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HouseHoldindustrial &institutionalCleaning Formulation Guide

ispcleaning.com

in the fast-paced world of household, industrial and institutional cleaningproducts, your customers are constantly expecting something better.

More effective performance•Unique delivery systems•Lower cost in use •

At ISP, we have created a broad portfolio of specialty ingredients that addresses a wide range of formulating challenges and can help you capitalize on trends in the market.

Contents

Household cleaning formulations 3 - 24

Handsoap formulations 24 - 25

Laundry formulations 26 - 30

Dishwashing formulations 30 - 36

Industrial & Institutional cleaning formulations 36 - 38

2

Pages

Application Reference number Title

Hard surface cleaners 11022-64-1 Hard surface cleaner featuring Surfadone® LP-100 & LP-300

11364-58-A8 Hard surface cleaner with ISP MicroBeads™ 20279

11364-136-16 Hard surface cleaner with Setleze™ 3000

11539-68-25 Hard surface cleaner with Triclosan ISP MicroCapsules™ 4448

11539-73-27 Hard surface cleaner with Tea Tree Oil ISP MicroCapsules™ 4371

11040-104-1 Multipurpose alkaline degreaser

11678-41-2 Concentrated all-purpose cleaner

11678-76-6 Plastic surface cleaner

Kitchen 11040-89-1 Kitchen cleaning wipes

11040-105-1 Kitchen disinfectant cleaner

11539-59-33 Kitchen gel cleaner

11678-13-22 Kitchen cream cleaner

Bathroom 11040-93-1 Bathroom cleaner (formula #1)

11539-26-32 Bathroom gel cleaner

11678-7-33 Bathroom cream cleaner

11678-69-19 Opaque toilet bowl cleaner ,chlorine based

11678-71-60 Acidic toilet bowl cleaner featuring Sorez™ HS-205

Wood 11363-152-43 Wooden surface cleaner

11364-62-B13 Wooden surface cleaner with ISP MicroBeads™ 20277

11539-66-25 Wooden surface polish and cleaner

Glass 11040-92-1 Glass cleaning wipes

11539-125-185 Anti-misting glass cleaner

11678-40-10 Anti-static screen cleaner featuring Ceraphyl R 60 and 65

Ceramic 11364-18-8 Ceramic tile cleaner

11364-72-F4 Ceramic tile cleaner with ISP MicroBeads™ 20277

Stainless steel 11364-145-10 Stainless steel cleaner

11539-118-25 Stainless steel gel cleaner

Carpet/floor 11040-77-1 Carpet cleaner

11040-81-1 Machine carpet cleaner

11678-29-11 Carpet spot cleaner

11040-76-2 Floor polish

Misc. 11539-63-14 Abrasive cleaner

11678-16-36 Power cream all purpose cleaner

11040-80-1 Air freshener (formula #1)

Household cleaning formulations

Formulations index

3

Hand soap formulations


Hand soap 11040-61-1 Liquid hand soap

11539-130-9 Paper soap

11364-61-C6 Hand gel cleaner with ISP MicroBeads™ 20279

laundry formulations


Detergent 11040-64-1 Liquid laundry detergent (clear & non-builder)

11364-31-9 Color safe liquid laundry detergent

Softener 11040-69 Fabric softener, 3 formulations

Pre-treatment 11363-25-39 Laundry pre-spotter

ISPM-18.06.2010-1 Stain remover featuring Sorez ™100

Protection 11126-67-1 Protective spray

Packaging 11178-142-1 Water soluble film

11178-142-2 Water soluble film with delayed solubility

11178-142-3 Water soluble flexible film

dishwashing formulations


Detergent 11040-96-1 Washing up liquid featuring Surfadone® LP-300 (formula #1)

11040-97-1 Washing up liquid featuring Surfadone® LP-300 (formula #2)

11040-98-1 Ecological washing up liquid

11364-71-D13 Washing up liquid with ISP MicroBeads™ 20278 (formula #1)

11364-72-E4 Washing up liquid with ISP MicroBeads™ 20278 (formula #2)

11364-79-10 Washing up liquid featuring Surfadone® LP-100

11539-72-22 Washing up liquid with ISP MicroCapsules™ 4449

Tablets 11040-100-1 Dishwasher detergent tablets

industrial & institutional cleaner formulations


Car 11678-10-26 Car shampoo

11678-10-17 Car wash & wax

11678-9-12 Tire wax

11539-152-7 Wheel spray cleaner

Metal 11040-74-1 Metal cleaner

4

FormulationIngredients % W/W Supplier

Aqua/water (D.I. Water) 60.480

Sodium lauryl sulphate (dodecyl sulphate, sodium salt 70%) 20.000 Sigma Aldrich

Coconut diethanolamide (Caflon Cd) 10.000 Ellis & Everard

Ethylene glycol monobutyl ether 5.000 Aldrich

surfadone® lP-300 1.500 isP


Tetrasodium EDTA (Nervanaid BA4) 1.000 Aston Chemicals

integra® 44 0.500 isP

Dye 0.010

Perfume/fragrance 0.010

total 100.000

Hard surface cleaner featuring surfadone® lP-100 & lP-30011022-64-1

Formulation instructions1. Mix all ingredients until uniform.



Jaypol™ tta 2.000 isP

C9-11 Alcohol/8EO (Synperonic 91/8) 2.900 Uniqema

easy-Wet™ 20 0.600 isP


Dye 0.200

Polysorbate 80 0.017 A & E Connock Ltd


Sodium hydroxide (NaOH 50 % aq. solution) 0.160

isP MicroBeads™ 20279 0.100 isP

total 100.000

Hard surface cleaner with isP MicroBeads™ 2027911364-58-a8

1. Add Jaypol™ TTA to water while mixing and neutralize with sodium hydroxide solution (50%).2. Add Synperonic 91/8, Easy-Wet™20 and dye solution (1%).3. Premix Polysorbate 80 & fragrance then add into formulation.4. Add Integra® 44 and ISP MicroBeads™ 20279 with slow, gentle mixing.

