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PRE-FEASIBILITY REPORT
“Expansion of Manufacturing capacity of
Herbicides/Fungicides/Plant Growth Regulators (PGRs) from
635.125 MT/A to 1006.25 MT/A”
At: M/S. Godrej Agrovet Limited,
E-24, E-24(Part), E-23/1, Lote Parashuram MIDC, Tal: Khed Dist: Ratnagiri
Report prepared by:
Dr. Subbarao’s Environment Center (QCI NABET Accredited Consulting Organization)
Godrej Agrovet Ltd., Lote Parashuram, Khed (Tq.) Ratnagiri (Dst.) PRE FEASIBILITY REPORT
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CONTENTS
CONTENTS ........................................................................................................................................ 1
1. EXECUTIVE SUMMARY .............................................................................................................. 3
2. INTRODUCTION OF THE PROJECT / BACKGROUND INFORMATION .................................. 4
2.1 Identification of Project and Project proponent ......................................................................... 4
2.2 Brief description of nature of the project................................................................................... 4
2.3 Need for the project and its importance to the country and or region ......................................... 4
2.4 Demand-Supply gap ................................................................................................................. 4
2.5 Imports vs. Indigenous products ............................................................................................... 4
2.6 Export possibility ..................................................................................................................... 4
2.7 Employment Generation (Direct and Indirect) due to the project ............................................... 4
3. PROJECT DESCRIPTION .............................................................................................................. 5
3.1 Type of project including interlinked and inter dependent projects, if any. ................................ 5
3.2 Location: .................................................................................................................................. 5
General Location: ............................................................................................................................ 5
Specific Location and Project boundaries: ........................................................................................ 5
3.3 Details of alternate sites considered and the basis of selecting the proposed site (particularly the
environmental considerations gone into should be highlighted) ............................................................ 6
3.4 Size or magnitude of operation ................................................................................................. 6
3.5 Project description with process details .................................................................................... 6
3.6 Raw material required along with estimated quantity, likely source, marketing area of final
product, Mode of transport of raw material and finished product. ......................................................... 6
3.7 Resource optimization / recycling and reuse envisaged in the project, should be briefly outlined.
9
3.8 Availability of water its source, Energy / Power requirement and source................................. 10
3.9 Quantity of waste to be generated (liquid and solid) and scheme for their Management/Disposal
10
4. SITE ANALYSIS .......................................................................................................................... 11
4.1 Connectivity........................................................................................................................... 11
4.2 Land Form, Land use and Land ownership ............................................................................. 11
4.3 Existing land use pattern (agriculture, non-agriculture, forest, water bodies (including area
under CRZ)) ...................................................................................................................................... 11
4.4 Existing Infrastructure ............................................................................................................ 11
4.5 Soil Classification .................................................................................................................. 11
4.6 Climatic data from stationary sources ..................................................................................... 11
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4.7 Social Infrastructure available ................................................................................................ 11
5. PLANNING BRIEF....................................................................................................................... 12
5.1 Planning Concept (type of industries, facilities, transportation etc.) Town and country planning /
Development authority Classification................................................................................................. 12
5.2 Population Projection ............................................................................................................. 12
5.3 Land use planning (breakup along with green belt etc)............................................................ 12
5.4 Assessment of Infrastructure Demand (Physical and Social) ................................................... 12
5.5 Amenities / Facilities .............................................................................................................. 12
6. PROPOSED INFRASTRUCTURE ................................................................................................ 13
6.1 Industrial Area (Processing Area) ........................................................................................... 13
6.2 Residential Area (Non Processing Area) ................................................................................. 13
6.3 Green belt .............................................................................................................................. 13
6.4 Social Infrastructure ............................................................................................................... 13
6.5 Connectivity (Traffic and Transportation Road/Rail/Metro/Water ways etc.) .......................... 13
6.6 Drinking Water Management (Source and Supply of water) ................................................... 13
6.7 Sewerage System ................................................................................................................... 13
6.8 Industrial Waste Management ................................................................................................ 13
6.9 Solid Waste Management ....................................................................................................... 13
6.10 Power requirement & Supply / Source .................................................................................... 13
7. PROJECT SCHEDULE AND COST ESTIMATES ....................................................................... 14
7.1 Likely date of start of construction and likely date of completion (Time schedule for the project
to be given)........................................................................................................................................ 14
7.2 Estimated project cost along with analysis in terms of economic viability of the project .......... 14
8. ANALYSIS OF PROPOSAL (Final recommendations) ................................................................. 15
8.1 Financial and social benefits with special emphasis on the benefit to the local people including
tribal population, if any, in the area. ................................................................................................... 15
Annexure – I ...................................................................................................................................... 16
Process Flow Diagrams: .................................................................................................................... 16
Annexure – II .................................................................................................................................... 25
Quantity of waste to be generated (Solid, Liquid and Hazardous) ....................................................... 25
Annexure – III ....................................................................................................................................... 26
Photographs ....................................................................................................................................... 26
Godrej Agrovet Ltd., Lote Parashuram, Khed (Tq.) Ratnagiri (Dst.) PRE FEASIBILITY REPORT
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1. EXECUTIVE SUMMARY
Godrej Agrovet Limited (GAVL) is a diversified, Research & Development focused agri-business
company, dedicated to improving the productivity of Indian farmers by innovating products and services that sustainably increase crop and livestock yields. It holds leading market positions in the different
businesses in which we operate - Animal Feed, Crop Protection, Oil Palm, Dairy and Poultry and
Processed Foods. In Decemeber 2013, GAVL took over M/s Gouldmohar Agrochem & Feeds Ltd which was formerly known as Bahar Agrochem & Feeds Ltd., which was established in 1986 & Commercial
production was started in 1987. The industry is located in Lote Parashuram MIDC area.
