request for proposal for 3g30a solar cell assemblies … · 2017. 3. 8. · gridlines for current...
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REQUEST FOR PROPOSAL
FOR
3G30A SOLAR CELL
ASSEMBLIES
AND
ALLIED MATERIALS FROM AZUR SPACE
May, 2016
ISRO SATELLITE CENTRE BANGALORE
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CONTENTS
1. PREAMBLE ............................................................................................................... 1 2. SPECIFICATIONS / PERFORMANCE REQUIREMENTS ....................................... 1 2.1 DESCRIPTION OF SCA ............................................................................................ 2 2.2 SCA CONSTITUENTS .............................................................................................. 2 2.2.1 SOLAR CELL ............................................................................................................ 2 2.2.1.1 SUBSTRATE AND EPILAYERS ............................................................................... 2 2.2.1.2 ANTI REFLECTION COATING (ARC)...................................................................... 3 2.2.1.3 FRONT CONTACT .................................................................................................... 4 2.2.1.4 REAR CONTACT ...................................................................................................... 4 2.2.2 BYPASS DIODE ........................................................................................................ 5 2.2.3 SERIES INTERCONNECT ........................................................................................ 6 2.2.4 COVER GLASS ......................................................................................................... 7 2.2.5 BARE CELLS ............................................................................................................ 8 2.2.6 SEMI-BARE CELLS .................................................................................................. 8 2.3 SCA MASS ................................................................................................................ 9 2.4 SCA ELECTRICAL OUTPUT .................................................................................... 9 2.5 SCA RADIOMETRIC PROPERTIES ...................................................................... 10 2.6 WORKING STANDARDS ....................................................................................... 10 2.7 POSITIVE END TERMINATIONS ........................................................................... 11 2.8 NEGATIVE END TERMINATIONS ......................................................................... 12 2.9 REPAIR INTERCONNECTS/ INTERCONNECTS FOR PULL TESTS .................. 13 2.10 VISUAL INSPECTION CRITERIA ........................................................................... 13 2.11 SCA FUNCTIONAL CHARACTERISTICS ............................................................. 13 2.11.1 RELIABILITY ........................................................................................................... 13 2.11.1.1 FAILURE RATE....................................................................................................... 13 2.11.1.2 LIFE REQUIREMENTS ........................................................................................... 14 2.11.2 ENVIRONMENTAL REQUIREMENTS ................................................................... 14 2.11.3 PHOTON IRRADIATION REQUIREMENTS ........................................................... 14 2.11.4 REVERSE CHARACTERISTICS REQUIREMENTS .............................................. 14 2.12 MATERIALS AND PROCESSES ............................................................................ 15 2.13 BENDING RADIUS ................................................................................................. 16 2.14 SCA BOWING ......................................................................................................... 16 2.15 CLEANLINESS AND MARKING ............................................................................ 16 2.16 WORKMANSHIP ..................................................................................................... 17 2.17 INTERCHANGEABILITY AND UNIFORMITY OF PRODUCT ............................... 17 2.18 QUALIFICATION AND HERITAGE ........................................................................ 17 2.19 PARTICIPATION AND CO-OPERATION ............................................................... 18 2.20 STORAGE ............................................................................................................... 18 2.21 TRANSPORTATION ............................................................................................... 18 3. PRODUCT ASSURANCE RELIABILITY AND TESTS .......................................... 19 3.1 QUALIFICATION AND ACCEPTANCE TEST REQUIREMENTS ......................... 20 3.1.1 QUALIFICATION REQUIREMENTS....................................................................... 20 3.1.1.1 PROCESS IDENTIFICATION DOCUMENT (PID) .................................................. 20 3.1.1.2 PRODUCTION CONTROL ...................................................................................... 21 3.1.1.3 QUALIFICATION TESTS ........................................................................................ 21 3.1.2 PANEL LIFE-TEST COUPON ................................................................................. 32 3.1.3 LOT ACCEPTANCE TESTS(LAT) ........................................................................... 33 3.2 QUALIFICATION TESTS AT ISRO ........................................................................ 35 4. TEST METHODS AND CONDITIONS .................................................................... 37 4.1 VISUAL INSPECTION ............................................................................................. 37 4.2 DIMENSIONS .......................................................................................................... 37 4.3 SCA MASS .............................................................................................................. 37 4.4 ELECTRICAL PERFORMANCE ............................................................................. 38 4.5 TEMPERATURE COEFFICIENTS .......................................................................... 39 4.6 WELDED CONTACT INTEGRITY .......................................................................... 39 4.7 CONTACT UNIFORMITY ........................................................................................ 39 4.8 THERMAL CYCLING TEST .................................................................................... 40
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4.9 HUMIDITY ................................................................................................................ 40 4.10 IRRADIATION ......................................................................................................... 41 4.10.1 PARTICLE IRRADIATION ...................................................................................... 41 4.10.1.1 ELECTRON IRRADIATION & PROTON IRRADIATION........................................ 42 4.10.2 PHOTON IRRADIATION ......................................................................................... 44 4.10.3 PHOTON IRRADIATION (SHORT DURATION) ..................................................... 45 4.10.4 UV IRRADIATION (FOR SCA ONLY)..................................................................... 45 4.11 RADIOMETRIC PROPERTIES ............................................................................... 45 4.11.1 SOLAR ABSORPTANCE ....................................................................................... 45 4.11.2 HEMISPHERICAL EMITTANCE ............................................................................. 45 4.12 CONTACT AND COATING ADHERENCE ............................................................. 46 4.12.1 TAPE PEEL TEST ................................................................................................... 46 4.13 INTERCONNECT FATIGUE ................................................................................... 46 4.14 SPECTRAL RESPONSE ........................................................................................ 46 4.15 REVERSE BIAS SCREENING ................................................................................ 47 4.16 ANGLE OF INCIDENCE TEST ............................................................................... 47 4.17 SHADOW TOLERANCE TEST ............................................................................... 47 4.18 BY PASS DIODE/SCA LIFE TEST ......................................................................... 48 4.19 THERMAL VACUUM SOAK ................................................................................... 48 4.20 CAPACITANCE MEASUREMENT ......................................................................... 48 5. PACKAGING, DELIVERY AND SCHEDULES ....................................................... 49 5.1 PACKAGING ........................................................................................................... 49 5.2 TRANSPORTATION AND PACKAGING ACCEPTANCE ..................................... 49 5.3 DELIVERABLE DOCUMENTS ............................................................................... 49 5.3.1 DATA/ DOCUMENTS REQUIREDALONG WITH THE PROPOSAL ..................... 50 5.3.2 ALONG WITH PID ................................................................................................... 52 5.3.3 ALONG WITH EACH LOT OF SCA ........................................................................ 53 5.4 HARDWARE DELIVERABLES ............................................................................... 54 ANNEXURE A – ENVIRONMENTAL REQUIREMENTS ................................................................... 56 A1. PRE-DEPLOYMENT ............................................................................................... 56 A2. DURING DEPLOYMENT ......................................................................................... 57 A3. POST DEPLOYMENTS ........................................................................................... 56 A4. RADIATION ............................................................................................................. 57 A4.1. GEO ORBIT ............................................................................................................. 57 A4.1.1. ELECTRON RADIATION ........................................................................................ 57 A4.1.2. PROTON RADIATION ............................................................................................ 58 TABLE 2A: PROTON FLUX - LOW ENERGY ..................................................................................... 58 TABLE 2B :PROTON FLUENCE - SOLAR FLARE ............................................................................ 59 A4.2 PLASMA .................................................................................................................. 59 A4.3 MICROMETEOROIDS ............................................................................................. 59 A4.4 SOLAR RADIATION ............................................................................................... 60
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1. PREAMBLE
Indian Space Research Organization (ISRO) is designing, fabricating, testing,
and launching its own satellites for different applications. These satellites are
launched by either own launch vehicle or being launched by other launch
vehicles. These satellites are powered using photovoltaic generated power for
its application. The solar arrays for power generation are also designed,
fabricated and tested in-house. The proposed Solar Cell Assemblies (SCAs)
also called as Cover Glass Integrated Cells (CICs) are to be procured for use
in one or more GEO/ LEO spacecraft.
