL ANALYSIS - Petroleum Parameters Thirteen Properties, High Park Project, Toronto, Ontario
Page 1 of 2Test HoleTest HoleTest HoleTest HoleTest HoleTest HoleSampleTH103-17TH103-8TH102-15TH102-14TH101-15TH101-13
MOE15.8 to 16.59.0 to 9.615.2 to 15.814.5 to 15.115.2 to 15.813.7 to 14.3Depth (m)Table 3Silty sandSilty sandSilty sandSilty sandSilty sandSilty sandRDL*Soil Type
Soil1/17/20081/17/20081/17/20081/17/20081/16/20081/16/2008Sample DateStandards**W85486W85485W85484W85483W80998W80997Maxxam I.D.
100 ppm425 ppm25 ppm25 ppm150 ppm175 ppmField Vapour Reading
5.3ndndndndndnd0.02Benzene
34ndndndndndnd0.02Toluene
290ndndndndndnd0.02Ethylbenzene
34nd1.48ndndnd0.620.04Xylenes
30nd220ndndnd9210F1 (C6 to C10 - BTEX)No valuend6.7ndnd<0.1370.2Aliphatic >C6 to C8No valuend170ndnd<0.414000.7Aliphatic >C8 to C10No valuend16ndnd<0.22000.1Aromatics >C8 to C10
150161900ndndnd290010F2 (C10 to C16)No valuena563nanana24605Aliphatic >C10 to C12No valuena54nanana925Aromatic >C10 to C12No valuena1800nanana757010Aliphatic >C12 to C16No valuena208nanana52515Aromatic >C12 to C16
400161400ndndnd220010F3 (C16 to C34)No valuena1320nanana608010Aliphatic >C16 to C21No valuena252nanana76210Aromatic >C16 to C21No valuena141nananand10Aliphatic >C21 to <C34No valuena161nanana35510Aromatic >C21 to <C34
2800ndndndndndnd10F4 (C34 to C50)No valuenandnananand10Aliphatic >C34No valuena58nanana4110Aromatic >C34
***7.917.897.787.967.967.80-pH
Analysis by Maxxam Analytics Inc. All results in ppm (ug/g) and based on dry weight basis; nd means "not detected" at reporting detection limit (RDL). na means "not applicable". * Analytical RDLs are shown except as indicated in brackets. ** Standards shown are for residential land use and coarse textured soils. *** pH range 5.0 to 9.0 for soil depths less than 1.5 m; pH range 5.0 to 11.0 for soil depths greater than 1.5 m Exceedances of Table 3 Standards are shown in bold.
07126 BARENCO INC.
Table 3
SOIL CHEMICAL ANALYSIS - Petroleum Parameters Thirteen Properties, High Park Project, Toronto, Ontario
Page 2 of 2Test HoleTest HoleTest HoleTest HoleTest HoleTest HoleSampleTH106-15TH106-14TH105-15TH105-14TH104-14TH104-12
MOE16.0 to 16.615.2 to 15.816.0 to 16.615.2 to 15.815.2 to 15.813.7 to 14.3Depth (m)Table 3Silty sandSilty sandSilty sandSilty sandSilty sandSilty sandRDL*Soil Type
Soil1/21/20081/21/20081/21/20081/21/20081/18/20081/18/2008Sample DateStandards**W837394W837393W837392W837391W85489W85488Maxxam I.D.
50 ppm50 ppm100 ppm100 ppm50 ppm50 ppmField Vapour Reading
5.3ndndndndndnd0.02Benzene
34ndndndndndnd0.02Toluene
290ndndndndndnd0.02Ethylbenzene
34ndndndndndnd0.04Xylenes
30ndndndndndnd10F1 (C6 to C10 - BTEX)No valuendndndndndnd0.2Aliphatic >C6 to C8No valuendndndndndnd0.7Aliphatic >C8 to C10No valuendndndndndnd0.1Aromatics >C8 to C10
150ndndndndnd1210F2 (C10 to C16)No valuenananananana5Aliphatic >C10 to C12No valuenananananana5Aromatic >C10 to C12No valuenananananana10Aliphatic >C12 to C16No valuenananananana15Aromatic >C12 to C16
400ndndndndnd1210F3 (C16 to C34)No valuenananananana10Aliphatic >C16 to C21No valuenananananana10Aromatic >C16 to C21No valuenananananana10Aliphatic >C21 to <C34No valuenananananana10Aromatic >C21 to <C34
2800ndndndndndnd10F4 (C34 to C50)No valuenananananana10Aliphatic >C34No valuenananananana10Aromatic >C34
***7.958.028.027.947.957.91-pH
Analysis by Maxxam Analytics Inc. All results in ppm (ug/g) and based on dry weight basis; nd means "not detected" at reporting detection limit (RDL). na means "not applicable". * Analytical RDLs are shown except as indicated in brackets. ** Standards shown are for residential land use and coarse textured soils. *** pH range 5.0 to 9.0 for soil depths less than 1.5 m; pH range 5.0 to 11.0 for soil depths greater than 1.5 m Exceedances of Table 3 Standards are shown in bold.
07126 BARENCO INC.
Table 4
SOIL CHEMICAL ANALYSIS - Polycyclic Aromatic Hydrocarbons Thirteen Properties, High Park Project, Toronto, Ontario
Page 1 of 1Test HoleTest HoleTest HoleSample
OntarioTH105-2TH104-2TH101-15Regulation 153/040.8 to 1.40.8 to 1.415.2 to 15.8Depth (m)
Table 3Silty sandSilty sandSilty sandRDL*Soil TypeSoil1/21/20081/18/20081/16/2008Sample Date
Standards**W87390W85487W80998Maxxam I.D.
1000ndndnd0.01Acenaphthene100ndndnd0.005Acenaphthylene28ndndnd0.005Anthracene40ndndnd0.01Benzo(a)anthracene1.2ndndnd0.005Benzo(a)pyrene12ndndnd0.005Benzo(b/j)fluoranthene40ndndnd0.02Benzo(g,h,i)perylene12ndndnd0.01Benzo(k)fluoranthene12ndndnd0.01Chrysene1.2ndndnd0.02Dibenzo(a,h)anthracene40ndndnd0.005Fluoranthene
350ndndnd0.005Fluorene12ndndnd0.02Indeno(1,2,3-cd)pyrene
280ndndnd0.0051-Methylnaphthalene280ndndnd0.0052-Methylnaphthalene40ndndnd0.005Naphthalene40ndndnd0.005Phenanthrene
250ndndnd0.005Pyrene***7.477.237.96-pH
Analysis by Maxxam Analytics Inc. All results in ppm (ug/g) and based on dry weight basis; nd means "not detected" at reporting detection limit (RDL). * Analytical RDLs are shown except as indicated in brackets. ** Standards shown are for residential land use and coarse textured soils. *** pH range 5.0 to 9.0 for soil depths less than 1.5 m; pH range 5.0 to 11.0 for soil depths greater than 1.5 m Exceedances of Table 3 Standards are shown in bold.
07126 BARENCO INC.
Table 5
GROUND WATER CHEMICAL ANALYSIS - Petroleum Parameters Thirteen Properties, High Park Project, Toronto, Ontario
Page 1 of 1MOEMonitorMonitorMonitorMonitorMonitorMonitor
Table 3TH106TH105TH104TH103TH102TH101SampleGround Water1/24/20081/24/20081/24/20081/24/20081/24/20081/24/2008RDL*Sample DateStandards**W93620W93619W93618W93617W93616W93615Maxxam I.D.
1900ndndndndndnd0.2Benzene
5900ndndndndndnd0.2Toluene
28000ndndndndndnd0.2Ethylbenzene
5600ndndndndnd1.00.4Xylenes
No valuendndndndndnd100F1 (C6 to C10 - BTEX)No valuendndndndndnd0.01Aliphatic >C6 to C8No valuendndnd0.01nd0.010.01Aliphatic >C8 to C10No valuendndndndndnd0.01Aromatics >C8 to C10
No valuend120ndndnd130100F2 (C10 to C16)No value0.03ndnd0.07nd0.450.01Aliphatic >C10 to C12No value0.03nd0.010.01nd0.150.01Aromatic >C10 to C12No value0.30ndnd0.15nd1.20.05Aliphatic >C12 to C16No value0.33ndnd0.05nd0.500.05Aromatic >C12 to C16
No valuend310ndndnd130100F3 (C16 to C34)No value0.36ndnd0.18nd1.20.05Aliphatic >C16 to C21No value0.33nd0.170.140.060.640.05Aromatic >C16 to C21No value0.1ndndndnd0.20.1Aliphatic >C21 to C32No value0.1nd0.1ndnd0.30.1Aromatic >C21 to C32
No valuendndndndndnd100F4 (C34 to C50)
Analysis by Maxxam Analytics Inc. All results in ppb (ug/L); nd means "not detected" at reporting detection limit (RDL). na means "not analysed". n/a means "not applicable". * Analytical RDLs are shown except as indicated in brackets. ** Standards shown are for residential land use and coarse textured soils. Exceedances of Table 3 Standards are shown in bold.
07126 BARENCO INC.
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PAGE 05/05DANIELS GRP0:1}10/2008 11:58 4169790415
4January 7, 2008Proposal - Phase II Environmental A~~~ssmentThirteen Pr Ontario
attachment: Terms and Cqnditions
Barenco U}c. to proceed with the work.
"tOocg"j'A,.j \0Date
Page 1
Terms and Conditions
1. SERVICES TO BE PROVIDED AND STANDARD OF CARE. Barenco Inc. ("Barenco") agrees to provide Client for its sole benefitand exclusive use, services set forth in Barenco's Proposal. Barenco's offer to perform shall be terminated if not accepted within sixty(60) days of the date of the Proposal. Barenco's services shall be performed in accordance with the standard of care of its professionwhich means generally accepted professional practices, related to the nature of the work accomplished, at the time and place theservices are performed. Subject to this standard of care, Barenco makes no express or implied warranties regarding its services exceptas otherwise expressly stated herein and all other representations and warranties, express or implied, are hereby expressly excluded.Both parties agree that no third-party beneficiaries are intended by this Agreement. 2. PAYMENT. Invoices will be submitted once a month for services performed during the prior month, or upon completion of the work,whichever is earlier. Payment terms are due upon receipt. Interest will be added to accounts thirty (30) days in arrears at the rate oftwo per cent (2%) of the arrears for each month of delinquency, not to exceed the maximum percentage rate allowed by law. In addition,Barenco may, after giving seven (7) days written notice, suspend services under this or any other Agreement with Client without liabilityuntil all past due accounts (including fees and accrued interest) have been paid. Timely payment is an essential requirement of Client'sperformance of any Agreement between Barenco and Client. All expenses incurred by Barenco for liening or collecting any delinquentamount including, without limitation, legal and other third-party fees and filing fees, shall be paid to Barenco by Client.3. RIGHT OF ENTRY AND PROPERTY RESPONSIBILITY. Client has responsibility for obtaining a right of entry to the property whichis the subject of the services. The right of entry shall allow Barenco, its agents, subcontractors and employees to enter the property,including buildings if required to complete the services as proposed, from time to time, as necessary to perform the agreed services.Barenco has responsibility for its own activities on the property including the safety of its employees; it does not assume control of norresponsibility for the property, the person in charge of the property, nor the safety of persons not in Barenco's employ. 4. INSURANCE. Barenco maintains Workers' Compensation insurance for its employees as required by provincial law. In addition,Barenco maintains the following insurance policies: Commercial General Liability, Pollution Liability and Professional Liability($1,000,000) each occurrence, $1,000,000 Policy Aggregate) and Automobile Third Party Liability ($2,000,000).5. DOCUMENTS. Barenco will furnish Client the agreed upon number of written reports and supporting documents. All such reportsand documents are furnished for Client's exclusive internal use and reliance, use of Client's counsel, and for regulatory submission asexpressly contemplated in connection with the services provided for in the Agreement, but not for advertising or other type of distribution,and are subject to the following: All documents generated by Barenco under this Agreement shall remain the sole property of Barenco.Any unauthorized use or distribution of Barenco's work shall be at Client's and recipient's sole risk and without liability to Barenco.Barenco retains a confidential file copy of its work product and related documents. If Client desires to release, or for Barenco to provide,its report to a third party, which is not entitled to receive or use the reports and documents as set out above, for that third party'sreliance, Barenco will agree to such release provided it receives written acceptance from such third party to be bound by acceptableterms and conditions similar to this Agreement, and provided payment by such third party of Barenco's standard fee. Reports providedfor disclosure of information only will not require separate agreement. Client acknowledges and agrees to inform such third party thatBarenco's report reflects conditions only at the time of the report and may not reflect conditions at a later time. Client furtheracknowledges that such request for release creates a potential conflict of interest for Barenco and by making any such request Clientwaives any such claim if Barenco complies with the request. Client agrees that all documents furnished to Client or Client's agent ordesignees, if not paid for, will be returned upon demand and will not be used by Client or any other person or entity for any purposewhatsoever. Client further agrees that documents produced by Barenco pursuant to this Agreement will not be used for any purposenot expressly provided for in this Agreement without Barenco's prior written approval. Client shall furnish documents or other informationreasonably within Client's control and deemed necessary by Barenco for proper performance of its services. Barenco may rely, withoutindependent investigation or enquiry, upon Client-provided documents in performing the services required under this Agreement;however, Barenco assumes no responsibility or liability for their accuracy. Client-provided documents will remain the property of Clientbut Barenco may retain one confidential file copy as needed to support its report. 6. CONFIDENTIALITY. Barenco will maintain as confidential any documents or information provided by Client and will not release,distribute or publish same to any third party without prior permission from Client, unless compelled by law or by order of a court orregulatory authority of competent jurisdiction. 7. INTELLECTUAL PROPERTY. All concepts, products, processes, inventions, trade-marks, works, designs and improvements to,and derivatives of, the foregoing, resulting from the services rendered by Barenco in connection with the project, or which are invented,authored, developed or first used or reduced to practise by Barenco in the performance of the services shall be and remain the propertyof Barenco. Client shall have a personal non-exclusive, royalty-free, non-assignable, non-sublicensable licence to use the IntellectualProperty in connection with the project, for the life of the project, and for no other purpose or project. Barenco does not make anyrepresentation or warranty that such Intellectual Property does not violate the rights of any other person. 8. WASTE. Client warrants that, if it knows or suspects that "waste" (within the meaning of the Ontario Environmental Protection Act)may exist on the property, it has so informed Barenco. Client also agrees that Barenco accepts no ownership of any waste and has noresponsibility as a generator of any waste found or identified at the project property. 9. LIMITATION OF LIABILITY. CLIENT EXPRESSLY AGREES THAT, TO THE FULLEST EXTENT PERMIT TED BY LAW, ITSMAXIMUM AGGREGATE RECOVERY AGAINST BARENCO, ITS DIRECTORS, EMPLOYEES, SUB-CONTRACTORS ANDREPRESENTATIVES, FOR ANY AND ALL CLAIMS BY CLIENT FOR ALL CAUSES INCLUDING, BUT NOT LIMITED TO, CLAIMSOF BREACH OF CONTRACT, BREACH OF WARRANTY AND/OR NEGLIGENCE, SHALL BE THE AMOUNT OF THE FEE PAID TOBARENCO FOR ITS PROFESSIONAL SERVICES RENDERED UNDER THE AGREEMENT WITH RESPECT TO THE PARTICULARSITE WHICH IS THE SUBJECT OF THE CLAIM BY CLIENT. PROVIDED THAT, IF THERE IS AN EVENTUAL FINALDETERMINATION BY A COURT OF COMPETENT JURISDICTION OF GROSS NEGLIGENCE OR WILLFUL MISCONDUCT BYBARENCO, THEN THE MAXIMUM AGGREGATE RECOVERY SHALL BE LIMITED AS FOLLOWS: THE GREATER OF (A) THE FEEOR (B) THE LESSER OF TWO TIMES (2x) THE FEE AND $25,000.
Page 2
Terms and Conditions (cont.)
10. INDEMNIFICATION. To the fullest extent permitted by law, Client agrees to defend, indemnify, and hold Barenco, its agents,subcontractors, and employees harmless from and against any and all claims, defence costs, including legal fees, damages and otherliabilities arising out of or in any way related to Barenco's reports or recommendations concerning this Agreement, Barenco’s presenceon the project property, or the presence, release or threatened release of contaminants on or from the project property provided thatClient shall not indemnify Barenco against liability for damages caused by or resulting from the sole negligence of Barenco, its agents,subcontractors or employees or against penalties or fines resulting from violations by Barenco of its own Certificates of Approval; andprovided further that Client shall indemnify Barenco against liability for damages caused by or resulting from the concurrent orcontributory negligence of (a) Client, its agents, or employees and (b) Barenco, its agents, subcontractors, or employees, only to theextent of Client's negligence or the negligence of Client's agents or subcontractors. Provided further that Barenco's obligation hereundershall not extend to indemnification or holding harmless for any claims of loss of profits or any other indirect, special, incidental, orconsequential damages of any nature whatsoever. 11. UNFORESEEN OCCURRENCES. If any unforeseen conditions or occurrences are encountered which, in Barenco's judgement,significantly affect or may affect the original services as proposed, then Barenco will promptly notify Client. After such notification, theparties agree that Barenco has the unilateral right to complete the original services as proposed, if appropriate, or agree with Client tomodify the Agreement, or terminate the Agreement. 12. TERMINATION AND RESTART. In the event that Client requests termination of work prior to completion or Barenco terminateswork under Paragraph 11, a final invoice will be rendered. Where the method of payment is based on time and materials, Barenco willbe paid for all work performed up to notice of termination and for all expenses incurred or committed to that cannot be cancelled. Wherethe method of payment is based on a fixed price, the final invoice will be based on the percentage of work completed by the date oftermination. Barenco also has the right to complete at client's expense the analyses and records Barenco considers necessary to protectits professional reputation. 13. WELL ABANDONMENT. Any monitoring wells installed as part of Barenco's work may later need to be abandoned in accordancewith applicable law. Unless expressly provided for in the proposal, well abandonment is not included in the work. 14. DISPOSAL OF SAMPLES. Samples not submitted for analysis will be discarded 90 days after sampling unless differentarrangements are agreed to in writing. 15. SUBSURFACE RISKS AND SITE DAMAGE. Client recognizes that special risks occur and guarantees cannot be expectedwhenever professional consulting services are applied to determine the composition of a site's subsurface or the existence or non-existence of waste materials. Barenco cannot eliminate these risks altogether, but Barenco can apply professional techniques to reducethe risks to a level deemed tolerable and Client agrees to accept that level of risk. Whenever Barenco is providing field services, Clientrecognizes that the use of exploration and test equipment may unavoidably damage or alter the property surface or subsurface. Barencowill not be responsible for personal and property damages due to its interference with subterranean structures, such as pipes, tanks,and utility lines that are not called to Barenco's attention in writing or correctly shown on plans provided by Client, or for which clearancescannot be obtained from utility owners or their agents, or which are incorrectly cleared by utility owners or their agents. 16. SEVERABILITY AND SURVIVAL. Any element of this Agreement later held to violate a law shall be deemed void, and all remainingprovisions shall continue in force. However, Client and Barenco will in good faith attempt to replace any invalid or unenforceableprovision with one that is valid and enforceable, and which comes as close as possible to expressing the intent of the original provision.All terms and conditions of this Agreement allocating liability between Client and Barenco shall survive the completion of the serviceshereunder and the termination of the Agreement. 17. DISPUTES RESOLUTION. All matters in dispute howsoever caused may with the consent of both parties be referred to arbitration.The award of the arbitrator shall be final and binding upon the parties. The provisions of the Ontario Arbitrations Act, 1991, shall apply.Alternatively, if the dispute requires litigation, (a) Client assents to exclusive jurisdiction of the courts of the Province of Ontario (b) theclaim will be brought and tried in the judicial jurisdiction where Barenco's principal place of business is located and Client waives theright to move the action to any other judicial jurisdiction and (c) the prevailing party will be entitled to recovery of all reasonable costsincurred, including staff time, court costs, legal fees and other claim-related expenses. 18. PRECEDENCE. These terms and conditions shall take precedence over any inconsistent or contradictory provisions contained inany proposal, contract, purchase order, requisition, or like document concerning Barenco's services. 19. GOVERNING LAW. This Agreement shall be governed in all respects by the laws of the Province of Ontario. 20. ENTIRE AGREEMENT. This Agreement, together with Barenco's Proposal, constitutes the entire agreement between Client andBarenco pertaining to the subject matter of this Agreement and supersedes all other agreements, understandings, negotiations anddiscussions, whether oral or written. There are no conditions, warranties, representations or other agreements between the parties inconnection with the subject matter of this Agreement (whether oral or written, express or implied, statutory or otherwise) except asspecifically set out in this Agreement. Barenco shall not be bound or deemed to be bound by any other document or instrument issuedby the Client, including without limitation, purchase orders, requisitions, or contracts unless a duly authorized officer of Barenco expressly agrees in writing to be bound by the terms of such documents or instruments, notwithstanding that documents or instruments maystate otherwise. 21. PREPARATION OF AGREEMENT. Notwithstanding any rule or maxim of law or construction to the contrary, the parties agree thatany ambiguity or uncertainty contained in this Agreement shall not be construed against Barenco merely because this Agreement wasdrafted or prepared by or on behalf of Barenco.
