re: july 2017 sampling results smr industrial … · industrial waste division ... enclosed is the...

August 31, 2017 Project No.:023-6105.017

Metropolitan Council Environmental ServicesIndustrial Waste Division390 Robert St. N.St. Paul, MN 55101

Attention: Ms. Ashley Corbeille

RE: JULY 2017 SAMPLING RESULTS SMRINDUSTRIAL DISCHARGE PERMIT NUMBER 2289SOUTHEAST PUMP AND TREAT SYSTEMCANADIAN PACIFIC SHOREHAM FACILITY

Dear Ms. Corbeille:

On behalf of Canadian Pacific, enclosed is the July 2017 Sampling Results Self-Monitoring Report for the site located at 28th & Central Avenue NE, Minneapolis MN. In accordance with the Metropolitan Council Environmental Services (MCES) Industrial Discharge Permit Number 2289, effective October 1, 2016(MCES permit), this submittal documents the quality of water discharged from the groundwater pump and treat system owned by Canadian Pacific.

Required information for the discharge is provided as follows:Attachment A – Sampling Results - SMR.Attachment B – Analytical data from Pace Analytical Services, LLC for the July 2017 monthly sampling event.Attachment C - Field Instrument pH Calibration Records

Analytical results from the July 2017 sampling event1 showed that the treated discharge water was in compliance with the MCES permit discharge limitations during this reporting period.

If you have any questions or comments, please do not hesitate to contact Barbara Johnson at (651) 697-9737. Thank you for your assistance in this matter.

Very truly yours,

GOLDER ASSOCIATES INC.

Alan Phillips Barbara Johnson, PEProject Geologist Associate

Cc: Ms. Aimee Zack, CPMs. Claire Mackler, Golder

1 Note that sample point SP-01 is identified as sample SE EFFLUENT in the analytical results from July 2017(Attachment B)

Golder Associates Inc.1751 West County Rd. B, Ste. 105

Roseville, MN USA 55113Tel: (651) 697-9737 Fax: (651) 697-9737 www.golder.com

Golder Associates: Operations in Africa, Asia, Australasia, Europe, North America and South America

Attachment A

SAMPLING RESULTS – SELF-MONITORING REPORT

Metropolitan Council Environmental Services Industrial Waste & Pollution Prevention Section 390 North Robert Street St. Paul, Minnesota 55101-1805

I For MCES Use Only l I

Permit No: Staff: __

L Received: 0 L 45 E 1

SAMPLING RESULTS - SMR for Standard and Special Discharge Permits Please complete Page 2 of this form for each monitoring point with sampling requirements in Attachment A of the Permit.

1. Permittee Name: Canadian Pacific Railway Permit No: 2289 ------2. Facility Address: 28th Ave NE & Central Ave NE, Minneapolis, MN 55418

3. Reporting Period: Year: 2017 Choose applicable period below:

D

Quarterly Reporter: D Jan-Mar

Semi-Annual Reporter: D Jan-Jun

Annual Reporter: D Jan-Dec

No discharge/No sampling this period.

D Apr-Jun EJ Jul-Sep

D Jul-Dec

D Oct-Dec

If checked, proceed to section 9 below and do not complete page 2.

4. Proper Sampling: Were all samples collected and composited according to permit requirements?

(!]Yes r-1 No If No, add explanation below:

5. Proper Analysis: Were all analyses conducted per permit requirements? [!] Yes D No If No, add explanation below:

6. Representative Discha~: Are the an~ical results representative of the wastewater discharged during this monitoring event? 1!..J Yes LJ No If No, add explanation below:

7. Compliance Status: Compare the analytical results with the corresponding discharge limits in your Permit. Do any analytical results exceed the corresponding discharge limit(s) in your Permit? D Yes [!] No If Yes, add explanation below:

When did you become aware of the exceedance(s)?

8. General comments regarding submission:

9. Certification Statement: "I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ensure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties under law for submitting false information, including the possibility of fine and imprisonment for known violations."

Name (print): Barbara Johnson, PE Title: Authorized Representative for Canadian Pacific

Signature: Date: 8/31/2017

Email: [email protected] Phone: 651-697-9737

Report form help sheet

Page 1of2 SMR-SR-2016

Sample Results: Submit one result sheet for each sampling day per monitoring point. Enter daily values for each sampling event from one monitoring point, in accordance with requirements in the Industrial Discharge Permit (Section 8). Daily and long-term values shall be compared to Discharge Limitations in Permit Section A.1 for compliance determinations. Attach all laboratory data sheets and supporting calculations.

Monitoring Point: SP-01 Description: Effluent discharge line

Sample Start Date & Time: 7/17/17 12:05 Sample End Date & Time: 7/17/17 12:05 ---------------------~

Discharge volume through monitoring point on sampling day: 30,938 (estimated)

Sample collected by: D Permittee EJ Other, name: Golder Associates Inc.

gallons

Method of collection: 0 Manual 0 Automatic

Sample composited by: D Permittee D Other, name: ------------- Composite method: N_A _____________________ _

Substance Analytical Result Unit Detection Limits Analysis Method Sample Method

Sample Laboratory Result Container Type Name

pH 6.0 s.u. 0-14 4500-H+ Grab-Single Other Field Measurement

Total Suspended Solids NS Grab - Single NA

Chemical Oxygen Demand NS Grab - Single NA

1, 1-Dichloroethane 0.0185 mg/I 0.00024 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

1, 1-Dichloroethene 0.0047 mg/I 0.00041 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

cis-1,2-Dichloroethene 0.0153 mg/I 0.00026 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

T etrachloroethene 0.0286 mg/I 0.00050 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

1, 1, 1-Trichloroethane 0.0123 mg/I 0.00050 EPA 8260 Grab- Single Vial - 40ml clear Pace Analytical Services, LLC

Trichloroethene 0.0048 mg/I 0.00033 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, LLC

Page 2 of 2 SMR-SR-2016

Attachment B

ANALYTICAL DATA FROM PACE ANALYTICAL SERVICES, LLC

July 2017

#=CL#

July 21, 2017

LIMS USE: FR - ALISON ZOLLLIMS OBJECT ID: 40153410

40153410Project:Pace Project No.:

RE:

Alison ZollGolder Associates Inc.744 Broad Street25th FloorNewark, NJ 07102

023-6105-017 CP-SHOREHAM YARD

Dear Alison Zoll:Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2017. Theresults relate only to the samples included in this report. Results reported herein conform to the mostcurrent, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, whereapplicable, unless otherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Laurie [email protected]

Project Manager(920)469-2436

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, LLC.