2. SPECIFICATIONS / PERFORMANCE REQUIREMENTS
This chapter gives the details of the specification and/or performance
requirements of the hardware being procured viz.
♦ Cover glass Integrated cells (SCAs)
♦ Hand held working standard SCAs (Secondary Standard SCAs)
♦ Positive end terminations
♦ Negative end terminations and
♦ Interconnects for pull tests
♦ Repair Interconnector
♦ Coverglass
♦ Bare Cells
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♦ Semi-bare cells - Fully fabricated super epi-wafers up to rear
contact metallization and ready for dicing.
An assessment on all specifications of hardware mentioned in this document
as provided by vendor will be done by ISRO.
2.1 DESCRIPTION OF SCA
The SCA and each constituent of the SCA offered shall be fully qualified to
meet the qualification and heritage requirements mentioned in 2.18. Each SCA
shall consist of:
• A monolithic and epitaxially grown n/p triple junction solar cell on Ge-
substrate,
• with built-in discrete Silicon bypass diode (SIBD)/ Monolithic diode, which
is integrated to the cell for protection of the self (mother) cell or the
neighboring cell.
• A series interconnect welded to the front contact to carry the power with
adequate redundancy and
• Cover glass bonded to the solar cell using DC 93500.
2.2 SCA CONSTITUENTS
2.2.1 SOLAR CELL
2.2.1.1 SUBSTRATE AND EPILAYERS
The solar cell shall consist of a mono crystalline germanium substrate of 40
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mm x 80 mm nominal size & Smaller size cells around 10 cm2 and 140
microns nominal thickness with two cropped corners with various suitably
doped and epitaxially grown layers which constitute the triple junction solar
cell. The vendor shall specify the following details about the solar cells.
• Nominal, minimum and maximum dimensions of the solar cells.
• Nominal, minimum and maximum thickness of the Ge substrate
• Nominal, minimum and maximum thickness of the solar cells
• Resistivity of the Ge substrate
• Cross sectional drawing of the solar cell specifying the materials and
polarity of all the layers of the solar cell such as nucleation layer, buffer
layer, BSFs, windows, tunnel junctions, cap layer, contacts and anti-
reflection coating (ARC) including active solar cell junctions.
2.2.1.2 ANTI REFLECTION COATING (ARC)
The front surface of the solar cell shall have multi-layer ARC of TiOx and
Al2O3. The coating material shall be designed to maximize the end of life
electrical output from the SCA. The ARC shall not delaminate, deteriorate
and/or degrade the performance of the SCA during fabrication, testing, storage
and use of the SCAs to fabricate solar panels. The vendor shall specify the
ARC material, its thickness and optical properties including the solar cell
reflectance curves. Vendor shall also specify the total uncoated AR-area as a
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percentage of the cell area.
2.2.1.3 FRONT CONTACT
The front contact geometry shall consist of pads for interconnection and
gridlines for current collection and reducing series resistance. The front
electrical contact of the solar cell shall be made of suitable contact material
and compatible for resistance welding process. The outermost layer of the
contact shall be silver of 5 µm (nominal thickness) and shall have an Au flash
on top of around 50 – 100 Å. The front contact shall be free of solder. The
vendor shall specify the following:
• Composition of the front contact and gridline material.
• Geometry of the front contacts and gridlines
• Location of the front contact pads in the solar cell
• Nominal, minimum and maximum thickness of each metal layer
• Front contacts and gridline area as a percentage of the solar cell area
• Surface roughness
2.2.1.4 REAR CONTACT
The rear electrical contact shall be deposited throughout the back surface of
the cell and shall be made of suitable contact material such that the outer layer
is silver of nominally 5 microns thickness with gold flash and compatible for
resistance welding process. The rear contact shall be free of solder. The
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vendor shall specify the following.
• Composition of the rear contact
• Nominal, minimum and maximum thickness of each layer
• Surface roughness of the rear contact
2.2.2 BYPASS DIODE
The bypass diode shall be a discrete/monolithic diode attached to the solar
cell. The bypass diode shall protect the solar cell from all electrical stresses
induced by full or partial shadow of the SCA, induced by other SCAs
connected in series and parallel and those induced by the test and switching
electronics. The interconnection between the solar cell and the bypass diode
shall be fully space qualified preferably with redundant interconnections at
both cathode and anode sides. In addition, the diode current carrying capacity
shall have sufficient de-rating to carry the light generated current and also to
carry the switching transients induced by Power Control Unit (PCU) due to the
solar cell junction capacitance. The vendor shall specify the following:
• Diode construction including materials used and thickness.
• Interconnection between solar cell and diode including the location of the
diode in the SCA.
• Diode-solar cell interconnect material, thickness, and geometry and weld
location.
• Electrical parameters including, current capacity, forward voltage drop at
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specified currents, PIV, leakage current at specified reverse voltages,
reverse recovery period and junction capacitance.
• Visual inspection criteria for diode acceptance.
• Flight heritage / Qualification of the bypass diode including when used as
a part of the SCA proposed.
• Documentary evidence for compliance to the functional requirements
after experiencing the environments specified in Annexure1.
• The Diode I/C shall be compatible with ISRO lay-down process in which
RTV S 691 / equivalent adhesive covers 100% of the area beneath the
diode and diode I/C
2.2.3 SERIES INTERCONNECT The series interconnect shall be made of 25 µm nominally thick silver plated
kovar (i.e.15 µm (nominal) thick Kovar with a nominal of 5 microns thick silver
coating on all sides) with a Au flash like cell rear contact. The interconnects
are attached to the p and n cell contacts by multiple cell welds. Interconnect
shall be compatible for resistance welding to the solar cell described in para
2.2.1 and shall be free of solder. The series interconnect shall be designed to
meet the following requirements:
• Shall have two or three tabs per cell + one tab for diode, each capable of
carrying the full solar cell generated current.
• Shall have two prongs per tab and shall be welded on top front contact
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pad
• Shall have stress relief loops to withstand fatigue induced by thermal
loads due to the mismatch between the SCA and solar panel substrate
with CFRP face sheets during GEO (2025 thermal cycles between
+130°C and -165°C and 4500 cycles between +130°C and -100°C)
missions.
• Shall be designed such that it should not abrade / puncture Kapton
insulation of 50 microns thickness.
• Shall be easy to handle.
• Shall not deform/damage due to handling and transportation.
The vendor shall provide the following details related to series interconnect:
• Dimensional drawing of the proposed interconnects with tolerances.
• Material and thickness of interconnect, including coatings if any.
• Interconnect flight heritage/ qualification of the proposed Interconnect life
for 15 year GEO mission shall be supported by the ground coupon test or
any other test and necessary analysis.
2.2.4 COVER GLASS
The cover glass shall be made of cerium oxide stabilized micro sheet of CMX
type from M/s Qioptiq, coated with MgF2 antireflection coating. The cover glass
maximum size shall be chosen by the vendor to cover the solar cell and by-
pass diode fully with the cover glass overhang not exceeding 250 micron on
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any side. The cover thickness shall be 150 ± 20 micron. Inverted coverglasses
with the ARC oriented toward active cell area are not permissible and
coverglasses shall have an etch symbol/ edge stain to ensure proper
installation. Cover glass shall be bonded to the cell with DC 93500 adhesive.
The thickness variation of the SCA after cover glass bonding shall be
controlled to ensure uniform glue line thickness over the solar cell area and
between SCA to SCA. The vendor shall provide the following details of the
cover glass and cover glass bonding adhesive:
• Nominal, minimum and maximum dimensions of the cover glass.
• Minimum and maximum overhang on each side of the SCA
• Nominal, minimum and maximum glue line thickness of cover glass
bonding adhesive. The cover glass bonding adhesive thickness
variations within a SCA and from SCA to SCA shall be minimum.