FORM TC1 -JANUARY 2007
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PROJECT #
TECHNICIAN
07126
D.Doherty
TEST HOLE LOG TH101DRILL DATE: January 16, 2008
SHEET#
WEATHER:
ONE of TWO
EQUIPMENT: Track Mount DrillTOP OF GROUND ELEVATION:
Overcast, -7C
GROUND WATER DEPTH: 15.59m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
1
2
3
4
5
6
7
8
9 9
8
7
6
5
4
3
2
1
Continued...
1 SS 01/02/03/02 ND 65%
0.6
2 SS 01/02/03/04 ND 75%
1.4
0.8
3 SS 10/13/13/16 25 85%PPM
2.1
1.5
4 SS 10/09/11/12 ND 90%
3.7
3.0
5 SS 10/14/20/21 ND 100%
5.2
4.6
6 SS 07/22/25/22 25 75%PPM
6.7
6.1
7 SS 08/16/20/28 ND 100%
8.2
7.6
8 SS 10/30/39/40 25 100%PPM
9.8
9.1
TOPSOIL : Dark brown, soft, TOPSOIL, moist. 0.1SILTY SAND : Light brown, loose to very dense,SAND, fine grained, becomes coarse grained at13.2m, silty, damp, wet at 15.2m, petroleum odourbetween 13.7m and 14.3m and between 15.2mand 15.9m.
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D.Doherty
TEST HOLE LOG TH101DRILL DATE: January 16, 2008
SHEET#
WEATHER:
TWO of TWO
EQUIPMENT: Track Mount DrillTOP OF GROUND ELEVATION:
Overcast, -7C
GROUND WATER DEPTH: 15.59m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
11
12
13
14
15
16
17
18
19 19
18
17
16
15
14
13
12
11
16.76 m - END OF TEST HOLE
9 SS 11/29/24/29 25 20%PPM
11.3
10.7
10 SS 10/22/34/32 ND 100%
12.0
11.4
11 SS 09/27/41/42 25 90%PPM
12.8
12.2
12 SS 08/32/37/50 ND 90%13.6
13.3
13 SS 07/16/29/24 175 90% BTEX-F1toF4-pHPPM
14.3
13.7
14 SS 05/10/17/19 ND 90%
15.1
14.5
15 SS 03/10/13/15 150 90% BTEX-F1toF4-PAHs-pHPPM
15.8
15.2
16 SS 04/15/27/32 50 100%PPM
16.6
16.0
SILTY SAND : Light brown, loose to very dense,SAND, fine grained, becomes coarse grained at13.2m, silty, damp, wet at 15.2m, petroleum odourbetween 13.7m and 14.3m and between 15.2mand 15.9m.
16.6
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D.Doherty
TEST HOLE LOG TH102DRILL DATE: January 17, 2008
SHEET#
WEATHER:
ONE of TWO
EQUIPMENT: Track Mount DrillTOP OF GROUND ELEVATION:
Overcast, -1C
GROUND WATER DEPTH: 15.56m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
1
2
3
4
5
6
7
8
9 9
8
7
6
5
4
3
2
1
Continued...
1 SS 01/02/02/02 ND 85%
0.6
2 SS 01/02/02/01 ND 85%
1.4
0.8
3 SS 02/06/07/08 25 85%PPM
2.1
1.5
4 SS 03/08/11/11 25 90%PPM
3.7
3.0
5 SS 06/11/17/12 50 90%PPM
5.2
4.6
6 SS 05/10/12/15 50 85%PPM
6.7
6.1
7 SS 07/20/27/35 ND 90%
8.2
7.6
8 SS 10/31/45/40 25 100%PPM
9.8
9.1
TOPSOIL : Dark Brown, very soft, TOPSOIL, damp.0.2
SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, damp, wet at15.2m, petroleum odour between 14.5m and15.1m.
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D.Doherty
TEST HOLE LOG TH102DRILL DATE: January 17, 2008
SHEET#
WEATHER:
TWO of TWO
EQUIPMENT: Track Mount DrillTOP OF GROUND ELEVATION:
Overcast, -1C
GROUND WATER DEPTH: 15.56m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
11
12
13
14
15
16
17
18
19 19
18
17
16
15
14
13
12
11
16.76 m - END OF TEST HOLE
9 SS 08/21/41/40 ND 100%
11.3
10.7
10 SS 08/21/28/30 25 100%PPM
12.0
11.4
11 SS 08/13/36/47 25 100%PPM
12.8
12.2
12 SS 06/12/15/17 25 90%PPM
13.6
13.0
13 SS 05/17/21/23 25 90%PPM
14.3
13.7
14 SS 05/14/23/26 25 90% BTEX-F1toF4-pHPPM
15.1
14.5
15 SS 12/06/08/13 25 85% BTEX-F1toF4-pHPPM
15.8
15.2
16 SS 12/05/12/10 25 85%PPM
16.6
16.0
SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, damp, wet at15.2m, petroleum odour between 14.5m and15.1m.
16.6
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D. Doherty
TEST HOLE LOG TH103DRILL DATE: January 17, 2008
SHEET#
WEATHER:
ONE of TWO
EQUIPMENT: Track Mount DrillTOP OF GROUND ELEVATION:
Overcast, -1C
GROUND WATER DEPTH: 15.62m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
1
2
3
4
5
6
7
8
9 9
8
7
6
5
4
3
2
1
Continued...
1 SS 06/18/21/22 ND 100%
4.3
3.7
2 SS 08/12/15/14 25 90%PPM
5.0
4.4
3 SS 08/11/18/24 150 85%PPM
5.8
5.2
4 SS 11/24/34/32 100 85%PPM
6.6
5.9
5 SS 05/07/11/17 125 100%PPM
7.3
6.7
6 SS 05/14/38/56 200 100%PPM
8.1
7.5
7 SS 10/39/38/50 275 100%PPM
8.8
8.2
8 SS 09/31/41/35 425 100% BTEX-F1toF4-pHPPM
9.6
9.0
9 SS 11/40/50/50 150 85%9.8
FILL : Light brown, dense, SAND (FILL), damp.
4.3SILTY SAND : Light Brown, compact to verydense, SAND, medium/fine grained, silty, damp,wet at 15.1m, petroleum odour and stainingbetween 5.2m and 15.7m.
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D. Doherty
TEST HOLE LOG TH103DRILL DATE: January 17, 2008
SHEET#
WEATHER:
TWO of TWO
EQUIPMENT: Track Mount DrillTOP OF GROUND ELEVATION:
Overcast, -1C
GROUND WATER DEPTH: 15.62m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
11
12
13
14
15
16
17
18
19 19
18
17
16
15
14
13
12
11
16.76 m - END OF TEST HOLE
9 SS 11/40/50/50 150 85%PPM
10.4
10 SS 04/23/25/40 125 85%PPM
11.1
10.5
11 SS 10/24/25/50 300 85%PPM
11.9
11.3
12 SS 10/21/30/45 250 85%PPM
12.6
12.0
13 SS 08/28/37/41 250 85%PPM
13.4
12.8
14 SS 06/23/36/50 250 100%PPM
14.2
13.6
15 SS 20/27/29/32 250 100%PPM
14.9
14.3
16 SS 05/14/35/27 275 100%PPM
15.7
15.1
17 SS 08/22/27/27 100 100% BTEX-F1toF4-pHPPM
16.5
15.8
SILTY SAND : Light Brown, compact to verydense, SAND, medium/fine grained, silty, damp,wet at 15.1m, petroleum odour and stainingbetween 5.2m and 15.7m.
16.6
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D. Doherty
TEST HOLE LOG TH104DRILL DATE: January 18, 2008
SHEET#
WEATHER:
ONE of TWO
EQUIPMENT: Truck Mount DrillTOP OF GROUND ELEVATION:
Overcast, -5C
GROUND WATER DEPTH: 15.86m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
1
2
3
4
5
6
7
8
9 9
8
7
6
5
4
3
2
1
Continued...
1 SS 01/01/01/01 ND 100%
0.6
2 SS 02/02/02/02 25 65% PAHs-pHPPM
1.4
0.8
3 SS 03/06/12/11 ND 100%
2.1
1.5
4 SS 07/14/14/19 25 85%PPM
3.7
3.0
5 SS 07/16/18/24 25 90%PPM
5.2
4.6
6 SS 07/10/17/22 25 85%PPM
6.7
6.1
7 SS 10/20/25/31 25 100%PPM
8.2
7.6
8 SS 06/16/13/13 25 100%PPM
9.8
9.1
TOPSOIL : Dark Brown, very soft, TOPSOIL, damp. 0.1SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, silty, damp,wet at 15.2m, petroleum odour between 13.7mand 14.3m.
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D. Doherty
TEST HOLE LOG TH104DRILL DATE: January 18, 2008
SHEET#
WEATHER:
TWO of TWO
EQUIPMENT: Truck Mount DrillTOP OF GROUND ELEVATION:
Overcast, -5C
GROUND WATER DEPTH: 15.86m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
11
12
13
14
15
16
17
18
19 19
18
17
16
15
14
13
12
11
16.76 m - END OF TEST HOLE
9 SS 10/20/24/32 50 100%PPM
11.3
10.7
10 SS 05/23/30/33 50 90%PPM
12.8
12.2
11 SS 07/20/26/30 25 85%PPM
13.6
13.0
12 SS 04/14/23/23 75 75% BTEX-F1toF4-pHPPM
14.3
13.7
13 SS 05/11/14/15 50 85%PPM
15.1
14.5
14 SS 02/12/25/25 50 85% BTEX-F1toF4-pHPPM
15.8
15.2
15 SS 04/15/18/25 25 85%PPM
16.6
16.0
SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, silty, damp,wet at 15.2m, petroleum odour between 13.7mand 14.3m.
16.8
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D. Doherty
TEST HOLE LOG TH105DRILL DATE: January 21, 2008
SHEET#
WEATHER:
ONE of TWO
EQUIPMENT: Truck Mount DrillTOP OF GROUND ELEVATION:
Clear, -15C
GROUND WATER DEPTH: 15.58m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
1
2
3
4
5
6
7
8
9 9
8
7
6
5
4
3
2
1
Continued...
1 SS 01/01/01/01 ND 60%
0.6
2 SS 02/02/03/02 ND 60% PAHs-pH
1.4
0.8
3 SS 02/03/04/07 ND 75%
2.1
1.5
4 SS 07/10/14/20 ND 90%
3.7
3.0
5 SS 06/10/15/25 25 85%PPM
5.2
4.6
6 SS 05/19/21/30 25 90%PPM
6.7
6.1
7 SS 10/20/22/26 25 100%PPM
8.2
7.6
8 SS 08/21/24/30 25 75%PPM
9.8
9.1
TOPSOIL : Dark Brown, very soft, TOPSOIL, damp. 0.1SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, silty, damp,wet at 16.0m, petroleum odour between 13.7mand 16.6m.
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D. Doherty
TEST HOLE LOG TH105DRILL DATE: January 21, 2008
SHEET#
WEATHER:
TWO of TWO
EQUIPMENT: Truck Mount DrillTOP OF GROUND ELEVATION:
Clear, -15C
GROUND WATER DEPTH: 15.58m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
11
12
13
14
15
16
17
18
19 19
18
17
16
15
14
13
12
11
16.76 m - END OF TEST HOLE
9 SS 08/21/26/32 50 90%PPM
11.3
10.7
10 SS 06/24/29/50 50 90%PPM
12.8
12.2
11 SS 11/21/35/50 50 90%PPM
13.6
13.0
12 SS 08/12/21/31 25 65%PPM
14.3
13.7
13 SS 06/18/29/40 50 90%PPM
15.1
14.5
14 SS 13/27/31/26 100 85% BTEX-F1toF4-pHPPM
15.8
15.2
15 SS 06/07/09/12 100 50% BTEX-F1toF4-pHPPM
16.6
16.0
SILTY SAND : Light Brown, very loose to verydense, SAND, medium/fine grained, silty, damp,wet at 16.0m, petroleum odour between 13.7mand 16.6m.
16.8
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D. Doherty
TEST HOLE LOG TH106DRILL DATE: January 21, 2008
SHEET#
WEATHER:
ONE of TWO
EQUIPMENT: Truck Mount DrillTOP OF GROUND ELEVATION:
Clear, -15C
GROUND WATER DEPTH: 15.61m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
1
2
3
4
5
6
7
8
9 9
8
7
6
5
4
3
2
1
Continued...
1 SS 06/02/02/03 ND 40%
0.6
2 SS 02/05/03/01 ND 50%
1.4
0.8
3 SS 02/03/05/06 25 60%PPM
2.1
1.5
4 SS 07/12/10/21 ND 85%
3.7
3.0
5 SS 05/16/18/31 ND 90%
5.2
4.6
6 SS 08/21/23/28 ND 75%
6.7
6.1
7 SS 05/21/24/29 25 90%PPM
8.2
7.6
8 SS 10/20/23/29 50 90%PPM
9.8
9.1
TOPSOIL : Dark Brown, soft, TOPSOIL, damp.0.2
SILTY SAND : Light Brown, loose to very dense,SAND, medium/fine grained, silty, damp, wet at15.2m.
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
PROJECT #
TECHNICIAN
07126
D. Doherty
TEST HOLE LOG TH106DRILL DATE: January 21, 2008
SHEET#
WEATHER:
TWO of TWO
EQUIPMENT: Truck Mount DrillTOP OF GROUND ELEVATION:
Clear, -15C
GROUND WATER DEPTH: 15.61m. (24/01/2008)
SITE: Thirteen PropertiesADDRESS: High Park Project, Toronto ON
UTM: 483 45 39Northing Easting 62 39 81
SA
MP
LE
#
CO
UN
T
BL
OW
TY
PE
RE
AD
ING
VA
PO
UR
RE
CO
VE
RY
%
ST
RA
TA
PL
OT
DE
PT
H (
M)
DE
PT
H (
M)
ANALYSISREQUESTED
DESCRIPTION OFSTRATIGRAPHY MONITOR
TOP OF MONITOR ELEVATION: NANA
(Blo
ws
per
ft)
11
12
13
14
15
16
17
18
19 19
18
17
16
15
14
13
12
11
16.76 m - END OF TEST HOLE
9 SS 12/21/24/34 25 85%PPM
11.3
10.7
10 SS 12/24/37/42 25 90%PPM
12.8
12.2
11 SS 10/20/26/30 25 85%PPM
13.6
13.0
12 SS 10/20/34/36 25 90%PPM
14.3
13.7
13 SS 10/21/30/38 50 85%PPM
15.1
14.5
14 SS 05/21/23/28 50 45% BTEX-F1toF4-pHPPM
15.8
15.2
15 SS 12/24/34/26 50 70% BTEX-F1toF4-pHPPM
16.6
16.0
SILTY SAND : Light Brown, loose to very dense,SAND, medium/fine grained, silty, damp, wet at15.2m.
16.8
BARENCOLEGEND: AU = Auger Sample SS = Split Spoon GR = Grab SampleND = non detect NM = not measured due to insufficient sample volume
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Attached are copies of the original Certificates of Analysis provided by thelaboratory. The data contained in these analyses is to be read only inconjunction with the report to which it is attached. For interpretation ofthe chemical data, see the attached text.
All samples are submitted to and reported by the laboratory usingpurchase order numbers and sample location codes. These are onlydiscernable to persons familiar with the purchase order system and thelocation codes. For descriptions of the locations of the samples, see theattached text.
Not all data contained in the original laboratory certificate of analysis mayhave been referenced in the report. Samples may have been submitted astravel or field blanks or as duplicates. Some samples may be for controlpurposes and represent soil that is no longer on the site and is notrelevant to the report.
Since the laboratory data contains scientific terms and references, onlytrained persons familiar with sampling and laboratory methods shouldattempt to interpret the raw data.
Your P.O. #: 07126 Your Project #: 07126 Your C.O.C. #: 00553371
Attention: Bernard ChanBarenco Inc2561 Stouffville RdPO Box 295Gormley, ONL0H 1G0
Report Date: 2008/02/04
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: A805178Received: 2008/01/17, 14:24
Sample Matrix: Soil# Samples Received: 2
Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceTEH in Soil (AA PIRI) ( 1 ) 2 N/A 2008/01/23 ATL SOP 00116 R2 Based on Atl. PIRI Petroleum Hydro. CCME F1 & BTEX in Soil 2 2008/01/21 2008/01/22 CAM SOP-00315 CCME CWS Petroleum Hydrocarbons F2-F4 in Soil 2 2008/01/21 2008/01/21 CAM SOP-00316 CCME CWS Moisture ( 1 ) 2 N/A 2008/01/21 ATL SOP 00001 R2 MOE Handbook 1983 MOISTURE 2 N/A 2008/01/19 Ont SOP-0114 MOE HANDBOOK(1983) PAH Compounds in Soil by GC/MS (SIM) 1 2008/01/18 2008/01/18 SOP - 00318 EPA 8270 pH CaCl2 EXTRACT 2 N/A 2008/01/23 Ont SOP-0067 4 5 0 0 - H + B VPH in Soil (PIRI2) ( 1 ) 2 N/A 2008/01/22 ATL SOP 00120 R2 Based on Atl. PIRI ModTPH (T2) Calc. for Soil ( 1 ) 2 N/A 2008/01/24 n/a Based on Atl. PIRI
* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.
(1) This test was performed by Bedford
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager.
