rulemaking hearing rule(s) filing form...2017/07/05 · pursuant to tenn. code ann. 4-5-229, any...

Department of State Division of Publications 312 Rosa L. Parks Avenue, 8th Floor Snodgrass/TN Tower Nashville, TN 37243 Phone: 615-741 -2650 Email: [email protected]

For Department of State Use Only

Sequence Number: OS'- o-=1-\1-Rule ID(s): C"o'5..2 l File Date: SI '1} 11-

Effective Date: _ ?>..._,_I _,71-'--J,__,l'-'1-'--------

Rulemaking Hearing Rule(s) Filing Form Rulemaking Hearing Rules are rules filed after and as a result of a rulemaking hearing (Tenn. Code Ann. § 4-5-205).

Pursuant to Tenn. Code Ann. § 4-5-229, any new fee or fee increase promulgated by state agency rule shall take effect on July 1, following the expiration of the ninety (90) day period as provided in § 4-5-207. This section shall not apply to rules that implement new fees or fee increases that are promulgated as emergency rules pursuant to§ 4-5-208(a) and to subsequent rules that make permanent such emergency rules, as amended during the rulemaking process. In addition, this section shall not apply to state agencies that did not, during the preceding two (2) fiscal years, collect fees in an amount sufficient to pay the cost of operating the board, commission or entity in accordance with § 4-29-121 (b).

Agen~y/B~ard/Commission: 1 E_ilvironme-nt c1nd_ConservatiQ,:, Division: , Solid Waste Management

Contact Person: ~-- Jackie Ok-oreeh-Baa-h -Address:

Zip: Phone: Email:

1 William R. Snodgrass TN Tower

1 312 Rosa L. Parks Avenue, 14th Floor

· N_as~_1Jille, Tennessee 37243

: (615) 53?-0825 _ [email protected]

Revision Type (check all that apply): X Amendment

New Repeal

Rule(s) Revised (ALL chapters and rules contained in filing must be listed here. If needed, copy and paste additional tables to accommodate multiple chapters . Please enter only ONE Rule Number/Rule Title per row)

Chapter Number Chapter Title 0400-12-01 Hazardous Waste Manaqement Rule Number Rule Title 0400-12-01-.02 Identification and Listinq of Hazardous Waste 0400-12-01-.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste

Treatment, Storaqe, and Disposal Facilities 0400-12-01 -.10 Land Disposal Restrictions

SS-7039 (November 2014) RDA 1693

75 Day Stay of Effective Date of Rules filed July 20, 2017; new effective date October 21, 2017. See page 104. 75 Day Stay of Effective Date of Rules filed September 7, 2017; new effective date January 4, 2018. See page 106.

(Place substance of rules and other info here. Statutory authority must be given for each rule change. For information on formatting rules go to http://state.tn.us/sos/rules/1 360/1360.htm)

Amendments

Chapter 0400-12-01 Hazardous Waste Management

Part 1 of subparagraph (c) of paragraph (4) of Rule 0400-12-01 -.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following :

Industry and Hazardous

Waste Code

Wood preservation:

K001

Inorganic pigments:

K002

K003

K004

K005

K006

KOO?

KOOB

Organic chemicals:

K009

K010

K011

K013

1. The following solid wastes are listed hazardous wastes from specific sources unless they are excluded under subparagraphs (a) and (c) of Rule 0400-12-01 -.01(3) and listed in paragraph (5) Appendix IX of this rule.

Hazardous Waste

Bottom sediment sludge from the treatment of wastewaters from wood preserving processes that use creosote and/or pentachlorophenol.

Wastewater treatment sludge from the production of chrome yellow and orange pigments .

Wastewater treatment sludge from the production of molybdate orange pigments.

Wastewater treatment sludge from the production of zinc yellow pigments.

Wastewater treatment sludge from the production of chrome green pigments.

Wastewater treatment sludge from the production of chrome oxide green pigments (anhydrous and hydrated).

