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Restricted REQUEST FOR PROPOSAL FOR 3G30A SOLAR CELL ASSEMBLIES AND ALLIED MATERIALS FROM AZUR SPACE May, 2016 ISRO SATELLITE CENTRE BANGALORE

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  • Restricted

    REQUEST FOR PROPOSAL

    FOR

    3G30A SOLAR CELL

    ASSEMBLIES

    AND

    ALLIED MATERIALS FROM AZUR SPACE

    May, 2016

    ISRO SATELLITE CENTRE BANGALORE

  • RFP For Triple Junction Solar Cells i

    CONTENTS

    1.  PREAMBLE ............................................................................................................... 1 2.  SPECIFICATIONS / PERFORMANCE REQUIREMENTS ....................................... 1 2.1  DESCRIPTION OF SCA ............................................................................................ 2 2.2  SCA CONSTITUENTS .............................................................................................. 2 2.2.1  SOLAR CELL ............................................................................................................ 2 2.2.1.1  SUBSTRATE AND EPILAYERS ............................................................................... 2 2.2.1.2  ANTI REFLECTION COATING (ARC)...................................................................... 3 2.2.1.3  FRONT CONTACT .................................................................................................... 4 2.2.1.4  REAR CONTACT ...................................................................................................... 4 2.2.2  BYPASS DIODE ........................................................................................................ 5 2.2.3  SERIES INTERCONNECT ........................................................................................ 6 2.2.4  COVER GLASS ......................................................................................................... 7 2.2.5  BARE CELLS ............................................................................................................ 8 2.2.6  SEMI-BARE CELLS .................................................................................................. 8 2.3  SCA MASS ................................................................................................................ 9 2.4  SCA ELECTRICAL OUTPUT .................................................................................... 9 2.5  SCA RADIOMETRIC PROPERTIES ...................................................................... 10 2.6  WORKING STANDARDS ....................................................................................... 10 2.7  POSITIVE END TERMINATIONS ........................................................................... 11 2.8  NEGATIVE END TERMINATIONS ......................................................................... 12 2.9  REPAIR INTERCONNECTS/ INTERCONNECTS FOR PULL TESTS .................. 13 2.10  VISUAL INSPECTION CRITERIA ........................................................................... 13 2.11  SCA FUNCTIONAL CHARACTERISTICS ............................................................. 13 2.11.1  RELIABILITY ........................................................................................................... 13 2.11.1.1  FAILURE RATE....................................................................................................... 13 2.11.1.2  LIFE REQUIREMENTS ........................................................................................... 14 2.11.2  ENVIRONMENTAL REQUIREMENTS ................................................................... 14 2.11.3  PHOTON IRRADIATION REQUIREMENTS ........................................................... 14 2.11.4  REVERSE CHARACTERISTICS REQUIREMENTS .............................................. 14 2.12  MATERIALS AND PROCESSES ............................................................................ 15 2.13  BENDING RADIUS ................................................................................................. 16 2.14  SCA BOWING ......................................................................................................... 16 2.15  CLEANLINESS AND MARKING ............................................................................ 16 2.16  WORKMANSHIP ..................................................................................................... 17 2.17  INTERCHANGEABILITY AND UNIFORMITY OF PRODUCT ............................... 17 2.18  QUALIFICATION AND HERITAGE ........................................................................ 17 2.19  PARTICIPATION AND CO-OPERATION ............................................................... 18 2.20  STORAGE ............................................................................................................... 18 2.21  TRANSPORTATION ............................................................................................... 18 3.  PRODUCT ASSURANCE RELIABILITY AND TESTS .......................................... 19 3.1  QUALIFICATION AND ACCEPTANCE TEST REQUIREMENTS ......................... 20 3.1.1  QUALIFICATION REQUIREMENTS....................................................................... 20 3.1.1.1  PROCESS IDENTIFICATION DOCUMENT (PID) .................................................. 20 3.1.1.2  PRODUCTION CONTROL ...................................................................................... 21 3.1.1.3  QUALIFICATION TESTS ........................................................................................ 21 3.1.2  PANEL LIFE-TEST COUPON ................................................................................. 32 3.1.3  LOT ACCEPTANCE TESTS(LAT) ........................................................................... 33 3.2 QUALIFICATION TESTS AT ISRO ........................................................................ 35 4.  TEST METHODS AND CONDITIONS .................................................................... 37 4.1  VISUAL INSPECTION ............................................................................................. 37 4.2  DIMENSIONS .......................................................................................................... 37 4.3  SCA MASS .............................................................................................................. 37 4.4  ELECTRICAL PERFORMANCE ............................................................................. 38 4.5  TEMPERATURE COEFFICIENTS .......................................................................... 39 4.6  WELDED CONTACT INTEGRITY .......................................................................... 39 4.7  CONTACT UNIFORMITY ........................................................................................ 39 4.8  THERMAL CYCLING TEST .................................................................................... 40 

  • RFP For Triple Junction Solar Cells ii

    4.9  HUMIDITY ................................................................................................................ 40 4.10  IRRADIATION ......................................................................................................... 41 4.10.1  PARTICLE IRRADIATION ...................................................................................... 41 4.10.1.1  ELECTRON IRRADIATION & PROTON IRRADIATION........................................ 42 4.10.2  PHOTON IRRADIATION ......................................................................................... 44 4.10.3  PHOTON IRRADIATION (SHORT DURATION) ..................................................... 45 4.10.4  UV IRRADIATION (FOR SCA ONLY)..................................................................... 45 4.11  RADIOMETRIC PROPERTIES ............................................................................... 45 4.11.1  SOLAR ABSORPTANCE ....................................................................................... 45 4.11.2  HEMISPHERICAL EMITTANCE ............................................................................. 45 4.12  CONTACT AND COATING ADHERENCE ............................................................. 46 4.12.1  TAPE PEEL TEST ................................................................................................... 46 4.13  INTERCONNECT FATIGUE ................................................................................... 46 4.14  SPECTRAL RESPONSE ........................................................................................ 46 4.15  REVERSE BIAS SCREENING ................................................................................ 47 4.16  ANGLE OF INCIDENCE TEST ............................................................................... 47 4.17  SHADOW TOLERANCE TEST ............................................................................... 47 4.18  BY PASS DIODE/SCA LIFE TEST ......................................................................... 48 4.19  THERMAL VACUUM SOAK ................................................................................... 48 4.20  CAPACITANCE MEASUREMENT ......................................................................... 48 5.  PACKAGING, DELIVERY AND SCHEDULES ....................................................... 49 5.1  PACKAGING ........................................................................................................... 49 5.2  TRANSPORTATION AND PACKAGING ACCEPTANCE ..................................... 49 5.3  DELIVERABLE DOCUMENTS ............................................................................... 49 5.3.1  DATA/ DOCUMENTS REQUIREDALONG WITH THE PROPOSAL ..................... 50 5.3.2  ALONG WITH PID ................................................................................................... 52 5.3.3  ALONG WITH EACH LOT OF SCA ........................................................................ 53 5.4  HARDWARE DELIVERABLES ............................................................................... 54 ANNEXURE A – ENVIRONMENTAL REQUIREMENTS ................................................................... 56 A1.  PRE-DEPLOYMENT ............................................................................................... 56 A2.  DURING DEPLOYMENT ......................................................................................... 57 A3.  POST DEPLOYMENTS ........................................................................................... 56 A4.  RADIATION ............................................................................................................. 57 A4.1.  GEO ORBIT ............................................................................................................. 57 A4.1.1.  ELECTRON RADIATION ........................................................................................ 57 A4.1.2.  PROTON RADIATION ............................................................................................ 58 TABLE 2A: PROTON FLUX - LOW ENERGY ..................................................................................... 58 TABLE 2B :PROTON FLUENCE - SOLAR FLARE ............................................................................ 59 A4.2  PLASMA .................................................................................................................. 59 A4.3  MICROMETEOROIDS ............................................................................................. 59 A4.4  SOLAR RADIATION ............................................................................................... 60 

  • RFP For Triple Junction Solar Cells for Indian Space Program 1 of 61

    REQUIREMENT RESPONSE FROM THE VENDOR

    REMARKS IF ANY

    1. PREAMBLE

    Indian Space Research Organization (ISRO) is designing, fabricating, testing,

    and launching its own satellites for different applications. These satellites are

    launched by either own launch vehicle or being launched by other launch

    vehicles. These satellites are powered using photovoltaic generated power for

    its application. The solar arrays for power generation are also designed,

    fabricated and tested in-house. The proposed Solar Cell Assemblies (SCAs)

    also called as Cover Glass Integrated Cells (CICs) are to be procured for use

    in one or more GEO/ LEO spacecraft.