SARA SAROOP, Campobello Customer serviceEmail: [email protected]# (905) 817-5700 Ext:5819
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
For Service Group specific validation please refer to the Validation Signature Page
Total cover pages: 1
Page 1 of 11
Barenco IncMaxxam Job #: A805178 Client Project #: 07126Report Date: 2008/02/04 Project name:
Your P.O. #: 07126Sampler Initials:
RESULTS OF ANALYSES OF SOIL
Maxxam ID W 8 0 9 9 7 W 8 0 9 9 8Sampling Date 2008/01/16 2008/01/16
12:00 12:15COC Number 00553371 00553371 U n i t s TH101-13 QC Batch TH101-15 R D L QC Batch
INORGANICS
Moisture % 8 1443911 16 1 1443911
Available (CaCl2) pH pH 7.80 1446001 7.96 1445535
RDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 2 of 11
Barenco IncMaxxam Job #: A805178 Client Project #: 07126Report Date: 2008/02/04 Project name:
Your P.O. #: 07126Sampler Initials:
ATLANTIC RBCA HYDROCARBONS (SOIL)
Maxxam ID W 8 0 9 9 7 W 8 0 9 9 8Sampling Date 2008/01/16 2008/01/16
12:00 12:15COC Number 00553371 00553371 U n i t s TH101-13 R D L TH101-15 R D L QC Batch
TPH COMPOUNDS
Benzene mg/kg ND 0.3 ND 0.03 1444618
Toluene mg/kg ND 0.3 ND 0.03 1444618
Ethylbenzene mg/kg ND 0.3 ND 0.03 1444618
Xylene (Total) mg/kg 14 0.5 ND 0.05 1444618
Aliphatic >C6-C8 mg/kg 37 1 ND 0.1 1444618
Aliphatic >C8-C10 mg/kg 1400 4 ND 0.4 1444618
>C8-C10 Aromatics (-EX) mg/kg 200 2 ND 0.2 1444618
Aliphatic >C10-C12 mg/kg 3200 8.0 ND 8.0 1444005
Aliphatic >C12-C16 mg/kg 11000 15 ND 15 1444005
Aliphatic >C16-C21 mg/kg 4900 15 ND 15 1444005
Aliphatic >C21-<C32 mg/kg 520 15 ND 15 1444005
Aromatic >C10-C12 mg/kg 850 4.0 ND 4.0 1444005
Aromatic >C12-C16 mg/kg 3500 15 ND 15 1444005
Aromatic >C16-C21 mg/kg 2100 15 ND 15 1444005
Aromatic >C21-<C32 mg/kg 620 15 ND 15 1444005
Modified TPH (Tier 2) mg/kg 28000 20 ND 20 1443083
Surrogate Recovery (%)
Isobutylbenzene - Extractable % 57 92 1444005
Isobutylbenzene - Volatile % 81 ( 1 ) 111 1444618
n-Dotriacontane - Extractable % 82 ( 2 ) 80 1444005
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) Elevated VPH RDL(s) due to sample dilution.( 2 ) Fuel oil fraction. TEH surrogate(s) not within acceptance limits. Analysis was repeated withsimilar results.
Page 3 of 11
Barenco IncMaxxam Job #: A805178 Client Project #: 07126Report Date: 2008/02/04 Project name:
Your P.O. #: 07126Sampler Initials:
SEMI-VOLATILE ORGANICS BY GC-MS (SOIL)
Maxxam ID W 8 0 9 9 8Sampling Date 2008/01/16
12:15COC Number 00553371 U n i t s TH101-15 R D L QC Batch
PAHs
Acenaphthene ug/g ND 0.01 1443550
Acenaphthylene ug/g ND 0.005 1443550
Anthracene ug/g ND 0.005 1443550
Benzo(a)anthracene ug/g ND 0.01 1443550
Benzo(a)pyrene ug/g ND 0.005 1443550
Benzo(b/j)fluoranthene ug/g ND 0.005 1443550
Benzo(g,h,i)perylene ug/g ND 0.02 1443550
Benzo(k)fluoranthene ug/g ND 0.01 1443550
Chrysene ug/g ND 0.01 1443550
Dibenz(a,h)anthracene ug/g ND 0.02 1443550
Fluoranthene ug/g ND 0.005 1443550
Fluorene ug/g ND 0.005 1443550
Indeno(1,2,3-cd)pyrene ug/g ND 0.02 1443550
1-Methylnaphthalene ug/g ND 0.005 1443550
2-Methylnaphthalene ug/g ND 0.005 1443550
Naphthalene ug/g ND 0.005 1443550
Phenanthrene ug/g ND 0.005 1443550
Pyrene ug/g ND 0.005 1443550
Surrogate Recovery (%)
D10-Anthracene % 113 1443550
D14-Terphenyl (FS) % 109 1443550
D7-Quinoline % 75 1443550
D8-Acenaphthylene % 71 1443550
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 4 of 11
Barenco IncMaxxam Job #: A805178 Client Project #: 07126Report Date: 2008/02/04 Project name:
Your P.O. #: 07126Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID W 8 0 9 9 7 W 8 0 9 9 8Sampling Date 2008/01/16 2008/01/16
12:00 12:15COC Number 00553371 00553371 U n i t s TH101-13 TH101-15 R D L QC Batch
F1 PHC and BTEX
Benzene ug/g ND ND 0.02 1443986
Toluene ug/g ND ND 0.02 1443986
Ethylbenzene ug/g ND ND 0.02 1443986
o-Xylene ug/g 0.40 ND 0.02 1443986
p+m-Xylene ug/g 0.22 ND 0.04 1443986
Total Xylenes ug/g 0.62 ND 0.04 1443986
F1 (C6-C10) ug/g 92 ND 10 1443986
F1 (C6-C10) - BTEX ug/g 92 ND 10 1443986
F2-F4 PHC
F2 (C10-C16 Hydrocarbons) ug/g 2900 ND 10 1443839
F3 (C16-C34 Hydrocarbons) ug/g 2200 ND 10 1443839
F4 (C34-C50 Hydrocarbons) ug/g ND ND 10 1443839
Reached Baseline at C50 ug/g Yes Yes 1443839
Surrogate Recovery (%)
1,4-Difluorobenzene % 103 106 1443986
4-Bromofluorobenzene % 96 94 1443986
D10-Ethylbenzene % 111 112 1443986
D4-1,2-Dichloroethane % 101 98 1443986
o-Terphenyl % 117 96 1443839
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 5 of 11
Barenco IncMaxxam Job #: A805178 Client Project #: 07126Report Date: 2008/02/04 Project name:
Your P.O. #: 07126Sampler Initials:
GENERAL COMMENTS
Results relate only to the items tested.
Page 6 of 11
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance ReportMaxxam Job Number: MA805178
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1443550 MWG MATRIX SPIKE[W80998-01] D10-Anthracene 2008/01/18 104 % 30 - 130
D14-Terphenyl (FS) 2008/01/18 105 % 30 - 130D7-Quinoline 2008/01/18 86 % 30 - 130D8-Acenaphthylene 2008/01/18 82 % 30 - 130Acenaphthene 2008/01/18 121 % 30 - 130Acenaphthylene 2008/01/18 90 % 30 - 130Anthracene 2008/01/18 102 % 30 - 130Benzo(a)anthracene 2008/01/18 108 % 30 - 130Benzo(a)pyrene 2008/01/18 112 % 30 - 130Benzo(b/j)fluoranthene 2008/01/18 108 % 30 - 130Benzo(g,h,i)perylene 2008/01/18 93 % 30 - 130Benzo(k)fluoranthene 2008/01/18 109 % 30 - 130Chrysene 2008/01/18 104 % 30 - 130Dibenz(a,h)anthracene 2008/01/18 87 % 30 - 130Fluoranthene 2008/01/18 110 % 30 - 130Fluorene 2008/01/18 109 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/18 83 % 30 - 1301-Methylnaphthalene 2008/01/18 97 % 30 - 1302-Methylnaphthalene 2008/01/18 95 % 30 - 130Naphthalene 2008/01/18 96 % 30 - 130Phenanthrene 2008/01/18 100 % 30 - 130Pyrene 2008/01/18 106 % 30 - 130
Spiked Blank D10-Anthracene 2008/01/18 112 % 30 - 130D14-Terphenyl (FS) 2008/01/18 107 % 30 - 130D7-Quinoline 2008/01/18 96 % 30 - 130D8-Acenaphthylene 2008/01/18 88 % 30 - 130Acenaphthene 2008/01/18 125 % 30 - 130Acenaphthylene 2008/01/18 98 % 30 - 130Anthracene 2008/01/18 112 % 30 - 130Benzo(a)anthracene 2008/01/18 109 % 30 - 130Benzo(a)pyrene 2008/01/18 112 % 30 - 130Benzo(b/j)fluoranthene 2008/01/18 109 % 30 - 130Benzo(g,h,i)perylene 2008/01/18 95 % 30 - 130Benzo(k)fluoranthene 2008/01/18 110 % 30 - 130Chrysene 2008/01/18 105 % 30 - 130Dibenz(a,h)anthracene 2008/01/18 92 % 30 - 130Fluoranthene 2008/01/18 116 % 30 - 130Fluorene 2008/01/18 114 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/18 87 % 30 - 1301-Methylnaphthalene 2008/01/18 104 % 30 - 1302-Methylnaphthalene 2008/01/18 102 % 30 - 130Naphthalene 2008/01/18 101 % 30 - 130Phenanthrene 2008/01/18 112 % 30 - 130Pyrene 2008/01/18 109 % 30 - 130
Method Blank D10-Anthracene 2008/01/18 105 % 30 - 130D14-Terphenyl (FS) 2008/01/18 99 % 30 - 130D7-Quinoline 2008/01/18 81 % 30 - 130D8-Acenaphthylene 2008/01/18 78 % 30 - 130Acenaphthene 2008/01/18 ND, RDL=0.01 ug/gAcenaphthylene 2008/01/18 ND, RDL=0.005 ug/gAnthracene 2008/01/18 ND, RDL=0.005 ug/gBenzo(a)anthracene 2008/01/18 ND, RDL=0.01 ug/gBenzo(a)pyrene 2008/01/18 ND, RDL=0.005 ug/gBenzo(b/j)fluoranthene 2008/01/18 ND, RDL=0.005 ug/g
Page 7 of 11
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA805178
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1443550 MWG Method Blank Benzo(g,h,i)perylene 2008/01/18 ND, RDL=0.02 ug/gBenzo(k)fluoranthene 2008/01/18 ND, RDL=0.01 ug/gChrysene 2008/01/18 ND, RDL=0.01 ug/gDibenz(a,h)anthracene 2008/01/18 ND, RDL=0.02 ug/gFluoranthene 2008/01/18 ND, RDL=0.005 ug/gFluorene 2008/01/18 ND, RDL=0.005 ug/gIndeno(1,2,3-cd)pyrene 2008/01/18 ND, RDL=0.02 ug/g1-Methylnaphthalene 2008/01/18 ND, RDL=0.005 ug/g2-Methylnaphthalene 2008/01/18 ND, RDL=0.005 ug/gNaphthalene 2008/01/18 ND, RDL=0.005 ug/gPhenanthrene 2008/01/18 ND, RDL=0.005 ug/gPyrene 2008/01/18 ND, RDL=0.005 ug/g
RPD [ W 8 0 9 9 8 - 0 1 ] Acenaphthene 2008/01/18 NC % 50Acenaphthylene 2008/01/18 NC % 50Anthracene 2008/01/18 NC % 50Benzo(a)anthracene 2008/01/18 NC % 50Benzo(a)pyrene 2008/01/18 NC % 50Benzo(b/j)fluoranthene 2008/01/18 NC % 50Benzo(g,h,i)perylene 2008/01/18 NC % 50Benzo(k)fluoranthene 2008/01/18 NC % 50Chrysene 2008/01/18 NC % 50Dibenz(a,h)anthracene 2008/01/18 NC % 50Fluoranthene 2008/01/18 NC % 50Fluorene 2008/01/18 NC % 50Indeno(1,2,3-cd)pyrene 2008/01/18 NC % 501-Methylnaphthalene 2008/01/18 NC % 502-Methylnaphthalene 2008/01/18 NC % 50Naphthalene 2008/01/18 NC % 50Phenanthrene 2008/01/18 NC % 50Pyrene 2008/01/18 NC % 50
1443806 MYG RPD Moisture 2008/01/19 0.8 % 501443823 MYG RPD Moisture 2008/01/19 0.9 % 501443839 JKA MATRIX SPIKE
[W80997-01] o-Terphenyl 2008/01/21 NC ( 1 ) % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/21 NC ( 2 ) % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/21 NC % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/21 NC % 60 - 130
Spiked Blank o-Terphenyl 2008/01/21 86 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/21 77 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/21 77 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/21 77 % 60 - 130
Method Blank o-Terphenyl 2008/01/21 87 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/21 ND, RDL=10 ug/gF3 (C16-C34 Hydrocarbons) 2008/01/21 ND, RDL=10 ug/gF4 (C34-C50 Hydrocarbons) 2008/01/21 ND, RDL=10 ug/g
RPD [ W 8 0 9 9 7 - 0 1 ] F2 (C10-C16 Hydrocarbons) 2008/01/21 22.1 % 50F3 (C16-C34 Hydrocarbons) 2008/01/21 28.0 % 50F4 (C34-C50 Hydrocarbons) 2008/01/21 NC % 50
1443986 AGA MATRIX SPIKE[W80997-01] 1,4-Difluorobenzene 2008/01/22 101 % 60 - 140
4-Bromofluorobenzene 2008/01/22 97 % 60 - 140D10-Ethylbenzene 2008/01/22 123 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 99 % 60 - 140Benzene 2008/01/22 110 % 60 - 140Toluene 2008/01/22 116 % 60 - 140
Page 8 of 11
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA805178
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1443986 AGA MATRIX SPIKE[W80997-01] Ethylbenzene 2008/01/22 116 % 60 - 140
o-Xylene 2008/01/22 116 % 60 - 140p+m-Xylene 2008/01/22 121 % 60 - 140F1 (C6-C10) 2008/01/22 NC ( 3 ) % 60 - 140
Spiked Blank 1,4-Difluorobenzene 2008/01/22 105 % 60 - 1404-Bromofluorobenzene 2008/01/22 95 % 60 - 140D10-Ethylbenzene 2008/01/22 107 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 98 % 60 - 140Benzene 2008/01/22 99 % 60 - 140Toluene 2008/01/22 105 % 60 - 140Ethylbenzene 2008/01/22 104 % 60 - 140o-Xylene 2008/01/22 106 % 60 - 140p+m-Xylene 2008/01/22 109 % 60 - 140F1 (C6-C10) 2008/01/22 93 % 60 - 140
Method Blank 1,4-Difluorobenzene 2008/01/22 103 % 60 - 1404-Bromofluorobenzene 2008/01/22 95 % 60 - 140D10-Ethylbenzene 2008/01/22 99 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 101 % 60 - 140Benzene 2008/01/22 ND, RDL=0.02 ug/gToluene 2008/01/22 ND, RDL=0.02 ug/gEthylbenzene 2008/01/22 ND, RDL=0.02 ug/go-Xylene 2008/01/22 ND, RDL=0.02 ug/gp+m-Xylene 2008/01/22 ND, RDL=0.04 ug/gTotal Xylenes 2008/01/22 ND, RDL=0.04 ug/gF1 (C6-C10) 2008/01/22 ND, RDL=10 ug/gF1 (C6-C10) - BTEX 2008/01/22 ND, RDL=10 ug/g
RPD [ W 8 0 9 9 7 - 0 1 ] Benzene 2008/01/22 NC % 50Toluene 2008/01/22 NC % 50Ethylbenzene 2008/01/22 NC % 50o-Xylene 2008/01/22 25.6 % 50p+m-Xylene 2008/01/22 27.6 % 50Total Xylenes 2008/01/22 26.3 % 50F1 (C6-C10) 2008/01/22 38.4 % 50F1 (C6-C10) - BTEX 2008/01/22 38.5 % 50
1444005 KKE Spiked Blank Aliphatic >C10-C12 2008/01/23 87 % 30 - 130Aliphatic >C12-C16 2008/01/23 87 % 30 - 130Aliphatic >C16-C21 2008/01/23 87 % 30 - 130Aliphatic >C21-<C32 2008/01/23 87 % 30 - 130Aromatic >C10-C12 2008/01/23 122 % 30 - 130Aromatic >C12-C16 2008/01/23 111 % 30 - 130Aromatic >C16-C21 2008/01/23 105 % 30 - 130Aromatic >C21-<C32 2008/01/23 98 % 30 - 130
Method Blank Isobutylbenzene - Extractable 2008/01/23 92 % 30 - 130n-Dotriacontane - Extractable 2008/01/23 86 % 30 - 130Aliphatic >C10-C12 2008/01/23 ND, RDL=8 mg/kgAliphatic >C12-C16 2008/01/23 ND, RDL=15 mg/kgAliphatic >C16-C21 2008/01/23 ND, RDL=15 mg/kgAliphatic >C21-<C32 2008/01/23 ND, RDL=15 mg/kgAromatic >C10-C12 2008/01/23 ND, RDL=4 mg/kgAromatic >C12-C16 2008/01/23 ND, RDL=15 mg/kgAromatic >C16-C21 2008/01/23 ND, RDL=15 mg/kgAromatic >C21-<C32 2008/01/23 ND, RDL=15 mg/kg
RPD [ W 8 0 9 9 7 - 0 3 ] Aliphatic >C10-C12 2008/01/23 15.0 % 50Aliphatic >C12-C16 2008/01/23 16.9 % 50
Page 9 of 11
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA805178
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1444005 KKE RPD [ W 8 0 9 9 7 - 0 3 ] Aliphatic >C16-C21 2008/01/23 14.0 % 50Aliphatic >C21-<C32 2008/01/23 13.8 % 50Aromatic >C10-C12 2008/01/23 8.0 % 50Aromatic >C12-C16 2008/01/23 7.3 % 50Aromatic >C16-C21 2008/01/23 9.0 % 50Aromatic >C21-<C32 2008/01/23 15.3 % 50
1444618 LMU Spiked Blank Isobutylbenzene - Volatile 2008/01/22 102 % 60 - 140Benzene 2008/01/22 94 % 60 - 140Toluene 2008/01/22 92 % 60 - 140Ethylbenzene 2008/01/22 92 % 60 - 140Xylene (Total) 2008/01/22 90 % 60 - 140
Method Blank Isobutylbenzene - Volatile 2008/01/22 97 % 60 - 140Benzene 2008/01/22 ND, RDL=0.03 mg/kgToluene 2008/01/22 ND, RDL=0.03 mg/kgEthylbenzene 2008/01/22 ND, RDL=0.03 mg/kgXylene (Total) 2008/01/22 ND, RDL=0.05 mg/kgAliphatic >C6-C8 2008/01/22 ND, RDL=0.1 mg/kgAliphatic >C8-C10 2008/01/22 ND, RDL=0.4 mg/kg>C8-C10 Aromatics (-EX) 2008/01/22 0.2, RDL=0.1 mg/kg
ND = Not detectedNC = Non-calculableRPD = Relative Percent DifferenceSPIKE = Fortified sample( 1 ) The extraction surrogate recovery is not calculated due to Matrix interferences.( 2 ) Matrix spike recoveries were not calculated (NC) because of high concentration of target compounds in the parent sample.( 3 ) The recovery in the matrix spiked is not calculated (NC) due to high concentration of this compound in the parent sample.
Page 10 of 11
Validation Signature Page
Maxxam Job #: A805178
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).
BRAD NEWMAN, Scientific Specialist
JAMES MACDONALD, Organics Manager
MEDHAT RISKALLAH, Manager, Hydrocarbon Department
MICHAEL WANG,
SUZANA POPOVIC, Supervisor, Hydrocarbons
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
Page 11 of 11
Your Project #: MA805178 Site: 07126
Attention: SUB CONTRACTORMAXXAM ANALYTICS INC.CAMPOBELLO6740 CAMPOBELLO ROADMISSISSAUGA, ONCANADA L5N 2L8
Report Date: 2008/02/01
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: A802778Received: 2008/01/21, 10:35
Sample Matrix: Soil# Samples Received: 2
Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodCCME Hydrocarbons (F2-F4 in soil) 2 2008/01/22 2008/01/22 CAL SOP-00086 CCME PHC-CWS Aliphatic and Aromatic Fractions C10-C50 1 2008/01/22 2008/01/30 CAL SOP-00184 CCME PHC-CWS Moisture 2 N/A 2008/01/22 CAL SOP-00023 McKeague MSSMA 2.411
* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager.
