r'j celsis analytical services - nrc

18
r'j Celsis Analytical Services September 28. 2011 US Nuclear Regulatory Commission Materials Licensing Branch Region ill 2443 W8.lTenville Rd. Suite 210 Lisle, IL 60532 To Whom It May Concern: We have contracted R. M. Wester & Associates, Inc .• located in st. Peters, Mjssouri, to assist us with termination of our USNRC Materials License. The Celsis laboratory has only used very small quantities ofHydtogen-3. for research purposes, and that which was used is accountable in our waste inventory logs. Please find the enclosed closeout survey in support of our license termination for your review. If you have any questions or comments, please contact either myself, or R. M. Wester & Associates, Inc., as appropriate. Thank you for your assistance in this matter. Sincerely. David Knysak Radiation Safety Officer Celsislt.bomtory GroIJp ()200 S, lifldhergh Blvd, SI L(,ui •. M<') ('3123 USA T +1 314 ASl 6176 F ,1 :H4 4117 8991 AnQlyl:t,.,JI rut."'!'}1:"\'" tiH11 1\)I} 11 Jt)lpflf'l "'VIW:':!' tUvy h.-: fls.C'!'d willtu by fJ"r',;finjl and !'II: ;. '':;''It :)1.' \1\;"(1 j., (,!I"IY '01 HI or wi,h'-'I}' writlt}rI p.:rIHis;.ion j",1-lol 'nil pt( !,I'I:II)"l ..... ':"vrt!ptlIlW" W'NW '.Il,ltl'

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Page 1: r'j Celsis Analytical Services - NRC

rj Celsis Analytical Services

September 28 2011

US Nuclear Regulatory Commission Materials Licensing Branch Region ill 2443 W8lTenville Rd Suite 210 Lisle IL 60532

To Whom It May Concern

We have contracted R M Wester amp Associates Inc bull located in st Peters Mjssouri to assist us with termination ofour USNRC Materials License The Celsis laboratory has only used very small quantities ofHydtogen-3 for research purposes and that which was used is accountable in our waste inventory logs

Please find the enclosed closeout survey in support of our license termination for your review If you have any questions or comments please contact either myself or R M Wester amp Associates Inc as appropriate Thank you for your assistance in this matter

Sincerely

~rr~ice

David Knysak Radiation Safety Officer

Celsisltbomtory GroIJp ()200 S lifldhergh Blvd SI L(ui bull Mlt) (3123 USA T +1 314 ASl 6176 F 1 H4 4117 8991

(tlli~ AnQlyltJI $Ijt~ rut1 tiH11 1)I I~ 11 (lmiddotiF~jdQtillJl Jt)lpflfl VIW tUvy h- flsCd willtu n)Jnit~d by fJrfinjl and 11~tthh (Hili(l~~ II It ~IJ )1 1(1 j (IIY 01 HI or (rlVcrt~HlII wih-I writltrI prIHision

j1-lol nil ~1~h1 liHI~IIHlr pt( IIII)l vrtptlIlW WNW I~~I~ Illtl

R M WESTER amp ASSOCIATES INC 215INOACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628 - FAX 928-9857

Radiation Survey Report

Celsis Analytical Services St Louis Missouri

Closeout Survey in Support of USNRC License Termination

Performed By

R M Wester amp Associates Inc Health Physicists Kenneth Bachmann Kenneth Barnes

Survey Dates September 22 23 28 2011

SPECIALIZING IN YOUR RAf)IA TION SAFETY NpoundpoundDS N

poundd WdleS0 110e Be das LSB6Be69pound9 ON 3NOHd ouI salEiooSSIj 8 -lalsaM W~ W~I

Celsis Closeout Survey Page 2 of16 Performed by R M Wester amp Associates Inc September 28 2011

1 Overview

Celsis Analytical Services Laboratory located in St Louis Missouri was approved for millishyCurie quantities ofHydrogen-3 and Carbon-14 however only Hydrogen-3 was used within the laboratory The radioactive material was used for skin absorption studies Currently all materials received are located in waste drums wi1hln the Building C SkinBiology Laboratory and contain liquid scintillation vials and associated dry waltrte

Areas where radioactive materials were received stored and used at the Celsis Analytical Services Laboratory wtrre surveyed for removable radioactive surface contamination The survey consisted ofa total of193 grid sections ofbuildingsurfaces and removable equipment items with one removable contamination sample in each grid section A sampling of horizonIa surfaces within the Building C Skin Biology LabOlatory were also surveyed for any remaining fixed radioactive presence Mr Brian A Dell Associate Director of Biological Sciences and Mr David Knysak Radiation Safety Officer (RSO) were the on-site point ofcontacts during the survey The size and geometry ofthe surface grid sections was approximately 1 meter square Please see Enclosure 1 for applicable grid diagrams