Formulation instructions

Formulations

5



Sodium laureth sulphate (70%) (Texapon N70) 1.000 Cognis


Cocoamide diethanol amide (Purton CFD) 0.500 Zschimmer & Schwarz

C12-C18 Alcohol/7EO (Dehydol LT 7) 0.500 Cognis


Sodium tripolyphosphate 0.400 Fisher

Soda ash 0.400 Fisher

Hydroxyethylcellulose (Cellosize QP 30000H) 0.385 Dow


setleze™ 3000 0.200 isP

Polysorbate 80 0.020 A & E Connock Ltd.

Dye 0.020


total 100.000

Hard surface cleaner with setleze™ 300011364-136-16

1. Add Cellosize HEC QP-30000-H in to water and mix very well until it dissolves.2. Add Soda ash and Sodium tri polyphosphate.3. Add Synperonic 91/8, Texapon N70, Dehydol LT7, Purton CFD, Surfadone® LP-100 and dye solution (1%).4. Add the fragrance in the Polysorbate and add to the mixture.5. Add Setleze™ 3000 and Integra® 44.


6

1. Add the Keltrol-T to the water and mix until it dissolves. 2. Add Protelan LS9011, Texapon N70, Surfadone® LP1-00, NaCl and dye solution (0.5%) in this order.3. Premix fragrance with Polysorbate 80.4. Add fragrance mix and Integra® 44.5. Add the ISP MicroCapsules™ and mix gently.



Xanthan gum (Keltrol T) 0.650 CP Kelco

Sodium lauryl ether sulphate 70% (Texapon N70) 5.000 Cognis

Sodium lauroyl sarcosinate (Protelan LS9011) 2.250 Zschimmer & Schwarz

Sodium chloride (NaCl solid) 0.800 Fisher



isP MicroCapsules™ 4448 0.100 isP

Dye 0.020



total 100.000

Hard surface cleaner with triclosan isP MicroCapsules™ 444811539-68-25


7

1. Prepare 2% gel by adding Stabileze® QM to water and heating to 80°C until it dissolves and forms gel.2. Add 18 g from gel Stabileze® QM and Neutralize with NaOH, 50%.3. Add Texapon N70, Surfadone® LP-100, Ceraphyl® 60 and dye solution (0.5%) in order.4. Dissolve the fragrance in the Polysorbate 80 and add to the mixture.5. Add Integra® 44.6. Add the ISP MicroCapsules™ and mixed sensitively.


1. Charge water into the vessel.2. Add caustic soda, followed by LABSA, stir until all neutralized.3. Add tetrapotassium pyrophosphate, Eltesol SX pellet and stir until dissolved.



Tetrapotassium pyrophosphate (28%) 5.000 Albright and Wilson

Sodium xylene sulphonate (Eltesol SX Pellets) 4.500

neP® solvent 2.000 isP

LABSA (linear alkyl benzene sulphonic acid) 1.500 Cognis


Sodium hydroxide 50% 0.500 Fisher



Dye 0.010

total 100.000

Multipurpose alkaline degreaser11040-104-1




stabileze® QM (2% aq. solution) 18.000 isP

Sodium hydroxide (NaOH 50% solution) 0.260 Fisher

Sodium lauryl ether sulphate (70%) (Texapon N70) 2.500 Cognis


Ceraphyl® 60 0.500 isP



Dye 0.100



total 100.000

Hard surface cleaner with tea tree oil isP MicroCapsules™ 437111539-73-27

4. Add Surfadone® LP-300, stir until all dissolved.5. Add the remaining ingredients and stir well until homogeneous.

8

1. Add ingredients respectively in to the water. While adding, make sure each one dissolves completely. 2. Adjust pH with citric acid around 7.00.3. Premix fragrance with Polysorbate 80.4. Add fragrance mixture and Integra® 44 to the formulation.

Formulation Ingredients % W/W Supplier


Lauryl dimethyl amine oxide (Amphotenside DMOX) 5.000 Zschimmer & Schwarz


Sodium lauryl sarcosinate (Protelan LS 9011 ) 8.000 Zschimmer & Schwarz


Sodium chloride (NaCl solid) 1.000 Local Supplier



Polysorbate 80 0.480 A&E Connock Ltd.

total 100.000

Concentrated all purpose cleaner11678-41-2


1. Add ingredients in order shown. While adding, make sure each one dissolves completely.2. Mix fragrance with Polysorbate 80.3. Add fragrance mix and then add Integra® 44.




neP® (solvent) 1.000 isP





total 100.000

Plastic surface cleaner11678- 76-6


9

1. Add the ingredients in the order listed, stirring thoroughly after each addition.2. Apply to wipe substrate in a 1:1 weight ratio.




Isopropyl alcohol (Isopropanol) 2.000 Fisher Scientific

Sodium cocoyl glutamate (Amisoft CS-11) 1.500 Ajinomoto


Sodium hydroxide (10% Aqueous) 1.180 Fisher Scientific



total 100.000

Kitchen cleaning wipes11040-89-1


1. Charge water into the vessel.2. Add tetrapotassium pyrophosphate and EDTA, stir until all dissolved.3. Add Empigen BAC 80, stir until homogeneous.4. Add Surfadone® LP-100, stir until dissolved.5. Add dye and fragrance.




Benzalkonium chloride (80%) (Empigen BAC80) 2.000 Huntsman


EDTA 38% (EDTA ) 0.200 Fisher

Perfume/Fragrance 0.010

Dye 0.010

total 100.000

Kitchen disinfectant cleaner11040-105-1


10

1. Add Jaypol™ AT4 into the water and neutralize with NaOH (50%).2. Mix until a clear solution is obtained.3. Add Sodium Hypochlorite, Stepanate SXS 40, NEP® and dye solution (1%).4. Premix Polysorbate 20 and fragrance then add into formulation. Adjust to desired pH with the NaOH.