GAVL has an existing manufacturing capacity of 635.125 MT/A. and it proposes to expand its capacity to
1006.25 MT/A. The industry has a valid Consent to Operate from Maharashtra Pollution Control Board, valid upto 30/06/2021. The present application is for Environmental Clearance for the proposed
expansion of the products Herbicides/Fungicides/PGRs.
The present water requirement is 36 m3/ day which is taken from MIDC water supply. After expansion
the water requirement shall be 116 m3/ day which shall be taken from MIDC for which necessary
application is being submitted. The effluent quantity after expansion shall be 23 m3/ day, out of which 6
m3/ day is domestic effluent. The effluent is treated to the Consent conditions of the Maharashtra
Pollution Control Board and treated effluent is sent to CETP for further treatment and disposal, for which
necessary application is being made to MIDC. The domestic effluent shall be treated based on Root zone
technology and treated effluent shall be used for gardening / Green belt development.
In order to reduce the effluent generation, the industry proposes to concentrate the effluents in Multiple Effect Evaporator (MEE) and concentrated effluents are dried by Agitating Thin Film Dryer (ATFG) and
the dried solids are disposed along with Hazardous waste.
The Hazardous waste generated is sent to MWML, Mumbai (CHWTSDF) for further treatment and disposal.
The Non-Hazardous solid waste such as Drums/Containers are being decontaminated and sold to
authorized recyclers. Other solid waste material such as Paper, Wood and Plastics etc. are sold to recyclers/open market.
The industry has developed Green belt area of 3545 sq. m. covering 33 % of the total area. As per the
CPCB guidelines, total of 535 trees are required. Industry have already planted 200 trees in Green belt
area, also it has planted some of the trees along the roadside.
The industry implemented Rain Water Harvesting system and collecting around 1,25,000 liters of water
which is being used for Process operations.
The industry has carried out Risk Assessment studies and implemented all the measures to avoid any
accidents and provides protective safeguards to all the employees. Regular health checkups once in three
months for all employees and special care and medical aids are given to the needy people.
The industry has undertaken a number of social and cultural activities to the nearby local population and
proposes to reserve 2.5 % of the capital cost of the project as CSR activities.
The industry has provided online monitoring system and connected to CPCB/MPCB servers.
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2. INTRODUCTION OF THE PROJECT / BACKGROUND INFORMATION
2.1 Identification of Project and Project proponent
This project is of expansion in manufacturing capacity of Herbicides/Fungicides/PGRs from 635.125
MT/A to 1006.25 MT/A by M/S. Godrej Agrovet Pvt. Ltd., Lote Parashuram, Taluka: Khed, District:
Ratnagiri.
Project Proponent:
Name: M/S. Godrej Agrovet Limited, Lote Parashuram, Taluka: Khed, District: Ratnagiri.
Address: Plot no. – E-24, E-24 (Part) and E-23/1,
MIDC Lote Parashuram, Taluka: Khed, District: Ratnagiri.
Latitude: 17º 36’ 26” N, Longitude: 73º 29’ 28” E
Phone no.: (02356) - 272214
Mobile no.: (+91) - 9920834388
2.2 Brief description of nature of the project
GAVL manufactures herbicides / fungicides/ PGRs for different applications. It has an existing capacity
of 635.125 MT/A and proposes to expand to 1006.25 MT/A.
2.3 Need for the project and its importance to the country and or region
Herbicides play an important role in maintaining plant health. India being an agro based country, the use
of herbicides / fungicides/ PGRs is being widely practiced. Besides, there is a tremendous potential to
export herbicides / fungicides/ PGRs in third world countries. The use of herbicides / PGRs would help to
improve the growth and weed out the unwanted material which would hinder the plant yield. It is also
productive and profitable for farmers to use Herbicides/ Fungicides / PGRs instead of conventional ways
of farming.
2.4 Demand-Supply gap
There is huge demand for Herbicides in Indian as well as in International markets.
2.5 Imports vs. Indigenous products
Some of the products / raw material are imported for manufacture of indigenous products.
2.6 Export possibility
At present, many of the products are exported to third world countries and the demand for exporting is
increasing day by day.
2.7 Employment Generation (Direct and Indirect) due to the project
There could be direct employment opportunities for local people due to this expansion project. Also,
increased transportation and other activities would generate additional indirect employment opportunities.
