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OptiMax™

Your Synthesis Workstation

OptiMax™ 1001 Standard Sets

1000 mL Glass Reactor Sets



Accessories & Spares

Dosing Unit SP-50

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2

Glossary of Terms Used

Glossary of Terms Used

ReactIR = Mid-IR spectroscopyFBRM® = Focused Beam Reflectance Measurement HC-22 = Hastelloy® C22PTFE GF25 = Teflon® (Polytetrafluoroethylene), 25 % glassPEEK = PolyetheretherketoneETFE = Ethylene tetrafluoroethyleneFFKM = Kalrez® (Perfluoroelastomer)FPM = Viton® (Fluorine rubber)

PA = PolyamidePVC = PolyvinylchlorideSAN = Styrene acrylonitrilePE = PolyethylenePP = Polypropylene PU = Polyurethane POM = Polyoxymethylene PBT = Polybutylene terephthalate VQM = Silicone rubber PVDF = Kynar® (Polyvinylidene Fluoride)

3

Contents

General Introduction 2 – 4

OptiMax™ Starter Kit 5

OptiMax™ Thermostat System 6 – 11

OptiMax™ 1000 mL Two-Piece Glass Reactor 12 – 15



OptiMax™ 1000 mL Single-Piece Glass Reactor 24 – 27



OptiMax™ Spare Parts, Adapters, and Stirrers 35 – 40

OptiMax™ Accessories and Probes 41 – 45

Compatibility List 46 – 47

4

General Introduction

No oil baths, ice baths, and cryostats required Precise temperature control from −40 to 180 °C Small and mobile Wide range of different reactors and stirrers Simple and intuitive touch screen operation No learning curve Programmable Secure unattended operation Data logging making experiments traceable and reproducible Data export into iControl and MS-Excel®

IntroductionOptiMax™ is a synthesis work-station that is beyond traditional synthesis equipment. It is geared towards today’s workflows in chemical and process development labs. It simplifies organic synthesis by eliminating cumbersome steps and ensures precise and accurate execution of chemical synthesis.It heats and cools efficiently with-out the need for cryostats, oil or ice baths, offers a large variety of different reactors and stirrers, and is operated by a simple touch screen. Even though its use is simple, experiments are carried out with highest precision, reproducible and traceable increasing produc-tivity in chemical and process development significantly.

A Remarkable ThermostatOptiMax™ is a single self-contained box with a built-in solid state thermostat covering the entire tempera-ture range without an additional cryostat. The powerful Peltier-based thermostat provides the necessary performance to control the temperature of the reaction mixture accurately and reproduc-ibly. It grants outstanding heating and cooling rates in the entire temperature range from −40 to 180 °C. Even strong chemical reactions are kept at constant temperature, ensuring that the experiment is carried out safely and the reaction kinetics remains unaffected.

OperationOptiMax™ is operated completely effortless using a smart and intui-tive touch screen. Changing experi-ment parameters, such as temper-ature or stirring speed is a matter of seconds and doesn’t require any training. The experiment is either carried out step-by-step or programmed and completely un-attended. The safety monitoring system ensures safe execution of the individual tasks without perma-nent supervision.All data and relevant information are displayed and recorded as the experiment proceeds. For further evaluation the recorded data can be transferred to either iControl™, the sophisticated PC software or MS-Excel®.

OptiMax™ – Your Synthesis WorkstationEditorial

5

OptiMax™ Starter Kit

OptiMax™ Starter Kit

51 162 830 OptiMax™ 1001 starter kit consists of the following items

51 162 701 OptiMax™ thermostat system

51 162 831 OptiMax™ 1000 mL two-piece glass reactor set

51 162 720 PTFE adapter for Tr, pH, and turbidity probe

51 162 839 Tr probe, HC-22

51 162 886 Accessories holder set

Details regarding these items

can be found on the following pages.

The OptiMax™ starter kit is a ready-to-go setup that simplifies the part evaluation and ordering process. The starter kit combines all the key items for an easy-to-use 1000 mL two-piece reactor setup in just one part number.

The OptiMax™ starter kit includes the following key components: OptiMax™ thermostat system incl. touchscreen Stirrer motor and adapter Tr temperature probe incl. adapter 1000 mL two-piece glass reactor Cover and reactor holders Pitched blade stirrer, downward, HC-22 Bar type baffle, HC-22 incl. adapter Stoppers and “Keck” clamps for all open ports Accessories holder

The OptiMax™ starter kit can be combined individually with any additional items in this catalog.