The areas surveyed were Building C Skin Biology Laboratory Building A Cytotoxicity Lab Building A Receiving Area Included in the survey were all accessible wall surfaces up to 2 meters in height floor surfaces exterior and interior offixed equipment items such as lab benches fixtures sinks and drains exterior and interior where appropriate ofremovable equipment items such as portable tables lab refrigerators drums and miscellaneous lab supply items Please see Enclosure 1 for a graphical representation of the rooms

2 Fixed Contamination Radiation Survey

A Berthold) Model LB 6255 Tritium Probe (SIN - 623 calibrated on 92811raquo was used to survey surfaces for any evidence of fixed contamination The above probe was paired with a Ludlum Measurements Inc Model 2350 (SIN ~79049) The survey was conducted within one centimeter of the surface Ambient background for the tritium detector was 160 CPM 25 CPM Ambient background was sampled in grid section AI just outside the Building C Skin Laboratory Please see Enclosure 2 forfixed contamination radiation survey data Conc1 usion of the fixed contamination radiation survey showed no net detectable readings ofsignitlcancc above the ambient background rate for the survey instrument used TIle fixed contamination radiation survey was performed on September 28 2011

3 Removable Contamination Survey

The grid surfaces were wiped within each onemiddotsquare-meter grid dcsignated In some cases a smaller grid size was used where applicable The approximate areaofeach wipe coverage was 100 cm2 within each grid section See Enclosure 3 for removable contamination survey data The removable contamination survey was performed on September 22 and September 232011

SPECIALIZING IN YOl)R RADIATION SAFETY NEEOSmiddot

Celsis Closeout Survey Page 3 of16 Performed by R M Wester amp Associates Inc SSember 28 2011

4 Removable Contamination Analysis

The wipes were analyzed using a Packard Instrument Company Tri-Cub 2100TR Liquid Scintillation Analyzer (SIN 416174) sensitive to beta and alpha radiation Conclusion oftbe contamination survey showed no net detectable readings of significance above the control background for the liquid scintillation testing Activities ofall wipes samples were measured below the applicable Minimal Detectable Activity (MDA) See enclosure 3 for details regarding the removable contamination survey results

Surveyor ~PhysiCist Date September 22 23 28 2011

Surveyor J~~

K~eth Bachmann Health Physicist Date September 22 2011

Reviewer ~~P~Ci~ Date September 28 2011

ffSPECIALIZING IN YOUR RAOIA nON SAFETY NEEDS

Sd WdeeS0 tT0e Be das

Celsis Closeout Survey Page 4 of 16 Perfonned by R M Wester amp Associates Inc September 28 2011

Enclosure 1 Facility Layout and Grid Locations

Figure 1 Building C Skin Biology Laboratory Layout

Figure 2 Building A Storage Room Grid

Cooler Back Interior A9 Right Side Interior AlO Interior Shelves All Bottom Interior Al2

Drawings nor to scale Dimensions are approximate Shadedareas indicate surveyed regions Grid locations are given in bold

Enclosure 1

SPECIALIZING IN YOUR flADIA (fON SAfETY NEEDS

9d Wd[eS0 110e Be das LSB6Be69[9

Celsis Closeout Survey Page 5 of16 Perfoxmed by R M Wester amp Associates Inc September 28 2011

Figure 3 Building A Receiving Area Grid

Lab Bench

Figure 4 Skin Biology Lab Floor 1 Grid

Enclosure 1

middotmiddotSPECIALIZING IN YOUR RAOtA TtON SAFETY NEEDSmiddot

Ld WdveS0 TT0e 8e ddS LS868e69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 5 Skin Biology Lab Wall 1 Grid

Page 6 of 16

Figure 6 Skin Biology Lab Wall 2 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON $AHTY NEEDS

8d WdSeS0 110e 8e odas LS868e69pound9

J ~ ~ bull G- shy L

Celsis Closeout Survey Page 7 of 16 Performed by R M Wester amp Associates Inc S~tember 28 2011

Figure 6 Skin Biology Lab Wall 3 Grid

Adjoining wall

behind this wall was

included in survey grids

Figure 7 Skin Biology Lab Wa1l4 Grid

Enclosure 1

SPECIAUZING IN YOUR RADIA TlON SAFETY NEIOS middotmiddot

6d WdLeS0 110e Be middotdas LSB6Be69pound9

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 2: r'j Celsis Analytical Services - NRC

R M WESTER amp ASSOCIATES INC 215INOACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628 - FAX 928-9857

Radiation Survey Report

Celsis Analytical Services St Louis Missouri

Closeout Survey in Support of USNRC License Termination

Performed By

R M Wester amp Associates Inc Health Physicists Kenneth Bachmann Kenneth Barnes

Survey Dates September 22 23 28 2011

SPECIALIZING IN YOUR RAf)IA TION SAFETY NpoundpoundDS N

poundd WdleS0 110e Be das LSB6Be69pound9 ON 3NOHd ouI salEiooSSIj 8 -lalsaM W~ W~I

Celsis Closeout Survey Page 2 of16 Performed by R M Wester amp Associates Inc September 28 2011

