results of analysis for case no. 2807 and case · pdf fileenclosed are the results of analysis...
TRANSCRIPT
ENVIRODYNEENGINEERS
June 18, 19842044
Dr. William LangleyUSEPA, Region VI6608 Hornwood DriveMonterey Park Plaza, Building cHouston, TX 77074
Dear Dr. Langley:
Enclosed are the results of analysis of one soil sample for 2,3,7,8-TCDD fromC&se Mo. 2807 and three water samples for 2,3,7,8-TCDD from SAS 1153F. Thecontents of this report are listed on the following page.
The data for sample DF000402 was omitted from1984) because the extract was dropped in preparationsamples were analyzed according to the proctidu(July 1982). The detection limits for thes^ s.the suggested method detection limit of 0.005sample were available for analysis rather thanrecommended in Method 613.
the original report (June 1 2,ration. The three water
idure described in EPA Method 613samples are slightly higher thanug/1 because only 200 ml ofthe 1 liter sample volune
If you have any questions regarding these data, please contact me.
Sincerely,
Earl M. Hansen, Ph.D.Senior Associate
EMH/csgEnclosures
TABLE OF CONTENTS
Form NO.
B-1
B-2
B-3
B-4
Attachment No.
Data Summary
Initial Calibration Summary
Continuing Calibration Summary
GC Operating Conditions
Mass Chromatograms, Colunrj Performance Check
Mass Chromatograms Standards
Mass Chromatograms Samples
Partial Scan Data
Mass Chromatograms, Rejected Analyses
GC/MS Calculation Notebook! Pages
Analytical Chronology - GC/MS Logbook Pages
Chain of Custody/Packing list
FORM h-1. T<; l ) l ) DATA REPORT FORM
I.ab: Rr
i-asr No.
Batch/Shi
SampleNumber
MBDF000422
l)ro00424
ivirodyne
: 1153F
pnent No.
ExtraCleanup
NN
N
Er
SV
iqinee
ampleol une( m i s )
200225
212
rs , Inc
TCDDMeas
NDNO
ND
(ug/1). D.L.
0.00510.1)0770.0076O.OU87
GC/MS AnalysisInstr.1.0. Date Time
2 6/17 16172 6/17 1707
2 6/17 1808
Rel. lo32U/322
1 .051 .0)
1 .H6
n Abund.332/134
0.770.77D.8 )0 .7B
SurrogateMeas. »
y.77q.H6
10.1 1
(ng)Accy.
•)a•»•)
1)1
320
1 115
25
R322
1115
13
elative2
F
Ion57
11
5
'eport Date:
Column:
i Abundance3283
588476
582
Page 1 of 1
6/18/84
SP-2330
FRN332 334 No.
1279 1671 105541027 1339 10555
1233 1585 10557
Notes: RB = Reagent Blank P = Part ial Scan/Confirmatory Analysis D = Duplicatf /Fnrt i t ied Field BlankFB = Field Blank KRN = File Reference Number D.I,. = Detection L i m i t
M -= Native TCDD SpikeND = Not Detected
by
0 0 1 5 9 0
FORM B-1. TCni) DATA RKPORT FORM
Lab: E
CasB No
Batch/sh
Samplenumber
[1P000402
[nvirodyne ]
..: 2807
ipment No.
ExtraCleanup
N
FB = Fiffid
Engineers
WetWelyht( y r a m s )
10.0
Biflnk
i. Inc.
TCDDMeas.
Nt)
FRN =
(ppb)n.L.
0.10
File
GC/MSInstr.I .D.
2
Referencf
Analysis
Date Time
6/17 1'?12
• Nunber
Rel. 1'320/322
0.620.6H
on Abund. Surr332/334 Meas
0.77 9.74
D.T,. = n"tectj
q[ate*
./FOL i '
( n g )Accy.
l.l7
m i t
Relative320 322 25
10 15
ND = Not
Re
Ion7
9
ryt
!port Date:
Column!
Abundance328'1
650
acted
Page 1 of 1
6/18/84
SP-2330
PRN332 334 No.
1420 1853 10551!
"r-orrecteii for co by native TCDD; 0.91 of m/z 322 suht€whf{\.