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3. PROJECT DESCRIPTION
3.1 Type of project including interlinked and inter dependent projects, if any.
The project is not of interlinked and interdependent type.
3.2 Location:
General Location:
Figure 1 General Location
Specific Location and Project boundaries:
Figure 2 Specific Location and Project Boundary
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Table 1 Location and Project boundaries with coordinates
Description Latitude Longitude
South 17° 36' 24" N 73° 29' 23" E
North 17° 36' 28" N 73° 29' 24" E
East 17° 36' 27" N 73° 29' 29" E
South West 17° 36' 25" N 73° 29' 22" E
3.3 Details of alternate sites considered and the basis of selecting the proposed site (particularly
the environmental considerations gone into should be highlighted)
The existing site facilities are adequate for the proposed expansion. Also, existing site is well connected
to National Highway (66) and available with all the amenities. Hence, no alternate site is necessary to be
considered.
3.4 Size or magnitude of operation
The proposed change in existing production capacity is as follows:
Sr.
No.
Products Quantity (MT/A)
Present Proposed Total
1 Liquid Vipul, Vipul granules, Diamore Suruchi, Ruchira 36 0 36
2 Achook Nimin 36 0 36
3 Combined (PGR) like super shakti & Diamore combine
&double
12 0 12
4 Bumper Bountee 12 0 12
5 Dapcoat 24 0 24
6 Homobrassinolide (HBR) 0.6 0.9 1.5
7 GOD –HH001 Pyrithioback Sodium Tech. 40 20 60
8 Agroneem 200 0 200
9 Hitweed Pyrithiobac Sodium 10% 36 0 36
10 Neem oil Emulsifiable 24 0 24
11 Bispyribac Sodium Technical 40 20 60
Bispyribac Sodium Formulation 144.405 0 144.405
12 Florchlorfenuron Technical 20 30 50
Florchlorfenuron Formulation. 10.12 0 10.12
13 Quizalofap-P-Ethyl Technical 00 60 60
14 Thiophanate Methyl technical 00 60 60
15 Metribuzin Technical 00 60 60
16 Trifloxystrobin Technical 00 60 60
17 Dimethomorph Technical 00 60 60
TOTAL 635.125 370.9 1006.25
3.5 Project description with process details
Process flow sheet diagrams indicating manufacturing process and raw material requirement is attached
as an Annexure – I.
3.6 Raw material required along with estimated quantity, likely source, marketing area of final
product, Mode of transport of raw material and finished product.
Raw materials are available in open market. Final products are sold in both Indian and International
markets. Both raw materials and products are transported by road.
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Raw material quantities with respect to the finished products are as per the following:
Sr.
No.
Raw Materials
Present
MT/A
Proposed
MT/A
Total
MT/A
1 Homobrassinolide (batch size : 1.10 kg) 0.600 0.900 1.500
1. Stigmasterol 1.143 1.715 2.858
2. Methyl Ethyl Ketone (M.E.K.) 27.818 41.727 69.545
3. Triethylamine 0.777 1.165 1.942
4. Methanesulphonyl Chloride (Mesyl chloride) 0.327 0.491 0.818
5. Chromium trioxide (CrO3) 0.202 0.303 0.505
6. Sulfuric acid (H2SO4 ) 0.176 0.263 0.439
7. Magnesium sulphate-(MgSO4) 0.545 0.818 1.364
8. Dimethyl formamide (D.M.F.) 11.018 16.527 27.545
9. Molecular sieves 1.091 1.636 2.727
10.p-Toluene sulphonic acid (P.T.S.A.) 0.106 0.159 0.265
11.Sodium bromide (NaBr) 0.144 0.216 0.360
12.Ethylacetate (E.A) 75.273 112.909 188.182
13. Silica gel 20.509 30.764 51.273
14. Petroleum ether / n-Hexane (60-80
oC) 174.545 261.818 436.364
15. Tetrahydrofuran (T.H.F.) 10.255 15.382 25.636
16. Osmium tetroxide 0.027 0.041 0.068
17. t-Butanol 0.901 1.352 2.253
18. N-Methyl morpholine-N-oxide (N.M.O.) 0.648 0.972 1.620
19. Sodium bisulfite solution 1.091 1.636 2.727
20. Celite 545 0.545 0.818 1.364
21. Pyrimidine 2.302 3.453 5.755
22. Potassium hydroxide (KOH) 0.218 0.327 0.545