Aqua/water (D.I Water) 69.390

Jaypol™ at4 3.000 isP

Sodium hydroxide (NaCl 50% aq. solution) 2.400 Fisher

Sodium hypochlorite (14% NaOCl active chlorine) 17.500 Fisher

Sodium xylene sulfonate 40% (Stepanate SXS 40) 5.000 Stepan


Polysorbate 20 0.760 A E Connock Ltd.

Dye 0.150


total 100.000

Kitchen gel cleaner11539-59-33


1. Add NEP®, Surfadone® LP-100, Protelan LS 9011, Plantacare 818, Antara® 430 and NaOH into water.2. Premix Polysorbate 80 & fragrance then add into formulation.3. Add Integra® 44.


Aqua/water (D.I.Water) 93.721


Coco-glycoside (Plantacare 818) 1.330 Cognis

Sodium lauryl sarcosinate (Protelan LS9011) 1.300 Zschimmer & Schwarz

antara® 430 0.830 isP



Sodium hydroxide (NaOH 50% aq. solution) 0.150 Fisher



total 100.000

Kitchen cream cleaner11678-13-22


11

1. Charge the mixing vessel with the water and commence stirring.2. Add the remaining ingredients with stirring in the order given above.


A. Aqua/water (D.I. Water) 89.580

Glycolic acid 65% 3.000 Aldrich

Lauryl dimethyl amine oxide (30%) 2.000 Zschimmer & Schwarz

Acetic acid (Glacial) 1.500 Fisher Scientific

Alkyl dimethyl benzyl ammonium chloride (50%) (Empigen BAC 50)

1.400 Huntsman

B. surfadone® lP-100 2.500 isP

Perfume 0.010

Dye 0.010

total 100.000

Bathroom cleaner (formula #1)11040-93-1


1. Put Rapifloc™ into water wait to dissolve and swell.2. Add citric acid and lactic acid in to water.3. Add sodium lauryl ether sulphate, Synperonic 91/8, NEP®, Easy-Wet™ 20 and dye solution (1%) respectively.4. Premix Polysorbate 80 and fragrance then add into formulation.5. Add Integra® 44.



C12-C14 / 30 EO Na sulfate (Disponil FES 77) 7.000 Cognis


Citric acid (solid) 4.000 Fisher


Lactic acid (Purac 88) 0.580 Purac

rapifloc™ 0.500 isP


Dye 0.180



total 100.000

Bathroom gel cleaner11539-26-32


12

1. Add citric acid and lactic acid into water.2. Add Synperonic 91/8, Styleze® W-20, Easy-Wet™ 20 and Antara® 430, respectively. While adding, make sure each one dissolves completely.3. Premix Polysorbate 80 & fragrance then add into formulation.4. Add Integra® 44.




C9-11 alcohol/8EO (Synperonic 91/8) 1.210 Uniqema


styleze® W-20 1.000 isP

Lactic acid 0.520 Fisher Scientific





total 100.000

Bathroom cream cleaner11678-7-33


1. Add Jaypol™ AT4 to water and mix. After mixing neutralize with NaOH.2. All ingredients are put respectively. While adding, make sure each one dissolves completely.3. Mix fragrance with Polysorbate 80.4. Add fragrance mixture to the formulation and Antara® 430.




Jaypol at4 5.000 isP

NaOH (50% aq. solution) 0.600 Local Supplier

Sodium hypochloride (14% active chlorine) 15.000 Local Supplier

Sodium xylene sulphonate (Stepanate SXS 40) 5.000 Stepan

Sodium lauryl sarcosinate (Protelan LS 9011 ) 1.500 Zschimmer& Schwarz

Lauryl dimethyl amine oxide (Amphotenside DMOX) 4.500 Zschimmer& Schwarz






total 100.000

opaque toilet bowl cleaner, chlorine based11678- 69-19

13

1. Add Rapifloc™ to water and mix until it dissolves.2. All ingredients are added respectively. While adding, make sure each one dissolves completely.3. Mix fragrance with Polysorbate 80.4. Add fragrance and dye solution (1%) mixture.



rapifloc™ 0.570 isP

sorez™ Hs-205 1.000 isP

Citric acid (solid) 4.000 Local Supplier

Lactic acid (Purac 88) 0.520 Purac




Dye 0.040




total 100.000

acidic toilet bowl cleaner featuring sorez™ Hs-20511678- 71-60


14

1. Solve PVP K-90 in water.2. Add Jaypol™ AT4.3. Neutralize with KOH.4. Add IPA, Flerogum K38, Surfadone® LP-100, lauryl dimethyl amine oxide, sodium lauryl sulphate (prepared 25% solution) and dye solution (1%), respectively.5. Premix Polysorbate 80 & fragrance then add into formulation.6. Add Integra® 44.




Potassium cocoate (Flerogum K38) 13.000 Zschimmer & Schwarz

Sodium lauryl sulphate (25% aq. solution) (Texapon K 12 P) 6.200 Cognis


Isopropanol (IPA) 0.520 Fisher Scientific



Dye 0.400

Potassium hydroxide (KOH 50% aq. solution) 0.350 Fisher

PVP K-90 0.200 isP



total 100.000

Wooden surface cleaner11363-152-43


15

1. Add Keltrol-T to water and mix for 20 minutes until dissolves.2. Add Flerogum K38, Surfadone® LP-100, lauryl dimethyl amine oxide, sodium lauryl sulphate and dye solution (1%) respectively.3. Premix Polysorbate 80 & fragrance then add into formulation.4. Add Integra® 44 and ISP MicroBeads™ 20277 with slow gentle mixing.