6

OptiMax™ Thermostat System

OptiMax™ 1001 reactor blockavailable only in a thermostat system set

Material Powder-coated stainless steel with FEP/PFA coated cover plate

Power supply voltages

100 – 240 VAC

Back-/frontlight 12 LEDs

Heating/cooling Solid state thermostat

Temperature mode Jacket control, reaction mixture control, distillation (constant or ramp)

Temperature range −40 to 180 °C, jacket temperature (Tj)

Size 388 x 414 x 539 mm (w, d, h), 388 x 414 x 780 mm (w, d, h with overhead stirrer)

Weight 35 kg, including touchscreen

Quantity 1


51 162 701 OptiMax™ thermostat system set consisting of

Order number Product description Quantity

OptiMax™ 1001 reactor block 1

51 161 873 7” TFT OptiMax™ touchscreen 1

51 191 728 Pen for OptiMax™ touchscreen 1

51 162 690 Overhead stirrer drive complete 1

51 161 099 Lab bar, 600 x 14 mm 4

51 162 860 Reactor block plug for bottom drain valve opening 1

51 161 187 PVC tube for coolant, length 2.5 m 2

51 191 125 PVC tube, soft, for reflux condenser, length 5 m 1

51 161 186 PVC tube for gas inlet, length 2 m 1

51 191 915 Flow indicator for coolant 1

51 191 916 Reducing connector for purge gas tubing 1

51 190 324 Quick connect coupling for purge gas inlet 5

51 192 126 Hose clamp for PVC tube 4

USB memory stick for data export 1

51 161 782 Bubble counter 1

51 161 603 Magnetic bubble counter holder 1

51 191 945 Purge gas regulation valve 1

11 132 570 OptiMax™ touchscreen protective cover 1

51 191 235 Identification clips for adhesive labels to label individual sensors, reactors etc. 1

51 712 001 OptiMax™ Operating Instructions 1

OptiMax™ Installation Check Report 1

OptiMax™ Product Catalog/Packing List 1

Factory Test Report 1

CE Certificate 1

7


51 161 873 7” TFT OptiMax™ touchscreen including protective cover

Material PA, aluminum

Size 195 x 135 x 60 mm (w, d, h)

Quantity 1

51 191 728 Pen for touch screen operation

Size Length 140 mm

Quantity 1

51 162 690 Overhead stirrer drive complete

Material Aluminium anodized, PTFE

Speed 30 to 1200 rpm

Quantity 1

51 161 099 Lab bar 600 x 14 mm

Material Stainless steel, 1.4435

Size Ø 14 mm x 600 mm

Quantity 1

USB 2.0 memory stick for data export

Memory size 2 GB

Size 55 x 15 x 6 mm

Quantity 1

available on special request only

51 161 187 PVC tube for coolant

Material PVC

Size Ø 8/12 mm, length 2.5 m

Quantity 1

51 191 125 PVC tube, soft, for reflux condenser

Material PVC

Size Ø 8/12 mm, length 5 m

Quantity 1

51 161 186 PVC tube for purge gas inlet

Material PVC

Size Ø 4/6 mm, length 2 m

Quantity 1

51 191 915 Flow indicator for coolant

Material SAN

Temperature Max. 30 °C

Size For tubes with inner Ø 6 to 9 mm

Quantity 1


51 191 916 Reducing connector for purge gas tubing

Material PP


Size For tubes with inner Ø 7 – 11 resp. 4 – 7 mm

Quantity 1

8


51 161 782 Bubble counter

Material Borosilicate glass

Size Ø 30 x 150 mm

Quantity 1

51 161 603 Magnetic bubble counter holder

Material PET

Size 30 x 33 x 68 mm

Quantity 1

51 191 945 Purge gas regulation valve

Material PA 6.6, NBR

Size Tube Ø 6 mm

Quantity 1

51 162 860 Reactor block plug for bottom drain valve opening

Material PTFE GF25

Size Ø 14 – 9.5 mm

Quantity 1

O-ring needed 51 192 209

51 192 209 O-ring for 51 162 860 plug

Material FPM

Size Ø 50.39 x 3.53 mm

Quantity 1

51 190 324 Quick connect coupling for purge gas in-/outlet

Material Stainless steel

Size For tubes with inner Ø 4 mm

Quantity 1

9

51 192 126 Hose clamp for PVC tube


Size Ø 14 – 9.5 mm

Quantity 1



51 191 235 Identification clips for adhesive labelsto label individual sensors, reactors etc.

Size For cables with Ø 2 – 4.5 mm

Quantity 1

11 132 570 OptiMax™ touchscreen protective cover

Material Barex® resin

Quantity 1

10


51 161 883 7” TFT OptiMax™ touchscreen including protective cover

Material PA, aluminum

Size 195 x 135 x 60 mm (w, d, h)

Quantity 1

51 162 763 Security ring to hold stirrer shaft

Material PEEK

Speed Inner Ø 10 mm

Quantity 1

51 162 643 Stirrer adapter, ST24

Material PTFE (Valflon 117)

Size Inner Ø 10 mm

Quantity 1

51 192 163 Bearing sleeve for overhead stirrer

Material PEEK/PTFE

Size Inner Ø 10 mm

Quantity 1

51 162 841 Overhead stirrer motor standard

Material Aluminium anodized, PTFE

Speed 30 to 1200 rpm ± 5 rpm

Quantity 1

51 162 820 Loosening nut for 51 162 643 stirrer adapter

Material PTFE (Valflon 117)

