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TRANSCRIPT
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T T"i'A ' ' •• ' ' '-I I""! Z\ . Post Office Box 12846 Phone 919-677-0090•*• -J* •*• Research Triangle Park, NC 27709 Fax 919'677-8702An Aquarion Company .
SDG Narrative
Case: 18832 , Contract: 68-DO )156
SDG No.: CDS76 }• Samples: 3 soils & 2 waters
The SDG includes samples CDS76 - CDS80. The samples were received in good condition onSeptember 30, 1992.
' . ' ' ' • . ' • 'Page one (1) of the Narrative section contains general comments and the sign off signature ofthe SDG and page two (2) contains comments concerning the Volatile analyses.
I certify that this data package is in compliance with the terms and conditions of the contract,both technically and for completeness, for other than the conditions detailed above. Release ofthe data contained in this hardcopy data package and in the computer-readable data submitted onfloppy diskette has been authorized "by the Laboratory manager or designee, as verified by thefollowing signature.
Lina F. MitchellDirector, Technical Support ServicesNovember 2, 1992
Monroc' Sunrise, . Schaumbuns. : riBilierica, Whippany, Essex Junction.Connecticut Florida Illinois Massachusetts New Jersey Vermont203:261-4458 305-846-1730 708-705-0740 617-272-5212' 201-4288181 802-878-5138
AR30Q39»4
TT7 A SDG Narrative Volatile FractionIJCi/VAn Aquarion Company , . , ~
CASE: 18832 ' SDG NO.r COST6 CONTRACT:68-00-0156
Thera is an air peak that is common to all of the volatileanalyses that is present at the beginning of some of theReconstructed Ion Chromatograms (RIC). The raw data for a fewvolatile samples have a Lab File ID.that exceeds seven digits.This.occurred when the autosampler was utilized. The forms listthe first seven digits, a period, and the extension. The GAS ,numbers on the Form I-TIC for yolatiles.do not include dashes.
Sample CDS?S matrix spike duplicate was analyzed one day outof contract required holding time, on the eleventh day from validatedtime of sample receipt (VTSR) due to instrumentation problems. ' Thesample was analyzed 1 hour after midnight on the tenth day from,VTSR. . ; . . . " . ' " . ' • . . . ' . • - ' . •
A copy of tha ISA internal chain of custody for each sampleaccompanies the case. Original chain of custody for each samplewill follow upon sample disposal.
I certify that this data package is in compliance with the 'terms and conditions of the contract, both technically and forcompleteness, for other than the conditions detailed- .above.Release of the data contained in this hardcopy data package andin'the computer-readable data submitted on floppy diskette hasbeen authorized by the Laboratory Manager or designee, as ''verified by the following signature.
H '.'•( asffaDawn A. CastoGC/MS Data Review Supervisor'
11/02/92
AR300395
4AVOLATILE METHOD BLANK SUMMARY
VBLK5Btab Name: INDUSTRIAL & ENVIRONMENTA Contract: 68-DO
Code: IEA Case No.: 18832 SAS No.:
Lab File ID: 1010E02.D Lab Sample ID: VBLK5B
Date Analyzed: 10/10/92 Time Analyzed: 1957
GC Column:DB-624 . ID: 0.53 (mm) . ' , ' . ' Heated
EPA SAMPLE NO. I
Ofi/G,,
SDG No.: CDS76
Purge: (Y/N) Y
THIS 1
01020304050607
, . 08•\ s: ' 09
1011• . 12
131415
„ ..... ig1718192021222324252627282930
' "MMENTS:X*
i . ' • • ' •'.••. ''"".'• ^METHOD BLANK APPLIES TO THE FOLLOWING SAM
EPA ,SAMPLE NO.
CDS78CDS77CDS76CDS76HSCDS76MSD
.... ..,_ ..... » — .......',
. . . ' • ' !ii'
, ' i .• ' ' : *
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LABSAMPLE ID
92097940392097940292097S4019209794 DIMS9209_79401MSD:;
. -.._ ,._.:-. ...
- .. ..... •.. . .......... . . •.'......... _,.... .... .