Allowable variation shall be specified by the vendor.
2.2.5 BARE CELLS
The bare cells shall have the same dimensions and shall be chosen from the
same MOCVD production lot/batch of SCAs to be delivered under this
contract.
2.2.6 SEMI-BARE CELLS The fully fabricated epi wafers up to the rear contact metallization and ready
for dicing (semi- bare cells) shall have the same contact configuration as the
SCAs and shall be configured for dicing two bare cells from one wafer. Vendor
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shall specify the edge exclusion to be considered while dicing the cell from the
wafer. These wafers shall be chosen from the same MOCVD production
lot/batch of SCAs to be delivered under this contract. The process and
qualification used in semi-bare cells shall be same as those for the SCAs.
2.3 SCA MASS
The vendor shall specify the average, minimum and maximum SCA mass.
2.4 SCA ELECTRICAL OUTPUT
Each SCA shall be capable of converting artificial or natural radiant solar
power as found outside the earth's atmosphere (1367 W/m2, WMO Spectrum)
into electrical power. The electrical performance of the solar cell/ SCA shall be
measured as per 4.4. The vendor shall specify a test voltage VT. The SCA
power output is defined as the product of VT and current at VT, henceforth
referred to as IT at 28°C. Vendor shall specify the SCA efficiency at VT
considering the solar cell active area and also considering the area of the
rectangle of sides equal to the maximum length and breadth of the cover
glass. The shipping lot average efficiency of SCAs considering the solar cell
area shall be greater than 28% at 28°C under 1 AM0. The minimum efficiency
of any SCA at 28°C under 1 AM0, in a shipping lot shall be within 95% of the
average efficiency. No SCA in the shipping lot shall have a Vmp lesser than VT-
50mV. The SCAs shall be grouped based on current at VT at 28°C with a
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bandwidth of 5mA.
The vendor shall specify the following electrical parameters of the SCA:
• Lot average, maximum and minimum efficiency of the SCAs as defined
above.
• VT (test point voltage) & Current at Vmp/2 and (Vmp +Voc)/2 [email protected] and I
@2.55V.
• Sun simulator(s) used and its spectral composition comparison with AM0,
over the wavelength band of interest, in the form of a tables and plots.
2.5 SCA RADIOMETRIC PROPERTIES
The solar absorptance in the non-operating condition and total hemispherical
emittance of the SCA top surface shall be specified by the vendor.
2.6 WORKING STANDARDS
A set of secondary working standards that include one full SCA and three
other SCAs consisting each any one of the top, middle or bottom junctions
with the other junctions simulated optically (i.e. iso type top, middle or bottom
junctions). The working standards calibration shall be traceable to a Shuttle /
balloon flown primary standard of the same type as the SCAs under
measurement. The working standard set shall be used to set the solar
simulator for electrical evaluation of the SCAs. The vendor shall provide the
following information related to the working standards:
• Cross section drawing including material and thickness of the various
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layers in each of the four SCAs that constitute a set of working
standards.
• Working standards calibration procedure specifying the primary
standard reference.
• Full I-V characteristics and spectral response in the form of a table
and plots for the full set of four SCAs of the working standards.
• Full dark I-V characteristics with digital data for the full set of four
SCAs of the working standards. This can be optional and shall be
discussed with vendor.
• Measured values of Series and Shunt Resistance of the four SCAs of the
working standards.
• A calibration certificate for each of standard SCAs supplied.
2.7 POSITIVE END TERMINATIONS
• These are assembly of interconnects and a terminal bus bar to be used
as the solar cell string positive termination with a provision to solder/ weld
multiple wires. The interconnect part shall be similar to the series
interconnect of the SCA and all specifications of 2.2.3 shall be applicable.
The termination part shall be a separate piece with provision for wire
termination and the interconnect part welded/ weldable to it. Silver plated
positive end terminations (bus bars) shall be made of Kovar material. The
positive end terminations shall be 75 μm (3 mil) thick kovar base material
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with 5 µm silver plating on each side and shall have Au flash like cell
rear contact. It requires three tubules at located such that the
interconnect and wire welding/ soldering don't affect each other. Material
of the positive end termination shall be the same as series interconnects.
The design of the positive end termination shall take into account the
aspects of translational and rotational forces encountered by it in the
panel during thermal cycling. The vendor shall provide data on the
positive end termination in similar lines as specified for the series
interconnect in 2.2.3. The component drawing shall be provided. Vendor
is free to offer an alternate design for the positive end termination to meet
the functional requirements specified.
2.8 NEGATIVE END TERMINATIONS These are similar to the positive termination without the interconnect part such
that after welding to the SCA series interconnect they provide wire welding/
soldering interface for the string negative termination. The design of the
negative end termination shall take into account the aspects of translational
and rotational forces encountered by it in the panel during thermal cycling. The
vendor shall provide data on the negative end termination in similar lines as
specified for the series interconnect in 2.2.3. The component drawing shall be
provided. Vendor is free to offer an alternate design for the positive end
termination to meet the functional requirements specified.
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2.9 REPAIR INTERCONNECTS/ INTERCONNECTS FOR PULL TESTS These are series interconnects used in the SCAs without the stress relief
loops. The vendor shall provide data on the interconnects for pull test, in
similar lines as specified for the series interconnect in 2.2.3. The series
interconnects; end terminations and Pull test interconnects when welded/
soldered shall have pull strengths per tab of 300 gram force and 150 gram
force when pulled at 0°and 45°respectively.
2.10 VISUAL INSPECTION CRITERIA Vendor shall provide its own standard visual inspection (VI) criteria for the
hardware being procured like solar cell, interconnects, bypass diode,
coverglass and its bonding process. The VI criteria shall be discussed with
ISRO and mutually agreed upon before the contract.
2.11 SCA FUNCTIONAL CHARACTERISTICS
2.11.1 RELIABILITY The SCA and allied material shall meet the operational requirements given
below. Reliability shall be considered of prime importance in the design and
manufacture of the CSAs and allied material.
2.11.1.1 FAILURE RATE
Each SCA shall have an average failure rate of less than 1x 10-9 failures per
hour.
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2.11.1.2 LIFE REQUIREMENTS
The CIC shall meet the requirements specified in this document for use in
GEO as well as LEO missions after storage for a maximum of five years under
specified conditions, in addition to the various tests on ground and
the manufacturing process of the solar array.
The CIC and the allied material and processes shall be compatible with ISRO
lay-down process in which adhesive (RTV S 691) covers 100% of the area
(grouting) beneath the CIC, series I/C and bypass Diode I/C.
GEO Requirements: 2025 thermal cycles between +130°C and -165°C and
4500 cycles between +130°C and -100°C
LEO requirements: (45000 cycles between +110°C and -100°C) missions
2.11.2 ENVIRONMENTAL REQUIREMENTS
Environments generally seen by the SCA and interconnects as a part of the
solar array are detailed in the Annexure 1. The SCA and the allied materials
shall be designed to meet the performance requirements before, during and
after exposure to the environments specified.
2.11.3 PHOTON IRRADIATION REQUIREMENTS
SCA design/manufacturing process shall be such that the SCAs shall not
degrade when exposed to standard AM0 spectrum throughout the mission life
of 15 years in GEO with 50% safety margin as specified in 2.11.1.2.
2.11.4 REVERSE CHARACTERISTICS REQUIREMENTS
The reverse characteristics of the SCAs shall be such that no SCA will have
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any permanent damage resulting in degradation of I at VT after the SCA is
biased in the reverse.
2.12 MATERIALS AND PROCESSES
The selection, documentation, qualification, approval and control of all parts,
materials and processes for the SCAs and allied materials shall be in
accordance with the reliability and quality assurance provisions of chapter 3.
All the SCAs and allied materials supplied to the specifications of this
document shall allow assembly after shipment handling and storage for 5
years and thereafter meet all the requirements. No material should be used in
the manufacture of SCAs, which are not compatible with the following
processes.
