phase ii environmental site assessment proposed lewistown

Phase II Environmental Site Assessment

Proposed Lewistown Road Improvements (Route 802) VDOT Project Number 0095-042-716 (90347)

Hanover County, Virginia

July 3, 2013

Prepared for: Ms. Karol Akers Virginia Department of Transportation 1618 Swinton Lane Richmond, Virginia 23238

Prepared by: Cardno MM&A 10988 Richardson Road Ashland, Virginia 23005 www.cardno.com www.cardnomma.com

http://www.cardno.com/

Cardno MM&A 10988 Richardson Road Ashland, VA 24605 Phone +1 804 798 6525 Fax +1 804 798 5907 www.cardno.com www.cardnomma.com

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July 3, 2013 Ms. Karol Akers Virginia Department of Transportation 1618 Swinton Lane Richmond, Virginia 23238 Subject: Phase II Environmental Site Assessment

Proposed Lewistown Road Improvements (Route 802) Hanover County, Virginia

VDOT Project Number 0095-042-716 (90347) MM&A Project Number VRICH245 Dear Ms. Akers: Cardno MM&A completed the attached Phase II Environmental Site Assessment Report for the proposed Lewistown Road (Route 802) improvement project in Hanover County, Virginia. The Virginia Department of Transportation (VDOT) requested this investigation as part of the preliminary engineering prior to right-of-way acquisition and road construction activities. For this investigation, Cardno MM&A established boreholes to investigate potential impacts at the following sites:

Travel Centers of America – TA Truck Stop (Parcel 019) Shell Station (Parcel 020) Southeast of Lewistown Rd/Airpark Rd intersection (Parcel 002) I-95 Bridge foundation (in median) beneath Lewistown Road (Existing right-of-way) I-95 north bound on-ramp from Lewistown Road (Existing right-of-way)

If you have any questions or require further information, please contact the undersigned.

Sincerely,

Joshua P. Shrader Project Scientist for Cardno MM&A Direct Line +1 804 433 3545 Email: [email protected]

James T. Martin, Jr., P.G. Senior Scientist for Cardno MM&A Direct Line +1 804 433 3540 Email: [email protected]

Enclosures

http://www.cardno.com/

Phase II Environmental Site Assessment Report Prepared for: Virginia Department of Transportation

July 3, 2013 Cardno MM&A i

Table of Contents 1 Introduction .......................................................................................................................... 1

1.1 Proposed Road Improvements ................................................................................................. 1 2 Subsurface Investigation Procedures ................................................................................ 3

2.1 Soil Sampling Methods ............................................................................................................. 3 2.2 Groundwater Sampling Methods .............................................................................................. 4 2.3 Data Comparisons .................................................................................................................... 4

3 Subsurface Investigation Results ....................................................................................... 4 3.1 Subsurface Soil Results ........................................................................................................... 5 3.2 Surface Soil Results ................................................................................................................. 6 3.3 Groundwater Results .............................................................................................................. 10

4 Conclusions ....................................................................................................................... 10

5 Recommendations ............................................................................................................. 12

6 Limitations .......................................................................................................................... 12

Appendices A ........................................................................................................................................................ Vicinity Map B ........................................................................................................................................................ Site Figures C ....................................................................................................................................................... Photographs D ................................................................................................................................................. Soil Boring Logs E ....................................................................................... Certificates of Analysis and Chain-of-Custody Forms


July 3, 2013 Cardno MM&A 1

1 Introduction

Cardno MM&A prepared this Phase II Environmental Site Assessment (ESA) Report for the proposed Lewistown Road (Route 802) improvement project in Hanover County, Virginia (see the Vicinity Map, Appendix A). The project improves Lewistown Road and replaces the Lewistown Road Bridge over I-95. The Virginia Department of Transportation (VDOT) requested this investigation as part of the preliminary engineering prior to right-of-way (R/W) acquisition and road/utility construction activities. VDOT desired to determine any impacts to existing R/W and drainage ditches and to any road improvement project excavations. For this investigation, Cardno MM&A implemented the VDOT developed sampling and testing program.

1.1 Proposed Road Improvements The proposed project includes the following improvements:

Widen Lewistown Road with two west bound lanes, one east bound lane and a left turn lane into the Travel America Truck Stop.

Relocate the current I-95 north exit ramp intersection with Lewistown Road further east. This new exit ramp will include turn lanes and four traffic signal poles at its intersection with Lewistown Road.

Relocate Airpark Road further east of its current intersection with Lewistown Road.

Replace the I-95/Lewistown Road Bridge with a new wider four lane bridge.

Improve surface drainage improvements with new ditches and 18 to 24-inch diameter stormwater pipes with drop inlets proposed to approximately 6.5 feet deep along Lewistown Road and approximately 8 feet deep crossing Lewistown Road.

Relocate utilities that include a 12-inch diameter water line to an approximate depth of 6.5 feet below ground and an 8-inch diameter sanitary sewer line to approximately 12 feet below ground.

The Virginia Department of Transportation (VDOT) identified sites of potential concern based on their review of regulatory files, site history and property inspections. These sites assessed in this Phase II

ESA Report are referred to as the following;

Travel Centers of America – TA Truck Stop (Parcel 019)

Shell Station (Parcel 020)

Southeast of Lewistown Rd/Airpark Rd intersection (Parcel 002)

I-95 Bridge foundation (in median) beneath Lewistown Road (Existing right-of-way)

I-95 north bound on-ramp from Lewistown Road (Existing right-of-way)

The sites of potential concern are depicted on Figures 1-3 in Appendix B and the photographs in Appendix C. During the sampling investigation, these properties were evaluated along the proposed R/W and/or proposed construction features. The following is a summary of the site history and potential concerns for each site.



Table 1 – Sites of Potential Concern

Site Name Parcel #/Owners

Address VDOT Plan Sheet/MM&A

Figure #

Proposed Construction Features/Issues

Potential Concerns

Travel Centers of America

019/HPT TA

Properties Trust

10134 Lewistown

Road 5&6/1&3

Drainage ditches and pipes. Water line relocation. Signal poles B &C. Features are in proposed R/W (or portions to

be proffered)

Active USTs and ASTs and closed

PC#s (1991-1010, 1996-4015, 1996-4091, 2003-4416 and 2009-4307).

Also VPDES discharge from

outfalls 001 and 002 along with run-off from truck stop

frontage.

Shell Station

020/Third Generation.

L.P.

10114 Lewistown

Road 6/1 Drainage pipe. Proposed

sewer line relocation.

Active USTs and one closed PC# is listed for the site (1991-

0053).

Southeast of

Lewistown Rd/Airpark

Rd.

002/ MG Lewistown

Road 3, LLC

Undeveloped 6/1

Drainage ditches and drainage pipes. Signal poles D & E. Water line relocation and sewer line relocation. Features are in proposed

R/W

Discharge/migration from upgradient TA

truck stop.

I-95 Bridge Footprint median below

Lewistown Road

Existing R/W N/A 5/3 Bridge pier

Runoff from automobiles and

possible metals from bridge paint.

I-95 Northbound Ramp from Lewistown

Road

Existing R/W N/A 5D/2 No construction.

Maintenance responsibility.

Discharge from adjacent TA truck

stop VPDES Outfall 003.

Gray shaded data designate existing right-of-way



2 ESA Procedures

On June 3-4, 2013, Cardno MM&A used a combination of field analytical and laboratory methods to evaluate impact on all sites of potential concern. These investigation procedures are based on the ASTM Phase II Environmental Site Assessment E-1903-97 (2002). The laboratory testing adhered to the United States Environmental Protection Agency (EPA) Test Methods for Evaluating Solid Wastes, US EPA SW-846.

2.1 Soil Sampling Methods Cardno MM&A implemented the VDOT developed sampling and testing program for this project as follows.

To evaluate subsurface soils, VDOT requested eight soil borings along the corridor using Geoprobe direct push technology. The Geoprobe® cores were collected in 1.5-inch diameter plastic liners in approximate four-foot increments and were examined and described upon recovery. Boreholes were established to approximately two feet below the invert elevations for each respective drainage feature or to sixteen feet for proposed traffic signal locations.

To evaluate surface soils, VDOT also requested shallow surface samples by hand auger from the following

o I-95/Lewistown Bridge footprint

o Discharge points and run-off from Parcel 019 (TA truck stop).

Composite soil samples were obtained from each interval, and a portion of each sample was placed into a Ziploc bag for approximately 15 minutes. Each bagged sample was then field screened for its soil-vapor concentration with a photo-ionization detector (PID). The laboratory bound soil samples were packed into sterile glass jars, sealed and stored on ice. The soil boring number, date obtained, sample interval and Cardno MM&A project number were recorded on labels and attached to the corresponding sample jars.

A Chain of Custody Form was properly completed and accompanied all samples to the laboratory. Samples were submitted to Air, Water and Soil Laboratories, Inc. (AWS) of Richmond, Virginia for analysis. VDOT determined the following test parameters for the project based on petroleum concerns along with parameters reportedly associated with truckstops and also monitored for the TA tuck stop VPDES permit (from permit # VA0061972) as detailed in Table 2.

Table 2 – Summary of Environmental Testing

Analysis Test Method Total Petroleum Hydrocarbons-Diesel Range Organics (TPH-DRO) SW8015C Total Petroleum Hydrocarbons-Gasoline Range Organics (TPH-GRO) SW8015C Oil & Grease SW9071 Volatile Organic Compounds (VOCs) SW8260 Semi-Volatile Organic Compounds (SVOCs) SW8270 Arsenic, Cadmium, Chromium and Lead SW6010 Selenium and Zinc SW6010 E. Coli Colilert 18/QT Fecal Coliform SM18/9221E



2.2 Groundwater Sampling Methods Groundwater was encountered in and sampled from one borehole (020-03). A temporary monitoring well was constructed by inserting one-inch diameter polyvinyl chloride (PVC) piping attached to a section of slotted (0.010-inch) screen. The temporary well was sampled by using a disposable polyethylene bailer. The groundwater sample was placed into glass 40-milliliter vials for submittal to AWS for analyses of BTEX to screen for petroleum impacts.

2.3 Data Comparisons The laboratory data from the soil and groundwater samples were compared to the standards discussed below:

The data were first compared to RCRA 40 CFR Part 261.24 Subpart C (Characteristics of

Hazardous Waste). Detected “totals” concentrations were divided by the 20 conversion factor to compare with the toxicity characteristic leaching procedure (TCLP) regulatory limits.

The data were next compared to the following Virginia Solid Waste Management Regulations (VSWMR).

o Petroleum data were compared to the DEQ clean-fill TPH limit of 50 mg/kg per 9 VAC20-80-700 (Soil Contaminated with Petroleum Products).

o Metals are naturally occurring and no site specific background data are known. Therefore to measure against background values, VDOT requested a comparison of the metals data to the following referenced documents:

Element Concentrations in Soils and Other Surficial Materials of the

Conterminous United States/ U.S.G.S. Professional paper 1270, 1984.

Review of National Ambient Air Quality Standards for Lead: Exposure Analysis

Methodology and Validation, EPA-450/2-89-011.

Agency for Toxic Substances & Disease Registry: Toxicological Profile for

Cadmium.

Units for soil and groundwater samples are discussed herein in milligrams per kilogram (mg/kg) and milligrams per liter (mg/l), which equate to parts per million.

3 ESA Results

The results of this study are provided as follows:

Borehole/temporary well locations are shown on Figures 1-3 in Appendix B.

Field screen readings are presented on the soil boring logs in Appendix D. Soil samples were selected for laboratory testing based on observations, field screen readings, and proposed construction plans. The sample identification contains the parcel/boring number and depth. For example, sample 002-01 @ 0’-4’ equals “Parcel 002, boring one collected from a depth of zero to four feet”.

The Certificates of Analysis and Chain of Custody Forms are provided in Appendix E.



3.1 Subsurface Soil Results Subsurface samples were collected from Geoprobe boreholes to evaluate “deeper” project excavations such as proposed signal pedestals, storm drains, and utility relocations (water and sewer), see Figure 1 and Table 3 below.

Table 3 – Subsurface Soil Results - Lewistown Road

Location Sample ID TPH-GRO (mg/kg)

TPH-DRO (mg/kg)

PID (ppm)

TA Truck Stop (Parcel 019)

019-01 0’-4’ BRL BRL 2.0 019-01 4’-8’ NT NT 0.0 019-01 8’-12’ BRL BRL 1.1 019-01 12’-16’ NT NT 0.0 019-02 0’-4’ BRL BRL 0.0 019-03 0’-4’ BRL BRL 0.0 019-03 4’-8’ BRL BRL 0.0 019-03 8’-12’ NT NT 0.0

Shell Station (Parcel 020)

020-01 0’-4’ NT NT 0.0 020-01 4’-8’ BRL BRL 0.0 020-02 0’-4’ NT NT 0.0 020-02 4’-8’ BRL BRL 0.0 020-03 0’-4’ BRL BRL 0.0 020-03 4’-8’ BRL BRL 0.0 020-03 8’-12’ NT NT 0.0 020-03 12’-16’ NT NT 0.0 020-03 16’- 20’ NT NT 0.0

Southeast of Lewistown Rd/Airpark Rd (Parcel 002)

002-01 0’-4’ NT NT 7.3 002-01 4’-8’ BRL BRL 12.1 002-01 8’-12’ NT NT 4.0 002-01 12’-16’ NT NT 4.1 002-02 0’-4’ NT NT 7.0 002-02 4’-8’ BRL BRL 11.2 002-02 8’-12’ BRL BRL 33.0 002-02 12’-16’ NT NT 25.0 002-02 16’-20’ NT NT 16.0

BRL = Below Laboratory Reporting Limits NT = Not Tested TPH = Total Petroleum Hydrocarbons ppm = parts per million DRO = Diesel Range Organics mg/kg = milligram per kilogram GRO = Gasoline Range Organics PID = photo ionization detector

The data from Table 3 for subsurface samples are described as follows.

The TPH-GRO and TPH-DRO results in subsurface samples were all below laboratory reporting limits (BRL).

Thus, no petroleum impact was identified within the proposed “deep” installation intervals on the project (proposed signal pedestals, storm drains or utility relocations).



3.2 Surface Soil Results Surface samples were collected from hand auger boreholes to evaluate “shallow” (< 2 feet deep) project excavations such as proposed drainage ditch excavations, see Figure 1.

Sample 019-03 (0-1’) characterizes shallow sediments/soils in the grassy area off the TA truck stop parking lot on the northwest corner of the Lewiston Road/truck stop entrance.

HA-01 and HA-02 (0-1’) characterize shallow sediments/soils in the ditch on the northeast corner of the Lewistown Road/TA truck stop entrance.

Samples “Lewis Ditch N & S” characterize sediments/soil in the concrete drainage ditch/pipe system that includes drainage from the TA truck stop from north to south beneath Lewistown Road (from outfalls 001 and 002 from permit # VA0061972).

Samples Ramp Ditch 1, 2 and 3 characterize shallow sediments/soils in a drainage ditch that flows from the TA truck stop (from outfall 003 from permit # VA0061972) onto VDOT R/W for the I-95 north ramp (see Figure 2). Note that no excavations are proposed here as part of the road improvement project. However, VDOT is responsible for ditch maintenance and therefore requested the additional sampling/testing to further identify any concerns with receiving VPDES permitted discharge from the truck stop.

Additionally, VDOT is responsible for its own discharges to waterways. VDOT reported that ditches/drainage features will all ultimately discharge to Lickinghole Creek. Thus the aforementioned VDPES Outfall 001, 002 and 003 discharges could potentially be attributed to VDOT unless distinguished from their own discharge.

The surface sample data are summarized in Table 4.



Table 4 – Shallow Soil Detections – Lewistown Road*

Location Sample ID

Petroleum (mg/kg)

Detected VOCs & SVOCs (mg/kg)

Metals (mg/kg) Bacteria (MPN/g)

TA Truck Stop

(Parcel 019)

019-03 0’- 1’ BRL NT Zn=103 NT

HA-02 0’- 1’

TPH-DRO=250

O&G=1,120 (HA-01 0-1’) BRL

As=1.29

NT

Cd=1.74

Cr=26.7

Pb=28.3

Zn=839

Lewis Ditch N

TPH-GRO=0.18

BRL

As=6.11

E. Coli=38,200 Fecal

Coliform=700,000

TPH-DRO=91.8

O&G=668

Cd=1.25

Cr=13.2

Pb=15.6

Zn=391 Southeast of Lewistown Rd/Airpark Rd (Parcel

002)

Lewis Ditch S TPH-DRO=128 NT NT E. Coli=53

Fecal Coliform=400

I-95 Northbound Ramp from Lewistown

Road

Ramp Ditch 1

TPH-DRO = 10.6

2-Butanone (MEK) = 0.00508 Acetone = 0.520

As=0.668

E. Coli=22 Fecal Coliform=31 O&G=1,470

Cd=0.636

Cr=5.63 Pb=4.93

Zn=3.98

Ramp Ditch 2 TPH-DRO=93.6 BRL NT NT

Ramp Ditch 3

TPH-DRO=970 O&G=166 BRL NT NT

BRL = Below Laboratory Reporting Limits VOCs = volatile organic compounds TPH = Total Petroleum Hydrocarbons SVOCs = semivolatile organic compounds DRO = Diesel Range Organics mg/kg = milligram per kilogram GRO = Gasoline Range Organics NT = Not Tested MPN/g = most probable number per gram O&G = Oil and Grease Shaded data exceed a comparison standard (impacted) *Note that not all analytes were tested in subsequent rounds. Once noted in an area, then further testing was requested as an indicator of continued impact downstream/flow.



The data from Table 4 are described below.

Table 4 shows that shallow samples contained petroleum (a combination of Oil and Grease, TPH-DRO and TPH-GRO) except borehole 019-03. Typically the highest concentrations were found in the oil and grease range. Furthermore, the petroleum concentrations in Table 4 exceeded the 50 mg/kg clean fill limit (VSWMR 9 VAC20-81-660).

None of the detected metals contained concentrations that would exceed a TCLP limit. To compare with solid waste management guidelines, VDOT requested Cardno MM&A to compare the metals data to the documents referenced in Section 2.3, which were arsenic (4.8 mg/kg), cadmium (0.5 mg/kg), chromium (33 mg/kg), lead (50 mg/kg) and zinc (40 mg/kg). Thus for every sample tested for metals, Table 4 shows that either zinc and/or cadmium exceeded the referenced background comparisons (VDOT identified as a solid waste).

The bacteria testing also detected E. Coli and Fecal Coliform, which may indicate influences from wastewater/sewage or wildlife. For bacteria, the VDOT provided comparison standard in solids is for fecal coliform: <1000MNP/g dry weight basis as in Class A fertilizers (i.e., no controls, can sell or use on lawns/gardens without restrictions, 9VAC25-31-560 and 9VAC25-31-710). Table 4 shows that the “Lewis Ditch N” sample exceeded this comparison.

For organics testing, only two VOCs (MEK and Acetone) were detected (from Ramp Ditch 1) outside the improvement project. The EPA considers MEK and acetone as common laboratory contaminants (used in laboratories and thus may be introduced into a sample from laboratory cross-contamination), Risk Assessment Guidance for Superfund, Volume I Human Health

Evaluation Manual, Part A. Additionally, no TCLP limits were exceeded.

In summary, the data set above support that run-off/discharge from the Travel America truck stop has impacted the drainage ditch system in the proposed R/W. Table 4 highlights the data that exceeded a comparison standard, and thus identifies impacted soils including petroleum, metals (cadmium and zinc) and fecal coliform. VDOT requested further categorizing the impacted soils as either in existing R/W or in proposed R/W, which are highlighted on the figures as follows:

o Purple highlight designates impacted soils in existing R/W.

o Yellow highlight designates impacted soils in proposed R/W.



Surface samples were also collected by hand auger (0-1 feet and 1-2 feet deep) in the I-95 median near the bridge pier (existing R/W) to evaluate project excavations for the bridge improvements, see Figure 3 and Table 5.

Table 5 – Soil Results for I-95/Lewistown Bridge Footprint

Location Sample ID TPH-GRO (mg/kg)

TPH-DRO (mg/kg)

Arsenic (mg/kg)

Cadmium (mg/kg)

Chromium (mg/kg)

Lead (mg/kg)

TCLP Lead

(mg/L)

Current Bridge Piers

NP 0’ -1’ BRL BRL 1.38 0.822 9.84 198 0.303 NP 1’ -2’ NT NT NT NT NT 40.7 NT SP 0’ -1’ NT NT NT NT NT NT NT SP 1’ -2’ NT NT NT NT NT NT NT

Proposed New

Bridge Footprint

N 0’ - 1’ NT NT NT NT NT NT NT N 1’ - 2’ NT NT NT NT NT NT NT S 0’ - 1’ BRL BRL 0.752 0.524 6.11 133 NT S 1’ - 2’ NT NT NT NT NT 7.91 NT

BRL = Below Laboratory Reporting Limits NT = Not Tested TPH = Total Petroleum Hydrocarbons ppm = parts per million DRO = Diesel Range Organics mg/kg = milligram per kilogram GRO = Gasoline Range Organics 1.38 = Detected concentration disposal Shaded data exceed a comparison standard (impacted)

The data from Table 5 for surface samples at the bridge foundation (median) are described below.

TPH-GRO and TPH-DRO were below laboratory reporting limits (BRL) in both samples tested.

The RCRA TCLP regulatory limits for the detected metals are 5.0 mg/l except for cadmium, which is 1.0 mg/L. Of the detected “totals” concentrations for metals in soil, all were below the maximum estimated TCLP value except for lead from the upper one foot. Thus the highest total lead concentration (total lead = 198 mg/kg) was tested for TCLP lead and resulted in 0.303 mg/L (< 5.0 mg/l TCLP limit). Therefore, concentrations did not exceed RCRA hazardous waste limits.

To compare with solid waste management guidelines, VDOT requested Cardno MM&A to compare the metals data to the documents referenced in Section 2.3, which were arsenic (4.8 mg/kg), cadmium (0.5 mg/kg), chromium (33 mg/kg) and lead (50 mg/kg). Thus of the detected metals, lead and cadmium from 0-1 foot exceeded the referenced background comparison (VDOT identified as a solid waste).

Table 5 highlights the lead and cadmium data (0-1 feet) that exceeded comparison standards (impacted). Likewise, Figure 3 depicts/highlights the impacted areas based on the metals data.



3.3 Groundwater Results Groundwater was encountered in one well (020-03/TW-01) at a depth of approximately 19 feet below ground surface (bgs). The Certificate of Analysis is provided in Appendix E and is summarized below in Table 6.