- ————————————— : —
• ' ' , - • ' •
. • "-..:
1 . ' . *« '. . •
LABFILE ID
1010E04.D1010E07010071010E08010081010E09010091010E1101011
•-.''-. . . _..... -
i
— .... ..._... — — . —
' ' ...•,>•. - ". ', ' '
~~ • ' ' • . ' ' • : ' - ' •' • - • ' ' ' . ' . - ' . . - " , '
PLES, MS AND MSD
.D
:S.p
---}-
• —
TIMEANALYZED
21122248231823520101
. . , . . .
~
*
'•'.-•;.-: •
.-.. -• - .••• .. -'
1 004. i ' •
page 01 of 01 AR3D0396I
4A • . •VOLATILE METHOD BLANK SUMMARY
Lab Hamas INDUSTRIE, & ENVIRONMENTA Contract: 68-DO
Lab Code: IEA Case No.: 18832 SAS No.:
.ORiC. EPA SAMPLE NO.
-0156VBLKJ1
. ' . . ' i • . • . : - • , ' ' • ' • - .Lab Pile ID: 10061002.D Lab Sanple ID: VBLKJ1
Date Analyzed: 10/06/92 Time Aaalyzed: 0953
GC'Column:DB-624 | ID: 0.53 (mm) Heated Purge: (Y/N) N
Instrument ID: MSD10i,. - . ' • • • ' ' • ' • i
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD
0102030405
^ 06070809101112131415
._.. ...— is1718192021222324252627282930
COMMENTS:
. - . . . • • i • ' • ' • ' - . . . - ,. • - j .;•••.-..:.--. • .................EPA
SAMPLE NO.
CDS79CDS80
• • • .
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LABSAMPLE ID
920979404920979405
, .- ..._. ._ .
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1
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LABPILE ID
100610401004100610501005
...... .:..- •
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• - . ' ' . ' . ' ' ' • • ' ' ' "
' . . ' • • . • •; • . ' : • . ". , ' ' ' • " , B Dpage 01 of 01 ; Hn
.D
.D
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TIMEANALYZED
11181151
—————— .. -,. ——— . ——
*
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1
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300397
1SDG No.: CDS?6 A—
iiM33
'1• -*
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I
VOLAT:
Lab Name: INDUSTRIEV • -
J&> Code: IEA
Matrix: (soil/water, -
Sample wt/vol:
Level: (low/med)- - - •. , _ !
% Moisture: not dec.
[LE ORGANICS ANALYSIS DATA
j & ENVIKONMENTA Contract
Case No.: 18832 SAS No.
SOIL" ' ; ' • ' - < • • ' "
5.0 (g/mL) G
LOW
.-16 ,'. .-,.' .' "-;. : •-. '•/ '
SHEET
: 68-DO
:•Lab Sa
Lab Fa
Date R
Data A
(1
-0156
sinple :
Le ID
eceiv<
ialyz<
SDG No.: CDS76
ID: 920979401
1010E0801008.D
: 09/30/92
lalyzed: 10/10/92
GC Column:DB-624 j ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(mL) Soil Aliquot Volume: (uL)
CONCENTRATIOH UNITS:GAS NO. : COMPOUND (ug/L or ug/Sg) UG/KG Q
74-87-3 ——————
75-01-4 ——————75-00-3 ——————
67-64-1 ——————•7 C 1 C A
75-35-4 ——————f J^J^" l^~t m—mm~~~~
67-66-3 ——————107 06-2 —————«7o o o "aT 1 C C C.'
56-23-5 ——————/ 3 4, i — '^— — •"—'—'— -•tti' Ot K
10061-01-5 ———TO n i c124-48-1 —————79-00-5 ——— ——•71 At 1
10061-02-6— r—
co 1 to et '127-18-4 ——— 4---79-34-5 ——— 4.—i nc_pn _^____2.__
100-41-4 —— ^—«100-42-5 ——— •- — •1330-20-7 —— f —
!