Pace Analytical Services, LLC1241 Bellevue Street - Suite 9

Green Bay, WI 54302(920)469-2436

Page 1 of 17

#=CP#

CERTIFICATIONS

Pace Project No.:Project:

40153410023-6105-017 CP-SHOREHAM YARD

Green Bay Certification IDs1241 Bellevue Street, Green Bay, WI 54302Florida/NELAP Certification #: E87948Illinois Certification #: 200050Kentucky UST Certification #: 82Louisiana Certification #: 04168Minnesota Certification #: 055-999-334New York Certification #: 12064North Dakota Certification #: R-150

Virginia VELAP ID: 460263South Carolina Certification #: 83006001Texas Certification #: T104704529-14-1Wisconsin Certification #: 405132750Wisconsin DATCP Certification #: 105-444USDA Soil Permit #: P330-16-00157Federal Fish & Wildlife Permit #: LE51774A-0




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#=SS#

SAMPLE SUMMARY


40153410023-6105-017 CP-SHOREHAM YARD

Lab ID Sample ID Matrix Date Collected Date Received

40153410001 071717-0800-200 Water 07/17/17 08:00 07/18/17 08:43

40153410002 SE EFFLUENT Water 07/17/17 12:05 07/18/17 08:43




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#=SA#

SAMPLE ANALYTE COUNT


40153410023-6105-017 CP-SHOREHAM YARD

Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

40153410001 071717-0800-200 EPA 8260 71 PASI-GMDS

40153410002 SE EFFLUENT EPA 8260 71 PASI-GMDS




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#=AR#

ANALYTICAL RESULTS


40153410023-6105-017 CP-SHOREHAM YARD

Sample: 071717-0800-200 Lab ID: 40153410001 Collected: 07/17/17 08:00 Received: 07/18/17 08:43 Matrix: Water

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL

Analytical Method: EPA 82608260 MSV

Acetone <3.0 ug/L 07/20/17 14:27 67-64-120.0 3.0 1Allyl chloride <2.2 ug/L 07/20/17 14:27 107-05-15.0 2.2 1Benzene <0.50 ug/L 07/20/17 14:27 71-43-21.0 0.50 1Bromobenzene <0.23 ug/L 07/20/17 14:27 108-86-11.0 0.23 1Bromochloromethane <0.34 ug/L 07/20/17 14:27 74-97-51.0 0.34 1Bromodichloromethane <0.50 ug/L 07/20/17 14:27 75-27-41.0 0.50 1Bromoform <0.50 ug/L 07/20/17 14:27 75-25-21.0 0.50 1Bromomethane <2.4 ug/L 07/20/17 14:27 74-83-9 L15.0 2.4 12-Butanone (MEK) <3.0 ug/L 07/20/17 14:27 78-93-320.0 3.0 1n-Butylbenzene <0.50 ug/L 07/20/17 14:27 104-51-81.0 0.50 1sec-Butylbenzene <2.2 ug/L 07/20/17 14:27 135-98-85.0 2.2 1tert-Butylbenzene <0.18 ug/L 07/20/17 14:27 98-06-61.0 0.18 1Carbon tetrachloride <0.50 ug/L 07/20/17 14:27 56-23-51.0 0.50 1Chlorobenzene <0.50 ug/L 07/20/17 14:27 108-90-71.0 0.50 1Chloroethane <0.37 ug/L 07/20/17 14:27 75-00-31.0 0.37 1Chloroform <2.5 ug/L 07/20/17 14:27 67-66-35.0 2.5 1Chloromethane <0.50 ug/L 07/20/17 14:27 74-87-31.0 0.50 12-Chlorotoluene <0.50 ug/L 07/20/17 14:27 95-49-81.0 0.50 14-Chlorotoluene <0.21 ug/L 07/20/17 14:27 106-43-41.0 0.21 11,2-Dibromo-3-chloropropane <2.2 ug/L 07/20/17 14:27 96-12-85.0 2.2 1Dibromochloromethane <0.50 ug/L 07/20/17 14:27 124-48-11.0 0.50 11,2-Dibromoethane (EDB) <0.18 ug/L 07/20/17 14:27 106-93-41.0 0.18 1Dibromomethane <0.43 ug/L 07/20/17 14:27 74-95-31.0 0.43 11,2-Dichlorobenzene <0.50 ug/L 07/20/17 14:27 95-50-11.0 0.50 11,3-Dichlorobenzene <0.50 ug/L 07/20/17 14:27 541-73-11.0 0.50 11,4-Dichlorobenzene <0.50 ug/L 07/20/17 14:27 106-46-71.0 0.50 1Dichlorodifluoromethane <0.22 ug/L 07/20/17 14:27 75-71-81.0 0.22 11,1-Dichloroethane <0.24 ug/L 07/20/17 14:27 75-34-31.0 0.24 11,2-Dichloroethane <0.17 ug/L 07/20/17 14:27 107-06-21.0 0.17 11,1-Dichloroethene <0.41 ug/L 07/20/17 14:27 75-35-41.0 0.41 1cis-1,2-Dichloroethene <0.26 ug/L 07/20/17 14:27 156-59-21.0 0.26 1trans-1,2-Dichloroethene <0.26 ug/L 07/20/17 14:27 156-60-51.0 0.26 1Dichlorofluoromethane <0.21 ug/L 07/20/17 14:27 75-43-41.0 0.21 11,2-Dichloropropane <0.23 ug/L 07/20/17 14:27 78-87-51.0 0.23 11,3-Dichloropropane <0.50 ug/L 07/20/17 14:27 142-28-91.0 0.50 12,2-Dichloropropane <0.48 ug/L 07/20/17 14:27 594-20-71.0 0.48 11,1-Dichloropropene <0.44 ug/L 07/20/17 14:27 563-58-61.0 0.44 1cis-1,3-Dichloropropene <0.50 ug/L 07/20/17 14:27 10061-01-51.0 0.50 1trans-1,3-Dichloropropene <0.23 ug/L 07/20/17 14:27 10061-02-61.0 0.23 1Diethyl ether (Ethyl ether) <2.2 ug/L 07/20/17 14:27 60-29-75.0 2.2 1Ethylbenzene <0.50 ug/L 07/20/17 14:27 100-41-41.0 0.50 1Hexachloro-1,3-butadiene <2.1 ug/L 07/20/17 14:27 87-68-35.0 2.1 1Isopropylbenzene (Cumene) <0.14 ug/L 07/20/17 14:27 98-82-81.0 0.14 1p-Isopropyltoluene <0.50 ug/L 07/20/17 14:27 99-87-61.0 0.50 1Methylene Chloride <0.23 ug/L 07/20/17 14:27 75-09-21.0 0.23 14-Methyl-2-pentanone (MIBK) <2.1 ug/L 07/20/17 14:27 108-10-15.0 2.1 1