1 Overview

Celsis Analytical Services Laboratory located in St Louis Missouri was approved for millishyCurie quantities ofHydrogen-3 and Carbon-14 however only Hydrogen-3 was used within the laboratory The radioactive material was used for skin absorption studies Currently all materials received are located in waste drums wi1hln the Building C SkinBiology Laboratory and contain liquid scintillation vials and associated dry waltrte

Areas where radioactive materials were received stored and used at the Celsis Analytical Services Laboratory wtrre surveyed for removable radioactive surface contamination The survey consisted ofa total of193 grid sections ofbuildingsurfaces and removable equipment items with one removable contamination sample in each grid section A sampling of horizonIa surfaces within the Building C Skin Biology LabOlatory were also surveyed for any remaining fixed radioactive presence Mr Brian A Dell Associate Director of Biological Sciences and Mr David Knysak Radiation Safety Officer (RSO) were the on-site point ofcontacts during the survey The size and geometry ofthe surface grid sections was approximately 1 meter square Please see Enclosure 1 for applicable grid diagrams

The areas surveyed were Building C Skin Biology Laboratory Building A Cytotoxicity Lab Building A Receiving Area Included in the survey were all accessible wall surfaces up to 2 meters in height floor surfaces exterior and interior offixed equipment items such as lab benches fixtures sinks and drains exterior and interior where appropriate ofremovable equipment items such as portable tables lab refrigerators drums and miscellaneous lab supply items Please see Enclosure 1 for a graphical representation of the rooms

2 Fixed Contamination Radiation Survey

A Berthold) Model LB 6255 Tritium Probe (SIN - 623 calibrated on 92811raquo was used to survey surfaces for any evidence of fixed contamination The above probe was paired with a Ludlum Measurements Inc Model 2350 (SIN ~79049) The survey was conducted within one centimeter of the surface Ambient background for the tritium detector was 160 CPM 25 CPM Ambient background was sampled in grid section AI just outside the Building C Skin Laboratory Please see Enclosure 2 forfixed contamination radiation survey data Conc1 usion of the fixed contamination radiation survey showed no net detectable readings ofsignitlcancc above the ambient background rate for the survey instrument used TIle fixed contamination radiation survey was performed on September 28 2011

3 Removable Contamination Survey

The grid surfaces were wiped within each onemiddotsquare-meter grid dcsignated In some cases a smaller grid size was used where applicable The approximate areaofeach wipe coverage was 100 cm2 within each grid section See Enclosure 3 for removable contamination survey data The removable contamination survey was performed on September 22 and September 232011

SPECIALIZING IN YOl)R RADIATION SAFETY NEEOSmiddot

Celsis Closeout Survey Page 3 of16 Performed by R M Wester amp Associates Inc SSember 28 2011

4 Removable Contamination Analysis

The wipes were analyzed using a Packard Instrument Company Tri-Cub 2100TR Liquid Scintillation Analyzer (SIN 416174) sensitive to beta and alpha radiation Conclusion oftbe contamination survey showed no net detectable readings of significance above the control background for the liquid scintillation testing Activities ofall wipes samples were measured below the applicable Minimal Detectable Activity (MDA) See enclosure 3 for details regarding the removable contamination survey results

Surveyor ~PhysiCist Date September 22 23 28 2011

Surveyor J~~

K~eth Bachmann Health Physicist Date September 22 2011

Reviewer ~~P~Ci~ Date September 28 2011

ffSPECIALIZING IN YOUR RAOIA nON SAFETY NEEDS

Sd WdeeS0 tT0e Be das

Celsis Closeout Survey Page 4 of 16 Perfonned by R M Wester amp Associates Inc September 28 2011

Enclosure 1 Facility Layout and Grid Locations

Figure 1 Building C Skin Biology Laboratory Layout

Figure 2 Building A Storage Room Grid

Cooler Back Interior A9 Right Side Interior AlO Interior Shelves All Bottom Interior Al2

Drawings nor to scale Dimensions are approximate Shadedareas indicate surveyed regions Grid locations are given in bold

Enclosure 1

SPECIALIZING IN YOUR flADIA (fON SAfETY NEEDS

9d Wd[eS0 110e Be das LSB6Be69[9

Celsis Closeout Survey Page 5 of16 Perfoxmed by R M Wester amp Associates Inc September 28 2011

Figure 3 Building A Receiving Area Grid

Lab Bench

Figure 4 Skin Biology Lab Floor 1 Grid

Enclosure 1

middotmiddotSPECIALIZING IN YOUR RAOtA TtON SAFETY NEEDSmiddot

Ld WdveS0 TT0e 8e ddS LS868e69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 5 Skin Biology Lab Wall 1 Grid

Page 6 of 16

Figure 6 Skin Biology Lab Wall 2 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON $AHTY NEEDS

8d WdSeS0 110e 8e odas LS868e69pound9

J ~ ~ bull G- shy L

Celsis Closeout Survey Page 7 of 16 Performed by R M Wester amp Associates Inc S~tember 28 2011