Size Inner Ø M26

Quantity 1

51 192 164 Compression spring for overhead stirrer

Material PEEK

Size Inner Ø 10 mm

Quantity 1

OptiMax™ Thermostat SystemSpare Parts

11

51 190 319 Plastic hose, straightwith silicone rubber seal, for GL14 screw cap

Material PP, VQM

Size For tube inner Ø 6 – 9 mm

Quantity 1

51 162 886 Accessories holder setto be attached to the lab bar of yourOptiMax™ system – for stirrer motor (ST24),for Ø 12 mm probes (ST19), for Ø 6 mm probes (ST14)

Material Stainless steel, PTFE GF25

Quantity in a set 2 x holders1 x adapter with ST14 aperture4 x adapters with ST19 aperture1 x adapter with ST24 aperture

51 190 317 Screw cap GL14, with aperture

Material PBT

Size Aperture Ø 9.5 mm

Quantity 1

51 192 208 Glass adapter ST19/26-GL14

Material Glass

Size Height 50 mm

Quantity 1

Accessories for OptiMax™ System

51 162 885 Touchscreen cable extensionto be ordered with base unit or assembled by a field service engineer

Size Length 3 m

Quantity 1

51 161 778 Purge gas set for overhead stirreravailable only as a set

Material Stainless steel, PVC, PP

Temperature PP max 30 °C

Quantity in a set 1 x bulkhead connector 2 x quick connect couplings (for tubes inner Ø 4 mm) 1 x reducing connector (for tubes inner Ø 7-11 mm and 4-7 mm)1 x PVC tube (inner Ø 4 mm)

51 103 947 Sealing ring with vulcanized-on PTFE washers for GL14 cap

Material Silicone rubber VQM, PTFE-coated

Size Ø 12 mm, aperture 6 mm

Quantity 1

Accessories for OptiMax™ System

12

OptiMax™ 1000 mL Two-Piece Glass Reactor Set

OptiMax™ 1000 mL two-piece glass reactor set consisting of


51 162 634 Glass reactor, 1000 mL 1

51 162 782 Reactor holder for 1000 mL reactor 1

51 162 671 Glass cover, for 1000/500 mL reactor, 7 ports 1

51 162 780 Cover holder for 1000/500 mL reactor cover 1

51 162 673 Reactor clamp for 1000/500 mL reactor 1

51 192 205 O-ring for 1000/500 mL reactor 1

51 162 722 Stirrer shaft for 1000/500 mL reactor, HC-22 1

103 504 Pitched stirrer blade, HC-22, downward 1

51 162 637 Bar type baffle for 1000 mL reactor, HC-22 1

51 104 154 PTFE adapter for baffle 1

51 162 685 Drain union, bended 1

51 192 169 Pinch clamp S19 1

71 518 Glass stopper ST29/32 2


51 190 878 Glass stopper ST14/23 1

51 192 168 ”Keck” clamp ST29 2

51 192 167 ”Keck” clamp ST24 1

51 191 429 ”Keck” clamp ST19 3

51 191 505 ”Keck” clamp ST14 1

51 162 831 1000 mL two-piece glass reactor set

The different OptiMax™ reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free.

The 1000 mL two-piece glass reactor is equipped with a bottom drain valve and has a working volume of 1000 mL, a nominal volume of 1310 mL and a starting volume of 200 mL.

OptiMax™ 1000 mL Glass Reactor SetTwo-Piece

13


51 162 634 1000 mL glass reactor

Material Borosilicate glass, PTFE, PEEK, silicone

Working volume Max. 1000 mL

Nominal volume 1310 mL

Temperature −40 to 180 °C

Size Inner Ø 101 mm, height 172 mm, wall 3 mm

Quantity 1

51 162 782 Reactor holder for 1000 mL reactor

Material Stainless steel 1.4404, PE

Quantity 1

51 162 673 Reactor clamp for 1000/500 mL reactor

Material Stainless steel 1.4404, Glastherm HT 220 (Thermalite 220M)

Quantity 1

51 162 671 Glass cover for 1000/500 mL reactor, 7 ports1 x ST14/23, 3 x ST19/26, 2 x ST29/32,center ST24/29



Size Inner Ø 98 mm

Quantity 1

51 162 780 Cover holder for 1000/500 mL reactor cover


Size Inner Ø 121 x 22 mm

Quantity 1

51 192 205 O-ring for 1000/500 mL reactor

Material Elastomer Vollkern Silicone VQM, Teflon FEP-coated


Size Ø 107.5 x 3.53 mm, AS No. 244

Quantity 1

ST19/26Bar type baffle, FBRM S/G400 long, pH probe Ø 12 mm, turbidity probe Ø 12 mm