• Assembly into modules by parallel gap resistance welding.
• Bonding of the modules to a 50 microns thick Kapton insulator over a
CFRP substrate using Wacker-Chemie RTV-S-691 Silicone. No oil,
grease or similar material, including adhesive tapes shall come in
contact with any portion of the SCAs and allied materials during
manufacture and testing.
• All the materials used in fabrication of SCAs and the allied material
shall be magnetically clean except interconnect in the solar cell contact.
However, these should not affect the solar array performance.
• Materials shall comply with the flammability, out gassing and other
requirements of NASA, ESA or ASTM applicable standards.
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• Cleaning solvents used in fabrication of solar cells shall not leave traces
of corrosive ions that can affect the performance of the cell, e.g.
chlorides, fluorides, sulphides, etc.
2.13 BENDING RADIUS
• The bending radius of the SCA, in a solar panel, shall be less than or
equal to 2 meters. When bent to 2 meter radius, the cell electrical and
mechanical performance shall not degrade. Vendor shall specify the
bending radius of the SCA being offered.
2.14 SCA BOWING
The SCA when placed with cover glass down free on a stable surface plate
shall not bow more than 250 μm (typical) in either convex or concave. The
vendor shall specify the nominal, minimum and maximum SCA bowing
parameter and shall demonstrate on a minimum of 32 SCAs during lot
acceptance.
2.15 CLEANLINESS AND MARKING
• Each SCA shall be fabricated in a clean environment to allow
weldability, bondability and stability of electrical output under standard
AM0 spectrum. The SCAs as received from the Vendor shall be
weldable by resistance welding and bondable using RTVS 691
adhesive without any cleaning. Each SCA shall have a UID (unique ID)
and a 2D barcode i.e. each Each SCA shall be numbered uniquely so
that traceability of different processes such as MOCVD, evaporation,
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SCA batch information, etc can easily be identified.
• The marking fixed at the center of the rear contact of the cell (away
from the rear weld zone) shall be readable after cleaning with water.
propanol or acetone and any environmental test. The marking shall not
affect the electrical, mechanical and environmental properties of the
SCAs and shall not interfere with the welding and bonding of the SCAs
2.16 WORKMANSHIP
The workmanship shall meet or exceed Vendor' manufacturing and process
standards that are documented and controlled and shall be approved by
ISRO. The vendor shall use only trained and certified personnel and
equipment to realize the SCAs offered.
2.17 INTERCHANGEABILITY AND UNIFORMITY OF PRODUCT
The SCAs shall provide for maximum interchangeability among similar group
of items. All SCAs shall be manufactured as per approved process
identification document (PID). The manufacturing process and materials used
shall be same as those of used in qualification testing of the cell/SCA as
described in chapter 3. No changes in vendors, materials, fabrication
technique, assembly procedures and inspection are allowed. If any change is
warranted, it shall be informed to ISRO for approval. ISRO reserves the right
to insist for additional qualification at the vendor’s cost.
2.18 QUALIFICATION AND HERITAGE
The vendor shall provide documentary evidence on the qualification status of
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the SCAs and allied material for use on commercial geo-stationary (15 years)
spacecraft and / or 5 years in low earth orbits as per existing industry
standards. The SCA offered by the vendor shall be from the regular cell
production line of the heritage space solar cell. The qualification shall be
demonstrated through in-flight heritage and/or ground testing.
2.19 PARTICIPATION AND CO-OPERATION
Vendor is expected to facilitate the participation of ISRO representatives
during design review, fabrication, qualification and lot acceptance. If any of the
tests done at other than Vendors premises, Vendor shall agree and facilitate
ISRO′s participation. ISRO reserves the right to position a resident engineer at
the vendor premises for the duration of manufacture and testing of hardware
deliverable under this contract. Vendor shall confirm concurrence and facilitate
this.
2.20 STORAGE
Each SCA shall meet all the requirements of this document after storage for a
minimum period of five years. Vendor shall specify the storage
conditions/procedure.
2.21 TRANSPORTATION
The SCAs and the allied material shall be transportable by air/ship and road,
when packed as per Chapter 5 of this document.
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3. PRODUCT ASSURANCE RELIABILITY AND TESTS
The vendor quality assurance requirements shall have applicable documents
for maintaining the overall quality, in addition to the tests and test philosophies
described herein:
The vendor shall be responsible for verifying all the requirements of this
specification in accordance with the following product assurance and reliability
specifications. The vendor shall also be responsible for compliance with all the
requirements of Chapter 2.0. One or more of the following methods shall
carry out verifications:
A. Analysis
B. Demonstration
C. Inspection
D. Test
Any specific test performed by ISRO instead of the vendor shall not relieve
vendor of the responsibility of compliance with all the requirements of
Chapter 2.0. The qualification and acceptance tests shall be carried out in
accordance with the test procedures approved by ISRO. Records of all tests
and equipment used shall also be maintained. ISRO reserves the right to
witness all or any of the tests. Records shall be maintained for at least 10
years in the form of permanent files and to be made available to ISRO for
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scrutiny as and when required. Failure or non-conformance during any stage
of qualification, manufacture or testing shall be immediately informed to ISRO.
A report giving details of failure, failure analysis, remedial action and impact of
the failure on schedules and performance of the SCAs shall be submitted to
ISRO and approval shall be obtained.
3.1 QUALIFICATION AND ACCEPTANCE TEST REQUIREMENTS
3.1.1 QUALIFICATION REQUIREMENTS
3.1.1.1 PROCESS IDENTIFICATION DOCUMENT (PID)
Vendor shall submit for approval, the Process Identification Document (PID)
describing the steps necessary to meet the requirements spelt out in Chapter
2. In order to optimize cost, quality and schedules these steps should utilize
the existing procedures, which have been established over the years as a
result of in-house programs. In case of variations to comply with the
requirements, the same may be proposed in details and sequence. The PID
should include, though not necessarily limited to the following:
• A detailed specification showing component parameters and other
data to fully describe the SCA, its components and the allied materials
proposed to be supplied.
• A detailed flow chart, showing all processing steps involved in the
production of the SCAs and the allied materials. A list of QA checkpoints
during manufacture of the SCAs shall be included.
• A product flow chart, including the qualification and acceptance tests.
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• Mechanical drawing of the SCAs and the allied materials, which complies
with the specifications and reflects the hardware configuration when
delivered.
3.1.1.2 PRODUCTION CONTROL The vendor shall have complete traceability and lot control over the complete
production flow line beginning from the wafer stage to SCA. The vendor shall
have SPC (statistical process control) charts for all materials, process and
tests. The lot control shall include information and traceability of wafer lot
used, the raw material, processing information, date of processing, operator
and equipment used to realize the SCA. ISRO reserves the right to station a
resident engineer at VENDOR’s facility for the period of the contract, to
monitor the hardware manufacture.
3.1.1.3 QUALIFICATION TESTS The qualification tests to be performed on SCAs shall demonstrate that the
SCAs satisfy the test requirements described below. Vendor shall provide
documentary proof that the SCAs being offered have successfully undergone
the ground qualification tests, meeting or exceeding the international
standards such as ECSS*-E-ST-20-08C, AIAA**S-111-2005, etc. The test
conditions shall equal or exceed the ground, launch and in orbit conditions so
as to locate the deficiencies and margins. However, ISRO reserves its right
to conduct a Type Approval Test (TAT) if deemed necessary. The TAT has to
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be conducted in presence of ISRO representative at vendor’s premises. The
typical TAT sequence shall include but not limited to the following. The tests
shall be conducted in the sequence indicated and shall demonstrate
compliance with the respective requirements. Tests of group A, C and G shall
be conducted on bare cells while group F tests, shall be conducted on series
interconnects. The remaining tests shall be conducted on SCAs. Vendor
shall quote for TAT giving the breakup in price for each test group. ISRO
reserves the right to conduct any or all of these tests.