Figure 6 Skin Biology Lab Wall 3 Grid

Adjoining wall

behind this wall was

included in survey grids

Figure 7 Skin Biology Lab Wa1l4 Grid

Enclosure 1

SPECIAUZING IN YOUR RADIA TlON SAFETY NEIOS middotmiddot

6d WdLeS0 110e Be middotdas LSB6Be69pound9

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 3: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Page 2 of16 Performed by R M Wester amp Associates Inc September 28 2011

1 Overview

Celsis Analytical Services Laboratory located in St Louis Missouri was approved for millishyCurie quantities ofHydrogen-3 and Carbon-14 however only Hydrogen-3 was used within the laboratory The radioactive material was used for skin absorption studies Currently all materials received are located in waste drums wi1hln the Building C SkinBiology Laboratory and contain liquid scintillation vials and associated dry waltrte

Areas where radioactive materials were received stored and used at the Celsis Analytical Services Laboratory wtrre surveyed for removable radioactive surface contamination The survey consisted ofa total of193 grid sections ofbuildingsurfaces and removable equipment items with one removable contamination sample in each grid section A sampling of horizonIa surfaces within the Building C Skin Biology LabOlatory were also surveyed for any remaining fixed radioactive presence Mr Brian A Dell Associate Director of Biological Sciences and Mr David Knysak Radiation Safety Officer (RSO) were the on-site point ofcontacts during the survey The size and geometry ofthe surface grid sections was approximately 1 meter square Please see Enclosure 1 for applicable grid diagrams

The areas surveyed were Building C Skin Biology Laboratory Building A Cytotoxicity Lab Building A Receiving Area Included in the survey were all accessible wall surfaces up to 2 meters in height floor surfaces exterior and interior offixed equipment items such as lab benches fixtures sinks and drains exterior and interior where appropriate ofremovable equipment items such as portable tables lab refrigerators drums and miscellaneous lab supply items Please see Enclosure 1 for a graphical representation of the rooms

2 Fixed Contamination Radiation Survey

A Berthold) Model LB 6255 Tritium Probe (SIN - 623 calibrated on 92811raquo was used to survey surfaces for any evidence of fixed contamination The above probe was paired with a Ludlum Measurements Inc Model 2350 (SIN ~79049) The survey was conducted within one centimeter of the surface Ambient background for the tritium detector was 160 CPM 25 CPM Ambient background was sampled in grid section AI just outside the Building C Skin Laboratory Please see Enclosure 2 forfixed contamination radiation survey data Conc1 usion of the fixed contamination radiation survey showed no net detectable readings ofsignitlcancc above the ambient background rate for the survey instrument used TIle fixed contamination radiation survey was performed on September 28 2011

3 Removable Contamination Survey

The grid surfaces were wiped within each onemiddotsquare-meter grid dcsignated In some cases a smaller grid size was used where applicable The approximate areaofeach wipe coverage was 100 cm2 within each grid section See Enclosure 3 for removable contamination survey data The removable contamination survey was performed on September 22 and September 232011

SPECIALIZING IN YOl)R RADIATION SAFETY NEEOSmiddot

Celsis Closeout Survey Page 3 of16 Performed by R M Wester amp Associates Inc SSember 28 2011

4 Removable Contamination Analysis

The wipes were analyzed using a Packard Instrument Company Tri-Cub 2100TR Liquid Scintillation Analyzer (SIN 416174) sensitive to beta and alpha radiation Conclusion oftbe contamination survey showed no net detectable readings of significance above the control background for the liquid scintillation testing Activities ofall wipes samples were measured below the applicable Minimal Detectable Activity (MDA) See enclosure 3 for details regarding the removable contamination survey results

Surveyor ~PhysiCist Date September 22 23 28 2011

Surveyor J~~

K~eth Bachmann Health Physicist Date September 22 2011

Reviewer ~~P~Ci~ Date September 28 2011

ffSPECIALIZING IN YOUR RAOIA nON SAFETY NEEDS

Sd WdeeS0 tT0e Be das

Celsis Closeout Survey Page 4 of 16 Perfonned by R M Wester amp Associates Inc September 28 2011

Enclosure 1 Facility Layout and Grid Locations

Figure 1 Building C Skin Biology Laboratory Layout

Figure 2 Building A Storage Room Grid

Cooler Back Interior A9 Right Side Interior AlO Interior Shelves All Bottom Interior Al2

Drawings nor to scale Dimensions are approximate Shadedareas indicate surveyed regions Grid locations are given in bold

Enclosure 1

SPECIALIZING IN YOUR flADIA (fON SAfETY NEEDS

9d Wd[eS0 110e Be das LSB6Be69[9

Celsis Closeout Survey Page 5 of16 Perfoxmed by R M Wester amp Associates Inc September 28 2011