-Chlorome thane-Bromomethane-Vinvl Chloride-Chloroethane-Methylene Chloride-Acetone . . . ' . • •-Carbon Disulf ide-1 , 1-Dichloroethene-1,1-Dichloroe thane-1,2-Dichlbroethene (total) _-Chloroform-1 , 2-Dichloroethane-2-Butanone-1 , 1 , 1-Trichloroe.thane-Carbon -Tetrachloride-Bromodichloromethane-1 , 2-Dichloropropane-cie-1 , 3-Dichloropropene-Trichloroethene-Dibromochloromethane-1,1,2 -Trichloroethane-Benzene-trans-1 , 3-Dichloropropene-Bromoform-4-Methyl-2-Pentanone-2-Hexanone-Tetrachloroethene-1,1,2 , 2-Tetrachloroethane __-Toluene-Chlorobenzene-Ethylbenzene-Styrene-Xylene (total)
( . . . - • • - . - . • • . • •• . • • • ' ' • I - : . . ' ' . . ' ' . " : ' • ' • ' ' " . ' . • •
121212121215121212121212121210- — - j./12121210012121212121212121212121212
• 12
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SAMPLE NO.(RED
CDS76
fiR3C0398
VOLATILE ORGANICS ANALYSIS DATA ,TENTATIVELY IDENTIFIED COMPOUN]
Lab Name : INDUSTRIAL & ENVIRONMENTA Contract :
Lab Code: IEA • Case No. : 18832 SAS No.:
Matrix: (soil/water) SOIL ]
Sample wt/vol: 5.0.(g/mL) G ]
Level: (low/med) : LOW ]' '• . • • .' ' • i ' . ': •• . '% Moisture: not dec; 16 » . -•- . : 3
. , i - ' : - - , -
GC Column :DB-62 4 ID: 0.53 (mm) 3
Soil Extract Volume : (uL) i
- - . ' . ' . , _ -CONCENTNumber TICs found: 1 (ug/L <
GAS NUMBER
i.2.3.4.5.6.7.,8.9.10.11.12.1 A J •
14.15.16.17 .18.19.20.21.22 .23.24.25.25.27.28.29.30.
I. . ; COMPOUND NAME
Unknown --, . ; . . . . •
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Date R
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19.
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Lved: 09/30/92 1
zed: 10/10/92 i
Factor: 1.0 i
lot Volume: (uL) •
JITS:UG/KG
EST. CONC.
37
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Matrix : ( e oil /water
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Level : ( low/med )
% Moisture : not dec ,f ' : . - • ' • ' • .
GC Column :DB-624
Soil Extract Volume:
' - •- 1A :' : .'•:LE ORGANICS ANALYSIS DATA
j & ENVIRONMENTA Contract:
Case No.: 18832 SAS No.:
SOIL
5.0 (g/mL) G
LOW . 1
ID: 0.53 (mm). . . • . . ,.• • . . _ _ . . - ,
|TT\Ti J • ' ' >
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6 8 -DC
Lab Sa
Lab Fa
Date B
Data A
Diluti
Soil. A
OIiIGln-i EPA SAMPLE NO. \(RFD) •)
CDS77 1-0156 \
SDG No.: CDS? 6 '
nple ID: 920979402
Le ID: 1010E0701007.D
sceived: 09/30/92 "
lalyzed: 10/10/92
on Factor: 1.0 . •-.
Liquot Volume: (uL) ]• • . - . • • - i -
Extract Volume:
CAS NO.