*ECSS : European Cooperation for Space Standardization
** AIAA : American Institute of Aeronautics and Astronautics
The significant requirements of the groups are as follows:
Group A - Top contact welding and thermal cycling.
32 bare cells with series interconnects welded to the top contact
Initial pull test on 10 similar samples shall be used as reference value.
Test Sequence Para Reference Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical Output 4.4
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Top contact welding 4.6
Appearance 4.1
Electrical output 4.4
Thermal cycling 4.8
Appearance 4.1
Electrical Output 4.4
Photon Irradiation 4.10.3
Appearance 4.1
Electrical Output 4.4
Contact Integrity 4.6
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Group B - Rear contact welding and thermal cycling 32 SCAs with series interconnects welded to the rear contact
Initial pull test on 10 similar samples shall be used as reference value.
Test Sequence Para Reference
Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical Output 4.4
Diode Characteristics TBD*
Welding 4.6
Appearance 4.1
Electrical Output 4.4
Thermal cycling 4.8
Appearance 4.1
Electrical output 4.4
Diode characteristics TBD*
Photon Irradiation 4.10.3
Appearance 4.1
Electrical Output 4.4
Contact Integrity 4.6
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* The test process shall be mutually agreed between the vendor and ISRO. Group C Particle Irradiation: Group C1- Particle Irradiation (Electron) - 36 bare cells .
Test Sequence Para Reference
Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical Output 4.4
Radiometric Properties 4.11
Temperature Coefficients 4.5
Spectral Response 4.14
Electrical Output 4.4
Electron Irradiation 4.10.1.1
Photon irradiation 4.10.3
Appearance 4.1
Electrical Output 4.4
Radiometric properties 4.11
Temperature Coefficients 4.5
Spectral Response 4.14
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Group C2 - Particle Irradiation (Proton) - 84 bare cells.
Test Sequence Para Reference
Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical output 4.4
Diode characteristics TBD*
Radiometric properties 4.11
Temperature Coefficients 4.5
Spectral Response 4.14
Electrical Output 4.4
Proton Irradiation 4.10.1.2
Photon Irradiation 4.10.3
Appearance 4.1
Electrical Output 4.4
Radiometric properties 4.11
Temperature Coefficients 4.5
Spectral Response 4.14
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Group D - Humidity - 32 SCAs
Test Sequence Para Reference Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical Output 4.4
Humidity 4.9
Tape peel test 4.12.1
Appearance 4.1
Electrical Output 4.4
Thermal Vacuum Soak 4.19
Appearance 4.1
Electrical Output 4.4
Photon Irradiation 4.10.3
Appearance 4.1
Electrical Output 4.4
Tape Peel Test 4.12.1
Group E - UV Irradiation - 32 SCAs
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Test Sequence Para Reference Appearance 4.1
Dimension 4.2
Mass 4.3
Group F - Interconnect fatigue (32 Series Interconnects)
Test Sequence Para Reference
Appearance 4.1
Dimension 4.2
Interconnect fatigue 4.13
Group G - Contacts, AR coating integrity-32 bare cells
Test Sequence Para Reference
Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical Output 4.4
Photon Irradiation 4.10.3
Appearance 4.1
Electrical Output 4.4
Coating Adherence 4.12
Group H - Angle of Incidence, Shadow Tolerance Test-32 SCAS
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Test Sequence Para Reference Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical Output 4.4
Angle of Incidence 4.16
Appearance 4.1
Electrical Output 4.4
Shadow Tolerance 4.17
Appearance 4.1
Electrical Output 4.4
Group I - Photon Irradiation Test-32 SCAs
Test Sequence Para Reference
Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical Output 4.4
Photon Irradiation 4.10.2
Appearance 4.1
Electrical Output 4.4
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Group J - BYPASS Diode/ SCA Life Test-32 SCAS
Test Sequence Para Reference Appearance 4.1
Dimension 4.2
Mass 4.3
Electrical Output 4.4
Bypass Diode/ SCA Life Test 4.18
Appearance 4.1
Electrical Output 4.4
Group K – Diode Electrical Performance Test (to be specified by the vendor) Group L – Diode Environmental Test (to be specified by the vendor) For the external bypass diode offered, the vendor shall provide documentary
evidence that the diodes as sub-assembly components have been qualified
fully on ground. The tests on the bypass diodes shall include performance
evaluation tests and environmental tests. These tests shall generally be
particle irradiation test on the diode (which includes proton and electron
irradiation), post particle irradiation performance evaluation, UV irradiation
test, thermal soaking and cycling, humidity, panel level thermal cycling and
reverse voltage test and any other tests deemed necessary for the shunt
diode performance evaluation.
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The vendor shall also provide the following details
i) Lot number and batch number details of the diode
ii) Lot Acceptance Test (LAT) results of the diode.
iii) Screening of these diodes.
iv) Storage aspects of these diodes.
v) Preferred interconnection.
The samples for the TAT may be selected by the internal QA at random, from
the first production lot of TBD size. After selecting the TAT test samples with
necessary spares, the remaining SCAs of this first lot shall be delivered to
ISRO for its own qualification testing including those for the lay-down process.
The remaining SCAs production shall be authorized only after successful
completion of the TAT at vendor and tests at ISRO.
The TAT samples shall contain SCAs from each group of current classification
such that the average power output of the samples at 28°C measured under
WMO standard AM0 spectrum is equal to the lot average. The samples
selected for each group shall have representation of a minimum two MOCVD
and two evaporation lots. If more than one type of reactor, evaporation/ARC
unit is planned for production, samples processed by each type of unit shall be
included. In the event of accidental damage to sample, SCAs prior to the
completion of the test sequence, each such SCA shall be replaced by a new
SCA of the same lot and the new SCAs shall be subjected to all the tests of
that sequence. Failure to meet the requirements of this specification of any
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group during qualification testing will call for retesting at the cost of vendor
with a new sampling plan mutually agreed with ISRO. The failures shall be
analyzed and suitable corrective actions shall be implemented accordingly.
The vendor shall demonstrate the qualification so as to verify the implemented
corrective actions would satisfy the qualification requirements.
The vendor shall provide the non-conformance report and the management of
non-conformances.
3.1.2 PANEL LIFE-TEST COUPON
Four numbers of Flight quality panel coupons manufactured by the vendor /
ISRO including circuits of SCAs and the positive and negative end
terminations proposed and samples of repaired SCAs will be subjected to an
accelerated thermal cycling life test as per 2.11.1.2., to demonstrate
the capability to survive the GEO / LEO orbital environment. The coupon
substrate will be provided by ISRO. 5 TVAC before and after cycling. The
coupon will also undergo tests to verify its performance in the acoustic,
vibration, and shock environments of Annexure 1.
Coupon ESD tests: One of the fabricated coupons shall be subjected to ESD
tests as per ECSS or AIAA test methods that can be agreed upon at the time
of contract finalization.
The Test coupons fabrication cost, accelerated life testing cost and ESD test
cost shall be quoted by the vendor with item wise breakup. The configuration
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of the coupon and test plans shall be mutually agreed between ISRO and the
vendor at the time of contract. ISRO reserves the right to carry out any or all
the tests specified.
3.1.3 LOT ACCEPTANCE TESTS (LAT) Lot Acceptance tests (LAT) shall be performed by vendor for every 10000
CICs shipped to ISRO as per test methods described in Chapter 4.0 and shall
be witnessed and certified by ISRO or a third party, agreed mutually between
ISRO and the vendor. The acceptance tests are described in table below:
1. For SCAs, BARE CELLS, SEMI-BARE CELLS
REQUIREMENT Test Method
SCAs
Bare Cells
Semi-Bare Cells
SAMPLE SIZE
Appearance 4.1 √ √ √ 100% In process
Identification 4.1 √ √ TBD 100% In process
Dimensions 4.2 √ √ TBD LTPD-7 – No failure
Bowing 4.2 √ √ † LTPD-7 – No failure
Mass 4.3 √ √ √ 100 samples per lot
Electrical output 4.4 √ √ TBD 100% In process
Contact uniformity 4.7 √ √ † In process,
on wafer edges
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Weld Contact
Integrity Test
(Rear)
4.6 √ † † LTPD-7-No failure
Humidity # 4.9 √ † † LTPD-7-No failure
Photon Irradiation 4.10.2 √ † † LTPD-7 No failure
Contact & Coating
Adherence
4.2 √ † † In process,
on wafer edges
Reverse Bias
Screening
4.15 √ √ TBD 100% In process
2. For ALLIED MATERIALS and RAW MATERIALS
MATERIAL SAMPLE SIZE
Series
Interconnect*
The results of the acceptance tests carried out by the sub-
contractor(s) and the incoming inspection by vendor shall
be included in this lot EIDP.