0 0 1 5 9 1
FORM B-2. INITIAL CALIBRATION SUMMARY
Date(198
5/65/65/65/65/65/65/65/115/115/115/115/115/115/115/115/115/115/115/11
MeanAccuRel.
Solu
PCCC1CC2CC3CC4CC5
Instr. FRN Solution4) I.D. Number I.D.
2 10091 PC2 10092 CC12 10093 CC22 10094 CC32 10095 CC42 10096 .CC52 10099 PC2 10108 PC2 10109 CC12 10110 CC22 10111 CC32 10112 CC42 10113 CC52 10115 CC22 10116 CC42 10118 CC32 10119 CC52 10120 CC12 10121 PC
Accuracy, Surrogate Measurements:racy, Fortified/Spike Field Blank;Diff . ( % ) , Duplicate Analysis:
tion ID Codes:
= Performance check solution= Concentration calibration solution= Concentration calibration solution= Concentration calibration solution= Concentration calibration solution= Concentration calibration solution
MeasuNative
1.040.970.960.930.90
0.930.900.870.830.830.910.850.870.831 .02——
QUA]
/
=f=No. 1 =No. 2 =No. 3 =No. 4 =No. 5 =
red RFSurrogate
1.201 .091.08--
1.030.960.94--
0.93-
0.94
———1^08
[/rTY CONTROL/
———-/-/
0.2 ug/ml1.0 ug/ml5.0 ug/ml
20.0 ug/m140.0 ug/ml
TCDMean RF Used
Native Surrogate (Ap
SUMMARY '--^'^
No. of Data Pornts:Sample NO . /Sample No. /
J/iv^
D Isomer ResolutionPercent Valleyplies for PC only)
2
22
1.5
\\
- )
.ie cwf11^'
00
FORM B-3. CONTINUING CALIBRATION SUMMARY
Date Instr. FRN Solution(1984) I.D. Number I.D.
6/17 2 10552 PC6/17 2 10553 CC16/17 2 10565 PC6/17 2 10566 CC1
Mean Accuracy, Surrogate Measurements:
Accuracy, Fortified/Spike Field Blank;
Rel. Dif f . (» ) , Duplicate Analysis:
Solution ID Codes:
PC = Performance check solutionCC1 = Concentration calibration solutionCC2 = Concentration calibration solutionCC3 = Concentration calibration solutionCC4 = Concentration calibration solutionCC5 = Concentration calibration solution
MeasuNative
0.90
0.85
OUAI4r /--
———^\—--•NA
NA
NO. 1 =No. 2 =No. 3 =No. 4 =No. 5 =
red RFSurrogate
0.98
1 .07
LITY CONTROL
^
0.2 ug/ml1.0 ug/ml5.0 ug/ml
20.0 ug/ml40.0 ug/ml
TCDD Isomer ResolMean RF Used percent Valley
Native Surrogate (Applies for PC o
10.91 1.02
10.91 1.02
-SI1MMARY ^ V^
No. of Data Points: ?7.8*3 J i Y 7
•"-————^ I -
Sample /Ro. ' ' \
\ ^m P^-\ ^ ^ r / '
ut
nl
V1
v
-on
y)
^
0 0 1 5 9 3
FORM B-4. GC OPERATING CONDITIONSConditions B
Column Coating
Film thickness
Column Dimensions
Helium
Initial Temperature
Initial Time
Temperature program
2,3,7,8-TCDD Retention Time
SP-2330
0.20 urn
60 m x 0.25 mm
26 psi
160°C
3 minutes
25°/min to 240°C and hold-.
19.2 minutes
j-
l'"'1 •,
LCi• —0
ATTACHMENT 1
MASS CHROMATOGRAM, COLUMM PERFORMANCE CHECK
1368
10££2ITCDD C O L U M N PERF 1NCE CK COND B 2UL|e.-17-84 TW J(»» -w..a- ' is'e
454 fain
AA
.A--,
A
Aw"A""ABBHHI
,A^E3EOD
/ \ I'BAJJH
nEBCTO
AAA
u—A
A
A
r S | |
^
^•-•^
———'———————————————————-——————
^0
sn•;—
0
O P T I O N S
RREfl TflELE ENTRIES: FRN 10552
Entr^ T i m e
20.720.720.720.720.620.6
Mass
319.9321.9322.9327.9331.9333.9
flr-eel
2492.3160.
431.64.
599.731.