Lauryl dimethyl amine oxide 4.500 Zschimmer & Schwarz




Dye 0.400



Sodium lauryl sulphate (25%) (Texapon K12P) 6.200 Cognis


total 100.000

Wooden surface cleaner with isP MicroBeads™ 2027711364-62-B13




PVP/Va W-735 9.000 isP

C9-11 Alcohol/8EO (Synperonic 918) 5.000 Uniqema

Jaypol™at4 2.000 isP

Wax emulsion (Poligen WE-1) 1.000 BASF


Tributoxy ethyl phosphate (Amgard TBEP) 1.000 Stepan






total 100.000

Wooden surface polish and cleaner11539-66-25

1. Add Jaypol™ AT4 in to water.2. Then neutralize with NaOH and mix to obtain clear solution.3. Add PVP/VA W 735, Antara® 430, TBEP, Easy-Wet™ 20,

Formulation instructions Synperonic 91/8, Poligen WE-1, respectively.4. Premix Polysorbate & fragrance then add into formulation.5. Add Integra® 44.

16

1. Add the ingredients in the order listed, stirring thoroughly after each addition.2. Spray onto wipes and package in air-tight containers.



Isopropyl alcohol (Isopropanol) 9.000 Fisher

Dipropylene glycol methyl ether (Dowanol DPM) 1.000 Dow



total 100.000

glass cleaning wipes11040-92-1


1. Add Easy-Wet™ 20, sodium lauryl ether sulphate, Gantrez® S-97 BF solution (as supplied), ammonium hydroxide and dye solution (1%) into water. During addition ensure that each one dissolves completely.2. Premix Polysorbate 80 & fragrance then add into formulation.3. Add Integra® 44.



gantrez® 97 BF solution (as supplied) 0.500 isP

Isopropanol (IPA) 5.000 As required

Sodium lauryl ether sulphate 70% paste (Texapon N70) 1.000 Cognis


Ammonium hydroxide (28%) 0.300 Fisher



Perfume/fragrance 0.050 As Required

Dye 0.020

total 100.000

anti-misting glass cleaner11539-125-185


17

1. Add ingredients respectively. Make sure ingredient dissolves before adding following one.2. Add Integra® 44 to the formulation.





C 9-11 alcohol / 8EO (Synperonic 91/8) 0.500 Uniqema



total 100.000

anti-static screen cleaner featuring Ceraphyl®11678- 40-10


1. Dissolve the Gantrez® AN-169 BF in water by heating at 50°C in water. Cool down to room temperature (add evaporated water).2. Neutralize with KOH.3. Add NEP®, Flerogum K38, Surfadone® LP-100, lauryl dimethyl amine oxide, Synperonic 91/8 and dye solution (1,0%) respectively.4. Premix Polysorbate 80 & fragrance then add into formulation.5. Add Integra® 44.








Dye 0.500

Potassium hydroxide (KOH 50% aq. solution) 0.500 Fisher

gantrez® an-169 BF (powder) 0.500 isP




total 100.000

Ceramic tile cleaner11364-18-8


18

1. Add Keltrol-T to water and mix until dissolves. 2. Add Flerogum K38, Surfadone® LP-100, lauryl dimethyl amine oxide, NEP®, Synperonic 91/8 and dye solution (0,5%) respectively.3. Premix Polysorbate 80 & fragrance then add into formulation.4. Add Integra® 44 and ISP MicroBeads™ 20277 with slow gentle mixing.





C9-11 Alcohol/8EO (Synperonic 918) 2.280 Uniqema






Dye 0.008



total 100.000

Ceramic tile cleaner with isP MicroBeads™ 2027711364-72-F4




PEG 12 dimethicone (SF-1288) 5.000 Bayer




C12-C18 Alcohol/ 7EO (Dehydol LT 7) 1.000 Cognis



Phosphoric acid (80%) 0.400 Fisher



total 100.000

stainless steel cleaner11364-145-10

1. Add citric acid and phosphoric acid into the water.2. Add NEP®, sodium lauryl ether sulphate, Dehydol LT 7, Surfadone® LP-100 and SF 1288 respectively.3. Premix Polysorbate 80 & fragrance then add into formulation.4. Add Integra® 44.


19

1. Put Keltrol into water to dissolve and swell.2. Add citric acid and phosphoric acid into water. 3. Add NEP®, sodium lauryl ether sulphate, Dehydol LT 7, Surfadone® LP-100 and SF 1288, respectively.4. Premix Polysorbate 80 & fragrance then add into formulation.5. Add Integra® 44.6. Add grey glitter to the formulation and stir.



PEG 12 Dimethicone (SF-1288) 5.000 Bayer




C12-C18 alcohol / 7EO (Dehydol LT 7) 1.000 Cognis




Phosphoric acid (80%) 0.400 Fisher

Glitter 0.080Nanyang Lingbao Pearl Pigment

Co., Ltd.



total 100.000

stainless steel gel cleaner11539-118-25


1. Dissolve sodium lauryl sulphate in water.2. Add the Cocamide DEA, isopropyl alcohol and Surfadone® LP-100.3. Add Integra® 44, dye and fragrance, mix until homogenous.




Sodium lauryl sulphate (dodecyl sulphate, sodium salt 70%) 10.000 Sigma Aldrich

Cocamide DEA (Purton CFD) 2.000 Zschimmer & Schwarz




Dye 0.010

total 100.000

Carpet cleaner11040-77-1


20

1. Dissolve all solids in water.2. Then add the remaining ingredients and mix until homogenous.



Butyl carbitol 8.000 Dow


Eltesol SX 40 6.500 Huntsman


EDTA 38% (EDTA) 0.500 Fisher


Phosphoric acid (85%) pH 7 0.010


Dye 0.010

total 100.000

Machine carpet cleaner11040-81-1


1. Add ingredients respectively to water. During addition ensure that each one dissolves completely.2. Premix fragrance with Polysorbate 80.3. Add fragrance mixture to the formulation. Add Integra® 44.