without the written consent of Pace Analytical Services, LLC.Date: 07/21/2017 02:53 PM


Green Bay, WI 54302(920)469-2436

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#=AR#

ANALYTICAL RESULTS


40153410023-6105-017 CP-SHOREHAM YARD

Sample: 071717-0800-200 Lab ID: 40153410001 Collected: 07/17/17 08:00 Received: 07/18/17 08:43 Matrix: Water



Methyl-tert-butyl ether <0.17 ug/L 07/20/17 14:27 1634-04-41.0 0.17 1Naphthalene <2.5 ug/L 07/20/17 14:27 91-20-35.0 2.5 1n-Propylbenzene <0.50 ug/L 07/20/17 14:27 103-65-11.0 0.50 1Styrene <0.50 ug/L 07/20/17 14:27 100-42-51.0 0.50 11,1,1,2-Tetrachloroethane <0.18 ug/L 07/20/17 14:27 630-20-61.0 0.18 11,1,2,2-Tetrachloroethane <0.25 ug/L 07/20/17 14:27 79-34-51.0 0.25 1Tetrachloroethene <0.50 ug/L 07/20/17 14:27 127-18-41.0 0.50 1Tetrahydrofuran <2.0 ug/L 07/20/17 14:27 109-99-95.0 2.0 1Toluene <0.50 ug/L 07/20/17 14:27 108-88-31.0 0.50 11,2,3-Trichlorobenzene <2.1 ug/L 07/20/17 14:27 87-61-65.0 2.1 11,2,4-Trichlorobenzene <2.2 ug/L 07/20/17 14:27 120-82-15.0 2.2 11,1,1-Trichloroethane <0.50 ug/L 07/20/17 14:27 71-55-61.0 0.50 11,1,2-Trichloroethane <0.20 ug/L 07/20/17 14:27 79-00-51.0 0.20 1Trichloroethene <0.33 ug/L 07/20/17 14:27 79-01-61.0 0.33 1Trichlorofluoromethane <0.18 ug/L 07/20/17 14:27 75-69-41.0 0.18 11,2,3-Trichloropropane <0.50 ug/L 07/20/17 14:27 96-18-41.0 0.50 11,1,2-Trichlorotrifluoroethane <0.81 ug/L 07/20/17 14:27 76-13-15.0 0.81 11,2,4-Trimethylbenzene <0.50 ug/L 07/20/17 14:27 95-63-61.0 0.50 11,3,5-Trimethylbenzene <0.50 ug/L 07/20/17 14:27 108-67-81.0 0.50 1Vinyl chloride <0.18 ug/L 07/20/17 14:27 75-01-41.0 0.18 1m&p-Xylene <1.0 ug/L 07/20/17 14:27 179601-23-12.0 1.0 1o-Xylene <0.50 ug/L 07/20/17 14:27 95-47-61.0 0.50 1Surrogates4-Bromofluorobenzene (S) 90 % 07/20/17 14:27 460-00-461-130 1Dibromofluoromethane (S) 107 % 07/20/17 14:27 1868-53-767-130 1Toluene-d8 (S) 99 % 07/20/17 14:27 2037-26-570-130 1




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#=AR#

ANALYTICAL RESULTS


40153410023-6105-017 CP-SHOREHAM YARD

Sample: SE EFFLUENT Lab ID: 40153410002 Collected: 07/17/17 12:05 Received: 07/18/17 08:43 Matrix: Water