7S..1 0 0 . 1
13.'2.
18.23.
CRLCULRTE •/. ON ENTRY #:RRER TRBLE ENTRIES; PRN 10552
Entr-i^ Time
20.720.720.720.720.620.6
CRLCULRTE •/;
Mass
3 1 9 . 93 2 1 . 9 ••322.9327.9331 .9333.9
ON ENTRY «:
Rrca
2492.3180.431.64.
5 9 9 .731.
340.9435.0
58.98.7
82.0100 0
ITCDD C O L U M N PERt '^^MNCE CK COND B 2UL16-17-84 1545 J@*
^ ^l110'
ITCDD COLUMN P@ERFORMflNCE CK MI.^:»2 COHIi S 2LIL1 6 - 1 7 - 8 4 2 2 1 6 JJC
A A.M. Aii E^
A AM A
/ <
21
.A.
f l R E f l T f l E L E E N T R I E S : F R H 18565
E n t r1 y T i in e-
20. 628. 628 .£28.620.5
CflLCULRTE •/.
3 1 9 . 9321 . 9322. 9331. 9333. 9
ON ENTRY » ;
Rr-ea
6266.7966.1082.15B4.1825.
78. 9iBe.e
13.618.922.9
RREfl TRBLE ENTRIES; FRN 10565
E n t r- y T i n'i e-
1 20.62 20. 63 28. 64 20.65 20.5
CflLCULRTE •/.
Mass
3 1 9 . 93 2 1 . 93 2 2 . 9331 . 93 3 3 . 9
ON ENTRY » ;
Rrea
6286.7 9 6 6 .1062.1504.1825.
344.5436.55 9 . 3B 2 . 4
1 3 6 . 0
ITCDD COLUMN P(?Et?rORMFlNCE CK MIX«2 CONti B 2UL16-17-84 2 2 1 8 JJC
V ^—i—21
^'/^W ,o
ATTACHMENT.2
MASS CHROMATOGRAMS STANDARDS
RREfl TRBLE ENTRIES; FPH 18553
E n t r y T 1 fil 6 Mass
123456
CRLCURRER
Entry
123456
CRLCU
28.628.628.62B.620.620.6
LflTE •-:TRELE
T i m e
20.626. 626.620.626.620.6
LRTE •/.
256.93 1 9 . 93 2 1 . 9327. 93 3 1 . 9333.9
ON ENTRY »:ENTRIES: FRN
Mass
256.93 1 9 . 93 2 1 . 9327.93 3 1 . 9333.9
ON ENTRY «:
Rr'ea
1 1 1 .330.412.247.
1798.2321.
1B553
Rrea
1 1 1 .330.412.247.
1798.2321.
26.980. 1
100.660. B
436 .2563.0
4 .814.217.810.677.5
100. 0
RREfi TflELE ENTRIES: FRH 1 6 5 6 6
Entr',' T i me Rrea
28.728. 620. 620. 62 0 . 628. 6
CRLCULRTE
2 5 6 . 93 1 9 . 93 2 1 . 9327.93 3 1 . 9333.9
ON ENTRY » ;
245.803.
1063.7 1 9 .
4850.6284.
2 2 . 674.2
1 8 6 . 06 6 . 4
448.0573. 1
flRER TfiELE ENTRIES: FRN 18566
Entr;.' T i me-
20.720.628.620.620.628.6
CflLCULRTE \
Mass.
2 5 6 . 93 1 9 . 9321. 9327. 93 3 1 . 93 3 3.9
ON ENTRY » :
Rrea
245.883.
1083.7 1 9 .
4856.6264.
3 . 91 2 . 91 7 . 41 1 . 678.2
100.0
ATTACHMENT 3
MASS CHROMATOGRAMS SAMPLES3 RAMS
RREfl TRELE ENTRIES: FRH 18554
Entry T i m e Mass Rrea
123456
CRLCURRER
Entry
123456
CRLCU
26.28.28.2S.20.20.
LRTETRELE
T i r n
20.20.26.20.20.20.
LRTE
88eS88•/;
S
88888S'/,
256.3 1 9 .3 2 1 .327.331 .333.
ON ENTENTRIES
Mas
256.3 1 9 ,321 .327.3 3 1 .333.
ON ENT
999999RY *:! FRN
S.