Table 6 – Groundwater Results

Location Temporary

Well Sample ID

Depth to Groundwater

(feet) Benzene (mg/L)

Toluene (mg/L)

Ethylbenzene (mg/L)

Xylenes (mg/L)

Shell Station

(Parcel 020) 020-03/TW-01 19 BRL BRL BRL BRL

BRL = Below Laboratory Reporting Limits mg/L = milligram per liter

The data from Table 6 are described below.

020-03/TW-01 was BRL of BTEX compounds. Thus, no petroleum-impacted groundwater was identified in proposed excavations.

4 Conclusions

The laboratory results defined impacted soils within both existing and proposed R/W for the Lewistown Road improvement project. With respect to handling excavated soils from these impacted areas, the following is a summary from the DEQ’s Management and Reuse of Contaminated Media, July 17, 2012. Note that some of the options would require a proposal/information by the selected road contractor to provide details for an approved site/compliance with regulations.

1. Appropriate reuse of contaminated media within the actual excavation. One such supporting document is the DEQs guidance on Management of Petroleum Contaminated Soil at VDOT Road Construction Sites that allows excavated soils to be replaced in the same excavation for utility projects if certain criteria are met However no/minimal space is expected for replacing material in most project excavations (such as for drainage ditches), which lessens this options availability.

2. Appropriate reuse of the contaminated material on the road improvement project site. For material handling, 9VAC20-81-95d allows nonhazardous, contaminated soil that has been excavated as part of a construction project to be used as backfill for the same excavation or excavations containing similar contaminants at the same site, at concentrations at the same level or higher. However, space limitations for excess fill and additional data requirements may lessen this option’s effectiveness.

3. Using a solid waste variance, reuse of the contaminated media on the road improvement site or at another site. However the Management and Reuse of Contaminated Media document describes all requirements such as concentration limits, setbacks, and notifications/documentation. Furthermore, the petroleum concentrations referenced above exceeded the clean fill limit thus prohibiting off-site re-use of petroleum soils.

4. The final option is off-site disposal at a treatment facility or a landfill. A disposal option may be more straight forward and quicker to implement, particularly for small soil volumes. As requested by VDOT, Table 7 contains a cost estimate for the transportation and disposal of the impacted soil to a local disposal facility.



Table 7 – Disposal Cost Estimate

Site Name Parcel # Detection Sample

Anticipated Impacted Extent

Impacted Volume/Tonnage

Disposal Cost Estimate*

TA Truck Stop

Existing R/W west of entrance

019-03/Zn Install new drainage ditch west of truck stop entrance (39+86L-41+00L)

70ft length X 5ft width X upper 2ft depth

39 tons X $65/ton = $2,535.00

019 Proposed R/W Project Excavations

019-03/Zn Install new drainage ditch west of truck stop entrance (41+00L-41+35L)


28 tons X $65/ton = $1,820.00

Existing R/W east of entrance

HA-01/02/ O&G & TPH-DRO, Cd, Zn

Install 12-inch Water Line crossing existing ditch east of truck stop from entrance at 44+34L-44+42L


16 tons X $65/ton = $1,040.00

019 Proposed R/W Project Excavations

HA-01/02/ O&G & TPH-DRO, Cd, Zn

Remove remaining drainage ditch (44+42L-45+10L) and install new surface drainage ditch/pipe east of truck stop entrance from structure 6-08 to 60 feet west of 6-08

117 total ft length X 5ft width X upper 2ft depth

65 tons X $65/ton = $4,225.00

Existing R/W – Drainage Pipe

Lewis Ditch N/O&G, Cd, fecal coliform

Sediment on/within concrete lined ditch/24-inch drainage pipes beneath Lewistown Road to be removed

Flush/clean pipes with vactor truck to remove sediment/water

$2,000.00

Southeast of Lewistown Rd/Airpark Rd

Existing R/W

Lewis Ditch S/TPH-DRO

Downflow of existing pipe outlet to existing R/W and 25ft north of existing R/W on proposed pipe (6-10to6-11)

50ft total length X 5ft width X upper 2ft depth

28 tons X $65/ton =$1,820.00

002 Proposed R/W

Lewis Ditch S/TPH-DRO

From existing R/W to 15ft south of 6-12 on existing & proposed drainage (6-11 to 6-12)

Upper 2ft depth estimated as 64 tons

64 tons X $65/ton =$4,160.00

I-95 Bridge Footprint

Existing R/W

NP and S/ Pb & Cd Excavate new Piers

Upper 1ft depth – estimated as 75 tons

75 tons X $65/ton =$4,875.00

I-95 Northbound Ramp from Lewistown Road

Existing R/W

Ramp Ditch 1 to 3/O&G, TPH-DRO, Cd

Excavate for maintenance clean-out

150 ft length X 5ft width X upper 2ft depth

83 tons X $65/ton =$5,395.00

Sediment in concrete pipes beneath ramp

Flush/clean pipes with vactor truck $500.00

Conversions are as follows: Ft3/27 = yd3 Yd3 X 1.5 = tons TOTAL=398 TONS $28,370 * Cost Estimate includes incidentals such as plastic sheeting based on 5% of the anticipated disposal fee. Purple highlight reflects disposing of impacted material from existing R/W

Yellow highlight reflects disposing of impacted material from proposed R/W



5 Recommendations

Based on the findings for this Phase II Environmental Site Assessment (ESA) Report for the proposed Lewistown Road improvement project in Hanover County, Virginia, VDOT should consider the following.

For R/W acquisition at the Travel Centers of America, negotiate compensation from the owner for clean-up costs for impacted soils related to truck stop run-off/discharge. Additionally, evaluate measures for improved water quality of future run-off/discharge onto VDOT R/W.

Include a special provision for handling impacted soils during utility/road construction. The special provisions should outline the various management/disposal procedures.

Provide the results of this study to the road/utility contractor so that proper health and safety measures can be implemented during construction.

6 Limitations

The investigation upon which this report is based represents an appropriate level of inquiry to satisfy the requirements as specified by VDOT and included in our work plan/opinion of probable cost dated May 23, 2013. No sampling investigation can wholly eliminate uncertainty regarding the potential for recognized environmental conditions/areas of concern. Performance of this study is intended to reduce, but not eliminate, uncertainty regarding the potential for such conditions, and this practice recognizes reasonable limits of time and cost.

This report is intended only for use by VDOT and its agents for the sole purpose of verifying the environmental status of the subject property. It should be understood that the findings contained herein represent the current regulatory and operational status of the property as of the date of this report. Future activities either adjacent to or on the subject property could result in environmental conditions that do not exist today. The conclusions of this report are based on the available data and the current plan sheets (dated 5/16/2013). Should road plans change such as different proposed R/W limits or modified construction details, then the conclusions of this report should be re-evaluated.

Subsurface Investigation Report Prepared for: Virginia Department of Transportation

June 26, 2013 Cardno MM&A 13

Subsurface Investigation Report

APPENDIX

A VICINITY MAP




APPENDIX

B SITE FIGURES

12" W

1

2

"

W

12" W

12" W

12" W

1

2

" W

8

"

S

8" S

8

"

S

C

B

E

D

002-01

Travel Centers

of America

Shell

Station

002-02

HA-01

HA-02

HA-03

019-02

019-01

LEWIS DITCH S

020-02

020-03/TW-01

020-01

MG LEWISTOWN

ROAD 3, LLC

019-03

LEWIS DITCH N

1

Figure

Hanover C

ounty, V

irginia

Virginia D

epartm

ent of T

ransportation

DR

AW

N:

7/3/2013

DE

SIG

NE

D:

CH

EC

KE

D:

DA

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FILE

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OF

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C.:

VR

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ite M

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ALE

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VR

IC

H245

AS

S

HO

WN

JT

M

DE

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CT

N

O.:

Ashland, V

A. U

SA

Lew

istow

n R

oad P

hase II

Pre

pa

re

d F

or:

SCALE: 1" = 50'

50' 0 50'

Note: Base map from VDOT Plan Sheets 5 & 6; Project 0095-042-716

SOIL BORING/TEMPORARY WELL LOCATION020-03/TW-01

SOIL BORING LOCATION

020-02

B

LEWIS DITCH S HAND AUGER LOCATION

PROPOSED SIGNAL PEDESTAL

IMPACTED ZONE IN PROPOSED R/W

EXISTING RIGHT-OF-WAY

IMPACTED ZONE IN EXISTING R/W

PROPOSED RIGHT-OF-WAY

I-95 North Bound Ramp

from Lewistown Road

RAMP DITCH 1

RAMP DITCH 2

RAMP DITCH 3

2

Figure

Hanover C

ounty, V

irginia

Virginia D

epartm

ent of T

ransportation

DR

AW

N:

7/3/2013

DE

SIG

NE

D:

CH

EC

KE

D:

DA

TE

:

FILE

N

O.:

OF

FIC

E LO

C.:

VR

IC

H245_S

ite M

ap 3.dw

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SC

ALE

:

VR

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H245

AS

S

HO

WN

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DE

S

JP

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PR

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CT

N

O.:

Ashland, V

A. U

SA

Lew

istow

n R

oad P

hase II

Pre

pa

re

d F

or:

SCALE: 1" = 50'

50' 0 50'

Note: Base map from VDOT Plan Sheet 5D; Project 0095-042-716

RAMP DITCH 1HAND AUGER LOCATION


I-95/L

ew

isto

w

n R

oad

B

rid

ge F

oo

tp

rin

t

I-95/L

ew

isto

w

n R

oad

B

rid

ge F

oo

tp

rin

t

12" W

SP

NP

N

S

3

Figure

Hanover C

ounty, V

irginia

Virginia D

epartm

ent of T

ransportation

DR

AW

N:

7/3/2013

DE

SIG

NE

D:

CH

EC

KE

D:

DA

TE

:

FILE

N

O.:

OF

FIC

E LO

C.:

VR

IC

H245_S

ite M

ap 3.dw

g

SC

ALE

:

VR

IC

H245

AS

S

HO

WN

JT

M

DE

S

JP

S

PR

OJE

CT

N

O.:

Ashland, V

A. U

SA

Lew

istow

n R

oad P

hase II

Pre

pa

re

d F

or:

SCALE: 1" = 50'

50' 0 50'

Note: Base map from VDOT Plan Sheet 5; Project 0095-042-716

HAND AUGER LOCATION

NP

(Composite Sample)


EXISTING RIGHT-OF-WAY

PROPOSED RIGHT-OF-WAY




APPENDIX

C PHOTOGRAPHS

Photodocumentation Subsurface Investigation Report

Lewistown Road Prepared for: Virginia Department of Transportation

Cardno 2

Client: Virginia Department of Transportation Site Location: Dinwiddie County, Virginia

Site Name: Parcel 019 (Travel Center of America) Project Number: VFRED242

Photo 1 Date:

June 3, 2013

Description: West view of Parcel 019 (Travel Centers of America). Area of samples HA-1 thru HA-3.

Photo 2 Date:

June 3, 2013

Description: Close-up view of Parcel 019 ditch line. Area of samples HA-1 thru HA-3.



Cardno 4



Photo 3 Date:

June 3, 2013

Description: View of Lewis Ditch N sample location (Parcel 019).

Photo 4 Date:

June 3, 2013

Description: Close view of Lewis Ditch N sample location (Parcel 019) of sediment on concrete ditch surface



Cardno 9

Client: Virginia Department of Transportation Site Location: Hanover County, Virginia Site Name: I-95/Lewistown Road On Ramp Project Number: VRICH245

Photo 5 Date:

June 4, 2013

Description: Northwest of Travel Centers of America entrance from Lewistown Rd.

Photo 6 Date:

June 4, 2013

Description: Additional view of Northwest of Travel Centers of America entrance from Lewistown Rd.



Cardno 5

Client: Virginia Department of Transportation Site Location: Hanover County, Virginia Site Name: Parcel 020 (Shell Station) Project Number: VRICH245

Photo 7 Date:

June 3, 2013

Description: View from Parcel 020 (Shell Station) looking west.

Photo 8 Date:

June 3, 2013

Description: View of Parcel 020 looking east.



Cardno 1

Client: Virginia Department of Transportation Site Location: Hanover County, Virginia Site Name: Parcel 002 Project Number: VRICH245

Photo 9 Date:

June 3, 2013

Description: View of Parcel 002 (Southeast Corner of Lewistown Rd/Airpark Rd)

Photo 10 Date:

June 3, 2013

Description: Close-up view of Lewistown Ditch S sample location (Southeast Corner of Lewistown Rd/Airpark Rd)



Cardno 3



Photo 11 Date:

June 3, 2013

Description: View of outfall 003 location on Parcel 019. Sample Ramp Ditch 1 taken just west of this location within VDOT R/W.

Photo 12 Date:

June 3, 2013 Description: Close-up view of outfall 003 Outfall 003.



Cardno 8


Photo 13 Date:

June 4, 2013

Description: View of sheen on water downstream of outfall 003.

Photo 14 Date:

June 4, 2013

Description: View of I-95 northbound on-ramp from Lewistown Road. Sample Ramp Ditch 1 to the right.



Cardno 7


Photo 15 Date:

June 4, 2013

Description: View of east side of pipe where Ramp Ditch 2 was collected.

Photo 16 Date:

June 4, 2013 Description:

View of west side of

pipe where Ramp

Ditch 3 was

collected.



Cardno 6

Client: Virginia Department of Transportation Site Location: Hanover County, Virginia Site Name: I-95/Lewistown Road Bridge Project Number: VRICH245

Photo 17 Date:

June 4, 2013

Description: I-95/Lewistown Road Bridge looking south.

Photo 18 Date:

June 4, 2013

Description: I-95/Lewistown Road Bridge looking north.




APPENDIX

D SOIL BORING LOGS

06

-19

-20

13

N

:\C

LIE

NT

PR

OJE

CT

FIL

ES

\VD

OT

\VR

ICH

24

5\0

19

-01

.bo

r

Virginia Department of TransportationLewistown RoadAshland, Virginia

Cardno MM&A Project #VRICH245

LOG OF BORING 019-01 (Travel America Truck Stop)

Date Started : 6/3/2013

Date Completed : 6/3/2013

Hole Diameter : 1"

Drilling Method : Geoprobe

Sampling Method :

Company Rep. : Josh Shrader

Logged By :

Drilling Firm : Cardno MM&A

Northing Coord. :

Eastling Coord. :

Depth

in

Feet

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

Surf.

Elev. DESCRIPTION

Four feet grey CLAY.


Four feet brown CLAY.

Two feet brown CLAY.

Boring terminated at 16 feet.

GR

AP

HIC

US

CS

CL

CL

CL

CL

Sample

Interval

(feet)

PID

Ready

(ppm)

2.0

0.0

1.1

0.0

Rec.

%

100

100

100

100

REMARKS

06

-19

-20

13

N

:\C

LIE

NT

PR

OJE

CT

FIL

ES

\VD

OT

\VR

ICH

24

5\0

19

-02

.bo

r






Hole Diameter : 1"


Sampling Method :


Logged By :


Northing Coord. :

Eastling Coord. :

Depth

in

Feet

0

1

2

3

4

Surf.

Elev. DESCRIPTION

Four feet red/brown CLAY.

Boring terminated at four feet.

GR

AP

HIC

US

CS

CL

Sample

Interval

(feet)

PID

Ready

(ppm)

0.0

Rec.

%

100

REMARKS

06

-19

-20

13

N

:\C

LIE

NT

PR

OJE

CT

FIL

ES

\VD

OT

\VR

ICH

24

5\0

19

-03

.bo

r






Hole Diameter : 1"


Sampling Method :


Logged By :


Northing Coord. :

Eastling Coord. :

Depth

in

Feet

0

1

2

3

4

5

6

7

8

9

10

11

12

Surf.

Elev. DESCRIPTION

Four feet grey CLAY, moist.

Four feet grey CLAY, moist.

Four feet grey to brown CLAY.


GR

AP

HIC

US

CS

CL

CL

CL

Sample

Interval

(feet)

PID

Ready

(ppm)

0.0

0.0

0.0

Rec.

%

100

100

100

REMARKS

06

-19

-20

13

N

:\C

LIE

NT

PR

OJE

CT

FIL

ES

\VD

OT

\VR

ICH

24

5\0

20

-01

.bo

r



LOG OF BORING 020-01 (Shell Station)



Hole Diameter : 1"


Sampling Method :


Logged By :


Northing Coord. :

Eastling Coord. :

Depth

in

Feet

0

1

2

3

4

5

6

7

8

Surf.

Elev. DESCRIPTION

Two feet brown CLAY and GRAVEL.


Boring terminated at eight feet.

GR

AP

HIC

US

CS

CL

CL

Sample

Interval

(feet)

PID

Ready

(ppm)

0.0

0.0

Rec.

%

50

100

REMARKS

06

-19

-20

13

N

:\C

LIE

NT

PR

OJE

CT

FIL

ES

\VD

OT

\VR

ICH

24

5\0

20

-02

.bo

r






Hole Diameter : 1"


Sampling Method :


Logged By :


Northing Coord. :

Eastling Coord. :

Depth

in

Feet

0

1

2

3

4

5

6

7

8

Surf.

Elev. DESCRIPTION

Four feet brown CLAY and GRAVEL.


Boring terminated at eight feet.

GR

AP

HIC

US

CS

CL

CL

Sample

Interval

(feet)

PID

Ready

(ppm)

0.0

0.0

Rec.

%

100

100

REMARKS

06

-19

-20

13

N

:\C

LIE

NT

PR

OJE

CT

FIL

ES

\VD

OT

\VR

ICH

24

5\0

20

-03

.bo

r






Hole Diameter : 1"


Sampling Method :


Logged By :


Northing Coord. :

Eastling Coord. :

Depth

in

Feet

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

Surf.

Elev. DESCRIPTION

Three feet grey CLAY and GRAVEL.



Two feet grey CLAY, two feet grey sandy clay.

Four feet grey SANDY CLAY, wet.


GR

AP

HIC

US

CS

CL

CL

CL

CL

CL

Sample

Interval

(feet)

PID

Ready

(ppm)

0.0

0.0

0.0

0.0

0.0

Rec.

%

75

100

100

100

100

020-03/TW-01

riser

screen

06

-19

-20

13

N

:\C

LIE

NT

PR

OJE

CT

FIL

ES

\VD

OT

\VR

ICH

24

5\0

02

-01

.bo

r



LOG OF BORING 002-01 (Southwest Corner)



Hole Diameter : 1"


Sampling Method :


Logged By :


Northing Coord. :

Eastling Coord. :

Depth

in

Feet

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

Surf.

Elev. DESCRIPTION

Four feet brown and grey CLAY.

Four feet brown and grey CLAY.




GR

AP

HIC

US

CS

CL

CL

CL

CL

Sample

Interval

(feet)

PID

Ready

(ppm)

7.3

12.1

4.0

4.1

Rec.

%

100

100

100

100

REMARKS

06

-19

-20

13

N

:\C

LIE

NT

PR

OJE

CT

FIL

ES

\VD

OT

\VR

ICH

24

5\0

02

-02

.bo

r



LOG OF BORING 002-02 (Southeast Corner)



Hole Diameter : 1"


Sampling Method :


Logged By :


Northing Coord. :

Eastling Coord. :

Depth

in

Feet

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

Surf.

Elev. DESCRIPTION




Four feet brown SANDY CLAY.

Four feet brown SANDY CLAY, wet.


GR

AP

HIC

US

CS

CL

CL

CL

CL

CL

Sample

Interval

(feet)

PID

Ready

(ppm)

7.0

11.2

33.0

25.0

16.0

Rec.

%

100

100

100

100

100

REMARKS




APPENDIX

E CERTIFICATES OF ANALYSIS AND CHAIN-OF-CUSTODY FORMS

2109A North Hamilton Street l Richmond, Virginia 23230 l Tel: (804)-358-8295 Fax: (804)-358-8297

Laboratory Order ID 13F0119

Certificate of Analysis

Client Name:

Enclosed are the results of analyses for samples received by the laboratory on 06/06/2013 11:40. If you have any questions concerning this report, please feel free to contact the laboratory.

Sincerely,

Ted SoyarsLaboratory Manager

Ashland, VA 23005

10988 Richardson Road

Purchase Order:

VRICH245Project Number:

Date Issued:

Date Received:

Submitted To:

Client Site I.D.:

June 13, 2013 13:18

June 6, 2013 11:40Cardno MM&A-Ashland

Joshua Shrader

End Notes:

The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory.

Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen, temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler included in the Certificate of Analysis are done so at the client™s request and are not included in the laboratory™s fields of certification nor have they been audited for adherence to a reference method or procedure.

The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified. For a complete list of the Laboratory™s NELAC certified parameters please contact customer service.

This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of Air Water & Soil Laboratories, Inc.

Lewistown Road

Final Report

Client Site I.D.:Project Number:Submitted To:

Date Issued:Cardno MM&A-Ashland10988 Richardson Road

VRICH245Joshua Shrader

Ashland VA, 23005




Client Name:

Purchase Order:

June 6, 2013 11:40Date Received:June 13, 2013 13:18

Lewistown Road

Final Report

Sample ID Laboratory ID Matrix Date Sampled Date Received

ANALYTICAL REPORT FOR SAMPLES

020-01 4'-8' 13F0119-01 06/06/2013 11:40Soil 06/03/2013 08:40

020-02 4'-8' 13F0119-02 06/06/2013 11:40Soil 06/03/2013 09:00

020-03 0'-4' 13F0119-03 06/06/2013 11:40Soil 06/03/2013 09:10

020-03 4'-8' 13F0119-04 06/06/2013 11:40Soil 06/03/2013 09:15

019-01 0'-4' 13F0119-05 06/06/2013 11:40Soil 06/03/2013 09:40

019-01 8'-12' 13F0119-06 06/06/2013 11:40Soil 06/03/2013 09:50

019-02 0'-4' 13F0119-07 06/06/2013 11:40Soil 06/03/2013 10:00

019-03 0'-4' 13F0119-08 06/06/2013 11:40Soil 06/03/2013 10:15

019-03 4'-8' 13F0119-09 06/06/2013 11:40Soil 06/03/2013 10:25

002-01 4'-8' 13F0119-10 06/06/2013 11:40Soil 06/03/2013 13:20

002-02 4'-8' 13F0119-11 06/06/2013 11:40Soil 06/03/2013 14:10

002-02 8'-12' 13F0119-12 06/06/2013 11:40Soil 06/03/2013 14:20

Page 2 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

ResultParameterReporting

LimitMethod Qual AnalystAnalysis

Date/TimeSample Prep

Date/Time

13F0119-01020-01 4'-8'

06/03/2013 08:40

Analytical Results

Laboratory Sample ID:Sample I.D.