ST24/29Overhead stirrer

ST29/32FBRM D/G600,PVM V819, RIR 5/8“


ST14/23Tr probe, RIR 3/8”, turbidity probe Ø 6 mm


14

51 192 167 ”Keck” clamp ST24

Material POM

Quantity 1

51 191 505 ”Keck” clamp ST14

Material POM

Quantity 1


51 192 168 ”Keck” clamp ST29

Material POM

Quantity 1

51 191 429 ”Keck” clamp ST19

Material POM

Quantity 1

51 192 169 Pinch clamp S19drain union clamp


Quantity 1

71 517 Glass stopper ST19/26

Material Glass

Quantity 1

51 162 685 Drain union, bended


Size Inner Ø 9 mm, spherical joint S19

Quantity 1


Material Glass

Quantity 1

51 190 878 Glass stopper ST14/23

Material Glass

Quantity 1

15


103 504 Pitched stirrer blade for 1000/500 mL reactordownward, 4 impellers, 45°, M8 thread

Material HC-22

Size Outer Ø 45 mm

Quantity 1

51 162 637 Bar type baffle for 1000 mL reactor

Material HC-22

Size Ø 10 mm, width 15 mm, length 249 mm

Quantity 1

51 162 722 Stirrer shaft for 1000/500 mL reactor M8 thread

Material HC-22

Size Ø 10 mm, length 400 mm

Quantity 1

51 104 154 PTFE adapter for baffle, eccentricfor baffle, including 103 047 sealing ring

Material PTFE

Size Inner Ø 10 mm, ST19

Quantity 1

16





51 162 783 Reactor holder for 500 mL reactor 1

51 162 671 Glass cover, for 1000/500 mL reactor, 7 ports 1

51 162 780 Cover holder for 1000/500 mL reactor cover 1

51 162 670 Receptacle for 500 mL reactor 1

51 162 673 Reactor clamp for 1000/500 mL reactor 1

51 192 205 O-ring for 1000/500 mL reactor 1

51 162 722 Stirrer shaft for 1000/500 mL reactor, HC-22 1

103 504 Pitched stirrer blade, HC-22, downward 1



51 162 685 Drain union, bended 1

51 192 169 Pinch clamp S19 1




51 192 168 ”Keck” clamp ST29 2

51 192 167 ”Keck” clamp ST24 1

51 191 429 ”Keck” clamp ST19 3

51 191 505 ”Keck” clamp ST14 1

51 162 832500 mL two-piece glass reactor set


The 500 mL two-piece glass reactor is equipped with a bottom drain valve and has a working volume of 500 mL, a nominal volume of 830 mL and a starting volume of 70 mL.


17


51 162 632 500 mL glass reactor

Material Borosilicate glass, PTFE, PEEK, silicone




Size Inner Ø 77 mm, height 172 mm, wall 2.5 mm

Quantity 1

51 162 783 Reactor holder for 500 mL reactor


Quantity 1

51 162 670 Receptacle for 500 mL reactorThermostat sleeve

Material Aluminium anodized

Quantity 1

51 162 671 Glass cover for 1000/500 mL reactor, 7 ports1 x ST14/23, 3 x ST19/26, 2 x ST29/32,center ST24/29



Size Inner Ø 98 mm

Quantity 1

51 162 780 Cover holder for 1000/500 mL reactor cover



Quantity 1








18


51 192 205 O-ring for 1000/500 mL reactor



Size Ø 107.5 x 3.53 mm, AS No. 244

Quantity 1

51 192 169 Pinch clamp S19drain union clamp


Quantity 1


Material Glass

Quantity 1

51 162 673 Reactor clamp for 1000/500 mL reactor


Quantity 1

51 162 685 Drain union, bended


Size Inner Ø 9 mm, spherical joint S19

Quantity 1


Material Glass

Quantity 1


Material Glass

Quantity 1

19

51 192 167 ”Keck” clamp ST24

Material POM

Quantity 1

51 191 505 ”Keck” clamp ST14

Material POM

Quantity 1


Material HC-22

Size Outer Ø 45 mm

Quantity 1


Material HC-22


Quantity 1


51 192 168 ”Keck” clamp ST29

Material POM

Quantity 1

51 191 429 ”Keck” clamp ST19

Material POM

Quantity 1


Material HC-22


Quantity 1


Material PTFE


Quantity 1

20





51 162 758 Reactor stand for 250 mL reactor 1

51 162 699 Glass cover for 250 mL reactor, 7 ports 1

51 162 781 Cover holder for 250 mL reactor cover 1


51 162 703 Reactor clamp for 250 mL reactor 1

51 192 170 O-ring for 250 mL reactor 1

51 162 417 Stirrer shaft for 250 mL reactor, HC-22 1

51 162 418 Pitched stirrer blade, HC-22, downward 1



51 192 167 ”Keck” clamp ST24 1

51 191 429 ”Keck” clamp ST19 4

51 191 505 ”Keck” clamp ST14 2

51 162 833250 mL two-piece glass reactor set


The 250 mL two-piece glass reactor has no bottom drain valve and has a working volume of 250 mL, a nominal volume of 370 mL and a starting volume of 50 mL.