99 ..9999RY «:
1 11 11 1
58812791 6 7 1
10554
Rrea
1 11 11 1
56812791 6 7 1
9 9 . 4105.2100.0
5475.81 1 9 1 9 . 115574.5
. 6
. 7
. 635.27 6 . 5
108.0
R R E R T f l E L E E N T R I E S : F R N 18555
Entr^' Time
1 20.82 28.S3 2 B . 74 28, 75 28.7
Mass
319.9321.9327.9331.9333.9
Rr-ea
15.15.
476.1827.1339.
180.9100. B
3179.06854.1893:3.2
CRLCULRTE •/; ON ENTRY » :RREfl TRBLE ENTRIES: FRH 18555
Entr^* T i m e
20 .620.820.720.720.7
CRLCULRTE ••'.
M&££
3 1 9 . 93 2 1 . 93 2 7 .9331 . 9333. 9
ON ENTRY » ;
Rrea
1 5 .1 5 .
476.1027.1339.
1. 11. 1
35.676.7
1 0 6 . 0
|2044-2Se7-lI53F;Dr"gS423 TOND B 2UL16-17-84 1737
-•,.-.. -i'--,A' -._'".y
787
28
f lREf l T f l B L E E N T R I E S ! F R N 18556
Entr",' T i f f i e Mass
2 0 . 628.820.820.820.8
CRLCULRTE
3 1 9 . 93 2 1 . 9327.93 3 1 . 9333. 9
ON ENTRY
20.20.
648.1537.1843.
9 9 . 7188.0
3 2 5 9 . 97727.I9 2 6 6 . 4
B R E R Tf lBLE E N T R I E S ; F R N 18556
E n t r y Time
20.828.820.820.820.8
CRLCULflTE •/.
Mass
319.9321.9327.9331 .9333. 9
ON E N T R ' i ' »:
Firea
26.20.
648.1537.1843.
1. 11. I
35.283. 4
180.0
f l R E R T R B L E E N T R I E S : FRt-1 10557
E n t r y T i m e
2 B . e20.820. S20.820.82 6 . 8
CflLCULRTE •/.
Mas-s
256. 93 1 9 . 93 2 1 . 93 2 7 .93 3 1 . 93 3 3 . 9
ON ENTRY »:
Rrea
5.25.1 3 .
582.1233.15S5.
36. 1185. 51B0. 6
4 3 1 6 . 39 1 4 8 . 9
1 1 7 6 4 . 4
FiRER TRBLE ENTRIES: FRN 10557
E n t r y T i m e
20.820.820.820.820.820.8
CRLCULRTE ;;
Mass
2 5 6 . 93 1 9 . 93 2 1 . 9 .3 2 7 . 93 3 1 . 93 3 3.9
ON ENTRY • :
flrea
5.25.13.
582.1233.15S5.
.31 . 6. 9
36.777.8
i a e . 0
™
2044-2807 :11E:THOi- BLBNK CONS E 2UL6-17-84 1846 JJC
A934
-I~19 23 £1
RRER TRBLE ENTRIES: FRN 18558
Eritr ' , ' T i m e
28.720.728.728 .720. 720.7
Mass2 5 6 . 93 1 9 . 93 2 1 . 9327.9331. 9333.9
Rr-ea
22.11.18.
743.1639.2064.
125.56 2 . 3
108.84248.19 3 6 5 . 7
1 1 7 9 5 . 6CRLCULRTE \ ON ENTRY t t :RRER TRBLE ENTRIES! FRN 10558
Ent ry T i m&
20.720.720.720.720.720.7
CRLCULRTE •/.
Mass
2 5 6 . 93 1 9 . 9 .3 2 1 . 9327.93 3 1 . 9333.9
ON ENTRY »:
Rrea
22.1 1 .18.
743.1 6 3 9 .2064.
1 . 1. 5. 8
3 6 . 07 9 . 4
100.0
B R E R T f l E L E E N T R I E S ; F R N 10559
Ent ry
1•->
3456
CRLCUflRER
Erit r','
123456
CflLCU
T 1 rn e
20. 626.620.62B. 626.620.6
LRTE 'ATRBLE
T i m e
20.620.620.620.620.620.6
LRTE \
Mass
256.93 1 9 . 93 2 1 . 9327.93 3 1 . 9333.9
ON ENTRY »;ENTRIES; FRN
Mass
256.93 1 9 . 93 2 1 . 9327.93 3 1 . 9333.9
ON ENTRY »!