Figure 3 Building A Receiving Area Grid

Lab Bench

Figure 4 Skin Biology Lab Floor 1 Grid

Enclosure 1

middotmiddotSPECIALIZING IN YOUR RAOtA TtON SAFETY NEEDSmiddot

Ld WdveS0 TT0e 8e ddS LS868e69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 5 Skin Biology Lab Wall 1 Grid

Page 6 of 16

Figure 6 Skin Biology Lab Wall 2 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON $AHTY NEEDS

8d WdSeS0 110e 8e odas LS868e69pound9

J ~ ~ bull G- shy L

Celsis Closeout Survey Page 7 of 16 Performed by R M Wester amp Associates Inc S~tember 28 2011

Figure 6 Skin Biology Lab Wall 3 Grid

Adjoining wall

behind this wall was

included in survey grids

Figure 7 Skin Biology Lab Wa1l4 Grid

Enclosure 1

SPECIAUZING IN YOUR RADIA TlON SAFETY NEIOS middotmiddot

6d WdLeS0 110e Be middotdas LSB6Be69pound9

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 4: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Page 3 of16 Performed by R M Wester amp Associates Inc SSember 28 2011

4 Removable Contamination Analysis

The wipes were analyzed using a Packard Instrument Company Tri-Cub 2100TR Liquid Scintillation Analyzer (SIN 416174) sensitive to beta and alpha radiation Conclusion oftbe contamination survey showed no net detectable readings of significance above the control background for the liquid scintillation testing Activities ofall wipes samples were measured below the applicable Minimal Detectable Activity (MDA) See enclosure 3 for details regarding the removable contamination survey results

Surveyor ~PhysiCist Date September 22 23 28 2011

Surveyor J~~

K~eth Bachmann Health Physicist Date September 22 2011

Reviewer ~~P~Ci~ Date September 28 2011

ffSPECIALIZING IN YOUR RAOIA nON SAFETY NEEDS

Sd WdeeS0 tT0e Be das

Celsis Closeout Survey Page 4 of 16 Perfonned by R M Wester amp Associates Inc September 28 2011

Enclosure 1 Facility Layout and Grid Locations

Figure 1 Building C Skin Biology Laboratory Layout

Figure 2 Building A Storage Room Grid

Cooler Back Interior A9 Right Side Interior AlO Interior Shelves All Bottom Interior Al2

Drawings nor to scale Dimensions are approximate Shadedareas indicate surveyed regions Grid locations are given in bold

Enclosure 1

SPECIALIZING IN YOUR flADIA (fON SAfETY NEEDS

9d Wd[eS0 110e Be das LSB6Be69[9

Celsis Closeout Survey Page 5 of16 Perfoxmed by R M Wester amp Associates Inc September 28 2011

Figure 3 Building A Receiving Area Grid

Lab Bench

Figure 4 Skin Biology Lab Floor 1 Grid

Enclosure 1

middotmiddotSPECIALIZING IN YOUR RAOtA TtON SAFETY NEEDSmiddot

Ld WdveS0 TT0e 8e ddS LS868e69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 5 Skin Biology Lab Wall 1 Grid

Page 6 of 16

Figure 6 Skin Biology Lab Wall 2 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON $AHTY NEEDS

8d WdSeS0 110e 8e odas LS868e69pound9

J ~ ~ bull G- shy L

Celsis Closeout Survey Page 7 of 16 Performed by R M Wester amp Associates Inc S~tember 28 2011

Figure 6 Skin Biology Lab Wall 3 Grid

Adjoining wall

behind this wall was

included in survey grids

Figure 7 Skin Biology Lab Wa1l4 Grid

Enclosure 1

SPECIAUZING IN YOUR RADIA TlON SAFETY NEIOS middotmiddot

6d WdLeS0 110e Be middotdas LSB6Be69pound9

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 5: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Page 4 of 16 Perfonned by R M Wester amp Associates Inc September 28 2011

Enclosure 1 Facility Layout and Grid Locations

Figure 1 Building C Skin Biology Laboratory Layout

Figure 2 Building A Storage Room Grid

Cooler Back Interior A9 Right Side Interior AlO Interior Shelves All Bottom Interior Al2

Drawings nor to scale Dimensions are approximate Shadedareas indicate surveyed regions Grid locations are given in bold

Enclosure 1

SPECIALIZING IN YOUR flADIA (fON SAfETY NEEDS

9d Wd[eS0 110e Be das LSB6Be69[9

Celsis Closeout Survey Page 5 of16 Perfoxmed by R M Wester amp Associates Inc September 28 2011

Figure 3 Building A Receiving Area Grid

Lab Bench

Figure 4 Skin Biology Lab Floor 1 Grid

Enclosure 1

middotmiddotSPECIALIZING IN YOUR RAOtA TtON SAFETY NEEDSmiddot

Ld WdveS0 TT0e 8e ddS LS868e69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 5 Skin Biology Lab Wall 1 Grid

Page 6 of 16

Figure 6 Skin Biology Lab Wall 2 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON $AHTY NEEDS