Acetone <3.0 ug/L 07/20/17 15:33 67-64-120.0 3.0 1Allyl chloride <2.2 ug/L 07/20/17 15:33 107-05-15.0 2.2 1Benzene <0.50 ug/L 07/20/17 15:33 71-43-21.0 0.50 1Bromobenzene <0.23 ug/L 07/20/17 15:33 108-86-11.0 0.23 1Bromochloromethane <0.34 ug/L 07/20/17 15:33 74-97-51.0 0.34 1Bromodichloromethane <0.50 ug/L 07/20/17 15:33 75-27-41.0 0.50 1Bromoform <0.50 ug/L 07/20/17 15:33 75-25-21.0 0.50 1Bromomethane <2.4 ug/L 07/20/17 15:33 74-83-9 L1,M05.0 2.4 12-Butanone (MEK) <3.0 ug/L 07/20/17 15:33 78-93-320.0 3.0 1n-Butylbenzene <0.50 ug/L 07/20/17 15:33 104-51-81.0 0.50 1sec-Butylbenzene <2.2 ug/L 07/20/17 15:33 135-98-85.0 2.2 1tert-Butylbenzene <0.18 ug/L 07/20/17 15:33 98-06-61.0 0.18 1Carbon tetrachloride <0.50 ug/L 07/20/17 15:33 56-23-51.0 0.50 1Chlorobenzene <0.50 ug/L 07/20/17 15:33 108-90-71.0 0.50 1Chloroethane <0.37 ug/L 07/20/17 15:33 75-00-31.0 0.37 1Chloroform <2.5 ug/L 07/20/17 15:33 67-66-35.0 2.5 1Chloromethane <0.50 ug/L 07/20/17 15:33 74-87-31.0 0.50 12-Chlorotoluene <0.50 ug/L 07/20/17 15:33 95-49-81.0 0.50 14-Chlorotoluene <0.21 ug/L 07/20/17 15:33 106-43-41.0 0.21 11,2-Dibromo-3-chloropropane <2.2 ug/L 07/20/17 15:33 96-12-8 R15.0 2.2 1Dibromochloromethane <0.50 ug/L 07/20/17 15:33 124-48-11.0 0.50 11,2-Dibromoethane (EDB) <0.18 ug/L 07/20/17 15:33 106-93-41.0 0.18 1Dibromomethane <0.43 ug/L 07/20/17 15:33 74-95-31.0 0.43 11,2-Dichlorobenzene <0.50 ug/L 07/20/17 15:33 95-50-11.0 0.50 11,3-Dichlorobenzene <0.50 ug/L 07/20/17 15:33 541-73-11.0 0.50 11,4-Dichlorobenzene <0.50 ug/L 07/20/17 15:33 106-46-71.0 0.50 1Dichlorodifluoromethane <0.22 ug/L 07/20/17 15:33 75-71-81.0 0.22 11,1-Dichloroethane 18.5 ug/L 07/20/17 15:33 75-34-31.0 0.24 11,2-Dichloroethane <0.17 ug/L 07/20/17 15:33 107-06-21.0 0.17 11,1-Dichloroethene 4.7 ug/L 07/20/17 15:33 75-35-41.0 0.41 1cis-1,2-Dichloroethene 15.3 ug/L 07/20/17 15:33 156-59-21.0 0.26 1trans-1,2-Dichloroethene <0.26 ug/L 07/20/17 15:33 156-60-51.0 0.26 1Dichlorofluoromethane <0.21 ug/L 07/20/17 15:33 75-43-41.0 0.21 11,2-Dichloropropane <0.23 ug/L 07/20/17 15:33 78-87-51.0 0.23 11,3-Dichloropropane <0.50 ug/L 07/20/17 15:33 142-28-91.0 0.50 12,2-Dichloropropane <0.48 ug/L 07/20/17 15:33 594-20-71.0 0.48 11,1-Dichloropropene <0.44 ug/L 07/20/17 15:33 563-58-61.0 0.44 1cis-1,3-Dichloropropene <0.50 ug/L 07/20/17 15:33 10061-01-51.0 0.50 1trans-1,3-Dichloropropene <0.23 ug/L 07/20/17 15:33 10061-02-61.0 0.23 1Diethyl ether (Ethyl ether) <2.2 ug/L 07/20/17 15:33 60-29-75.0 2.2 1Ethylbenzene <0.50 ug/L 07/20/17 15:33 100-41-41.0 0.50 1Hexachloro-1,3-butadiene <2.1 ug/L 07/20/17 15:33 87-68-35.0 2.1 1Isopropylbenzene (Cumene) <0.14 ug/L 07/20/17 15:33 98-82-81.0 0.14 1p-Isopropyltoluene <0.50 ug/L 07/20/17 15:33 99-87-61.0 0.50 1Methylene Chloride <0.23 ug/L 07/20/17 15:33 75-09-21.0 0.23 14-Methyl-2-pentanone (MIBK) <2.1 ug/L 07/20/17 15:33 108-10-15.0 2.1 1




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#=AR#

ANALYTICAL RESULTS


40153410023-6105-017 CP-SHOREHAM YARD

Sample: SE EFFLUENT Lab ID: 40153410002 Collected: 07/17/17 12:05 Received: 07/18/17 08:43 Matrix: Water



Methyl-tert-butyl ether <0.17 ug/L 07/20/17 15:33 1634-04-41.0 0.17 1Naphthalene <2.5 ug/L 07/20/17 15:33 91-20-35.0 2.5 1n-Propylbenzene <0.50 ug/L 07/20/17 15:33 103-65-11.0 0.50 1Styrene <0.50 ug/L 07/20/17 15:33 100-42-51.0 0.50 11,1,1,2-Tetrachloroethane <0.18 ug/L 07/20/17 15:33 630-20-61.0 0.18 11,1,2,2-Tetrachloroethane <0.25 ug/L 07/20/17 15:33 79-34-51.0 0.25 1Tetrachloroethene 28.6 ug/L 07/20/17 15:33 127-18-41.0 0.50 1Tetrahydrofuran <2.0 ug/L 07/20/17 15:33 109-99-95.0 2.0 1Toluene <0.50 ug/L 07/20/17 15:33 108-88-31.0 0.50 11,2,3-Trichlorobenzene <2.1 ug/L 07/20/17 15:33 87-61-65.0 2.1 11,2,4-Trichlorobenzene <2.2 ug/L 07/20/17 15:33 120-82-15.0 2.2 11,1,1-Trichloroethane 12.3 ug/L 07/20/17 15:33 71-55-61.0 0.50 11,1,2-Trichloroethane <0.20 ug/L 07/20/17 15:33 79-00-51.0 0.20 1Trichloroethene 4.8 ug/L 07/20/17 15:33 79-01-61.0 0.33 1Trichlorofluoromethane <0.18 ug/L 07/20/17 15:33 75-69-41.0 0.18 11,2,3-Trichloropropane <0.50 ug/L 07/20/17 15:33 96-18-41.0 0.50 11,1,2-Trichlorotrifluoroethane <0.81 ug/L 07/20/17 15:33 76-13-15.0 0.81 11,2,4-Trimethylbenzene <0.50 ug/L 07/20/17 15:33 95-63-61.0 0.50 11,3,5-Trimethylbenzene <0.50 ug/L 07/20/17 15:33 108-67-81.0 0.50 1Vinyl chloride <0.18 ug/L 07/20/17 15:33 75-01-41.0 0.18 1m&p-Xylene <1.0 ug/L 07/20/17 15:33 179601-23-12.0 1.0 1o-Xylene <0.50 ug/L 07/20/17 15:33 95-47-61.0 0.50 1Surrogates4-Bromofluorobenzene (S) 88 % 07/20/17 15:33 460-00-461-130 1Dibromofluoromethane (S) 104 % 07/20/17 15:33 1868-53-767-130 1Toluene-d8 (S) 96 % 07/20/17 15:33 2037-26-570-130 1