21









51 162 635 Glass reactor, 250 mL






Quantity 1

51 162 758 Reactor stand for 250 mL reactor

Material PE

Size Ø 108 x 105 mm

Quantity 1



Quantity 1

51 162 699 Glass cover for 250 mL reactor, 7 ports2 x ST14/23, 4 x ST19/26, center ST24/29



Size Inner Ø 68 mm

Quantity 1

51 162 781 Cover holder for 250 mL reactor cover



Quantity 1

22

51 192 170 O-ring for 250 mL reactor



Size Ø 69.44 x 3.53 mm

Quantity 1

51 162 418 Pitched stirrer blade for 250 mL reactordownward, 4 impellers, 45°, M3 thread

Material HC-22

Size Outer Ø 38 mm

Quantity 1


Material Glass

Quantity 1

51 162 703 Reactor clamp for 250 mL reactor


Quantity 1

51 162 417 Stirrer shaft for 250 mL reactor M3 thread

Material HC-22

Size Ø 10/8 mm, length 400 mm

Quantity 1


Material Glass

Quantity 1


23


51 191 429 ”Keck” clamp ST19

Material POM

Quantity 1

51 192 167 ”Keck” clamp ST24

Material POM

Quantity 1

51 191 505 ”Keck” clamp ST14

Material POM

Quantity 1

24

OptiMax™ 1000 mL Single-Piece Glass Reactor Set

OptiMax™ 1000 mL single-piece glass reactor set consisting of


51 162 732 Single-piece glass reactor, 1000 mL 1


51 162 681 Glass stirrer shaft for 1000/500/250 mL single-piece reactor 1

51 161 682 Half-moon stirrer blade, 71 mm 1






51 192 168 ”Keck” clamp ST29 1

51 192 167 ”Keck” clamp ST24 1

51 191 429 ”Keck” clamp ST19 4

51 191 505 ”Keck” clamp ST14 1

51 162 834 1000 mL single-piece glass reactor set


The 1000 mL single-piece glass reactor has a working volume of 1000 mL, a nominal volume of 1150 mL and a starting volume of 200 mL.

OptiMax™ 1000 mL Glass Reactor SetSingle-Piece

25

51 162 760 Reactor stand for 1000 mL single-piece reactor

Material PE


Quantity 1


Material HC-22


Quantity 1


Material PTFE


Quantity 1


51 162 732 1000 mL single-piece glass reactor, 7 ports1 x ST14/23, 4 x ST19/26, 1 x ST29/32,center ST24/29






Quantity 1

51 162 681 Glass stirrer shaft for 1000/500/250 mL reactor



Quantity 1

51 162 682 Half-moon stirrer blade for 1000 mL reactor

Material PTFE

Size 19 x 71 mm

Quantity 1








26



Material Glass

Quantity 1


Material Glass

Quantity 1


Material Glass

Quantity 1

27


51 192 167 ”Keck” clamp ST24

Material POM

Quantity 1

51 191 505 ”Keck” clamp ST14

Material POM

Quantity 1

51 192 168 ”Keck” clamp ST29

Material POM

Quantity 1

51 191 429 ”Keck” clamp ST19

Material POM

Quantity 1

28













51 192 168 ”Keck” clamp ST29 1

51 192 167 ”Keck” clamp ST24 1

51 191 429 ”Keck” clamp ST19 4

51 191 505 ”Keck” clamp ST14 2





29


51 162 733 500 mL single-piece glass reactor2 x ST14/23, 4 x ST19/26, center ST29/32






Quantity 1




Quantity 1

51 162 683 Half-moon stirrer blade for 500 mL reactor

Material PTFE

Size 19 x 54 mm

Quantity 1










Quantity 1

51 162 759 Reactor stand for 500 mL single-piece reactor

Material PE


Quantity 1

30



Material HC-22


Quantity 1


Material Glass

Quantity 1


Material PTFE


Quantity 1


Material Glass

Quantity 1

31

51 192 168 ”Keck” clamp ST29

Material POM

Quantity 1

51 191 429 ”Keck” clamp ST19

Material POM

Quantity 1

51 192 167 ”Keck” clamp ST24

Material POM

Quantity 1

51 191 505 ”Keck” clamp ST14

Material POM

Quantity 1


323232











51 192 167 ”Keck” clamp ST24 1

51 191 429 ”Keck” clamp ST19 4

51 191 505 ”Keck” clamp ST14 2





3333









51 162 734 Single-piece glass reactor, 250 mL2 x ST14/23, 4 x ST19/26, center ST24/29






Quantity 1




Quantity 1

51 162 684 Half-moon stirrer blade, 43 mm

Material PTFE

Size 19 x 43 mm

Quantity 1



Quantity 1

51 162 758 Reactor stand for 250 mL reactor

Material PE


Quantity 1

34

OptiMax™ 250 mL Single-Piece Glass Reactor


Material Glass

Quantity 1

51 191 429 ”Keck” clamp ST19

Material POM

Quantity 1


Material Glass

Quantity 1

51 192 167 ”Keck” clamp ST24

Material POM

Quantity 1

51 191 505 ”Keck” clamp ST14

Material POM

Quantity 1

3535

OptiMax™ Spare Parts, Adapters, and Stirrers

OptiMax™ ReactorSpare Parts and PTFE Adapters

51 162 631 Glass vessel for two-piece 1000 mL reactorwithout parts for bottom drain valve