23. 4-Dimethylamino pyrimidine (D.M.A.P.) 0.158 0.237 0.395
24. Acetic anhydride 1.584 2.376 3.960
25. Ethylene dichloride (EDC) 16.364 24.545 40.909
26. Dichloromethane (CH2Cl2) 70.909 106.364 177.273
27. Trifluoroacetic anhydride ((CF3CO)2O 4.429 6.644 11.073
28. Hydrogen peroxide (H2O2) 1.211 1.816 3.027
29. Disodium hydrogen phosphate (Na2HPO4) 4.135 6.202 10.336
30. Methanol (CH3OH) 22.505 33.758 56.264
31. Potassium carbonate 1.527 2.291 3.818
32. Chloroform (CHCl3) 27.273 40.909 68.182
33. Acetone 21.818 32.727 54.545
34. Calcium chloride (CaCl2) 0.218 0.327 0.545
35. Sodium chloride (NaCl) 21.382 32.073 53.455
36. Sodium bicarbonate (NaHCO3) 0.665 0.998 1.664
37. Sodium sulphate ( Na2SO4) 14.182 21.273 35.455
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38. Hydrochloric acid ( Hcl) 7.855 11.782 19.636
2 PYRITHIOBAC SODIUM BATCH SIZE: 110kg 40.000 20 60.000
Step –I
1 2, 6 Dichloro benzonitrile 41.818 20.909 62.727
2 N-methyl pyrilidone 250.909 125.455 376.364
3 Sodium sulphide-60% 79.273 39.636 118.909
Step-II
1. Product of Step-I MCBN
2. Sodium sulphide-60% 14.545 7.273 21.818
3. Sodium hydroxide flakes 54.182 27.091 81.273
4. Water 236.364 118.182 354.545
5. Hydrochloric acid (1:1) 472.727 236.364 709.091
6. Dichloromethane 327.273 163.636 490.909
Step-III
1. Product of Step-II MCBA 40.000 20 60.000
2. 2-Methylsulfonyl 4,6-Dimethoxypyrimidine 381.819 190.909 572.728
3. Potassium carbonate 45.455 22.727 68.182
4. Tetra butyl ammonium bromide 0.909 0.455 1.364
5. Sodium sulphate 1.818 0.909 2.727
6. Hydrochloric acid (1:1) 109.091 54.545 163.636
Step-IV
1. Product of Step-III Pyrithiobac acid
2. Sodium carbonate 8.327 4.164 12.491
3. Methanol 290.909 145.455 436.364
3 CPPU (BATCH SIZE:0.9 Kgs) 20.000 30 50.000
1. 2-CPA 2.222 3.333 5.555
2. Dichloromethane 33.333 50.000 83.333
3. Phenyl Isocyanate 2.222 3.333 5.555
4. Petroleum ether 6.667 10.001 16.668
5. Methanol 6.667 10.001 16.668
6. Toluene 33.333 50.000 83.333
4 BIS PYRIBAC SODIUM (BATCH SIZE: 150 KG) 40.000 20 60.000
1. DHBA 27.200 13.6 40.800
2.Sodium Hydroxide prills 20.800 10.4 31.200
3. 2-Methylsulfonyl 4,6-Dimethoxypyrimidine 76.000 38.000 114.000
4. Tetra butyl ammonium bromide 533.000 266.500 799.500
5. Toluene 133.333 66.667 200.000
6. Ethyl acetate 146.667 73.334 220.001
5 Quizalofop ethyl Techanical 0 60 60
1. OHOP 0 44.34 44.34
2. Sulphuric acid 0 6.12 6.12
3. Ethanol 0 21.6 21.6
4. Etyl acetate 0 330 330
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5. Sodium bicarbonate 0 20.94 20.94
6. DCQ 0 41.58 41.58
7. Potssium carbonate 0 35.16 35.16
8. Acetonitrile 0 186 186
6 MetriBuzin Tech 0 60 60
t-Butyl methyl ketone 0 42 42
Thionyl Chloride 0 60 60
Dichloro methane 0 9 9
Dimethyl amine 0 60 60
20% NaOH in water( including Scrubber) 0 360 360
Thiocarbohydrazide 0 48 48
Methyl Bromide 0 42 42
Dichloro ethane 0 21 21
7 Dimethomorph tech 0 60 60
4-Chloro-3,4-Dimethoxy bezophenone 0 60 60
Catalyst Zn-Cu- V 0 0.6 0.6
N- Acetyl Morpholine 0 30 30
Toluene 0 9 9
Methanol 0 30 30
8 Thiophanate methyl Tech 0 60 60
Methyl Chloroformate 0 19.8 19.8
Sodium thiocyanate 0 17.4 17.4
Solvent -I(EDC) 0 15 15
O-phenylenediamine 0 22.8 22.8
Solvent -II(MDC) 0 9 9
9 Trifloxystrobin Tech 0 60 60
3-Trifluoromethy acetophenone 0 66 66
Ethanol 0 5 5
Hydroxylamine hydrochloride 0 30 30
2-methyl phenyl(oxo)acetic acid 0 60 60
20% NaOH in water( including Scrubber) 0 180 180
Terabutyl ammonium bromide 0 6 6
Dichloro ethane 0 21 21
Thionyl chloride 0 36 36
Methanol 0 9 9
Acetonitrile 0 7.5 7.5
N-Bromosuccinamide 0 51 51
Methyl isobutylketone 0 150 150
Potassium Carbonate 0 48 48
Water 0 120 120
3.7 Resource optimization / recycling and reuse envisaged in the project, should be briefly
outlined.