Wastewater treatment sludge from the production of iron blue pigments .

Oven residue from the production of chrome oxide green pigments.

Distillation bottoms from the production of acetaldehyde from ethylene.

Distillation side cuts from the production of acetaldehyde from ethylene.

Bottom stream from the wastewater stripper in the production of acrylonitrile.

Bottom stream from the acetonitrile column in the production of acrylonitrile.

Hazard Code

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(R, T)

(R, T)

SS-7039 (November 2014) 2 RDA 1693

K014

K015

K016

K017

K018

K019

K020

K021

K022

K023

K024

K025

K026

K027

K028

K029

K030

K083

K085

K093

K094

K095

K096

K103

Bottoms from the acetonitrile purification column in the production of acrylonitrile.

Still bottoms from the distillation of benzyl chloride.

Heavy ends or distillation residues from the production of carbon tetrachloride.

Heavy ends (still bottoms) from the purification column in the production of epichlorohydrin.

Heavy ends from the fractionation column in ethyl chloride production.

Heavy ends from the distillation of ethylene dichloride in ethylene dichloride production.

Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer production.

Aqueous spent antimony catalyst waste from fluoromethanes production.

Distillation bottom tars from the production of phenol/acetone from cumene.

Distillation light ends from the production of phthalic anhydride from naphthalene.

Distillation bottoms from the production of phthalic anhydride from naphthalene.

Distillation bottoms from the production of nitrobenzene by the nitration of benzene.

Stripping still tails from the production of methyl ethyl pyridines.

Centrifuge and distillation residues from toluene diisocyanate production.

Spent catalyst from the hydrochlorinator reactor in the production of 1, 1, 1-trichloroethane.

Waste from the product steam stripper in the production of 1, 1, 1-trichloroethane.

Column bottoms or heavy ends from the combined production of trichloroethylene and perchloroethylene.

Distillation bottoms from aniline production.

Distillation or fractionation column bottoms from the production of chlorobenzenes.

Distillatio.n light ends from the production of phthalic anhydride from ortho-xylene.

Distillation bottoms from the production of phthalic anhydride from ortho-xylene.

Distillation bottoms from the production of 1, 1, 1-trichloroethane.

Heavy ends from the heavy ends column from the production of 1, 1, 1-trichloroethane.

Process residues from aniline extraction from the production of aniline.

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(R, T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

K104 Combined wastewater streams generated from nitrobenzene/aniline (T) production.

SS-7039 (November 2014) 3 RDA 1693

K105

K107

K108

K109

K110

K111

K112

K113

K114

K115

K116

K117

K118

K136

K149

K150

K151

Separated aqueous stream from the reactor product washing step in the production of chlorobenzenes .

Column bottoms from product separation from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

Condensed column overheads from product separation and condensed reactor vent gases from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

Spent filter cartridges from product purification from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

Condensed column overheads from intermediate separation from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

Product washwaters from the production of dinitrotoluene via nitration of toluene.

Reaction by-product water from the drying column in the production of toluenediamine via hydrogenation of dinitrotoluene.

Condensed liquid light ends from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.

Vicinals from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.

Heavy ends from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.

Organic condensate from the solvent recovery column in the production of toluene diisocyanate via phosgenation of toluenediamine.

Wastewater from the reactor vent gas scrubber in the production of ethylene dibromide via bromination of ethene.

Spent adsorbent solids from purification of ethylene dibromide in the production of ethylene dibromide via bromination of ethene.

Still bottoms from the purification of ethylene dibromide in the production of ethylene dibromide via bromination of ethene.

Distillation bottoms from the production of alpha- (or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups, (This waste does not include still bottoms from the distillation of benzyl chloride.).

Organic res iduals, excluding spent carbon adsorbent, from the spent chlorine gas and hydrochloric acid recovery processes associated with the production of alpha- (or methyl-) chlorinated toluenes, ringchlorinated toluenes, benzoyl chlorides , and compounds with mixtures of these functional groups.

