references [1] geim ak and novoselov ks, “the rise of graphene”, nature materials,...

1
References [1] Geim AK and Novoselov KS, “The rise of graphene”, Nature materials, 2007,6,183-191. [2] Youngbin Lee, Sukang Bae, Houk Jang, Sukjae Jang, Shou-En Zhu,Sung Hyun Sim, Young Il Song, Byung Hee Hong, and Jong-Hyun Ahn ,“Wafer-Scale Synthesis and Transfer of Graphene Films” , Nano letters, 2010, 10, 490-493. [3] John A. Rogers,Takao Someya and Yonggang Huang,“ Materials and Mechanics for Stretchable Electronics”, Science, 2010, 327, 1603-1607. Acknowledgement The authors are grateful to the Center for Nano Science and Engineering (CeNSE), IISc, Bangalore, for providing the Characterization facility. Also we would like to thank Mr. Sankaran and Veera Pandian for their kind help in testing of the device as well for supporting necessary electronic circuitry. Introduction Graphene: Carbon class of 2D sheets with honey comb lattice structure. Possess unique properties such as structural, optical, thermal, mechanical and electrical properties. Wide range of applications are found in energy, electronics and sensors. Strain Sensor challenges: Adhesion Fixed directional Low resolution at nanoscale Integration of structural materials Our interest of present work Fabrication of Highly flexible, High resolution, Integrated and sensitive graphene– silver nanocomposite based strain sensor. Conclusions The RGO nanosheets were successfully synthesized by using modified Hummers method. The piezoresistive nanocomposite based strain sensor was fabricated using RGO and Ag nanoparticles. The fabricated nanocomposite strain sensor exhibits a gauge factor of about 9 to 12. It can also be used for chemical, biological and vibrational, sensor applications. Material synthesis and characterization . Sensor/Device fabrication Results Gauge factor(G.F)= (∆R⁄R) /ε Principle: Piezoresistive Fabrication of nanocomposite Strain Sensor Mechanical mask preparation with stainless steel for micro mold structural patterns. Prepared RGO-Ag nanocomposite solution was drop casted on kapton substrate. Annealing process at 80 °C for 1 hr. Electrodes preparation process . AbstractWe are reporting, a novel reduced graphene oxide (RGO) and silver (Ag) nanocomposite based piezoresistive thin film sensor realized on kapton (polyimide) membrane by drop casting method for strain sensing applications. Incorporation of small quantity of (Ag) fillers into RGO can create a novel nanocomposite with improved structural and functional properties. The as- synthesized RGO and nanocomposite were characterized using X-ray diffraction (XRD) & field emission- scanning electron microscope (FE-SEM) for their structural properties and morphology analysis. Fabricated nanocomposite strain sensor undergoes piezoresistive behavior when mechanical strain is applied to the flexible substrate and its output resistance variations have been observed. The electromechanical property of nanocomposite was analyzed with mechanical cantilever bending method and the gauge factor of about 9 to 12 was recorded. The change of electrical resistance of the nanocomposite film can be used in sensing mechanism for changes in chemical, biological, vibrational, temperature, pressure, load or force and displacement sensor applications. Paper ID:1841 Highly Flexible and Sensitive Graphene–Silver Nanocomposite Strain Sensor Nagarjuna Neella 1 , Venkateswarlu Gaddam 1 , M.M. Nayak 2 , T.Srinivas 3 and K. Rajanna 1* 1 Dept. of Instrumentation & Applied Physics, Indian Institute of Science (IISc), Bangalore-12, INDIA 2 Centre for Nano Science and Engineering, Indian Institute of Science (IISc), Bangalore-12, INDIA 3 Dept. of Electrical Communication Engineering , Indian Institute of Science (IISc), Bangalore-12, INDIA Preparation of RGO RGO was synthesized by modified Hummers method. Dispersion of GO with DI water and ultrasonication process. Reduction of Graphene oxide(GO) at 95 ºC with Hydrazine hydrate solution for 4 hrs. Filtration process. Annealing at 80 °C for 2 hrs. Preparation of RGO – Ag nanocomposite The RGO-Ag nanoparticles composite was prepared by dispersing RGO nanosheets and Ag nanoparticles in an N-Methyl-2-pyrrolidone (NMP) solution at weight ratio of 0.5:1. Ultrasonication process for homogenous dispersion of RGO and Ag nanoparticles. Contact details Nagarjuna Neella, Sensors Laboratory Dept of Instrumentation and Applied Physics, IISc Bangalore-12, INDIA Contact no: 080-22933188 or 07760556035 E-mail: [email protected] ,

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Page 1: References [1] Geim AK and Novoselov KS, “The rise of graphene”, Nature materials, 2007,6,183-191. [2] Youngbin Lee, Sukang Bae, Houk Jang, Sukjae Jang,

References[1] Geim AK and Novoselov KS, “The rise of graphene”, Nature materials, 2007,6,183-191.