Date/Time Sampled:

Volatile Petroleum Hydrocarbons by GC

TPH-Volatiles (GRO) SW8015C DMB<0.10 mg/kg 06/10/2013 13:04 06/10/2013 13:040.10

Semivolatile Petroleum Hydrocarbons by GC

TPH-Semi-Volatiles (DRO) SW8015C JHV<10.0 mg/kg 06/10/2013 16:10 06/11/2013 20:3010.0

40-160111 %Surrogate: Pentacosane 06/10/2013 16:10 JHV06/11/2013 20:30




Date/Time

13F0119-02020-02 4'-8'

06/03/2013 09:00

Analytical Results


Date/Time Sampled:





40-16088.3 %Surrogate: Pentacosane 06/10/2013 16:10 JHV06/11/2013 20:57

Page 3 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0119-03020-03 0'-4'

06/03/2013 09:10

Analytical Results


Date/Time Sampled:









Date/Time

13F0119-04020-03 4'-8'

06/03/2013 09:15

Analytical Results


Date/Time Sampled:






Page 4 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0119-05019-01 0'-4'

06/03/2013 09:40

Analytical Results


Date/Time Sampled:









Date/Time

13F0119-06019-01 8'-12'

06/03/2013 09:50

Analytical Results


Date/Time Sampled:






Page 5 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0119-07019-02 0'-4'

06/03/2013 10:00

Analytical Results


Date/Time Sampled:









Date/Time

13F0119-08019-03 0'-4'

06/03/2013 10:15

Analytical Results


Date/Time Sampled:






Page 6 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0119-09019-03 4'-8'

06/03/2013 10:25

Analytical Results


Date/Time Sampled:









Date/Time

13F0119-10002-01 4'-8'

06/03/2013 13:20

Analytical Results


Date/Time Sampled:







Date/Time

13F0119-10RE1002-01 4'-8'

06/03/2013 13:20

Analytical Results


Date/Time Sampled:



Page 7 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0119-11002-02 4'-8'

06/03/2013 14:10

Analytical Results


Date/Time Sampled:









Date/Time

13F0119-12002-02 8'-12'

06/03/2013 14:20

Analytical Results


Date/Time Sampled:






Page 8 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Summary of Analytical QC Batches

QC Batch ID Method Sample List

13F0119-01,13F0119-02,13F0119-03,13F0119-04BWF0187 SW8015C

13F0119-01,13F0119-02,13F0119-03,13F0119-04,13F0119-05,13F011

9-06,13F0119-07,13F0119-08,13F0119-09,13F0119-10,13F0119-11,1

3F0119-12

BWF0214 SW8015C

13F0119-05,13F0119-06,13F0119-07,13F0119-08,13F0119-09,13F011

9-10,13F0119-11,13F0119-12

BWF0218 SW8015C

13F0119-10RE1BWF0233 SW8015C

Page 9 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

Volatile Petroleum Hydrocarbons by GC - Quality Control

Air Water & Soil Laboratories, Inc.

Batch BWF0214 - SW5030B

Blank (BWF0214-BLK1) Prepared & Analyzed: 06/10/2013

TPH-Volatiles (GRO) 0.10 mg/kg<0.10 mg/kg

100 80-120Surrogate: 2,5-Dibromotoluene [2C] 94.694.6 ug/L

LCS (BWF0214-BS1) Prepared & Analyzed: 06/10/2013

TPH-Volatiles (GRO) 0.10 0.992 70-13096.4mg/kg0.96 mg/kg

100 80-120Surrogate: 2,5-Dibromotoluene [2C] 100100 ug/L

LCS Dup (BWF0214-BSD1) Prepared & Analyzed: 06/10/2013

TPH-Volatiles (GRO) 0.10 0.969 2070-13093.8 5.05mg/kg0.91 mg/kg


Matrix Spike (BWF0214-MS1) Prepared & Analyzed: 06/10/2013Source: 13F0119-03

TPH-Volatiles (GRO) 0.10 0.956 70-13092.5mg/kg0.88 mg/kg <0.10 mg/kg


Matrix Spike Dup (BWF0214-MSD1) Prepared & Analyzed: 06/10/2013Source: 13F0119-03

TPH-Volatiles (GRO) 0.10 0.967 2070-13090.3 1.26mg/kg0.87 mg/kg <0.10 mg/kg









Page 10 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte







Page 11 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

Semivolatile Petroleum Hydrocarbons by GC - Quality Control


Batch BWF0187 - SW3510C

Blank (BWF0187-BLK1) Prepared: 06/10/2013 Analyzed: 06/11/2013

TPH-Semi-Volatiles (DRO) 10.0 mg/kg<10.0 mg/kg

5.00 40-160Surrogate: Pentacosane 78.43.92 mg/kg

LCS (BWF0187-BS1) Prepared: 06/10/2013 Analyzed: 06/11/2013

TPH-Semi-Volatiles (DRO) 10.0 100 40-16083.3mg/kg83.3 mg/kg


LCS Dup (BWF0187-BSD1) Prepared: 06/10/2013 Analyzed: 06/11/2013

TPH-Semi-Volatiles (DRO) 10.0 100 2040-16086.5 3.73mg/kg86.5 mg/kg


Matrix Spike (BWF0187-MS1) Prepared: 06/10/2013 Analyzed: 06/11/2013Source: 13F0119-03

TPH-Semi-Volatiles (DRO) 10.0 100 40-16087.9mg/kg87.9 mg/kg <10.0 mg/kg

5.00 40-160Surrogate: Pentacosane 1005.01 mg/kg

Matrix Spike Dup (BWF0187-MSD1) Prepared: 06/10/2013 Analyzed: 06/11/2013Source: 13F0119-03

TPH-Semi-Volatiles (DRO) 10.0 100 2040-16080.0 9.38mg/kg80.0 mg/kg <10.0 mg/kg







TPH-Semi-Volatiles (DRO) 10.0 98.2 40-160102mg/kg99.8 mg/kg


Page 12 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





TPH-Semi-Volatiles (DRO) 10.0 98.4 2040-160108 6.76mg/kg107 mg/kg



TPH-Semi-Volatiles (DRO) 10.0 98.4 40-16090.8mg/kg89.4 mg/kg <10.0 mg/kg



TPH-Semi-Volatiles (DRO) 10.0 98.4 2040-160107 16.3mg/kg105 mg/kg <10.0 mg/kg


Page 13 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Certified Analyses included in this Report

CertificationsAnalyte

SW8015C in Solids

TPH-Semi-Volatiles (DRO) VELAP,NC,WVDEPTPH-Volatiles (GRO) VELAP,NC,WVDEP

Code Description Number Expires341Maryland DE Drinking Water 12/31/2013MdDOE495North Carolina DENR 12/13/2013NC460021NELAC-Virginia 06/15/2013VELAP350West Virginia DEP 11/01/2013WVDEP

Page 14 of 15




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Qualifiers and Definitions

Relative Percent DifferenceRPD

QualifersQual

Denotes sample was re-analyzed-RE

Page 15 of 15




Client Name:


Sincerely,

Carmela TombesLaboratory Director

Ashland, VA 23005


Purchase Order:


Date Issued:

Date Received:

Submitted To:

Client Site I.D.:

June 18, 2013 11:10


Joshua Shrader

End Notes:





Lewistown Road

Final Report




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



NP 0'-1' 13F0120-01 06/06/2013 11:40Soil 06/04/2013 08:35

S 0'-1' 13F0120-02 06/06/2013 11:40Soil 06/04/2013 09:10

HA-02 0'-1' 13F0120-04 06/06/2013 11:40Soil 06/04/2013 09:35

Lewis Ditch N 13F0120-05 06/06/2013 11:40Soil 06/04/2013 13:00

Ramp Ditch 1 13F0120-06 06/06/2013 11:40Soil 06/04/2013 14:00

Analysis for Oil and Grease was subcontracted to Test America. The subcontracted results are attached at the end of this Certificate of Analysis.

Page 2 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-01NP 0'-1'

06/04/2013 08:35

Analytical Results


Date/Time Sampled:

Metals (Total) by EPA 6000/7000 Series Methods

Arsenic SW6010C 1.38 mg/kg 06/10/2013 15:06 06/14/2013 15:59 JPV0.500

Cadmium SW6010C 0.822 mg/kg 06/10/2013 15:06 06/14/2013 15:58 JPV0.200

Chromium SW6010C 9.84 mg/kg 06/10/2013 15:06 06/14/2013 15:58 JPV0.500

Lead SW6010C 198 mg/kg 06/10/2013 15:06 06/14/2013 15:58 JPV0.500






Date/Time

13F0120-01RE1NP 0'-1'

06/04/2013 08:35

Analytical Results


Date/Time Sampled:




Page 3 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-02S 0'-1'

06/04/2013 09:10

Analytical Results


Date/Time Sampled:





Lead SW6010C 133 mg/kg 06/10/2013 15:06 06/14/2013 16:01 JPV0.500






Page 4 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-04HA-02 0'-1'

06/04/2013 09:35

Analytical Results


Date/Time Sampled:





Lead SW6010C 28.3 mg/kg 06/10/2013 15:06 06/14/2013 16:05 JPV0.500

Selenium SW6010C JPV<2.50 mg/kg 06/10/2013 15:06 06/14/2013 16:052.50

Zinc SW6010C 839 mg/kg 06/10/2013 15:06 06/14/2013 16:04 JPV0.500

Volatile Organic Compounds by GCMS

1,1,1,2-Tetrachloroethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

1,1,1-Trichloroethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00



1,1-Dichloroethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

1,1-Dichloroethylene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

1,1-Dichloropropene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

1,2,3-Trichlorobenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

1,2,3-Trichloropropane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00


1,2,4-Trimethylbenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

1,2-Dibromo-3-chloropropane (DBCP) SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

1,2-Dibromoethane (EDB) SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

1,2-Dichlorobenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00


1,2-Dichloropropane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00






Page 5 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-04HA-02 0'-1'

06/04/2013 09:35

Analytical Results


Date/Time Sampled:


2-Butanone (MEK) SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

2-Chlorotoluene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

2-Hexanone (MBK) SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00


4-Isopropyltoluene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

4-Methyl-2-pentanone (MIBK) SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Acetone SW8260B MKD<10.0 ug/kg 06/12/2013 11:21 06/12/2013 11:2110.0

Benzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Bromobenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Bromochloromethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Bromodichloromethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Bromoform SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Bromomethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Carbon disulfide SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Carbon tetrachloride SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Chlorobenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Chloroethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Chloroform SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Chloromethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

cis-1,2-Dichloroethylene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

cis-1,3-Dichloropropene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Dibromochloromethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Dibromomethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Dichlorodifluoromethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Di-isopropyl ether (DIPE) SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Ethylbenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Hexachlorobutadiene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Iodomethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Isopropylbenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Page 6 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-04HA-02 0'-1'

06/04/2013 09:35

Analytical Results


Date/Time Sampled:


m+p-Xylenes SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Methylene chloride SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Methyl-t-butyl ether (MTBE) SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Naphthalene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

n-Butylbenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

n-Propylbenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

o-Xylene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

sec-Butylbenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Styrene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

tert-Butylbenzene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Tetrachloroethylene (PCE) SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Toluene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

trans-1,2-Dichloroethylene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

trans-1,3-Dichloropropene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Trichloroethylene SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Trichlorofluoromethane SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Vinyl acetate SW8260B MKD<10.0 ug/kg 06/12/2013 11:21 06/12/2013 11:2110.0

Vinyl chloride SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

Xylenes, Total SW8260B MKD<5.00 ug/kg 06/12/2013 11:21 06/12/2013 11:215.00

80-120116 %Surrogate: 1,2-Dichloroethane-d4 06/12/2013 11:21 MKD06/12/2013 11:2185-12089.5 %Surrogate: 4-Bromofluorobenzene 06/12/2013 11:21 MKD06/12/2013 11:2178-119104 %Surrogate: Dibromofluoromethane 06/12/2013 11:21 MKD06/12/2013 11:2185-11596.1 %Surrogate: Toluene-d8 06/12/2013 11:21 MKD06/12/2013 11:21

Semivolatile Organic Compounds by GCMS

1,2,4,5-Tetrachlorobenzene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

1,2,4-Trichlorobenzene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

1,2-Dichlorobenzene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

1,2-Diphenylhydrazine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670


Page 7 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-04HA-02 0'-1'

06/04/2013 09:35

Analytical Results


Date/Time Sampled:



1-Chloronaphthalene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

1-Naphthylamine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

2,3,4,6-Tetrachlorophenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

2,4,5-Trichlorophenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670


2,4-Dichlorophenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

2,4-Dimethylphenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

2,4-Dinitrophenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

2,4-Dinitrotoluene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670




2-Chlorophenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

2-Methylnaphthalene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670


2-Nitroaniline SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

2-Nitrophenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

3,3'-Dichlorobenzidine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

3-Methylcholanthrene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670


4,6-Dinitro-2-methylphenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

4-Aminobiphenyl SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

4-Bromophenyl phenyl ether SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

4-Chloroaniline SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

4-Chlorophenyl phenyl ether SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670



7,12-Dimethylbenz (a) anthracene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Page 8 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-04HA-02 0'-1'

06/04/2013 09:35

Analytical Results


Date/Time Sampled:


Acenaphthene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Acenaphthylene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Acetophenone SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Aniline SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Anthracene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Benzidine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Benzo (a) anthracene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Benzo (a) pyrene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Benzo (b) fluoranthene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Benzo (g,h,i) perylene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Benzo (k) fluoranthene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Benzoic acid SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Benzyl alcohol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

bis (2-Chloroethoxy) methane SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

bis (2-Chloroethyl) ether SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

bis (2-Chloroisopropyl) ether SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

bis (2-Ethylhexyl) phthalate SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Butyl benzyl phthalate SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Chrysene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Dibenz (a,h) anthracene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Dibenz (a,j) acridine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Dibenzofuran SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Diethyl phthalate SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Dimethyl phthalate SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Di-n-butyl phthalate SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Di-n-octyl phthalate SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Diphenylamine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Ethyl methanesulfonate SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Fluoranthene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Page 9 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-04HA-02 0'-1'

06/04/2013 09:35

Analytical Results


Date/Time Sampled:


Fluorene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Hexachlorobenzene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Hexachlorobutadiene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Hexachlorocyclopentadiene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Hexachloroethane SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Indeno (1,2,3-cd) pyrene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Isophorone SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

m+p-Cresols SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Methyl methanesulfonate SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Naphthalene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Nitrobenzene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

n-Nitrosodimethylamine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

n-Nitrosodi-n-butylamine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

n-Nitrosodi-n-propylamine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

n-Nitrosodiphenylamine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

n-Nitrosopiperidine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

o+m+p-Cresols SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

o-Cresol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

p-(Dimethylamino) azobenzene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

p-Chloro-m-cresol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Pentachloronitrobenzene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Pentachlorophenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Phenacetin SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Phenanthrene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Phenol SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Pronamide SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Pyrene SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

Pyridine SW8270D JHV<1670 ug/kg 06/11/2013 10:25 06/12/2013 06:491670

35-12535.6 %Surrogate: 2,4,6-Tribromophenol 06/11/2013 10:25 JHV06/12/2013 06:49

Page 10 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-04HA-02 0'-1'

06/04/2013 09:35

Analytical Results


Date/Time Sampled:


45-105 %Surrogate: 2-Fluorobiphenyl DS 06/11/2013 10:25 JHV06/12/2013 06:4935-105 %Surrogate: 2-Fluorophenol DS 06/11/2013 10:25 JHV06/12/2013 06:4935-100 %Surrogate: Nitrobenzene-d5 DS 06/11/2013 10:25 JHV06/12/2013 06:4940-100 %Surrogate: Phenol-d5 DS 06/11/2013 10:25 JHV06/12/2013 06:4930-125 %Surrogate: p-Terphenyl-d14 DS 06/11/2013 10:25 JHV06/12/2013 06:49




Date/Time

13F0120-04RE1HA-02 0'-1'

06/04/2013 09:35

Analytical Results


Date/Time Sampled:






TPH-Semi-Volatiles (DRO) SW8015C 250 mg/kg 06/11/2013 16:35 06/13/2013 11:36 JHV49.6

40-16025.7 %Surrogate: Pentacosane S 06/11/2013 16:35 JHV06/13/2013 11:36

Page 11 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-05Lewis Ditch N

06/04/2013 13:00

Analytical Results


Date/Time Sampled:





Lead SW6010C 15.6 mg/kg 06/10/2013 15:06 06/14/2013 16:08 JPV0.500

Zinc SW6010C 391 mg/kg 06/10/2013 15:06 06/14/2013 16:07 JPV0.500


TPH-Volatiles (GRO) SW8015C 0.18 mg/kg 06/10/2013 18:43 06/10/2013 18:43 DMB0.10






















Page 12 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 13:00

Analytical Results


Date/Time Sampled:



2-Butanone (MEK) SW8260B MKD<5.00 ug/kg 06/12/2013 11:43 06/12/2013 11:435.00






Acetone SW8260B MKD<10.0 ug/kg 06/12/2013 11:43 06/12/2013 11:4310.0






















Page 13 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 13:00

Analytical Results


Date/Time Sampled:






















80-120101 %Surrogate: 1,2-Dichloroethane-d4 06/12/2013 11:43 MKD06/12/2013 11:4385-12095.0 %Surrogate: 4-Bromofluorobenzene 06/12/2013 11:43 MKD06/12/2013 11:4378-11999.9 %Surrogate: Dibromofluoromethane 06/12/2013 11:43 MKD06/12/2013 11:4385-11598.5 %Surrogate: Toluene-d8 06/12/2013 11:43 MKD06/12/2013 11:43

Page 14 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 13:00

Analytical Results


Date/Time Sampled:


1,2,4,5-Tetrachlorobenzene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

1,2,4-Trichlorobenzene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660


1,2-Diphenylhydrazine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660





2,3,4,6-Tetrachlorophenol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660




2,4-Dimethylphenol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

2,4-Dinitrophenol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660





2-Chlorophenol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

2-Methylnaphthalene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660




3,3'-Dichlorobenzidine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

3-Methylcholanthrene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660


4,6-Dinitro-2-methylphenol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

4-Aminobiphenyl SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

4-Bromophenyl phenyl ether SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Page 15 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 13:00

Analytical Results


Date/Time Sampled:


4-Chloroaniline SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

4-Chlorophenyl phenyl ether SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660



7,12-Dimethylbenz (a) anthracene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Acenaphthene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Acenaphthylene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Acetophenone SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Aniline SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Anthracene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Benzidine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Benzo (a) anthracene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Benzo (a) pyrene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Benzo (b) fluoranthene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Benzo (g,h,i) perylene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Benzo (k) fluoranthene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Benzoic acid SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Benzyl alcohol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

bis (2-Chloroethoxy) methane SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

bis (2-Chloroethyl) ether SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

bis (2-Chloroisopropyl) ether SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

bis (2-Ethylhexyl) phthalate SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Butyl benzyl phthalate SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Chrysene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Dibenz (a,h) anthracene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Dibenz (a,j) acridine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Dibenzofuran SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Diethyl phthalate SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Dimethyl phthalate SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Page 16 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 13:00

Analytical Results


Date/Time Sampled:


Di-n-butyl phthalate SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Di-n-octyl phthalate SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Diphenylamine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Ethyl methanesulfonate SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Fluoranthene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Fluorene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Hexachlorobenzene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Hexachlorobutadiene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Hexachlorocyclopentadiene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Hexachloroethane SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Indeno (1,2,3-cd) pyrene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Isophorone SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

m+p-Cresols SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Methyl methanesulfonate SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Naphthalene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Nitrobenzene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

n-Nitrosodimethylamine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

n-Nitrosodi-n-butylamine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

n-Nitrosodi-n-propylamine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

n-Nitrosodiphenylamine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

n-Nitrosopiperidine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

o+m+p-Cresols SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

o-Cresol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

p-(Dimethylamino) azobenzene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

p-Chloro-m-cresol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Pentachloronitrobenzene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Pentachlorophenol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Phenacetin SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Phenanthrene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Page 17 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 13:00

Analytical Results


Date/Time Sampled:


Phenol SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Pronamide SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Pyrene SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

Pyridine SW8270D JHV<1660 ug/kg 06/11/2013 10:25 06/12/2013 07:231660

35-12543.8 %Surrogate: 2,4,6-Tribromophenol 06/11/2013 10:25 JHV06/12/2013 07:2345-105 %Surrogate: 2-Fluorobiphenyl DS 06/11/2013 10:25 JHV06/12/2013 07:2335-105 %Surrogate: 2-Fluorophenol DS 06/11/2013 10:25 JHV06/12/2013 07:2335-100 %Surrogate: Nitrobenzene-d5 DS 06/11/2013 10:25 JHV06/12/2013 07:2340-100 %Surrogate: Phenol-d5 DS 06/11/2013 10:25 JHV06/12/2013 07:2330-125 %Surrogate: p-Terphenyl-d14 DS 06/11/2013 10:25 JHV06/12/2013 07:23




Date/Time

13F0120-05RE1Lewis Ditch N

06/04/2013 13:00

Analytical Results


Date/Time Sampled:




TPH-Semi-Volatiles (DRO) SW8015C 91.8 mg/kg 06/11/2013 16:35 06/13/2013 12:01 JHV49.3


Page 18 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0120-06Ramp Ditch 1

06/04/2013 14:00

Analytical Results


Date/Time Sampled:





Lead SW6010C 4.93 mg/kg 06/10/2013 15:06 06/14/2013 16:11 JPV0.500

Zinc SW6010C 3.98 mg/kg 06/10/2013 15:06 06/14/2013 16:11 JPV0.500
























Page 19 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 14:00

Analytical Results


Date/Time Sampled:



2-Butanone (MEK) SW8260B 5.08 ug/kg 06/12/2013 12:06 06/12/2013 12:06 MKD5.00




























Page 20 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 14:00

Analytical Results


Date/Time Sampled:





















80-120106 %Surrogate: 1,2-Dichloroethane-d4 06/12/2013 12:06 MKD06/12/2013 12:0685-12096.4 %Surrogate: 4-Bromofluorobenzene 06/12/2013 12:06 MKD06/12/2013 12:0678-119102 %Surrogate: Dibromofluoromethane 06/12/2013 12:06 MKD06/12/2013 12:0685-11598.1 %Surrogate: Toluene-d8 06/12/2013 12:06 MKD06/12/2013 12:06


1,2,4,5-Tetrachlorobenzene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

1,2,4-Trichlorobenzene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

1,2-Dichlorobenzene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

1,2-Diphenylhydrazine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3


Page 21 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 14:00

Analytical Results


Date/Time Sampled:



1-Chloronaphthalene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

1-Naphthylamine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,3,4,6-Tetrachlorophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,4,5-Trichlorophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,4,6-Trichlorophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,4-Dichlorophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,4-Dimethylphenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,4-Dinitrophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,4-Dinitrotoluene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,6-Dichlorophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2,6-Dinitrotoluene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2-Chloronaphthalene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2-Chlorophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2-Methylnaphthalene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2-Naphthylamine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2-Nitroaniline SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