Wastewater treatment sludges, excluding neutralization and biological sludges, generated during the treatment of wastewaters from the production of alpha-(or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups.

(T)

(C,T)

(1,T}

(T}

(T)

(C,T)

(T}

(T}

(T)

(T}

(T)

(T)

(T}

(T}

(T)

(T)

(T}

SS-7039 (November 2014) 4 RDA 1693

K156

K157

K158

K159

K161

K174

K175

Organic waste (including heavy ends, still bottoms, light ends, spent solvents, filtrates, and decantates) from the production of carbamates and carbamoyl oximes. (This listing does not apply to wastes generated from the manufacture of 3-iodo-2-propynyl n-butylcarbamate.)

Wastewaters (including scrubber waters, condenser waters, washwaters, and separation waters) from the production of carbamates and carbamoyl oximes. (This listing does not apply to wastes generated from the manufacture of 3-iodo-2-propynyl nbutylcarbamate.)

Bag house dusts and filter/separation solids from the production of carbamates and carbamoyl oximes. (This listing does not apply to wastes generated from the manufacture of 3-iodo-2-propynyl nbutylcarbamate.).

Organics from the treatment of thiocarbamate wastes

Purification solids (including filtration, evaporation, and centrifugation solids), bag house dust and floor sweepings from the production of dithiocarbamate acids and their salts. (This listing does not include K125 or K126.)

Wastewater treatment sludges from the production of ethylene dichloride or vinyl chloride monomer (including sludges that result from commingled ethylene dichloride or vinyl chloride monomer wastewater and other wastewater), unless the sludges meet the following conditions: (i) they are disposed of in a Subtitle C or nonhazardous landfill licensed or permitted by the state or federal government; (ii) they are not otherwise placed on the land prior to final disposal; and (iii) the generator maintains documentation demonstrating that the waste was either disposed of in an on-site landfill or consigned to a transporter or disposal facility that provided a written commitment to dispose of the waste in an off-site landfill. Respondents in any action brought to enforce the requirements of Subtitle C must, upon a showing by the government that the respondent managed wastewater treatment sludges from the production of vinyl chloride monomer or ethylene dichloride, demonstrate that they meet the terms of the exclusion set forth above. In doing so, they must provide appropriate documentation (e.g., contracts between the generator and the landfill owner/operator, invoices documenting delivery of waste to landfill , etc.) that the terms of the exclusion were met.

Wastewater treatment sludges from the production of vinyl chloride monomer using mercuric chloride catalyst in an acetylene-based process.

(T)

(T)

(T)

(T)

(R,T)

(T)

(T)

SS-7039 (November 2014) 5 RDA 1693

K181

Inorganic chemicals:

K071

K073

K106

K176

K177

K178

Pesticides:

K031

K032

K033

K034

K035

Nonwastewaters from the production of dyes and/or pigments (including nonwastewaters commingled at the point of generation with nonwastewaters from other processes) that, at the point of generation, contain mass loadings of any of the constituents identified in part 3 of this subparagraph that are equal to or greater than the corresponding part 3 levels, as determined on a calendar year basis . These wastes will not be hazardous if the nonwastewaters are: (i) disposed in a Subtitle D landfill unit subject to the design criteria in 40 CFR 258.40, (ii) disposed in a Subtitle C landfill unit subject to either Rule 0400-12-01-.06(14)(b) or Rule 0400-12-01 -.05(14)(b); (iii) disposed in other Subtitle D landfill units that meet the design criteria in 40 CFR 258.40, Rule 0400-12-01-.06(14)(b), or Rule 0400-12-01 -. 05(14)(b); or (iv) treated in a combustion unit that is permitted under Subtitle C, or an onsite combustion unit that is permitted under the Clean Air Act. For the purposes of this listing, dyes and/or pigments production is defined in subpart 2(i) of this subparagraph . Part 4 of this subparagraph describes the process for demonstrating that a facility's nonwastewaters are not K181. This listing does not apply to wastes that are otherwise identified as hazardous under subparagraphs (b) through (e) of paragraph (3) of this rule and subparagraphs (b) through (d) of paragraph (4) of this rule at the point of generation. Also, the listing does not apply to wastes generated before any annual mass loading limit is met.