Rrea
9 .10.1 5 ,
65B.1420.1853.
10559
Rrea
9 .10.1 5 .
650.1420.1853.
5 9 . 36 6 . 2
10B.04306.69 4 1 2 . 412277.0
. 5
. 6
. 835. 17 6 . 7
100. 0
ATTACHMJEMT 4
GC/MS CALCULATION NOTEBOOK PAGES
19Notebook No..D^^«
,
! ;i
•
'~r /^L^ ^, JuqA .'\; L<<V
(^VYe^-.. X" ]
'„ i-/-'' i i
^^^^^
- ———
. . . -——i
"•t-'Jfd on P«ge
',• - ' , 1 / ^Date
pRn.iFnT2C2^ -^-y o?o -APo-l-^
F-t?M^hA£) '-Tc-nTi ^ui; L»/<;i. !i=iflpf: ! i -vJ^ra ^.f i7a/-t a,i9 r-
~ » - / • ! . - ' V -/
!r R^; QA-JS-^ rc n o Co L •J Pert ^r^
: : 1 • Jol'sAa^'--/^0/^I : ; 1 , : i
, JAO/SAo) -- 7 ^[
J3aA5- / -' ^a': , 1 ' 1 • . ! ; ;
; t -PA. ' iC>.5A3 rc-r^p Li jLey<-^ isrio*+Aa'7 ;" ; ^
\ . • , 33,0 33o -/ :
. -132- ^ ; 3 ^
^ 3 ah °?^7 ••: —— - ..... 3^- . ,^'7<5?.,..
- - - - ...-5^--- -^a; r' -
^•r r.. w'- ^5'- •r ^-y -'' ! -y^l-"??? ^«3AlJ!
^ r - S.^.t - (^n- /^C ; W-t ^^j 0. 0(»
-tf.^.^Ss^ 3. o^^ -a t c ,7 - ( ^SF ; lYkT. . . . - - . - - & ^ - ? . J < - ; - .
; 23S, n ^i ^ a.? '5"^ ''
is 5, fd,T^ -' ,. - ^3.^ . . U?i . . .:
: L-^- . ^ i+l( ^„<5^)^^.&/(;^ /^<?</(f^^0.c^
; - . P-r, -.. ^ .X 30 / !,J ? T! i!^ .0. - 3
; !
•
! . , .— •
1 . . • • ' ' ' ' i . . - 1
Ji^j. f JJ.C^ ^. //^Y' ' / "S.gnea Date
/£>3 i? ^lll'l^ rnn,inu.dP,o
r ^flr. LL' ( ^^A A 7 q " ^3^.' ^^a..^ ,
^J • Jl .
ho^£ Ck ,c<rt> 8 <3^
'/o.
t1/. > ' ' '
1 CO»J.O R , c?^ .'57 --»o ''/ p o , ^ ' r iy .so^)- -
/ /n? "lOCi
o.xi-. o,.3 o ^oAa.1 ! l?• C-E
--o,9?^...o.9£..:, 7 - -
^..^•. ^.^ .............'o^,i 00
- 1 1IQQ
i i,-)0o»v.3-. O.OOS-I^-^O^
w- Q^ ^"• -- • '
\ •. \ , ,
^^*r^~^> '——\ '~^ ^ •^'
^^A . ^r
i/ ',0
% .-i———-———-- . . v0
.
— — - - . - .0
^- - .
^•^.-d-^^ Cf^Q.^t.- 1
A (TO (-t-.f'^"*' :• J
- - ,^a,^^T- '
^^ -
'ficA'.'. . .r, '
• - —
Con,.-.,,..r., •.. .
"^~ ^/^/ef.
Notebook NoP P OJ E CT_^ =>1M^aS01 -.05 P o o
^ e.^J.flLSAs .ap'44-aso q-._PO<i+icJ?. HJ:l(Ji<-—A<-V. -- .5l5^-_-^.,^-LS^.,- Jot:(t>^.- .
: _JAo._^^_i_..._JJ. ^ ^^J^, .._.. . ^_.Mt2.__._. __.. ._J^ < .J-fl-0 . . . .. _._.-_3.as . . . ,,-l^J^ .3L .