[2] Youngbin Lee, Sukang Bae, Houk Jang, Sukjae Jang, Shou-En Zhu,Sung Hyun Sim, Young Il Song, Byung Hee Hong, and Jong-Hyun Ahn ,“Wafer-Scale Synthesis and Transfer of Graphene Films” , Nano letters, 2010, 10, 490-493.

[3] John A. Rogers,Takao Someya and Yonggang Huang,“ Materials and Mechanics for Stretchable Electronics”, Science, 2010, 327, 1603-1607. 

Acknowledgement The authors are grateful to the Center for Nano Science and Engineering

(CeNSE), IISc, Bangalore, for providing the Characterization facility. Also we would like to thank Mr. Sankaran and Veera Pandian for their

kind help in testing of the device as well for supporting necessary electronic circuitry.

IntroductionGraphene: Carbon class of 2D sheets with honey comb lattice structure. Possess unique properties such as structural, optical, thermal,

mechanical and electrical properties. Wide range of applications are found in energy, electronics and

sensors.Strain Sensor challenges: Adhesion Fixed directional Low resolution at nanoscale Integration of structural materials

Our interest of present workFabrication of Highly flexible, High resolution, Integrated and sensitive graphene–silver nanocomposite based strain sensor.

ConclusionsThe RGO nanosheets were successfully synthesized by using modified Hummers method.The piezoresistive nanocomposite based strain sensor was fabricated using RGO and Ag nanoparticles.The fabricated nanocomposite strain sensor exhibits a gauge factor of about 9 to 12. It can also be used for chemical, biological and vibrational, sensor applications.

Material synthesis and characterization

.

Sensor/Device fabrication

Results

Gauge factor(G.F)= (∆R⁄R) /ε Principle: Piezoresistive

Fabrication of nanocomposite Strain Sensor Mechanical mask preparation with stainless steel for micro mold

structural patterns. Prepared RGO-Ag nanocomposite solution was drop casted on

kapton substrate. Annealing process at 80 °C for 1 hr. Electrodes preparation process .

Abstract— We are reporting, a novel reduced graphene oxide (RGO) and silver (Ag) nanocomposite based piezoresistive thin film sensor realized on kapton (polyimide) membrane by drop casting method for strain sensing applications. Incorporation of small quantity of (Ag) fillers into RGO can create a novel nanocomposite with improved structural and functional properties. The as-synthesized RGO and nanocomposite were characterized using X-ray diffraction (XRD) & field emission- scanning electron microscope (FE-SEM) for their structural properties and morphology analysis. Fabricated nanocomposite strain sensor undergoes piezoresistive behavior when mechanical strain is applied to the flexible substrate and its output resistance variations have been observed. The electromechanical property of nanocomposite was analyzed with mechanical cantilever bending method and the gauge factor of about 9 to 12 was recorded. The change of electrical resistance of the nanocomposite film can be used in sensing mechanism for changes in chemical, biological, vibrational, temperature, pressure, load or force and displacement sensor applications.

 

Paper ID:1841Highly Flexible and Sensitive Graphene–Silver

Nanocomposite Strain SensorNagarjuna Neella1, Venkateswarlu Gaddam1 , M.M. Nayak2, T.Srinivas3 and K. Rajanna1*

1Dept. of Instrumentation & Applied Physics, Indian Institute of Science (IISc), Bangalore-12, INDIA2Centre for Nano Science and Engineering, Indian Institute of Science (IISc), Bangalore-12, INDIA

3Dept. of Electrical Communication Engineering , Indian Institute of Science (IISc), Bangalore-12, INDIA

Preparation of RGO RGO was synthesized by modified

Hummers method. Dispersion of GO with DI water

and ultrasonication process. Reduction of Graphene oxide(GO)

at 95 ºC with Hydrazine hydrate solution for 4 hrs.

Filtration process. Annealing at 80 °C for 2 hrs.

Preparation of RGO – Ag nanocomposite The RGO-Ag nanoparticles composite was prepared by

dispersing RGO nanosheets and Ag nanoparticles in an N-Methyl-2-pyrrolidone (NMP) solution at weight ratio of 0.5:1.

Ultrasonication process for homogenous dispersion of RGO and Ag nanoparticles.

Contact detailsNagarjuna Neella, Sensors LaboratoryDept of Instrumentation and Applied Physics, IISc Bangalore-12, INDIAContact no: 080-22933188 or 07760556035

E-mail: [email protected] , [email protected]