    2. SPECIFICATIONS / PERFORMANCE REQUIREMENTS

    This chapter gives the details of the specification and/or performance

    requirements of the hardware being procured viz.

    ♦ Cover glass Integrated cells (SCAs)

    ♦ Hand held working standard SCAs (Secondary Standard SCAs)

    ♦ Positive end terminations

    ♦ Negative end terminations and

    ♦ Interconnects for pull tests

    ♦ Repair Interconnector

    ♦ Coverglass

    ♦ Bare Cells

  • RFP For Triple Junction Solar Cells for Indian Space Program 2 of 61

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    ♦ Semi-bare cells - Fully fabricated super epi-wafers up to rear

    contact metallization and ready for dicing.

    An assessment on all specifications of hardware mentioned in this document

    as provided by vendor will be done by ISRO.

    2.1 DESCRIPTION OF SCA

    The SCA and each constituent of the SCA offered shall be fully qualified to

    meet the qualification and heritage requirements mentioned in 2.18. Each SCA

    shall consist of:

    • A monolithic and epitaxially grown n/p triple junction solar cell on Ge-

    substrate,

    • with built-in discrete Silicon bypass diode (SIBD)/ Monolithic diode, which

    is integrated to the cell for protection of the self (mother) cell or the

    neighboring cell.

    • A series interconnect welded to the front contact to carry the power with

    adequate redundancy and

    • Cover glass bonded to the solar cell using DC 93500.

    2.2 SCA CONSTITUENTS

    2.2.1 SOLAR CELL

    2.2.1.1 SUBSTRATE AND EPILAYERS

    The solar cell shall consist of a mono crystalline germanium substrate of 40

  • RFP For Triple Junction Solar Cells for Indian Space Program 3 of 61

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    mm x 80 mm nominal size & Smaller size cells around 10 cm2 and 140

    microns nominal thickness with two cropped corners with various suitably

    doped and epitaxially grown layers which constitute the triple junction solar

    cell. The vendor shall specify the following details about the solar cells.

    • Nominal, minimum and maximum dimensions of the solar cells.

    • Nominal, minimum and maximum thickness of the Ge substrate

    • Nominal, minimum and maximum thickness of the solar cells

    • Resistivity of the Ge substrate

    • Cross sectional drawing of the solar cell specifying the materials and

    polarity of all the layers of the solar cell such as nucleation layer, buffer

    layer, BSFs, windows, tunnel junctions, cap layer, contacts and anti-

    reflection coating (ARC) including active solar cell junctions.

    2.2.1.2 ANTI REFLECTION COATING (ARC)

    The front surface of the solar cell shall have multi-layer ARC of TiOx and

    Al2O3. The coating material shall be designed to maximize the end of life

    electrical output from the SCA. The ARC shall not delaminate, deteriorate

    and/or degrade the performance of the SCA during fabrication, testing, storage

    and use of the SCAs to fabricate solar panels. The vendor shall specify the

    ARC material, its thickness and optical properties including the solar cell

    reflectance curves. Vendor shall also specify the total uncoated AR-area as a

  • RFP For Triple Junction Solar Cells for Indian Space Program 4 of 61

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    percentage of the cell area.

    2.2.1.3 FRONT CONTACT

    The front contact geometry shall consist of pads for interconnection and

    gridlines for current collection and reducing series resistance. The front

    electrical contact of the solar cell shall be made of suitable contact material

    and compatible for resistance welding process. The outermost layer of the

    contact shall be silver of 5 µm (nominal thickness) and shall have an Au flash

    on top of around 50 – 100 Å. The front contact shall be free of solder. The

    vendor shall specify the following:

    • Composition of the front contact and gridline material.

    • Geometry of the front contacts and gridlines

    • Location of the front contact pads in the solar cell

    • Nominal, minimum and maximum thickness of each metal layer

    • Front contacts and gridline area as a percentage of the solar cell area

    • Surface roughness

    2.2.1.4 REAR CONTACT

    The rear electrical contact shall be deposited throughout the back surface of

    the cell and shall be made of suitable contact material such that the outer layer

    is silver of nominally 5 microns thickness with gold flash and compatible for

    resistance welding process. The rear contact shall be free of solder. The

  • RFP For Triple Junction Solar Cells for Indian Space Program 5 of 61

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    vendor shall specify the following.

    • Composition of the rear contact

    • Nominal, minimum and maximum thickness of each layer

    • Surface roughness of the rear contact

    2.2.2 BYPASS DIODE

    The bypass diode shall be a discrete/monolithic diode attached to the solar

    cell. The bypass diode shall protect the solar cell from all electrical stresses

    induced by full or partial shadow of the SCA, induced by other SCAs

    connected in series and parallel and those induced by the test and switching

    electronics. The interconnection between the solar cell and the bypass diode

    shall be fully space qualified preferably with redundant interconnections at

    both cathode and anode sides. In addition, the diode current carrying capacity

    shall have sufficient de-rating to carry the light generated current and also to

    carry the switching transients induced by Power Control Unit (PCU) due to the

    solar cell junction capacitance. The vendor shall specify the following:

    • Diode construction including materials used and thickness.

    • Interconnection between solar cell and diode including the location of the

    diode in the SCA.

    • Diode-solar cell interconnect material, thickness, and geometry and weld

    location.

    • Electrical parameters including, current capacity, forward voltage drop at

  • RFP For Triple Junction Solar Cells for Indian Space Program 6 of 61

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    specified currents, PIV, leakage current at specified reverse voltages,

    reverse recovery period and junction capacitance.

    • Visual inspection criteria for diode acceptance.

    • Flight heritage / Qualification of the bypass diode including when used as

    a part of the SCA proposed.

    • Documentary evidence for compliance to the functional requirements

    after experiencing the environments specified in Annexure1.

    • The Diode I/C shall be compatible with ISRO lay-down process in which

    RTV S 691 / equivalent adhesive covers 100% of the area beneath the

    diode and diode I/C

    2.2.3 SERIES INTERCONNECT The series interconnect shall be made of 25 µm nominally thick silver plated

    kovar (i.e.15 µm (nominal) thick Kovar with a nominal of 5 microns thick silver

    coating on all sides) with a Au flash like cell rear contact. The interconnects

    are attached to the p and n cell contacts by multiple cell welds. Interconnect

    shall be compatible for resistance welding to the solar cell described in para

    2.2.1 and shall be free of solder. The series interconnect shall be designed to

    meet the following requirements:

    • Shall have two or three tabs per cell + one tab for diode, each capable of

    carrying the full solar cell generated current.

    • Shall have two prongs per tab and shall be welded on top front contact

  • RFP For Triple Junction Solar Cells for Indian Space Program 7 of 61

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    pad

    • Shall have stress relief loops to withstand fatigue induced by thermal

    loads due to the mismatch between the SCA and solar panel substrate

    with CFRP face sheets during GEO (2025 thermal cycles between

    +130°C and -165°C and 4500 cycles between +130°C and -100°C)

    missions.

    • Shall be designed such that it should not abrade / puncture Kapton

    insulation of 50 microns thickness.

    • Shall be easy to handle.

    • Shall not deform/damage due to handling and transportation.

    The vendor shall provide the following details related to series interconnect:

    • Dimensional drawing of the proposed interconnects with tolerances.

    • Material and thickness of interconnect, including coatings if any.

    • Interconnect flight heritage/ qualification of the proposed Interconnect life

    for 15 year GEO mission shall be supported by the ground coupon test or

    any other test and necessary analysis.

    2.2.4 COVER GLASS

    The cover glass shall be made of cerium oxide stabilized micro sheet of CMX

    type from M/s Qioptiq, coated with MgF2 antireflection coating. The cover glass

    maximum size shall be chosen by the vendor to cover the solar cell and by-

    pass diode fully with the cover glass overhang not exceeding 250 micron on

  • RFP For Triple Junction Solar Cells for Indian Space Program 8 of 61

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    REMARKS IF ANY

    any side. The cover thickness shall be 150 ± 20 micron. Inverted coverglasses

    with the ARC oriented toward active cell area are not permissible and

    coverglasses shall have an etch symbol/ edge stain to ensure proper

    installation. Cover glass shall be bonded to the cell with DC 93500 adhesive.