HEATHER ECCLES,Email: [email protected]# (403) 291-3077
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
For Service Group specific validation please refer to the Validation Signature Page
Total cover pages: 1
Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468
Page 1 of 7
MAXXAM ANALYTICS INC.Maxxam Job #: A802778 Client Project #: MA805178Report Date: 2008/02/01 Site Reference: 07126
Sampler Initials:
RESULTS OF CHEMICAL ANALYSES OF SOIL
Maxxam ID I 6 2 4 7 8 I 6 2 4 8 2Sampling Date 2008/01/16 2008/01/16 U n i t s TH101-13 TH101-15 R D L QC Batch
(W80997-02R) (W80998-02R)
Physical Properties
Moisture % 9.2 15.9 0.3 2079421
RDL = Reportable Detection Limit
Page 2 of 7
MAXXAM ANALYTICS INC.Maxxam Job #: A802778 Client Project #: MA805178Report Date: 2008/02/01 Site Reference: 07126
Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID I 6 2 4 7 8 I 6 2 4 8 2Sampling Date 2008/01/16 2008/01/16 U n i t s TH101-13 QC Batch TH101-15 R D L QC Batch
(W80997-02R) (W80998-02R)
Ext. Pet. Hydrocarbon
F2 (C10-C16 Hydrocarbons) mg/kg 12000 2082057 <10 10 2082057
F3 (C16-C34 Hydrocarbons) mg/kg 5900 2082057 <10 10 2082057
F4 (C34-C50 Hydrocarbons) mg/kg 16 2082057 <10 10 2082057
Reached Baseline at C50 mg/kg Yes 2082057 Yes N/A 2082057
Hydrocarbons
>C10 - C12 Aliphatic mg/kg 2460 2079711 N/A 5 2079711
>C10 - C12 Aromatic mg/kg 92 2079711 N/A 5 2079711
>C12 - C16 Aliphatic mg/kg 7570 2079711 N/A 10 2079711
>C12 - C16 Aromatic mg/kg 525 2079711 N/A 10 2079711
>C16 - C21 Aliphatic mg/kg 6080 2079711 N/A 10 2079711
>C16 - C21 Aromatic mg/kg 762 2079711 N/A 10 2079711
>C21 - C34 Aliphatic mg/kg <10 2079711 N/A 10 2079711
>C21 - C34 Aromatic mg/kg 355 2079711 N/A 10 2079711
>C34 Aliphatic (up to C50) mg/kg <10 2079711 N/A 10 2079711
>C34 Aromatic (up to C50) mg/kg 41 2079711 N/A 10 2079711
Surrogate Recovery (%)
O-TERPHENYL (sur.) % 112 2079711 100 N/A 2082057
N/A = Not ApplicableRDL = Reportable Detection Limit
Page 3 of 7
MAXXAM ANALYTICS INC.Maxxam Job #: A802778 Client Project #: MA805178Report Date: 2008/02/01 Site Reference: 07126
Sampler Initials:
PETROLEUM HYDROCARBONS (CCME) Comments
Sample I62478-01 CCME Hydrocarbons (F2-F4 in soil): Matrix spike recovery non calculable, due to high concentration of original analyte.
Sample I62482-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are <DL.
Sample I62478-01 Aliphatic and Aromatic Fractions C10-C50: Matrix spike recovery non calculable, due to high concentration of original analyte.
Results relate only to the items tested.
Page 4 of 7
MAXXAM ANALYTICS INC.Attention: SUB CONTRACTOR Client Project #: MA805178P.O. #: Site Reference: 07126
Quality Assurance ReportMaxxam Job Number: CA802778
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
2079421 RM2 RPD Moisture 2008/01/22 7.0 % 202079711 LSH Calibration Check >C10 - C12 Aliphatic 2008/01/30 94 % 80 - 120
>C10 - C12 Aromatic 2008/01/30 97 % 80 - 120>C12 - C16 Aliphatic 2008/01/30 95 % 80 - 120>C12 - C16 Aromatic 2008/01/30 97 % 80 - 120>C16 - C21 Aliphatic 2008/01/30 94 % 80 - 120>C16 - C21 Aromatic 2008/01/30 98 % 80 - 120>C21 - C34 Aliphatic 2008/01/30 92 % 80 - 120>C21 - C34 Aromatic 2008/01/30 95 % 80 - 120>C34 Aliphatic (up to C50) 2008/01/30 93 % 80 - 120>C34 Aromatic (up to C50) 2008/01/30 90 % 80 - 120
MATRIX SPIKE[I62478-01] O-TERPHENYL (sur.) 2008/01/30 88 % 30 - 130
>C21 - C34 Aliphatic 2008/01/30 93 % 50 - 130>C34 Aliphatic (up to C50) 2008/01/30 108 % 50 - 130
QC STANDARD >C10 - C12 Aliphatic 2008/01/30 77 % 70 - 130>C10 - C12 Aromatic 2008/01/30 95 % 70 - 130>C12 - C16 Aliphatic 2008/01/30 84 % 70 - 130>C12 - C16 Aromatic 2008/01/30 96 % 70 - 130>C16 - C21 Aliphatic 2008/01/30 87 % 70 - 130>C16 - C21 Aromatic 2008/01/30 94 % 70 - 130>C21 - C34 Aliphatic 2008/01/30 86 % 70 - 130>C21 - C34 Aromatic 2008/01/30 96 % 70 - 130>C34 Aliphatic (up to C50) 2008/01/30 88 % 70 - 130>C34 Aromatic (up to C50) 2008/01/30 129 % 70 - 130
SPIKE O-TERPHENYL (sur.) 2008/01/30 79 % 30 - 130>C10 - C12 Aliphatic 2008/01/30 71 % 70 - 130>C10 - C12 Aromatic 2008/01/30 121 % 70 - 130>C12 - C16 Aliphatic 2008/01/30 83 % 70 - 130>C12 - C16 Aromatic 2008/01/30 117 % 70 - 130>C16 - C21 Aliphatic 2008/01/30 78 % 70 - 130>C16 - C21 Aromatic 2008/01/30 72 % 70 - 130>C21 - C34 Aliphatic 2008/01/30 86 % 70 - 130>C21 - C34 Aromatic 2008/01/30 89 % 70 - 130>C34 Aliphatic (up to C50) 2008/01/30 125 % 70 - 130>C34 Aromatic (up to C50) 2008/01/30 73 % 70 - 130
BLANK O-TERPHENYL (sur.) 2008/01/30 100 % 30 - 130>C10 - C12 Aliphatic 2008/01/30 <5 mg/kg>C10 - C12 Aromatic 2008/01/30 <5 mg/kg>C12 - C16 Aliphatic 2008/01/30 <10 mg/kg>C12 - C16 Aromatic 2008/01/30 <10 mg/kg>C16 - C21 Aliphatic 2008/01/30 <10 mg/kg>C16 - C21 Aromatic 2008/01/30 <10 mg/kg>C21 - C34 Aliphatic 2008/01/30 <10 mg/kg>C21 - C34 Aromatic 2008/01/30 <10 mg/kg>C34 Aliphatic (up to C50) 2008/01/30 <10 mg/kg>C34 Aromatic (up to C50) 2008/01/30 <10 mg/kg
RPD >C10 - C12 Aliphatic 2008/01/30 33.1 % 40>C10 - C12 Aromatic 2008/01/30 23.9 % 40>C12 - C16 Aliphatic 2008/01/30 33.1 % 40>C12 - C16 Aromatic 2008/01/30 13.3 % 40>C16 - C21 Aliphatic 2008/01/30 30.5 % 40>C16 - C21 Aromatic 2008/01/30 5.0 % 40>C21 - C34 Aliphatic 2008/01/30 25.3 % 40>C21 - C34 Aromatic 2008/01/30 3.7 % 40
Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468
Page 5 of 7
MAXXAM ANALYTICS INC.Attention: SUB CONTRACTOR Client Project #: MA805178P.O. #: Site Reference: 07126
Quality Assurance Report (Continued)Maxxam Job Number: CA802778
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
2079711 LSH RPD >C34 Aliphatic (up to C50) 2008/01/30 NC % 40>C34 Aromatic (up to C50) 2008/01/30 15.7 % 40
2082057 LSH Calibration Check F2 (C10-C16 Hydrocarbons) 2008/01/22 105 % 80 - 120F3 (C16-C34 Hydrocarbons) 2008/01/22 104 % 80 - 120F4 (C34-C50 Hydrocarbons) 2008/01/22 104 % 80 - 120
MATRIX SPIKE[I62478-01] O-TERPHENYL (sur.) 2008/01/22 104 % 50 - 130
F2 (C10-C16 Hydrocarbons) 2008/01/22 NA % 50 - 130F3 (C16-C34 Hydrocarbons) 2008/01/22 NA % 50 - 130F4 (C34-C50 Hydrocarbons) 2008/01/22 NA % 50 - 130
QC STANDARD F2 (C10-C16 Hydrocarbons) 2008/01/22 103 % 85 - 115F3 (C16-C34 Hydrocarbons) 2008/01/22 110 % 85 - 115F4 (C34-C50 Hydrocarbons) 2008/01/22 106 % 85 - 115
SPIKE O-TERPHENYL (sur.) 2008/01/22 85 % 50 - 130F2 (C10-C16 Hydrocarbons) 2008/01/22 100 % 50 - 130F3 (C16-C34 Hydrocarbons) 2008/01/22 98 % 50 - 130F4 (C34-C50 Hydrocarbons) 2008/01/22 113 % 50 - 130
BLANK O-TERPHENYL (sur.) 2008/01/22 99 % 50 - 130F2 (C10-C16 Hydrocarbons) 2008/01/22 <10 mg/kgF3 (C16-C34 Hydrocarbons) 2008/01/22 <10 mg/kgF4 (C34-C50 Hydrocarbons) 2008/01/22 <10 mg/kgReached Baseline at C50 2008/01/22 YES mg/kg
RPD [ I 6 2 4 7 8 - 0 1 ] F2 (C10-C16 Hydrocarbons) 2008/01/22 3.7 % 50F3 (C16-C34 Hydrocarbons) 2008/01/22 0.3 % 50F4 (C34-C50 Hydrocarbons) 2008/01/22 NC % 50Reached Baseline at C50 2008/01/22 NC % 50
NC = Non-calculableRPD = Relative Percent Difference
Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468
Page 6 of 7
Validation Signature Page
Maxxam Job #: A802778
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).
LUBA SHYMUSHOVSKA,
VERONICA FALK,
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
Page 7 of 7
Your P.O. #: 07126 Your Project #: 07126 Your C.O.C. #: 00553374
Attention: Bernard ChanBarenco Inc2561 Stouffville RdPO Box 295Gormley, ONL0H 1G0
Report Date: 2008/02/05
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: A806235Received: 2008/01/21, 14:55
Sample Matrix: Soil# Samples Received: 7
Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceTEH in Soil (AA PIRI) ( 1 ) 6 N/A 2008/01/25 ATL SOP 00116 R2 Based on Atl. PIRI Petroleum Hydro. CCME F1 & BTEX in Soil 6 2008/01/22 2008/01/22 CAM SOP-00315 CCME CWS Petroleum Hydrocarbons F2-F4 in Soil 6 2008/01/22 2008/01/22 CAM SOP-00316 CCME CWS Moisture ( 1 ) 6 N/A 2008/01/23 ATL SOP 00001 R2 MOE Handbook 1983 MOISTURE 7 N/A 2008/01/23 Ont SOP-0114 MOE HANDBOOK(1983) PAH Compounds in Soil by GC/MS (SIM) 1 2008/01/23 2008/01/23 SOP - 00318 EPA 8270 pH CaCl2 EXTRACT 7 N/A 2008/01/25 Ont SOP-0067 4 5 0 0 - H + B VPH in Soil (PIRI2) ( 1 ) 6 N/A 2008/01/25 ATL SOP 00120 R2 Based on Atl. PIRI ModTPH (T2) Calc. for Soil ( 1 ) 6 N/A 2008/01/28 n/a Based on Atl. PIRI
* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.
(1) This test was performed by Bedford
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager.
SARA SAROOP, Campobello Customer serviceEmail: [email protected]# (905) 817-5700 Ext:5819
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
For Service Group specific validation please refer to the Validation Signature Page
Total cover pages: 1
Page 1 of 13
Barenco IncMaxxam Job #: A806235 Client Project #: 07126Report Date: 2008/02/05 Project name:
Your P.O. #: 07126Sampler Initials:
RESULTS OF ANALYSES OF SOIL
Maxxam ID W 8 5 4 8 3 W 8 5 4 8 4 W 8 5 4 8 5 W 8 5 4 8 6Sampling Date 2008/01/17 2008/01/17 2008/01/17 2008/01/17
12:00 12:30 14:00 14:30COC Number 00553374 00553374 00553374 00553374 U n i t s TH102-14 TH102-15 TH103-8 TH103-17 R D L QC Batch
INORGANICS
Moisture % 11 20 17 16 1 1445659
Available (CaCl2) pH pH 7.96 7.78 7.89 7.91 1447134
RDL = Reportable Detection LimitQC Batch = Quality Control Batch
Maxxam ID W 8 5 4 8 7 W 8 5 4 8 8Sampling Date 2008/01/18 2008/01/18
10:00 13:00COC Number 00553374 00553374 U n i t s TH104-2 R D L QC Batch TH104-12 R D L QC Batch
INORGANICS
Moisture % 20 0.2 1445548 17 1 1445659
Available (CaCl2) pH pH 7.23 1447139 7.91 1447134
RDL = Reportable Detection LimitQC Batch = Quality Control Batch
Maxxam ID W 8 5 4 8 9Sampling Date 2008/01/18
13:30COC Number 00553374 U n i t s TH104-14 R D L QC Batch
INORGANICS
Moisture % 16 1 1445659
Available (CaCl2) pH pH 7.95 1447134
RDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 2 of 13
Barenco IncMaxxam Job #: A806235 Client Project #: 07126Report Date: 2008/02/05 Project name:
Your P.O. #: 07126Sampler Initials:
ATLANTIC RBCA HYDROCARBONS (SOIL)
Maxxam ID W 8 5 4 8 3 W 8 5 4 8 4 W 8 5 4 8 5Sampling Date 2008/01/17 2008/01/17 2008/01/17
12:00 12:30 14:00COC Number 00553374 00553374 00553374 U n i t s TH102-14 TH102-15 TH103-8 R D L QC Batch
TPH COMPOUNDS
Benzene mg/kg ND ND ND 0.03 1446082
Toluene mg/kg ND ND ND 0.03 1446082
Ethylbenzene mg/kg ND ND 0.05 0.03 1446082
Xylene (Total) mg/kg ND ND 2.0 0.05 1446082
Aliphatic >C6-C8 mg/kg ND ND 6.7 0.2 1446082
Aliphatic >C8-C10 mg/kg ND ND 170 0.7 1446082
>C8-C10 Aromatics (-EX) mg/kg ND ND 16 0.1 1446082
Aliphatic >C10-C12 mg/kg ND ND 370 8.0 1445718
Aliphatic >C12-C16 mg/kg ND ND 920 15 1445718
Aliphatic >C16-C21 mg/kg ND ND 880 15 1445718
Aliphatic >C21-<C32 mg/kg ND ND 76 15 1445718
Aromatic >C10-C12 mg/kg ND ND 120 4.0 1445718
Aromatic >C12-C16 mg/kg ND ND 440 15 1445718
Aromatic >C16-C21 mg/kg ND ND 390 15 1445718
Aromatic >C21-<C32 mg/kg ND ND 88 15 1445718
Modified TPH (Tier 2) mg/kg ND ND 3500 20 1444752
Surrogate Recovery (%)
Isobutylbenzene - Extractable % 82 76 73 1445718
Isobutylbenzene - Volatile % 102 110 77 1446082
n-Dotriacontane - Extractable % 78 91 90 ( 1 ) 1445718
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) Fuel oil fraction.
Page 3 of 13
Barenco IncMaxxam Job #: A806235 Client Project #: 07126Report Date: 2008/02/05 Project name:
Your P.O. #: 07126Sampler Initials:
ATLANTIC RBCA HYDROCARBONS (SOIL)
Maxxam ID W 8 5 4 8 6 W 8 5 4 8 8 W 8 5 4 8 9Sampling Date 2008/01/17 2008/01/18 2008/01/18
14:30 13:00 13:30COC Number 00553374 00553374 00553374 U n i t s TH103-17 TH104-12 TH104-14 R D L QC Batch
TPH COMPOUNDS
Benzene mg/kg ND ND ND 0.03 1446082
Toluene mg/kg ND ND ND 0.03 1446082
Ethylbenzene mg/kg ND ND ND 0.03 1446082
Xylene (Total) mg/kg ND ND ND 0.05 1446082
Aliphatic >C6-C8 mg/kg ND ND ND 0.2 1446082
Aliphatic >C8-C10 mg/kg ND ND ND 0.7 1446082
>C8-C10 Aromatics (-EX) mg/kg ND ND ND 0.1 1446082
Aliphatic >C10-C12 mg/kg ND ND ND 8.0 1445718
Aliphatic >C12-C16 mg/kg ND ND ND 15 1445718
Aliphatic >C16-C21 mg/kg ND ND ND 15 1445718
Aliphatic >C21-<C32 mg/kg ND ND ND 15 1445718
Aromatic >C10-C12 mg/kg ND ND ND 4.0 1445718
Aromatic >C12-C16 mg/kg ND ND ND 15 1445718
Aromatic >C16-C21 mg/kg ND ND ND 15 1445718
Aromatic >C21-<C32 mg/kg ND ND ND 15 1445718
Modified TPH (Tier 2) mg/kg ND ND ND 20 1444752
Surrogate Recovery (%)
Isobutylbenzene - Extractable % 84 83 82 1445718
Isobutylbenzene - Volatile % 103 105 104 1446082
n-Dotriacontane - Extractable % 93 86 91 1445718
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 4 of 13
Barenco IncMaxxam Job #: A806235 Client Project #: 07126Report Date: 2008/02/05 Project name:
Your P.O. #: 07126Sampler Initials:
SEMI-VOLATILE ORGANICS BY GC-MS (SOIL)
Maxxam ID W 8 5 4 8 7Sampling Date 2008/01/18
10:00COC Number 00553374 U n i t s TH104-2 R D L QC Batch
PAHs
Acenaphthene ug/g ND 0.01 1445735
Acenaphthylene ug/g ND 0.005 1445735
Anthracene ug/g ND 0.005 1445735
Benzo(a)anthracene ug/g ND 0.01 1445735
Benzo(a)pyrene ug/g ND 0.005 1445735
Benzo(b/j)fluoranthene ug/g ND 0.005 1445735
Benzo(g,h,i)perylene ug/g ND 0.02 1445735
Benzo(k)fluoranthene ug/g ND 0.01 1445735
Chrysene ug/g ND 0.01 1445735
Dibenz(a,h)anthracene ug/g ND 0.02 1445735
Fluoranthene ug/g ND 0.005 1445735
Fluorene ug/g ND 0.005 1445735
Indeno(1,2,3-cd)pyrene ug/g ND 0.02 1445735
1-Methylnaphthalene ug/g ND 0.005 1445735
2-Methylnaphthalene ug/g ND 0.005 1445735
Naphthalene ug/g ND 0.005 1445735
Phenanthrene ug/g ND 0.005 1445735
Pyrene ug/g ND 0.005 1445735
Surrogate Recovery (%)
D10-Anthracene % 84 1445735
D14-Terphenyl (FS) % 100 1445735
D7-Quinoline % 83 1445735
D8-Acenaphthylene % 81 1445735
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 5 of 13
Barenco IncMaxxam Job #: A806235 Client Project #: 07126Report Date: 2008/02/05 Project name:
Your P.O. #: 07126Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID W 8 5 4 8 3 W 8 5 4 8 4 W 8 5 4 8 5Sampling Date 2008/01/17 2008/01/17 2008/01/17
12:00 12:30 14:00COC Number 00553374 00553374 00553374 U n i t s TH102-14 TH102-15 TH103-8 R D L QC Batch
F1 PHC and BTEX
Benzene ug/g ND ND ND 0.02 1445289
Toluene ug/g ND ND ND 0.02 1445289
Ethylbenzene ug/g ND ND ND 0.02 1445289
o-Xylene ug/g ND ND 1.1 0.02 1445289
p+m-Xylene ug/g ND ND 0.38 0.04 1445289
Total Xylenes ug/g ND ND 1.5 0.04 1445289
F1 (C6-C10) ug/g ND ND 220 10 1445289
F1 (C6-C10) - BTEX ug/g ND ND 220 10 1445289
F2-F4 PHC
F2 (C10-C16 Hydrocarbons) ug/g ND ND 1900 10 1445221
F3 (C16-C34 Hydrocarbons) ug/g ND ND 1400 10 1445221
F4 (C34-C50 Hydrocarbons) ug/g ND ND ND 10 1445221
Reached Baseline at C50 ug/g Yes Yes Yes 1445221
Surrogate Recovery (%)
1,4-Difluorobenzene % 103 107 101 1445289
4-Bromofluorobenzene % 94 100 97 1445289
D10-Ethylbenzene % 94 100 111 1445289
D4-1,2-Dichloroethane % 120 124 116 1445289
o-Terphenyl % 110 111 129 1445221
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 6 of 13
Barenco IncMaxxam Job #: A806235 Client Project #: 07126Report Date: 2008/02/05 Project name:
Your P.O. #: 07126Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID W 8 5 4 8 6 W 8 5 4 8 8 W 8 5 4 8 9Sampling Date 2008/01/17 2008/01/18 2008/01/18
14:30 13:00 13:30COC Number 00553374 00553374 00553374 U n i t s TH103-17 TH104-12 TH104-14 R D L QC Batch
F1 PHC and BTEX
Benzene ug/g ND ND ND 0.02 1445289
Toluene ug/g ND ND ND 0.02 1445289
Ethylbenzene ug/g ND ND ND 0.02 1445289
o-Xylene ug/g ND ND ND 0.02 1445289
p+m-Xylene ug/g ND ND ND 0.04 1445289
Total Xylenes ug/g ND ND ND 0.04 1445289
F1 (C6-C10) ug/g ND ND ND 10 1445289
F1 (C6-C10) - BTEX ug/g ND ND ND 10 1445289
F2-F4 PHC
F2 (C10-C16 Hydrocarbons) ug/g 16 12 ND 10 1445221
F3 (C16-C34 Hydrocarbons) ug/g 16 12 ND 10 1445221
F4 (C34-C50 Hydrocarbons) ug/g ND ND ND 10 1445221
Reached Baseline at C50 ug/g Yes Yes Yes 1445221
Surrogate Recovery (%)
1,4-Difluorobenzene % 105 103 106 1445289
4-Bromofluorobenzene % 94 94 100 1445289
D10-Ethylbenzene % 87 93 93 1445289
D4-1,2-Dichloroethane % 105 98 104 1445289
o-Terphenyl % 109 111 110 1445221
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 7 of 13
Barenco IncMaxxam Job #: A806235 Client Project #: 07126Report Date: 2008/02/05 Project name:
Your P.O. #: 07126Sampler Initials:
GENERAL COMMENTS
Note: F1BTEX - all soils were Methanol extracted on 2008/01/22
ATLANTIC RBCA HYDROCARBONS (SOIL)
VPH in Soil (PIRI2): Elevated VPH RDL(s) due to detected levels in the method blank.