8d WdSeS0 110e 8e odas LS868e69pound9

J ~ ~ bull G- shy L

Celsis Closeout Survey Page 7 of 16 Performed by R M Wester amp Associates Inc S~tember 28 2011

Figure 6 Skin Biology Lab Wall 3 Grid

Adjoining wall

behind this wall was

included in survey grids

Figure 7 Skin Biology Lab Wa1l4 Grid

Enclosure 1

SPECIAUZING IN YOUR RADIA TlON SAFETY NEIOS middotmiddot

6d WdLeS0 110e Be middotdas LSB6Be69pound9

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 6: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Page 5 of16 Perfoxmed by R M Wester amp Associates Inc September 28 2011

Figure 3 Building A Receiving Area Grid

Lab Bench

Figure 4 Skin Biology Lab Floor 1 Grid

Enclosure 1

middotmiddotSPECIALIZING IN YOUR RAOtA TtON SAFETY NEEDSmiddot

Ld WdveS0 TT0e 8e ddS LS868e69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 5 Skin Biology Lab Wall 1 Grid

Page 6 of 16

Figure 6 Skin Biology Lab Wall 2 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON $AHTY NEEDS

8d WdSeS0 110e 8e odas LS868e69pound9

J ~ ~ bull G- shy L

Celsis Closeout Survey Page 7 of 16 Performed by R M Wester amp Associates Inc S~tember 28 2011

Figure 6 Skin Biology Lab Wall 3 Grid

Adjoining wall

behind this wall was

included in survey grids

Figure 7 Skin Biology Lab Wa1l4 Grid

Enclosure 1

SPECIAUZING IN YOUR RADIA TlON SAFETY NEIOS middotmiddot

6d WdLeS0 110e Be middotdas LSB6Be69pound9

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 7: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 5 Skin Biology Lab Wall 1 Grid

Page 6 of 16

Figure 6 Skin Biology Lab Wall 2 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON $AHTY NEEDS

8d WdSeS0 110e 8e odas LS868e69pound9

J ~ ~ bull G- shy L

Celsis Closeout Survey Page 7 of 16 Performed by R M Wester amp Associates Inc S~tember 28 2011

Figure 6 Skin Biology Lab Wall 3 Grid

Adjoining wall

behind this wall was

included in survey grids

Figure 7 Skin Biology Lab Wa1l4 Grid

Enclosure 1

SPECIAUZING IN YOUR RADIA TlON SAFETY NEIOS middotmiddot

6d WdLeS0 110e Be middotdas LSB6Be69pound9

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 8: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Page 7 of 16 Performed by R M Wester amp Associates Inc S~tember 28 2011

Figure 6 Skin Biology Lab Wall 3 Grid

Adjoining wall

behind this wall was

included in survey grids

Figure 7 Skin Biology Lab Wa1l4 Grid

Enclosure 1

SPECIAUZING IN YOUR RADIA TlON SAFETY NEIOS middotmiddot

6d WdLeS0 110e Be middotdas LSB6Be69pound9

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 9: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Page 8 of16 Perfonned by R M Wester amp Associates Inc September 28 2011

Figure 8 Skin Biology Lab Floor 2 Grid

Figure 9 Skin Biology Lab Wall 5 Grid

Enclosure 1

SPECIALIZING IN YOUR RADIA TlON SAFETY NEEDS

LS868c69[9

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 10: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Performed by R M Wester amp Associates Inc September 28 2011

Figure 10 Skin Biology Lab Wall 6 Grid

Page 9 of 16

Figure 11 Skin Biology Lab Wall 7 Grid

Shelf A 79 A80 A81 Rad Fridge Exterior A89 A90 A91 Sink Exterior A82A83 Rad Fridge Interior A 92 A 93 A94

Sink Drain A84A85 Storage Container A 95 A96 Misc Items on Shelf A86 Misc Items on Sink A87 Misc Items on Floor A88

Enclosure 1

SPpoundCIAVZING IN YOUR RADIATION SAFETY NEEDS

LS868c69pound9

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 11: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Performed by R- M Wester amp Associates Inc September 28 2011

Figure 12 Skin Biology Lab Floor 3 Grid

Page 10 ofl6

Figure 13 Skin Biology Lab Wall 8 Grid

Enclosure 1

SPECIALIZING IN YOUR RAOIA TfON SAFETY NEEDSmiddot

eTd Wdpoundpoundpound0 TT0e Be das LpoundB6Be69pound9

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 12: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Perfonned by R M Wester amp Associates Inc September 28~ 2011

Figure 14 Skin Biology Lab Wall 9 Grid

Page 11 of16

Figure 15 Skin Biology Lab WalllO Grid

Enclosure 1

middotSPpoundCIALfZfNG fN YOUR RADfA TfON SAFETY NEEDS

LS868G69~9

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 13: r'j Celsis Analytical Services - NRC