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#=QC#

QUALITY CONTROL DATA


40153410023-6105-017 CP-SHOREHAM YARD

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

262036EPA 8260

EPA 82608260 MSV

Associated Lab Samples: 40153410001, 40153410002

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 1542599Associated Lab Samples: 40153410001, 40153410002

Matrix: Water

AnalyzedMDL

1,1,1,2-Tetrachloroethane ug/L <0.18 1.0 07/20/17 11:290.181,1,1-Trichloroethane ug/L <0.50 1.0 07/20/17 11:290.501,1,2,2-Tetrachloroethane ug/L <0.25 1.0 07/20/17 11:290.251,1,2-Trichloroethane ug/L <0.20 1.0 07/20/17 11:290.201,1,2-Trichlorotrifluoroethane ug/L <0.81 5.0 07/20/17 11:290.811,1-Dichloroethane ug/L <0.24 1.0 07/20/17 11:290.241,1-Dichloroethene ug/L <0.41 1.0 07/20/17 11:290.411,1-Dichloropropene ug/L <0.44 1.0 07/20/17 11:290.441,2,3-Trichlorobenzene ug/L <2.1 5.0 07/20/17 11:292.11,2,3-Trichloropropane ug/L <0.50 1.0 07/20/17 11:290.501,2,4-Trichlorobenzene ug/L <2.2 5.0 07/20/17 11:292.21,2,4-Trimethylbenzene ug/L <0.50 1.0 07/20/17 11:290.501,2-Dibromo-3-chloropropane ug/L <2.2 5.0 07/20/17 11:292.21,2-Dibromoethane (EDB) ug/L <0.18 1.0 07/20/17 11:290.181,2-Dichlorobenzene ug/L <0.50 1.0 07/20/17 11:290.501,2-Dichloroethane ug/L <0.17 1.0 07/20/17 11:290.171,2-Dichloropropane ug/L <0.23 1.0 07/20/17 11:290.231,3,5-Trimethylbenzene ug/L <0.50 1.0 07/20/17 11:290.501,3-Dichlorobenzene ug/L <0.50 1.0 07/20/17 11:290.501,3-Dichloropropane ug/L <0.50 1.0 07/20/17 11:290.501,4-Dichlorobenzene ug/L <0.50 1.0 07/20/17 11:290.502,2-Dichloropropane ug/L <0.48 1.0 07/20/17 11:290.482-Butanone (MEK) ug/L <3.0 20.0 07/20/17 11:293.02-Chlorotoluene ug/L <0.50 1.0 07/20/17 11:290.504-Chlorotoluene ug/L <0.21 1.0 07/20/17 11:290.214-Methyl-2-pentanone (MIBK) ug/L <2.1 5.0 07/20/17 11:292.1Acetone ug/L <3.0 20.0 07/20/17 11:293.0Allyl chloride ug/L <2.2 5.0 07/20/17 11:292.2Benzene ug/L <0.50 1.0 07/20/17 11:290.50Bromobenzene ug/L <0.23 1.0 07/20/17 11:290.23Bromochloromethane ug/L <0.34 1.0 07/20/17 11:290.34Bromodichloromethane ug/L <0.50 1.0 07/20/17 11:290.50Bromoform ug/L <0.50 1.0 07/20/17 11:290.50Bromomethane ug/L <2.4 5.0 07/20/17 11:292.4Carbon tetrachloride ug/L <0.50 1.0 07/20/17 11:290.50Chlorobenzene ug/L <0.50 1.0 07/20/17 11:290.50Chloroethane ug/L <0.37 1.0 07/20/17 11:290.37Chloroform ug/L <2.5 5.0 07/20/17 11:292.5Chloromethane ug/L <0.50 1.0 07/20/17 11:290.50cis-1,2-Dichloroethene ug/L <0.26 1.0 07/20/17 11:290.26cis-1,3-Dichloropropene ug/L <0.50 1.0 07/20/17 11:290.50




Green Bay, WI 54302(920)469-2436

Page 9 of 17

#=QC#



40153410023-6105-017 CP-SHOREHAM YARD


Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 1542599Associated Lab Samples: 40153410001, 40153410002

Matrix: Water

AnalyzedMDL

Dibromochloromethane ug/L <0.50 1.0 07/20/17 11:290.50Dibromomethane ug/L <0.43 1.0 07/20/17 11:290.43Dichlorodifluoromethane ug/L <0.22 1.0 07/20/17 11:290.22Dichlorofluoromethane ug/L <0.21 1.0 07/20/17 11:290.21Diethyl ether (Ethyl ether) ug/L <2.2 5.0 07/20/17 11:292.2Ethylbenzene ug/L <0.50 1.0 07/20/17 11:290.50Hexachloro-1,3-butadiene ug/L <2.1 5.0 07/20/17 11:292.1Isopropylbenzene (Cumene) ug/L <0.14 1.0 07/20/17 11:290.14m&p-Xylene ug/L <1.0 2.0 07/20/17 11:291.0Methyl-tert-butyl ether ug/L <0.17 1.0 07/20/17 11:290.17Methylene Chloride ug/L <0.23 1.0 07/20/17 11:290.23n-Butylbenzene ug/L <0.50 1.0 07/20/17 11:290.50n-Propylbenzene ug/L <0.50 1.0 07/20/17 11:290.50Naphthalene ug/L <2.5 5.0 07/20/17 11:292.5o-Xylene ug/L <0.50 1.0 07/20/17 11:290.50p-Isopropyltoluene ug/L <0.50 1.0 07/20/17 11:290.50sec-Butylbenzene ug/L <2.2 5.0 07/20/17 11:292.2Styrene ug/L <0.50 1.0 07/20/17 11:290.50tert-Butylbenzene ug/L <0.18 1.0 07/20/17 11:290.18Tetrachloroethene ug/L <0.50 1.0 07/20/17 11:290.50Tetrahydrofuran ug/L <2.0 5.0 07/20/17 11:292.0Toluene ug/L <0.50 1.0 07/20/17 11:290.50trans-1,2-Dichloroethene ug/L <0.26 1.0 07/20/17 11:290.26trans-1,3-Dichloropropene ug/L <0.23 1.0 07/20/17 11:290.23Trichloroethene ug/L <0.33 1.0 07/20/17 11:290.33Trichlorofluoromethane ug/L <0.18 1.0 07/20/17 11:290.18Vinyl chloride ug/L <0.18 1.0 07/20/17 11:290.184-Bromofluorobenzene (S) % 89 61-130 07/20/17 11:29Dibromofluoromethane (S) % 105 67-130 07/20/17 11:29Toluene-d8 (S) % 100 70-130 07/20/17 11:29