Positive End
termination*
Negative End
termination*
Interconnect for
pull test*
Bypass Diode*
Ge Wafer
Coverglass
Cover glass
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bonding adhesive
(DC 93500)
# Except the humidity test and Weldability tests, all other acceptance tests are nondestructive and hence the tests may be conducted on samples selected
from the shipping lot. Weldability tests are to be carried out on 32 SCAs and
32 weld samples have to be realized from them. Humidity test are to be
carried on 32 SCAs. The humidity and Weldability SCA samples shall be long
to the same manufacturing lot as the shipping lot but not part of the shipping lot.
* Vendor to specify.
ISRO reserves the right to carry out any additional test(s) mentioned in
qualification test plan if necessary, after discussing with the vendor. The
acceptance test plan, sample size for such tests shall be finalized after
discussion.
3.2 QUALIFICATION TESTS AT ISRO
• A development model Panel/ Coupon will be fabricated by ISRO using
flight representative CFRP substrate and the first lot SCAs supplied by
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the vendor. This panel will be subjected to qualification level acoustic,
vibration and thermovac cycling. The test conditions and acceptance
criteria will be supplied to the vendor and in case of failure in any of
these tests, vendor will assist ISRO in resolving the problem.
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4 TEST METHODS AND CONDITIONS The in-process, qualification and acceptance tests for the SCAs and allied
materials manufactured according to the required specification shall be
performed in accordance with the test methods and test conditions specified
in this chapter.
4.1 VISUAL INSPECTION
The SCAs shall be visually inspected using stereo zoom microscope of 10x
magnification. The inspection criteria for 40mm X 80mm cells nominal
dimension shall be provided by vendor and shall be mutually agreed upon as
mentioned in 2.10. The SCAs shall also be inspected using EL
(electroluminescence) technique and vendor shall provide the acceptance /
rejection criteria.
4.2 DIMENSIONS
The overall dimensions of the cell, the dimensions of the cover glass, its
position, interconnect and its position shall be measured with optical
templates or in a profile projector for conformance to the drawings.
4.3 SCA MASS Weighing the samples with an accuracy of within ± 1.0%, and dividing by the
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number of samples shall determine the average SCA mass.
4.4 ELECTRICAL PERFORMANCE The electrical performance of the SCAs shall be measured under 1 AM0
(1367 W/m2, WMO spectrum) illumination simulated by a class A sun
simulator, whose spectral response over the wavelength band of interest
closely matches that of the sun at 1AU from the sun in all the three
wavelength bands. The sun simulator intensity shall be set to match the Isc
and Voc at 28°C, using a set of secondary standards traceable to a balloon
flown primary standard (or any Govt. / non Govt. organization with history of
carrying out such balloon flight experiments. Vendor shall ensure that the
secondary standards are evaluated under class A solar simulator whose
spectral composition is close to WMO e.g. ESA/ESTEC) of the type
identical to the SCA being measured.
After setting the intensity and temperature, four reference SCAs of the type
under measurement shall be evaluated. The set-up shall be considered ready
for electrical evaluation of SCAs/ solar cells, if the Isc and IT of the reference
SCAs match within 1% of their standard value and the Voc matches within
1°C in temperature setting. Otherwise, the exercise shall be repeated after
adjusting the sun simulator intensity again. Suitable load and data acquisition
units shall be used for evaluating the SCAs/ solar cells.
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4.5 TEMPERATURE COEFFICIENTS The open circuit voltage, short circuit current, maximum power, the current
and voltage at the maximum power point, the fill factor and the efficiency shall
be measured between +28°C & +100°C and between +28°C & -50°C to
determine their first order temperature coefficients. Measurement shall be
made at 5 different temperatures in each of the two ranges.
4.6 WELDED CONTACT INTEGRITY The welding procedure adopted shall not degrade the output current of the
SCA including the diode. Series interconnects welded to the front contact of
the bare cell and the bypass diode and rear contact of the SCA including the
diode shall be tested, by pulling the interconnect tabs both in 0°and 45°. The
cell, diode or SCA shall be clamped to Unitek micro-pull tester or equivalent
such that the restraining force is applied on at least 40% of the cell/SCA area
and pulled at a speed not exceeding 40 mm/min. Minimum acceptable pull
strength per tab is 300 gram force and 150 gram force when pulled at @0°
and 45° respectively.
4.7 CONTACT UNIFORMITY The contact thickness uniformity for each fabrication lot shall be within
specified limits as defined in PID. Front and rear contact thickness shall be
measured using a Beta scope or equivalent. Measurement shall be carried
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out for each evaporation batch (metallization lot).
4.8 THERMAL CYCLING TEST
The SCAs/cells/diode shall be subjected to the following tests:
• Prior to thermal cycling, samples shall be subjected to a high
temperature soak at +150°C in an inert atmosphere for one hour.
• 50 thermal cycles –100°C to +150°C in vacuum, 30°C/minute,
maximum average temperature rate, no dwell is required.
• 2025 thermal cycles from –175°C to +130°C in an inert atmosphere
with 30°C/minute, maximum average temperature rate, no dwell
is required.
During the post thermal cycling electrical evaluation as per 4.4, the power
degradation due to the test shall be within 2%. This and weld strength
specifications shall be met on every SCA/cell/diode. Vendor shall specify the
acceptance criteria for the bypass diodes.
4.9 HUMIDITY
The SCAs shall be stored for 96 hours in a chamber at a temperature not less
than 65°C and relative humidity 95±5% at ambient pressure. Subsequently
the cells shall be dried for 2hrs at 80°C. Following the exposure the SCA
electrical output measured as per 4.4 shall not degrade more than 2%. It
shall also meet the requirements of tape peel test as per para 4.12.1
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4.10 IRRADIATION
4.10.1 PARTICLE IRRADIATION
Electrical evaluation of the radiation test samples before and after irradiation
shall be carried out by standard third party lab like JPL or SPASOLAB.
Test Condition:
Measure I-V data of the solar cells at +28°C before and after proton radiation.
Requirements:
• Establish normalized radiation degradation curves for Voc, Isc, Vmp, Imp,
and Pmp, including nominal and 90% confidence values.
• Subsequently the cells shall be subjected to Photon Irradiation Test as
in 4.10.3.
• Spectral Response (SR), External quantum efficiency (EQE), Internal
quantum efficiency (IQE), Temperature Co-efficient and Radiometric
properties to be measured before and after radiation of the samples.
Data to be provided:
• Remaining factor of all the parameters for each fluence.
(i.e. Ratio of EOL and BOL efficiencies for each fluence level)
• Establish EOL Eff. vs. Blue/Red ratio curve for each fluence.
• Each new reactor shall be validated at one energy/fluence, and
The vendor shall also provide the following data related to the cells used for
this test (i.e. Electron irradiation & Proton irradiation) along with the
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corresponding population averages.
• Blue/Red Ratio
• BOL Efficiency
• Voc
4.10.1.1 ELECTRON & PROTON IRRADIATION
Vendor shall provide the results of electron and proton irradiation testing of
the proposed solar cell for the following energies and fluences (typical).
Vendor shall also include in the price bid as option, the pricing for carrying out
these tests.