Maximum recycling and recovery of solvents is carried out in the manufacturing process
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3.8 Availability of water its source, Energy / Power requirement and source
Water permission is already available from the MIDC. At present, water requirement is 36 m3/ day and
after expansion, it shall be 116 m3/ day. Effluent quantity generated shall be increased from 15 m
3/ day to
23 m3/ day, out of which 6 m
3/ day shall be domestic effluent.
Table 2 Water budget
PRESENT (m3/day) PROPOSED (m
3/day) TOTAL (m
3/day)
CONSU
MPTION
LOSSES
/USED
EFFL
UENT
CONSU
MPTION
LOSSES
/USED
EFFL
UENT
CONSU
MPTION
LOSSES
/USED
EFFL
UENT
Domestic 08 04 04 4 2 02 12 06 06
Industrial 11 0.5 10.5 6 1 5 17 1.5 15.5
Boiler 05 4.5 0.5 50 49 1 55 53.5 1.5
Cooling 2 2 0 18 18 0 20 20 0
Gardening 10 10 00 2 2 0 12 12 0
TOTAL 36 21 15 80 72 8 116 93 23
3.9 Quantity of waste to be generated (liquid and solid) and scheme for their
Management/Disposal
Details of the waste generation are attached in this report as an Annexure - II
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4. SITE ANALYSIS
4.1 Connectivity
Existing Site is conveniently located in Lote Parashuram MIDC.
4.2 Land Form, Land use and Land ownership
Land is in MIDC area.
4.3 Existing land use pattern (agriculture, non-agriculture, forest, water bodies (including area
under CRZ))
Existing land comes under industrial estate. There is no reserved forest, eco sensitive areas, wild life
sanctuaries and CRZ within 10 km radius of industry.
4.4 Existing Infrastructure
Existing infrastructure is adequate for the proposed expansion.
4.5 Soil Classification
Soil observed in the study area is mostly Clayey Loam.
4.6 Climatic data from stationary sources
The wind direction is predominantly blowing from West to East. Normal temperature range is 10 ºC to
42ºC and the relative humidity varies from 50% to 85 %. The maximum rainfall observed is around 880
mm.
4.7 Social Infrastructure available
The factory situated in Lote Parashuram industrial area which has facilities of Gymkhana, Sports complex
and recreational club, restaurants. The entire MIDC area is well connected by 20 m wide roads. It has
national highway (NH-66) 1 km away.
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5. PLANNING BRIEF
5.1 Planning Concept (type of industries, facilities, transportation etc.) Town and country
planning / Development authority Classification
It is situated in Industrial area.
5.2 Population Projection
Not Applicable.
5.3 Land use planning (breakup along with green belt etc)
Sr. No. Description Area in Sq. m.
1 Built up area
a. Existing
b. Proposed
3108.43
849
2 Storage area
(Raw material, finished product and hazardous waste)
476.62
3 Internal Roads 1100
4 ETP 598
5 Parking 545
6 Greenbelt 3544.86
7 Vacant Land 520.09
Total 10742
5.4 Assessment of Infrastructure Demand (Physical and Social)
The existing infrastructure facilities for the proposed expansion project would be adequate. The social
infrastructure facilities are available in the MIDC area, which would be adequate.
5.5 Amenities / Facilities
Being situated in MIDC area, all the infrastructure facilities are available.
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6. PROPOSED INFRASTRUCTURE
6.1 Industrial Area (Processing Area)
Total of 849 sq. m. area shall be used for the proposed expansion activities.
6.2 Residential Area (Non Processing Area)
Not applicable
6.3 Green belt
Total area of 3544.86 sq. m. is provided, which approximately 33 % of total plot area. As per the CPCB
guidelines, there should be 1500 trees per hectare. GAVL needs to have 540 trees (0.3534 ha). GAVL
already planted 200 trees so far, remaining trees shall be planted along with the expansion.
6.4 Social Infrastructure
MIDC facilities.
6.5 Connectivity (Traffic and Transportation Road/Rail/Metro/Water ways etc.)
Not Applicable.
6.6 Drinking Water Management (Source and Supply of water)
MIDC
6.7 Sewerage System
CETP
6.8 Industrial Waste Management
CETP
6.9 Solid Waste Management
MWML, Mumbai (CHWTSDF)
6.10 Power requirement & Supply / Source
At present, Power requirement of 550 KVA is fulfilled by MSEDCL grids. After proposed expansion, it
shall be 1100 KVA. DG Set is used as a power backup of 200 KVA capacity, after expansion it shall be
500 KVA.
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7. PROJECT SCHEDULE AND COST ESTIMATES
7.1 Likely date of start of construction and likely date of completion (Time schedule for the
project to be given)
Construction shall be started once the Environmental Clearance is obtained. And the project shall be
completed within 1 year of receipt of Environmental Clearance.
7.2 Estimated project cost along with analysis in terms of economic viability of the project
The project cost estimated is around 10 crore rupees.
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8. ANALYSIS OF PROPOSAL (Final recommendations)
8.1 Financial and social benefits with special emphasis on the benefit to the local people
including tribal population, if any, in the area.