Quantity 1

51 162 730 Bottom drain connect setfor bottom drain valve

Material PEEK, PTFE

Size Ø 52 mm

Quantity 1

51 191 774 Spindle, bottom drain valve115 mm, with spring

Material PTFE

Size Ø 14 x 115 mm

Quantity 1

51 162 633 Glass vessel for two-piece 500 mL reactorwithout parts for bottom drain valve






Quantity 1

71 540 Sealing ring for bottom drain

Material FEP

Size Inner Ø 22 mm, 14 mm

Quantity 1

51 160 970 PTFE adapter, eccentricfor PVM/D600 probe, including 51 160 973 sealing ring

Material PTFE


Quantity 1

51 160 973 Sealing ring for 51 160 970 PTFE adapter

Material PTFE cord

Size Inner Ø 19 mm

Quantity 1

36



Material PTFE


Quantity 1

51 162 880 PTFE adapterfor G400, including 51 162 879 sealing ring

Material PTFE


Quantity 1

51 162 717 PTFE adapter, eccentricfor pH and turbidity probe, including 51 162 765 sealing ring

Material PTFE


Quantity 1

51 162 713 PTFE adapter, eccentricfor turbidity probe, including 51 162 716 sealing ring

Material PTFE


Quantity 1

51 162 720 PTFE adapter, eccentricfor Tr and turbidity probe, including 51 162 716 sealing ring

Material PTFE


Quantity 1

103 047 Sealing ring for 51 104 154 PTFE adapter

Material PTFE cord

Size Inner Ø 10 mm

Quantity 1


Material GoreTex-GR®

Size Inner Ø 14 mm

Quantity 1



Size Inner Ø 12 mm

Quantity 1

51 162 716 Sealing ring for 51 162 713 and 51 162 720 PTFE adapters


Size Inner Ø 6 mm

Quantity 1

37


103 507 Anchor blade for 1000 mL reactorM8 thread

Material HC-22

Size Outer Ø 90 mm, height 100 mm

Quantity 1

51 160 025 Pitched stirrer blade for 1000/500 mL reactorupward, 4 impellers, 45°, M8 thread

Material HC-22

Size Outer Ø 45 mm

Quantity 1


Material HC-22

Size Outer Ø 45 mm

Quantity 1

51 162 825 Pitched-blade glass stirrer for 1000/500 mL reactorsdownward, 4 impellers, 45°


Size Outer Ø 45 mm, length 400 mm

Quantity 1


Material HC-22


Quantity 1

51 162 826 Pitched-blade glass stirrer for 1000/500 mL reactorupward, 4 impellers, 45°



Quantity 1

OptiMax™ Mixing DeviceAvailable Stirrers

For 1000 mL reactor

38


51 162 677 Anchor blade for 500 mL reactorM8 thread

Material HC-22


Quantity 1

51 160 025 Pitched stirrer blade for 1000/500 mL reactorupward, 4 impellers, 45°, M8 thread

Material HC-22

Size Outer Ø 45 mm

Quantity 1


Material HC-22

Size Outer Ø 45 mm

Quantity 1

51 162 825 Pitched-blade glass stirrer for 1000/500 mL reactorsdownward, 4 impellers, 45°



Quantity 1


Material HC-22


Quantity 1

51 162 826 Pitched-blade glass stirrer for 1000/500 mL reactorupward, 4 impellers, 45°



Quantity 1

For 500 mL reactor

39


51 162 678 Anchor stirrer for 250 mL reactorM3 thread

Material HC-22


Quantity 1

51 162 442 Pitched stirrer blade for 250 mL reactorupward, 4 impellers, 45°, M3 thread

Material HC-22

Size Outer Ø 38 mm

Quantity 1

51 162 418 Pitched stirrer blade for 250 mL reactordownward, 4 impellers, 45°, M3 thread

Material HC-22

Size Outer Ø 38 mm

Quantity 1

51 162 423 Pitched-blade glass stirrer for 250 mL reactordownward, 4 impellers, 45°



Quantity 1

51 162 417 Stirrer shaft for 250 mL reactor M3 thread

Material HC-22

Size Ø 10/8 mm, length 400 mm

Quantity 1

51 162 424 Pitched-blade glass stirrer for 250 mL reactorupward, 4 impellers, 45°