Results relate only to the items tested.
Page 8 of 13
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance ReportMaxxam Job Number: MA806235
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1445221 BLZ MATRIX SPIKE o-Terphenyl 2008/01/22 97 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/22 87 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/22 87 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/22 87 % 60 - 130
Spiked Blank o-Terphenyl 2008/01/22 108 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/22 98 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/22 98 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/22 98 % 60 - 130
Method Blank o-Terphenyl 2008/01/22 106 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/22 ND, RDL=10 ug/gF3 (C16-C34 Hydrocarbons) 2008/01/22 ND, RDL=10 ug/gF4 (C34-C50 Hydrocarbons) 2008/01/22 ND, RDL=10 ug/g
RPD F2 (C10-C16 Hydrocarbons) 2008/01/22 NC % 50F3 (C16-C34 Hydrocarbons) 2008/01/22 24.5 % 50F4 (C34-C50 Hydrocarbons) 2008/01/22 11.0 % 50
1445289 DTI MATRIX SPIKE 1,4-Difluorobenzene 2008/01/22 101 % 60 - 1404-Bromofluorobenzene 2008/01/22 95 % 60 - 140D10-Ethylbenzene 2008/01/22 98 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 101 % 60 - 140Benzene 2008/01/22 89 % 60 - 140Toluene 2008/01/22 89 % 60 - 140Ethylbenzene 2008/01/22 92 % 60 - 140o-Xylene 2008/01/22 97 % 60 - 140p+m-Xylene 2008/01/22 96 % 60 - 140F1 (C6-C10) 2008/01/22 99 % 60 - 140
Spiked Blank 1,4-Difluorobenzene 2008/01/22 103 % 60 - 1404-Bromofluorobenzene 2008/01/22 97 % 60 - 140D10-Ethylbenzene 2008/01/22 86 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 101 % 60 - 140Benzene 2008/01/22 82 % 60 - 140Toluene 2008/01/22 85 % 60 - 140Ethylbenzene 2008/01/22 87 % 60 - 140o-Xylene 2008/01/22 88 % 60 - 140p+m-Xylene 2008/01/22 93 % 60 - 140F1 (C6-C10) 2008/01/22 104 % 60 - 140
Method Blank 1,4-Difluorobenzene 2008/01/22 103 % 60 - 1404-Bromofluorobenzene 2008/01/22 96 % 60 - 140D10-Ethylbenzene 2008/01/22 96 % 30 - 130D4-1,2-Dichloroethane 2008/01/22 99 % 60 - 140Benzene 2008/01/22 ND, RDL=0.02 ug/gToluene 2008/01/22 ND, RDL=0.02 ug/gEthylbenzene 2008/01/22 ND, RDL=0.02 ug/go-Xylene 2008/01/22 ND, RDL=0.02 ug/gp+m-Xylene 2008/01/22 ND, RDL=0.04 ug/gTotal Xylenes 2008/01/22 ND, RDL=0.04 ug/gF1 (C6-C10) 2008/01/22 ND, RDL=10 ug/gF1 (C6-C10) - BTEX 2008/01/22 ND, RDL=10 ug/g
RPD F1 (C6-C10) 2008/01/22 NC % 50F1 (C6-C10) - BTEX 2008/01/22 NC % 50
1445548 AC RPD [ W 8 5 4 8 7 - 0 1 ] Moisture 2008/01/23 1.0 % 501445718 KKE Spiked Blank Aliphatic >C10-C12 2008/01/25 78 % 30 - 130
Aliphatic >C12-C16 2008/01/25 78 % 30 - 130Aliphatic >C16-C21 2008/01/25 86 % 30 - 130Aliphatic >C21-<C32 2008/01/25 85 % 30 - 130Aromatic >C10-C12 2008/01/25 100 % 30 - 130
Page 9 of 13
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA806235
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1445718 KKE Spiked Blank Aromatic >C12-C16 2008/01/25 93 % 30 - 130Aromatic >C16-C21 2008/01/25 92 % 30 - 130Aromatic >C21-<C32 2008/01/25 89 % 30 - 130
Method Blank Isobutylbenzene - Extractable 2008/01/25 86 % 30 - 130n-Dotriacontane - Extractable 2008/01/25 88 % 30 - 130Aliphatic >C10-C12 2008/01/25 ND, RDL=8 mg/kgAliphatic >C12-C16 2008/01/25 ND, RDL=15 mg/kgAliphatic >C16-C21 2008/01/25 ND, RDL=15 mg/kgAliphatic >C21-<C32 2008/01/25 ND, RDL=15 mg/kgAromatic >C10-C12 2008/01/25 ND, RDL=4 mg/kgAromatic >C12-C16 2008/01/25 ND, RDL=15 mg/kgAromatic >C16-C21 2008/01/25 ND, RDL=15 mg/kgAromatic >C21-<C32 2008/01/25 ND, RDL=15 mg/kg
RPD [ W 8 5 4 8 3 - 0 2 ] Aliphatic >C10-C12 2008/01/25 NC % 50Aliphatic >C12-C16 2008/01/25 NC % 50Aliphatic >C16-C21 2008/01/25 NC % 50Aliphatic >C21-<C32 2008/01/25 NC % 50Aromatic >C10-C12 2008/01/25 NC % 50Aromatic >C12-C16 2008/01/25 NC % 50Aromatic >C16-C21 2008/01/25 NC % 50Aromatic >C21-<C32 2008/01/25 NC % 50
1445719 SPU RPD [ W 8 5 4 8 9 - 0 1 ] Moisture 2008/01/23 0.6 % 501445735 PMO MATRIX SPIKE D10-Anthracene 2008/01/23 102 % 30 - 130
D14-Terphenyl (FS) 2008/01/23 99 % 30 - 130D7-Quinoline 2008/01/23 62 % 30 - 130D8-Acenaphthylene 2008/01/23 73 % 30 - 130Acenaphthene 2008/01/23 NC % 30 - 130Acenaphthylene 2008/01/23 NC % 30 - 130Anthracene 2008/01/23 NC ( 1 ) % 30 - 130Benzo(a)anthracene 2008/01/23 NC % 30 - 130Benzo(a)pyrene 2008/01/23 NC % 30 - 130Benzo(b/j)fluoranthene 2008/01/23 NC % 30 - 130Benzo(g,h,i)perylene 2008/01/23 NC % 30 - 130Benzo(k)fluoranthene 2008/01/23 NC % 30 - 130Chrysene 2008/01/23 NC % 30 - 130Dibenz(a,h)anthracene 2008/01/23 NC % 30 - 130Fluoranthene 2008/01/23 NC % 30 - 130Fluorene 2008/01/23 NC % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/23 NC % 30 - 1301-Methylnaphthalene 2008/01/23 NC % 30 - 1302-Methylnaphthalene 2008/01/23 NC % 30 - 130Naphthalene 2008/01/23 NC % 30 - 130Phenanthrene 2008/01/23 NC % 30 - 130Pyrene 2008/01/23 NC % 30 - 130
Spiked Blank D10-Anthracene 2008/01/23 114 % 30 - 130D14-Terphenyl (FS) 2008/01/23 111 % 30 - 130D7-Quinoline 2008/01/23 87 % 30 - 130D8-Acenaphthylene 2008/01/23 86 % 30 - 130Acenaphthene 2008/01/23 117 % 30 - 130Acenaphthylene 2008/01/23 91 % 30 - 130Anthracene 2008/01/23 111 % 30 - 130Benzo(a)anthracene 2008/01/23 102 % 30 - 130Benzo(a)pyrene 2008/01/23 111 % 30 - 130Benzo(b/j)fluoranthene 2008/01/23 111 % 30 - 130Benzo(g,h,i)perylene 2008/01/23 86 % 30 - 130
Page 10 of 13
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA806235
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1445735 PMO Spiked Blank Benzo(k)fluoranthene 2008/01/23 114 % 30 - 130Chrysene 2008/01/23 102 % 30 - 130Dibenz(a,h)anthracene 2008/01/23 77 % 30 - 130Fluoranthene 2008/01/23 109 % 30 - 130Fluorene 2008/01/23 108 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/23 77 % 30 - 1301-Methylnaphthalene 2008/01/23 97 % 30 - 1302-Methylnaphthalene 2008/01/23 101 % 30 - 130Naphthalene 2008/01/23 95 % 30 - 130Phenanthrene 2008/01/23 107 % 30 - 130Pyrene 2008/01/23 103 % 30 - 130
Method Blank D10-Anthracene 2008/01/23 107 % 30 - 130D14-Terphenyl (FS) 2008/01/23 95 % 30 - 130D7-Quinoline 2008/01/23 79 % 30 - 130D8-Acenaphthylene 2008/01/23 78 % 30 - 130Acenaphthene 2008/01/23 ND, RDL=0.01 ug/gAcenaphthylene 2008/01/23 ND, RDL=0.005 ug/gAnthracene 2008/01/23 ND, RDL=0.005 ug/gBenzo(a)anthracene 2008/01/23 ND, RDL=0.01 ug/gBenzo(a)pyrene 2008/01/23 ND, RDL=0.005 ug/gBenzo(b/j)fluoranthene 2008/01/23 ND, RDL=0.005 ug/gBenzo(g,h,i)perylene 2008/01/23 ND, RDL=0.02 ug/gBenzo(k)fluoranthene 2008/01/23 ND, RDL=0.01 ug/gChrysene 2008/01/23 ND, RDL=0.01 ug/gDibenz(a,h)anthracene 2008/01/23 ND, RDL=0.02 ug/gFluoranthene 2008/01/23 ND, RDL=0.005 ug/gFluorene 2008/01/23 ND, RDL=0.005 ug/gIndeno(1,2,3-cd)pyrene 2008/01/23 ND, RDL=0.02 ug/g1-Methylnaphthalene 2008/01/23 ND, RDL=0.005 ug/g2-Methylnaphthalene 2008/01/23 ND, RDL=0.005 ug/gNaphthalene 2008/01/23 ND, RDL=0.005 ug/gPhenanthrene 2008/01/23 ND, RDL=0.005 ug/gPyrene 2008/01/23 ND, RDL=0.005 ug/g
RPD D14-Terphenyl (FS) 2008/01/23 14.8 % N/AAcenaphthene 2008/01/23 1 3 6 ( 2 ) % 50Acenaphthylene 2008/01/23 6 9 . 8 ( 2 ) % 50Anthracene 2008/01/23 1 4 5 ( 2 ) % 50Benzo(a)anthracene 2008/01/23 1 3 7 ( 2 ) % 50Benzo(a)pyrene 2008/01/23 1 3 6 ( 2 ) % 50Benzo(b/j)fluoranthene 2008/01/23 1 3 3 ( 2 ) % 50Benzo(g,h,i)perylene 2008/01/23 1 4 6 ( 2 ) % 50Benzo(k)fluoranthene 2008/01/23 1 3 2 ( 2 ) % 50Chrysene 2008/01/23 1 2 4 ( 2 ) % 50Dibenz(a,h)anthracene 2008/01/23 1 3 8 ( 2 ) % 50Fluoranthene 2008/01/23 1 3 5 ( 2 ) % 50Fluorene 2008/01/23 1 1 8 ( 2 ) % 50Indeno(1,2,3-cd)pyrene 2008/01/23 1 3 7 ( 2 ) % 501-Methylnaphthalene 2008/01/23 7 7 . 1 ( 2 ) % 502-Methylnaphthalene 2008/01/23 8 1 . 6 ( 2 ) % 50Naphthalene 2008/01/23 5 5 . 5 ( 2 ) % 50Phenanthrene 2008/01/23 1 3 0 ( 2 ) % 50Pyrene 2008/01/23 1 4 0 ( 2 ) % 50
1445905 SPU RPD Moisture 2008/01/23 1.9 % 501446082 LMU MATRIX SPIKE
[W85483-02] Isobutylbenzene - Volatile 2008/01/25 90 % 60 - 140
Page 11 of 13
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA806235
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1446082 LMU MATRIX SPIKE[W85483-02] Benzene 2008/01/25 71 % 60 - 140
Toluene 2008/01/25 88 % 60 - 140Ethylbenzene 2008/01/25 71 % 60 - 140Xylene (Total) 2008/01/25 87 % 60 - 140
Spiked Blank Isobutylbenzene - Volatile 2008/01/25 93 % 60 - 140Benzene 2008/01/25 83 % 60 - 140Toluene 2008/01/25 83 % 60 - 140Ethylbenzene 2008/01/25 84 % 60 - 140Xylene (Total) 2008/01/25 83 % 60 - 140
Method Blank Isobutylbenzene - Volatile 2008/01/25 97 % 60 - 140Benzene 2008/01/25 ND, RDL=0.03 mg/kgToluene 2008/01/25 ND, RDL=0.03 mg/kgEthylbenzene 2008/01/25 ND, RDL=0.03 mg/kgXylene (Total) 2008/01/25 ND, RDL=0.05 mg/kgAliphatic >C6-C8 2008/01/25 0.1, RDL=0.1 mg/kgAliphatic >C8-C10 2008/01/25 0.6, RDL=0.4 mg/kg>C8-C10 Aromatics (-EX) 2008/01/25 ND, RDL=0.1 mg/kg
RPD [ W 8 5 4 8 3 - 0 2 ] Benzene 2008/01/25 NC % 50Toluene 2008/01/25 NC % 50Ethylbenzene 2008/01/25 NC % 50Xylene (Total) 2008/01/25 NC % 50Aliphatic >C6-C8 2008/01/25 NC % 50Aliphatic >C8-C10 2008/01/25 NC % 50>C8-C10 Aromatics (-EX) 2008/01/25 NC % 50
ND = Not detectedN/A = Not ApplicableNC = Non-calculableRPD = Relative Percent DifferenceSPIKE = Fortified sample( 1 ) The recovery in the matrix spike was not calculated (NC). Because of the high concentration of this analyte in the parent sample, therelative difference between the spiked and unspiked concentrations is not sufficiently significant to permit a reliable recovery calculation.( 2 ) Duplicate results exceeded RPD acceptance criteria due to sample heterogeneity.
Page 12 of 13
Validation Signature Page
Maxxam Job #: A806235
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).
EWA PRANJIC, M.Sc., C.Chem, Scientific Specialist
GREG GILBERT, Scientific Specialist
MEDHAT RISKALLAH, Manager, Hydrocarbon Department
ALINA SEGAL, Manager Main Lab - Organics
SUZANA POPOVIC, Supervisor, Hydrocarbons
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
Page 13 of 13
Your Project #: MA806235 Site: 07126
Attention: SUB CONTRACTORMAXXAM ANALYTICS INC.CAMPOBELLO6740 CAMPOBELLO ROADMISSISSAUGA, ONCANADA L5N 2L8
Report Date: 2008/02/01
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: A803092Received: 2008/01/23, 8:50
Sample Matrix: Soil# Samples Received: 6
Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodCCME Hydrocarbons (F2-F4 in soil) 6 2008/01/24 2008/01/24 CAL SOP-00086 CCME PHC-CWS Aliphatic and Aromatic Fractions C10-C50 1 2008/01/22 2008/01/30 CAL SOP-00184 CCME PHC-CWS Moisture 6 N/A 2008/01/24 CAL SOP-00023 McKeague MSSMA 2.411
* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager.