Celsis Closeout Survey Page l2of16 Performed by R M Wester amp Associates Inc September 28 2011

Figure 16 Skin Biology Lab Wall 11 Grid

Removable Equipment in Lab

Table Items on Table Titration Table Items on Titration Table LSA Table LSA Exterior LSA Interior LSA Monitor LSA Printer Supplies on LSA Table Dry ltid Waste Drum Exterior Scintillation Vial Drum Exterior Liquid Rad Waste Drum Exterior Misc Bucket (Ext Int) Lab Coats Small Table Towel Rack

A 153 A154 A155 A156 A157A158 A159 A160 A161 A162 A163A164 A165A166A167 A168A169A170 A171A172 A173 A174 A175A176 A177A178 A179 Al80 A181A182 A183A184 A185A186 A187A188 A189A190 AJ91 A192 A193

Enclosure 1

SPECfALlZING IN YOUR RADfA TION SAFETY NEEDS

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 14: r'j Celsis Analytical Services - NRC

Celsis Analytical Services License Closeout Survey September 28 2011

Enclosure 2 Fixed Contamination Radiation Survey Data Page 13 of 16

Berthold Model LB 6255 Grid Raw AvgBkg Net Net No CPM CPM CPM eff DPM A97 15800 16000 000 0056 000 A98 J6300 16000 300 0056 5357 A99 J6700 16000 700 0056 12500 AlOO 15S00 16000 000 0056 000 AIOI 15500 16000 000 0056 000 At02 15500 16000 000 0056 000 AI03 16800 16000 800 0056 14286 AI04 16000 16000 000 0056 000 AIOS 15600 16000 000 0056 000 A 106 16400 16000 400 0056 7143 AI07 15600 16000 000 0056 000 AIOS 15500 16000 000 0056 000 A109 18200 16000 2200 0056 39286 AlIO 18400 16000 2400 0056 42857 Al11 14100 16000 000 0056 000 All2 15200 16000 000 0056 000 All3 17600 16000 1600 0056 28571 All 11800 16000 000 0056 000 AilS 14600 16000 000 0056 000 AU6 14800 16000 000 0056 000 AI53 1S100 16000 000 0056 000 A1S4 13500 16000 000 0056 000 A160 14400 16000 000 0036 000 A161 13400 16000 000 0056 000 A161 16600 16000 600 0056 10714 A168 11800 16000 000 0056 000 A169 13100 16000 000 0056 000 A170 14600 16000 000 0056 000 A17S 19900 16000 3900 0056 69643 A176 19200 16000 3200 0056 57143

160 CPM +1- ZS CPM Boekground 56 C-14 eff (2 Pi) 11 em) Window Area

Enclosure 2

Std WdBpoundS0 tt0e Be das

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 15: r'j Celsis Analytical Services - NRC

Celsis Analytical Services License Closeout Survey Seprernber282011

Enclosure 3 Removable Contamination Survey nata Page 14 of 16

LiquidSdntillatlon AnaIY$is Packard Tri-Carb 2l00TR Liquid Scintillation Analysis Packald Tri-Carb 2tOOTR Grid Net lNet Grid Net Net No CPM bull DPM No CPM DPM Al 000 s 214 A48 069 s 214 Ai 153 s 214 A49 000 s 214 A3 064 ~ 214 ASO 124 s 214 A4 000 t 214 AS) 1209 t 214 AS 000 s2L4 A52 000 214 A6 004 s 214 AS3 000 s214 A7 329 s 214 A54 024 s 214 A8 144 s 214 ASS 2929 s 214 A9 009 s 214 A56 064 s 214 AIO 044 s 214 AS7 024 ~ 214 AU 249 214 AS8 000 So 214 All 064 So 214 AS9 000 s 214 A13 024 s 214 A60 000 s 214 At4 000 s2L4 A61 004 s 214 A15 233 s 214 A62 129 s 214 A16 004 s 214 A63 000 s 214 A17 064 s 214 A64 000 214 Al8 1113 214 A65 024 s 214 A 19 000 s 214 A66 000 214 AlO 000 s 214 A67 044 s 214 All 064 s 214 A68 000 ~ 214 All 000 Ii 214 A69 000 s 214 All 2S3 s 214 A70 089 214 A14 084 ~ 214 A71 000 214 AlS 000 s 214 A72 004 5 214 Al6 000 s 214 A73 000 s 214 A27 084 5214 A74 024 s 214 Al8 024 pound 214 A7S 000 214 A29 049 5214 A76 044 pound 214 A30 004 ~ 214 A77 000 5214 All 069 s 214 A78 044 s 214 A32 000 s 214 A79 004 214 A33 318 1 214 ASO 004 ~ 214 A34 089 s 214 AS1 044 s 214 A35 000 214 A82 000 1 214 A36 204 s 214 AS3 311 s 214 A37 104 s 214 A84 000 s 214 A38 000 s 214 A8S 024 s 214 A39 044 5214 A86 000 ~ 214