74-87-3 —————
75-01-4 ———— —75-00-3 —————75-09-2 ———— T-67-64-1-— ———75-15-0 ——— 7—75-35-4 —————75-34-3 —————540-59-0 ————67-66-3— ———' 1 rt T A f O
71-55-6 —————56-23-5 —— i~—75-27-4-— — r-78-87-5 —— t—^-10061-01-5— f-•7 o_m _£_______124-48-1 ——— —TO nn K. 'nA 1 t '
10061-02-6— ••-•v f ^ p ^ I75-25-2—— — T-eo 1 _ *7O_ £__ __ |L _
100-41-4 ——— •!•-
1330-20-7 —— --1 ,•
• • ' ' i
. i
•v
(mL) • . "... • Soil J. - • -• • " . " . - . . - • • . • • . —..--...-
CONCENTRATIC. COMPOUND (ug/L or ugy
— -Chloromethane— Bromomethane• — Vinyl Chloride: — Chloroethane— Methylene Chloride—-Acetone - — . - - .— Carbon Disulf ide -— 1 ,1-Dichloroethene-r 1 , 1-Dichloroethane— 1,2-Dichloroethene (total), _—Chloroform—1,2 -Dichloroethane— 2-Butanone .—1,1, 1-Trichioroethane—Carbon Tetrachloride" ~ " '--Bromodichloromethane— 1,2-Dichloropropane—cis-1 , 3-Dichloropropene
X JL XWltXUJ. UC l*lJdJ.C
— Dibromochloromethane--1,1, 2-Trichloroethanej>onz6H6 . -
--trans-l , 3-Dichloropropene— Bromof orm ,— 4 -Methyl-2 -Pentanone— 2-Hexanone— Tetrachlorbiethene— 1,1, 2 , 2-Tetrachloroethane __• — Toluene—Chlorobenzene ' . . , - - .• — Ethylbenzene
w ** jf *• ** * _.__— Xylene (total)
. • . • •
AR30
Liguot Volume
H UNITS:Kg) UG/KG
121212
_. _ 1212
12121212
141212
. .. 1212
...L. _....:.,__ 122112121212121212121212121212
• 12
: (uL)
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VOLATTEN1
Lab Name: INDUSTRIE
Lab Code: IEA
Matrix: (soil /water
Sample wt/vol:
Level: (low/med)
i Moisture: not dec
3C Column:DB-624
Soil Extract. Volume
Number TICs found:
. CAS NUMBER
1. 1239112. 556672
.••3. ' '• .'4. '.5.6.7.8.9.10 .11.12.13. _14.1 5 . . . • - • -16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
• --• .. ' IE :ILB ORGANICS ANALYSIS DATAPATIVELY IDENTIFIED COMPOUN]L & ENVIRONMENTA Contract:; i .' Case No. : 18832 SAS No. :
( SOIL . :
5.0 (g/mL) G ]
LOW ' . , , ' • ' • . ]
,".•16. -.-.-.:.-. ..'.'. ' ; "-• , 3
ID: 0.53 (mm) J
(ui) ; {- ' ' . CONCENT
3 (ug/L <
\ COMPOUND NAME
103Ul
p4-Dioxaherclotetrasiloxane , octamethyiknown - ".".-,' .'. ":".:; "~"-'~'~::~ :.: .
..._..._ .. . . . ,
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SHEETDS '
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Date R
Data A
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rRATIOar ug/
RTS5SSSS5SS*
12.18.22.
. . -
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SDG No.: CDS76 'vs :
s ID: 920979402
ID: 1010E0701007.D
Lved: 09/30/92
fzed: 10/10/92
Factor: 1.0 ;
lot Volume: (uL) ;
1ITS:UG/KG
EST. CONC.
2026
••::•.: : : 78: " • • - • - • • '
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(RED!CDS78
Name: INDUSTRIAL & ENVIKONMENTA Contract: 68-DO-015G
Code: IEA Case No. : 18832 SASNo.: SDGNo.: CDS 7 6' • ' • ' • • • . " ' ' - . ' ' ' • • . ' . . - • : '
Matrix: (Boil/water) SOIL Lab Sample ID: 920979403
Sample wt/vol: 5.0 (g/mL) G Lab File ID: 1010E04.D
Level: (low/med) LOW Date Received: 09/30/92
% iioieture: not dec. 14 Data Analyzed: 10/10/92
GC Column :DB-624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _ ___ _(mL) Soil Aliquot Volume: ,J
" - CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG
•7 * C*7 '"S
74-83-9 ———75-01-4 ———75-00-3 ————
67-64-1 ———— •75-15-0-p*- —— •75-35-4 ——— •75-34-3 ———— •540-59-0 ——— •67-66-3—— T-107-06-2 ——— •«yp_o^«'S •••••.
71-55-6 ——— •cir_<>'a^c_____.75-27-4 ———— ••7 O_O •!_£_____.
10061-01-5—79-01-6 ——— •124-48-1——79-00-5 ——— •71-43-2 ——— •
-—— Bromomethahe— — Chloroethane— —Methylene Chloride
— — 1 , 1-Dichloroethane
-——Chloroform— -1 i 2-Dichloroethane
— — 1 , 1 , l-TricKloroethane—— Carbon -Tetrachloride ————
•---I., 2 -Dichloropropane— — cis-1 , 3-Dichloropropene-r— Trichloroethene "-—— Dibromochloromethane•—— 1 , 1 , 2-Trichloroethane- — 'Benzene
10061-02-6 ———— trans-1 , 3-Dichloropropene
108-10-1 ——— •C0 1 —TO _£____.