Brine purification muds from the mercury cell process in chlorine production, where separately prepurified brine is not used.

Chlorinated hydrocarbon waste from the purification step of the diaphragm cell process using graphite anodes in chlorine production.

Wastewater treatment sludge from the mercury cell process in chlorine production.

Baghouse filters from the production of antimony oxide, including filters from the production of intermediates (e. g., antimony metal or crude antimony oxide).

Slag from the production of antimony oxide that is speculatively accumulated or disposed, including slag from the production of intermediates (e.g., antimony metal or crude antimony oxide).

Residues from manufacturing and manufacturing-site storage of ferric chloride from acids formed during the production of titanium dioxide using the chloride-ilmenite process.

By-product salts generated in the production of MSMA and cacodylic acid.

Wastewater treatment sludge from the production of chlordane.

Wastewater and scrub water from the chlorination of cyclopentadiene in the production of chlordane.

Filter solids from the filtration of hexachlorocyclopentadiene in the production of chlordane.

Wastewater treatment sludges generated in the production of creosote.

(T)

(T)

(T)

(T)

(E)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

SS-7039 (November 2014) 6 RDA 1693

K036

K037

K038

K039

K040

K041

K042

K043

K097

K098

K099

K123

K124

K125

K126

K131

K132

Explosives:

K044

K045

K046

K047

Petroleum refining:

K048

K049

KOSO

K051

Still bottoms from toluene reclamation distillation in the production of disulfoton.

Wastewater treatment sludges from the production of disulfoton.

Wastewater from the washing and stripping of phorate production.

Filter cake from the filtration of diethylphosphorodithioic acid in the production of phorate.

Wastewater treatment sludge from the production of phorate.

Wastewater treatment sludge from the production of toxaphene.

Heavy ends or distillation residues from the distillation of tetrachlorobenzene in the production of 2,4,5-T.

2,6-Dichlorophenol waste from the production of 2,4-D.

Vacuum stripper discharge from the chlordane chlorinator in the production of chlordane.

Untreated process wastewater from the production of toxaphene.

Untreated wastewater from the production of 2,4-D.

Process wastewater (including supernates, filtrates, and washwaters) from the production of ethylenebisdithiocarbamic acid and its salt.

Reactor vent scrubber water from the production of ethylenebisdithiocarbamic acid and its salts .

Filtration, evaporation, and centrifugation solids from the production of ethylenebisdithiocarbamic acid and its salts.

Baghouse dust and floor sweepings in milling and packaging operations from the production or formulation of ethylenebisdithiocarbamic acid and its salts.

Wastewater from the reactor and spent sulfuric acid from the acid dryer from the production of methyl bromide.

Spent absorbent and wastewater separator solids from the production of methyl bromide.

Wastewater treatment sludges from the manufacturing and processing of explosives.

Spent carbon from the treatment of wastewater containing explosives.

Wastewater treatment sludges from the manufacturing, formulation and loading of lead-based initiating compounds .

Pink/red water from TNT operations.

Dissolved air flotation (OAF) float from the petroleum refining industry.

Slop oil emulsion solids from the petroleum refining industry.

Heat exchanger bundle cleaning sludge from the petroleum refining industry.

API separator sludge from the petroleum refining industry.

(T)

(T)

(T)

(T}

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T}

(C, T)

(T)

(T)

(C,T}

(T)

(R)

(R)

(T)

(R)

(T}

(T)

(T}

K052 Tank bottoms (leaded) from the petroleum refining industry.

(T)

(T)

RDA 1693 SS-7039 (November 2014) 7

K169

K170

K171

K172

Iron and steel:

K061

K062

Primary aluminum:

K088

Secondary lead:

K069

K100

Veterinary pharmaceuticals:

K084

K101

K102

Ink formulation:

Crude oil storage tank sediment from petroleum refining operations .