2-Nitrophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

3,3'-Dichlorobenzidine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

3-Methylcholanthrene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3


4,6-Dinitro-2-methylphenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

4-Aminobiphenyl SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

4-Bromophenyl phenyl ether SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

4-Chloroaniline SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

4-Chlorophenyl phenyl ether SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3


4-Nitrophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

7,12-Dimethylbenz (a) anthracene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Page 22 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 14:00

Analytical Results


Date/Time Sampled:


Acenaphthene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Acenaphthylene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Acetophenone SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Aniline SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Anthracene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Benzidine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Benzo (a) anthracene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Benzo (a) pyrene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Benzo (b) fluoranthene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Benzo (g,h,i) perylene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Benzo (k) fluoranthene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Benzoic acid SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Benzyl alcohol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

bis (2-Chloroethoxy) methane SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

bis (2-Chloroethyl) ether SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

bis (2-Chloroisopropyl) ether SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

bis (2-Ethylhexyl) phthalate SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Butyl benzyl phthalate SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Chrysene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Dibenz (a,h) anthracene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Dibenz (a,j) acridine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Dibenzofuran SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Diethyl phthalate SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Dimethyl phthalate SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Di-n-butyl phthalate SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Di-n-octyl phthalate SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Diphenylamine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Ethyl methanesulfonate SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Fluoranthene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Page 23 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 14:00

Analytical Results


Date/Time Sampled:


Fluorene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Hexachlorobenzene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Hexachlorobutadiene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Hexachlorocyclopentadiene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Hexachloroethane SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Indeno (1,2,3-cd) pyrene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Isophorone SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

m+p-Cresols SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Methyl methanesulfonate SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Naphthalene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Nitrobenzene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

n-Nitrosodimethylamine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

n-Nitrosodi-n-butylamine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

n-Nitrosodi-n-propylamine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

n-Nitrosodiphenylamine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

n-Nitrosopiperidine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

o+m+p-Cresols SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

o-Cresol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

p-(Dimethylamino) azobenzene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

p-Chloro-m-cresol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Pentachloronitrobenzene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Pentachlorophenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Phenacetin SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Phenanthrene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Phenol SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Pronamide SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Pyrene SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

Pyridine SW8270D JHV<83.3 ug/kg 06/11/2013 10:25 06/12/2013 06:1483.3

35-12560.6 %Surrogate: 2,4,6-Tribromophenol 06/11/2013 10:25 JHV06/12/2013 06:14

Page 24 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 14:00

Analytical Results


Date/Time Sampled:


45-10557.0 %Surrogate: 2-Fluorobiphenyl 06/11/2013 10:25 JHV06/12/2013 06:1435-10554.8 %Surrogate: 2-Fluorophenol 06/11/2013 10:25 JHV06/12/2013 06:1435-10058.9 %Surrogate: Nitrobenzene-d5 06/11/2013 10:25 JHV06/12/2013 06:1440-10053.4 %Surrogate: Phenol-d5 06/11/2013 10:25 JHV06/12/2013 06:1430-12566.1 %Surrogate: p-Terphenyl-d14 06/11/2013 10:25 JHV06/12/2013 06:14







Date/Time

13F0120-06RE1Ramp Ditch 1

06/04/2013 14:00

Analytical Results


Date/Time Sampled:




Acetone SW8260B 520 ug/kg 06/12/2013 15:51 06/12/2013 15:51 MKD500

80-120104 %Surrogate: 1,2-Dichloroethane-d4 06/12/2013 15:51 MKD06/12/2013 15:5185-12096.7 %Surrogate: 4-Bromofluorobenzene 06/12/2013 15:51 MKD06/12/2013 15:5178-11999.5 %Surrogate: Dibromofluoromethane 06/12/2013 15:51 MKD06/12/2013 15:5185-115100 %Surrogate: Toluene-d8 06/12/2013 15:51 MKD06/12/2013 15:51

Page 25 of 51




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



13F0120-01,13F0120-02,13F0120-04,13F0120-04RE1,13F0120-05,13

F0120-05RE1,13F0120-06,13F0120-06RE1

BWF0170 SW6010C

13F0120-04,13F0120-05,13F0120-06BWF0198 SW8270D

13F0120-01,13F0120-02,13F0120-04,13F0120-05,13F0120-06BWF0214 SW8015C

13F0120-01,13F0120-01RE1,13F0120-02,13F0120-04,13F0120-04RE1

,13F0120-05,13F0120-05RE1,13F0120-06

BWF0218 SW8015C

13F0120-04RE1BWF0233 SW8015C

13F0120-04,13F0120-05,13F0120-06,13F0120-06RE1BWF0248 SW8260B

13F0120-03,13F0120-05,13F0120-06SW9071B

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Ashland VA, 23005




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Purchase Order:


Lewistown Road

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Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

Metals (Total) by EPA 6000/7000 Series Methods - Quality Control




Lead 0.500 mg/kg<0.500 mg/kg

Selenium 2.50 mg/kg<2.50 mg/kg

Arsenic 0.500 mg/kg<0.500 mg/kg

Zinc 0.500 mg/kg<0.500 mg/kg

Chromium 0.500 mg/kg<0.500 mg/kg

Cadmium 0.200 mg/kg<0.200 mg/kg


Cadmium 0.200 24.8 80-12099.8mg/kg24.8 mg/kg

Selenium 2.50 24.8 80-12090.7mg/kg22.5 mg/kg

Chromium 0.500 24.8 80-120101mg/kg25.1 mg/kg

Lead 0.500 24.8 80-12099.7mg/kg24.7 mg/kg

Arsenic 0.500 24.8 80-12099.6mg/kg24.7 mg/kg

Zinc 0.500 24.8 80-12099.7mg/kg24.7 mg/kg


Selenium 2.50 23.0 2080-12095.2 2.96mg/kg21.8 mg/kg

Lead 0.500 23.0 2080-120103 4.53mg/kg23.6 mg/kg

Chromium 0.500 23.0 2080-120105 4.43mg/kg24.0 mg/kg

Arsenic 0.500 23.0 2080-120102 5.32mg/kg23.4 mg/kg

Cadmium 0.200 23.0 2080-120103 4.88mg/kg23.6 mg/kg

Zinc 0.500 23.0 2080-120103 4.41mg/kg23.7 mg/kg

Matrix Spike (BWF0170-MS1) Prepared: 06/10/2013 Analyzed: 06/14/2013Source: 13F0100-04RE1

Lead 0.500 24.9 75-12558.1mg/kg69.1 mg/kg M54.6 mg/kg

Selenium 2.50 24.9 75-12539.4mg/kg9.81 mg/kg M<2.50 mg/kg

Cadmium 0.200 24.9 75-12567.3mg/kg20.0 mg/kg M3.28 mg/kg

Zinc 0.500 24.9 75-12571.9mg/kg61.4 mg/kg M43.5 mg/kg

Chromium 0.500 24.9 75-12562.1mg/kg42.3 mg/kg M26.8 mg/kg

Arsenic 0.500 24.9 75-12552.5mg/kg22.7 mg/kg M9.57 mg/kg

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Ashland VA, 23005




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Lewistown Road

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Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Arsenic 0.500 23.3 75-12582.8mg/kg48.0 mg/kg 28.8 mg/kg

Cadmium 0.200 23.3 75-12574.6mg/kg21.2 mg/kg M3.85 mg/kg

Lead 0.500 23.3 75-125144mg/kg166 mg/kg M132 mg/kg

Chromium 0.500 23.3 75-12568.5mg/kg39.9 mg/kg M23.9 mg/kg

Zinc 0.500 23.3 75-12577.3mg/kg51.3 mg/kg 33.3 mg/kg

Matrix Spike Dup (BWF0170-MSD1) Prepared: 06/10/2013 Analyzed: 06/14/2013Source: 13F0100-04RE1

Chromium 0.500 24.0 2075-12582.5 9.69mg/kg46.6 mg/kg 26.8 mg/kg

Arsenic 0.500 24.0 2075-12558.1 3.68mg/kg23.5 mg/kg M9.57 mg/kg

Zinc 0.500 24.0 2075-12572.2 0.967mg/kg60.8 mg/kg M43.5 mg/kg

Cadmium 0.200 24.0 2075-12572.5 3.06mg/kg20.7 mg/kg M3.28 mg/kg

Selenium 2.50 24.0 2075-12541.3 1.00mg/kg9.91 mg/kg M<2.50 mg/kg

Lead 0.500 24.0 2075-12569.6 3.13mg/kg71.3 mg/kg M54.6 mg/kg


Arsenic 0.500 24.9 2075-12552.5 13.8mg/kg41.8 mg/kg M28.8 mg/kg

Lead 0.500 24.9 2075-1258.51 20.9mg/kg135 mg/kg M, P132 mg/kg

Chromium 0.500 24.9 2075-12583.9 11.7mg/kg44.8 mg/kg 23.9 mg/kg

Cadmium 0.200 24.9 2075-12579.8 11.2mg/kg23.7 mg/kg 3.85 mg/kg

Zinc 0.500 24.9 2075-12581.6 4.44mg/kg53.7 mg/kg 33.3 mg/kg

Page 28 of 51




Ashland VA, 23005




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Lewistown Road

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Reporting

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Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte









100 80-120Surrogate: 2,5-Dibromotoluene [2C] 100100 ug/L








TPH-Volatiles (GRO) 0.10 0.967 2070-13090.3 1.26mg/kg0.87 mg/kg <0.10 mg/kg









Page 29 of 51




Ashland VA, 23005




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Lewistown Road

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RPD

Limit Qual Analyte







Page 30 of 51




Ashland VA, 23005




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Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

Volatile Organic Compounds by GCMS - Quality Control




1,1,1,2-Tetrachloroethane 5.00 ug/kg<5.00 ug/kg

1,1,1-Trichloroethane 5.00 ug/kg<5.00 ug/kg



1,1-Dichloroethane 5.00 ug/kg<5.00 ug/kg

1,1-Dichloroethylene 5.00 ug/kg<5.00 ug/kg

1,1-Dichloropropene 5.00 ug/kg<5.00 ug/kg

1,2,3-Trichlorobenzene 5.00 ug/kg<5.00 ug/kg

1,2,3-Trichloropropane 5.00 ug/kg<5.00 ug/kg


1,2,4-Trimethylbenzene 5.00 ug/kg<5.00 ug/kg

1,2-Dibromo-3-chloropropane (DBCP) 5.00 ug/kg<5.00 ug/kg

1,2-Dibromoethane (EDB) 5.00 ug/kg<5.00 ug/kg

1,2-Dichlorobenzene 5.00 ug/kg<5.00 ug/kg


1,2-Dichloropropane 5.00 ug/kg<5.00 ug/kg






2-Butanone (MEK) 5.00 ug/kg<5.00 ug/kg

2-Chlorotoluene 5.00 ug/kg<5.00 ug/kg

2-Hexanone (MBK) 5.00 ug/kg<5.00 ug/kg


4-Isopropyltoluene 5.00 ug/kg<5.00 ug/kg

4-Methyl-2-pentanone (MIBK) 5.00 ug/kg<5.00 ug/kg

Acetone 10.0 ug/kg<10.0 ug/kg

Benzene 5.00 ug/kg<5.00 ug/kg

Bromobenzene 5.00 ug/kg<5.00 ug/kg

Bromochloromethane 5.00 ug/kg<5.00 ug/kg

Bromodichloromethane 5.00 ug/kg<5.00 ug/kg

Bromoform 5.00 ug/kg<5.00 ug/kg

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Ashland VA, 23005




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Limits RPD

RPD

Limit Qual Analyte





Bromomethane 5.00 ug/kg<5.00 ug/kg

Carbon disulfide 5.00 ug/kg<5.00 ug/kg

Carbon tetrachloride 5.00 ug/kg<5.00 ug/kg

Chlorobenzene 5.00 ug/kg<5.00 ug/kg

Chloroethane 5.00 ug/kg<5.00 ug/kg

Chloroform 5.00 ug/kg<5.00 ug/kg

Chloromethane 5.00 ug/kg<5.00 ug/kg

cis-1,2-Dichloroethylene 5.00 ug/kg<5.00 ug/kg

cis-1,3-Dichloropropene 5.00 ug/kg<5.00 ug/kg

Dibromochloromethane 5.00 ug/kg<5.00 ug/kg

Dibromomethane 5.00 ug/kg<5.00 ug/kg

Dichlorodifluoromethane 5.00 ug/kg<5.00 ug/kg

Di-isopropyl ether (DIPE) 5.00 ug/kg<5.00 ug/kg

Ethylbenzene 5.00 ug/kg<5.00 ug/kg

Hexachlorobutadiene 5.00 ug/kg<5.00 ug/kg

Iodomethane 5.00 ug/kg<5.00 ug/kg

Isopropylbenzene 5.00 ug/kg<5.00 ug/kg

m+p-Xylenes 5.00 ug/kg<5.00 ug/kg

Methylene chloride 5.00 ug/kg<5.00 ug/kg

Methyl-t-butyl ether (MTBE) 5.00 ug/kg<5.00 ug/kg

Naphthalene 5.00 ug/kg<5.00 ug/kg

n-Butylbenzene 5.00 ug/kg<5.00 ug/kg

n-Propylbenzene 5.00 ug/kg<5.00 ug/kg

o-Xylene 5.00 ug/kg<5.00 ug/kg

sec-Butylbenzene 5.00 ug/kg<5.00 ug/kg

Styrene 5.00 ug/kg<5.00 ug/kg

tert-Butylbenzene 5.00 ug/kg<5.00 ug/kg

Tetrachloroethylene (PCE) 5.00 ug/kg<5.00 ug/kg

Toluene 5.00 ug/kg<5.00 ug/kg

trans-1,2-Dichloroethylene 5.00 ug/kg<5.00 ug/kg

trans-1,3-Dichloropropene 5.00 ug/kg<5.00 ug/kg

Trichloroethylene 5.00 ug/kg<5.00 ug/kg

Trichlorofluoromethane 5.00 ug/kg<5.00 ug/kg

Page 32 of 51




Ashland VA, 23005




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Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Vinyl acetate 10.0 ug/kg<10.0 ug/kg

Vinyl chloride 5.00 ug/kg<5.00 ug/kg

Xylenes, Total 5.00 ug/kg<5.00 ug/kg

50.0 80-120Surrogate: 1,2-Dichloroethane-d4 10251.1 ug/L

50.0 85-120Surrogate: 4-Bromofluorobenzene 97.448.7 ug/L

50.0 78-119Surrogate: Dibromofluoromethane 10050.1 ug/L

50.0 85-115Surrogate: Toluene-d8 99.149.6 ug/L


1,1,1,2-Tetrachloroethane 50.0 75-12589.8ug/L44.9 ug/L

1,1,1-Trichloroethane 50.0 70-13587.1ug/L43.5 ug/L

1,1,2,2-Tetrachloroethane 50.0 55-130111ug/L55.4 ug/L

1,1,2-Trichloroethane 50.0 60-125104ug/L52.2 ug/L

1,1-Dichloroethane 50.0 75-12590.3ug/L45.1 ug/L

1,1-Dichloroethylene 50.0 65-13587.3ug/L43.6 ug/L

1,1-Dichloropropene 50.0 70-13587.4ug/L43.7 ug/L

1,2,3-Trichlorobenzene 50.0 60-135102ug/L50.9 ug/L

1,2,3-Trichloropropane 50.0 65-130115ug/L57.3 ug/L


1,2,4-Trimethylbenzene 50.0 65-13592.1ug/L46.0 ug/L

1,2-Dibromo-3-chloropropane (DBCP) 50.0 40-135128ug/L63.9 ug/L

1,2-Dibromoethane (EDB) 50.0 70-125105ug/L52.4 ug/L

1,2-Dichlorobenzene 50.0 75-120101ug/L50.6 ug/L

1,2-Dichloroethane 50.0 70-13595.1ug/L47.5 ug/L

1,2-Dichloropropane 50.0 70-12095.4ug/L47.7 ug/L

1,3,5-Trimethylbenzene 50.0 65-13589.9ug/L44.9 ug/L


1,3-Dichloropropane 50.0 75-125102ug/L50.8 ug/L

1,4-Dichlorobenzene 50.0 70-12596.1ug/L48.0 ug/L

2,2-Dichloropropane 50.0 65-13591.0ug/L45.5 ug/L

2-Butanone (MEK) 50.0 30-160186ug/L92.8 ug/L L

2-Chlorotoluene 50.0 70-130100ug/L50.2 ug/L

2-Hexanone (MBK) 50.0 45-145156ug/L78.2 ug/L L

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Reporting

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Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





4-Chlorotoluene 50.0 75-125101ug/L50.6 ug/L

4-Isopropyltoluene 50.0 75-13597.8ug/L48.9 ug/L

4-Methyl-2-pentanone (MIBK) 50.0 45-145138ug/L69.2 ug/L

Acetone 50.0 20-160234ug/L117 ug/L L

Benzene 50.0 75-12588.4ug/L44.2 ug/L

Bromobenzene 50.0 65-12091.0ug/L45.5 ug/L

Bromochloromethane 50.0 70-12597.0ug/L48.5 ug/L

Bromodichloromethane 50.0 70-13091.9ug/L45.9 ug/L

Bromoform 50.0 55-13598.7ug/L49.4 ug/L

Bromomethane 50.0 30-16090.2ug/L45.1 ug/L

Carbon disulfide 50.0 45-16086.9ug/L43.5 ug/L

Carbon tetrachloride 50.0 65-13586.2ug/L43.1 ug/L

Chlorobenzene 50.0 75-12595.4ug/L47.7 ug/L

Chloroethane 50.0 40-15582.5ug/L41.3 ug/L

Chloroform 50.0 70-12588.5ug/L44.3 ug/L

Chloromethane 50.0 50-13080.2ug/L40.1 ug/L

cis-1,2-Dichloroethylene 50.0 65-12587.2ug/L43.6 ug/L

cis-1,3-Dichloropropene 50.0 70-12593.7ug/L46.9 ug/L

Dibromochloromethane 50.0 65-130101ug/L50.7 ug/L

Dibromomethane 50.0 75-130101ug/L50.5 ug/L

Dichlorodifluoromethane 50.0 35-13555.5ug/L27.7 ug/L

Ethylbenzene 50.0 75-12589.0ug/L44.5 ug/L

Hexachlorobutadiene 50.0 55-14087.5ug/L43.7 ug/L

Isopropylbenzene 50.0 75-13094.3ug/L47.2 ug/L

m+p-Xylenes 100 80-12593.9ug/L93.9 ug/L

Methylene chloride 50.0 55-14092.5ug/L46.2 ug/L

Methyl-t-butyl ether (MTBE) 50.0 65-125106ug/L52.8 ug/L

Naphthalene 50.0 40-125113ug/L56.3 ug/L

n-Butylbenzene 50.0 65-14094.3ug/L47.1 ug/L

n-Propylbenzene 50.0 65-135100ug/L50.2 ug/L

o-Xylene 50.0 75-12596.6ug/L48.3 ug/L

sec-Butylbenzene 50.0 65-13096.1ug/L48.1 ug/L

Styrene 50.0 75-12596.2ug/L48.1 ug/L

Page 34 of 51




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Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





tert-Butylbenzene 50.0 65-130100ug/L50.0 ug/L

Tetrachloroethylene (PCE) 50.0 65-14087.9ug/L43.9 ug/L

Toluene 50.0 70-12588.4ug/L44.2 ug/L

trans-1,2-Dichloroethylene 50.0 65-13584.7ug/L42.4 ug/L

trans-1,3-Dichloropropene 50.0 65-125104ug/L52.1 ug/L

Trichloroethylene 50.0 75-12588.7ug/L44.4 ug/L

Trichlorofluoromethane 50.0 25-18570.7ug/L35.4 ug/L

Vinyl chloride 50.0 60-12563.0ug/L31.5 ug/L


50.0 85-120Surrogate: 4-Bromofluorobenzene 10251.2 ug/L

50.0 78-119Surrogate: Dibromofluoromethane 10250.9 ug/L



1,1,1,2-Tetrachloroethane 50.0 3075-12593.2 3.71ug/L46.6 ug/L

1,1,1-Trichloroethane 50.0 3070-13589.4 2.62ug/L44.7 ug/L

1,1,2,2-Tetrachloroethane 50.0 3055-130105 4.97ug/L52.7 ug/L

1,1,2-Trichloroethane 50.0 3060-125101 2.81ug/L50.7 ug/L

1,1-Dichloroethane 50.0 3075-12592.8 2.78ug/L46.4 ug/L

1,1-Dichloroethylene 50.0 3065-13591.1 4.28ug/L45.6 ug/L

1,1-Dichloropropene 50.0 3070-13590.2 3.17ug/L45.1 ug/L

1,2,3-Trichlorobenzene 50.0 3060-135104 2.42ug/L52.2 ug/L

1,2,3-Trichloropropane 50.0 3065-130108 6.23ug/L53.9 ug/L


1,2,4-Trimethylbenzene 50.0 3065-13595.9 4.12ug/L48.0 ug/L

1,2-Dibromo-3-chloropropane (DBCP) 50.0 3040-135120 6.13ug/L60.1 ug/L

1,2-Dibromoethane (EDB) 50.0 3070-125104 1.11ug/L51.9 ug/L

1,2-Dichlorobenzene 50.0 3075-120105 3.88ug/L52.6 ug/L

1,2-Dichloroethane 50.0 3070-13595.3 0.237ug/L47.7 ug/L

1,2-Dichloropropane 50.0 3070-12094.9 0.570ug/L47.4 ug/L

1,3,5-Trimethylbenzene 50.0 3065-13593.9 4.39ug/L47.0 ug/L


1,3-Dichloropropane 50.0 3075-125100 1.55ug/L50.0 ug/L

Page 35 of 51




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Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