127-18-4 ——— •79-34-5 ——— -108-88 3 ——— •
100-41-4 —— -100-42-5 —— -1330-20-7 —— •
—— 4 -Methyl-2 -Pent anone•—— 2-Eexanone•« — Tetrachloroethene— — 1 ,1,2, 2-Tetrachloroethane __——Toluene
Ci Ulijr XA^wIl ACllC
—— Styrene.——Xylene (total)
~
1212121212221212121212121012- . . ' . - i < j._. . — .— .-........±£121212..... ......... .. 12121212121212121212121212
. . 12
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• IE . • ' .'. .VOLATILE ORGANICS ANALYSIS DATA,TENTATIVELY IDENTIFIED COMPOUN
Lab Name: INDUSTRIAL & ENVIRONMENTA Contract:
Lab Code: IEA Case No. : 18332 SASNo.:
Matrix: (soil/water SOIL :f - , ;. . " " , • ' • ' .
Sample wt/vol: 5.0 (g/mL) G ]
^Levels (low/med) LOW "V ]
..% Moisture: not dec 14 . ]
GC Column: DB-624 ID: 0.53 (mm) _ ]
Soil Extract Volume: (uL) J
! ; . CONCENTNumber TICs found: ; 3 (ug/L <
CAS NUMBER
1. 1239112. 5566723.
' 4.5. - •- -- • -•.•-6.7.8.9.10.11.12.
: 13. ..14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
COMPOUND NAME
1,4-DioxaneCyclot e trasiloxane , octamethyUnknown " '"'.:'
- ; . . . . . . . . . . . . . . . . .
. . :
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SHEETDS
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ID: ' 1010E04.D
ived: 09/30/92
yzed: 10/10/92
Factor: 1.0
not Volume: (uL)
HITS:UG/KG
EST; CONC.
25U10
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Lab Name: INDUSTRIAL £ ENVIRONMENTA Contract: 68-DO
Code: IEA
Matrix: (soil/water
Sample wt/vol:
Case No.: 18832 SAS No.:
WATER Lab Saaple ID: 920979404
5.0 (g/mL) mL Lab File ID: 100610401004.D
»(]//«', EPA .SAMPLE NO.
-0156CDS79
SD6 No.: CDS?6
.Level: (low/med) | LOW \Date Received: 09/30/92
% Moisture: not dec! _________ : Data Analyzed: lo
GC Column:DB-624 ID: 0.53 (mm) Dilution Factor: 1.0- " • . .i . . ..•./; 'i' -.
Soil Extract Volume: __________(uL) Soil Aliquot Volume: ;___(uL)I -' '.' -"•'.. " ' • - . - ' •;• - •
I CONCENTRATION UNITS:CAS NO. ' COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3 ———— ——74-83-9 ——————75-01-4 ----- ——75-00-3 ——————«7C_ A Q_0 _________
67-64-1 —— - ———75-15-0- ——— --75-35-4 —————— •75-34-3 — —— ——540-59-0 —————ei—cc—t __,_.___'__.107-06-2 —————
71-55-6 ---—— —56-23-5 ——————
1 f*r e o *r jt
78-87-5— —— ---
-Chloromethane-Bromomethane-Vinvl Chloride-Chloroethane-Methvlene Chloride«4ww L Uilw -- - • •
-Carbon Bisulfide .-1 , 1-Dichloroethehe-1 , 1-Dichloroethane- 1 , 2-Dichloroethene (total ) .-Chloroform-1 , 2-Dichloroethane-2-Butanone-1,1, 1-Trichloroethane—Carbon - Tetrachloride - — — - —-Bromodichloromethane-1 , 2-Dichloropropane
10061-01-5 — r— • 'Tcis-l,3-Dichloropropene
124-48-1- —— r—79-00-5 ———— f—•7 « - M •% A '
10061-02-6— p—• *J £•** m* ;i nfi_i n_i __._!.__591-78-6 ——— f—ml O 4 ••« f\ M g p * ' 1
1 OC.RP_?_>__1.__
108-90-7 ——— f—100-41-4 —— -----100-42-5— —— .—
-Dibromochloromethane- 1 , 1 , 2-Trichloroethane-Benzene-trans-1 , 3-Dichloropropene_ __— Bromoforoi '-4 -Methyl-2 -Pentanone-2-Hexanone
•L ti L»JLciwIlXO^ Ocl liCllC
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1330-20-7 ————— Xylene (total)
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1.2.3.4.5.6.7.8.9.10.11.12.13. - ..... :..-...