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

1542600LABORATORY CONTROL SAMPLE:LCSSpike

1,1,1-Trichloroethane ug/L 51.150 102 70-1301,1,2,2-Tetrachloroethane ug/L 53.350 107 70-1301,1,2-Trichloroethane ug/L 48.650 97 70-1301,1,2-Trichlorotrifluoroethane ug/L 54.050 108 50-1501,1-Dichloroethane ug/L 47.950 96 71-1321,1-Dichloroethene ug/L 49.850 100 75-1301,2,4-Trichlorobenzene ug/L 42.650 85 70-1301,2-Dibromo-3-chloropropane ug/L 51.250 102 63-1231,2-Dibromoethane (EDB) ug/L 55.750 111 70-1301,2-Dichlorobenzene ug/L 50.950 102 70-130




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#=QC#



40153410023-6105-017 CP-SHOREHAM YARD


Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

1542600LABORATORY CONTROL SAMPLE:LCSSpike

1,2-Dichloroethane ug/L 48.650 97 70-1311,2-Dichloropropane ug/L 54.350 109 80-1201,3-Dichlorobenzene ug/L 49.650 99 70-1301,4-Dichlorobenzene ug/L 48.750 97 70-130Benzene ug/L 49.650 99 73-145Bromodichloromethane ug/L 50.950 102 70-130Bromoform ug/L 49.750 99 67-130Bromomethane ug/L 80.8 L150 162 26-128Carbon tetrachloride ug/L 50.050 100 70-133Chlorobenzene ug/L 50.650 101 70-130Chloroethane ug/L 51.250 102 58-120Chloroform ug/L 49.350 99 80-121Chloromethane ug/L 50.450 101 40-127cis-1,2-Dichloroethene ug/L 49.350 99 70-130cis-1,3-Dichloropropene ug/L 53.350 107 70-130Dibromochloromethane ug/L 51.450 103 70-130Dichlorodifluoromethane ug/L 28.050 56 20-135Ethylbenzene ug/L 50.150 100 87-129Isopropylbenzene (Cumene) ug/L 49.850 100 70-130m&p-Xylene ug/L 99.1100 99 70-130Methyl-tert-butyl ether ug/L 48.350 97 66-143Methylene Chloride ug/L 52.550 105 70-130o-Xylene ug/L 51.050 102 70-130Styrene ug/L 50.750 101 70-130Tetrachloroethene ug/L 46.650 93 70-130Toluene ug/L 49.150 98 82-130trans-1,2-Dichloroethene ug/L 50.850 102 75-132trans-1,3-Dichloropropene ug/L 49.250 98 70-130Trichloroethene ug/L 52.350 105 70-130Trichlorofluoromethane ug/L 52.050 104 76-133Vinyl chloride ug/L 50.450 101 57-1364-Bromofluorobenzene (S) % 98 61-130Dibromofluoromethane (S) % 99 67-130Toluene-d8 (S) % 100 70-130

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

1542601MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

40153410002

1542602

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1-Trichloroethane ug/L 50 107 70-134111 2 205012.3 66.0 67.61,1,2,2-Tetrachloroethane ug/L 50 108 70-130117 8 2050<0.25 54.1 58.71,1,2-Trichloroethane ug/L 50 104 70-130109 4 2050<0.20 52.1 54.41,1,2-Trichlorotrifluoroethane ug/L 50 110 50-150113 3 2050<0.81 55.1 56.71,1-Dichloroethane ug/L 50 106 71-13398 6 205018.5 71.4 67.51,1-Dichloroethene ug/L 50 101 75-136101 0 20504.7 55.4 55.5




Green Bay, WI 54302(920)469-2436

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#=QC#



40153410023-6105-017 CP-SHOREHAM YARD


Parameter UnitsMS

Result% RecLimits Qual% RecConc.

1542601MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

40153410002

1542602

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4-Trichlorobenzene ug/L 50 90 70-13094 4 2050<2.2 44.9 46.81,2-Dibromo-3-chloropropane