Quantity 1

For 250 mL reactor

40


51 162 682 Half-moon stirrer blade for 1000 mL single-piece reactor

Material PTFE

Size 19 x 71 mm

Quantity 1


Material PTFE

Size 19 x 54 mm

Quantity 1


Material PTFE

Size 19 x 43 mm

Quantity 1

51 162 681 Glass stirrer shaft for 1000/500/250 mL single-piece reactor



Quantity 1




Quantity 1




Quantity 1

For 1000 mL single-piece reactor



41

OptiMax™ Accessories and Probes

OptiMax™ AccessoriesReflux Condenser, Tr and pH Probes

51 192 166 Reflux condenser glass, ST19


Size 250 x 40 mm

Quantity 1

51 162 839 HC-22 temp. sensor, incl. chip

Material HC-22

Size Ø 6 mm, 300 mm

Quantity 1

51 162 827 Glass temp. sensor, incl. chip

Material Glass

Size Ø 6 mm, 300 mm

Quantity 1

51 162 829 pH sensor OptiMax, incl. chip

Material Lead-free glass (shaft), high alkaline glass (membrane)

Size Ø 12 mm, 325 mm (glass body only)

Quantity 1

51 162 888 Cable for 51 162 829 pH sensor

Size Length 100 cm

Quantity 1

42


Dosing unit SP-50 set consisting of


Dosing Unit SP-50, only available in the set 1

51 109 886 CAN cable 60 cm 1

51 191 306 PTFE dosing tube Ø 3.2 mm 3

51 191 304 PTFE dosing tube Ø 1.6 mm 2

51 191 515 Nut for UNF 1/4 28 threads, outer Ø max. 3.2 mm , 4 pcs in a set 1

51 191 514 Ferrule for tubing and sensors of outer Ø 3.2 mm, 4 pcs in a set 1

51 191 204 Plug for UNF 1/4 28 threads, 4 pcs in a set 1

51 191 203 Nut for UNF 1/4 28 threads, outer Ø max. 1.6 mm, 4 pcs in a set 1

51 191 202 Ferrule for tubing and sensors of outer Ø 1.6 mm, 4 pcs in a set 1

51 191 267 Glass adapter ST14/23-GL14 2

51 190 318 Screw cap GL14, closed 3

51 191 170 Silicone rubber seal (septum), 10 pcs in a set 1

51 191 972 Distributor cap GL45 2 x GL14 1

51 191 591 Bottle GL45 250 mL with cap 1

51 161 558 Adapter GL14-UNF 3

51 190 317 Screw cap GL14, with aperture 3

51 103 947 Silicone rubber sealing ring, outer Ø 12 mm, aperture 6 mm 6

51 191 687 Assorted heat-shrink tubings, 8 pcs in a set 1

51 161 770 Dosing unit SP-50 set

This unit will allow you to dose 1 reagent in 2 reactors completely independent and in parallel via touchpad or PC software.

Only available in the set.

Dosing Unit SP-50 Set

43


51 191 515 Nut for UNF 1/4 28 threads

Material ETFE

Size Outer Ø max. 3.2 mm

Quantity 4 pcs in a set

51 191 514 Ferrule for tubing and sensors of outer Ø 3.2 mm

Material ETFE



51 191 204 Plug for UNF 1/4 28 threads

Material ETFE



51 191 203 Nut for UNF 1/4 28 threads

Material ETFE



51 191 202 Ferrule for tubing and sensors of outer Ø 1.6 mm

Material ETFE



Dosing unit SP-50

Quantity 1

only available in the set

51 109 886 CAN cable 60 cm

Size Length 60 cm

Quantity 1

51 191 306 PTFE dosing tube Ø 3.2 mm

Material PTFE

Size Ø 3.2 mm, length 2.5 m

Quantity 1

51 191 304 PTFE dosing tube Ø 1.6 mm

Material PTFE

Size Ø 1.6 mm, length 2.5 m

Quantity 1

44


51 161 558 Adapter GL14-UNF

Material PTFE GF25

Size 36.14 x 2.62 mm

Quantity 1

51 190 317 Screw cap GL14, with aperture

Material PBT


Size Aperture Ø 9.5 mm

Quantity 1

51 103 947 Sealing ring with vulcanized-on PTFE washers for GL14 cap

Material Silicone rubber VQM, PTFE-coated

Size Ø 12 mm, aperture 6 mm

Quantity 1

51 191 687 Assorted heat-shrink tubings8 pcs in a set

Material Polyolefin

Quantity 1

51 191 267 Glass adapter ST14/23-GL14

Material Glass

Size Height 54 mm

Quantity 1

51 190 318 Screw cap GL14, closedwith PTFE sealing

Material PBT


Quantity 1

51 191 170 Silicone rubber seal (septum)for screw cap GL14

Material Silicone rubber VQM

Size Ø 12 mm, thickness 2 mm


51 191 972 Distributor cap GL45 2x GL14

Material PP

Quantity 1

51 191 591 Bottle GL45 250 mL with cap

Material Glass, PP

Quantity 1

45


Dosing Unit SP-50Syringes

51 191 793 Syringe 1 mL

Material Glass, PTFE, metal

Volume 1 mL

Quantity 1

51 191 792 Syringe 10 mL


Volume 10 mL

Quantity 1

51 191 794 Syringe 25 mL


Volume 25 mL

Quantity 1

51 191 987 Syringe 50 mL


Volume 50 mL

Quantity 1

Flexible volumes from 1, 10, 25, and 50 mL syringes Automatic refill of syringes possible with Dosing Unit SP-50 Interchangeable at all times during an experiment