, 14*15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
. - IE . V ' 'MILE ORGANICS ANALYSIS DATA .BNTATIVELY IDENTIFIED COMPOUN]
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Case No.: 18832 SAS No.:
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j & ENVIRONMENTA Contract:
Case No.: 18832 SASNo.:
WATER
5.0 (g/mL) mL
LOW•' . "'"'.•'• -. • • '
% Moisture: not dec.
GC Column :DB-624 ID: 0.53 (mm)
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UNITS:Kg) UG/L Q
74-87-3 — — ——
75-01-4 —————75-00-3 — —— —75-09-2 —— ———67-64-1 ----- —75-15-0^ ——— —•1C ^ C Jt '
75-34-3 ———— -
67-66-3 —— -——107-06-2 ————"7 C_Q1 _•)_______
71-55-6 —————56-23-5 —————» *^ «• • Tt*t Q ty t? • • '
— Chloromethane— Bromome thane— Vinyl Chloride— Chloroethane— Methylene Chloride— Acetone— Carbon Disulfide--1 , 1-Dichloroethene— 1 , 1-Dichloroe thane--1,2-Dichloroethene I total)—Chloroform—1,2 -Dichloroethane— 2-Butanone— 1 ,1 , 1-Trichloroetbane—Carbon Tetrachloride— Bromodichloromethane— 1,2 -Dichloropropane
10061-01-5 — - —— cis-1, 3-Dichloropropene
124-48-1 —— ——79-00-5 — — ——
10061-02-6 ———75-25-2 ——— •-108-10-1 ——— •-
' C 0 1 1 0 C.
127-18-4 — — —79-34-5 —————m_ep_O______
100-41-4 —— «—100-42-5 ——— •-
• — Trxcnioroetnene— Dibromochloromettiane—1,1,2 -Trichloroethane— Benzene• — trans-1 , 3-Dichloropropene __ _— Bromof orm— 4 -Methyl-2-Pentanone— 2-Hexanone
J. *S i clwIlJLU Qc L»il6X16—1,1,2, 2-Tetrachloroethane __
x(J Uw<ll6 • . • • -
— Chlorobenzene— Ethylbenzene— Styrene— Xylene (total)
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Lab name: INDUSTRIAL S ENVIRONMENTA Contract:
Lab Code: IEA ' Case No. : 18832 SASNo.:- . ' ' . • ' " - . -
Matrix: (soil/water WATER :- . ' ' • • •' . :. • '• {
Sample wt/vol: 5.0 (g/mL) mL , ]
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GAS NUMBER
1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
, COMPOUND NAME
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CAS NO.
74-87-3 ———— -74-83-9 ——— -75-01-4 ——— —75-00-3 ————75-09-2 ———— -67-64-1 ———— -75-15-0 ———— -75-35-4 ————75-34-3 ————
67-66-3 ————107-06-2 ———
71-55-6— ——56-23-5— ——*7 C ** *9 A '
10061-01-5 — i
124-48-1 ——— •nK O 1 '
10061-02-6 ——/ «J A«J «• j
108-10-1- —— TKOI —TO £___!.!