ug/L R150 99 63-123121 21 2050<2.2 49.4 60.7

1,2-Dibromoethane (EDB) ug/L 50 119 70-130118 0 2050<0.18 59.3 59.01,2-Dichlorobenzene ug/L 50 102 70-130107 5 2050<0.50 50.9 53.71,2-Dichloroethane ug/L 50 104 70-131106 2 2050<0.17 51.9 53.21,2-Dichloropropane ug/L 50 109 80-120114 5 2050<0.23 54.5 57.21,3-Dichlorobenzene ug/L 50 99 70-130105 7 2050<0.50 49.3 52.61,4-Dichlorobenzene ug/L 50 101 70-130106 6 2050<0.50 50.3 53.2Benzene ug/L 50 102 73-145105 3 2050<0.50 51.1 52.7Bromodichloromethane ug/L 50 105 70-130111 6 2050<0.50 52.3 55.3Bromoform ug/L 50 110 67-130110 0 2050<0.50 54.9 55.0Bromomethane ug/L M050 170 26-129156 9 2050<2.4 85.2 78.1Carbon tetrachloride ug/L 50 106 70-134106 0 2050<0.50 53.0 53.1Chlorobenzene ug/L 50 106 70-130105 1 2050<0.50 52.8 52.3Chloroethane ug/L 50 110 58-120107 3 2050<0.37 55.1 53.5Chloroform ug/L 50 103 80-121108 5 2050<2.5 51.5 54.1Chloromethane ug/L 50 108 40-128101 7 2050<0.50 53.8 50.4cis-1,2-Dichloroethene ug/L 50 108 70-130109 1 205015.3 69.2 70.0cis-1,3-Dichloropropene ug/L 50 108 70-130114 6 2050<0.50 53.8 57.1Dibromochloromethane ug/L 50 107 70-130107 1 2050<0.50 53.7 53.4Dichlorodifluoromethane ug/L 50 56 20-14652 6 2050<0.22 27.8 26.2Ethylbenzene ug/L 50 106 87-129106 0 2050<0.50 53.2 53.2Isopropylbenzene (Cumene) ug/L 50 105 70-130106 1 2050<0.14 52.4 52.8m&p-Xylene ug/L 100 106 70-130105 1 20100<1.0 106 105Methyl-tert-butyl ether ug/L 50 111 66-14392 19 2050<0.17 55.6 45.9Methylene Chloride ug/L 50 109 70-130102 6 2050<0.23 54.5 51.2o-Xylene ug/L 50 108 70-130105 2 2050<0.50 53.8 52.7Styrene ug/L 50 108 70-130106 2 2050<0.50 53.9 52.9Tetrachloroethene ug/L 50 105 70-130100 3 205028.6 81.1 78.4Toluene ug/L 50 104 82-131106 1 2050<0.50 52.2 52.8trans-1,2-Dichloroethene ug/L 50 109 75-135101 8 2050<0.26 54.4 50.3trans-1,3-Dichloropropene ug/L 50 107 70-130103 4 2050<0.23 53.6 51.6Trichloroethene ug/L 50 106 70-130115 7 20504.8 57.7 62.2Trichlorofluoromethane ug/L 50 107 76-150104 2 2050<0.18 53.4 52.2Vinyl chloride ug/L 50 98 56-14397 1 2050<0.18 48.9 48.34-Bromofluorobenzene (S) % 101 61-13097Dibromofluoromethane (S) % 101 67-13098Toluene-d8 (S) % 100 70-13098




Green Bay, WI 54302(920)469-2436

Page 12 of 17

#=QL#

QUALIFIERS


40153410023-6105-017 CP-SHOREHAM YARD

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.ND - Not Detected at or above adjusted reporting limit.TNTC - Too Numerous To CountJ - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.PQL - Practical Quantitation Limit.RL - Reporting Limit.S - Surrogate1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.SG - Silica Gel - Clean-UpU - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - Green BayPASI-G

ANALYTE QUALIFIERS

Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results may be biased high.L1Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0RPD value was outside control limits.R1




Green Bay, WI 54302(920)469-2436

Page 13 of 17

#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE


40153410023-6105-017 CP-SHOREHAM YARD

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

40153410001 262036071717-0800-200 EPA 826040153410002 262036SE EFFLUENT EPA 8260




Green Bay, WI 54302(920)469-2436

Page 14 of 17

Pag

e 15

of 1

7

Company Name:

UPPER MIDWEST REGION

MN: 612-607-1700 ge ..•• 1. __ ~"'

'f D/v-->'f /O Branch/Location:

Project Contact:

Phone:

Project Number:

Project Name:

Project State:

Sampled By (Print):

Sampled By (Sign):

PO#:

Data Package Options (billable)

D EPA Level Ill

D EPA Level IV

MS/MSD

Regulatory Program:

'CeAnalytical• . ,

CHA~;;; CUSTOD~ *Preservation Codes

A=None B=HCL. C=H2S04 D=HN03 E=DI Water F=Methanol G=NaOH

H=Sodium Bisulfate Solution !=Sodium Thiosulfate J=Other

FILTERED? (YES/NO)

PRESERVATION (CODE)*

Matrix Codes A=Air W=Water B =Biota C= Charcoal

_.., .. Quote#:

Mail To Contact:

Mail To Company:

Mail To Address:

Invoice To Contact:

Invoice To Company:

Invoice To Address:

Invoice To Phone: D On your sample

(billable) D NOT needed on

your sample

O=Oil S=Soil SI= Sludae

OW= Drinking Water GW = Ground Water SW = Surface Water WW= Waste Water WP=Wi CLIENT

COMMENTS LAB COMMENTS

(lab Use Only) Profile#

Rush Turnaround Time Requested - Prelims PACE Project No.

(Rush TAT subject to approval/surcharge) f AO ·\U/(.) Date Needed: ·-1 JI

Transmit Prelim Rush Results by (complete what you want): Receipt Temp= .:20-.'± Email #1: ..-J. . Dauirnme: C'! ,$

Sample Receipt pH

Fax: OK I Adjusted

Samples on HOLD are subject to

special pricing and release of liability

C019a(27Jun2006)

Daternme: Received By: Dateffime:

ot Intact

•c

of 17 Document Name: Minneapolis Cooler Transfer Checl1 List

Document Number:

Revised Date: 28Sep2016 Page 1of1

Issuing Authority: F-MN-C-214-Rev.01 Pace Minnesota Quality Office

Minneapo~is Service Center Cooler Transfer Check list

Client:

Destination Lab:

6d,<t4 /f:S0(<'af-ej

~reev7 &C><-::;

Received with Custody Seal: Yes

Custody Seal Intact: Yes No

Temp Read Corrected Temp Correction Factor

Temperature c --)0/f - iuc ·3rn IR Gun

f-.Samples on ice, cooling process has ~egun

Rush/Short Hold /J a Containers Intact: No

Re-packed and Re-Iced. ;JQ

Temp Blank Included d No

Shipped By/Date: 1-/11/(3= Notes:

of 17

Sample Condition Upon Receipt Pace Analytical Services, LLC. - Green Bay WI 1241 Bellevue Street, Suite 9

Green Bay, WI 54302

ce Analytical" ~lient Name: \?o\°'~ Courier: Fed Ex r l_!.PS - Client pace Other: cbhl t C.0 Tracking#: IL) :Z,.. ,.) t.f 9q -s:3 Custody Seal on Cooler/Box Present: pYes - no Seals intact J;?"yes