Clarified slurry oil tank sediment and/or in-line filter/separation solids from petroleum refining operations.

Spent Hydrotreating catalyst from petroleum refining operations, including guard beds used to desulfurize feeds to other catalytic reactors (this listing does not include inert support media).

Spent Hydrorefining catalyst from petroleum refining operations, including guard beds used to desulfurize feeds to other catalytic reactors (this listing does not include inert support media).

Emission control dust/sludge from the primary production of steel in electric furnaces.

Spent pickle liquor generated by steel finishing operations of facilities within the iron and steel industry {SIC Codes 331 and 332).

Spent potliners from primary aluminum reduction .

Emission control dust/sludge from secondary lead smelting. (Note: This listing is stayed administratively for sludge generated from secondary acid scrubber systems. The stay will remain in effect until further administrative action is taken . If EPA takes further action effecting this stay, EPA will publish a notice of the action in the Federal Register).

Waste leaching solution from acid leaching of emission control dust/sludge from secondary lead smelting .

Wastewater treatment sludges generated during the production of veterinary pharmaceuticals from arsenic or organo-arsenic compounds .

Distillation tar residues from the distillation of aniline-based compounds in the production of veterinary pharmaceuticals from arsenic or organo-arsenic compounds.

Residue from the use of activated carbon for decolorization in the production of veterinary pharmaceuticals from arsenic or organoarsenic compounds.

(T)

(T)

(l,T)

(1,T)

(T)

(C,T)

{T)

{T}

(T)

{T}

{T}

{T}

SS-7039 (November 2014) 8 RDA 1693

K086

Coking:

K060

K087

K141

K142

K143

K144

K145

K147

K148

Solvent washes and sludges, caustic washes and sludges, or water washes and sludges from cleaning tubs and equipment used in the formulation of ink from pigments, driers, soaps, and stabilizers containing chromium and lead.

Ammonia still lime sludge from coking operations.

Decanter tank tar sludge from coking operations.

Process residues from the recovery of coal tar, including, but not limited to, collecting sump residues from the production of coke from coal or the recovery of coke by-products produced from coal. This listing does not include K087 (decanter tank tar sludges from coking operations).

Tar storage tank residues from the production of coke from coal or from the recovery of coke by-products produced from coal.

Process residues from the recovery of light oil, including, but not limited to, those generated in stills, decanters, and wash oil recovery units from the recovery of coke by-products produced from coal.

Wastewater sump residues from light oil refining, including, but not limited to, intercepting or contamination sump sludges from the recovery of coke by-products produced from coal.

Residues from naphthalene collection and recovery operations from the recovery of coke by-products produced from coal.

Tar storage tank residues from coal tar refining.

Residues from coal tar distillation, including but not limited to, still bottoms.

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

Authority: T.C.A. §§ 68-212-101 et seq . and 4-5-201 et seq.

Part 6 ofsubparagraph (d) of paragraph (4) of Rule 0400-12-01 -.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following:

Hazardous Waste No.

U394

U001

U034

6. The commercial chemical products, manufacturing chemical intermediates, or offspecification commercial chemical products referred to in parts 1 through 4 of this subparagraph, are identified as toxic wastes (T), unless otherwise designated and are subject to the small quantity generator exclusion defined in parts (1 )(e) 1 and 7 of this rule.

(Comment: For the convenience of the regulated community, the primary hazardous properties of these materials have been indicated by the letters T (Toxicity), R (Reactivity), I (lgnitability) and C (Corrosivity). Absence of a letter indicates that the compound is only listed for toxicity.)

These wastes and their corresponding Hazardous Waste Codes are:

Chemical Substance Abstracts No.

30558-43-1 A2213.