C12-C18 Alcohol /7EO (Dehydol LT 7) 0.600 Cognis




total 100.000

Carpet spot cleaner11678-29-11


21

1. Mix chemicals in the following order: Water, Surfactant FC-120, Surfadone® LP-300, Wacker SRE, Dipropylene glycol methyl ether, NEP®, Dibutyl phthalate, Tributoxy ethyl phosphate and Integra® 44. Agitate for a few minutes.2. Slowly add Primal B-924 with constant stirring and continue to stir for 30 minutes.3. Slowly add Primal E-1531 with constant stirring and continue to stir for 10 minutes.4. Slowly add Poligen WE-1 with constant stirring and continue to stir for 1 hour.5. Stand for a day before use.



Primal B924 (Primal B-924) 37.310 Rohm & Haas

Wax emulsion (Poligen WE-1) 7.590 BASF

Primal E-1531 5.920 Rohm & Haas

Dipropylene glycol methyl ether (Dowanol DPM) 3.340 Dow


Tributoxy ethyl phosphate 1.130 Aldrich

Dibutyl phthalate 1.130 Aldrich


Wacker SRE (Polydimethylsiloxane) 0.100 Wacker

Surfactant FC-120 0.040 3M


total 100.000

Floor polish11040-76-2


22

1. Add Carbopol ETD to water and mix until dissolves. Neutralize with NaOH. 2. Mix to obtain clear solution. Add ammonium hydroxide.3. Add calcium carbonate and mix.4. Add Disponil LBDS 25, Dehydol LT 7, Easy-Wet™ 20 respectively.5. Premix Polysorbate 80 & fragrance then add into formulation.6. Add Integra® 44.



Calcium Carbonate (CACO3 Omyacarb 40 GZ) 50.000 Omya UK

C12-C18 EO (Dehydol LT 7) 2.000 Cognis

Lauryl alkyl benzene sulphonate (Disponil LDBS-25) 2.000 Cognis

Crosslinked polyacrylic acid polymer/ rheology modifier(Carbopol ETD 2623)

0.300 Noveon

easy- Wet™20 0.500 isP


Ammonium hydroxide (28%) 0.130 Fisher



Perfume /fragrance 0.100

total 100.000

abrasive cleaner11539-63-14


1. Add sodium hypochlorite, sodium xylene sulphonate, Protelan LS 9011, NEP® and Easy-Wet™ 20 in to water. During addition ensure each one dissolves completely.2. Premix Polysorbate 80 & fragrance then add into formulation.



Sodium hypochlorite (14% active chlorine) 15.000 Fisher

Sodium xylene sulfonate (Stapanate SXS 40) 5.000 Aldrich

Sodium lauryl sarcosinate (Protelan LS9011) 1.500 Zschimmer & Schwarz





total 100.000

Power cream all-purpose cleaner11678-16-36


23

1. Add isopropyl alcohol, and Surfadone® LP-300 to the lemon fragrance.2. Add water, followed by dye and Integra® 44.




Perfume/fragrance lemon 2.000



Dye 0.010

total 100.000

air freshener (formula #1)11040-80-1


1. Dissolve sodium lauryl ether sulphate, Surfadone® LP-300 and Empigen BB in water.2. Add NaCl and adjust pH to 6.5~7.0 with citric acid or caustic soda.3. Add Integra® 44, dye and fragrance.



Sodium lauryl ether sulphate 70% paste (Zetesol 270 N) 15.000 Zschimmer & Schwarz

Alkyl dimetyl amine betaine (Empigen BB) 2.000 Huntsman

Sodium chloride 1.500 Fisher



Citric acid 0.010


Dye 0.010

total 100.000

liquid hand soap11040-61-1


24

1. Add Aquazol® 500 in to water and mix well until it dissolves completely.2. Add sodium lauryl sulphate (prepared 25% solution), Ceraphyl® 60 and dye solution (1%).3. Premix Polysorbate 80 & fragrance and add into formulation.4. Add Integra® 44.5. Then pour constant amount of solution into a mold. Put in an oven and keep it 100°C until all the water has evaporated.6. Remove it from the mold.



Sodium lauryl sulphate (25% aq. solution) (Texapon K 12 P) 20.580 Huntsman, Rhodia

aquazol® 500 5.000 isP



Polysorbate 80 0.184 A&E Connock Ltd


Dye 0.020

total 100.000

Paper soap11539-130-9


1. Add Jaypol™ TTA to water and mix for 20 minutes at high speed at 80°C.2. After hydration, cool and add NaOH to neutralize.3. Add sodium laureth sulphate, Ceraphyl® 60 and prepared dye solution (1%) and mix.4. Premix Polysorbate 80 & Perfume 2:1 add into formulation.5. Add Integra® 44 and ISP MicroBeads™ 20279 with slow, gentle mixing.



Jaypol™ tta 3.000 isP






Dye 0.100



total 100.000

Hand gel cleaner with isP MicroBeads™ 2027911364-61-C6


25

1. Dissolve Unisan SS5053 in water.2. Add Tinopal CBS-X, soda ash and PVP K-30.3. Add sodium lauryl ether sulphate, C9–11 Alcohol /8EO (Synperonic 91/8) and Surfadone® LP-100 and stir until all ingredients are dissolved.4. Add Integra® 44, dye and fragrance.



Sodium alkyl benzene sulphonate 50% paste (Unisan SS5053) 25.600 Rhodia

Sodium lauryl ether sulphate 70% Paste (Zetosol 270 N) 15.000 Zschimmer & Schwarz

C9–11 Alcohol /8EO (Synperonic 91/8) 3.000 Uniqema

Soda ash 1.000 Fisher


PVP K-30 0.500 isP


CI fluorescent brightener 35 (Tinopal CBS-X) 0.050 Ciba Geigy

Perfume/fragrance qs

Dye qs

total 100.000

liquid laundry detergent (clear and non-builder)11040-64-1


26

1. Dissolve the Genapol LA 050, Disponil LDBS25 and sodium lauryl ether sulphate in the water.2. Add other ingredients respectively.3. Prepare 0.5% solution with the dye and add to the mixture.4. Dissolve the fragrance in Polysorbate 80 and add mix to the mixture.5. Add Integra® 44.