127-18-4 ——— ••
• • ' 1A.'1. :' "••"••• " ' " ':LE ORGANICS ANALYSIS DATA SHEET
< & ENVIRONMENTA Contract: 68-DC
Case No.: 18832 SAS No.:• • . *
SOIL Lab S«
5.0 (g/mL) G Lab Pi
LOW ; ••/;_.•;;. Date I
0 - . Data t
ID: 0.53 (mm) Diluta
-• (mL) Soil f
, CONCENTRATICCOMPOUND • (Ug/L or ug/
—— Chloromethane—— Bromomethane. —— vinvl Chloride
— — Methylene Chloride•——Acetone• — -Carbon bisulfide• — - 1 , 1-Dichloroethene— — 1,1-Dichloroethane *• —— 1,2 -Dichloroe t hene ( total ) _ _
— — 1 , 2-Dichloroethane— — 2-Butanone— — 1,1, 1-Trictiioroethane•• — Carbon Tetrachloride -- --— - -----
• — -1,2-Dichloropropane— -cis-1 , 3-Dichloropropene .• —— Trichloroethene• —— Dibromochloromethane—— 1,1, 2-Trichloroethane
— - — 4 -Methyl-2 -Pentanone—— 2-Hexanone.. —— Tetrachloroethene
100-41-4 ——— -100-42-5 ——— r1330-20-7 —— 7
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-— Chlorobenzene—— Ethylbenzene—— Styrene .
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Number TICs fount
GAS NUMBER
1*2.3.4.5.6.7.8.9.10.11.12..13.14.15.16.17.18.19.20..21. .22.23.24.25.26.27.28.29.30.
IEATILE ORGANICS ANALYSIS DATAENTAT VELY IDENTIFIED COMPOUN
IAL & ENViRONMENTA Contract:
Case No. t 18832 SASNo.:
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5.0 (g/raL) G :
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SC. ; 0 .- :-.;-•;--..•.:•;• /—rrr;: •••..:••:• -.. . ..v.r- 3
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CAS NO.
' • 1A - '. .' -;" 'ILE ORGANICS ANALYSIS DATA
j & ENVIRONMENTA Contract:
Case No.: 18832 SAg No.:
WATER
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N UNITS:Kg) UG/L Q
74-87-3 —————•JA _O 1_Q_______
75-01-4 —————75-00-3 —————•j c_no_ i— J. ______67-64-1 —— ———75-15-0 —————75-35-4 —————fm f ' *% * •%75-34-3 — • — ——540-59-0 ————67-66-3 —————107-06-2 —— ——
71-55-6 —————ee"_O'3_e_______
75-27-4 ———— 4--*7G_C*7_C____ : _
10061-01-5—7-•7 A _ /\ »_!;_____'_
124-48-1 ——— f-•V 4 • Jt 1* f\ ' • 1
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108-10-1 ——— f-591-78-6 ——— }-127-18-4 ——— •!•-infi_QQ_*3____^_1 AO_QA_«7____1._
100-41-4 ——— --100-42-5 —— --1330-20-7 —— --i .
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— Chloromethane— Bromome thane—Vinyl Chloride— Chloroethane— Methvlehe Chloride/icev.oue
— Carbon Disulf ide— 1 , 1-Dichloroethehe— 1,1-Dichlbroethane— 1,2-Dichloroethene (total) _—Chloroform-r 1 r 2 -Dichloroethane— 2-Butanone• — 1 1 1 1 1-Trichloroethane— Carbon -Tetrachloride -— Bromodichlorome thane—1,2 -Dichloropropane— cis-1 , 3-Dichloropropene— Trichloroethene— Dibromoqhloromethane— 1,1,2-Trichloroethane—Benzene .--trans-1 , 3-Dichloropropene __— Bromoform— 4-Methyl-2-Pentanone— 2-Eexanone— Tetrachloroethene— 1,1,2 r 2-Tetrachloroethane—Toluene— Chlorobenzene— Ethylbenzene— Styrene— Xylene (total)
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Lab Code: IEA Case No.: 18832' SASNo.:
Matrix: (soil /water WATER Lab Sa
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GAS NUMBER
1.2.
"3. ' . '4.
•— 5 . -• •6.7.8.9.10.11.12.
_13. •_ ••' . -.• ... ........ ....14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
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CAS NO.
/ -
•-.