HEATHER ECCLES,Email: [email protected]# (403) 291-3077
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
For Service Group specific validation please refer to the Validation Signature Page
Total cover pages: 1
Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468
Page 1 of 8
MAXXAM ANALYTICS INC.Maxxam Job #: A803092 Client Project #: MA806235Report Date: 2008/02/01 Site Reference: 07126
Sampler Initials:
CCME F2-F4 (SOIL)
Maxxam ID I 6 4 4 2 2 I 6 4 4 4 7 I 6 4 4 4 8 I 6 4 4 4 9Sampling Date 2008/01/17 2008/01/17 2008/01/17 2008/01/17 U n i t s TH102-15 THIO2-14 TH103-17 TH103-8 R D L QC Batch
(W85484-03R) (W85483-03R) (W85486-03R) (W85485-03R)
Ext. Pet. Hydrocarbon
F2 (C10-C16 Hydrocarbons) mg/kg <10 <10 <10 2800 10 2083622
F3 (C16-C34 Hydrocarbons) mg/kg <10 <10 <10 1500 10 2083622
F4 (C34-C50 Hydrocarbons) mg/kg <10 <10 <10 <10 10 2083622
Reached Baseline at C50 mg/kg Yes Yes Yes Yes N/A 2083622
Surrogate Recovery (%)
O-TERPHENYL (sur.) % 99 99 99 98 N/A 2083622
N/A = Not ApplicableRDL = Reportable Detection Limit
Maxxam ID I 6 4 4 5 0 I 6 4 4 5 1Sampling Date 2008/01/18 2008/01/18 U n i t s TH104-12 TH104-14 R D L QC Batch
(W85488-02R) (W85489-02R)
Ext. Pet. Hydrocarbon
F2 (C10-C16 Hydrocarbons) mg/kg <10 <10 10 2083622
F3 (C16-C34 Hydrocarbons) mg/kg <10 <10 10 2083622
F4 (C34-C50 Hydrocarbons) mg/kg <10 <10 10 2083622
Reached Baseline at C50 mg/kg Yes Yes N/A 2083622
Surrogate Recovery (%)
O-TERPHENYL (sur.) % 91 89 N/A 2083622
N/A = Not ApplicableRDL = Reportable Detection Limit
Page 2 of 8
MAXXAM ANALYTICS INC.Maxxam Job #: A803092 Client Project #: MA806235Report Date: 2008/02/01 Site Reference: 07126
Sampler Initials:
RESULTS OF CHEMICAL ANALYSES OF SOIL
Maxxam ID I 6 4 4 2 2 I 6 4 4 4 7 I 6 4 4 4 8 I 6 4 4 4 9Sampling Date 2008/01/17 2008/01/17 2008/01/17 2008/01/17 U n i t s TH102-15 THIO2-14 TH103-17 TH103-8 R D L QC Batch
(W85484-03R) (W85483-03R) (W85486-03R) (W85485-03R)
Physical Properties
Moisture % 19.5 15.6 17.1 4.5 0.3 2085878
RDL = Reportable Detection Limit
Maxxam ID I 6 4 4 5 0 I 6 4 4 5 1Sampling Date 2008/01/18 2008/01/18 U n i t s TH104-12 TH104-14 R D L QC Batch
(W85488-02R) (W85489-02R)
Physical Properties
Moisture % 17.0 16.2 0.3 2085878
RDL = Reportable Detection Limit
Page 3 of 8
MAXXAM ANALYTICS INC.Maxxam Job #: A803092 Client Project #: MA806235Report Date: 2008/02/01 Site Reference: 07126
Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID I 6 4 4 4 9Sampling Date 2008/01/17 U n i t s TH103-8 R D L QC Batch
(W85485-03R)
Hydrocarbons
>C10 - C12 Aliphatic mg/kg 563 5 2079711
>C10 - C12 Aromatic mg/kg 54 5 2079711
>C12 - C16 Aliphatic mg/kg 1800 10 2079711
>C12 - C16 Aromatic mg/kg 208 10 2079711
>C16 - C21 Aliphatic mg/kg 1320 10 2079711
>C16 - C21 Aromatic mg/kg 252 10 2079711
>C21 - C34 Aliphatic mg/kg 141 10 2079711
>C21 - C34 Aromatic mg/kg 161 10 2079711
>C34 Aliphatic (up to C50) mg/kg <10 10 2079711
>C34 Aromatic (up to C50) mg/kg 58 10 2079711
Surrogate Recovery (%)
O-TERPHENYL (sur.) % 101 N/A 2079711
N/A = Not ApplicableRDL = Reportable Detection Limit
Page 4 of 8
MAXXAM ANALYTICS INC.Maxxam Job #: A803092 Client Project #: MA806235Report Date: 2008/02/01 Site Reference: 07126
Sampler Initials:
CCME F2-F4 (SOIL) Comments
Sample I64422-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Sample I64447-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Sample I64448-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Sample I64450-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Sample I64451-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Results relate only to the items tested.
Page 5 of 8
MAXXAM ANALYTICS INC.Attention: SUB CONTRACTOR Client Project #: MA806235P.O. #: Site Reference: 07126
Quality Assurance ReportMaxxam Job Number: CA803092
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
2079711 LSH Calibration Check >C10 - C12 Aliphatic 2008/01/30 94 % 80 - 120>C10 - C12 Aromatic 2008/01/30 97 % 80 - 120>C12 - C16 Aliphatic 2008/01/30 95 % 80 - 120>C12 - C16 Aromatic 2008/01/30 97 % 80 - 120>C16 - C21 Aliphatic 2008/01/30 94 % 80 - 120>C16 - C21 Aromatic 2008/01/30 98 % 80 - 120>C21 - C34 Aliphatic 2008/01/30 92 % 80 - 120>C21 - C34 Aromatic 2008/01/30 95 % 80 - 120>C34 Aliphatic (up to C50) 2008/01/30 93 % 80 - 120>C34 Aromatic (up to C50) 2008/01/30 90 % 80 - 120
MATRIX SPIKE O-TERPHENYL (sur.) 2008/01/30 88 % 30 - 130>C21 - C34 Aliphatic 2008/01/30 93 % 50 - 130>C34 Aliphatic (up to C50) 2008/01/30 108 % 50 - 130
QC STANDARD >C10 - C12 Aliphatic 2008/01/30 77 % 70 - 130>C10 - C12 Aromatic 2008/01/30 95 % 70 - 130>C12 - C16 Aliphatic 2008/01/30 84 % 70 - 130>C12 - C16 Aromatic 2008/01/30 96 % 70 - 130>C16 - C21 Aliphatic 2008/01/30 87 % 70 - 130>C16 - C21 Aromatic 2008/01/30 94 % 70 - 130>C21 - C34 Aliphatic 2008/01/30 86 % 70 - 130>C21 - C34 Aromatic 2008/01/30 96 % 70 - 130>C34 Aliphatic (up to C50) 2008/01/30 88 % 70 - 130>C34 Aromatic (up to C50) 2008/01/30 129 % 70 - 130
SPIKE O-TERPHENYL (sur.) 2008/01/30 79 % 30 - 130>C10 - C12 Aliphatic 2008/01/30 71 % 70 - 130>C10 - C12 Aromatic 2008/01/30 121 % 70 - 130>C12 - C16 Aliphatic 2008/01/30 83 % 70 - 130>C12 - C16 Aromatic 2008/01/30 117 % 70 - 130>C16 - C21 Aliphatic 2008/01/30 78 % 70 - 130>C16 - C21 Aromatic 2008/01/30 72 % 70 - 130>C21 - C34 Aliphatic 2008/01/30 86 % 70 - 130>C21 - C34 Aromatic 2008/01/30 89 % 70 - 130>C34 Aliphatic (up to C50) 2008/01/30 125 % 70 - 130>C34 Aromatic (up to C50) 2008/01/30 73 % 70 - 130
BLANK O-TERPHENYL (sur.) 2008/01/30 100 % 30 - 130>C10 - C12 Aliphatic 2008/01/30 <5 mg/kg>C10 - C12 Aromatic 2008/01/30 <5 mg/kg>C12 - C16 Aliphatic 2008/01/30 <10 mg/kg>C12 - C16 Aromatic 2008/01/30 <10 mg/kg>C16 - C21 Aliphatic 2008/01/30 <10 mg/kg>C16 - C21 Aromatic 2008/01/30 <10 mg/kg>C21 - C34 Aliphatic 2008/01/30 <10 mg/kg>C21 - C34 Aromatic 2008/01/30 <10 mg/kg>C34 Aliphatic (up to C50) 2008/01/30 <10 mg/kg>C34 Aromatic (up to C50) 2008/01/30 <10 mg/kg
RPD [ I 6 4 4 4 9 - 0 1 ] >C10 - C12 Aliphatic 2008/01/30 33.1 % 40>C10 - C12 Aromatic 2008/01/30 23.9 % 40>C12 - C16 Aliphatic 2008/01/30 33.1 % 40>C12 - C16 Aromatic 2008/01/30 13.3 % 40>C16 - C21 Aliphatic 2008/01/30 30.5 % 40>C16 - C21 Aromatic 2008/01/30 5.0 % 40>C21 - C34 Aliphatic 2008/01/30 25.3 % 40>C21 - C34 Aromatic 2008/01/30 3.7 % 40>C34 Aliphatic (up to C50) 2008/01/30 NC % 40>C34 Aromatic (up to C50) 2008/01/30 15.7 % 40
Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468
Page 6 of 8
MAXXAM ANALYTICS INC.Attention: SUB CONTRACTOR Client Project #: MA806235P.O. #: Site Reference: 07126
Quality Assurance Report (Continued)Maxxam Job Number: CA803092
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
2083622 LSH Calibration Check F2 (C10-C16 Hydrocarbons) 2008/01/24 105 % 80 - 120F3 (C16-C34 Hydrocarbons) 2008/01/24 104 % 80 - 120F4 (C34-C50 Hydrocarbons) 2008/01/24 104 % 80 - 120
MATRIX SPIKE[I64449-01] O-TERPHENYL (sur.) 2008/01/24 71 % 50 - 130
F2 (C10-C16 Hydrocarbons) 2008/01/24 87 % 50 - 130F3 (C16-C34 Hydrocarbons) 2008/01/24 78 % 50 - 130F4 (C34-C50 Hydrocarbons) 2008/01/24 86 % 50 - 130
QC STANDARD F2 (C10-C16 Hydrocarbons) 2008/01/24 103 % 85 - 115F3 (C16-C34 Hydrocarbons) 2008/01/24 110 % 85 - 115F4 (C34-C50 Hydrocarbons) 2008/01/24 106 % 85 - 115
SPIKE O-TERPHENYL (sur.) 2008/01/24 82 % 50 - 130F2 (C10-C16 Hydrocarbons) 2008/01/24 89 % 80 - 120F3 (C16-C34 Hydrocarbons) 2008/01/24 94 % 80 - 120F4 (C34-C50 Hydrocarbons) 2008/01/24 120 % 80 - 120
BLANK O-TERPHENYL (sur.) 2008/01/24 99 % 50 - 130F2 (C10-C16 Hydrocarbons) 2008/01/24 <10 mg/kgF3 (C16-C34 Hydrocarbons) 2008/01/24 <10 mg/kgF4 (C34-C50 Hydrocarbons) 2008/01/24 <10 mg/kgReached Baseline at C50 2008/01/24 YES mg/kg
RPD [ I 6 4 4 4 9 - 0 1 ] F2 (C10-C16 Hydrocarbons) 2008/01/24 22.0 % 50F3 (C16-C34 Hydrocarbons) 2008/01/24 29.4 % 50F4 (C34-C50 Hydrocarbons) 2008/01/24 NC % 50Reached Baseline at C50 2008/01/24 NC % 50
2085878 RM2 RPD Moisture 2008/01/24 5.3 % 20
NC = Non-calculableRPD = Relative Percent Difference
Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468
Page 7 of 8
Validation Signature Page
Maxxam Job #: A803092
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).
LUBA SHYMUSHOVSKA,
VERONICA FALK,
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
Page 8 of 8
Your P.O. #: 07126 Your Project #: 07126 Your C.O.C. #: 00553375
Attention: Bernard ChanBarenco Inc2561 Stouffville RdPO Box 295Gormley, ONL0H 1G0
Report Date: 2008/01/29
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: A806695Received: 2008/01/22, 14:58
Sample Matrix: Soil# Samples Received: 5
Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceTEH in Soil (AA PIRI) ( 1 ) 4 N/A 2008/01/29 ATL SOP 00116 R2 Based on Atl. PIRI Petroleum Hydro. CCME F1 & BTEX in Soil 4 2008/01/23 2008/01/24 CAM SOP-00315 CCME CWS Petroleum Hydrocarbons F2-F4 in Soil 4 2008/01/25 2008/01/25 CAM SOP-00316 CCME CWS Moisture ( 1 ) 4 N/A 2008/01/25 ATL SOP 00001 R2 MOE Handbook 1983 MOISTURE 5 N/A 2008/01/25 Ont SOP-0114 MOE HANDBOOK(1983) PAH Compounds in Soil by GC/MS (SIM) 1 2008/01/24 2008/01/24 SOP - 00318 EPA 8270 pH CaCl2 EXTRACT 5 N/A 2008/01/28 Ont SOP-0067 4 5 0 0 - H + B VPH in Soil (PIRI2) ( 1 ) 4 N/A 2008/01/25 ATL SOP 00120 R2 Based on Atl. PIRI ModTPH (T2) Calc. for Soil ( 1 ) 4 N/A 2008/01/29 n/a Based on Atl. PIRI
* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.
(1) This test was performed by Bedford
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager.
SARA SAROOP, Campobello Customer serviceEmail: [email protected]# (905) 817-5700 Ext:5819
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
For Service Group specific validation please refer to the Validation Signature Page
Total cover pages: 1
Page 1 of 13
Barenco IncMaxxam Job #: A806695 Client Project #: 07126Report Date: 2008/01/29 Project name:
Your P.O. #: 07126Sampler Initials:
RESULTS OF ANALYSES OF SOIL
Maxxam ID W 8 7 3 9 0 W 8 7 3 9 1Sampling Date 2008/01/21 2008/01/21
09:00 10:00COC Number 00553375 00553375 U n i t s TH105-2 R D L QC Batch TH105-14 R D L QC Batch
INORGANICS
Moisture % 13 0.2 1447106 12 1 1446268
Available (CaCl2) pH pH 7.47 1448098 7.94 1448098
RDL = Reportable Detection LimitQC Batch = Quality Control Batch
Maxxam ID W 8 7 3 9 2 W 8 7 3 9 3 W 8 7 3 9 4Sampling Date 2008/01/21 2008/01/21 2008/01/21
10:15 12:00 12:15COC Number 00553375 00553375 00553375 U n i t s TH105-15 TH106-14 TH106-15 R D L QC Batch
INORGANICS
Moisture % 17 17 20 1 1446268
Available (CaCl2) pH pH 8.02 8.02 7.95 1448098
RDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 2 of 13
Barenco IncMaxxam Job #: A806695 Client Project #: 07126Report Date: 2008/01/29 Project name:
Your P.O. #: 07126Sampler Initials:
ATLANTIC RBCA HYDROCARBONS (SOIL)
Maxxam ID W 8 7 3 9 1 W 8 7 3 9 2 W 8 7 3 9 3Sampling Date 2008/01/21 2008/01/21 2008/01/21
10:00 10:15 12:00COC Number 00553375 00553375 00553375 U n i t s TH105-14 TH105-15 TH106-14 R D L QC Batch
TPH COMPOUNDS
Benzene mg/kg ND ND ND 0.03 1446082
Toluene mg/kg ND ND ND 0.03 1446082
Ethylbenzene mg/kg ND ND ND 0.03 1446082
Xylene (Total) mg/kg ND ND ND 0.05 1446082
Aliphatic >C6-C8 mg/kg ND ND ND 0.2 1446082
Aliphatic >C8-C10 mg/kg ND ND ND 0.7 1446082
>C8-C10 Aromatics (-EX) mg/kg ND ND ND 0.1 1446082
Aliphatic >C10-C12 mg/kg ND ND ND 8.0 1446440
Aliphatic >C12-C16 mg/kg ND ND ND 15 1446440
Aliphatic >C16-C21 mg/kg ND ND ND 15 1446440
Aliphatic >C21-<C32 mg/kg ND ND ND 15 1446440
Aromatic >C10-C12 mg/kg ND ND ND 4.0 1446440
Aromatic >C12-C16 mg/kg ND ND ND 15 1446440
Aromatic >C16-C21 mg/kg ND ND ND 15 1446440
Aromatic >C21-<C32 mg/kg ND ND ND 15 1446440
Modified TPH (Tier 2) mg/kg ND ND ND 20 1444752
Surrogate Recovery (%)
Isobutylbenzene - Extractable % 79 82 87 1446440
Isobutylbenzene - Volatile % 117 116 132 1446082
n-Dotriacontane - Extractable % 78 85 90 1446440
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 3 of 13
Barenco IncMaxxam Job #: A806695 Client Project #: 07126Report Date: 2008/01/29 Project name:
Your P.O. #: 07126Sampler Initials:
ATLANTIC RBCA HYDROCARBONS (SOIL)
Maxxam ID W 8 7 3 9 4Sampling Date 2008/01/21
12:15COC Number 00553375 U n i t s TH106-15 R D L QC Batch
TPH COMPOUNDS
Benzene mg/kg ND 0.03 1446082
Toluene mg/kg ND 0.03 1446082
Ethylbenzene mg/kg ND 0.03 1446082
Xylene (Total) mg/kg ND 0.05 1446082
Aliphatic >C6-C8 mg/kg ND 0.2 1446082
Aliphatic >C8-C10 mg/kg ND 0.7 1446082
>C8-C10 Aromatics (-EX) mg/kg ND 0.1 1446082
Aliphatic >C10-C12 mg/kg ND 8.0 1446440
Aliphatic >C12-C16 mg/kg ND 15 1446440
Aliphatic >C16-C21 mg/kg ND 15 1446440
Aliphatic >C21-<C32 mg/kg ND 15 1446440
Aromatic >C10-C12 mg/kg ND 4.0 1446440
Aromatic >C12-C16 mg/kg ND 15 1446440
Aromatic >C16-C21 mg/kg ND 15 1446440
Aromatic >C21-<C32 mg/kg ND 15 1446440
Modified TPH (Tier 2) mg/kg ND 20 1444752
Surrogate Recovery (%)
Isobutylbenzene - Extractable % 84 1446440
Isobutylbenzene - Volatile % 127 1446082
n-Dotriacontane - Extractable % 91 1446440
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 4 of 13
Barenco IncMaxxam Job #: A806695 Client Project #: 07126Report Date: 2008/01/29 Project name:
Your P.O. #: 07126Sampler Initials:
SEMI-VOLATILE ORGANICS BY GC-MS (SOIL)
Maxxam ID W 8 7 3 9 0Sampling Date 2008/01/21
09:00COC Number 00553375 U n i t s TH105-2 R D L QC Batch
PAHs
Acenaphthene ug/g ND 0.01 1446489
Acenaphthylene ug/g ND 0.005 1446489
Anthracene ug/g ND 0.005 1446489
Benzo(a)anthracene ug/g ND 0.01 1446489
Benzo(a)pyrene ug/g ND 0.005 1446489
Benzo(b/j)fluoranthene ug/g ND 0.005 1446489
Benzo(g,h,i)perylene ug/g ND 0.02 1446489
Benzo(k)fluoranthene ug/g ND 0.01 1446489
Chrysene ug/g ND 0.01 1446489
Dibenz(a,h)anthracene ug/g ND 0.02 1446489
Fluoranthene ug/g ND 0.005 1446489
Fluorene ug/g ND 0.005 1446489
Indeno(1,2,3-cd)pyrene ug/g ND 0.02 1446489
1-Methylnaphthalene ug/g ND 0.005 1446489
2-Methylnaphthalene ug/g ND 0.005 1446489
Naphthalene ug/g ND 0.005 1446489
Phenanthrene ug/g ND 0.005 1446489
Pyrene ug/g ND 0.005 1446489
Surrogate Recovery (%)
D10-Anthracene % 87 1446489
D14-Terphenyl (FS) % 87 1446489
D7-Quinoline % 58 1446489
D8-Acenaphthylene % 64 1446489
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 5 of 13
Barenco IncMaxxam Job #: A806695 Client Project #: 07126Report Date: 2008/01/29 Project name:
Your P.O. #: 07126Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID W 8 7 3 9 1 W 8 7 3 9 2 W 8 7 3 9 3Sampling Date 2008/01/21 2008/01/21 2008/01/21
10:00 10:15 12:00COC Number 00553375 00553375 00553375 U n i t s TH105-14 TH105-15 TH106-14 R D L QC Batch
F1 PHC and BTEX
Benzene ug/g ND ND ND 0.02 1446054
Toluene ug/g ND ND ND 0.02 1446054
Ethylbenzene ug/g ND ND ND 0.02 1446054
o-Xylene ug/g ND ND ND 0.02 1446054
p+m-Xylene ug/g ND ND ND 0.04 1446054
Total Xylenes ug/g ND ND ND 0.04 1446054
F1 (C6-C10) ug/g ND ND ND 10 1446054
F1 (C6-C10) - BTEX ug/g ND ND ND 10 1446054
F2-F4 PHC
F2 (C10-C16 Hydrocarbons) ug/g ND ND ND 10 1447307
F3 (C16-C34 Hydrocarbons) ug/g ND ND ND 10 1447307
F4 (C34-C50 Hydrocarbons) ug/g ND ND ND 10 1447307
Reached Baseline at C50 ug/g Yes Yes Yes 1447307
Surrogate Recovery (%)
1,4-Difluorobenzene % 99 100 99 1446054
4-Bromofluorobenzene % 104 99 96 1446054
D10-Ethylbenzene % 88 89 85 1446054
D4-1,2-Dichloroethane % 100 96 91 1446054
o-Terphenyl % 112 106 103 1447307
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 6 of 13
Barenco IncMaxxam Job #: A806695 Client Project #: 07126Report Date: 2008/01/29 Project name:
Your P.O. #: 07126Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID W 8 7 3 9 4Sampling Date 2008/01/21
12:15COC Number 00553375 U n i t s TH106-15 R D L QC Batch
F1 PHC and BTEX
Benzene ug/g ND 0.02 1446054
Toluene ug/g ND 0.02 1446054
Ethylbenzene ug/g ND 0.02 1446054
o-Xylene ug/g ND 0.02 1446054
p+m-Xylene ug/g ND 0.04 1446054
Total Xylenes ug/g ND 0.04 1446054
F1 (C6-C10) ug/g ND 10 1446054
F1 (C6-C10) - BTEX ug/g ND 10 1446054
F2-F4 PHC
F2 (C10-C16 Hydrocarbons) ug/g ND 10 1447307
F3 (C16-C34 Hydrocarbons) ug/g ND 10 1447307
F4 (C34-C50 Hydrocarbons) ug/g ND 10 1447307
Reached Baseline at C50 ug/g Yes 1447307
Surrogate Recovery (%)
1,4-Difluorobenzene % 103 1446054
4-Bromofluorobenzene % 101 1446054
D10-Ethylbenzene % 92 1446054
D4-1,2-Dichloroethane % 94 1446054
o-Terphenyl % 111 1447307
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 7 of 13
Barenco IncMaxxam Job #: A806695 Client Project #: 07126Report Date: 2008/01/29 Project name:
Your P.O. #: 07126Sampler Initials:
GENERAL COMMENTS
Note: F1BTEX - all soils were Methanol extracted on 2008/01/23
ATLANTIC RBCA HYDROCARBONS (SOIL)
VPH in Soil (PIRI2): Elevated VPH RDL(s) due to detected levels in the method blank.