    The thickness variation of the SCA after cover glass bonding shall be

    controlled to ensure uniform glue line thickness over the solar cell area and

    between SCA to SCA. The vendor shall provide the following details of the

    cover glass and cover glass bonding adhesive:

    • Nominal, minimum and maximum dimensions of the cover glass.

    • Minimum and maximum overhang on each side of the SCA

    • Nominal, minimum and maximum glue line thickness of cover glass

    bonding adhesive. The cover glass bonding adhesive thickness

    variations within a SCA and from SCA to SCA shall be minimum.

    Allowable variation shall be specified by the vendor.

    2.2.5 BARE CELLS

    The bare cells shall have the same dimensions and shall be chosen from the

    same MOCVD production lot/batch of SCAs to be delivered under this

    contract.

    2.2.6 SEMI-BARE CELLS The fully fabricated epi wafers up to the rear contact metallization and ready

    for dicing (semi- bare cells) shall have the same contact configuration as the

    SCAs and shall be configured for dicing two bare cells from one wafer. Vendor

  • RFP For Triple Junction Solar Cells for Indian Space Program 9 of 61

    REQUIREMENT RESPONSE FROM THE VENDOR

    REMARKS IF ANY

    shall specify the edge exclusion to be considered while dicing the cell from the

    wafer. These wafers shall be chosen from the same MOCVD production

    lot/batch of SCAs to be delivered under this contract. The process and

    qualification used in semi-bare cells shall be same as those for the SCAs.

    2.3 SCA MASS

    The vendor shall specify the average, minimum and maximum SCA mass.

    2.4 SCA ELECTRICAL OUTPUT

    Each SCA shall be capable of converting artificial or natural radiant solar

    power as found outside the earth's atmosphere (1367 W/m2, WMO Spectrum)

    into electrical power. The electrical performance of the solar cell/ SCA shall be

    measured as per 4.4. The vendor shall specify a test voltage VT. The SCA

    power output is defined as the product of VT and current at VT, henceforth

    referred to as IT at 28°C. Vendor shall specify the SCA efficiency at VT

    considering the solar cell active area and also considering the area of the

    rectangle of sides equal to the maximum length and breadth of the cover

    glass. The shipping lot average efficiency of SCAs considering the solar cell

    area shall be greater than 28% at 28°C under 1 AM0. The minimum efficiency

    of any SCA at 28°C under 1 AM0, in a shipping lot shall be within 95% of the

    average efficiency. No SCA in the shipping lot shall have a Vmp lesser than VT-

    50mV. The SCAs shall be grouped based on current at VT at 28°C with a

  • RFP For Triple Junction Solar Cells for Indian Space Program 10 of 61

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    bandwidth of 5mA.

    The vendor shall specify the following electrical parameters of the SCA:

    • Lot average, maximum and minimum efficiency of the SCAs as defined

    above.

    • VT (test point voltage) & Current at Vmp/2 and (Vmp +Voc)/2 [email protected] and I

    @2.55V.

    • Sun simulator(s) used and its spectral composition comparison with AM0,

    over the wavelength band of interest, in the form of a tables and plots.

    2.5 SCA RADIOMETRIC PROPERTIES

    The solar absorptance in the non-operating condition and total hemispherical

    emittance of the SCA top surface shall be specified by the vendor.

    2.6 WORKING STANDARDS

    A set of secondary working standards that include one full SCA and three

    other SCAs consisting each any one of the top, middle or bottom junctions

    with the other junctions simulated optically (i.e. iso type top, middle or bottom

    junctions). The working standards calibration shall be traceable to a Shuttle /

    balloon flown primary standard of the same type as the SCAs under

    measurement. The working standard set shall be used to set the solar

    simulator for electrical evaluation of the SCAs. The vendor shall provide the

    following information related to the working standards:

    • Cross section drawing including material and thickness of the various

  • RFP For Triple Junction Solar Cells for Indian Space Program 11 of 61

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    layers in each of the four SCAs that constitute a set of working

    standards.

    • Working standards calibration procedure specifying the primary

    standard reference.

    • Full I-V characteristics and spectral response in the form of a table

    and plots for the full set of four SCAs of the working standards.

    • Full dark I-V characteristics with digital data for the full set of four

    SCAs of the working standards. This can be optional and shall be

    discussed with vendor.

    • Measured values of Series and Shunt Resistance of the four SCAs of the

    working standards.

    • A calibration certificate for each of standard SCAs supplied.

    2.7 POSITIVE END TERMINATIONS

    • These are assembly of interconnects and a terminal bus bar to be used

    as the solar cell string positive termination with a provision to solder/ weld

    multiple wires. The interconnect part shall be similar to the series

    interconnect of the SCA and all specifications of 2.2.3 shall be applicable.

    The termination part shall be a separate piece with provision for wire

    termination and the interconnect part welded/ weldable to it. Silver plated

    positive end terminations (bus bars) shall be made of Kovar material. The

    positive end terminations shall be 75 μm (3 mil) thick kovar base material

  • RFP For Triple Junction Solar Cells for Indian Space Program 12 of 61

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    REMARKS IF ANY

    with 5 µm silver plating on each side and shall have Au flash like cell

    rear contact. It requires three tubules at located such that the

    interconnect and wire welding/ soldering don't affect each other. Material

    of the positive end termination shall be the same as series interconnects.

    The design of the positive end termination shall take into account the

    aspects of translational and rotational forces encountered by it in the

    panel during thermal cycling. The vendor shall provide data on the

    positive end termination in similar lines as specified for the series

    interconnect in 2.2.3. The component drawing shall be provided. Vendor

    is free to offer an alternate design for the positive end termination to meet

    the functional requirements specified.

    2.8 NEGATIVE END TERMINATIONS These are similar to the positive termination without the interconnect part such

    that after welding to the SCA series interconnect they provide wire welding/

    soldering interface for the string negative termination. The design of the

    negative end termination shall take into account the aspects of translational

    and rotational forces encountered by it in the panel during thermal cycling. The

    vendor shall provide data on the negative end termination in similar lines as

    specified for the series interconnect in 2.2.3. The component drawing shall be

    provided. Vendor is free to offer an alternate design for the positive end

    termination to meet the functional requirements specified.

  • RFP For Triple Junction Solar Cells for Indian Space Program 13 of 61

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    2.9 REPAIR INTERCONNECTS/ INTERCONNECTS FOR PULL TESTS These are series interconnects used in the SCAs without the stress relief

    loops. The vendor shall provide data on the interconnects for pull test, in

    similar lines as specified for the series interconnect in 2.2.3. The series

    interconnects; end terminations and Pull test interconnects when welded/

    soldered shall have pull strengths per tab of 300 gram force and 150 gram

    force when pulled at 0°and 45°respectively.

    2.10 VISUAL INSPECTION CRITERIA Vendor shall provide its own standard visual inspection (VI) criteria for the

    hardware being procured like solar cell, interconnects, bypass diode,

    coverglass and its bonding process. The VI criteria shall be discussed with

    ISRO and mutually agreed upon before the contract.

    2.11 SCA FUNCTIONAL CHARACTERISTICS

    2.11.1 RELIABILITY The SCA and allied material shall meet the operational requirements given

    below. Reliability shall be considered of prime importance in the design and

    manufacture of the CSAs and allied material.

    2.11.1.1 FAILURE RATE

    Each SCA shall have an average failure rate of less than 1x 10-9 failures per

    hour.

  • RFP For Triple Junction Solar Cells for Indian Space Program 14 of 61

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    2.11.1.2 LIFE REQUIREMENTS

    The CIC shall meet the requirements specified in this document for use in

    GEO as well as LEO missions after storage for a maximum of five years under

    specified conditions, in addition to the various tests on ground and

    the manufacturing process of the solar array.

    The CIC and the allied material and processes shall be compatible with ISRO

    lay-down process in which adhesive (RTV S 691) covers 100% of the area

    (grouting) beneath the CIC, series I/C and bypass Diode I/C.

    GEO Requirements: 2025 thermal cycles between +130°C and -165°C and

    4500 cycles between +130°C and -100°C

    LEO requirements: (45000 cycles between +110°C and -100°C) missions

    2.11.2 ENVIRONMENTAL REQUIREMENTS

    Environments generally seen by the SCA and interconnects as a part of the

    solar array are detailed in the Annexure 1. The SCA and the allied materials

    shall be designed to meet the performance requirements before, during and

    after exposure to the environments specified.

    2.11.3 PHOTON IRRADIATION REQUIREMENTS

    SCA design/manufacturing process shall be such that the SCAs shall not

    degrade when exposed to standard AM0 spectrum throughout the mission life

    of 15 years in GEO with 50% safety margin as specified in 2.11.1.2.