46

Compatibility List

1000 mL glass reactor and cover



51 160 025 Pitched stirrer blade, upward 1 1

103 504 Pitched stirrer blade, downward 1 1

103 507 Anchor blade 1

51 162 677 Anchor blade 1

51 162 826 Pitched-blade stirrer, upward 1 1

51 162 825 Pitched-blade stirrer, downward 1 1

51 162 442 Pitched stirrer blade, upward 2

51 162 418 Pitched stirrer blade, downward 2

51 162 678 Anchor blade 2

51 162 424 Pitched-blade stirrer, upward 2

51 162 423 Pitched-blade stirrer, downward 2

51 162 637 Bar type baffle 3


51 162 839 Temp. sensor, HC-22, 6 mm x 300 mm, incl. chip 4 4 4

51 162 827 Temp. sensor, glass, 6 mm x 300 mm, incl. chip 4 4 4

51 162 829 pH sensor OptiMax, incl. chip 4 4 4

51 192 166 Reflux condenser glass, ST19, 250 x 40 mm

Needed items

1) 51 162 722 Stirrer shaft2) 51 162 417 Stirrer shaft3) 51 104 154 PTFE adapter for baffle4) 51 162 720 PTFE adapter, ST145) 51 162 681 Stirrer shaft 51

162

634

10

00 m

L gl

ass

reac

tor

51 1

62 6

71

Gla

ss c

over

51 1

62 6

32

500

mL

glas

s re

acto

r51

162

671

G

lass

cov

er

51 1

62 6

35

250

mL

glas

s re

acto

r51

162

699

G

lass

cov

er

47

Compatibility List

1000 mL single-piece glass reactor



51 162 682 Half-moon stirrer blade 5





51 162 839 Tr-HC-6/300 (incl. programmed Chip) 4 4 4

51 162 839 Temp. sensor, HC-22, 6 mm x 300 mm, incl. chip 4 4 4

51 162 827 Temp. sensor, glass, 6 mm x 300 mm, incl. chip 4 4 4

51 162 829 pH sensor OptiMax, incl. chip 4 4 4

51 192 166 Reflux condenser glass, ST19, 250 x 40 mm

Needed items

1) 51 162 722 Stirrer shaft2) 51 162 417 Stirrer shaft3) 51 104 154 PTFE adapter for baffle4) 51 162 720 PTFE adapter, ST145) 51 162 681 Stirrer shaft 51

162

732

10

00 m

L si

ngle

-pie

ce

gl

ass

reac

tor

51 1

62 7

33

500

mL

sing

le-p

iece

glas

s re

acto

r

51 1

62 7

34

250

mL

sing

le-p

iece

glas

s re

acto

r

For more informationwww.mt.com/OptiMax

Quality certificate. Development, production and testing according to ISO 9001.

Environmental man agement system according to ISO 14001.

European conformity. The CE conformity mark provides you with the assurance that our products comply with the EU directives.

Mettler-Toledo AutoChem Inc.7075 Samuel Morse DriveColumbia, MD 21046, USAPhone +1-410 910 8500Fax +1-410 910 8600

Mettler-Toledo AG, AutoChemSonnenbergstrasse 74CH-8603 Schwerzenbach, SwitzerlandPhone +41-44 806 7711Fax +41-44 806 7290

E-Mail [email protected] www.mt.com/autochem

Subject to technical changes.© 04/2011 Mettler-Toledo AG, MarCom RXEPrinted in Switzerland, 51727001

In chemical and process development, experiment quality is key. METTLER TOLEDO’s OptiMax™ is designed to help make better decisions faster. It executes experiments with great accuracy, providing critical and information-rich data. Often, chemistry can be understood only when additional information, such as the reaction mechanism or the kinetics, is available.

Key reaction species including intermediates and by-products are easily monitored in real-time with ReactIR™, an FTIR-based in-situ reaction analysis tool. The analysis is conducted in the reaction mixture itself, eliminating errors associated by taking samples, and allowing organic chemists to quickly understand if the correct reaction occurred and to observe its start- and endpoint.

The precise temperature control and the high reproducibility of an experi-ment makes the OptiMax™ the ideal workstation to optimize crystalliza-tion processes when combined with the particle characterization system FBRM®. It provides immediate insight into the particle system, enabling chemists and chemical engineers to quickly screen experimental param-eters and develop a scalable process in early process development.

The iC software suite allows scientists and engineers within the pharma-ceutical, chemical and specialty chemical industries to convert the data collected in their experiments into important process knowledge. It provides a unique perspective when it comes to integration of data sets from other equipment, and shares a common design, so users learn the software once and use many instruments. The seamless integration of complementary data sets contributes to the faster understanding of the process under investigation.

Characterize the Process While Optimizing the Chemistry

product catalog - soquimicasoquimica.pt/files/catalogo_optimax_news14.pdfsize for cables with Ø 2...

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