Employment opportunities are generated to local people and strengthening the financial condition of the
industry. The products are import substitution and savings in foreign exchange. Industry has earmarked
2.5 % of the total project cost for Corporate Social Responsibility (CSR) activities. Details of CSR
activities undertaken so far are given as under:
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Annexure – I
Process Flow Diagrams:
Title: PROCESS FLOW DIAGRAM FOR PYRITHIOBAC SODIUM
Water: 1540
Kg
Solvent: 4100 Kg Recovered.
Solvent: 4400 Kg Sodium Sulphide: 1726
Kg
Chlorinated Benzonitrile (DCBN): 885
Kg
DEHALOGENATION: R1
Sodium Hydroxide: 3500
Kg
Water: 885 Kg HYDROLYSISR3 7951 Kg
HCL (25%): 2500 Kg ACIDIFICATION-1R213241 kg
Effluent: 3860Kg
Water (ICE): 1990 Kg
Potassium Carbonate: 840 Kg Water: 4400 Kg
Pyrimidine: 590 Kg
Methylene Chloride: 800 Kg
COUPLING
R415229 kg
WORK-UP SEPARATOR
9381 Kg
Water Wash: 3300 Lit
Effluent: 3300Kg
Tetra butyl Ammonium
Bromide: 18Kg
Acidification – 2 R2 18549 kg HCL (25%): 1550 Kg Water: 1770 Kg
Centrifuge Effluent: 21667Kg
Pyrithiobac Sodium Tech.
1000 Kg
Water Wash: 4118 Kg
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Title: PROCESS FLOW DIAGRAM FOR HOMOBRASSINOLIDE
MESSYLATION
67 kg
LACTONISATION626
Kg
ACETYLATION 540.19
Kg
625.319 Kg
HYDROXYLATION
526.05 kg
475.
REARRANGEMENT
495.5 Kg
OXIDATION
415.kg
SOLVOLYSIS
124 kg
HYDROLYSIS 541.44
Kg
Stigma sterol: 2 Kg. Triethyl Amine:
1.5 Kg, Messyl Chloride: 0.5 Kg
Methyl Ethyl Ketone (Recycled): 50 Kg
Effluent: 13 Kg
Chromium Tri Oxide: 250 gm ,
Sulphuric Acid : 322 Kg , Water : 0.75 Kg
8% Sodium Bicarbonate Sol. 10 Kg
Effluent: 72 Kg
Effluent: 40 Kg Di Methyl Formamide: 20 Kg, sodium
Bromide: 250gm, P-toluene Sulphonic
Acid: 250gm, Ethyl Acetate (Recycled): 50 Kg
Effluent: 40.5
Kg Tetra Hydro furon : 20 Kg , Osmium
Tetroxide : 50 gm, T-Butanol : 1.5 Kg
N-Methyl Morpholene N-Oxide: 1.5 Kg
Sodium bisulphite Soin: 2 Kg, Celite
545: 1 kg, Water: 5 Kg
Effluent: 45.05 Kg
Pyrimidine: 4 Kg , Acetic Anhydride: 2.90 Kg , Ethylene Di Chloride: 10 Kg
4 Dimethyl Ameno Pyrimidine: 290
gm.
Tri Fluro Acetic Anhidride: 8 Kg,
Hydrogen peroxide 2 Kg, Disodium
Hydrogen Phosphate: 8 Kg, Dichlormethane 80 Kg
Effluent: 42.19 Kg
Effluent: 134.82 kg
Effluent: 540.44 Kg
Methanol (Recovered) :10 Kg , Potassium Carbonate :1 Kg, Chloroform 5 Kg ,
10 Kg Water Wash, 3
Kg Bi carbonate wash
60 Kg Water Wash
40 Kg Water Wash
Water50 Kg Reactor washing
30 Kg Water for washing
10 Kg Water -5% HCL
wash
32 Kg Water For reactor wash, 5% HCL Wash, 10 Kg
20 Kg Water wash, 10 Kg Bi
Carbonate wash.
1000 gm
HOMOBRASSINOLIDE
20 Kg water
14.26 Kg Bi Carbonate wash.
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Title: PROCESS FLOW SHEET DIAGRAM FOR BISPYRIBAC SODIUM TECHNICAL
Manufacturing Process: 2,6- dihydroxy benzoic acid undergo condensation reaction with Pyrimidine
(MSDP) compound in aromatic hydrocarbon to give Bispyribac sodium under alkaline condition. The
product is isolated by filtration at room temperature and washed with toluene, ethyl acetate and water.
The product is dried under vacuum.