- - 333. . . . . .'(t^^ .0 ^ -. - .- ,..-33^.. ... -.AOl.^-f. JQO . .
. . . _._.-„....-.-..-.. .[.^ .. - - . ^. . - ^ - y• ^-OR ' (s" •r 'J\5aXoLJ'.yC' T'-^O^^) 0.9J^-1.0^.-^'. Iv'Ls'^O^lLm^lyr^
.C^-^- r?^ ^ x.^o / ^7<-^4 ,20L^ f Mp 9^^ ^ ^^Z «^__,. .. _ J. ,W^^^r^
—.^JC.-S.S'?. -^aoa^-^Eii?-c^ooowA, j.Ce^J B . ^u,y . Jo o^-.\. . . . . ——A57-—.- - - ^ . - " - - ^ ( ?- -^ - . - - .- . - ^ - .
. 3'5t0 . }Q ^ ^(t^ . - - - - - — . - . - - . . - -2o) 5 . . ._ ^a' .^ . y 0 C.3c3E' . . .((^"-' •' 3c - . . . . .3J.2, n^ -- n-7 .-33 ^J5i.J '". |;;0 . . . .
. . . . . . . , . . ^'\: c TJ '\5'QJi! 5 0" ao -1? 53') 0.9/ A. ' 3 c^ ^ 0</ 0 f '- Q. ;C -r^ | n
.ws. r^ - ^A-O XA'O / (/ ^o!a + /^£3y 0^--^=^- -- <? 7 . ._ . . .. . . . . .^ - ,^^i
^-<^_ - . .*—<(" - 4 " --i • "-^•y^^"-'^^ .CY.^-^. — ^C^'.y^fe.)
' . - - - - ^"/ . -'^-r1-"^c^-v^-. — ^'/c^'-y
- - - - /l/ -/(:
. . .^A. L///'"'
'- •cs - -, ^-^•^ / -- / ">.'" • ' -'^L^. ^- /^
P R OJ E CT_SQ_a3 ' OOai.57 Continued from Page- —_
Notebook No
i. rc.p0 a^O * / Orr ft. i . ^— - —^ fl . —~»<.J^c, ^-
• J^ .&5^--_-
_3ao_,__._s^_s..^...__• i^_-_39ia^. _ _.. _i .& 3 .- _. __(.£o-. _.._._. -_ai J' _''o9 •- .'c
-...3x3^ . . ' J ' 9 •[- . . ,-n .- .. . ^ - .___il3t? , -_ US^^ -/ - — _75 —•^_-__-_- - . - _ - _ _ . .
T c p p -- .^o3^j^3^J7--i£A'o^_^^o.^^.^O»S'J3 .L/^ ' 0 ^ .' -
r^ftr.^--. C?^^-^^;^^?^^^-^^^^^.?-^"^^^--^^.?., :-' '-"'/"c-. -0
?- o -
Notebook NoP R OJ E CT_ao_a3 -_ooAo^2_____<t//7lS-V
; •-$r-^J^s(^,_^LQ^_Le.,£.i. r^gp s-^o */ gp^y' 6 S,<-J! ' . .^-.-,.- &g7 an S ^ -^.s. -h,t- ^,fis^______'•- .
; - ..-.- - , , 333^ _ _ ^ ^ S J 3 3 , ^ . ___2^_K ' . ._.__. . . ._ _^ .' -_^__-_saa. _ . . J^.S 3 .. , _^..J-3... _ ._ _-^i^' .'•09 •- .•r" -^
Au) ^ i 0 ^ , r!
. _ . . .._i3a - ^y-S^<-'-^._ -_-3S ^-'. _ „_ __. _ . . - - _ _ . . • .,-,. ^-^ ___ i2 • } . _ _ _ _ _ _ L.-ti- .C-__J_o^a______________ .