    2.11.4 REVERSE CHARACTERISTICS REQUIREMENTS

    The reverse characteristics of the SCAs shall be such that no SCA will have

  • RFP For Triple Junction Solar Cells for Indian Space Program 15 of 61

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    any permanent damage resulting in degradation of I at VT after the SCA is

    biased in the reverse.

    2.12 MATERIALS AND PROCESSES

    The selection, documentation, qualification, approval and control of all parts,

    materials and processes for the SCAs and allied materials shall be in

    accordance with the reliability and quality assurance provisions of chapter 3.

    All the SCAs and allied materials supplied to the specifications of this

    document shall allow assembly after shipment handling and storage for 5

    years and thereafter meet all the requirements. No material should be used in

    the manufacture of SCAs, which are not compatible with the following

    processes.

    • Assembly into modules by parallel gap resistance welding.

    • Bonding of the modules to a 50 microns thick Kapton insulator over a

    CFRP substrate using Wacker-Chemie RTV-S-691 Silicone. No oil,

    grease or similar material, including adhesive tapes shall come in

    contact with any portion of the SCAs and allied materials during

    manufacture and testing.

    • All the materials used in fabrication of SCAs and the allied material

    shall be magnetically clean except interconnect in the solar cell contact.

    However, these should not affect the solar array performance.

    • Materials shall comply with the flammability, out gassing and other

    requirements of NASA, ESA or ASTM applicable standards.

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    • Cleaning solvents used in fabrication of solar cells shall not leave traces

    of corrosive ions that can affect the performance of the cell, e.g.

    chlorides, fluorides, sulphides, etc.

    2.13 BENDING RADIUS

    • The bending radius of the SCA, in a solar panel, shall be less than or

    equal to 2 meters. When bent to 2 meter radius, the cell electrical and

    mechanical performance shall not degrade. Vendor shall specify the

    bending radius of the SCA being offered.

    2.14 SCA BOWING

    The SCA when placed with cover glass down free on a stable surface plate

    shall not bow more than 250 μm (typical) in either convex or concave. The

    vendor shall specify the nominal, minimum and maximum SCA bowing

    parameter and shall demonstrate on a minimum of 32 SCAs during lot

    acceptance.

    2.15 CLEANLINESS AND MARKING

    • Each SCA shall be fabricated in a clean environment to allow

    weldability, bondability and stability of electrical output under standard

    AM0 spectrum. The SCAs as received from the Vendor shall be

    weldable by resistance welding and bondable using RTVS 691

    adhesive without any cleaning. Each SCA shall have a UID (unique ID)

    and a 2D barcode i.e. each Each SCA shall be numbered uniquely so

    that traceability of different processes such as MOCVD, evaporation,

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    SCA batch information, etc can easily be identified.

    • The marking fixed at the center of the rear contact of the cell (away

    from the rear weld zone) shall be readable after cleaning with water.

    propanol or acetone and any environmental test. The marking shall not

    affect the electrical, mechanical and environmental properties of the

    SCAs and shall not interfere with the welding and bonding of the SCAs

    2.16 WORKMANSHIP

    The workmanship shall meet or exceed Vendor' manufacturing and process

    standards that are documented and controlled and shall be approved by

    ISRO. The vendor shall use only trained and certified personnel and

    equipment to realize the SCAs offered.

    2.17 INTERCHANGEABILITY AND UNIFORMITY OF PRODUCT

    The SCAs shall provide for maximum interchangeability among similar group

    of items. All SCAs shall be manufactured as per approved process

    identification document (PID). The manufacturing process and materials used

    shall be same as those of used in qualification testing of the cell/SCA as

    described in chapter 3. No changes in vendors, materials, fabrication

    technique, assembly procedures and inspection are allowed. If any change is

    warranted, it shall be informed to ISRO for approval. ISRO reserves the right

    to insist for additional qualification at the vendor’s cost.

    2.18 QUALIFICATION AND HERITAGE

    The vendor shall provide documentary evidence on the qualification status of

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    the SCAs and allied material for use on commercial geo-stationary (15 years)

    spacecraft and / or 5 years in low earth orbits as per existing industry

    standards. The SCA offered by the vendor shall be from the regular cell

    production line of the heritage space solar cell. The qualification shall be

    demonstrated through in-flight heritage and/or ground testing.

    2.19 PARTICIPATION AND CO-OPERATION

    Vendor is expected to facilitate the participation of ISRO representatives

    during design review, fabrication, qualification and lot acceptance. If any of the

    tests done at other than Vendors premises, Vendor shall agree and facilitate

    ISRO′s participation. ISRO reserves the right to position a resident engineer at

    the vendor premises for the duration of manufacture and testing of hardware

    deliverable under this contract. Vendor shall confirm concurrence and facilitate

    this.

    2.20 STORAGE

    Each SCA shall meet all the requirements of this document after storage for a

    minimum period of five years. Vendor shall specify the storage

    conditions/procedure.

    2.21 TRANSPORTATION

    The SCAs and the allied material shall be transportable by air/ship and road,

    when packed as per Chapter 5 of this document.

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    3. PRODUCT ASSURANCE RELIABILITY AND TESTS

    The vendor quality assurance requirements shall have applicable documents

    for maintaining the overall quality, in addition to the tests and test philosophies

    described herein:

    The vendor shall be responsible for verifying all the requirements of this

    specification in accordance with the following product assurance and reliability

    specifications. The vendor shall also be responsible for compliance with all the

    requirements of Chapter 2.0. One or more of the following methods shall

    carry out verifications:

    A. Analysis

    B. Demonstration

    C. Inspection

    D. Test

    Any specific test performed by ISRO instead of the vendor shall not relieve

    vendor of the responsibility of compliance with all the requirements of

    Chapter 2.0. The qualification and acceptance tests shall be carried out in

    accordance with the test procedures approved by ISRO. Records of all tests

    and equipment used shall also be maintained. ISRO reserves the right to

    witness all or any of the tests. Records shall be maintained for at least 10

    years in the form of permanent files and to be made available to ISRO for

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    scrutiny as and when required. Failure or non-conformance during any stage

    of qualification, manufacture or testing shall be immediately informed to ISRO.

    A report giving details of failure, failure analysis, remedial action and impact of

    the failure on schedules and performance of the SCAs shall be submitted to

    ISRO and approval shall be obtained.

    3.1 QUALIFICATION AND ACCEPTANCE TEST REQUIREMENTS

    3.1.1 QUALIFICATION REQUIREMENTS

    3.1.1.1 PROCESS IDENTIFICATION DOCUMENT (PID)

    Vendor shall submit for approval, the Process Identification Document (PID)

    describing the steps necessary to meet the requirements spelt out in Chapter

    2. In order to optimize cost, quality and schedules these steps should utilize

    the existing procedures, which have been established over the years as a

    result of in-house programs. In case of variations to comply with the

    requirements, the same may be proposed in details and sequence. The PID

    should include, though not necessarily limited to the following:

    • A detailed specification showing component parameters and other

    data to fully describe the SCA, its components and the allied materials

    proposed to be supplied.

    • A detailed flow chart, showing all processing steps involved in the

    production of the SCAs and the allied materials. A list of QA checkpoints

    during manufacture of the SCAs shall be included.

    • A product flow chart, including the qualification and acceptance tests.

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    • Mechanical drawing of the SCAs and the allied materials, which complies

    with the specifications and reflects the hardware configuration when

    delivered.

    3.1.1.2 PRODUCTION CONTROL The vendor shall have complete traceability and lot control over the complete

    production flow line beginning from the wafer stage to SCA. The vendor shall

    have SPC (statistical process control) charts for all materials, process and

    tests. The lot control shall include information and traceability of wafer lot

    used, the raw material, processing information, date of processing, operator

    and equipment used to realize the SCA. ISRO reserves the right to station a

    resident engineer at VENDOR’s facility for the period of the contract, to

    monitor the hardware manufacture.