Electron and Proton Irradiation Test on the cells shall be carried out as
follows:
For each irradiation level a minimum of 12 cells shall be taken. These cells
shall be selected such that, they are from 3 different current classes namely
maximum, average and minimum and from 2 evaporation lots and from a
minimum of 2 MOCVD reactors in case more than one reactor is used for
production of deliverable lot. Electron and proton uniformity shall be
maintained at ±10% and temperature maintained at 20°C±10°C during
irradiation. The test shall be performed in accordance with JPL standard
procedures as published in JPL Publication 92-09 at a standard facility, which
has a heritage of being used for space quality solar cell irradiation. If any,
alternative standards established by other space agencies are used details
shall be provided. Subsequent to the electron irradiation, the cells shall be
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subjected to 8Hrs photon irradiation as in 4.10.3.
The vendor shall furnish the degradation factors for power, current and
voltage at the fluence levels defined earlier in addition to the omni directional
electron relative damage co-efficient (RDC) as function of electron energy
and shielding thickness.
SR, EQE, IQE, temperature coefficients and radiometric properties should
also be measured before and after the test.
The energy and fluence table for Electron irradiation test is given below:
Samples
Energy (MeV)
Fluence per cm2
12 0.6 2x1013
2x1014
1x1015
2x1015
12 1 3x1013
1x1014
5x1014
1x1015
12 12 1x1013
1x1013
5x1013
1x1014
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The energy and fluence table for Protron irradiation test is given below:
SAMPLES ENERGY FLUENCE PER CM2
1E10 3E10 1E11 3E11 1E12 3E12 12 20 KeV X X X X X X 12 50 KeV X X X X X X 12 100KeV X X X X X X 12 300KeV X X X X X X 12 1MeV X X X X X X 12 3MeV X X X X X X 12 10MeV X X X X X X
4.10.2 PHOTON IRRADIATION
The SCA samples shall be subjected for 48 hrs of standard AM0 spectrum
exposure under a suitable solar simulator. The cells shall not show
degradation more than 2% from the original current at load point voltage as a
result of photon exposure.
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4.10.3 PHOTON IRRADIATION (SHORT DURATION)
The SCA samples shall be subjected for 8 hrs of standard AM0 spectrum
exposure under a suitable solar simulator. The cells shall not show
degradation more than 2% from the original current at load point voltage as a
result of photon exposure.
4.10.4 UV IRRADIATION (FOR SCA ONLY)
SCAs shall be subjected to a UV equivalent of 1000 sun hours of WMO
standard AM0 spectrum, under minimum of 10-5 Torr vacuum, at temperature
≤ 40°C. Within 48 hours after the completion of the irradiation, the samples
should be electrically evaluated, as per 2.4 and the average short circuit
current degradation shall not exceed 2%.
4.11 RADIOMETRIC PROPERTIES
4.11.1 SOLAR ABSORPTANCE
The spectral reflectance of electromagnetic energy shall be measured from
0.28 to2.5 micrometers with Edwards’s type integrating sphere equipment or
equivalent. The test data shall be integrated over the solar irradiance and the
integral subtracted from unity to yield the solar absorptance.
4.11.2 HEMISPHERICAL EMITTANCE
Measure spectral reflectance in the wavelength ranges from 2.0 to 26
micrometers and integrate over 300K planckian radiator functions. The
measured data should comply with the requirement of 2.5.
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4.12 CONTACT AND COATING ADHERENCE
The cells shall be exposed to a relative humidity of 95 ± 5% at a temperature
of 95°C for a period of 2 hours. Before and after this test, tape peel test as
described below shall be conducted on the cell front side.
4.12.1 TAPE PEEL TEST
Scotch brand Magic transparent tape No.810/ 600 with an adhesion to steel
value equal to or exceeding 33 grams per cm width shall be placed on the
surface to be tested. The tape shall be rubbed well ensuring that it adheres
firmly to the surface and stripped at 90° to the surface. Not more than 1% of
rear contact, 5% of the AR coating shall be removed by the tape and there
shall be no peeling of top contact pads.
4.13 INTERCONNECT FATIGUE
The interconnect loop in the form to be used in SCAs shall be subjected to
the mechanical flex test to establish the interconnect fatigue life. The
configuration of the flex test and the deflection shall be jointly worked out by
the vendor and ISRO after studying the proposed interconnect drawing.
4.14 SPECTRAL RESPONSE
The spectral response (SR) of the SCAs shall be measured by comparison of
the short circuit current of the test cell with the output of a spectral standard
of known relative spectral response under monochromatic irradiation.
• At various discrete wavelength intervals between 0.3 and 2
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micrometer using narrow band interference filters or
• By means of a high intensity monochromatic light, for continuous
recording between 0.3 and 2 micrometer wavelengths. The
minimum spectral irradiance shall be 100 microwatts/cm2.
EQE and IQE of SCAs shall also be measured similarly following the
standard protocol.
4.15 REVERSE BIAS SCREENING
Reverse bias screening test for the cell shall be spelt out by the vendor to
assess that the solar cell shall not degrade due to reverse bias applied on the
cell. The vendor shall specify test specification, test methodology and
allowable degradation criteria. Samples failed once shall not be subjected for
retest. The supplier shall also provide the yield of the reverse bias screening
test. The screen shall be performed on the 100% samples selected for ISRO.
4.16 ANGLE OF INCIDENCE TEST
SCAs should be taken from random current classes and should be subjected
to angle of incidence tests. The I-V characteristics of the SCAs shall be
measured at 0°, 20°, 40°, 60° and 80°.
4.17 SHADOW TOLERANCE TEST
The mean IT of SCAs shall not decrease by > 2 % and any individual SCA IT
shall not degrade by more than 3%, when subjected to partial shadowing.
This condition shall be simulated by reverse biasing the test samples to 1.22
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Isc at 90 + 5°C/ -0°C for 30 minutes in dark.
4.18 BY PASS DIODE / SCA LIFE TEST
Qualification test SCAs shall be subjected to 3000 Reverse Bias Cycles
from 1.1 Isc for 30 Secs to zero mA for 30 sec in a Thermo Vacuum Chamber
(
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5 PACKAGING, DELIVERY AND SCHEDULES 5.1 PACKAGING
The SCAs and allied materials shall be packed in containers of design
approved by ISRO with adequate protection from damage during transport
and handling. Special care should be given for interconnects. The
containers shall be heat sealed in an airtight water proof barrier as per MIL-B-
22191, together with sufficient bagged, activated dry desiccant as per MIL-D-
3464 and tarnish inhibitor to prevent contamination to assure compliance as
per chapter 2.0. A card type humidity indicator scaled 10 to 80% of relative
humidity shall be placed in each sealed bag. Any packaging or desiccating
material used shall not affect the electrical and mechanical properties of the
SCAs and allied materials. The vendor shall submit a packaging and storage
plan for ISRO approval prior to the first lot shipment.
5.2 TRANSPORTATION AND PACKAGING ACCEPTANCE
Inspection of the packaging for shipment shall be as per 5.1 of this
document. Contents of the damaged containers will be rejected. In case, the
humidity indicator accompanying the SCAs indicates a humidity level greater
than 40%, the defective container shall be rejected. Any SCA, which does not
meet one or more of the acceptance test requirements, shall be rejected.
5.3 DELIVERABLE DOCUMENTS
The following documents shall be submitted in the form of permanent files at
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the appropriate time. All documentation shall be in English.
The quotation shall contain the following.
• Technical Data on the proposed SCA as per 5.3.1
• Export Control Document requirements of the proposed SCAs.
• Quotation for
o the proposed SCA
o Allied Material as per of 5.5 (Sl. No. 3 to 10)
o Lot Acceptance Test (LAT) as per 3.1.3
o Type Approval Test (TAT) giving group wise breakup
o Life test Coupon Fabrication as per 3.1.2
o Life test Coupon testing as per 3.1.2
o ESD test on Coupon As per 3.1.2
• For preparation of the quotation, commercial guidelines shall be
followed.