Results relate only to the items tested.
Page 8 of 13
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance ReportMaxxam Job Number: MA806695
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1446054 GBA MATRIX SPIKE 1,4-Difluorobenzene 2008/01/24 96 % 60 - 1404-Bromofluorobenzene 2008/01/24 106 % 60 - 140D10-Ethylbenzene 2008/01/24 96 % 30 - 130D4-1,2-Dichloroethane 2008/01/24 94 % 60 - 140Benzene 2008/01/24 85 % 60 - 140Toluene 2008/01/24 98 % 60 - 140Ethylbenzene 2008/01/24 94 % 60 - 140o-Xylene 2008/01/24 90 % 60 - 140p+m-Xylene 2008/01/24 97 % 60 - 140F1 (C6-C10) 2008/01/24 96 % 60 - 140
Spiked Blank 1,4-Difluorobenzene 2008/01/24 96 % 60 - 1404-Bromofluorobenzene 2008/01/24 105 % 60 - 140D10-Ethylbenzene 2008/01/24 90 % 30 - 130D4-1,2-Dichloroethane 2008/01/24 92 % 60 - 140Benzene 2008/01/24 75 % 60 - 140Toluene 2008/01/24 89 % 60 - 140Ethylbenzene 2008/01/24 87 % 60 - 140o-Xylene 2008/01/24 83 % 60 - 140p+m-Xylene 2008/01/24 90 % 60 - 140F1 (C6-C10) 2008/01/24 94 % 60 - 140
Method Blank 1,4-Difluorobenzene 2008/01/24 101 % 60 - 1404-Bromofluorobenzene 2008/01/24 100 % 60 - 140D10-Ethylbenzene 2008/01/24 93 % 30 - 130D4-1,2-Dichloroethane 2008/01/24 95 % 60 - 140Benzene 2008/01/24 ND, RDL=0.02 ug/gToluene 2008/01/24 ND, RDL=0.02 ug/gEthylbenzene 2008/01/24 ND, RDL=0.02 ug/go-Xylene 2008/01/24 ND, RDL=0.02 ug/gp+m-Xylene 2008/01/24 ND, RDL=0.04 ug/gTotal Xylenes 2008/01/24 ND, RDL=0.04 ug/gF1 (C6-C10) 2008/01/24 ND, RDL=10 ug/gF1 (C6-C10) - BTEX 2008/01/24 ND, RDL=10 ug/g
RPD Benzene 2008/01/24 NC % 50Toluene 2008/01/24 NC % 50Ethylbenzene 2008/01/24 NC % 50o-Xylene 2008/01/24 NC % 50p+m-Xylene 2008/01/24 NC % 50Total Xylenes 2008/01/24 NC % 50F1 (C6-C10) 2008/01/24 NC % 50F1 (C6-C10) - BTEX 2008/01/24 NC % 50
1446082 LMU MATRIX SPIKE Isobutylbenzene - Volatile 2008/01/25 90 % 60 - 140Benzene 2008/01/25 71 % 60 - 140Toluene 2008/01/25 88 % 60 - 140Ethylbenzene 2008/01/25 71 % 60 - 140Xylene (Total) 2008/01/25 87 % 60 - 140
Spiked Blank Isobutylbenzene - Volatile 2008/01/25 93 % 60 - 140Benzene 2008/01/25 83 % 60 - 140Toluene 2008/01/25 83 % 60 - 140Ethylbenzene 2008/01/25 84 % 60 - 140Xylene (Total) 2008/01/25 83 % 60 - 140
Method Blank Isobutylbenzene - Volatile 2008/01/25 97 % 60 - 140Benzene 2008/01/25 ND, RDL=0.03 mg/kgToluene 2008/01/25 ND, RDL=0.03 mg/kgEthylbenzene 2008/01/25 ND, RDL=0.03 mg/kgXylene (Total) 2008/01/25 ND, RDL=0.05 mg/kg
Page 9 of 13
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA806695
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1446082 LMU Method Blank Aliphatic >C6-C8 2008/01/25 0.1, RDL=0.1 mg/kgAliphatic >C8-C10 2008/01/25 0.6, RDL=0.4 mg/kg>C8-C10 Aromatics (-EX) 2008/01/25 ND, RDL=0.1 mg/kg
RPD Benzene 2008/01/25 NC % 50Toluene 2008/01/25 NC % 50Ethylbenzene 2008/01/25 NC % 50Xylene (Total) 2008/01/25 NC % 50Aliphatic >C6-C8 2008/01/25 NC % 50Aliphatic >C8-C10 2008/01/25 NC % 50>C8-C10 Aromatics (-EX) 2008/01/25 NC % 50
1446440 KKE Spiked Blank Aliphatic >C10-C12 2008/01/29 75 % 30 - 130Aliphatic >C12-C16 2008/01/29 75 % 30 - 130Aliphatic >C16-C21 2008/01/29 81 % 30 - 130Aliphatic >C21-<C32 2008/01/29 83 % 30 - 130Aromatic >C10-C12 2008/01/29 105 % 30 - 130Aromatic >C12-C16 2008/01/29 98 % 30 - 130Aromatic >C16-C21 2008/01/29 94 % 30 - 130Aromatic >C21-<C32 2008/01/29 94 % 30 - 130
Method Blank Isobutylbenzene - Extractable 2008/01/29 87 % 30 - 130n-Dotriacontane - Extractable 2008/01/29 83 % 30 - 130Aliphatic >C10-C12 2008/01/29 ND, RDL=8 mg/kgAliphatic >C12-C16 2008/01/29 ND, RDL=15 mg/kgAliphatic >C16-C21 2008/01/29 ND, RDL=15 mg/kgAliphatic >C21-<C32 2008/01/29 ND, RDL=15 mg/kgAromatic >C10-C12 2008/01/29 ND, RDL=4 mg/kgAromatic >C12-C16 2008/01/29 ND, RDL=15 mg/kgAromatic >C16-C21 2008/01/29 ND, RDL=15 mg/kgAromatic >C21-<C32 2008/01/29 ND, RDL=15 mg/kg
RPD Aliphatic >C10-C12 2008/01/29 NC % 50Aliphatic >C12-C16 2008/01/29 NC % 50Aliphatic >C16-C21 2008/01/29 NC % 50Aliphatic >C21-<C32 2008/01/29 NC % 50Aromatic >C10-C12 2008/01/29 4.6 % 50Aromatic >C12-C16 2008/01/29 NC % 50Aromatic >C16-C21 2008/01/29 NC % 50Aromatic >C21-<C32 2008/01/29 NC % 50
1446489 PMO MATRIX SPIKE D10-Anthracene 2008/01/24 84 % 30 - 130D14-Terphenyl (FS) 2008/01/24 87 % 30 - 130D7-Quinoline 2008/01/24 69 % 30 - 130D8-Acenaphthylene 2008/01/24 79 % 30 - 130Acenaphthene 2008/01/24 86 % 30 - 130Acenaphthylene 2008/01/24 88 % 30 - 130Anthracene 2008/01/24 86 % 30 - 130Benzo(a)anthracene 2008/01/24 88 % 30 - 130Benzo(a)pyrene 2008/01/24 86 % 30 - 130Benzo(b/j)fluoranthene 2008/01/24 84 % 30 - 130Benzo(g,h,i)perylene 2008/01/24 87 % 30 - 130Benzo(k)fluoranthene 2008/01/24 92 % 30 - 130Chrysene 2008/01/24 85 % 30 - 130Dibenz(a,h)anthracene 2008/01/24 86 % 30 - 130Fluoranthene 2008/01/24 93 % 30 - 130Fluorene 2008/01/24 83 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/24 77 % 30 - 1301-Methylnaphthalene 2008/01/24 83 % 30 - 1302-Methylnaphthalene 2008/01/24 88 % 30 - 130
Page 10 of 13
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA806695
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1446489 PMO MATRIX SPIKE Naphthalene 2008/01/24 80 % 30 - 130Phenanthrene 2008/01/24 88 % 30 - 130Pyrene 2008/01/24 82 % 30 - 130
Spiked Blank D10-Anthracene 2008/01/24 102 % 30 - 130D14-Terphenyl (FS) 2008/01/24 109 % 30 - 130D7-Quinoline 2008/01/24 90 % 30 - 130D8-Acenaphthylene 2008/01/24 94 % 30 - 130Acenaphthene 2008/01/24 98 % 30 - 130Acenaphthylene 2008/01/24 105 % 30 - 130Anthracene 2008/01/24 111 % 30 - 130Benzo(a)anthracene 2008/01/24 99 % 30 - 130Benzo(a)pyrene 2008/01/24 118 % 30 - 130Benzo(b/j)fluoranthene 2008/01/24 108 % 30 - 130Benzo(g,h,i)perylene 2008/01/24 113 % 30 - 130Benzo(k)fluoranthene 2008/01/24 116 % 30 - 130Chrysene 2008/01/24 104 % 30 - 130Dibenz(a,h)anthracene 2008/01/24 114 % 30 - 130Fluoranthene 2008/01/24 113 % 30 - 130Fluorene 2008/01/24 99 % 30 - 130Indeno(1,2,3-cd)pyrene 2008/01/24 104 % 30 - 1301-Methylnaphthalene 2008/01/24 97 % 30 - 1302-Methylnaphthalene 2008/01/24 100 % 30 - 130Naphthalene 2008/01/24 99 % 30 - 130Phenanthrene 2008/01/24 106 % 30 - 130Pyrene 2008/01/24 105 % 30 - 130
Method Blank D10-Anthracene 2008/01/24 101 % 30 - 130D14-Terphenyl (FS) 2008/01/24 102 % 30 - 130D7-Quinoline 2008/01/24 90 % 30 - 130D8-Acenaphthylene 2008/01/24 92 % 30 - 130Acenaphthene 2008/01/24 ND, RDL=0.01 ug/gAcenaphthylene 2008/01/24 ND, RDL=0.005 ug/gAnthracene 2008/01/24 ND, RDL=0.005 ug/gBenzo(a)anthracene 2008/01/24 ND, RDL=0.01 ug/gBenzo(a)pyrene 2008/01/24 ND, RDL=0.005 ug/gBenzo(b/j)fluoranthene 2008/01/24 ND, RDL=0.005 ug/gBenzo(g,h,i)perylene 2008/01/24 ND, RDL=0.02 ug/gBenzo(k)fluoranthene 2008/01/24 ND, RDL=0.01 ug/gChrysene 2008/01/24 ND, RDL=0.01 ug/gDibenz(a,h)anthracene 2008/01/24 ND, RDL=0.02 ug/gFluoranthene 2008/01/24 ND, RDL=0.005 ug/gFluorene 2008/01/24 ND, RDL=0.005 ug/gIndeno(1,2,3-cd)pyrene 2008/01/24 ND, RDL=0.02 ug/g1-Methylnaphthalene 2008/01/24 ND, RDL=0.005 ug/g2-Methylnaphthalene 2008/01/24 ND, RDL=0.005 ug/gNaphthalene 2008/01/24 ND, RDL=0.005 ug/gPhenanthrene 2008/01/24 ND, RDL=0.005 ug/gPyrene 2008/01/24 ND, RDL=0.005 ug/g
RPD D14-Terphenyl (FS) 2008/01/24 5.5 % N/AAcenaphthene 2008/01/24 NC % 50Acenaphthylene 2008/01/24 NC % 50Anthracene 2008/01/24 NC % 50Benzo(a)anthracene 2008/01/24 NC % 50Benzo(a)pyrene 2008/01/24 NC % 50Benzo(b/j)fluoranthene 2008/01/24 NC % 50Benzo(g,h,i)perylene 2008/01/24 NC % 50
Page 11 of 13
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA806695
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1446489 PMO RPD Benzo(k)fluoranthene 2008/01/24 NC % 50Chrysene 2008/01/24 NC % 50Dibenz(a,h)anthracene 2008/01/24 NC % 50Fluoranthene 2008/01/24 NC % 50Fluorene 2008/01/24 NC % 50Indeno(1,2,3-cd)pyrene 2008/01/24 NC % 501-Methylnaphthalene 2008/01/24 NC % 502-Methylnaphthalene 2008/01/24 NC % 50Naphthalene 2008/01/24 NC % 50Phenanthrene 2008/01/24 NC % 50Pyrene 2008/01/24 NC % 50
1447106 MYG RPD Moisture 2008/01/25 5.9 % 501447307 BWW MATRIX SPIKE o-Terphenyl 2008/01/25 106 % 30 - 130
F2 (C10-C16 Hydrocarbons) 2008/01/25 104 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/25 104 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/25 104 % 60 - 130
Spiked Blank o-Terphenyl 2008/01/25 107 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/25 91 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/25 91 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/25 91 % 60 - 130
Method Blank o-Terphenyl 2008/01/25 103 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/25 ND, RDL=10 ug/gF3 (C16-C34 Hydrocarbons) 2008/01/25 ND, RDL=10 ug/gF4 (C34-C50 Hydrocarbons) 2008/01/25 ND, RDL=10 ug/g
RPD F2 (C10-C16 Hydrocarbons) 2008/01/25 NC % 50F3 (C16-C34 Hydrocarbons) 2008/01/25 NC % 50F4 (C34-C50 Hydrocarbons) 2008/01/25 NC % 50
ND = Not detectedN/A = Not ApplicableNC = Non-calculableRPD = Relative Percent DifferenceSPIKE = Fortified sample
Page 12 of 13
Validation Signature Page
Maxxam Job #: A806695
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).
BRAD NEWMAN, Scientific Specialist
GREG GILBERT, Scientific Specialist
MEDHAT RISKALLAH, Manager, Hydrocarbon Department
SUZANA POPOVIC, Supervisor, Hydrocarbons
TIM MUNSHAW, Lab Manager
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
Page 13 of 13
Your Project #: MA806695 Site: 07126
Attention: SUB CONTRACTORMAXXAM ANALYTICS INC.CAMPOBELLO6740 CAMPOBELLO ROADMISSISSAUGA, ONCANADA L5N 2L8
Report Date: 2008/01/28
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: A803322Received: 2008/01/24, 8:40
Sample Matrix: Soil# Samples Received: 4
Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodCCME Hydrocarbons (F2-F4 in soil) 4 2008/01/24 2008/01/24 CAL SOP-00086 CCME PHC-CWS Moisture 4 N/A 2008/01/25 CAL SOP-00023 McKeague MSSMA 2.411
* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager.
HEATHER ECCLES,Email: [email protected]# (403) 291-3077
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
For Service Group specific validation please refer to the Validation Signature Page
Total cover pages: 1
Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468
Page 1 of 6
MAXXAM ANALYTICS INC.Maxxam Job #: A803322 Client Project #: MA806695Report Date: 2008/01/28 Site Reference: 07126
Sampler Initials:
CCME F2-F4 (SOIL)
Maxxam ID I 6 5 5 0 6 I 6 5 5 1 2 I 6 5 5 1 3 I 6 5 5 1 4Sampling Date 2008/01/21 2008/01/21 2008/01/21 2008/01/21 U n i t s TH106-14 TH105-15 TH105-14 TH106-15 R D L QC Batch
(W87393-01R) (W87392-01R) (W87391-01R) (W87394-01R)
Ext. Pet. Hydrocarbon
F2 (C10-C16 Hydrocarbons) mg/kg <10 <10 <10 <10 10 2086431
F3 (C16-C34 Hydrocarbons) mg/kg <10 <10 <10 <10 10 2086431
F4 (C34-C50 Hydrocarbons) mg/kg <10 <10 <10 <10 10 2086431
Reached Baseline at C50 mg/kg Yes Yes Yes Yes N/A 2086431
Surrogate Recovery (%)
O-TERPHENYL (sur.) % 94 92 91 93 N/A 2086431
N/A = Not ApplicableRDL = Reportable Detection Limit
Page 2 of 6
MAXXAM ANALYTICS INC.Maxxam Job #: A803322 Client Project #: MA806695Report Date: 2008/01/28 Site Reference: 07126
Sampler Initials:
RESULTS OF CHEMICAL ANALYSES OF SOIL
Maxxam ID I 6 5 5 0 6 I 6 5 5 1 2 I 6 5 5 1 3 I 6 5 5 1 4Sampling Date 2008/01/21 2008/01/21 2008/01/21 2008/01/21 U n i t s TH106-14 TH105-15 TH105-14 TH106-15 R D L QC Batch
(W87393-01R) (W87392-01R) (W87391-01R) (W87394-01R)
Physical Properties
Moisture % 16.1 15.7 8.4 16.1 0.3 2088155
RDL = Reportable Detection Limit
Page 3 of 6
MAXXAM ANALYTICS INC.Maxxam Job #: A803322 Client Project #: MA806695Report Date: 2008/01/28 Site Reference: 07126
Sampler Initials:
CCME F2-F4 (SOIL) Comments
Sample I65506-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Sample I65512-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Sample I65513-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Sample I65514-01 CCME Hydrocarbons (F2-F4 in soil): Fractionation not needed because F2-F4 are < DL.
Results relate only to the items tested.