1,4-Dichlorobenzene 50.0 3070-12596.6 0.567ug/L48.3 ug/L

2,2-Dichloropropane 50.0 3065-13593.8 3.02ug/L46.9 ug/L

2-Butanone (MEK) 50.0 3030-160166 11.1ug/L83.0 ug/L L

2-Chlorotoluene 50.0 3070-130106 5.85ug/L53.2 ug/L

2-Hexanone (MBK) 50.0 3045-145141 10.1ug/L70.7 ug/L

4-Chlorotoluene 50.0 3075-125106 4.18ug/L52.8 ug/L

4-Isopropyltoluene 50.0 3075-135102 4.66ug/L51.2 ug/L

4-Methyl-2-pentanone (MIBK) 50.0 3045-145123 11.6ug/L61.6 ug/L

Acetone 50.0 3020-160201 15.4ug/L100 ug/L L

Benzene 50.0 3075-12591.0 2.97ug/L45.5 ug/L

Bromobenzene 50.0 3065-12093.9 3.19ug/L47.0 ug/L

Bromochloromethane 50.0 3070-12597.0 0.0454ug/L48.5 ug/L

Bromodichloromethane 50.0 3070-13095.4 3.72ug/L47.7 ug/L

Bromoform 50.0 3055-13598.6 0.150ug/L49.3 ug/L

Bromomethane 50.0 3030-16098.1 8.42ug/L49.1 ug/L

Carbon disulfide 50.0 3045-16088.0 1.24ug/L44.0 ug/L

Carbon tetrachloride 50.0 3065-13588.3 2.41ug/L44.2 ug/L

Chlorobenzene 50.0 3075-12599.1 3.79ug/L49.5 ug/L

Chloroethane 50.0 3040-15583.6 1.23ug/L41.8 ug/L

Chloroform 50.0 3070-12591.1 2.81ug/L45.5 ug/L

Chloromethane 50.0 3050-13082.1 2.31ug/L41.1 ug/L

cis-1,2-Dichloroethylene 50.0 3065-12590.4 3.53ug/L45.2 ug/L

cis-1,3-Dichloropropene 50.0 3070-12595.0 1.32ug/L47.5 ug/L

Dibromochloromethane 50.0 3065-130102 0.560ug/L51.0 ug/L

Dibromomethane 50.0 3075-130101 0.362ug/L50.7 ug/L

Dichlorodifluoromethane 50.0 3035-13557.8 4.04ug/L28.9 ug/L

Ethylbenzene 50.0 3075-12593.3 4.73ug/L46.6 ug/L

Hexachlorobutadiene 50.0 3055-14093.4 6.54ug/L46.7 ug/L

Isopropylbenzene 50.0 3075-13098.5 4.30ug/L49.2 ug/L

m+p-Xylenes 100 3080-12597.0 3.21ug/L97.0 ug/L

Methylene chloride 50.0 3055-14094.2 1.84ug/L47.1 ug/L

Methyl-t-butyl ether (MTBE) 50.0 3065-125105 0.914ug/L52.4 ug/L

Naphthalene 50.0 3040-125111 1.47ug/L55.5 ug/L

Page 36 of 51




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Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





n-Butylbenzene 50.0 3065-14098.4 4.29ug/L49.2 ug/L

n-Propylbenzene 50.0 3065-135104 3.16ug/L51.9 ug/L

o-Xylene 50.0 3075-125101 4.95ug/L50.7 ug/L

sec-Butylbenzene 50.0 3065-13099.9 3.86ug/L50.0 ug/L

Styrene 50.0 3075-12597.2 1.09ug/L48.6 ug/L

tert-Butylbenzene 50.0 3065-130103 3.09ug/L51.6 ug/L

Tetrachloroethylene (PCE) 50.0 3065-14090.2 2.57ug/L45.1 ug/L

Toluene 50.0 3070-12591.4 3.31ug/L45.7 ug/L

trans-1,2-Dichloroethylene 50.0 3065-13587.1 2.79ug/L43.6 ug/L

trans-1,3-Dichloropropene 50.0 3065-125104 0.294ug/L51.9 ug/L

Trichloroethylene 50.0 3075-12591.5 3.10ug/L45.8 ug/L

Trichlorofluoromethane 50.0 3025-18572.4 2.38ug/L36.2 ug/L

Vinyl chloride 50.0 3060-12568.8 8.75ug/L34.4 ug/L



50.0 78-119Surrogate: Dibromofluoromethane 99.849.9 ug/L


Page 37 of 51




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Lewistown Road

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Reporting

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Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

Semivolatile Organic Compounds by GCMS - Quality Control




1,2,4,5-Tetrachlorobenzene 83.3 ug/kg<83.3 ug/kg



1,2-Diphenylhydrazine 83.3 ug/kg<83.3 ug/kg



1-Chloronaphthalene 83.3 ug/kg<83.3 ug/kg

1-Naphthylamine 83.3 ug/kg<83.3 ug/kg

2,3,4,6-Tetrachlorophenol 83.3 ug/kg<83.3 ug/kg

2,4,5-Trichlorophenol 83.3 ug/kg<83.3 ug/kg

2,4,6-Trichlorophenol 83.3 ug/kg<83.3 ug/kg

2,4-Dichlorophenol 83.3 ug/kg<83.3 ug/kg

2,4-Dimethylphenol 83.3 ug/kg<83.3 ug/kg

2,4-Dinitrophenol 83.3 ug/kg<83.3 ug/kg

2,4-Dinitrotoluene 83.3 ug/kg<83.3 ug/kg

2,6-Dichlorophenol 83.3 ug/kg<83.3 ug/kg

2,6-Dinitrotoluene 83.3 ug/kg<83.3 ug/kg

2-Chloronaphthalene 83.3 ug/kg<83.3 ug/kg

2-Chlorophenol 83.3 ug/kg<83.3 ug/kg

2-Methylnaphthalene 83.3 ug/kg<83.3 ug/kg

2-Naphthylamine 83.3 ug/kg<83.3 ug/kg

2-Nitroaniline 83.3 ug/kg<83.3 ug/kg

2-Nitrophenol 83.3 ug/kg<83.3 ug/kg

3,3'-Dichlorobenzidine 83.3 ug/kg<83.3 ug/kg

3-Methylcholanthrene 83.3 ug/kg<83.3 ug/kg


4,6-Dinitro-2-methylphenol 83.3 ug/kg<83.3 ug/kg

4-Aminobiphenyl 83.3 ug/kg<83.3 ug/kg

4-Bromophenyl phenyl ether 83.3 ug/kg<83.3 ug/kg

4-Chloroaniline 83.3 ug/kg<83.3 ug/kg

4-Chlorophenyl phenyl ether 83.3 ug/kg<83.3 ug/kg


4-Nitrophenol 83.3 ug/kg<83.3 ug/kg

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Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





7,12-Dimethylbenz (a) anthracene 83.3 ug/kg<83.3 ug/kg

Acenaphthene 83.3 ug/kg<83.3 ug/kg

Acenaphthylene 83.3 ug/kg<83.3 ug/kg

Acetophenone 83.3 ug/kg<83.3 ug/kg

Aniline 83.3 ug/kg<83.3 ug/kg

Anthracene 83.3 ug/kg<83.3 ug/kg

Benzidine 83.3 ug/kg<83.3 ug/kg

Benzo (a) anthracene 83.3 ug/kg<83.3 ug/kg

Benzo (a) pyrene 83.3 ug/kg<83.3 ug/kg

Benzo (b) fluoranthene 83.3 ug/kg<83.3 ug/kg

Benzo (g,h,i) perylene 83.3 ug/kg<83.3 ug/kg

Benzo (k) fluoranthene 83.3 ug/kg<83.3 ug/kg

Benzoic acid 83.3 ug/kg<83.3 ug/kg

Benzyl alcohol 83.3 ug/kg<83.3 ug/kg

bis (2-Chloroethoxy) methane 83.3 ug/kg<83.3 ug/kg

bis (2-Chloroethyl) ether 83.3 ug/kg<83.3 ug/kg

bis (2-Chloroisopropyl) ether 83.3 ug/kg<83.3 ug/kg

bis (2-Ethylhexyl) phthalate 83.3 ug/kg<83.3 ug/kg

Butyl benzyl phthalate 83.3 ug/kg<83.3 ug/kg

Chrysene 83.3 ug/kg<83.3 ug/kg

Dibenz (a,h) anthracene 83.3 ug/kg<83.3 ug/kg

Dibenz (a,j) acridine 83.3 ug/kg<83.3 ug/kg

Dibenzofuran 83.3 ug/kg<83.3 ug/kg

Diethyl phthalate 83.3 ug/kg<83.3 ug/kg

Dimethyl phthalate 83.3 ug/kg<83.3 ug/kg

Di-n-butyl phthalate 83.3 ug/kg<83.3 ug/kg

Di-n-octyl phthalate 83.3 ug/kg<83.3 ug/kg

Diphenylamine 83.3 ug/kg<83.3 ug/kg

Ethyl methanesulfonate 83.3 ug/kg<83.3 ug/kg

Fluoranthene 83.3 ug/kg<83.3 ug/kg

Fluorene 83.3 ug/kg<83.3 ug/kg

Hexachlorobenzene 83.3 ug/kg<83.3 ug/kg


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Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Hexachlorocyclopentadiene 83.3 ug/kg<83.3 ug/kg

Hexachloroethane 83.3 ug/kg<83.3 ug/kg

Indeno (1,2,3-cd) pyrene 83.3 ug/kg<83.3 ug/kg

Isophorone 83.3 ug/kg<83.3 ug/kg

m+p-Cresols 83.3 ug/kg<83.3 ug/kg

Methyl methanesulfonate 83.3 ug/kg<83.3 ug/kg


Nitrobenzene 83.3 ug/kg<83.3 ug/kg

n-Nitrosodimethylamine 83.3 ug/kg<83.3 ug/kg

n-Nitrosodi-n-butylamine 83.3 ug/kg<83.3 ug/kg

n-Nitrosodi-n-propylamine 83.3 ug/kg<83.3 ug/kg

n-Nitrosodiphenylamine 83.3 ug/kg<83.3 ug/kg

n-Nitrosopiperidine 83.3 ug/kg<83.3 ug/kg

o+m+p-Cresols 83.3 ug/kg<83.3 ug/kg

o-Cresol 83.3 ug/kg<83.3 ug/kg

p-(Dimethylamino) azobenzene 83.3 ug/kg<83.3 ug/kg

p-Chloro-m-cresol 83.3 ug/kg<83.3 ug/kg

Pentachloronitrobenzene 83.3 ug/kg<83.3 ug/kg

Pentachlorophenol 83.3 ug/kg<83.3 ug/kg

Phenacetin 83.3 ug/kg<83.3 ug/kg

Phenanthrene 83.3 ug/kg<83.3 ug/kg

Phenol 83.3 ug/kg<83.3 ug/kg

Pronamide 83.3 ug/kg<83.3 ug/kg

Pyrene 83.3 ug/kg<83.3 ug/kg

Pyridine 83.3 ug/kg<83.3 ug/kg

3320 35-125Surrogate: 2,4,6-Tribromophenol 73.42440 ug/kg

1660 45-105Surrogate: 2-Fluorobiphenyl 69.81160 ug/kg

3320 35-105Surrogate: 2-Fluorophenol 62.72080 ug/kg

1660 35-100Surrogate: Nitrobenzene-d5 72.41200 ug/kg

3320 40-100Surrogate: Phenol-d5 61.82050 ug/kg

1660 30-125Surrogate: p-Terphenyl-d14 83.71390 ug/kg

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Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





1,2,4-Trichlorobenzene 83.3 1610 44-142ug/kg<83.3 ug/kg L

1,4-Dichlorobenzene 83.3 1620 20-124ug/kg<83.3 ug/kg L

4-Nitrophenol 83.3 3240 15-14067.6ug/kg2190 ug/kg

Acenaphthene 83.3 1610 45-11052.4ug/kg843 ug/kg

n-Nitrosodi-n-propylamine 83.3 1610 40-11570.3ug/kg1130 ug/kg

Pentachlorophenol 83.3 3200 25-12076.0ug/kg2430 ug/kg

Phenol 83.3 3240 40-100ug/kg<83.3 ug/kg L

Pyrene 83.3 1620 45-12577.1ug/kg1250 ug/kg


1620 45-105Surrogate: 2-Fluorobiphenyl 44.2716 ug/kg S

3240 35-105Surrogate: 2-Fluorophenol ND ug/kg S

1620 35-100Surrogate: Nitrobenzene-d5 5.3286.1 ug/kg S

3240 40-100Surrogate: Phenol-d5 ND ug/kg S



1,2,4-Trichlorobenzene 83.3 1620 2044-14267.3ug/kg1090 ug/kg

1,4-Dichlorobenzene 83.3 1630 2020-12450.1 200ug/kg819 ug/kg P

4-Nitrophenol 83.3 3270 2015-14064.3 4.12ug/kg2100 ug/kg

Acenaphthene 83.3 1630 2045-11060.1 14.8ug/kg977 ug/kg

n-Nitrosodi-n-propylamine 83.3 1630 2040-11580.6 14.7ug/kg1310 ug/kg

Pentachlorophenol 83.3 3240 2025-12075.0 0.274ug/kg2430 ug/kg

Phenol 83.3 3270 2040-10049.6ug/kg1620 ug/kg

Pyrene 83.3 1630 2045-12578.4 2.66ug/kg1280 ug/kg







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Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





1,2,4-Trichlorobenzene 83.3 1630 44-14245.6ug/kg745 ug/kg <83.3 ug/kg

1,4-Dichlorobenzene 83.3 1640 20-12436.8ug/kg606 ug/kg <83.3 ug/kg

4-Nitrophenol 83.3 3290 15-14036.9ug/kg1210 ug/kg <83.3 ug/kg

Acenaphthene 83.3 1640 45-11034.9ug/kg571 ug/kg M<83.3 ug/kg

n-Nitrosodi-n-propylamine 83.3 1640 40-11545.6ug/kg748 ug/kg <83.3 ug/kg

Pentachlorophenol 83.3 3260 25-12043.5ug/kg1420 ug/kg <83.3 ug/kg

Phenol 83.3 3290 40-10034.7ug/kg1140 ug/kg M<83.3 ug/kg

Pyrene 83.3 1640 45-12546.6ug/kg766 ug/kg <83.3 ug/kg


1640 45-105Surrogate: 2-Fluorobiphenyl 38.7637 ug/kg S



3290 40-100Surrogate: Phenol-d5 37.01220 ug/kg S



1,2,4-Trichlorobenzene 83.3 1630 2044-14252.6 14.3ug/kg860 ug/kg <83.3 ug/kg

1,4-Dichlorobenzene 83.3 1640 2020-12442.1 13.4ug/kg692 ug/kg <83.3 ug/kg

4-Nitrophenol 83.3 3290 2015-14071.7 64.1ug/kg2360 ug/kg P<83.3 ug/kg

Acenaphthene 83.3 1640 2045-11054.4 43.6ug/kg890 ug/kg P<83.3 ug/kg

n-Nitrosodi-n-propylamine 83.3 1640 2040-11557.1 22.3ug/kg935 ug/kg P<83.3 ug/kg

Pentachlorophenol 83.3 3260 2025-12088.9 68.6ug/kg2890 ug/kg P<83.3 ug/kg

Phenol 83.3 3290 2040-10041.5 17.9ug/kg1370 ug/kg <83.3 ug/kg

Pyrene 83.3 1640 2045-12583.8 57.1ug/kg1380 ug/kg P<83.3 ug/kg







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Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte








TPH-Semi-Volatiles (DRO) 10.0 98.2 40-160102mg/kg99.8 mg/kg



TPH-Semi-Volatiles (DRO) 10.0 98.4 2040-160108 6.76mg/kg107 mg/kg



TPH-Semi-Volatiles (DRO) 10.0 98.4 40-16090.8mg/kg89.4 mg/kg <10.0 mg/kg



TPH-Semi-Volatiles (DRO) 10.0 98.4 2040-160107 16.3mg/kg105 mg/kg <10.0 mg/kg


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SW6010C in Solids

Arsenic VELAP,NCCadmium VELAP,NC,WVDEPChromium VELAP,NCLead VELAP,NC,WVDEPSelenium VELAP,NC,WVDEPZinc VELAP,NC

SW8015C in Solids


SW8260B in Solids

1,1,1,2-Tetrachloroethane NC,VELAP1,1,1-Trichloroethane NC,VELAP1,1,2,2-Tetrachloroethane NC,VELAP1,1,2-Trichloroethane NC,VELAP1,1-Dichloroethane NC,VELAP1,1-Dichloroethylene NC,VELAP1,1-Dichloropropene NC,VELAP1,2,3-Trichlorobenzene NC,VELAP1,2,3-Trichloropropane NC,VELAP1,2,4-Trichlorobenzene NC,VELAP1,2,4-Trimethylbenzene NC,VELAP1,2-Dibromo-3-chloropropane (DBCP) NC,VELAP1,2-Dibromoethane (EDB) NC,VELAP1,2-Dichlorobenzene NC,VELAP1,2-Dichloroethane NC,VELAP1,2-Dichloropropane NC,VELAP1,3,5-Trimethylbenzene NC,VELAP

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1,3-Dichlorobenzene NC,VELAP1,3-Dichloropropane NC,VELAP1,4-Dichlorobenzene NC,VELAP2,2-Dichloropropane NC,VELAP2-Butanone (MEK) NC,VELAP2-Chlorotoluene NC,VELAP2-Hexanone (MBK) NC,VELAP4-Chlorotoluene NC,VELAP4-Isopropyltoluene NC,VELAP4-Methyl-2-pentanone (MIBK) NC,VELAPAcetone NC,VELAPBenzene NC,VELAPBromobenzene NC,VELAPBromochloromethane NC,VELAPBromodichloromethane NC,VELAPBromoform NC,VELAPBromomethane NC,VELAPCarbon disulfide NC,VELAPCarbon tetrachloride NC,VELAPChlorobenzene NC,VELAPChloroethane NC,VELAPChloroform NC,VELAPChloromethane NC,VELAPcis-1,2-Dichloroethylene NC,VELAPcis-1,3-Dichloropropene NC,VELAPDibromochloromethane NC,VELAPDibromomethane NC,VELAPDichlorodifluoromethane NC,VELAPDi-isopropyl ether (DIPE) NC,VELAP

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Ethylbenzene NC,VELAPHexachlorobutadiene NC,VELAPIodomethane NC,VELAPIsopropylbenzene NC,VELAPm+p-Xylenes NC,VELAPMethylene chloride NC,VELAPMethyl-t-butyl ether (MTBE) NC,VELAPNaphthalene NC,VELAPn-Butylbenzene NC,VELAPn-Propylbenzene NC,VELAPo-Xylene NC,VELAPsec-Butylbenzene NC,VELAPStyrene NC,VELAPtert-Butylbenzene NC,VELAPTetrachloroethylene (PCE) NC,VELAPToluene NC,VELAPtrans-1,2-Dichloroethylene NC,VELAPtrans-1,3-Dichloropropene NC,VELAPTrichloroethylene NC,VELAPTrichlorofluoromethane NC,VELAPVinyl acetate NC,VELAPVinyl chloride NC,VELAPXylenes, Total NC,VELAPDibromofluoromethane VELAP

SW8270D in Solids

1,2,4,5-Tetrachlorobenzene NC,VELAP1,2,4-Trichlorobenzene NC,VELAP1,2-Dichlorobenzene NC,VELAP1,2-Diphenylhydrazine NC,VELAP

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1,3-Dichlorobenzene NC,VELAP1,4-Dichlorobenzene NC,VELAP1-Chloronaphthalene NC,VELAP1-Naphthylamine NC,VELAP2,3,4,6-Tetrachlorophenol NC,VELAP2,4,5-Trichlorophenol NC,VELAP2,4,6-Trichlorophenol NC,VELAP2,4-Dichlorophenol NC,VELAP2,4-Dimethylphenol NC,VELAP2,4-Dinitrophenol NC,VELAP2,4-Dinitrotoluene NC,VELAP2,6-Dichlorophenol NC,VELAP2,6-Dinitrotoluene NC,VELAP2-Chloronaphthalene NC,VELAP2-Chlorophenol NC,VELAP2-Methylnaphthalene NC,VELAP2-Naphthylamine NC,VELAP2-Nitroaniline NC,VELAP2-Nitrophenol NC,VELAP3,3'-Dichlorobenzidine NC,VELAP3-Methylcholanthrene NC,VELAP3-Nitroaniline NC,VELAP4,6-Dinitro-2-methylphenol NC,VELAP4-Aminobiphenyl NC,VELAP4-Bromophenyl phenyl ether NC,VELAP4-Chloroaniline NC,VELAP4-Chlorophenyl phenyl ether NC,VELAP4-Nitroaniline NC,VELAP4-Nitrophenol NC,VELAP

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7,12-Dimethylbenz (a) anthracene NC,VELAPAcenaphthene NC,VELAPAcenaphthylene NC,VELAPAcetophenone NC,VELAPAniline NC,VELAPAnthracene NC,VELAPBenzidine NC,VELAPBenzo (a) anthracene NC,VELAPBenzo (a) pyrene NC,VELAPBenzo (b) fluoranthene NC,VELAPBenzo (g,h,i) perylene NC,VELAPBenzo (k) fluoranthene NC,VELAPBenzoic acid NC,VELAPBenzyl alcohol NC,VELAPbis (2-Chloroethoxy) methane NC,VELAPbis (2-Chloroethyl) ether NC,VELAPbis (2-Chloroisopropyl) ether NC,VELAPbis (2-Ethylhexyl) phthalate NC,VELAPButyl benzyl phthalate NC,VELAPChrysene NC,VELAPDibenz (a,h) anthracene NC,VELAPDibenz (a,j) acridine NC,VELAPDibenzofuran NC,VELAPDiethyl phthalate NC,VELAPDimethyl phthalate NC,VELAPDi-n-butyl phthalate NC,VELAPDi-n-octyl phthalate NC,VELAPDiphenylamine NC,VELAPEthyl methanesulfonate NC,VELAP

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Fluoranthene NC,VELAPFluorene NC,VELAPHexachlorobenzene NC,VELAPHexachlorobutadiene NC,VELAPHexachlorocyclopentadiene NC,VELAPHexachloroethane NC,VELAPIndeno (1,2,3-cd) pyrene NC,VELAPIsophorone NC,VELAPm+p-Cresols NC,VELAPMethyl methanesulfonate NC,VELAPNaphthalene NC,VELAPNitrobenzene NC,VELAPn-Nitrosodimethylamine NC,VELAPn-Nitrosodi-n-butylamine NC,VELAPn-Nitrosodi-n-propylamine NC,VELAPn-Nitrosodiphenylamine NC,VELAPn-Nitrosopiperidine NC,VELAPo+m+p-Cresols NC,VELAPo-Cresol NC,VELAPp-(Dimethylamino) azobenzene NC,VELAPp-Chloro-m-cresol NC,VELAPPentachloronitrobenzene NCPentachlorophenol NC,VELAPPhenacetin NC,VELAPPhenanthrene NC,VELAPPhenol NC,VELAPPronamide NC,VELAPPyrene NC,VELAPPyridine NC,VELAP

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DS Surrogate concentration reflects a dilution factor.