T C D P ?£-- ^a3^J5-S3,!'».l Jla-Sfl'c'^-^^o.-f^.A ^0.°.5'3 ^ ./^ (- •3 ^ 1.—
':^-r.^,-- . ('.7^ q-JbJ / / ^.(-'^-"r^^a^O.O^^^^i-J 37'^'- '---'.'c 0
ATTACHMENT 5
ANALYTICAL CHRONOLOGIC - GC/MS LOGBOOK PAGES
oto^-a'iOT-^y-F f/Y\V-- lAoocdMfc^ -F KN JQJS < X .£) F/flCT m^s-^ QBT& 6 O?A,O1'ltHl TTC •)S'aJ3'C f « 7 ( » + 6/Y\V^^I»00
CftN^ •PK^^os.s-^ TCOO CB^y^^^LnS-oL crf^^> oLJ?< |KS- ;r-r<- , '^^\IS1S 3-3C Hl-t\SH -
C.R^(fl9 ^f>H IQ5~£3 TC.DD /o^e-eJ. sro»/ Co»«)t S ^AJ^J (p 30 JJC.
ci^Ndi^l ^KNJOS-S^ (3,&n4-a^o-7+(/&3^; irnfc+Yi.0 ft-x cano B A*^I w*^ ) ^•^ ^- '
CR»J(9^ ^K.^\Q££-£' £>oim-St'ro7-ft^3f--Wooo^a.3 ^-0 Q a^J?no73--3^
Cfc)J(cO| ^e.Nio&?(? o^o^•o!£o7-^A'3F.•0(t 000^3 CoNp P> oli\Vi')S'7.33'- ^^
Ce^t/^ ^HfJ105£'? o>02;^-s^o7-1^3?;0-<oooiA^ Coi^D 6 o?<J}1 ff rt & •T TCi e o & JJ-^
C^^bR 4'^^'o^^g ^o^i^-aso? n0aik°o '&LL{ Cfrn9 ft ^0)S^033-C. ' •
CRPb^f •FEO'o5£>(? ao^H-oifop-JD-Cooo^oa. ^(rrQ 6 o?-aJqia-ra'i^- ,-\
<^e^^ S")E-^)o£<i& o?Qt3i3-QQ3^7 (coa^o OptO ^"D 6 Q^J/''it-lJ-rc
CP.Md'l ^H)06(»; ^033-00^57 (,oa^3 Op-tO CCPT^ b -')-QAi'O M^ ^ r ^<
C.^^(,q ^(N^O^f;^ oioc33-OOA5L(!>OoH(( OptO C<rrS! B o^^,0^^ ^J^
C(?^fo^ ^PfJ^^fc^ o? Oo^-00^6-7. 6od^°( Oc-rr> ( rrSi 6 c^.Oa»» <~( sy-
CR^kq SR^ IO^ (<4 <^0al3-00o!&-? G0^3^0A)TD GcySfc ^^^'45 73^
C(Z»J (fq iFRt 1 0 5 b 5 T^DO <^1o^T-> PCR^ C^ ^^3. ^'- r\-'^.Aa;^ -3-3 •= . '-"
c.H^ W j?^ (o^t'G' 7 .00 ks^ l&ve/. STD^I Conofc a<i_9ol,3oo<tJ<-
ATTACHMENT 6
CHAIN OF CUSTODY/PACKING LIST
CLP Sample ManagementP.O. Box 818 - AlexandraPhone; 703/557-2490 -
Sampling Office:D^.AS.
Sampling Contact:IJIWCE 'St^H^,L-
(namey
l^ W»l,-fcfcc 1(phone)
SampleNumbers
i. nFo&Ol&i -''2. LiFftOOSOI. /
3. DFoRo4c^ ••4. O F f t ^ O M c ^5. OFftcO^OS -6. DFft f t040fc -/
7. PiFO^cyc'?- -/
8. ni-nft0</^9. D-F^O^&I
^0. 'DFoftc^lO ' '11. F.«a ^..lt "'12. F ^ i A ^>„^ •13.1».15.16.17.
IS.19.20.
Otticea, Virginia 22313FTS/557-2190
SPECIAL ANA1PACK
Sampling Date(s):^I^WDate Shipped:^lM/Site Name/Code;
^.h /^6i^w^^
Sampt.e.J Analysis,
.2 ^, ^ S'-T-fM^1 •i ,
i •i ,i 'i 't ,
1 ii (i ,( ,
/
LYTICAL SERVICE(ING LIST
Ship To: EyvJiftoOSlJt &IMHB\ . l L l f c l ^ALt.l-ATM& 6.0.