Condensation Reaction 2380 Kg
Centrifuge 1250 Kg
Sodium Hydroxide
390 Kg
Pyrimidine
1490 Kg 2,6Dihydroxy Benzoic
acid 500 Kg
Crude Product 1250 KG Toluene for recycle
2020 Kg
Toluene for washing 2000 Kg
Effluent 1030 Kg
Crude Product 1230 KG Ethyl Acetate for
washing 1000 Kg
Residue
40 Kg Toluene for recycle
1980 Kg
Ethyl Acetate for recycle
1000 Kg
Toluene for recycle
970 Kg Residue
20 Kg
Crude Product 1230 KG Water washing 500 Kg
Effluent 630 Kg
Drying 1100 KG
Finished Product 1000 KG
Loss 100 Kg
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Title: PROCESS FLOW SHEET DIAGRAM FOR FORCHLORFENURON TECHNICAL
Manufacturing Process: The technical grade product forchlorfenuron is obtained by the reaction of phenyl
isocynate with 2-chloro, 4-aminopyridine. The product form is then reflux with the solvents like dichloromethane
acetone and chloroform. Then water wash is given to get the finished product.
Mixing & Distillation 4550 Kg
2-Chloro-4-aminopyrimidine
1030 Kg
Dichloromethane
2500 Kg Phenyl Isocyanate
1020 Kg
Reflux for 7 Hr. &
Distillation 3300 Kg Acetone 1000 KG Rec. Acetone 900 KG
Reflux 2400 Kg
Rec. Dichloromethane
2250 KG
Chloroform 1000 KG Rec. Chloroform 950 KG
Solvent Distillation Crude Solvent 400 Kg
Rec Solvent
350 Kg
Residue
50 Kg
CRUDE PRODUCT 1050 Water Wash 1200 KG
Effluent 1250 Kg FINISHED PRODUCT
1000 Kg
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Title: PROCESS FLOW DIAGRAM FOR QUIZALOFOP-P-ETHYL
ETHANOL
6050Kg
SULPHURIC ACID: 112
Kg
OPHP 812 Kg
REACTION 6974 kg
DISTILLATION
ETHYL
ACETATE 10320 REACTION MASS 1529 KG
REACTION MASS 10115 KG
REC. ETHANOL 5445
KG
HEATING 11849 KG
REC ETHYL
ACETATE
9804 KG
Sodium Bicarbonate
380 Kg + Water 7690
Kg
DCQ 1058 KG
STIRRING 15158 KG
Effluent: 9057Kg
REACTION MASS 2371 KG
POTASSIUM
CARBONATE 640
KG +
ACETONITRILE
13460 KG
DISTILLATION
DISTILLATION
REC
ACETONITRILE
12787 KG
ETHYL
ACETATE
13750 KG
DISTILLATION 16121 KG
REC ETHYL
ACETATE
13075 KG
REACTION MASS 3041 KG ETHANOL 9690
KG
DISTILLATION 12731 KG REC ETHANOL
9200KG
REACTION MASS 3041 KG WATER WASH 7690
KG
EFFLUENT 9731KG
FINAL PRODUCT 1000 KG
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21
Title: Process flow diagram for Dimethomorph – Technical
1250 kg ETP
Condensation reaction
Reaction
N- Acetyl Morpholine
500 Kg
4-Chloro-3,4-Dimethoxy
benzophenone 1000 Kg
g
Methanol 10000 KG Methanol MLR 10300 KG
Toluene 3000 KG Rec. Toluene 3150 KG
Wet product 1060 kg
Zinc copper- vanadium
catalyst 10 Kg
g
Crude Dimethomorph 1510
kg+ Methanol 10000 kg
Crude Dimethomorph
1210 kg + 3000 kg
Toluene
Pure product 1000 kg
Dryer Loss 60 kg
Distillation: 2700 KG
Distillation 9500
KG
200 kg
loss
Residue
250 kg
Scrubber
500 kg
550 kg loss
1050 kg to ETP
Residue
250 kg
Scrubber
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22
Title: Process flow diagram for Metribuzin – Technical
Manufacturing Process:- : Manufacturing of Metribuzin technical is three-step process.
In the first step, t-Butylmethylketone on chlorination with thionyl chloride dichloroethane, followed by reaction
with dimethylamine to give intermediate-A. In step-2 Intermediate –A reacted with thiocarbohydrazide to give Intermediate –B.
In step-3 Intermediate –B methylated with methyl bromide to give Metribuzin.
t-Butyl methyl ketone 700 kg
Chlorination, Intermediate A 1300 kg
Thionyl Chloride
1000 Kg
Dimetyl amine 1000 Kg Dichloromethane 3000 kg
Intermediate A, 2000 kg Thiocarbohydrazide
700 kg
Hydrolysis &CycIization
Intermediate B, 2800 kg
Methyl bromide 800 kg
Metribuzin 2000 kg
Recovered DCM 3400 kg
Effluent send to ETP 4000 kg
Caustic scrubber 2.0 Kl
Residue 150 kg
Residue 500
kg
Dichloroethane 7000kg
Recovered
Dichloroethane 7800 kg
Dichloroethane for
distillation 6650 kg
3.0kl effluent to ETP
Pure Metribuzin 1000 kg
Water 3000 kg for purification
Residue 350
kg
DCM for distillation
2850 kg
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Product Name:- Thiophanate Methyl – Technical
Manufacturing Process:-
Manufacturing of Thiophanate methyl technical is two-step process.