    3.1.1.3 QUALIFICATION TESTS The qualification tests to be performed on SCAs shall demonstrate that the

    SCAs satisfy the test requirements described below. Vendor shall provide

    documentary proof that the SCAs being offered have successfully undergone

    the ground qualification tests, meeting or exceeding the international

    standards such as ECSS*-E-ST-20-08C, AIAA**S-111-2005, etc. The test

    conditions shall equal or exceed the ground, launch and in orbit conditions so

    as to locate the deficiencies and margins. However, ISRO reserves its right

    to conduct a Type Approval Test (TAT) if deemed necessary. The TAT has to

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    be conducted in presence of ISRO representative at vendor’s premises. The

    typical TAT sequence shall include but not limited to the following. The tests

    shall be conducted in the sequence indicated and shall demonstrate

    compliance with the respective requirements. Tests of group A, C and G shall

    be conducted on bare cells while group F tests, shall be conducted on series

    interconnects. The remaining tests shall be conducted on SCAs. Vendor

    shall quote for TAT giving the breakup in price for each test group. ISRO

    reserves the right to conduct any or all of these tests.

    *ECSS : European Cooperation for Space Standardization

    ** AIAA : American Institute of Aeronautics and Astronautics

    The significant requirements of the groups are as follows:

    Group A - Top contact welding and thermal cycling.

    32 bare cells with series interconnects welded to the top contact

    Initial pull test on 10 similar samples shall be used as reference value.

    Test Sequence Para Reference Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical Output 4.4

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    Top contact welding 4.6

    Appearance 4.1

    Electrical output 4.4

    Thermal cycling 4.8

    Appearance 4.1

    Electrical Output 4.4

    Photon Irradiation 4.10.3

    Appearance 4.1

    Electrical Output 4.4

    Contact Integrity 4.6

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    Group B - Rear contact welding and thermal cycling 32 SCAs with series interconnects welded to the rear contact

    Initial pull test on 10 similar samples shall be used as reference value.

    Test Sequence Para Reference

    Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical Output 4.4

    Diode Characteristics TBD*

    Welding 4.6

    Appearance 4.1

    Electrical Output 4.4

    Thermal cycling 4.8

    Appearance 4.1

    Electrical output 4.4

    Diode characteristics TBD*

    Photon Irradiation 4.10.3

    Appearance 4.1

    Electrical Output 4.4

    Contact Integrity 4.6

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    * The test process shall be mutually agreed between the vendor and ISRO. Group C Particle Irradiation: Group C1- Particle Irradiation (Electron) - 36 bare cells .

    Test Sequence Para Reference

    Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical Output 4.4

    Radiometric Properties 4.11

    Temperature Coefficients 4.5

    Spectral Response 4.14

    Electrical Output 4.4

    Electron Irradiation 4.10.1.1

    Photon irradiation 4.10.3

    Appearance 4.1

    Electrical Output 4.4

    Radiometric properties 4.11

    Temperature Coefficients 4.5

    Spectral Response 4.14

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    Group C2 - Particle Irradiation (Proton) - 84 bare cells.

    Test Sequence Para Reference

    Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical output 4.4

    Diode characteristics TBD*

    Radiometric properties 4.11

    Temperature Coefficients 4.5

    Spectral Response 4.14

    Electrical Output 4.4

    Proton Irradiation 4.10.1.2

    Photon Irradiation 4.10.3

    Appearance 4.1

    Electrical Output 4.4

    Radiometric properties 4.11

    Temperature Coefficients 4.5

    Spectral Response 4.14

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    Group D - Humidity - 32 SCAs

    Test Sequence Para Reference Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical Output 4.4

    Humidity 4.9

    Tape peel test 4.12.1

    Appearance 4.1

    Electrical Output 4.4

    Thermal Vacuum Soak 4.19

    Appearance 4.1

    Electrical Output 4.4

    Photon Irradiation 4.10.3

    Appearance 4.1

    Electrical Output 4.4

    Tape Peel Test 4.12.1

    Group E - UV Irradiation - 32 SCAs

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    Test Sequence Para Reference Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Group F - Interconnect fatigue (32 Series Interconnects)

    Test Sequence Para Reference

    Appearance 4.1

    Dimension 4.2

    Interconnect fatigue 4.13

    Group G - Contacts, AR coating integrity-32 bare cells

    Test Sequence Para Reference

    Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical Output 4.4

    Photon Irradiation 4.10.3

    Appearance 4.1

    Electrical Output 4.4

    Coating Adherence 4.12

    Group H - Angle of Incidence, Shadow Tolerance Test-32 SCAS

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    Test Sequence Para Reference Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical Output 4.4

    Angle of Incidence 4.16

    Appearance 4.1

    Electrical Output 4.4

    Shadow Tolerance 4.17

    Appearance 4.1

    Electrical Output 4.4

    Group I - Photon Irradiation Test-32 SCAs

    Test Sequence Para Reference

    Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical Output 4.4

    Photon Irradiation 4.10.2

    Appearance 4.1

    Electrical Output 4.4

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    Group J - BYPASS Diode/ SCA Life Test-32 SCAS

    Test Sequence Para Reference Appearance 4.1

    Dimension 4.2

    Mass 4.3

    Electrical Output 4.4

    Bypass Diode/ SCA Life Test 4.18

    Appearance 4.1

    Electrical Output 4.4

    Group K – Diode Electrical Performance Test (to be specified by the vendor) Group L – Diode Environmental Test (to be specified by the vendor) For the external bypass diode offered, the vendor shall provide documentary

    evidence that the diodes as sub-assembly components have been qualified

    fully on ground. The tests on the bypass diodes shall include performance

    evaluation tests and environmental tests. These tests shall generally be

    particle irradiation test on the diode (which includes proton and electron

    irradiation), post particle irradiation performance evaluation, UV irradiation

    test, thermal soaking and cycling, humidity, panel level thermal cycling and

    reverse voltage test and any other tests deemed necessary for the shunt

    diode performance evaluation.

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    The vendor shall also provide the following details

    i) Lot number and batch number details of the diode

    ii) Lot Acceptance Test (LAT) results of the diode.

    iii) Screening of these diodes.

    iv) Storage aspects of these diodes.

    v) Preferred interconnection.

    The samples for the TAT may be selected by the internal QA at random, from

    the first production lot of TBD size. After selecting the TAT test samples with

    necessary spares, the remaining SCAs of this first lot shall be delivered to

    ISRO for its own qualification testing including those for the lay-down process.

    The remaining SCAs production shall be authorized only after successful

    completion of the TAT at vendor and tests at ISRO.

    The TAT samples shall contain SCAs from each group of current classification

    such that the average power output of the samples at 28°C measured under

    WMO standard AM0 spectrum is equal to the lot average. The samples

    selected for each group shall have representation of a minimum two MOCVD

    and two evaporation lots. If more than one type of reactor, evaporation/ARC

    unit is planned for production, samples processed by each type of unit shall be

    included. In the event of accidental damage to sample, SCAs prior to the

    completion of the test sequence, each such SCA shall be replaced by a new

    SCA of the same lot and the new SCAs shall be subjected to all the tests of

    that sequence. Failure to meet the requirements of this specification of any

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    group during qualification testing will call for retesting at the cost of vendor

    with a new sampling plan mutually agreed with ISRO. The failures shall be

    analyzed and suitable corrective actions shall be implemented accordingly.

    The vendor shall demonstrate the qualification so as to verify the implemented

    corrective actions would satisfy the qualification requirements.

    The vendor shall provide the non-conformance report and the management of

    non-conformances.

    3.1.2 PANEL LIFE-TEST COUPON

    Four numbers of Flight quality panel coupons manufactured by the vendor /

    ISRO including circuits of SCAs and the positive and negative end

    terminations proposed and samples of repaired SCAs will be subjected to an

    accelerated thermal cycling life test as per 2.11.1.2., to demonstrate

    the capability to survive the GEO / LEO orbital environment. The coupon

    substrate will be provided by ISRO. 5 TVAC before and after cycling. The

    coupon will also undergo tests to verify its performance in the acoustic,

    vibration, and shock environments of Annexure 1.

    Coupon ESD tests: One of the fabricated coupons shall be subjected to ESD

    tests as per ECSS or AIAA test methods that can be agreed upon at the time

    of contract finalization.

    The Test coupons fabrication cost, accelerated life testing cost and ESD test

    cost shall be quoted by the vendor with item wise breakup. The configuration

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    of the coupon and test plans shall be mutually agreed between ISRO and the

    vendor at the time of contract. ISRO reserves the right to carry out any or all

    the tests specified.