Page 4 of 6
MAXXAM ANALYTICS INC.Attention: SUB CONTRACTOR Client Project #: MA806695P.O. #: Site Reference: 07126
Quality Assurance ReportMaxxam Job Number: CA803322
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
2086431 LSH Calibration Check F2 (C10-C16 Hydrocarbons) 2008/01/24 86 % 80 - 120F3 (C16-C34 Hydrocarbons) 2008/01/24 85 % 80 - 120F4 (C34-C50 Hydrocarbons) 2008/01/24 91 % 80 - 120
MATRIX SPIKE[I65506-01] O-TERPHENYL (sur.) 2008/01/24 82 % 50 - 130
F2 (C10-C16 Hydrocarbons) 2008/01/24 89 % 50 - 130F3 (C16-C34 Hydrocarbons) 2008/01/24 93 % 50 - 130F4 (C34-C50 Hydrocarbons) 2008/01/24 123 % 50 - 130
QC STANDARD F2 (C10-C16 Hydrocarbons) 2008/01/24 97 % 85 - 115F3 (C16-C34 Hydrocarbons) 2008/01/24 102 % 85 - 115F4 (C34-C50 Hydrocarbons) 2008/01/24 91 % 85 - 115
SPIKE O-TERPHENYL (sur.) 2008/01/24 82 % 50 - 130F2 (C10-C16 Hydrocarbons) 2008/01/24 88 % 50 - 130F3 (C16-C34 Hydrocarbons) 2008/01/24 93 % 50 - 130F4 (C34-C50 Hydrocarbons) 2008/01/24 118 % 50 - 130
BLANK O-TERPHENYL (sur.) 2008/01/24 90 % 50 - 130F2 (C10-C16 Hydrocarbons) 2008/01/24 <10 mg/kgF3 (C16-C34 Hydrocarbons) 2008/01/24 <10 mg/kgF4 (C34-C50 Hydrocarbons) 2008/01/24 <10 mg/kgReached Baseline at C50 2008/01/24 YES mg/kg
RPD [ I 6 5 5 0 6 - 0 1 ] F2 (C10-C16 Hydrocarbons) 2008/01/24 NC % 50F3 (C16-C34 Hydrocarbons) 2008/01/24 NC % 50F4 (C34-C50 Hydrocarbons) 2008/01/24 NC % 50Reached Baseline at C50 2008/01/24 NC % 50
2088155 RM2 RPD Moisture 2008/01/25 2.3 % 20
NC = Non-calculableRPD = Relative Percent Difference
Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 FAX(403) 291-9468
Page 5 of 6
Validation Signature Page
Maxxam Job #: A803322
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).
LUBA SHYMUSHOVSKA,
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
Page 6 of 6
Your P.O. #: 07126 Your Project #: 07126 Your C.O.C. #: 00553384
Attention: Bernard ChanBarenco Inc2561 Stouffville RdPO Box 295Gormley, ONL0H 1G0
Report Date: 2008/02/07
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: A808263Received: 2008/01/25, 14:52
Sample Matrix: Water# Samples Received: 6
Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceTEH in Water (AA PIRI) ( 1 ) 6 N/A 2008/02/07 ATL SOP 00116 R2 Based on Atl. PIRI Petroleum Hydro. CCME F1 & BTEX in Water 6 N/A 2008/01/29 CAM SOP-00315 CCME CWS Petroleum Hydrocarbons F2-F4 in Water 6 2008/01/29 2008/01/29 CAM SOP-00316 CCME Hydrocarbons VPH in Water (PIRI2) ( 1 ) 6 N/A 2008/02/04 ATL SOP 00120 R2 Based on Atl. PIRI ModTPH (T2) Calc. for Water ( 1 ) 6 N/A 2008/02/07 Based on Atl. PIRI
* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.
(1) This test was performed by Bedford
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager.
SARA SAROOP, Campobello Customer serviceEmail: [email protected]# (905) 817-5700 Ext:5819
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
For Service Group specific validation please refer to the Validation Signature Page
Total cover pages: 1
Page 1 of 10
Barenco IncMaxxam Job #: A808263 Client Project #: 07126Report Date: 2008/02/07 Project name:
Your P.O. #: 07126Sampler Initials:
ATLANTIC RBCA HYDROCARBONS (WATER)
Maxxam ID W 9 3 6 1 5 W 9 3 6 1 6 W 9 3 6 1 7Sampling Date 2008/01/24 2008/01/24 2008/01/24
11:00 11:30 12:00COC Number 00553384 00553384 00553384 U n i t s TH 101 TH 102 TH 103 R D L QC Batch
TPH COMPOUNDS
Benzene mg/L ND ND ND 0.001 1451710
Toluene mg/L ND ND ND 0.001 1451710
Ethylbenzene mg/L ND ND ND 0.001 1451710
Xylene (Total) mg/L ND ND ND 0.002 1451710
Aliphatic >C6-C8 mg/L ND ND ND 0.01 1451710
Aliphatic >C8-C10 mg/L 0.01 ND 0.01 0.01 1451710
>C8-C10 Aromatics (-EX) mg/L ND ND ND 0.01 1451710
Aliphatic >C10-C12 mg/L 0.45 ND 0.07 0.01 1449839
Aliphatic >C12-C16 mg/L 1.2 ND 0.15 0.05 1449839
Aliphatic >C16-C21 mg/L 1.2 ND 0.18 0.05 1449839
Aliphatic >C21-<C32 mg/L 0.2 ND ND 0.1 1449839
Aromatic >C10-C12 mg/L 0.15 ND 0.01 0.01 1449839
Aromatic >C12-C16 mg/L 0.50 ND 0.05 0.05 1449839
Aromatic >C16-C21 mg/L 0.64 0.06 0.14 0.05 1449839
Aromatic >C21-<C32 mg/L 0.3 ND ND 0.1 1449839
Modified TPH (Tier 2) mg/L 4.6 ND 0.6 0.1 1449033
Surrogate Recovery (%)
Isobutylbenzene - Extractable % 47 63 59 1449839
Isobutylbenzene - Volatile % 116 113 114 1451710
n-Dotriacontane - Extractable % 58 ( 1 ) 85 ( 2 ) 83 ( 3 ) 1449839
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) Fuel oil fraction. TEH sample contained sediment. TEH surrogate(s) not within acceptance limits.Insufficient sample to repeat.( 2 ) TEH sample contained sediment.( 3 ) Weathered fuel oil fraction. One product in the fuel/lube oil range. TEH sample contained sediment. TEHsurrogate(s) not within acceptance limits. Insufficient sample to repeat.
Page 2 of 10
Barenco IncMaxxam Job #: A808263 Client Project #: 07126Report Date: 2008/02/07 Project name:
Your P.O. #: 07126Sampler Initials:
ATLANTIC RBCA HYDROCARBONS (WATER)
Maxxam ID W 9 3 6 1 8 W 9 3 6 1 9Sampling Date 2008/01/24 2008/01/24
12:30 13:00COC Number 00553384 00553384 U n i t s TH 104 TH 105 R D L QC Batch
TPH COMPOUNDS
Benzene mg/L ND ND 0.001 1451710
Toluene mg/L ND ND 0.001 1451710
Ethylbenzene mg/L ND ND 0.001 1451710
Xylene (Total) mg/L ND ND 0.002 1451710
Aliphatic >C6-C8 mg/L ND ND 0.01 1451710
Aliphatic >C8-C10 mg/L ND ND 0.01 1451710
>C8-C10 Aromatics (-EX) mg/L ND ND 0.01 1451710
Aliphatic >C10-C12 mg/L ND ND 0.01 1449839
Aliphatic >C12-C16 mg/L ND ND 0.05 1449839
Aliphatic >C16-C21 mg/L ND ND 0.05 1449839
Aliphatic >C21-<C32 mg/L ND ND 0.1 1449839
Aromatic >C10-C12 mg/L 0.01 ND 0.01 1449839
Aromatic >C12-C16 mg/L ND ND 0.05 1449839
Aromatic >C16-C21 mg/L 0.17 ND 0.05 1449839
Aromatic >C21-<C32 mg/L 0.1 ND 0.1 1449839
Modified TPH (Tier 2) mg/L 0.3 ND 0.1 1449033
Surrogate Recovery (%)
Isobutylbenzene - Extractable % 66 54 1449839
Isobutylbenzene - Volatile % 116 116 ( 1 ) 1451710
n-Dotriacontane - Extractable % 92 ( 2 ) 79 ( 3 ) 1449839
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) VPH analysis performed on previously opened vial.( 2 ) One product in the fuel/lube oil range. TEH sample contained sediment.( 3 ) TEH sample decanted due to sediment. TEH surrogate(s) not within acceptance limits.Insufficient sample to repeat.
Page 3 of 10
Barenco IncMaxxam Job #: A808263 Client Project #: 07126Report Date: 2008/02/07 Project name:
Your P.O. #: 07126Sampler Initials:
ATLANTIC RBCA HYDROCARBONS (WATER)
Maxxam ID W 9 3 6 2 0Sampling Date 2008/01/24
13:30COC Number 00553384 U n i t s TH 106 R D L QC Batch
TPH COMPOUNDS
Benzene mg/L ND 0.001 1451710
Toluene mg/L ND 0.001 1451710
Ethylbenzene mg/L ND 0.001 1451710
Xylene (Total) mg/L ND 0.002 1451710
Aliphatic >C6-C8 mg/L ND 0.01 1451710
Aliphatic >C8-C10 mg/L ND 0.01 1451710
>C8-C10 Aromatics (-EX) mg/L ND 0.01 1451710
Aliphatic >C10-C12 mg/L 0.03 0.01 1449839
Aliphatic >C12-C16 mg/L 0.30 0.06 1449839
Aliphatic >C16-C21 mg/L 0.36 0.06 1449839
Aliphatic >C21-<C32 mg/L 0.1 0.1 1449839
Aromatic >C10-C12 mg/L 0.03 0.01 1449839
Aromatic >C12-C16 mg/L 0.33 0.06 1449839
Aromatic >C16-C21 mg/L 0.33 0.06 1449839
Aromatic >C21-<C32 mg/L 0.1 0.1 1449839
Modified TPH (Tier 2) mg/L 1.5 0.1 1449033
Surrogate Recovery (%)
Isobutylbenzene - Extractable % 77 1449839
Isobutylbenzene - Volatile % 121 ( 1 ) 1451710
n-Dotriacontane - Extractable % 76 ( 2 ) 1449839
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch( 1 ) VPH analysis performed on previously opened vial.( 2 ) One product in the fuel/lube oil range. TEH sample containedsediment.
Page 4 of 10
Barenco IncMaxxam Job #: A808263 Client Project #: 07126Report Date: 2008/02/07 Project name:
Your P.O. #: 07126Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID W 9 3 6 1 5 W 9 3 6 1 6 W 9 3 6 1 7Sampling Date 2008/01/24 2008/01/24 2008/01/24
11:00 11:30 12:00COC Number 00553384 00553384 00553384 U n i t s TH 101 TH 102 TH 103 R D L QC Batch
F1 PHC and BTEX
Benzene ug/L ND ND ND 0.2 1449242
Toluene ug/L ND ND ND 0.2 1449242
Ethylbenzene ug/L ND ND ND 0.2 1449242
o-Xylene ug/L 1.0 ND ND 0.2 1449242
p+m-Xylene ug/L ND ND ND 0.4 1449242
Total Xylenes ug/L 1.0 ND ND 0.4 1449242
F1 (C6-C10) ug/L ND ND ND 100 1449242
F1 (C6-C10) - BTEX ug/L ND ND ND 100 1449242
F2-F4 PHC
F2 (C10-C16 Hydrocarbons) ug/L 130 ND ND 100 1449135
F3 (C16-C34 Hydrocarbons) ug/L 130 ND ND 100 1449135
F4 (C34-C50 Hydrocarbons) ug/L ND ND ND 100 1449135
Reached Baseline at C50 ug/L Yes Yes Yes 1449135
Surrogate Recovery (%)
1,4-Difluorobenzene % 102 101 100 1449242
4-Bromofluorobenzene % 106 81 92 1449242
D10-Ethylbenzene % 105 96 99 1449242
D4-1,2-Dichloroethane % 104 124 122 1449242
o-Terphenyl % 106 106 106 1449135
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 5 of 10
Barenco IncMaxxam Job #: A808263 Client Project #: 07126Report Date: 2008/02/07 Project name:
Your P.O. #: 07126Sampler Initials:
PETROLEUM HYDROCARBONS (CCME)
Maxxam ID W 9 3 6 1 8 W 9 3 6 1 9 W 9 3 6 2 0Sampling Date 2008/01/24 2008/01/24 2008/01/24
12:30 13:00 13:30COC Number 00553384 00553384 00553384 U n i t s TH 104 TH 105 TH 106 R D L QC Batch
F1 PHC and BTEX
Benzene ug/L ND ND ND 0.2 1449242
Toluene ug/L ND ND ND 0.2 1449242
Ethylbenzene ug/L ND ND ND 0.2 1449242
o-Xylene ug/L ND ND ND 0.2 1449242
p+m-Xylene ug/L ND ND ND 0.4 1449242
Total Xylenes ug/L ND ND ND 0.4 1449242
F1 (C6-C10) ug/L ND ND ND 100 1449242
F1 (C6-C10) - BTEX ug/L ND ND ND 100 1449242
F2-F4 PHC
F2 (C10-C16 Hydrocarbons) ug/L ND 120 ND 100 1449135
F3 (C16-C34 Hydrocarbons) ug/L ND 310 ND 100 1449135
F4 (C34-C50 Hydrocarbons) ug/L ND ND ND 100 1449135
Reached Baseline at C50 ug/L Yes Yes Yes 1449135
Surrogate Recovery (%)
1,4-Difluorobenzene % 102 97 99 1449242
4-Bromofluorobenzene % 91 84 100 1449242
D10-Ethylbenzene % 98 94 95 1449242
D4-1,2-Dichloroethane % 109 123 124 1449242
o-Terphenyl % 105 103 103 1449135
ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control Batch
Page 6 of 10
Barenco IncMaxxam Job #: A808263 Client Project #: 07126Report Date: 2008/02/07 Project name:
Your P.O. #: 07126Sampler Initials:
GENERAL COMMENTS
Results relate only to the items tested.
Page 7 of 10
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance ReportMaxxam Job Number: MA808263
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1449135 ZZ MATRIX SPIKE o-Terphenyl 2008/01/29 116 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/29 111 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/29 111 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/29 111 % 60 - 130
Spiked Blank o-Terphenyl 2008/01/29 115 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/29 97 % 60 - 130F3 (C16-C34 Hydrocarbons) 2008/01/29 97 % 60 - 130F4 (C34-C50 Hydrocarbons) 2008/01/29 97 % 60 - 130
Method Blank o-Terphenyl 2008/01/29 103 % 30 - 130F2 (C10-C16 Hydrocarbons) 2008/01/29 ND, RDL=100 ug/LF3 (C16-C34 Hydrocarbons) 2008/01/29 ND, RDL=100 ug/LF4 (C34-C50 Hydrocarbons) 2008/01/29 ND, RDL=100 ug/L
RPD F2 (C10-C16 Hydrocarbons) 2008/01/29 NC % 50F3 (C16-C34 Hydrocarbons) 2008/01/29 NC % 50F4 (C34-C50 Hydrocarbons) 2008/01/29 NC % 50
1449242 GRU MATRIX SPIKE 1,4-Difluorobenzene 2008/01/29 102 % 70 - 1304-Bromofluorobenzene 2008/01/29 110 % 70 - 130D10-Ethylbenzene 2008/01/29 105 % 70 - 130D4-1,2-Dichloroethane 2008/01/29 113 % 70 - 130Benzene 2008/01/29 99 % 70 - 130Toluene 2008/01/29 100 % 70 - 130Ethylbenzene 2008/01/29 102 % 70 - 130o-Xylene 2008/01/29 100 % 70 - 130p+m-Xylene 2008/01/29 106 % 70 - 130F1 (C6-C10) 2008/01/29 83 % 70 - 130
Spiked Blank 1,4-Difluorobenzene 2008/01/29 108 % 70 - 1304-Bromofluorobenzene 2008/01/29 116 % 70 - 130D10-Ethylbenzene 2008/01/29 113 % 70 - 130D4-1,2-Dichloroethane 2008/01/29 108 % 70 - 130Benzene 2008/01/29 103 % 70 - 130Toluene 2008/01/29 101 % 70 - 130Ethylbenzene 2008/01/29 101 % 70 - 130o-Xylene 2008/01/29 104 % 70 - 130p+m-Xylene 2008/01/29 110 % 70 - 130F1 (C6-C10) 2008/01/29 96 % 70 - 130
Method Blank 1,4-Difluorobenzene 2008/01/29 109 % 70 - 1304-Bromofluorobenzene 2008/01/29 96 % 70 - 130D10-Ethylbenzene 2008/01/29 102 % 70 - 130D4-1,2-Dichloroethane 2008/01/29 105 % 70 - 130Benzene 2008/01/29 ND, RDL=0.2 ug/LToluene 2008/01/29 ND, RDL=0.2 ug/LEthylbenzene 2008/01/29 ND, RDL=0.2 ug/Lo-Xylene 2008/01/29 ND, RDL=0.2 ug/Lp+m-Xylene 2008/01/29 ND, RDL=0.4 ug/LTotal Xylenes 2008/01/29 ND, RDL=0.4 ug/LF1 (C6-C10) 2008/01/29 ND, RDL=100 ug/LF1 (C6-C10) - BTEX 2008/01/29 ND, RDL=100 ug/L
RPD Benzene 2008/01/29 NC % 40Toluene 2008/01/29 NC % 40Ethylbenzene 2008/01/29 NC % 40o-Xylene 2008/01/29 NC % 40p+m-Xylene 2008/01/29 NC % 40Total Xylenes 2008/01/29 NC % 40F1 (C6-C10) 2008/01/29 NC % 40F1 (C6-C10) - BTEX 2008/01/29 NC % 40
Page 8 of 10
Barenco IncAttention: Bernard Chan Client Project #: 07126P.O. #: 07126Project name:
Quality Assurance Report (Continued)Maxxam Job Number: MA808263
QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits
1449839 KKE Spiked Blank Aliphatic >C10-C12 2008/02/07 80 % 30 - 130Aliphatic >C12-C16 2008/02/07 79 % 30 - 130Aliphatic >C16-C21 2008/02/07 83 % 30 - 130Aliphatic >C21-<C32 2008/02/07 78 % 30 - 130Aromatic >C10-C12 2008/02/07 107 % 30 - 130Aromatic >C12-C16 2008/02/07 108 % 30 - 130Aromatic >C16-C21 2008/02/07 104 % 30 - 130Aromatic >C21-<C32 2008/02/07 93 % 30 - 130
Method Blank Isobutylbenzene - Extractable 2008/02/07 62 % 30 - 130n-Dotriacontane - Extractable 2008/02/07 82 % 30 - 130Aliphatic >C10-C12 2008/02/07 ND, RDL=0.01 mg/LAliphatic >C12-C16 2008/02/07 ND, RDL=0.05 mg/LAliphatic >C16-C21 2008/02/07 ND, RDL=0.05 mg/LAliphatic >C21-<C32 2008/02/07 ND, RDL=0.1 mg/LAromatic >C10-C12 2008/02/07 ND, RDL=0.01 mg/LAromatic >C12-C16 2008/02/07 ND, RDL=0.05 mg/LAromatic >C16-C21 2008/02/07 ND, RDL=0.05 mg/LAromatic >C21-<C32 2008/02/07 ND, RDL=0.1 mg/L
1451710 GTH Spiked Blank Isobutylbenzene - Volatile 2008/02/04 112 % 70 - 130Benzene 2008/02/04 109 % 70 - 130Toluene 2008/02/04 109 % 70 - 130Ethylbenzene 2008/02/04 113 % 70 - 130Xylene (Total) 2008/02/04 116 % 70 - 130
Method Blank Isobutylbenzene - Volatile 2008/02/04 114 % 70 - 130Benzene 2008/02/04 ND, RDL=0.001 mg/LToluene 2008/02/04 ND, RDL=0.001 mg/LEthylbenzene 2008/02/04 ND, RDL=0.001 mg/LXylene (Total) 2008/02/04 ND, RDL=0.002 mg/LAliphatic >C6-C8 2008/02/04 ND, RDL=0.01 mg/LAliphatic >C8-C10 2008/02/04 ND, RDL=0.01 mg/L>C8-C10 Aromatics (-EX) 2008/02/04 ND, RDL=0.01 mg/L
ND = Not detectedNC = Non-calculableRPD = Relative Percent DifferenceSPIKE = Fortified sample
Page 9 of 10
Validation Signature Page
Maxxam Job #: A808263
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).
GREG GILBERT, Scientific Specialist
MEDHAT RISKALLAH, Manager, Hydrocarbon Department
SUZANA POPOVIC, Supervisor, Hydrocarbons
====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CAEAL have approved this reporting process and electronic report format.
Page 10 of 10