5.3.1 DATA/ DOCUMENTS REQUIREDALONG WITH THE PROPOSAL
The technical proposal shall include but not limited to the following.
1. A compliance matrix for this proposal in a spreadsheet.
2. Description of the hardware offered including necessary drawing
and images.
3. Manufacturing & Qualification / flight heritage.
4. Comparison of the qualification status of the hardware offered
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against standard international specifications.
5. I-V characteristics of a typical SCA with lot average efficiency
specified in the form of a table and plot at 28°C to 60°C and
110°C under standard AM0 spectrum before and after
irradiation with 1x1014 1 MeV electrons/cm2 and 5 x1014 1 MeV
electrons/cm2.
6. Bending radius of the SCA at maximum curvature.
7. Quality manual
8. Cross sectional diagram of the SCA with thickness of the
different layers.
9. Product assurance plan including fabrication and process control
aspects reliability analysis. Non-conformance control and
approval of configuration control and traceability.
10. Maximum Panel size and test levels of CFRP qualification panel
tested by vendor for qualifying the triple junction SCAs.
11. Qualification test reports on the SCA and allied materials
including the bypass diode.
12. Documentation of bare cells, semi-bare cells, and cover glass.
13. Absolute typical spectral response of the proposed solar cell.
14. Remaining factor of the parameters Isc, Imp, Vmp, Voc and Pmp
for each of the fluence levels 3x1013, 1 x 1014, 5 x 1014, and 1 x
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1015 of 1MeV electrons /cm2. (i.e. Ratio of EOL and BOL
efficiencies for each fluence level).
15. Details of solar simulator used to evaluate the triple junction
solar cell.
16. Export Control Document requirements of the proposed SCA.
5.3.2 ALONG WITH PID
All documentation shall be submitted as three hard copies and one copy in
electronic form. The PID as per 3.1.1.1 shall be submitted on receipt of the
contract document. The PID shall include all the details specified in Chapter
2.0 of this document. The PID shall be accompanied by the following
documentation.
1. The omni directional relative damage coefficients of the triple
junction solar cells as a function of the shielding thickness for the
following electron and proton energy ranges. Electron 40 KeV to
7 MeV. Proton 100 KeV to 200 MeV.
2. Blue/ red ratio of the proposed solar cell at the beginning of life
and after experiencing 5E14 and 1E15 equivalent 1MeV electron
fluence.
3. List of materials used, with their quality levels derating criteria
and failure rates.
4. Cell diffusion capacitance as a function of voltage and
temperature (28°C, 65°C and 110°C at BOL and after irradiation
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at 1 x 1015 and 5x10141MeV electrons).
5. Dimensional drawings of all hardware with tolerances.
6. Spectrum of the sun simulators used by the vendor in the form of
a table and plot.
7. Calibration procedures for the secondary standards.
8. Thermal conductivity of the solar cell.
9. Thermal coefficient of expansion of the solar cell.
10. Packing and storage conditions for the SCAs.
5.3.3 ALONG WITH EACH LOT OF SCA
The following documentation shall accompany every deliverable lot. All
documentation is to be submitted as three hard copies and one copy in
electronic form.
1. The entire acceptance test records and results shall accompany
each shipment of SCA.
2. The vendor shall provide measured performance data (Voc, Vmp,
Isc, Imp, IT, I at 1.2V, I at 2.55V and measured Vr during reverse
bias screening)) for all delivered SCAs in electronic format.
3. A certificate from the vendor that the lot has successfully passed
the acceptance tests shall accompany each deliverable lot.
4. Standard SCAs (set of four) I-V characteristics measured as per
specification and spectral response in the form of a table and
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plots (with digital data in excel).
5. Waivers and non-conformances during cell/ SCA manufacture by
vendor or Sub-contractor and dispositions thereof.
6. Quality control results in the form of Statistical Process Control
(SPC) Charts for the various processes including SCA making.
5.4 HARDWARE DELIVERABLES ISRO decides the no of SCA’s to be procured as per the requirement. Vendor has to
quote from 10000 to 100000 SCAs in slabs of 10000 SCA’s. The no. of shipments be
mutually agreed between vendor and ISRO, First shipment to last shipment time
period is 24 months.
Sl. No ITEM Quantity
1 SCAs Number of allied materials required for 10000
SCAs is as follows
2 Secondary Standards Set (Each set consisting of 3 sub cells and 1 full cell)
3 sets
3 Positive end terminations (consists of 1busbar and interconnects equal to the number of
2000 sets
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interconnects in the SCA)
4 Negative end terminations
2000
5 Interconnects For Pull Test (equal to the no. of interconnects in the SCA)
2000 sets
6 Repair Interconnects (equal to the no. of interconnects in the SCA)
2000 sets
7 Germanium Substrates (4 inch and 6 inch)
50 each
8 Smaller size cells area around 10 cm2
1000
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ANNEXURE A – ENVIRONMENTAL REQUIREMENTS
The SCA and the allied materials shall be designed to meet the performance
requirements before, during and after exposure to the environments specified
below. The environments experienced during fabrication, transportation and
storage of the SCAs and allied materials shall be significantly less severe
than them.
A1. PRE-DEPLOYMENT A. On Ground : Relative humidity (Rh) of 70% max at 760 ± 25 mm of
Hg barometric pressure over 23± 5°C temperature range
B. In Space : -180°C to +125 °C (10 cycles).
C Acoustic noise : 146 dB overall for 2 minutes.
D. Sine vibration : 30g peak, 20-50 Hz; 10g peak, 50-100 Hz
E. Shock : 113g @ 200 Hz increasing to 450g @ 400 Hz;
450g max. @ 400 to 500 Hz;
600g max.@ 1600 to 4000 Hz.
A2. DURING DEPLOYMENT A. Barometric pressure : < 1.0 x 10-10 Torr
B. Temperature : -180°C to +125°C
A3. POST DEPLOYMENTS
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A. The SCA shall be designed and manufactured to withstand 15 years of
GEO life (2025 thermal cycles between +130°C to -165°C and 4500
thermal cycles between +130°C and -100°C)
B. Barometric Pressure less than 1 x 10-10 Torr.
A4. RADIATION A4.1. GEO ORBIT
A4.1.1. ELECTRON RADIATION The minimum-trapped electron environment in synchronous equatorial
orbit, which the SCAs shall account, for, based on the AE-8 model is presented in Table 1.
TABLE 1: ELECTRON FLUENCE AE-8¸ MAX MODEL Energy Level
(> MeV) Flux: e/cm2/sec
0.04 4.6 x 107
0.1 4.2 x 107
0.5 4.0 x 106
1.0 4.9 x 105
1.5 1.2 x 105
2.0 4.1 x 104
2.5 1.1 x 104
4.0 4.9 x 103
4.5 1.6 x 103
4.0 4.5 x 102
4.5 1.2 x 102
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5.0 4.5 x 101
A4.1.2. PROTON RADIATION
Table 2(A) describes the low energy proton environment, which the design
shall account for, for time averaged integral flux spectrum. The estimate for
the high-energy proton spectrum, which represents the solar flare Content of
the 20th cycle, is shown in table 2(B)
TABLE 2A: PROTON FLUX - LOW ENERGY
Energy Level
(> MeV) Flux: p/cm2/sec
0.01 2.74 x 107
0.03 2.0 x 107
0.05 1.51 x 107
0.07 1.12 x 107
0.10 7.21 x 106
0.20 1.64 x 106
0.30 6.54 x 105
0.40 2.61 x 105
0.50 1.04 x 105
0.60 4.17 x 104
0.70 1.65 x 104
0.80 6.52 x 103
0.90 2.58 x 102
1.00 1.02 x 102
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1.25 1.00 x 102
1.50 9.85 x 100
TABLE 2B: PROTON FLUENCE - SOLAR FLARE Energy Level
(MeV) Fluence : p/cm2/cycle
1 1.2 x 1011
4 5.5 x 1010
10 4.28 x 1010
30 9.78 x 109
60 2.95 x 109
100 6.69 x 108