L LCS recovery is outside of established acceptance limits

M Matrix spike recovery is outside established acceptance limits

P Duplicate analysis does not meet the acceptance criteria for precision

S Surrogate recovery was outside acceptance criteria


QualifersQual


Page 51 of 51

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Nashville2960 Foster Creighton DriveNashville, TN 37204Tel: (615)726-0177

TestAmerica Job ID: 490-28301-1TestAmerica Sample Delivery Group: 13F0120Client Project/Site: Air Water & Soil Laboratories (7091)

For:Air Water & Soil Laboratories Inc2109 A North Hamilton StreetRichmond, Virginia 23230

Attn: AWS PM

Authorized for release by:6/12/2013 4:48:57 PM

Roxanne Connor, Senior Project [email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Air Water & Soil Laboratories IncProject/Site: Air Water & Soil Laboratories (7091)

TestAmerica Job ID: 490-28301-1SDG: 13F0120

Page 2 of 16TestAmerica Nashville

6/12/2013

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

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Sample SummaryTestAmerica Job ID: 490-28301-1Client: Air Water & Soil Laboratories Inc

SDG: 13F0120Project/Site: Air Water & Soil Laboratories (7091)

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

490-28301-1 13F0120-03 Soil 06/04/13 09:30 06/07/13 08:55

490-28301-2 13F0120-05 Soil 06/04/13 13:00 06/07/13 08:55

490-28301-3 13F0120-06 Soil 06/04/13 14:00 06/07/13 08:55

TestAmerica Nashville

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Case NarrativeClient: Air Water & Soil Laboratories Inc TestAmerica Job ID: 490-28301-1Project/Site: Air Water & Soil Laboratories (7091) SDG: 13F0120

Job ID: 490-28301-1

Laboratory: TestAmerica Nashville

Narrative

Job Narrative

490-28301-1

Comments

No additional comments.

Receipt

The samples were received on 6/7/2013 8:55 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 3.4º C.

Organic Prep

No analytical or quality issues were noted.

TestAmerica NashvillePage 4 of 16 6/12/2013

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Definitions/GlossaryTestAmerica Job ID: 490-28301-1Client: Air Water & Soil Laboratories Inc


Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basisAbbreviation

%R Percent Recovery

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)


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Client Sample ResultsTestAmerica Job ID: 490-28301-1Client: Air Water & Soil Laboratories Inc


Lab Sample ID: 490-28301-1Client Sample ID: 13F0120-03

Matrix: SoilDate Collected: 06/04/13 09:30

Date Received: 06/07/13 08:55

General ChemistryRL MDL

HEM 1120 48.1 mg/Kg 06/11/13 12:22 06/11/13 15:21 1Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier


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QC Sample ResultsTestAmerica Job ID: 490-28301-1Client: Air Water & Soil Laboratories Inc


Method: 9071B - HEM and SGT-HEM

Client Sample ID: Method BlankLab Sample ID: MB 490-85410/1-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 85482 Prep Batch: 85410

RL MDL

HEM ND 50.0 mg/Kg 06/11/13 12:22 06/11/13 15:21 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-85410/2-A

Matrix: Solid Prep Type: Total/NA


HEM 4000 3990 mg/Kg 100 75 - 117Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: 13F0120-03Lab Sample ID: 490-28301-1 MS

Matrix: Soil Prep Type: Total/NA


HEM 1120 3950 4437 mg/Kg 84 66 - 117Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: 13F0120-03Lab Sample ID: 490-28301-1 DU

Matrix: Soil Prep Type: Total/NA


HEM 1120 803.7 mg/Kg 33 50Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD


Page 9 of 16 6/12/2013

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QC Association SummaryTestAmerica Job ID: 490-28301-1Client: Air Water & Soil Laboratories Inc


General Chemistry

Prep Batch: 85410

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Soil��

490-28301-1 13F0120-03 Total/NA

Soil��

13F0120-03 Total/NA

Soil��

490-28301-1 MS 13F0120-03 Total/NA

Soil��

490-28301-2 13F0120-05 Total/NA

Soil��

490-28301-3 13F0120-06 Total/NA � �� LCS 490-85410/2-A �� Total/NA � �� Total/NA

Analysis Batch: 85482

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Soil��

85410490-28301-1 13F0120-03 Total/NA

Soil��

85410��

13F0120-03 Total/NA

Soil��

85410490-28301-1 MS 13F0120-03 Total/NA

Soil��

85410490-28301-2 13F0120-05 Total/NA

Soil��

85410490-28301-3 13F0120-06 Total/NA � �� 85410LCS 490-85410/2-A �� Total/NA � �� 85410

�� Total/NA


Page 10 of 16 6/12/2013

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Lab ChronicleClient: Air Water & Soil Laboratories Inc TestAmerica Job ID: 490-28301-1Project/Site: Air Water & Soil Laboratories (7091) SDG: 13F0120

Client Sample ID: 13F0120-03 Lab Sample ID: 490-28301-1



Prep!"#$%

06/11/13 12:22 AK85410 TAL NSHType

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA &'()*+,+ !"#$%1 85482 06/11/13 15:21 AK TAL NSHTotal/NA



Date Received: 06/07/13 08:55-./0 !"#$%06/11/13 12:22 AK85410 TAL NSH

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor




Date Received: 06/07/13 08:55-./0 !"#$%06/11/13 12:22 AK85410 TAL NSH

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor


Laboratory References:1&2 345 6 1/+7&8/.,9( 3(+:;,))/< =!>" ?@+7/. A./,B:7@' C.,;/< 3(+:;,))/< 13 D#="E< 1F2 G>$HI#=>J"$##


Page 11 of 16 6/12/2013

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Method SummaryTestAmerica Job ID: 490-28301-1Client: Air Water & Soil Laboratories Inc


Method Method Description LaboratoryProtocol

SW846KLMNO PQR STU VWXYPQR TAL NSH

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177


Page 12 of 16 6/12/2013

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Certification SummaryClient: Air Water & Soil Laboratories Inc TestAmerica Job ID: 490-28301-1Project/Site: Air Water & Soil Laboratories (7091) SDG: 13F0120

Laboratory: TestAmerica NashvilleZ[[ \]^_à`\b_`cde f][g hi _fè [bhc^b_cî b^] [è_]gj kc_ b[[ \]^_à`\b_`cde b^] bll[`\bh[] _c _fè ^]lc^_jAuthority Program EPA Region Certification ID Expiration Date

393ACIL 10-30-13

A2LAmnopmqr stuvw

0453.07 12-31-13Z[bexb yzn{|State Program 10 UST-087 07-24-13Z^`}cdbState Program 9

Z~u�t� uw�uw�s� �Z^xbdebe �q�State Program 6 88-0737 04-25-14rb[àc^d`bNELAP 9 1168CA 10-31-13

Connecticut State Program 1 PH-0220 12-31-13

Florida NELAP 4 E87358 06-30-13

Illinois NELAP 5 200010 12-09-13mc�bState Program 7 131 05-01-14�bdebeNELAP 7 E-10229 10-31-13�]d_�\xi yzn{|State Program 4 19 09-15-13

Louisiana NELAP 6 30613 06-30-13

Maryland State Program 3 316 03-31-14

Massachusetts State Program 1 M-TN032 06-30-13

Minnesota NELAP 5 047-999-345 12-31-13

Mississippi State Program 4 N/A 06-30-13

Montana (UST) State Program 8 NA 01-01-15

Nevada State Program 9 TN00032 07-31-13k]� �b�lef`^]NELAP 1 2963 10-10-13k]� �]ê]iNELAP 2 TN965 06-30-13k]� �c^xNELAP 2 11342 04-01-14kc^_f rb^c[`db �qk�State Program 4 387 12-31-13kc^_f �bxc_bState Program 8

��s��06-30-13of`c �Z�

State Program 5 CL0033 01-19-14ox[bfc�bState Program 6 9412 08-31-13o^]�cdNELAP 10 TN200001 04-29-14

Pennsylvania NELAP 3 68-00585 06-30-13�fcg] me[bdgState Program 1

�Zouuv��12-30-13

South Carolina State Program 4 84009 (001) 02-28-14

South Carolina State Program 4 84009 (002) 02-23-14

Tennessee State Program 4 2008 02-23-14{]�beNELAP 6

{su�tu�utt�u��{�08-31-13

USDA Federal S-48469 11-02-13

Utah NELAP 8 TAN 06-30-13�`^�`d`bNELAP 3 460152 06-14-14

Washington State Program 10 C789 07-19-13�]e_ �`^�`d`b �q�State Program 3 219 02-28-14

Wisconsin State Program 5 998020430 08-31-13

Wyoming (UST) A2LA 8 453.07 12-31-13


� q�l`^]g \]^_à`\b_`cd è \�^^]d_[i l]dg`d� ^]d]�b[ bdg è \cde`g]^]g �b[`gjPage 13 of 16 6/12/2013

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of 16 6/12/2013

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!"#$%&'()*+,&-,.,$*/&01,.2+$3/

!"#$%&'()#*(+,&$*(-(./#"(0,1/*,&/*#$2(3%4 5/1(6781$*'(9:;<=>?;@<@

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!$3/&45)6,78&=

D*7$E,F#/,4&#G#&H(I,2%J&(4K$4L$F(/*(#2(MNO(1,4LP*/7%F(,2(8$,27*$F(1H(,(

27*G$H(8$&$*Q

6N)DK$(4//"$*J2(472&/FH(2$,"R(#S(T*$2$%&R(#2(#%&,4&Q

6N).,8T"$(472&/FH(2$,"2R(#S(T*$2$%&R(,*$(#%&,4&Q

D*7$DK$(4//"$*(/*(2,8T"$2(F/(%/&(,TT$,*(&/(K,G$(1$$%(4/8T*/8#2$F(/*(

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D*7$32(&K$(C#$"F(.,8T"$*J2(%,8$(T*$2$%&(/%(!U!V

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D*7$.,8T"$2(,*$(*$4$#G$F(I#&K#%(W/"F#%P(D#8$Q

D*7$.,8T"$(4/%&,#%$*2(K,G$("$P#1"$(",1$"2Q

D*7$!/%&,#%$*2(,*$(%/&(1*/L$%(/*("$,L#%PQ

D*7$.,8T"$(4/""$4&#/%(F,&$N&#8$2(,*$(T*/G#F$FQ

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E,3/?),7$.(&4(31F$++,Page 16 of 16 6/12/2013

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Client Name:


Sincerely,


Ashland, VA 23005


Purchase Order:


Date Issued:

Date Received:

Submitted To:

Client Site I.D.:

June 24, 2013 16:47


Joshua Shrader

End Notes:





Lewistown Road

Final Report




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



Lewis Ditch S 13F0281-01 06/17/2013 12:05Soil 06/06/2013 13:30

Ramp Ditch 2 13F0281-02 06/17/2013 12:05Soil 06/06/2013 09:30

Ramp Ditch 3 13F0281-03 06/17/2013 12:05Soil 06/06/2013 09:35

Analysis for Oil and Grease was subcontracted to Pace Analytical . The subcontracted results are attached at the end of this Certificate of Analysis.

Page 2 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0281-01Lewis Ditch S

06/06/2013 13:30

Analytical Results


Date/Time Sampled:







Date/Time

13F0281-01RE2Lewis Ditch S

06/06/2013 13:30

Analytical Results


Date/Time Sampled:



Page 3 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/06/2013 09:30

Analytical Results


Date/Time Sampled:


1,1,1,2-Tetrachloroethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

1,1,1-Trichloroethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250



1,1-Dichloroethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

1,1-Dichloroethylene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

1,1-Dichloropropene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

1,2,3-Trichlorobenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

1,2,3-Trichloropropane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250


1,2,4-Trimethylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

1,2-Dibromo-3-chloropropane (DBCP) SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

1,2-Dibromoethane (EDB) SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

1,2-Dichlorobenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250


1,2-Dichloropropane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250






2-Butanone (MEK) SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

2-Chlorotoluene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

2-Hexanone (MBK) SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250


4-Isopropyltoluene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

4-Methyl-2-pentanone (MIBK) SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Acetone SW8260B MKD<500 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 500

Benzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Page 4 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/06/2013 09:30

Analytical Results


Date/Time Sampled:


Bromobenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Bromochloromethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Bromodichloromethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Bromoform SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Bromomethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Carbon disulfide SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Carbon tetrachloride SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Chlorobenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Chloroethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Chloroform SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Chloromethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

cis-1,2-Dichloroethylene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

cis-1,3-Dichloropropene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Dibromochloromethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Dibromomethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Dichlorodifluoromethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Di-isopropyl ether (DIPE) SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Ethylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Hexachlorobutadiene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Iodomethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Isopropylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

m+p-Xylenes SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Methylene chloride SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Methyl-t-butyl ether (MTBE) SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Naphthalene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

n-Butylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

n-Propylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

o-Xylene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

sec-Butylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Page 5 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/06/2013 09:30

Analytical Results


Date/Time Sampled:


Styrene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

tert-Butylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Tetrachloroethylene (PCE) SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Toluene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

trans-1,2-Dichloroethylene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

trans-1,3-Dichloropropene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Trichloroethylene SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Trichlorofluoromethane SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Vinyl acetate SW8260B MKD<500 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 500

Vinyl chloride SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

Xylenes, Total SW8260B MKD<250 ug/kg 06/21/2013 00:15 06/21/2013 00:15H 250

80-12094.3 %Surrogate: 1,2-Dichloroethane-d4 H 06/21/2013 00:15 MKD06/21/2013 00:1585-12098.0 %Surrogate: 4-Bromofluorobenzene H 06/21/2013 00:15 MKD06/21/2013 00:1578-11991.3 %Surrogate: Dibromofluoromethane H 06/21/2013 00:15 MKD06/21/2013 00:1585-115102 %Surrogate: Toluene-d8 H 06/21/2013 00:15 MKD06/21/2013 00:15




Page 6 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/06/2013 09:35

Analytical Results


Date/Time Sampled:







1,1-Dichloroethylene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

1,1-Dichloropropene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250


1,2,3-Trichloropropane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250



1,2-Dibromo-3-chloropropane (DBCP) SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

1,2-Dibromoethane (EDB) SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250









2-Butanone (MEK) SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250


2-Hexanone (MBK) SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250


4-Isopropyltoluene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

4-Methyl-2-pentanone (MIBK) SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Acetone SW8260B MKD<500 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 500

Benzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Page 7 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/06/2013 09:35

Analytical Results


Date/Time Sampled:


Bromobenzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Bromochloromethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Bromodichloromethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Bromoform SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Bromomethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Carbon disulfide SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Carbon tetrachloride SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Chlorobenzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Chloroethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Chloroform SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Chloromethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

cis-1,2-Dichloroethylene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

cis-1,3-Dichloropropene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Dibromochloromethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Dibromomethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Dichlorodifluoromethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Di-isopropyl ether (DIPE) SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Ethylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Hexachlorobutadiene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Iodomethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Isopropylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

m+p-Xylenes SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Methylene chloride SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Methyl-t-butyl ether (MTBE) SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Naphthalene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

n-Butylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

n-Propylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

o-Xylene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

sec-Butylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Page 8 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/06/2013 09:35

Analytical Results


Date/Time Sampled:


Styrene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

tert-Butylbenzene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Tetrachloroethylene (PCE) SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Toluene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

trans-1,2-Dichloroethylene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

trans-1,3-Dichloropropene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Trichloroethylene SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Trichlorofluoromethane SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Vinyl acetate SW8260B MKD<500 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 500

Vinyl chloride SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

Xylenes, Total SW8260B MKD<250 ug/kg 06/21/2013 00:38 06/21/2013 00:38H 250

80-12093.3 %Surrogate: 1,2-Dichloroethane-d4 H 06/21/2013 00:38 MKD06/21/2013 00:3885-12094.2 %Surrogate: 4-Bromofluorobenzene H 06/21/2013 00:38 MKD06/21/2013 00:3878-11991.1 %Surrogate: Dibromofluoromethane H 06/21/2013 00:38 MKD06/21/2013 00:3885-11597.9 %Surrogate: Toluene-d8 H 06/21/2013 00:38 MKD06/21/2013 00:38



40-160 %Surrogate: Pentacosane S 06/17/2013 16:25 JHV06/19/2013 00:58

Page 9 of 28




Ashland VA, 23005




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Purchase Order:


Lewistown Road

Final Report



13F0281-01,13F0281-02,13F0281-03BWF0321 SW8015C

13F0281-01BWF0339 SW8015C

13F0281-01RE1BWF0354 SW8015C

13F0281-01RE2BWF0393 SW8015C

13F0281-02,13F0281-03BWF0430 SW8260B

13F0281-01,13F0281-02,13F0281-03SW9071B

Page 10 of 28




Ashland VA, 23005




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Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte









TPH-Volatiles (GRO) 0.10 0.978 2070-13098.8 25.7mg/kg0.97 mg/kg P


TPH-Volatiles (GRO) 0.10 0.949 70-13044.0mg/kg0.42 mg/kg M<0.10 mg/kg


TPH-Volatiles (GRO) 0.10 0.855 2070-13053.0 7.99mg/kg0.45 mg/kg M<0.10 mg/kg








Duplicate (BWF0354-DUP1) Prepared & Analyzed: 06/18/2013Source: 13F0270-03

TPH-Volatiles (GRO) 0.10 20NAmg/kg<0.10 mg/kg <0.10 mg/kg

Page 11 of 28




Ashland VA, 23005




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Purchase Order:


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Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte




Duplicate (BWF0354-DUP2) Prepared & Analyzed: 06/18/2013Source: 13F0281-01RE1

TPH-Volatiles (GRO) 0.10 20NAmg/kg<0.10 mg/kg <0.10 mg/kg










Matrix Spike (BWF0393-MS1) Prepared & Analyzed: 06/19/2013Source: 13F0281-01RE2

TPH-Volatiles (GRO) 0.10 1.00 70-130102mg/kg1.02 mg/kg <0.10 mg/kg

Matrix Spike Dup (BWF0393-MSD1) Prepared & Analyzed: 06/19/2013Source: 13F0281-01RE2


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Ashland VA, 23005




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Purchase Order:


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Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte










1,1-Dichloroethylene 5.00 ug/kg<5.00 ug/kg

1,1-Dichloropropene 5.00 ug/kg<5.00 ug/kg


1,2,3-Trichloropropane 5.00 ug/kg<5.00 ug/kg



1,2-Dibromo-3-chloropropane (DBCP) 5.00 ug/kg<5.00 ug/kg

1,2-Dibromoethane (EDB) 5.00 ug/kg<5.00 ug/kg









2-Butanone (MEK) 5.00 ug/kg<5.00 ug/kg


2-Hexanone (MBK) 5.00 ug/kg<5.00 ug/kg


4-Isopropyltoluene 5.00 ug/kg<5.00 ug/kg

4-Methyl-2-pentanone (MIBK) 5.00 ug/kg<5.00 ug/kg

Acetone 10.0 ug/kg<10.0 ug/kg

Benzene 5.00 ug/kg<5.00 ug/kg

Bromobenzene 5.00 ug/kg<5.00 ug/kg

Bromochloromethane 5.00 ug/kg<5.00 ug/kg

Bromodichloromethane 5.00 ug/kg<5.00 ug/kg

Bromoform 5.00 ug/kg<5.00 ug/kg

Page 13 of 28




Ashland VA, 23005




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Purchase Order:


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Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Bromomethane 5.00 ug/kg<5.00 ug/kg

Carbon disulfide 5.00 ug/kg<5.00 ug/kg

Carbon tetrachloride 5.00 ug/kg<5.00 ug/kg

Chlorobenzene 5.00 ug/kg<5.00 ug/kg

Chloroethane 5.00 ug/kg<5.00 ug/kg

Chloroform 5.00 ug/kg<5.00 ug/kg

Chloromethane 5.00 ug/kg<5.00 ug/kg

cis-1,2-Dichloroethylene 5.00 ug/kg<5.00 ug/kg

cis-1,3-Dichloropropene 5.00 ug/kg<5.00 ug/kg

Dibromochloromethane 5.00 ug/kg<5.00 ug/kg

Dibromomethane 5.00 ug/kg<5.00 ug/kg

Dichlorodifluoromethane 5.00 ug/kg<5.00 ug/kg

Di-isopropyl ether (DIPE) 5.00 ug/kg<5.00 ug/kg

Ethylbenzene 5.00 ug/kg<5.00 ug/kg


Iodomethane 5.00 ug/kg<5.00 ug/kg

Isopropylbenzene 5.00 ug/kg<5.00 ug/kg

m+p-Xylenes 5.00 ug/kg<5.00 ug/kg

Methylene chloride 5.00 ug/kg<5.00 ug/kg

Methyl-t-butyl ether (MTBE) 5.00 ug/kg<5.00 ug/kg


n-Butylbenzene 5.00 ug/kg<5.00 ug/kg

n-Propylbenzene 5.00 ug/kg<5.00 ug/kg

o-Xylene 5.00 ug/kg<5.00 ug/kg

sec-Butylbenzene 5.00 ug/kg<5.00 ug/kg

Styrene 5.00 ug/kg<5.00 ug/kg

tert-Butylbenzene 5.00 ug/kg<5.00 ug/kg

Tetrachloroethylene (PCE) 5.00 ug/kg<5.00 ug/kg

Toluene 5.00 ug/kg<5.00 ug/kg

trans-1,2-Dichloroethylene 5.00 ug/kg<5.00 ug/kg

trans-1,3-Dichloropropene 5.00 ug/kg<5.00 ug/kg

Trichloroethylene 5.00 ug/kg<5.00 ug/kg

Trichlorofluoromethane 5.00 ug/kg<5.00 ug/kg

Page 14 of 28




Ashland VA, 23005




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Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Vinyl acetate 10.0 ug/kg<10.0 ug/kg

Vinyl chloride 5.00 ug/kg<5.00 ug/kg

Xylenes, Total 5.00 ug/kg<5.00 ug/kg

50.0 80-120Surrogate: 1,2-Dichloroethane-d4 97.148.5 ug/L



50.0 85-115Surrogate: Toluene-d8 10150.4 ug/L






1,1-Dichloroethane 50.0 75-125110ug/L55.2 ug/L

1,1-Dichloroethylene 50.0 65-135128ug/L64.0 ug/L

1,1-Dichloropropene 50.0 70-135123ug/L61.7 ug/L


1,2,3-Trichloropropane 50.0 65-130100ug/L50.2 ug/L


1,2,4-Trimethylbenzene 50.0 65-135125ug/L62.4 ug/L

1,2-Dibromo-3-chloropropane (DBCP) 50.0 40-135107ug/L53.3 ug/L

1,2-Dibromoethane (EDB) 50.0 70-125114ug/L56.8 ug/L

1,2-Dichlorobenzene 50.0 75-120126ug/L63.2 ug/L L

1,2-Dichloroethane 50.0 70-135103ug/L51.7 ug/L

1,2-Dichloropropane 50.0 70-120121ug/L60.3 ug/L L

1,3,5-Trimethylbenzene 50.0 65-135121ug/L60.7 ug/L

1,3-Dichlorobenzene 50.0 70-125131ug/L65.5 ug/L L




2-Butanone (MEK) 50.0 30-160102ug/L51.1 ug/L

2-Chlorotoluene 50.0 70-130134ug/L66.9 ug/L L

2-Hexanone (MBK) 50.0 45-145113ug/L56.4 ug/L

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Purchase Order:


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Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





4-Chlorotoluene 50.0 75-125129ug/L64.5 ug/L L

4-Isopropyltoluene 50.0 75-135136ug/L68.1 ug/L L

4-Methyl-2-pentanone (MIBK) 50.0 45-145110ug/L55.1 ug/L

Acetone 50.0 20-16099.9ug/L50.0 ug/L

Benzene 50.0 75-125119ug/L59.4 ug/L

Bromobenzene 50.0 65-120116ug/L58.0 ug/L

Bromochloromethane 50.0 70-125111ug/L55.4 ug/L

Bromodichloromethane 50.0 70-130121ug/L60.3 ug/L

Bromoform 50.0 55-13599.8ug/L49.9 ug/L

Bromomethane 50.0 30-160109ug/L54.4 ug/L

Carbon disulfide 50.0 45-160123ug/L61.7 ug/L

Carbon tetrachloride 50.0 65-135118ug/L59.2 ug/L

Chlorobenzene 50.0 75-125126ug/L63.2 ug/L L

Chloroethane 50.0 40-155113ug/L56.4 ug/L

Chloroform 50.0 70-125109ug/L54.4 ug/L

Chloromethane 50.0 50-130128ug/L64.2 ug/L

cis-1,2-Dichloroethylene 50.0 65-125113ug/L56.6 ug/L

cis-1,3-Dichloropropene 50.0 70-125113ug/L56.6 ug/L

Dibromochloromethane 50.0 65-130103ug/L51.3 ug/L

Dibromomethane 50.0 75-130108ug/L54.1 ug/L

Dichlorodifluoromethane 50.0 35-135105ug/L52.6 ug/L

Ethylbenzene 50.0 75-125126ug/L62.8 ug/L L

Hexachlorobutadiene 50.0 55-140121ug/L60.5 ug/L

Isopropylbenzene 50.0 75-130132ug/L65.8 ug/L L

m+p-Xylenes 100 80-125127ug/L127 ug/L L

Methylene chloride 50.0 55-140114ug/L57.0 ug/L

Methyl-t-butyl ether (MTBE) 50.0 65-12597.1ug/L48.6 ug/L

Naphthalene 50.0 40-125110ug/L55.1 ug/L

n-Butylbenzene 50.0 65-140127ug/L63.6 ug/L

n-Propylbenzene 50.0 65-135139ug/L69.3 ug/L L

o-Xylene 50.0 75-125133ug/L66.7 ug/L L

sec-Butylbenzene 50.0 65-130137ug/L68.6 ug/L L

Styrene 50.0 75-125106ug/L53.2 ug/L

Page 16 of 28




Ashland VA, 23005




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Purchase Order:


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Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





tert-Butylbenzene 50.0 65-130139ug/L69.4 ug/L L

Tetrachloroethylene (PCE) 50.0 65-140113ug/L56.4 ug/L

Toluene 50.0 70-125123ug/L61.4 ug/L

trans-1,2-Dichloroethylene 50.0 65-135116ug/L57.8 ug/L

trans-1,3-Dichloropropene 50.0 65-125111ug/L55.5 ug/L

Trichloroethylene 50.0 75-125123ug/L61.6 ug/L

Trichlorofluoromethane 50.0 25-18594.7ug/L47.3 ug/L

Vinyl chloride 50.0 60-125102ug/L51.1 ug/L







1,1,1-Trichloroethane 50.0 3070-135128 6.61ug/L64.2 ug/L


1,1,2-Trichloroethane 50.0 3060-125126 11.5ug/L62.9 ug/L L

1,1-Dichloroethane 50.0 3075-125114 3.12ug/L57.0 ug/L

1,1-Dichloroethylene 50.0 3065-135131 2.16ug/L65.4 ug/L

1,1-Dichloropropene 50.0 3070-135128 3.73ug/L64.0 ug/L


1,2,3-Trichloropropane 50.0 3065-130112 10.9ug/L56.0 ug/L


1,2,4-Trimethylbenzene 50.0 3065-135132 5.24ug/L65.8 ug/L

1,2-Dibromo-3-chloropropane (DBCP) 50.0 3040-135122 13.1ug/L60.8 ug/L

1,2-Dibromoethane (EDB) 50.0 3070-125121 6.54ug/L60.7 ug/L

1,2-Dichlorobenzene 50.0 3075-120135 6.68ug/L67.6 ug/L L

1,2-Dichloroethane 50.0 3070-135108 4.49ug/L54.1 ug/L

1,2-Dichloropropane 50.0 3070-120124 2.48ug/L61.8 ug/L L

1,3,5-Trimethylbenzene 50.0 3065-135129 6.03ug/L64.4 ug/L

1,3-Dichlorobenzene 50.0 3070-125136 3.90ug/L68.1 ug/L L


Page 17 of 28




Ashland VA, 23005




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Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte







2-Butanone (MEK) 50.0 3030-160122 17.6ug/L60.9 ug/L

2-Chlorotoluene 50.0 3070-130141 5.12ug/L70.4 ug/L L

2-Hexanone (MBK) 50.0 3045-145128 12.9ug/L64.2 ug/L

4-Chlorotoluene 50.0 3075-125137 6.26ug/L68.6 ug/L L

4-Isopropyltoluene 50.0 3075-135141 3.26ug/L70.3 ug/L L

4-Methyl-2-pentanone (MIBK) 50.0 3045-145128 14.7ug/L63.9 ug/L

Acetone 50.0 3020-160111 10.8ug/L55.7 ug/L

Benzene 50.0 3075-125124 4.23ug/L61.9 ug/L

Bromobenzene 50.0 3065-120123 5.72ug/L61.4 ug/L L

Bromochloromethane 50.0 3070-125122 9.34ug/L60.8 ug/L

Bromodichloromethane 50.0 3070-130130 7.66ug/L65.1 ug/L L

Bromoform 50.0 3055-135112 11.4ug/L55.9 ug/L

Bromomethane 50.0 3030-160120 9.98ug/L60.1 ug/L

Carbon disulfide 50.0 3045-160126 1.89ug/L62.8 ug/L

Carbon tetrachloride 50.0 3065-135124 4.89ug/L62.1 ug/L

Chlorobenzene 50.0 3075-125132 4.58ug/L66.2 ug/L L

Chloroethane 50.0 3040-155119 4.99ug/L59.3 ug/L

Chloroform 50.0 3070-125113 4.28ug/L56.7 ug/L

Chloromethane 50.0 3050-130132 2.62ug/L65.9 ug/L L

cis-1,2-Dichloroethylene 50.0 3065-125117 3.66ug/L58.7 ug/L

cis-1,3-Dichloropropene 50.0 3070-125120 5.60ug/L59.9 ug/L

Dibromochloromethane 50.0 3065-130111 8.22ug/L55.7 ug/L

Dibromomethane 50.0 3075-130120 10.2ug/L59.9 ug/L

Dichlorodifluoromethane 50.0 3035-135111 5.51ug/L55.6 ug/L

Ethylbenzene 50.0 3075-125131 4.32ug/L65.5 ug/L L

Hexachlorobutadiene 50.0 3055-140129 6.65ug/L64.7 ug/L

Isopropylbenzene 50.0 3075-130138 4.87ug/L69.1 ug/L L

m+p-Xylenes 100 3080-125133 4.88ug/L133 ug/L L

Methylene chloride 50.0 3055-140118 3.14ug/L58.8 ug/L

Methyl-t-butyl ether (MTBE) 50.0 3065-125106 8.75ug/L53.0 ug/L

Naphthalene 50.0 3040-125126 13.8ug/L63.2 ug/L L

Page 18 of 28




Ashland VA, 23005




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Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





n-Butylbenzene 50.0 3065-140132 3.81ug/L66.0 ug/L

n-Propylbenzene 50.0 3065-135146 4.92ug/L72.8 ug/L L

o-Xylene 50.0 3075-125141 5.38ug/L70.4 ug/L L

sec-Butylbenzene 50.0 3065-130144 4.55ug/L71.8 ug/L L

Styrene 50.0 3075-125114 7.00ug/L57.1 ug/L

tert-Butylbenzene 50.0 3065-130144 3.65ug/L72.0 ug/L L

Tetrachloroethylene (PCE) 50.0 3065-140117 3.44ug/L58.3 ug/L

Toluene 50.0 3070-125127 3.15ug/L63.4 ug/L L

trans-1,2-Dichloroethylene 50.0 3065-135121 4.89ug/L60.7 ug/L

trans-1,3-Dichloropropene 50.0 3065-125119 7.07ug/L59.5 ug/L

Trichloroethylene 50.0 3075-125129 4.62ug/L64.5 ug/L L

Trichlorofluoromethane 50.0 3025-18599.3 4.81ug/L49.7 ug/L

Vinyl chloride 50.0 3060-125105 2.99ug/L52.6 ug/L






1,1,1,2-Tetrachloroethane 50.0 75-125115ug/L57.5 ug/L < ug/L

1,1,1-Trichloroethane 50.0 70-135115ug/L57.3 ug/L < ug/L



1,1-Dichloroethane 50.0 75-125110ug/L55.1 ug/L < ug/L

1,1-Dichloroethylene 50.0 65-135119ug/L59.5 ug/L < ug/L

1,1-Dichloropropene 50.0 70-135117ug/L58.6 ug/L < ug/L

1,2,3-Trichlorobenzene 50.0 60-135109ug/L59.8 ug/L 5.19 ug/L

1,2,3-Trichloropropane 50.0 65-13097.8ug/L48.9 ug/L < ug/L


1,2,4-Trimethylbenzene 50.0 65-135110ug/L59.5 ug/L 4.46 ug/L

1,2-Dibromo-3-chloropropane (DBCP) 50.0 40-135104ug/L51.9 ug/L < ug/L

1,2-Dibromoethane (EDB) 50.0 70-125111ug/L55.4 ug/L < ug/L

1,2-Dichlorobenzene 50.0 75-120117ug/L61.4 ug/L 2.81 ug/L

Page 19 of 28




Ashland VA, 23005




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Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





1,2-Dichloroethane 50.0 70-13594.8ug/L52.2 ug/L 4.75 ug/L

1,2-Dichloropropane 50.0 70-120115ug/L57.5 ug/L < ug/L






2-Butanone (MEK) 50.0 30-16095.6ug/L47.8 ug/L < ug/L

2-Chlorotoluene 50.0 70-130128ug/L63.9 ug/L < ug/L

2-Hexanone (MBK) 50.0 45-145105ug/L52.7 ug/L < ug/L

4-Chlorotoluene 50.0 75-125124ug/L62.1 ug/L < ug/L

4-Isopropyltoluene 50.0 75-135120ug/L64.2 ug/L 4.27 ug/L

4-Methyl-2-pentanone (MIBK) 50.0 45-145104ug/L52.1 ug/L < ug/L

Acetone 50.0 20-16039.9ug/L59.8 ug/L 39.9 ug/L

Benzene 50.0 75-125112ug/L57.6 ug/L 1.41 ug/L

Bromobenzene 50.0 65-120116ug/L58.0 ug/L < ug/L

Bromochloromethane 50.0 70-125108ug/L54.1 ug/L < ug/L

Bromodichloromethane 50.0 70-130116ug/L57.8 ug/L < ug/L

Bromoform 50.0 55-13597.9ug/L48.9 ug/L < ug/L

Bromomethane 50.0 30-16056.3ug/L28.1 ug/L < ug/L

Carbon disulfide 50.0 45-160114ug/L57.8 ug/L 1.07 ug/L

Carbon tetrachloride 50.0 65-135112ug/L56.2 ug/L < ug/L

Chlorobenzene 50.0 75-125125ug/L62.5 ug/L < ug/L

Chloroethane 50.0 40-155103ug/L51.3 ug/L < ug/L

Chloroform 50.0 70-125107ug/L53.6 ug/L < ug/L

Chloromethane 50.0 50-130118ug/L63.5 ug/L 4.61 ug/L

cis-1,2-Dichloroethylene 50.0 65-125113ug/L56.6 ug/L < ug/L

cis-1,3-Dichloropropene 50.0 70-125108ug/L54.2 ug/L < ug/L

Dibromochloromethane 50.0 65-13095.3ug/L47.7 ug/L < ug/L

Dibromomethane 50.0 75-130104ug/L52.2 ug/L < ug/L

Dichlorodifluoromethane 50.0 35-13598.7ug/L49.4 ug/L < ug/L

Ethylbenzene 50.0 75-125117ug/L60.8 ug/L 2.18 ug/L

Hexachlorobutadiene 50.0 55-140116ug/L57.9 ug/L < ug/L

Page 20 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Isopropylbenzene 50.0 75-130125ug/L64.6 ug/L 2.09 ug/L

m+p-Xylenes 100 80-125123ug/L123 ug/L < ug/L

Methylene chloride 50.0 55-140-70.7ug/L56.1 ug/L M91.5 ug/L

Methyl-t-butyl ether (MTBE) 50.0 65-125103ug/L51.3 ug/L < ug/L

Naphthalene 50.0 40-12580.0ug/L56.0 ug/L 16.1 ug/L

n-Butylbenzene 50.0 65-140115ug/L59.5 ug/L 1.79 ug/L

n-Propylbenzene 50.0 65-135129ug/L66.0 ug/L 1.50 ug/L

o-Xylene 50.0 75-125132ug/L66.1 ug/L M< ug/L

sec-Butylbenzene 50.0 65-130125ug/L64.1 ug/L 1.75 ug/L

Styrene 50.0 75-125106ug/L52.9 ug/L < ug/L

tert-Butylbenzene 50.0 65-130129ug/L65.7 ug/L 0.97 ug/L

Tetrachloroethylene (PCE) 50.0 65-140108ug/L53.8 ug/L < ug/L

Toluene 50.0 70-12599.1ug/L57.9 ug/L 8.39 ug/L

trans-1,2-Dichloroethylene 50.0 65-135112ug/L55.9 ug/L < ug/L

trans-1,3-Dichloropropene 50.0 65-125105ug/L52.5 ug/L < ug/L

Trichloroethylene 50.0 75-125121ug/L60.4 ug/L < ug/L

Trichlorofluoromethane 50.0 25-18580.9ug/L44.2 ug/L 3.73 ug/L

Vinyl chloride 50.0 60-12593.6ug/L46.8 ug/L < ug/L










1,1-Dichloroethane 50.0 3075-125122ug/L61.1 ug/L < ug/L

1,1-Dichloroethylene 50.0 3065-135129ug/L64.3 ug/L < ug/L

1,1-Dichloropropene 50.0 3070-135127ug/L63.6 ug/L < ug/L


1,2,3-Trichloropropane 50.0 3065-130115ug/L57.7 ug/L < ug/L

Page 21 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte







1,2-Dibromo-3-chloropropane (DBCP) 50.0 3040-135121ug/L60.7 ug/L < ug/L

1,2-Dibromoethane (EDB) 50.0 3070-125123ug/L61.5 ug/L < ug/L

1,2-Dichlorobenzene 50.0 3075-120131ug/L68.1 ug/L M2.81 ug/L

1,2-Dichloroethane 50.0 3070-135108ug/L58.6 ug/L 4.75 ug/L

1,2-Dichloropropane 50.0 3070-120126ug/L62.9 ug/L M< ug/L


1,3-Dichlorobenzene 50.0 3070-125131ug/L67.3 ug/L M1.79 ug/L




2-Butanone (MEK) 50.0 3030-160144ug/L72.0 ug/L < ug/L

2-Chlorotoluene 50.0 3070-130136ug/L67.9 ug/L M< ug/L

2-Hexanone (MBK) 50.0 3045-145126ug/L62.9 ug/L < ug/L

4-Chlorotoluene 50.0 3075-125133ug/L66.5 ug/L M< ug/L

4-Isopropyltoluene 50.0 3075-135129ug/L68.5 ug/L 4.27 ug/L

4-Methyl-2-pentanone (MIBK) 50.0 3045-145126ug/L63.0 ug/L < ug/L

Acetone 50.0 3020-16042.6ug/L61.2 ug/L 39.9 ug/L

Benzene 50.0 3075-125122ug/L62.5 ug/L 1.41 ug/L

Bromobenzene 50.0 3065-120123ug/L61.5 ug/L M< ug/L

Bromochloromethane 50.0 3070-125125ug/L62.5 ug/L < ug/L

Bromodichloromethane 50.0 3070-130126ug/L62.9 ug/L < ug/L

Bromoform 50.0 3055-135109ug/L54.6 ug/L < ug/L

Bromomethane 50.0 3030-16058.2ug/L29.1 ug/L < ug/L

Carbon disulfide 50.0 3045-160116ug/L59.1 ug/L 1.07 ug/L

Carbon tetrachloride 50.0 3065-135121ug/L60.7 ug/L < ug/L

Chlorobenzene 50.0 3075-125132ug/L66.0 ug/L M< ug/L

Chloroethane 50.0 3040-155108ug/L54.1 ug/L < ug/L

Chloroform 50.0 3070-125117ug/L58.7 ug/L < ug/L

Chloromethane 50.0 3050-130133ug/L70.9 ug/L M4.61 ug/L

cis-1,2-Dichloroethylene 50.0 3065-125123ug/L61.7 ug/L < ug/L

cis-1,3-Dichloropropene 50.0 3070-125119ug/L59.7 ug/L < ug/L

Page 22 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Dibromochloromethane 50.0 3065-130108ug/L54.1 ug/L < ug/L

Dibromomethane 50.0 3075-130119ug/L59.3 ug/L < ug/L

Dichlorodifluoromethane 50.0 3035-135106ug/L53.2 ug/L < ug/L

Ethylbenzene 50.0 3075-125126ug/L65.0 ug/L M2.18 ug/L

Hexachlorobutadiene 50.0 3055-140127ug/L63.4 ug/L < ug/L

Isopropylbenzene 50.0 3075-130133ug/L68.5 ug/L M2.09 ug/L

m+p-Xylenes 100 3080-125131ug/L131 ug/L M< ug/L

Methylene chloride 50.0 3055-140-58.4ug/L62.2 ug/L M91.5 ug/L

Methyl-t-butyl ether (MTBE) 50.0 3065-125119ug/L59.5 ug/L < ug/L

Naphthalene 50.0 3040-12597.5ug/L64.8 ug/L 16.1 ug/L

n-Butylbenzene 50.0 3065-140125ug/L64.5 ug/L 1.79 ug/L

n-Propylbenzene 50.0 3065-135139ug/L70.8 ug/L M1.50 ug/L

o-Xylene 50.0 3075-125140ug/L70.2 ug/L M< ug/L

sec-Butylbenzene 50.0 3065-130135ug/L69.3 ug/L M1.75 ug/L

Styrene 50.0 3075-125115ug/L57.5 ug/L < ug/L

tert-Butylbenzene 50.0 3065-130140ug/L70.8 ug/L M0.97 ug/L

Tetrachloroethylene (PCE) 50.0 3065-140116ug/L58.0 ug/L < ug/L

Toluene 50.0 3070-125106ug/L61.2 ug/L 8.39 ug/L

trans-1,2-Dichloroethylene 50.0 3065-135127ug/L63.6 ug/L < ug/L

trans-1,3-Dichloropropene 50.0 3065-125115ug/L57.5 ug/L < ug/L

Trichloroethylene 50.0 3075-125128ug/L63.8 ug/L M< ug/L

Trichlorofluoromethane 50.0 3025-18589.0ug/L48.2 ug/L 3.73 ug/L

Vinyl chloride 50.0 3060-12599.7ug/L49.9 ug/L < ug/L





Page 23 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte








TPH-Semi-Volatiles (DRO) 10.0 99.6 40-16088.9mg/kg88.5 mg/kg



TPH-Semi-Volatiles (DRO) 10.0 98.4 2040-16091.0 1.16mg/kg89.5 mg/kg



TPH-Semi-Volatiles (DRO) 10.0 99.2 40-16018.3mg/kg146 mg/kg M128 mg/kg

4.96 40-160Surrogate: Pentacosane 16.80.833 mg/kg S


TPH-Semi-Volatiles (DRO) 10.0 99.2 2040-16028.5 6.73mg/kg156 mg/kg M128 mg/kg

4.96 40-160Surrogate: Pentacosane 29.21.45 mg/kg S

Page 24 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



SW8015C in Solids


SW8260B in Solids

1,1,1,2-Tetrachloroethane NC,VELAP1,1,1-Trichloroethane NC,VELAP1,1,2,2-Tetrachloroethane NC,VELAP1,1,2-Trichloroethane NC,VELAP1,1-Dichloroethane NC,VELAP1,1-Dichloroethylene NC,VELAP1,1-Dichloropropene NC,VELAP1,2,3-Trichlorobenzene NC,VELAP1,2,3-Trichloropropane NC,VELAP1,2,4-Trichlorobenzene NC,VELAP1,2,4-Trimethylbenzene NC,VELAP1,2-Dibromo-3-chloropropane (DBCP) NC,VELAP1,2-Dibromoethane (EDB) NC,VELAP1,2-Dichlorobenzene NC,VELAP1,2-Dichloroethane NC,VELAP1,2-Dichloropropane NC,VELAP1,3,5-Trimethylbenzene NC,VELAP1,3-Dichlorobenzene NC,VELAP1,3-Dichloropropane NC,VELAP1,4-Dichlorobenzene NC,VELAP2,2-Dichloropropane NC,VELAP2-Butanone (MEK) NC,VELAP2-Chlorotoluene NC,VELAP2-Hexanone (MBK) NC,VELAP4-Chlorotoluene NC,VELAP

Page 25 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



4-Isopropyltoluene NC,VELAP4-Methyl-2-pentanone (MIBK) NC,VELAPAcetone NC,VELAPBenzene NC,VELAPBromobenzene NC,VELAPBromochloromethane NC,VELAPBromodichloromethane NC,VELAPBromoform NC,VELAPBromomethane NC,VELAPCarbon disulfide NC,VELAPCarbon tetrachloride NC,VELAPChlorobenzene NC,VELAPChloroethane NC,VELAPChloroform NC,VELAPChloromethane NC,VELAPcis-1,2-Dichloroethylene NC,VELAPcis-1,3-Dichloropropene NC,VELAPDibromochloromethane NC,VELAPDibromomethane NC,VELAPDichlorodifluoromethane NC,VELAPDi-isopropyl ether (DIPE) NC,VELAPEthylbenzene NC,VELAPHexachlorobutadiene NC,VELAPIodomethane NC,VELAPIsopropylbenzene NC,VELAPm+p-Xylenes NC,VELAPMethylene chloride NC,VELAPMethyl-t-butyl ether (MTBE) NC,VELAPNaphthalene NC,VELAP

Page 26 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



n-Butylbenzene NC,VELAPn-Propylbenzene NC,VELAPo-Xylene NC,VELAPsec-Butylbenzene NC,VELAPStyrene NC,VELAPtert-Butylbenzene NC,VELAPTetrachloroethylene (PCE) NC,VELAPToluene NC,VELAPtrans-1,2-Dichloroethylene NC,VELAPtrans-1,3-Dichloropropene NC,VELAPTrichloroethylene NC,VELAPTrichlorofluoromethane NC,VELAPVinyl acetate NC,VELAPVinyl chloride NC,VELAPXylenes, Total NC,VELAPDibromofluoromethane VELAP


Page 27 of 28




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report


H Analysis was performed outside of the method prescribed holding time.