Formulation

Ingredients% W/W

SupplierA B C

Aqua/water (D.I.Water) 92.630 92.950 92.950

Adogen® 442 ditallow dimethyl ammonium chloride 6.70 6.70 / Degussa

surfadone® lP-100 0.50 / / isP

integra® 44 0.15 0.15 0.15 isP

Perfume/fragrance 0.010 0.010 0.010

Dye 0.010 0.010 0.010

Arquad® 2HT-75 ditallow dimethyl ammonium chloride / / 6.70 Akzo Nobel

total 100.00 100.00 100.00 100.00

Fabric softener, 3 formulations a, B and C11040-69

1. Warm Adogen® or Arquad® to 55°C, then add into water and stir well at 55°C.





Lauryl alkyl benzene sulphonate (Disponil LDBS-25) 6.040 Cognis

Trisodium citrate dihydrate 6.040 Fisher

Propylene glycol 3.620 Aldrich

Fatty alcohol polyglycol ether laureth 5 (Genapol LA-050) 3.620 Clariant

Alkyl polyglycol ether with 11 EO (Emulsogen LCN 118) 3.620 Clairant




Chromabond™ s-403 e 0.600 isP

sorez™100 0.600 isP


Dye 0.040



total 100.000

Color safe liquid laundry detergent11364-31-9

2. Cool to 35°C.3. Add Surfadone® LP-100, Integra® 44, fragrance and dye.

27

1. Dissolve disodium EDTA in water. 2. After dissolving EDTA add Tergitol 15-S-7, citric acid, Sorez 100, Acusol 820, NEP and Easy-Wet™20 respectively.3. Neutralize with NaOH.4. Dissolve the fragrance in Polysorbate 80 and add mix in to the mixture.5. Add Integra® 44.


1. Dissolve Dehydol LT in water at 30°C.2. Add Dehydol LS-54 and sodium lauryl ether sulphate (30%).3. Prepare 0.5% solution with the dye and add to the mixture.4. Add Sorez ™ 100 (transparent) and then Integra® 44.



Dehydol LT (100% Fatty Alcohol 7 Moles EO) 4.500 Cognis

Dehypon LS-54 (100% Fatty Alcohol EO and 4 moles P07) 1.500 Cognis

Sodium lauryl ether sulphate (30%) 1.000

sorez™100 1.000 isP


total 100.000

Pre-treatment stain remover featuring sorez™ 100isPM – 18.06.2010-1





Secondary ethoxylated alcohol (Tergitol 15-S-7) 3.050 Dow


Citric acid (solid) 2.000 Aldrich



sorez™ 100 0.500 isP


Titriplex III (Disodium EDTA) 0.200 S. Black



total 100.000

laundry pre-spotter11363-25-39

28

1. Heat the water to 60°C.2. Add the Aquazol® 500 with high speed stirring.3. Stir for 1 - 2.5 hours until all the Aquazol® 500 has dissolved.4. Leave to let the air disperse.5. Cast a film of the solution onto a non stick surface using a Meyer bar to give a dry film of 100 -150 microns.6. Dry for 5 minutes at 130°C.




total 100.000

Water soluble film11178-142-1


1. Heat the water and the propylene glycol to 60°C.2. Add the Aquazol® 500 with high speed stirring.3. Stir for 1 - 2.5 hours until all the Aquazol® 500 has dissolved.4. Add the Styleze® CC-10 and stir for 30 minutes.




styleze® CC-10 19.610 isP


total 100.000

Water soluble film with delayed solubility11178-142-2


1. Mix the deionized water and ethanol together.2. Under high sheer, add in the Aquazol® 200 and mix for 1 hour.3. Leave to stand overnight to fully dissolve.



Alcohol denat. (Ethanol Absolute) 45.000 Fisher


total 100.000

Protective spray11126-67-1


5. Leave to let the air disperse.6. Cast a film of the solution onto a non stick surface using a Meyer bar to give a dry film of 100 - 150 microns.7. Dry for 5 minutes at 130°C.

29

1. Heat the water and the propylene glycol to 60°C.2. Add the Aquazol® 500 with high speed stirring.3. Stir for 1 - 2.5 hours until all the Aquazol® 500 has dissolved.4. Leave to let the air disperse.5. Cast a film of the solution onto a non stick surface using a Meyer bar to give a dry film of 100 - 150 microns.6. Dry for 5 minutes at 130°C.





total 100.000

Water soluble flexible film11178-142-3


1. Add sodium hydroxide to water.2. Add alkyl benzene sulphonic acid, stir until neutralized.3. Add sodium lauryl ether sulphate, coco-diethanol amide and Surfadone® LP-300, and stir until all ingredients are dissolved.4. Add Integra® 44, dye, lemon and citric acid.5. Add sodium chloride.



Alkyl benzene sulphonic acid (LABSA) 9.800 Huntsman, Rhodia

Sodium lauryl ether sulphate 70% Paste 5.800 Huntsman, Rhodia

Sodium hydroxide 50% 2.550 Fisher

surfadone® lP- 300 1.000 isP

Cocamide DEA (Coco/Diethanol amide) 1.000 Aldrich



Citric acid (10% aqueous solution) 1.000 Fisher


Dye 0.010

total 100.000

Washing up liquid featuring surfadone® lP-300 (formula #1)11040-96-1


30

1. Charge the water into the vessel.2. Add the sodium lauryl ether sulphate 70% paste, stir with mechanical stirrer until dissolved.3. Add coconut diethanolamine and Surfadone® LP-300, stir until dissolved.4. Add Integra® 44, dye and fragrance, stir until homogeneous.5. Add Sodium chloride.6. Adjust pH to 6.8~7.0 with citric acid.