74-87-3 ———— -74-83-9 ————75-01-4 —— ——75-00-3 ————75-09-2 ——— •67-64-1 ————75-15-0-———75-35-4 ————«H •> «% M 0%
540-59-0 ———C.1 C.C. 1
107-06-2 ——— r78-93-3 -----71-55-6— —— --56-23-5 ————t C O™' Jt
*7 O_C*7_C ______
10061-01-5 ——79-01-6 ———— T124-48-1 ——— t*T ft ft ft f? '
71-43-2 ———— \10061-02-6—-T7C 1C 1
- . ' : , ,
rORGANICS ANALYSIS DATA SHEET•>• : •• '••••[, & ENVIRONMENTA Contract: 68-DC
Case No.: 18832 SASNo.:
SOIL Lab S«
5.0 (g/mLJ G Lab FJLOW : _ .Pate I
"16 -""*"---:-. .. ._. . :.Data I
ID: 0.53 .(mm) Dilutd
(mL) .» J SOJL! 1
CONCENTRATICCOMPOUND (ug/L or ug/
•—— Chloromethane
. —— vinyl Chloride— — Chloroethane— — Methylene Chloride
* A.AGGtOriG ^ - - .
—-Carbon" Disulfide• — -1,1-Dichloroethehe— — 1,1-Dichloroethane .—— 1,2-Dichloroethene (total) _• —— Chloroform• — —1,2-Dichloroefhane—— 2-Butanone .——1,1, 1-Trichloroethane•—— Carbon -Tetrachloride - — —— -• —— Bromodichloromethane
-->• — ci6-l,3rDichloropropene•—— Trichloroethene— -Dibromochloromethane—— 1 , 1 , 2-Trichloroethane—— Benzene—— trans-1 , 3-Dichloropropene __
108-10-1 ——— TCO 1 TO £ '
127-18-4 ——— •
— -4 -Methyl-2 -Pentanone• — -2-Hexanone—— Tetrachloroethene
1 t *1 *O m««4-«M*h^»l. l M.»I*_M j* w _«L^k
100-41-4 — ——100-42-5 ——— f
• ;•
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—— Styrene—— Xylene (total)
ORIGINAL(RED)
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09/30/92
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74-87-3 ——— -74-83-9 ——— -•TC A1 4
75-00-3 ——— -75-09-2-———67-64-1 ——— -75-15-0 ——— -75-35-4 ——— -75-34-3 ——— •540-59-0 ——— •67-66-3 ——— -107-06-2 ——— •*7Q_Q "}_•}_____.
71-55-6— —— •56-23-5 ————75-27-4 ————78-87-5— --T10061-01-5 — I79-01-6-———
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• 1A . .CLB ORGANICS ANALYSIS DATA SHEET
i & ENVIRONMENTA Contract: 68-DC
Case No. : 18832 SAS No. :
SOIL Lab Sa
5.0 (g/mL) G Lab Pi
LOW . _ _'..'; ...._Pate r, -.16 --•--r~ r :.-r ::::--.::;-r--T--7r-t--: ~---Data I
IDs 0 . 53 ; (mm) ;.;_ ;f 1, ;J Diluti, _., ,.v , .,.,_ . ^ j- -r-: ••-..?• .r,--; r-1 soil J
•"'•T. •' " ' '' CONCENTRATICCOMPOUND (ug/L or ug/
— — Bromomethane• —— Vihvl Chloride— — Chloroethane < ' .• —— Met hylehe Chloride• —— Acetone ~. . ..:-•...• —— Carbon Bisulfide ~ ; : : : ;: : :
— — 1 , 1-Dichloroethane• — — 1,2-Dichloroathena (total]• — ;-Chlorofonn• — — 1,2-Dichlorbethane ~ -
• — — Carbon -Tetrachloride ——— — -
—— 1 , 2-Dichl6ropropahe -. —— cis-1 , 3-Dichloropropene—— Trichloroethene -• — -Dibromochloromethane— — 1 , 1 , 2-Trichloroethane
• — -4-Methyl-2-Pentanone—— 2-Hexanone
XcioJ^clwilJiU^WUUilciics •
• — 1,1 , 2 , 2-Tetrachloroethane __AUJLUBilQ
—— Chlorobenzene r- — Ethylbenzene—— Styrene—— Xylene ( total )
AH300«i
, EPA SAMPLE NO.ORIGlNfei(RED) CDS76MSD
1-0156 1\ .
SDG No. : CDS76 \ >
tnple ID: 920979401MSD
.Le ID: lOlOEHOlOllio
teceived: 09/30/92 ;lalyzed: 10/11/92 : - ~ ^ r
on Factor: 1.0
liquot Volume: ' (uL) .
S UNITS: -Kg) UG/KG Q
12121212
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