Project#:

no

Custody Seal on Samples Present: yes no Seals intact yes no

Packing Material: r Bubble Wrap !:Bubble Bags r None Other

W0#.40153410 1111111111111111 111111 40153410

Thermometer Used ~ll1fl'l S2_- 5'"8 Type of Ice:@ Blue Dry None Samples on ice, cooling process has begun

yes Cooler Temperature Uncorr: ~ /Corr: ..=,-: 'f5"' Biological Tissue is Frozen:

Temp Blank Present: .P"';es r no J(?'no Person el!,a)l)i!WIA c:;_g.q.tents:

Temp should be above freezing to 6°C. Biota Samples may be received at < 0°C. Comments:

Date: '"'111 {(' //..~/.Initials: •t '7"'.TLf

Chain of Custody Present

Chain of Custody Filled Out

Chain of Custody Relinquished:

Sampler Name & Signature on COC:

Samples Arrived within Hold Time:

- VOA Samples frozen upon receipt

Short Hold Time Analysis (<72hr):

Rush Turn Around Time Requested:

Sufficient Volume:

Correct Containers Used:

-Pace Containers Used:

-Pace IR Containers Used:

Containers Intact:

Filtered volume received for Dissolved tests

-Includes date/time/ID/Analysis Matrix:li\ \

Sample Labels match COC:

Zves ONo

efv"es ONo

~s ONo

.!:)>(es ONo

efves ONo

0Yes ~o 0Yes ~o 0Yes ~o

J'.'.]Yes ONo

£ves ONo

£s 0No

0Yes_,0No

£es ONo

ON/A 1.

ON/A 2.

ON/A 3.

ON/A 4.

ON/A 5.

DatefTime:

ON/A 6.

ON/A 7.

ON/A 8.

ON/A 9.

ON/A

;efu1A ON/A 10.

0Yes ,L21'No ON/A 11.

efves 0No ON/A 12.

All containers needing preservation have been checked. .L (Non-Compliance noted in 13.) 0Yes 0No .UN/A 13. - --- - -- --- --- --- --- --- --- - -- --- --- --...

All containers needing preservation are found to be in _/ compliance with EPA recommendation. OYes ONo )l!N/A (HN03, H2S04 ~2; NaOH+ZnAct <':9, NaOH ;:o;12) e~ptio~ ~ ~~f~~ TOC, TOXrOH,- - - - - - - - - -/- - - - - - - Initial when O&G, WIDR~. Phenolics, OTHER: )l!Yes ONo completed

Headspace in VOA Vials ( >6mm):

Trip Blank Present:

Trip Blank Custody Seals Present , A Pace Trip Blank Lot# (if purchased)·;? ~ Client Notification/ Resolution:

0Yes ONo ON/A 14.

0(es ONo ON/A 15.

£-res ONo ON/A

Person Contacted: Date/Time: ---------------------------Comments/ Resolution:

HN03 H2S04

l Lab Std #ID of preservative

NaOH NaOH + ZnAct

II Date/ Time:

If checked, see attached form for additional comments D

---------------------------------------------------------------------------------

Project Manager Review:

F-GB-C-031-Rev.04 (12Dec2016) SCUR.xls Pace Analytical Services LLC. - Green Bay WI

Date: __ -i_\ .... >§-+\-..O'------

Attachment C

FIELD INSTRUMENT pH CALIBRATION RECORDS

<9' Goldfr l\ssociates

Page _l_of_l_

Field Instrument pH Calibration Records

INSTRUMENT (MAKE/MODEL NO.) Sper Scientific/850051 INSTRUMENT NO. ____ _

STANDARD INFORMATION

Project Number: 0236105017 Project Name: GP-Shoreham Yard

Standard Vendor: Field Environmental Instruments

Prepared Date: NA Where Prepared: ______ N_A

Purchase Date: 1 ·~ ~~ '1!!©$6 Expiration Date: Varies Grade: NIA Units: Standard Units

Standard

Standard

Standard

4.0 (@25 °c 7.0 (@25 °c 10.0 (@25 °c

DATE TIME TEMP (mm/dd/yy) (hr: min) DEGC

)flr//7 f 5~3 2-1-. ~

~/'f (/7 1 ]'( 7 2-L.O

) //j/(7 / 311 l..L.f

G iti111 l l.(5~ ~~ .D

~· · 1(/D f·Vf.f7 b~. s-I

r (5/(J t1ot 2-1.5 b1 ... , . -

?Jf7/17 t6n Lt.O 1ff7iil l 6 '2-,l. 2-.?, f

7 //7/17 l6L-7 , )_?~o 7 /Vt/17 r 13i ~ .~ . 1/1/\{/) l !f'1 Sl 12._ l..O

1 /L'-t/11 ~,, ~(,~

-

Lot# F158-18 Ex~ Date

Lot# F172-18 Ex~ Date

Lot# G030-04 Ex~ Date

STD INSTRUMENT VALUE RESPONSE

7~0 7.o 4.0 '1 . 0

lo. o (0. 0 7-,;0 -z~o

ttvO '-l, 0

f o.o l ()l 0 7,0 7, ()

l( e-0 ·l.L-O tcr>,o ltJ~O 7~-1l 7.?'l I .. CJ 'i .-'t> L,~ , cJ /Or a

06/14/18 Purchased 11 /17 /2016

06/29/18 Purchesed 11/17/2016

02/01/18 Purchased 05/11/2017

%DEV PASS/ CALIBRATED SAMPLER FAIL (YES, NO) INITIALS

0 p y 4/ 6 ? V"' 41 \

CJ ) ·y Jf 0 ~ y !IP CJ p ~ .H

0 e '1 H 0 p y H (j f

. l ;f;P

0 p I ~/) ~ p \ Af 0 p ~ ASf a t '1 .t-O

Acceptable calibration check is if the meter reads within +/- 0.2 pH units of the value of appropriate calibration standard.

\\MIN 1-V-FS 1 \Projects\Golder Projects\023 PROJECTS\023-6105 Shoreham Yard File Review\East Side Southeast P&T System\Data\2017\pH_ Calibration Form.doc

Golder Associates REV-2-03107

re: july 2017 sampling results smr industrial … · industrial waste division ... enclosed is the...

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