    3.1.3 LOT ACCEPTANCE TESTS (LAT) Lot Acceptance tests (LAT) shall be performed by vendor for every 10000

    CICs shipped to ISRO as per test methods described in Chapter 4.0 and shall

    be witnessed and certified by ISRO or a third party, agreed mutually between

    ISRO and the vendor. The acceptance tests are described in table below:

    1. For SCAs, BARE CELLS, SEMI-BARE CELLS

    REQUIREMENT Test Method

    SCAs

    Bare Cells

    Semi-Bare Cells

    SAMPLE SIZE

    Appearance 4.1 √ √ √ 100% In process

    Identification 4.1 √ √ TBD 100% In process

    Dimensions 4.2 √ √ TBD LTPD-7 – No failure

    Bowing 4.2 √ √ † LTPD-7 – No failure

    Mass 4.3 √ √ √ 100 samples per lot

    Electrical output 4.4 √ √ TBD 100% In process

    Contact uniformity 4.7 √ √ † In process,

    on wafer edges

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    Weld Contact

    Integrity Test

    (Rear)

    4.6 √ † † LTPD-7-No failure

    Humidity # 4.9 √ † † LTPD-7-No failure

    Photon Irradiation 4.10.2 √ † † LTPD-7 No failure

    Contact & Coating

    Adherence

    4.2 √ † † In process,

    on wafer edges

    Reverse Bias

    Screening

    4.15 √ √ TBD 100% In process

    2. For ALLIED MATERIALS and RAW MATERIALS

    MATERIAL SAMPLE SIZE

    Series

    Interconnect*

    The results of the acceptance tests carried out by the sub-

    contractor(s) and the incoming inspection by vendor shall

    be included in this lot EIDP.

    Positive End

    termination*

    Negative End

    termination*

    Interconnect for

    pull test*

    Bypass Diode*

    Ge Wafer

    Coverglass

    Cover glass

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    bonding adhesive

    (DC 93500)

    # Except the humidity test and Weldability tests, all other acceptance tests are nondestructive and hence the tests may be conducted on samples selected

    from the shipping lot. Weldability tests are to be carried out on 32 SCAs and

    32 weld samples have to be realized from them. Humidity test are to be

    carried on 32 SCAs. The humidity and Weldability SCA samples shall be long

    to the same manufacturing lot as the shipping lot but not part of the shipping lot.

    * Vendor to specify.

    ISRO reserves the right to carry out any additional test(s) mentioned in

    qualification test plan if necessary, after discussing with the vendor. The

    acceptance test plan, sample size for such tests shall be finalized after

    discussion.

    3.2 QUALIFICATION TESTS AT ISRO

    • A development model Panel/ Coupon will be fabricated by ISRO using

    flight representative CFRP substrate and the first lot SCAs supplied by

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    the vendor. This panel will be subjected to qualification level acoustic,

    vibration and thermovac cycling. The test conditions and acceptance

    criteria will be supplied to the vendor and in case of failure in any of

    these tests, vendor will assist ISRO in resolving the problem.

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    FROM THE VENDOR

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    4 TEST METHODS AND CONDITIONS The in-process, qualification and acceptance tests for the SCAs and allied

    materials manufactured according to the required specification shall be

    performed in accordance with the test methods and test conditions specified

    in this chapter.

    4.1 VISUAL INSPECTION

    The SCAs shall be visually inspected using stereo zoom microscope of 10x

    magnification. The inspection criteria for 40mm X 80mm cells nominal

    dimension shall be provided by vendor and shall be mutually agreed upon as

    mentioned in 2.10. The SCAs shall also be inspected using EL

    (electroluminescence) technique and vendor shall provide the acceptance /

    rejection criteria.

    4.2 DIMENSIONS

    The overall dimensions of the cell, the dimensions of the cover glass, its

    position, interconnect and its position shall be measured with optical

    templates or in a profile projector for conformance to the drawings.

    4.3 SCA MASS Weighing the samples with an accuracy of within ± 1.0%, and dividing by the

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    number of samples shall determine the average SCA mass.

    4.4 ELECTRICAL PERFORMANCE The electrical performance of the SCAs shall be measured under 1 AM0

    (1367 W/m2, WMO spectrum) illumination simulated by a class A sun

    simulator, whose spectral response over the wavelength band of interest

    closely matches that of the sun at 1AU from the sun in all the three

    wavelength bands. The sun simulator intensity shall be set to match the Isc

    and Voc at 28°C, using a set of secondary standards traceable to a balloon

    flown primary standard (or any Govt. / non Govt. organization with history of

    carrying out such balloon flight experiments. Vendor shall ensure that the

    secondary standards are evaluated under class A solar simulator whose

    spectral composition is close to WMO e.g. ESA/ESTEC) of the type

    identical to the SCA being measured.

    After setting the intensity and temperature, four reference SCAs of the type

    under measurement shall be evaluated. The set-up shall be considered ready

    for electrical evaluation of SCAs/ solar cells, if the Isc and IT of the reference

    SCAs match within 1% of their standard value and the Voc matches within

    1°C in temperature setting. Otherwise, the exercise shall be repeated after

    adjusting the sun simulator intensity again. Suitable load and data acquisition

    units shall be used for evaluating the SCAs/ solar cells.

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    4.5 TEMPERATURE COEFFICIENTS The open circuit voltage, short circuit current, maximum power, the current

    and voltage at the maximum power point, the fill factor and the efficiency shall

    be measured between +28°C & +100°C and between +28°C & -50°C to

    determine their first order temperature coefficients. Measurement shall be

    made at 5 different temperatures in each of the two ranges.

    4.6 WELDED CONTACT INTEGRITY The welding procedure adopted shall not degrade the output current of the

    SCA including the diode. Series interconnects welded to the front contact of

    the bare cell and the bypass diode and rear contact of the SCA including the

    diode shall be tested, by pulling the interconnect tabs both in 0°and 45°. The

    cell, diode or SCA shall be clamped to Unitek micro-pull tester or equivalent

    such that the restraining force is applied on at least 40% of the cell/SCA area

    and pulled at a speed not exceeding 40 mm/min. Minimum acceptable pull

    strength per tab is 300 gram force and 150 gram force when pulled at @0°

    and 45° respectively.

    4.7 CONTACT UNIFORMITY The contact thickness uniformity for each fabrication lot shall be within

    specified limits as defined in PID. Front and rear contact thickness shall be

    measured using a Beta scope or equivalent. Measurement shall be carried

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    out for each evaporation batch (metallization lot).

    4.8 THERMAL CYCLING TEST

    The SCAs/cells/diode shall be subjected to the following tests:

    • Prior to thermal cycling, samples shall be subjected to a high

    temperature soak at +150°C in an inert atmosphere for one hour.

    • 50 thermal cycles –100°C to +150°C in vacuum, 30°C/minute,

    maximum average temperature rate, no dwell is required.

    • 2025 thermal cycles from –175°C to +130°C in an inert atmosphere

    with 30°C/minute, maximum average temperature rate, no dwell

    is required.

    During the post thermal cycling electrical evaluation as per 4.4, the power

    degradation due to the test shall be within 2%. This and weld strength

    specifications shall be met on every SCA/cell/diode. Vendor shall specify the

    acceptance criteria for the bypass diodes.

    4.9 HUMIDITY

    The SCAs shall be stored for 96 hours in a chamber at a temperature not less

    than 65°C and relative humidity 95±5% at ambient pressure. Subsequently

    the cells shall be dried for 2hrs at 80°C. Following the exposure the SCA

    electrical output measured as per 4.4 shall not degrade more than 2%. It

    shall also meet the requirements of tape peel test as per para 4.12.1

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    4.10 IRRADIATION

    4.10.1 PARTICLE IRRADIATION

    Electrical evaluation of the radiation test samples before and after irradiation

    shall be carried out by standard third party lab like JPL or SPASOLAB.

    Test Condition:

    Measure I-V data of the solar cells at +28°C before and after proton radiation.

    Requirements:

    • Establish normalized radiation degradation curves for Voc, Isc, Vmp, Imp,

    and Pmp, including nominal and 90% confidence values.

    • Subsequently the cells shall be subjected to Photon Irradiation Test as

    in 4.10.3.

    • Spectral Response (SR), External quantum efficiency (EQE), Internal

    quantum efficiency (IQE), Temperature Co-efficient and Radiometric

    properties to be measured before and after radiation of the samples.

    Data to be provided:

    • Remaining factor of all the parameters for each fluence.

    (i.e. Ratio of EOL and BOL efficiencies for each fluence level)

    • Establish EOL Eff. vs. Blue/Red ratio curve for each fluence.

    • Each new reactor shall be validated at one energy/fluence, and

    The vendor shall also provide the following data related to the cells used for

    this test (i.e. Electron irradiation & Proton irradiation) along with the

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    corresponding population averages.