75-07-0 Acetaldehyde (I)

75-87-6 Acetaldehyde, trichloro-

SS-7039 (November 2014) 9 RDA 1693

U187 62-44-2

U005 53-96-3

U240 194-75-7

U112 141 -78-6

U144 301-04-2

U214 563-68-8

see F027 93-76-5

U002 67-64-1

U003 75-05-8

U004 98-86-2

U005 53-96-3

U006 75-36-5

U007 79-06-1

U008 79-10-7

U009 107-13-1

U011 61 -82-5

U012 62-53-3

U136 75-60-5

U014 492-80-8

U015 115-02-6

U010 50-07-7

U280 101-27-9

U278 22781 -23-3

U364 22961-82-6

U271 17804-35-2

U157 56-49-5

U016 225-51-4

U017 98-87-3

U192 23950-58-5

U018 56-55-3

U094 57-97-6

U012 62-53-3

U014 492-80-8

U049 3165-93-3

U093 60-11 -7

U328 95-53-4

SS-7039 (November 2014)

Acetamide, N-(4-ethoxyphenyl)

Acetamide, N-9H-fluoren-2-yl-

Acetic acid, (2,4-dichlorophenoxy)-, salts & esters

Acetic acid, ethyl ester (1)

Acetic acid, lead(2+) salt

Acetic acid, thallium(1+) salt

Acetic acid, (2,4,5-trichlorophenoxy)

Acetone (I)

Acetonitrile (l,T)

Acetophenone

2-Acetylaminofluorene

Acetyl chloride (C,R,T)

Acrylamide

Acrylic acid (I)

Acrylonitrile

Amitrole

Aniline (1,T)

Arsinic acid, dimethyl

Auramine

Azaserine

Azirino[2' ,3' :3, 4 ]pyrrolo[ 1 ,2-a ]indole-4, 7-dione, 6-amino-8-[[ ( aminocarbonyl)oxy ]methyl]-1, 1 a,2,8,8a,8b-hexahydro-8a-methoxy-5-methyl-, (1 aS-(1 aalpha, 8beta,8aalpha,8balpha)]-

Barban.

Bendiocarb.

Bendiocarb phenol.

Benomyl.

BenzU]aceanthrylene, 1,2-dihydro-3-methyl-

Benz[c]acridine

Benzal chloride

Benzamide, 3,5-dichloro-N-(1 , 1-dimethyl-2-propynyl)-

Benz[a]anthracene

Benz[ a]anthracene, 7, 12-dimethyl-

Benzenamine (l,T)

Benzenamine, 4,4'-carbonimidoylbis[N,N-dimethyl-

Benzenamine, 4-chloro-2-methyl-, hydrochloride

Benzenamine, N,N-dimethyl-4-(phenylazo)-

Benzenamine, 2-methyl-

10 RDA 1693

U353 106-49-0 Benzenamine, 4-methyl-

U158 101 -14-4 Benzenamine, 4,4'-methylenebis[2-chloro-

U222 636-21 -5 Benzenamine, 2-methyl-, hydrochloride

U181 99-55-8 Benzenamine, 2-methyl-5-nitro-

U019 71 -43-2 Benzene (l,T)

U038 510-15-6 Benzeneacetic acid, 4-chloro-alpha-(4-chlorophenyl)-alpha-hydroxy-, ethyl ester

U030 101 -55-3 Benzene, 1-bromo-4-phenoxy-

U035 305-03-3 Benzenebutanoic acid, 4-[bis(2-chloroethyl)amino]-

U037 108-90-7 Benzene, chloro-

U221 25376-45-8 Benzenediamine, ar-methyl-

U028 117-81 -7 1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) ester

U069 84-74-2 1,2-Benzenedicarboxylic acid, dibutyl ester

U088 84-66-2 1,2-Benzenedicarboxylic acid, diethyl ester

U102 131 -11 -3 1,2-Benzenedicarboxylic acid, dimethyl ester

U107 117-84-0 1,2-Benzenedicarboxylic acid, dioctyl ester

U070 95-50-1 Benzene, 1,2-dichloro-

U071 541 -73-1 Benzene, 1,3-dichloro-


U060 72-54-8 Benzene, 1, 1 '-(2,2-dichloroethylidene)bis[4-chloro-

U017 98-87-3 Benzene, (dichloromethyl)-

U223 26471 -62-5 Benzene, 1,3-diisocyanatomethyl- (R,T)