In the first step, methyl chloroformate is reacted with sodium thiocyanate in an appropriate solvent at low temperature.
This reaction forms methoxy carbonyl isothiocyanate.
This is separated and is subsequently reacted with ortho phenylene diamine to form crude Thiophanate methyl.
Condensation 5685 kg
Reaction
Ethylene dichloride 5000
Kg
Methyl Chloroformate
360 Kg
g
Rec. EDC 5025 KG
Dichloromethane 3000
KG
Rec.
Dichloromethane
3040 KG
Addition reaction 1020Kg
Wet product 1020 kg
Sodium Thiocyanate
325 Kg
g
Separation
Crude 660 kg
O-phenylenediamine 400 kg
Pure product 1000 kg
Dryer Loss 20 kg
Distillation
2800 KG
Distillation 4750
KG
Residue
200 kg
Loss 100 kg
Residue
80 Kg
Scrubber
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Title: Process flow Diagram for Trifloxystrobin Technical
Intermediate-I1280 kg
3-Trifluoromethy
acetophenone550Kg
Ethanol500 Kg
g Dichloromethane1050 kg
Thionyl chloride300 KG
Rec. Methanol 1050 kg
Intermedite-III2540
Intermedite-IV2340
Hydroxylamine
hydrochloride230 Kg
g Reaction
2340 kg
Intermediate-II2590 kg
Methanol 1000 kg
Crude product 1
1040 kg
Potassium Carbonate 200 kg
Methyl isobutylketone1000 kg
Dichloroethane1000 KG
Dichloroethane1000 KG
Terabutyl ammonium
bromide10 KG
2 methyl phenyl (oxo)
acetic acid 500 kg
Acetonitrile 1000 kg
Rec. Dichloromethane1100 kg
N-Bromosuccinamide
100 kg
Intermedite-II2490 kg
Rec ethanol 450
kg
Rec. Acetonitrile 1200 kg
Scrubber
2500 Lit Scrubber
Distillation
Mass 950 kg+
Loss 25
Distillation
DCE950 kg +
Loss 25 Kg
Residue
75kg
Distillation Mass 950 kg Loss 25 Kg
Kg
Residue
75 kg
Residue
125 kg
Distillation
950 kg +
Loss
150Kg Kg
Residue
100 kg
2600 Lit Effluent
ETP
Pure product 1000 kg Water 3500 lit. purification Effluent 3540 kg to
ETP
MIBK 1300 Kg
Residue
100 kg
Distillation
Mass 950 kg
++ Loss
250Kg
Solvent
Separation to
recycle
Godrej Agrovet Ltd., Lote Parashuram, Khed (Tq.) Ratnagiri (Dst.) PRE FEASIBILITY REPORT
25
Annexure – II
Quantity of waste to be generated (Solid, Liquid and Hazardous)
PRODUCT
S LIST
Mfg. Qty MT/A Mfg. Qty KG/D Effluent Generation
in Lit / Day
Residue Generation In
KG/D
PR
ES
EN
T
PR
OP
OS
ED
TO
TA
L
PRES
ENT
PRO
POS
ED
TOT
AL
Efflu
ent
/T
PRES
ENT
PR
OP
OS
ED
TOT
AL
KG
PER
MT
PR
ES
EN
T
PR
OP
OS
ED
TO
TA
L
Homobrass
inolide
(HBR) 0.6 0.9 1.5 1.64
2.47 4.11 9284
50 557 836
1392.
675
0 0 0 0
GOD –
HH001
Pyrithiobac
k Sodium
Tech.
40 20
60
109.5
9
54.79 164.3
8 2882
7 1153 577
1729.
62
0 0 0 0
Bispyribac
Sodium
Technical 40 20 60
109.5
9
54.79 164.3
8 1760 70 35 105.6
60 7 3 10
Florchlorfe
nuron
Technical 20 30 50 54.79
82.19 136.9
9 1250 25 38 62.5
50 2.7
4 4 7
Quizalofap
-P-Ethyl
Technical 0 60 60 0.00
164.3
8
164.3
8 1879
6 0
112
8
1127.
76
0 0 0 0
Thiophana
te Methyl
technical 0 60 60 0.00
164.3
8
164.3
8 500 0 30 280
85 0 14 14
Metribuzin
Technical 0 60 60 0.00
164.3
8
164.3
8 7400 0 444 444 500 0 82 82
Trifloxystr
obin
Technical 0 60 60 0.00
164.3
8
164.3
8 6040 0 362 362
475 0 78 78
Dimethomo
rph
Technical
0 60
60 0.00
164.3
8
164.3
8 1500
0 90 90
500 0 82 82
Total 100
.6
370.
9
471.
5 276 1016
1291.
78
1805.
55
353
9 5595 9 264 273
Godrej Agrovet Ltd., Lote Parashuram, Khed (Tq.) Ratnagiri (Dst.) PRE FEASIBILITY REPORT
26
Annexure – III
Photographs
Factory Main Gate Internal Roads
Green Belt
ETP RO Plant