L LCS recovery is outside of established acceptance limits


P Duplicate analysis does not meet the acceptance criteria for precision

S Surrogate recovery was outside acceptance criteria


QualifersQual


Page 28 of 28

#=CL#

June 24, 2013

LIMS USE: FR - JESSICA REICH

LIMS OBJECT ID: 92161812

92161812Project:Pace Project No.:

RE:

Ms. Jessica ReichAir Water Soil Lab2109A North Hamilton StreetRichmond, VA 23230

13F0281

Dear Ms. Reich:Enclosed are the analytical results for sample(s) received by the laboratory on June 18, 2013. Theresults relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unlessotherwise noted in the body of the report.

Analyses were performed at the Pace Analytical Services location indicated on the sample analytepage for analysis unless otherwise footnoted.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Kevin Godwin

[email protected] Manager

Enclosures

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc.

9800 Kincey Ave. Suite 100

Huntersville, NC 28078

(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176


205 East Meadow Road - Suite A

Eden, NC 27288

(336)623-8921

Page 1 of 11

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

92161812

13F0281

Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001

Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84West Virginia Certification #: 357Virginia/VELAP Certification #: 460221







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 2 of 11

#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

92161812

13F0281

Lab ID Sample ID Matrix Date Collected Date Received

92161812001 13F0281-01 Solid 06/06/13 13:30 06/18/13 10:00

92161812002 13F0281-02 Solid 06/06/13 09:30 06/18/13 10:00

92161812003 13F0281-03 Solid 06/06/13 09:35 06/18/13 10:00







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 3 of 11

#=SA#

SAMPLE ANALYTE COUNT

Pace Project No.:

Project:

92161812

13F0281

Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

92161812001 13F0281-01 9071B 1 PASI-CCLW

ASTM D2974-87 1 PASI-CJEA

92161812002 13F0281-02 9071B 1 PASI-CCLW


92161812003 13F0281-03 9071B 1 PASI-CCLW








(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 4 of 11

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

92161812

13F0281

Sample: 13F0281-01 Lab ID: 92161812001 Collected: 06/06/13 13:30 Received: 06/18/13 10:00 Matrix: Solid

Results reported on a "dry-weight" basis

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimitReport

9071 Oil and Grease Analytical Method: 9071B Preparation Method: 9071B

Oil and Grease ND mg/kg 06/19/13 15:4606/19/13 15:1391.0 91.0 1

Percent Moisture Analytical Method: ASTM D2974-87

Percent Moisture 23.1 % 06/24/13 14:340.10 0.10 1





Oil and Grease ND mg/kg 06/19/13 15:4606/19/13 15:13129 129 1







Oil and Grease 166 mg/kg 06/19/13 15:4606/19/13 15:1385.1 85.1 1





without the written consent of Pace Analytical Services, Inc..Date: 06/24/2013 04:38 PM




(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 5 of 11

#=QC#

QUALITY CONTROL DATA

Pace Project No.:

Project:

92161812

13F0281

QC Batch:

QC Batch Method:

Analysis Method:

Analysis Description:

GCSV/14895

9071B

9071B

9071 Oil and Grease

Associated Lab Samples: 92161812001, 92161812002, 92161812003

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 995428


Matrix: Solid

Analyzed

Oil and Grease mg/kg ND 70.0 06/19/13 15:46

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

995429LABORATORY CONTROL SAMPLE:

LCSSpike

Oil and Grease mg/kg 11101330 83 78-114

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

995430MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

92161965006

995431

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Oil and Grease mg/kg 1330 83 78-11487 5 201330ND 1150 1210







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 6 of 11

#=QC#


Pace Project No.:

Project:

92161812

13F0281

QC Batch:

QC Batch Method:

Analysis Method:


PMST/5619

ASTM D2974-87

ASTM D2974-87

Dry Weight/Percent Moisture


Parameter UnitsDup

ResultMaxRPD QualifiersRPDResult

92161812001

996008SAMPLE DUPLICATE:

Percent Moisture % 22.1 4 2523.1

Parameter UnitsDup


92161965003









(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 7 of 11

#=QL#

QUALIFIERS

Pace Project No.:

Project:

92161812

13F0281

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL - Adjusted Method Detection Limit.

PRL - Pace Reporting Limit.

RL - Reporting Limit.

S - Surrogate

1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - CharlottePASI-C







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 8 of 11

#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Pace Project No.:

Project:

92161812

13F0281

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

92161812001 GCSV/14895 GCSV/1489813F0281-01 9071B 9071B92161812002 GCSV/14895 GCSV/1489813F0281-02 9071B 9071B92161812003 GCSV/14895 GCSV/1489813F0281-03 9071B 9071B

92161812001 PMST/561913F0281-01 ASTM D2974-8792161812002 PMST/561913F0281-02 ASTM D2974-8792161812003 PMST/561913F0281-03 ASTM D2974-87







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 9 of 11




Client Name:


Sincerely,


Ashland, VA 23005


Purchase Order:


Date Issued:

Date Received:

Submitted To:

Client Site I.D.:

June 25, 2013 16:04


Joshua Shrader

End Notes:





Lewistown Road

Final Report




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



019-03 0'-1' 13F0366-01 06/21/2013 08:34Soil 06/20/2013 16:00

Analysis for Oil and Grease was subcontracted to Pace Analytical . The subcontracted results are attached at the end of this Certificate of Analysis.

Page 2 of 6




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0366-01019-03 0'-1'

06/20/2013 16:00

Analytical Results


Date/Time Sampled:


Zinc SW6010C 103 mg/kg 06/21/2013 10:35 06/24/2013 14:33 JPV0.500



13F0366-01BWF0420 SW6010C

13F0366-01SW9071B

Page 3 of 6




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Zinc 0.500 mg/kg<0.500 mg/kg


Zinc 0.500 24.9 80-12098.5mg/kg24.5 mg/kg


Zinc 0.500 24.9 2080-12098.0 0.512mg/kg24.4 mg/kg


Zinc 0.500 23.9 75-12564.9mg/kg43.7 mg/kg M28.1 mg/kg


Zinc 0.500 24.2 2075-12558.0 3.51mg/kg42.2 mg/kg M28.1 mg/kg

Page 4 of 6




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



SW6010C in Solids

Zinc VELAP,NC


Page 5 of 6




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




QualifersQual


Page 6 of 6

#=CL#

June 25, 2013

LIMS USE: FR - JESSICA REICH

LIMS OBJECT ID: 92162502

92162502Project:Pace Project No.:

RE:

Ms. Jessica ReichAir Water Soil Lab2109A North Hamilton StreetRichmond, VA 23230

13F0366

Dear Ms. Reich:Enclosed are the analytical results for sample(s) received by the laboratory on June 22, 2013. Theresults relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unlessotherwise noted in the body of the report.

Analyses were performed at the Pace Analytical Services location indicated on the sample analytepage for analysis unless otherwise footnoted.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Kevin Godwin

[email protected] Manager

Enclosures







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 1 of 11

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

92162502

13F0366

Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001

Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84West Virginia Certification #: 357Virginia/VELAP Certification #: 460221







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 2 of 11

#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

92162502

13F0366

Lab ID Sample ID Matrix Date Collected Date Received

92162502001 13F0366-01 Solid 06/20/13 16:00 06/22/13 09:50







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 3 of 11

#=SA#

SAMPLE ANALYTE COUNT

Pace Project No.:

Project:

92162502

13F0366

Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

92162502001 13F0366-01 9071B 1 PASI-CCLW








(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 4 of 11

#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

92162502

13F0366





Oil and Grease ND mg/kg 06/24/13 14:5906/24/13 14:43108 108 1









(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 5 of 11

#=QC#


Pace Project No.:

Project:

92162502

13F0366

QC Batch:

QC Batch Method:

Analysis Method:


GCSV/14928

9071B

9071B

9071 Oil and Grease

Associated Lab Samples: 92162502001

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 998134


Matrix: Solid

Analyzed

Oil and Grease mg/kg ND 70.0 06/24/13 14:59

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

998135LABORATORY CONTROL SAMPLE & LCSD:

LCSSpike LCSD% Rec RPD

MaxRPD

LCSDResult

998136

Oil and Grease mg/kg 12501330 94 78-114951270 2 20







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 6 of 11

#=QC#


Pace Project No.:

Project:

92162502

13F0366

QC Batch:

QC Batch Method:

Analysis Method:


PMST/5625

ASTM D2974-87

ASTM D2974-87

Dry Weight/Percent Moisture


Parameter UnitsDup


92162321002



Parameter UnitsDup


92162345014









(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 7 of 11

#=QL#

QUALIFIERS

Pace Project No.:

Project:

92162502

13F0366

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL - Adjusted Method Detection Limit.

PRL - Pace Reporting Limit.

RL - Reporting Limit.

S - Surrogate

1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - CharlottePASI-C







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 8 of 11

#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Pace Project No.:

Project:

92162502

13F0366

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

92162502001 GCSV/14928 GCSV/1493213F0366-01 9071B 9071B

92162502001 PMST/562513F0366-01 ASTM D2974-87







(704)875-9092


2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176



Eden, NC 27288

(336)623-8921

Page 9 of 11




Client Name:


Sincerely,


Ashland, VA 23005


Purchase Order:


Date Issued:

Date Received:

Submitted To:

Client Site I.D.:

June 21, 2013 16:18


Joshua Shrader

End Notes:





VDOT Lewistown Road

Final Report




Ashland VA, 23005




Client Name:

Purchase Order:


VDOT Lewistown Road

Final Report



NP 0'-1' 13F0307-01 06/18/2013 15:50Soil 06/04/2013 08:35

NP 1'-2' 13F0307-02 06/18/2013 15:50Soil 06/04/2013 08:40

S 1'-2' 13F0307-03 06/18/2013 15:50Soil 06/04/2013 09:15

Page 2 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


VDOT Lewistown Road

Final Report




Date/Time

13F0307-01NP 0'-1'

06/04/2013 08:35

Analytical Results


Date/Time Sampled:

TCLP Metals by 6000/7000 Series Methods

Lead SW6010C 0.303 mg/L 06/20/2013 09:39 06/20/2013 15:23 JPV0.100

Extraction Fluid SW1311 1 # 06/18/2013 16:45 06/20/2013 09:38 KEW




Date/Time

13F0307-02NP 1'-2'

06/04/2013 08:40

Analytical Results


Date/Time Sampled:


Lead SW6010C 40.7 mg/kg 06/20/2013 11:00 06/21/2013 12:49 JPV0.500




Date/Time

13F0307-03S 1'-2'

06/04/2013 09:15

Analytical Results


Date/Time Sampled:


Lead SW6010C 7.91 mg/kg 06/20/2013 11:00 06/21/2013 12:53 JPV0.500

Page 3 of 8




Ashland VA, 23005




Client Name:

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Final Report



13F0307-01BWF0379 SW1311

13F0307-01BWF0380 SW6010C

13F0307-02,13F0307-03BWF0409 SW6010C

Page 4 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


VDOT Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte





Lead 0.500 mg/kg<0.500 mg/kg


Lead 0.500 24.7 80-120101mg/kg24.9 mg/kg


Lead 0.500 22.8 2080-120103 5.77mg/kg23.5 mg/kg


Lead 0.500 24.6 75-125105mg/kg33.8 mg/kg 7.91 mg/kg


Lead 0.500 24.5 2075-125109 2.30mg/kg34.6 mg/kg 7.91 mg/kg

Page 5 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


VDOT Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

TCLP Metals by 6000/7000 Series Methods - Quality Control


Batch BWF0379 - SW1311


Extraction Fluid #1 #

Batch BWF0380 - SW3010A


Lead 0.100 mg/L<0.100 mg/L


Lead 0.100 2.50 80-120101mg/L2.53 mg/L


Lead 0.100 2.50 2080-120102 1.17mg/L2.56 mg/L


Lead 0.100 2.50 75-125103mg/L2.87 mg/L 0.303 mg/L


Lead 0.100 2.50 2075-125105 1.83mg/L2.92 mg/L 0.303 mg/L

Page 6 of 8




Ashland VA, 23005




Client Name:

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Final Report



SW1311 in Solids

Extraction Fluid VELAP

SW6010C in Non-Potable Water

Lead VELAP,NC

SW6010C in Solids

Lead VELAP,NC,WVDEP


Page 7 of 8




Ashland VA, 23005




Client Name:

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VDOT Lewistown Road

Final Report



QualifersQual


Page 8 of 8




Client Name:


Sincerely,


Ashland, VA 23005


Purchase Order:


Date Issued:

Date Received:

Submitted To:

Client Site I.D.:

July 2, 2013 11:28


Joshua Shrader

End Notes:


Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen, temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler included in the Certificate of Analysis are done so at the client�s request and are not included in the laboratory�s fields of certification nor have they been audited for adherence to a reference method or procedure.

The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified. For a complete list of the Laboratory�s NELAC certified parameters please contact customer service.


Lewistown Road

Final Report




Ashland VA, 23005




Client Name:

Purchase Order:

June 4, 2013 14:40Date Received:July 2, 2013 11:28

Lewistown Road

Final Report



Lewis Ditch N 13F0045-01 06/04/2013 14:40Soil 06/04/2013 13:00

Lewis Ditch S 13F0045-02 06/04/2013 14:40Soil 06/04/2013 13:30

Ramp Ditch 1 13F0045-03 06/04/2013 14:40Soil 06/04/2013 14:00

This Certificate of Analysis is being reissued on July 2, 2013 to reflect results calculated based on dry weight.

Page 2 of 7




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 13:00

Analytical Results


Date/Time Sampled:

Wet Chemistry Analysis

Percent Solids SM18/2540G 12.8 % 06/28/2013 16:15 06/28/2013 16:15 LRGH 0.1




Date/Time

13F0045-01RE1Lewis Ditch N

06/04/2013 13:00

Analytical Results


Date/Time Sampled:

Microbiological Analysis

E. Coli Colilert 18/QT 38200 MPN/g dry 06/06/2013 15:49 06/06/2013 15:49 MFMH 783

Fecal Coliform SM18/9221E 700000 MPN/g dry 06/06/2013 14:35 06/06/2013 14:35 MFMH 78




Date/Time

13F0045-02Lewis Ditch S

06/04/2013 13:30

Analytical Results


Date/Time Sampled:




E. Coli Colilert 18/QT 53 MPN/g dry 06/04/2013 16:20 06/04/2013 16:20 MFM1

Fecal Coliform SM18/9221E 400 MPN/g dry 06/04/2013 17:18 06/04/2013 17:18 MFM13

Page 3 of 7




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time


06/04/2013 14:00

Analytical Results


Date/Time Sampled:




E. Coli Colilert 18/QT 22 MPN/g dry 06/04/2013 16:20 06/04/2013 16:20 MFM1

Fecal Coliform SM18/9221E 31 MPN/g dry 06/04/2013 17:18 06/04/2013 17:18 MFM13



13F0045-01,13F0045-01RE1,13F0045-02,13F0045-03BWF0101 Colilert 18/QT

13F0045-01,13F0045-01RE1,13F0045-02,13F0045-03BWF0103 SM18/9221E

13F0045-01,13F0045-02,13F0045-03BWG0013 SM18/2540G

Page 4 of 7




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

Wet Chemistry Analysis - Quality Control


Batch BWG0013 - No Prep Halides

Blank (BWG0013-BLK1) Prepared & Analyzed: 06/28/2013

Percent Solids 0.1 %100 %

Duplicate (BWG0013-DUP1) Prepared & Analyzed: 06/28/2013Source: 13F0045-03

Percent Solids 0.1 200.280%74.9 % 75.2 %

Page 5 of 7




Ashland VA, 23005




Client Name:

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Final Report



Code Description Cert Number Expires

341 12/31/2013Maryland DE Drinking WaterMdDOE

495 12/13/2013North Carolina DENRNC

460021 06/14/2014NELAC-VirginiaVELAP Certificate #2113

350 11/01/2013West Virginia DEPWVDEP

Page 6 of 7




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report


H Analysis was performed outside of the method prescribed holding time.


QualifersQual


Page 7 of 7




Client Name:


Sincerely,


Ashland, VA 23005


Purchase Order:


Date Issued:

Date Received:

Submitted To:

Client Site I.D.:

June 11, 2013 14:37


Joshua Shrader

End Notes:





Lewistown Road

Final Report




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



020-03/TW-01 13F0118-01 06/06/2013 11:40Waste Water 06/03/2013 09:35

Trip Blank 13F0118-02 06/06/2013 11:40Waste Water 05/31/2013 10:45

Page 2 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report




Date/Time

13F0118-01020-03/TW-01

06/03/2013 09:35

Analytical Results


Date/Time Sampled:

Volatile Organic Compounds by GC

Benzene SW8021B DMB<1.00 ug/L 06/10/2013 14:50 06/10/2013 14:501.00

Toluene SW8021B <1.00 ug/L 06/10/2013 14:50 06/10/2013 14:50 DMB1.00

Ethylbenzene SW8021B DMB<1.00 ug/L 06/10/2013 14:50 06/10/2013 14:501.00

m+p-Xylenes SW8021B DMB<4.00 ug/L 06/10/2013 14:50 06/10/2013 14:504.00

o-Xylene SW8021B DMB<2.00 ug/L 06/10/2013 14:50 06/10/2013 14:502.00

Xylenes, Total SW8021B DMB<6.00 ug/L 06/10/2013 14:50 06/10/2013 14:506.00

80-12087.3 %Surrogate: 2,5-Dibromotoluene 06/10/2013 14:50 DMB06/10/2013 14:50




Date/Time

13F0118-02Trip Blank

05/31/2013 10:45

Analytical Results


Date/Time Sampled:

Volatile Organic Compounds by GC

Benzene SW8021B DMB<1.00 ug/L 06/10/2013 14:03 06/10/2013 14:031.00

Toluene SW8021B DMB<1.00 ug/L 06/10/2013 14:03 06/10/2013 14:031.00

Ethylbenzene SW8021B DMB<1.00 ug/L 06/10/2013 14:03 06/10/2013 14:031.00

m+p-Xylenes SW8021B DMB<4.00 ug/L 06/10/2013 14:03 06/10/2013 14:034.00

o-Xylene SW8021B DMB<2.00 ug/L 06/10/2013 14:03 06/10/2013 14:032.00

Xylenes, Total SW8021B DMB<6.00 ug/L 06/10/2013 14:03 06/10/2013 14:036.00

80-12094.2 %Surrogate: 2,5-Dibromotoluene 06/10/2013 14:03 DMB06/10/2013 14:03

Page 3 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



13F0118-01,13F0118-02BWF0192 SW8021B

Page 4 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

Volatile Organic Compounds by GC - Quality Control




Benzene 1.00 ug/L<1.00 ug/L

Toluene 1.00 ug/L<1.00 ug/L

Ethylbenzene 1.00 ug/L<1.00 ug/L

m+p-Xylenes 4.00 ug/L<4.00 ug/L

o-Xylene 2.00 ug/L<2.00 ug/L

Xylenes, Total 6.00 ug/L<6.00 ug/L

100 80-120Surrogate: 2,5-Dibromotoluene 100100 ug/L


Benzene 1.00 100 70-13084.4ug/L84.4 ug/L

Toluene 1.00 100 70-13083.7ug/L83.7 ug/L

Ethylbenzene 1.00 100 70-13094.2ug/L94.2 ug/L

m+p-Xylenes 4.00 200 70-130101ug/L202 ug/L

o-Xylene 2.00 100 70-130102ug/L102 ug/L



Benzene 1.00 100 2070-13084.8 0.426ug/L84.8 ug/L

Toluene 1.00 100 2070-13082.5 1.42ug/L82.5 ug/L

Ethylbenzene 1.00 100 2070-13092.1 2.25ug/L92.1 ug/L

m+p-Xylenes 4.00 200 2070-13098.7 2.21ug/L197 ug/L

o-Xylene 2.00 100 2070-130100 1.89ug/L100 ug/L



Benzene 1.00 100 70-13084.2ug/L84.2 ug/L <1.00 ug/L

Toluene 1.00 100 70-13081.8ug/L81.8 ug/L <1.00 ug/L

Ethylbenzene 1.00 100 70-13090.3ug/L90.3 ug/L <1.00 ug/L

m+p-Xylenes 4.00 200 70-13096.0ug/L192 ug/L <4.00 ug/L

o-Xylene 2.00 100 70-13097.8ug/L97.8 ug/L <2.00 ug/L

100 80-120Surrogate: 2,5-Dibromotoluene 94.694.6 ug/L

Page 5 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Qual Analyte

Volatile Organic Compounds by GC - Quality Control




Benzene 1.00 100 2070-13084.0 0.202ug/L84.0 ug/L <1.00 ug/L

Toluene 1.00 100 2070-13082.0 0.195ug/L82.0 ug/L <1.00 ug/L

Ethylbenzene 1.00 100 2070-13090.9 0.629ug/L90.9 ug/L <1.00 ug/L

m+p-Xylenes 4.00 200 2070-13097.2 1.27ug/L194 ug/L <4.00 ug/L

o-Xylene 2.00 100 2070-13098.9 1.09ug/L98.9 ug/L <2.00 ug/L

100 80-120Surrogate: 2,5-Dibromotoluene 94.994.9 ug/L

Page 6 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



SW8021B in Non-Potable Water

Benzene VELAP,NC,WVDEPToluene VELAP,NC,WVDEPEthylbenzene VELAP,NC,WVDEPm+p-Xylenes VELAP,NC,WVDEPo-Xylene VELAP,NC,WVDEPXylenes, Total VELAP,NC,WVDEP


Page 7 of 8




Ashland VA, 23005




Client Name:

Purchase Order:


Lewistown Road

Final Report



QualifersQual


Page 8 of 8

phase ii environmental site assessment proposed lewistown

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