Sodium lauryl ether sulphate 70% paste 15.000 Huntsman, Rhodia



Coconut diethanolamine 1.000 Aldrich




Dye 0.010

total 100.000

Washing up liquid featuring surfadone® lP-300 (formula #2)11040-97-1




Sodium lauryl ether sulphate 70% paste (Zetosol 270 N0) 16.900 Zschimmer & Schwarz

Empigen BB (N, N-Dimethyl-N-dodecylglycerine Betaine) 6.500 Huntsman

Empigen OB (lauryl dimethyl amine oxide) (Empigen OB) 3.500 Huntsman



Empilan KB9 (lauryl alcohol ethoxylate (9EO) 1.000 Huntsman




Dye 0.010

total 100.000

ecological washing up liquid11040-98-1

1. Charge water to the vessel.2. Add sodium lauryl ether sulphate 70% paste and stir until dissolved.3. Add Empigen BB, Empilan KB9 and Empigen OB, stir until dissolved.

Formulation instructions4. Add Integra® 44, dye and lemon fragrance. 5. Add NaCl.6. Adjust pH to 6.8~7.0 with citric acid or NaOH

31

1. Add calcium chloride to water then add Keltrol-T and mix at very high speed for 20 minutes until dissolved.2. Add sodium lauryl ether sulphate, Cocoamide DEA, Surfadone® LP-300, NaCl and dye solution (1%) and mix well.3. Dissolve Fragrance in Polysorbate 80 and add mix into the mixture.4. Add Integra® 44.5. Add the ISP MicroBeads™ with slow gentle mixing.



Sodium lauryl ether sulphate (Texapon N70) 15.000 Cognis



Cocamide diethanol amide (Purton CFD) 1.000 Zschimmer & Schwarz


Dye 0.400



Calcium chloride (CaCl2 solid) 0.120 Fisher



total 100.000

Washing up liquid with isP MicroBeads™ 20278 (formula #1)11364-71-d13


32

1. Add the Keltrol-T to the water at very high speed and mix 20 minutes until dissolves.2. Add the Genapol LA 050, sodium lauryl ether sulphate, Disponil LDBS 25, Easy-Wet™ 20, CaCl2 and NaCl into the mixture.3. Prepare a 0.5% solution with the dye and add in to the mixture.4. Dissolve the fragrance in the polysorbate 80 and add mix in to the mixture.5. Add Integra® 44.6. Add the ISP MicroBeads™ with slow, gentle mixing.




Lauryl alkyl benzene sulphonate (Disponil LDBS-25) 5.000 Huntsman



Fatty alcohol polyglycol ether Laureth 5 (Genapol LA-050) 1.000 Clariant



Dye 0.400


Calcium chloride (CaCl2 solid) 0.100 Fisher



total 100.000

liquid laundry detergent with isP MicroBeads™ 20278 (formula #2)11364-72-e4


33

1. Add Jaypol™ AT4 in to water and add NaOH to neutralize Jaypol™ AT4. 2. Mix to obtain clear solution.3. Add Hostapur SAS, sodium lauryl ether sulphate, Genapol LA 050, Surfadone® LP-100, lauryl dimethyl amine oxide and NaCl.4. Dissolve the fragrance in the Polysorbate 80 and add to the mixture.5. Add Integra® 44.




Sodium lauryl ether sulphate (Texapon N70) 13.500 Cognis

Sodium C14-17 alkyl sec sulfonate (Hostapur SAS 60) 6.000 Clariant

Fatty alcohol polyglycol ether laureth 5 (Genapol LA-050) 3.000 Clariant



Lauryl dimethyl amine oxide (30%) (Amphotenside DMOX) 1.000 Zschimmer &Schwarz






total 100.000

Washing up liquid featuring surfadone® lP-10011364-79-10

34

1. Add Jaypol™ AT4, Laponite RD into water and add NaOH to neutralize Jaypol™ AT4.2. Mix to obtain clear solution.3. Add Hostapur SAS, sodium lauryl ether sulphate, Genapol LA 050, Surfadone® LP-100, Amphotenside DMOX and NaCl.4. Dissolve the fragrance in Polysorbate 80 and add to the mixture.5. Add Integra® 44.6. Add the ISP MicroCapsules™ 4449 with gentle stirring.




Sodium C14-17 alkyl sec sulfonate (Hostapur SAS 60) 6.000 Clariant

Fatty alcohol polyglycol ether Laureth 5 (Genapol LA-050) 3.000 Clariant



Lauryl dimethyl amine oxide (Amphotenside DMOX) 1.000 Aldrich

Synthetic clay (Laponite RD) 0.700 Rockwood







total 100.000

Washing up liquid with isP MicroCapsules™ 444911539-72-22


35

1. Dissolve the Gantrez® S-97 BF into the water with mechanical mixing.2. Neutralize Gantrez® S-97 BF with TEA.3. Add PVP K-90 while mixing. Wait until it completely dissolves.4. Add sodium lauryl ether sulphate, Surfadone® LP-300, and citric acid one by one. Allow 3 minutes for each to be mixed. Add dye solution (1%) in to the mixture.5. Premix Polysorbate 80 & fragrance then add into the formulation.6. Add Integra® 44.