5t-. l-OLu-i> ,1<\&.l/•3,1^1
Attn:Fa.T-\- rt-fst^iAt-^
Ie DexriptionMatrix, Concentrationrtu>l /-^/i^L^k/Y-i
i
, ,
> ,• • woa.-<~-i
i / ^-^r^ "i- ^ i.
CA .—a^h
^
es For Lat
Date Sany ' yReceiveOb-^
Sample CReceip
Of
^dumber^0 ^-
a USE Only
nples Rec'd:f-^——
d By:/ - 9 - t y
^>nditionontat Labk
/
For Lab Use Only
White - SMO Copy, Yellow - Region Copy, Pink - Lab Copy for return to SMO, Gold - Lab Copy
UA ENVIRONMENTAL PROTECTION AGENCYCLP Sample Management OfficeP.O. Box 818 - Alexandria, Virginia 22313Phone: 703/557-2l|90 - FTS/557-2490
flKLX, __Atf Number^07-
SPECIAL ANALYTICAL SERVICEPACKING LIST
Sampling Office:T^l\^
Sampling Contact:3»>M-<- S^\M\^^-
(name)'
[^\U^<0.-^(.C>|•'• • (phone)
SampleNudbcrs
Sampling Date(s):5/3"-^>MDate Shipped:.^//HSit&Name/Code:
v^cVAEbW
Sampi.e.. Analysis,
Ship To:EAi»/ie.ciCMt'4E ^•"rtriEee1
laitl V-Ac-fc^"^ ®d•3+.l-o^&,^o.y^(
Attn;gai4 fta^S.o^
Ie DescriptionMatrix, Concentration
For Lab Use Only
Date Samples Rec'd:i-t-sV
Received By:,^/^-
Sample Condition onReceipt at Lab
i.2.3.t.5.6.7.8.9.
10.1 1 .12.13.14.
15.16.17.
18.19.20.
IYFC>OC,4.t5r^&&64il<.T^C.-O1^DFdiX^^Fr^^QFc>b&490n V f t n o ^ l lrip&oo4i3.nF 600 4/3DF^O^'rF,.llh\^npooo-^ai
/
-
Sl-\^&-V&^
1 1
1 ,
1 '
"
I '( 1
1 1
To at ' tsl
^fY\4A
i
•—)——
—]———
11
1 "
^v-^—a—"—'-
. Crr.
< .
\'
i
,
fT"-y uJc.^^li •K.is/ S/'li^C
For Lab Use Only
White - SMO Copy, Yellow - Region Copy, Pink - Lab Copy (or return to SMO, Gold - Lab Copy
€..»..<ONI«ici<iALrouiEC11.Office of Enforcemer
l-fl
CHAIN OF CUSTODY RECORD
REuluiJ6pint Internalioflal BIdg , 1201 .Elm St.
Dallas, Temi 75270PRO.) NO PROJECT NAME
SAMPLERS IS.,nk^J^^!S.^ -^..^C.^^9»1°"-*,$. l^^"-' -^ /—— ^ » **-
STATION LOCATION
Date/Time Received by: (Signature)RellnQuiitiad by: iS'frniuf*!
CONTAINEH
__,.g^^£.' ^^B aF.JA .'aS^ ;y^n>tfyJi_^r. i—f i if 6 r~———————,——aA ^5»s /'o. se'^d • M-> •Agl^.i.^ll/ddg^.f.,^'^' •7g^y.ffxu/<rv- Tfticirflrfl.»F.AiL*/»'. ''p -y^^^f /»/^.^iy-5%«. »p- -^F**^ •^A^f^t</'-/fc-fTi^vjt^iAv^^-_A»>^ voc^^f4*^^^k^^f.^n!FiWi s .d*.'y^Vc^£^^ t»» i tJ>^< •»<-•-
y-y^^
_y.
y^
' ^^^^ ••<:^.t/St^/g-y *'< • ••^ —
Received by: ls<yMiwel
F tloTrJt ?fP^^
^L - oV3g?
^X,v
Relinquished by: {Signature!elinquished by: {Signature! swt Date /Time Received by: {Swuturvl
•^^- ^/fy //•/^~Relinquished by: {S'ynaiufef Date Time Received by; fS'ynfti^
Received tor Labora ory by:ISiynmnf
Doinbunon. OfifnBl Arcomp«niei Shipmani. Copy 10 Cuordinalur I ield Fill
0 0