    • Blue/Red Ratio

    • BOL Efficiency

    • Voc

    4.10.1.1 ELECTRON & PROTON IRRADIATION

    Vendor shall provide the results of electron and proton irradiation testing of

    the proposed solar cell for the following energies and fluences (typical).

    Vendor shall also include in the price bid as option, the pricing for carrying out

    these tests.

    Electron and Proton Irradiation Test on the cells shall be carried out as

    follows:

    For each irradiation level a minimum of 12 cells shall be taken. These cells

    shall be selected such that, they are from 3 different current classes namely

    maximum, average and minimum and from 2 evaporation lots and from a

    minimum of 2 MOCVD reactors in case more than one reactor is used for

    production of deliverable lot. Electron and proton uniformity shall be

    maintained at ±10% and temperature maintained at 20°C±10°C during

    irradiation. The test shall be performed in accordance with JPL standard

    procedures as published in JPL Publication 92-09 at a standard facility, which

    has a heritage of being used for space quality solar cell irradiation. If any,

    alternative standards established by other space agencies are used details

    shall be provided. Subsequent to the electron irradiation, the cells shall be

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    subjected to 8Hrs photon irradiation as in 4.10.3.

    The vendor shall furnish the degradation factors for power, current and

    voltage at the fluence levels defined earlier in addition to the omni directional

    electron relative damage co-efficient (RDC) as function of electron energy

    and shielding thickness.

    SR, EQE, IQE, temperature coefficients and radiometric properties should

    also be measured before and after the test.

    The energy and fluence table for Electron irradiation test is given below:

    Samples

    Energy (MeV)

    Fluence per cm2

    12 0.6 2x1013

    2x1014

    1x1015

    2x1015

    12 1 3x1013

    1x1014

    5x1014

    1x1015

    12 12 1x1013

    1x1013

    5x1013

    1x1014

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    The energy and fluence table for Protron irradiation test is given below:

    SAMPLES ENERGY FLUENCE PER CM2

    1E10 3E10 1E11 3E11 1E12 3E12 12 20 KeV X X X X X X 12 50 KeV X X X X X X 12 100KeV X X X X X X 12 300KeV X X X X X X 12 1MeV X X X X X X 12 3MeV X X X X X X 12 10MeV X X X X X X

    4.10.2 PHOTON IRRADIATION

    The SCA samples shall be subjected for 48 hrs of standard AM0 spectrum

    exposure under a suitable solar simulator. The cells shall not show

    degradation more than 2% from the original current at load point voltage as a

    result of photon exposure.

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    4.10.3 PHOTON IRRADIATION (SHORT DURATION)

    The SCA samples shall be subjected for 8 hrs of standard AM0 spectrum

    exposure under a suitable solar simulator. The cells shall not show

    degradation more than 2% from the original current at load point voltage as a

    result of photon exposure.

    4.10.4 UV IRRADIATION (FOR SCA ONLY)

    SCAs shall be subjected to a UV equivalent of 1000 sun hours of WMO

    standard AM0 spectrum, under minimum of 10-5 Torr vacuum, at temperature

    ≤ 40°C. Within 48 hours after the completion of the irradiation, the samples

    should be electrically evaluated, as per 2.4 and the average short circuit

    current degradation shall not exceed 2%.

    4.11 RADIOMETRIC PROPERTIES

    4.11.1 SOLAR ABSORPTANCE

    The spectral reflectance of electromagnetic energy shall be measured from

    0.28 to2.5 micrometers with Edwards’s type integrating sphere equipment or

    equivalent. The test data shall be integrated over the solar irradiance and the

    integral subtracted from unity to yield the solar absorptance.

    4.11.2 HEMISPHERICAL EMITTANCE

    Measure spectral reflectance in the wavelength ranges from 2.0 to 26

    micrometers and integrate over 300K planckian radiator functions. The

    measured data should comply with the requirement of 2.5.

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    4.12 CONTACT AND COATING ADHERENCE

    The cells shall be exposed to a relative humidity of 95 ± 5% at a temperature

    of 95°C for a period of 2 hours. Before and after this test, tape peel test as

    described below shall be conducted on the cell front side.

    4.12.1 TAPE PEEL TEST

    Scotch brand Magic transparent tape No.810/ 600 with an adhesion to steel

    value equal to or exceeding 33 grams per cm width shall be placed on the

    surface to be tested. The tape shall be rubbed well ensuring that it adheres

    firmly to the surface and stripped at 90° to the surface. Not more than 1% of

    rear contact, 5% of the AR coating shall be removed by the tape and there

    shall be no peeling of top contact pads.

    4.13 INTERCONNECT FATIGUE

    The interconnect loop in the form to be used in SCAs shall be subjected to

    the mechanical flex test to establish the interconnect fatigue life. The

    configuration of the flex test and the deflection shall be jointly worked out by

    the vendor and ISRO after studying the proposed interconnect drawing.

    4.14 SPECTRAL RESPONSE

    The spectral response (SR) of the SCAs shall be measured by comparison of

    the short circuit current of the test cell with the output of a spectral standard

    of known relative spectral response under monochromatic irradiation.

    • At various discrete wavelength intervals between 0.3 and 2

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    micrometer using narrow band interference filters or

    • By means of a high intensity monochromatic light, for continuous

    recording between 0.3 and 2 micrometer wavelengths. The

    minimum spectral irradiance shall be 100 microwatts/cm2.

    EQE and IQE of SCAs shall also be measured similarly following the

    standard protocol.

    4.15 REVERSE BIAS SCREENING

    Reverse bias screening test for the cell shall be spelt out by the vendor to

    assess that the solar cell shall not degrade due to reverse bias applied on the

    cell. The vendor shall specify test specification, test methodology and

    allowable degradation criteria. Samples failed once shall not be subjected for

    retest. The supplier shall also provide the yield of the reverse bias screening

    test. The screen shall be performed on the 100% samples selected for ISRO.

    4.16 ANGLE OF INCIDENCE TEST

    SCAs should be taken from random current classes and should be subjected

    to angle of incidence tests. The I-V characteristics of the SCAs shall be

    measured at 0°, 20°, 40°, 60° and 80°.

    4.17 SHADOW TOLERANCE TEST

    The mean IT of SCAs shall not decrease by > 2 % and any individual SCA IT

    shall not degrade by more than 3%, when subjected to partial shadowing.

    This condition shall be simulated by reverse biasing the test samples to 1.22

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    Isc at 90 + 5°C/ -0°C for 30 minutes in dark.

    4.18 BY PASS DIODE / SCA LIFE TEST

    Qualification test SCAs shall be subjected to 3000 Reverse Bias Cycles

    from 1.1 Isc for 30 Secs to zero mA for 30 sec in a Thermo Vacuum Chamber

    (

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    5 PACKAGING, DELIVERY AND SCHEDULES 5.1 PACKAGING

    The SCAs and allied materials shall be packed in containers of design

    approved by ISRO with adequate protection from damage during transport

    and handling. Special care should be given for interconnects. The

    containers shall be heat sealed in an airtight water proof barrier as per MIL-B-

    22191, together with sufficient bagged, activated dry desiccant as per MIL-D-

    3464 and tarnish inhibitor to prevent contamination to assure compliance as

    per chapter 2.0. A card type humidity indicator scaled 10 to 80% of relative

    humidity shall be placed in each sealed bag. Any packaging or desiccating

    material used shall not affect the electrical and mechanical properties of the

    SCAs and allied materials. The vendor shall submit a packaging and storage

    plan for ISRO approval prior to the first lot shipment.

    5.2 TRANSPORTATION AND PACKAGING ACCEPTANCE

    Inspection of the packaging for shipment shall be as per 5.1 of this

    document. Contents of the damaged containers will be rejected. In case, the

    humidity indicator accompanying the SCAs indicates a humidity level greater

    than 40%, the defective container shall be rejected. Any SCA, which does not

    meet one or more of the acceptance test requirements, shall be rejected.

    5.3 DELIVERABLE DOCUMENTS

    The following documents shall be submitted in the form of permanent files at

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    the appropriate time. All documentation shall be in English.

    The quotation shall contain the following.

    • Technical Data on the proposed SCA as per 5.3.1

    • Export Control Document requirements of the proposed SCAs.

    • Quotation for

    o the proposed SCA

    o Allied Material as per of 5.5 (Sl. No. 3 to 10)

    o Lot Acceptance Test (LAT) as per 3.1.3

    o Type Approval Test (TAT) giving group wise breakup

    o Life test Coupon Fabrication as per 3.1.2

    o Life test Coupon testing as per 3.1.2

    o ESD test on Coupon As per 3.1.2

    • For preparation of the quotation, commercial guidelines shall be

    followed.