A40 149 s 214 AS7 089 oS 214 A41 000 s 214 ASS 004 s 214 A42 000 214 AS9 164 s 214 A43 000 s 214 A90 004 S214 A44 000 214 A9l 229 pound214 A45 000 gt 214 A92 242 oS 214 A46 000 214 A93 000 214 A47 000 s 214 A94 069 5214 LSA 0925 eJJC-14 0574 effH-3 3078 BackgrQund CPM 2]4 DPM MDA WmdoHI O 2(JOO keV

Enclosure 3

LS868C69pound9 ON 3NOHd lUI salEPoSSlI 8 alSCif WtI I-lOtl

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 16: r'j Celsis Analytical Services - NRC

Celsis Analytical Services License Closeout Survey September 28 2011

Page 15 of16

Liquid ScintillatioD Analysis Packard Tri-Carb llOOTR Liquld Scintillation Analysis Packard 1imiddotCar-b 2100TR Grid Raw lNet Grid Raw Net No~ CPM middotDPM No CPM middotDPM MS 004 s 214 A142 000 ~ 214 A96 024 s 2lA AI43 000 s 214 A97 229 214 Al44 044 s 214 A98 084 ~ 214 Al45 000 s 214 A99 000 214 AI46 229 214 AlOO 693 s 214 A147 104 oS 214 A10 000 s 214 A148 000 so 214 AIOZ 000 ~ 214 A149 004 214 AI03 000 s 214 AlSO 004 s 214 AI04 164 -s 214 At1 000 It 214 AIOS 004 s 214 Al2 004 214 AI06 000 t 214 A153 000 214 AI07 144 s 214 Al54 000 s 214 AIOS 124 ~ 214 AISS 000 s 214 Al09 089 s 214 A156 004 s 214 AUO 000 s 214 AI57 000 s 214 AUt 024 ~ 214 A158 169 ~ 214 AllZ 000 214 A1S9 084 s 214 A113 044 s 214 AI60 029 so 214 A114 024 s 214 AI61 044 s 214 AilS 000 s 214 AI(il 000 s 214 All 6 044 s 214 AI63 024 s 214 All7 000 214 AI64 129 i 214 AilS 024 i 214 A16S 000 s 214 A1l9 004 oS 214 Al66 044 s 214 AilO 000 s 214 AI67 044 s 214 A121 000 2L4 A168 000 s 214 Al22 064 ~ 214 A169 1529 s 214

A123 000 oS 214 A170 000 s 214 Al24 393 214 At7t 009 s 214 AIlS 084 214 Al72 000 ~ 214 A126 000 s 214 AI3 184 s 214 AU7 000 214 AI7 000 s 214 All8 364 s 214 AI7S 000 s 214 All9 000 214 A176 000 s 214 A130 000 214 AI77 000 s 214 Al31 064 214 AI78 000 214 A132 000 SO 214 A179 073 s 214 Al33 000 s 214 AlSO 000 s 214 At34 000 s 214 AlaI 049 s 214 A135 424 s 214 Al8l 000 s 214 Al36 000 5214 Al13 044 s 214 Atl7 024 ~ 214 Al84 064 s 214 AilS 000 s 214 A18S 000 s 214 A139 044 pound 214 AI86 124 -5 214 A140 000 -s 214 Al87 000 s 214 A141 004 214 A188 000 s 214 LSA 0925 eJlC-14 0574 iffH-J 3078 BackgrQund CPM 214 DPM MDA WindQW 0 middot10110 keV

Enclosure 3

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 17: r'j Celsis Analytical Services - NRC

Celsis Analytical Services License Closeout Survey September 28~ 2011

Page 16 of16

Liquid Scintillation Analysis Paekard Tri--Carb 2100TR Grid Raw 1 Net No CPM PPM A189 000 2t4 Al90 000 s 214 A191 004 s 214 A19Z 000 s 214 A193 000 So 214

LSA 0915 ejfC14 0574 effH-3 3078 Background CPM 214 DPMMDA Window Omiddot 2000 keV

Enclosure 3

Btd Wd6poundS0 tt0e Be odas LSB6Be69E9

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~

Page 18: r'j Celsis Analytical Services - NRC

R M WESTER amp ASSOCIATES INC 215lNDACOM DRIVE-ST PETERS MISSOURI 63376

wwwrmwestercom (636) 928-9628middot FAX (636) 928-9857

C 0 V E R

FAX 5 H E E T

fo NRC Region III - Materials Licensing Branch Fnx 630-515-1078 Date September 29 2011 Pages 18 including this cover sheet

COMMENTS

Please review at your earliest convenience regarding termination of Celsis USNRC License

Kevin McCann R M Wester amp Associates Inc 215 Indacom Drive St Peters Missouri 63366-2434

Cell 636-448-114 t Office 636-928-9628 Fax 636middot928-9857

LS868c69pound9 ON 3NOHd middotour s~+e100SS~ ~ ~~+S~M middotWmiddot~ wo~~