Sodium lauryl ether sulphate 70% paste (Texapon N70) 7.500 Cognis


PVP K-90 1.500 isP


Triethanolamine (TEA) 0.600 Aldrich


Dye 0.100




total 100.000

Car shampoo11678-10-26

1. Prepare base powder with ingredients listed above in stage A.2. Mix base powder and Disintex™ 200 disintegrating agent in a V-mixer for 30 minutes.3. Press mixed powder at 11 tons pressure using dry compression to make 20 g tablets. (lab tabs were pressed using a Carver Automated Press at 387 psi and 1 sec. Dwell time) 4. Individual tabs were tested by submerging in 3 liters of DI water agitated at 700 rpm until complete dissolution enabled tab granules to pass through a metal gauze cage.


A. Sodium tripolyphosphate 39.200 Huntsman, Rhodia

Sodium carbonate 32.144 Aldrich

Sodium sulphate 18.914 Aldrich

Sodium metasilicate (Pentahydrate) 6.272 Huntsman, Rhodia

Sodium stearate (OP-100) 0.784 Huntsman, Rhodia

C13-15 fatty alcohol 7EO (C13-15) 0.686 Huntsman, Rhodia

B. disintex™ 200 2.000 isP

total 100.000

dishwasher detergent tablets11040-100-1


36



Paraffinum liquidum (Paraffin Light) 35.000 Merck/S. Black

Petroleum jelly (Vaseline) 15.000 Fisher

antaron® V-220 3.000 isP

Carnuba wax 82.5 - 86.0°C Melting Point 3.000 Merck/S. Black

Polyglyceryl-3 Oleate 2.300 A & E Connock Ltd




total 100.000

tire wax11678-9-12

1. Carnauba wax, liquid paraffin, vaseline and Antaron® V-220 are heated to 80°C while mixing.2. Polyglyceryl 3 oleate added to the mix.3. Add water and stir.4. Premix Polysorbate 80 & fragrance then add into formulation.5. Add Integra® 44.




Sodium lauryl sulphate (20%) (Texapon K 12 P) 2.750 Cognis

Cerasynt® 945 2.500 isP


Paraffinum liquidum (Paraffin Light) 1.000 Merck/S.Black






Carnuaba wax 82.5 - 86.0°C melting point 3.000 S Black

total 100.000

Car wash and wax11678-10-17

1. Add sodium lauryl sulphate into water while mixing.2. Add lauryl dimethyl amine oxide and Surfadone® LP-300 and heat to 80°C while stirring.3. Carnauba wax, liquid paraffin and Cerasynt® 945 are heated to 80°C while mixing.4. These are mixed together at 80°C then mixed 3 minutes.5. Cool down formulation to room temperature while mixing.6. Premix Polysorbate & fragrance then add into formulation.7. Add Integra® 44 and citric acid to the formulation. Mix well.


37

1. Add Gantrez® S-97 BF in to D.I Water.2. Neutralize Gantrez® S-97 BF with NaOH 10%.3. Add PVP K-30 while mixing. Wait completely dissolves.4. Put sodium carbonate, IPA, NEP, sodium lauryl sulphate, surfadone® LP-100 and citric acid one by one, waiting each time for 3 minutes while mixing.5. Premix Polysorbate 80 & fragrance then add into formulation.6. Add Integra® 44.


1. Add acid to NEP® and water with continuous stirring.2. A slight exothermic reaction will occur.3. Mix all ingredients until you have a homogenous cleaner solution.



Phosphoric acid (85%) 12.000 Aldrich


total 100.000

Metal cleaner11040-74-1




Isopropanol (IPA) 3.000 Fisher


C12-C14 / 30 EO Na Sulfate (Disponil FES 77) 2.000 Cognis



PVP K-30 1.000 isP



Sodium carbonate (NaCO3) 0.300 Fisher




total 100.000

Wheel spray cleaner11539-152-7

38

Committed to your formulationISP global R&D and technical serviceAt ISP, we’re continually working on developing ideas and technology that will help your cleaning

products stand out in the marketplace. Our global R&D network develops new chemistries for use

in innovative cleaning products and develops applications technology targeted to meeting the

changing needs of the marketplace.

To support your product development efforts, ISP maintains a regional technical service group with

locations in North America, Europe, the Middle East and Asia. Our experienced team can use their

expertise with ISP chemistries to help you achieve your formulation goals.

For more information, contact us at: [email protected]

Customer serviceToll free: 1 (800) 622-4423 Fax: +1 973 [email protected]

sample CenterToll free: 1 (800) [email protected]

Cologne, germany Emil-Hoffmann-Strasse 1-aD-50996 Koln-Rodenkirchen Germany Telephone: +49 (2236) 9649-0

Poole, uK Unit 9, Stepnell Reach, Poole, Dorset, BH16 5BW, UK Telephone: +44 (0) 1202 627353

World HeadquartersINTERNATIONAL SPECIALTY PRODUCTS1361 Alps Road, Wayne, NJ 07470, USATel: +1 973 628-4000Fax: +1 973 628-3311ispcorp.com ∙ [email protected]

north american Headquarters

european HeadquartersCustomer serviceTel: +49 (2236) 9649-260Fax: +49 (2236) 9649-295

™ Trademark registration applied for ® Registered trademark of the ISP group © International Specialty Products. 2010 Designed & Printed in USA.

The information contained in this document and the various products described are intended for use only by persons having technical skill and at their own discretion and risk after they have performed necessary technical investigations, tests and evaluations of the products and their uses. While the information herein is believed to be reliable, we do not guarantee its accuracy and a purchaser must make its own determination of a product’s suitability for purchaser’s use, for the protection of the environment, and for the health and safety of its employees and the purchasers of its products. Neither ISP nor its affiliates shall be responsible for the use of this information, or of any product, method or apparatus described in this document. Nothing herein waives any of ISP’s or its affiliates’ conditions of sale, and WE MAKE NO WARRANTY, EXPRESS OR IMPLIED, OF MERCHANTABILITY OR FITNESS OF ANY PRODUCT FOR A PARTICULAR USEOR PURPOSE. We also make no warranty against infringement of any patents by reason of purchaser’s use of any information, product, method or apparatus described in this document.

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