    5.3.1 DATA/ DOCUMENTS REQUIREDALONG WITH THE PROPOSAL

    The technical proposal shall include but not limited to the following.

    1. A compliance matrix for this proposal in a spreadsheet.

    2. Description of the hardware offered including necessary drawing

    and images.

    3. Manufacturing & Qualification / flight heritage.

    4. Comparison of the qualification status of the hardware offered

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    against standard international specifications.

    5. I-V characteristics of a typical SCA with lot average efficiency

    specified in the form of a table and plot at 28°C to 60°C and

    110°C under standard AM0 spectrum before and after

    irradiation with 1x1014 1 MeV electrons/cm2 and 5 x1014 1 MeV

    electrons/cm2.

    6. Bending radius of the SCA at maximum curvature.

    7. Quality manual

    8. Cross sectional diagram of the SCA with thickness of the

    different layers.

    9. Product assurance plan including fabrication and process control

    aspects reliability analysis. Non-conformance control and

    approval of configuration control and traceability.

    10. Maximum Panel size and test levels of CFRP qualification panel

    tested by vendor for qualifying the triple junction SCAs.

    11. Qualification test reports on the SCA and allied materials

    including the bypass diode.

    12. Documentation of bare cells, semi-bare cells, and cover glass.

    13. Absolute typical spectral response of the proposed solar cell.

    14. Remaining factor of the parameters Isc, Imp, Vmp, Voc and Pmp

    for each of the fluence levels 3x1013, 1 x 1014, 5 x 1014, and 1 x

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    1015 of 1MeV electrons /cm2. (i.e. Ratio of EOL and BOL

    efficiencies for each fluence level).

    15. Details of solar simulator used to evaluate the triple junction

    solar cell.

    16. Export Control Document requirements of the proposed SCA.

    5.3.2 ALONG WITH PID

    All documentation shall be submitted as three hard copies and one copy in

    electronic form. The PID as per 3.1.1.1 shall be submitted on receipt of the

    contract document. The PID shall include all the details specified in Chapter

    2.0 of this document. The PID shall be accompanied by the following

    documentation.

    1. The omni directional relative damage coefficients of the triple

    junction solar cells as a function of the shielding thickness for the

    following electron and proton energy ranges. Electron 40 KeV to

    7 MeV. Proton 100 KeV to 200 MeV.

    2. Blue/ red ratio of the proposed solar cell at the beginning of life

    and after experiencing 5E14 and 1E15 equivalent 1MeV electron

    fluence.

    3. List of materials used, with their quality levels derating criteria

    and failure rates.

    4. Cell diffusion capacitance as a function of voltage and

    temperature (28°C, 65°C and 110°C at BOL and after irradiation

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    at 1 x 1015 and 5x10141MeV electrons).

    5. Dimensional drawings of all hardware with tolerances.

    6. Spectrum of the sun simulators used by the vendor in the form of

    a table and plot.

    7. Calibration procedures for the secondary standards.

    8. Thermal conductivity of the solar cell.

    9. Thermal coefficient of expansion of the solar cell.

    10. Packing and storage conditions for the SCAs.

    5.3.3 ALONG WITH EACH LOT OF SCA

    The following documentation shall accompany every deliverable lot. All

    documentation is to be submitted as three hard copies and one copy in

    electronic form.

    1. The entire acceptance test records and results shall accompany

    each shipment of SCA.

    2. The vendor shall provide measured performance data (Voc, Vmp,

    Isc, Imp, IT, I at 1.2V, I at 2.55V and measured Vr during reverse

    bias screening)) for all delivered SCAs in electronic format.

    3. A certificate from the vendor that the lot has successfully passed

    the acceptance tests shall accompany each deliverable lot.

    4. Standard SCAs (set of four) I-V characteristics measured as per

    specification and spectral response in the form of a table and

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    plots (with digital data in excel).

    5. Waivers and non-conformances during cell/ SCA manufacture by

    vendor or Sub-contractor and dispositions thereof.

    6. Quality control results in the form of Statistical Process Control

    (SPC) Charts for the various processes including SCA making.

    5.4 HARDWARE DELIVERABLES ISRO decides the no of SCA’s to be procured as per the requirement. Vendor has to

    quote from 10000 to 100000 SCAs in slabs of 10000 SCA’s. The no. of shipments be

    mutually agreed between vendor and ISRO, First shipment to last shipment time

    period is 24 months.

    Sl. No ITEM Quantity

    1 SCAs Number of allied materials required for 10000

    SCAs is as follows

    2 Secondary Standards Set (Each set consisting of 3 sub cells and 1 full cell)

    3 sets

    3 Positive end terminations (consists of 1busbar and interconnects equal to the number of

    2000 sets

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    interconnects in the SCA)

    4 Negative end terminations

    2000

    5 Interconnects For Pull Test (equal to the no. of interconnects in the SCA)

    2000 sets

    6 Repair Interconnects (equal to the no. of interconnects in the SCA)

    2000 sets

    7 Germanium Substrates (4 inch and 6 inch)

    50 each

    8 Smaller size cells area around 10 cm2

    1000

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    ANNEXURE A – ENVIRONMENTAL REQUIREMENTS

    The SCA and the allied materials shall be designed to meet the performance

    requirements before, during and after exposure to the environments specified

    below. The environments experienced during fabrication, transportation and

    storage of the SCAs and allied materials shall be significantly less severe

    than them.

    A1. PRE-DEPLOYMENT A. On Ground : Relative humidity (Rh) of 70% max at 760 ± 25 mm of

    Hg barometric pressure over 23± 5°C temperature range

    B. In Space : -180°C to +125 °C (10 cycles).

    C Acoustic noise : 146 dB overall for 2 minutes.

    D. Sine vibration : 30g peak, 20-50 Hz; 10g peak, 50-100 Hz

    E. Shock : 113g @ 200 Hz increasing to 450g @ 400 Hz;

    450g max. @ 400 to 500 Hz;

    600g max.@ 1600 to 4000 Hz.

    A2. DURING DEPLOYMENT A. Barometric pressure : < 1.0 x 10-10 Torr

    B. Temperature : -180°C to +125°C

    A3. POST DEPLOYMENTS

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    A. The SCA shall be designed and manufactured to withstand 15 years of

    GEO life (2025 thermal cycles between +130°C to -165°C and 4500

    thermal cycles between +130°C and -100°C)

    B. Barometric Pressure less than 1 x 10-10 Torr.

    A4. RADIATION A4.1. GEO ORBIT

    A4.1.1. ELECTRON RADIATION The minimum-trapped electron environment in synchronous equatorial

    orbit, which the SCAs shall account, for, based on the AE-8 model is presented in Table 1.

    TABLE 1: ELECTRON FLUENCE AE-8¸ MAX MODEL Energy Level

    (> MeV) Flux: e/cm2/sec

    0.04 4.6 x 107

    0.1 4.2 x 107

    0.5 4.0 x 106

    1.0 4.9 x 105

    1.5 1.2 x 105

    2.0 4.1 x 104

    2.5 1.1 x 104

    4.0 4.9 x 103

    4.5 1.6 x 103

    4.0 4.5 x 102

    4.5 1.2 x 102

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    5.0 4.5 x 101

    A4.1.2. PROTON RADIATION

    Table 2(A) describes the low energy proton environment, which the design

    shall account for, for time averaged integral flux spectrum. The estimate for

    the high-energy proton spectrum, which represents the solar flare Content of

    the 20th cycle, is shown in table 2(B)

    TABLE 2A: PROTON FLUX - LOW ENERGY

    Energy Level

    (> MeV) Flux: p/cm2/sec

    0.01 2.74 x 107

    0.03 2.0 x 107

    0.05 1.51 x 107

    0.07 1.12 x 107

    0.10 7.21 x 106

    0.20 1.64 x 106

    0.30 6.54 x 105

    0.40 2.61 x 105

    0.50 1.04 x 105

    0.60 4.17 x 104

    0.70 1.65 x 104

    0.80 6.52 x 103

    0.90 2.58 x 102

    1.00 1.02 x 102

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    1.25 1.00 x 102

    1.50 9.85 x 100

    TABLE 2B: PROTON FLUENCE - SOLAR FLARE Energy Level

    (MeV) Fluence : p/cm2/cycle

    1 1.2 x 1011

    4 5.5 x 1010

    10 4.28 x 1010

    30 9.78 x 109

    60 2.95 x 109

    100 6.69 x 108