U239 1330-20-7 Benzene, dimethyl- (I)

U201 108-46-3 1,3-Benzenediol

U127 118-74-1 Benzene, hexachloro-

U056 110-82-7 Benzene, hexahydro- (I)

U220 108-88-3 Benzene, methyl-

U105 121-14-2 Benzene, 1-methyl-2,4-dinitro-

U106 606-20-2 Benzene, 2-methyl-1 ,3-dinitro-

U055 98-82-8 Benzene, (1 -methylethyl)- (1)

U169 98-95-3 Benzene, nitro-

U183 608-93-5 Benzene, pentachloro-

U185 82-68-8 Benzene, pentachloronitro-

U020 98-09-9 Benzenesulfonic acid chloride (C,R)

U020 98-09-9 Benzenesulfonyl chloride (C,R)

U207 95-94-3 Benzene, 1,2,4,5-tetrachloro-

U061 50-29-3 Benzene, 1, 1 '-(2,2,2-trichloroethylidene)bis[4-chloro-

U247 72-43-5 Benzene, 1, 1 '-(2,2,2-trichloroethylidene)bis[4- methoxy-

SS-7039 (November 2014) 11 RDA 1693

U023

U234

U021

U278

U364

U203

U141

U090

U367

U064

U248

U022

U197

U023

U085

U021

U073

U091

U095

U225

U030

U128

U172

U031

U159

U160

U053

U074

U143

U031

U136

U032

U372

U271

U280

98-07-7

99-35-4

92-87-5

22781-23-3

22961-82-6

94-59-7

120-58-1

94-58-6

1563-38-8

189-55-9

181 -81 -2

50-32-8

106-51-4

98-07-7

1464-53-5

92-87-5

91 -94-1

119-90-4

119-93-7

75-25-2

101 -55-3

87-68-3

924-16-3

71 -36-3

78-93-3

1338-23-4

4170-30-3

764-41 -0

303-34-4

Benzene, (trichloromethyl)

Benzene, 1,3,5-trinitro

Benzidine

1,3-Benzodioxol-4-ol, 2,2-dimethyl-, methyl carbamate.

1,3-Benzodioxol-4-ol, 2,2-dimethyl-,

1,3-Benzodioxole, 5-(2-propenyl)-

1,3-Benzodioxole, 5-(1 -propenyl)-

1,3-Benzodioxole, 5-propyl-

7-Benzofuranol, 2,3-dihydro-2,2-dimethyl

Benzo[rst]pentaphene

2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-oxo-1-phenylbutyl)-, & salts, when present at concentrations of 0.3% or less

Benzo[ a]pyrene

p-Benzoquinone

Benzotrichloride (C,R,T)

2,2'-Bioxirane

[1 , 1 '-Biphenyl]-4,4'-diamine

[1, 1 '-Biphenyl]-4,4'-diamine, 3,3'-dichloro

[1, 1 '-Biphenyl]-4,4'-diamine, 3,3'-dimethoxy

[1 , 1 '-Biphenyl]-4,4'-diamine, 3,3'-dimethyl

Bromoform

4-Bromophenyl phenyl ether

1,3-Butadiene, 1, 1,2,3,4,4-hexachloro-

1-Butanamine, N-butyl-N-nitroso-

1-Butanol (1)

2-Butanone (l,T)

2-Butanone peroxide (R,T)

2-Butenal

2-Butene, 1,4-dichloro- (l,T)

2-Butenoic acid, 2-methyl-, 7-[[2,3-dihydroxy- 2-(1-methoxyethyl)-3-methyl-1 -oxobutoxy]methyl]- 2,3,5,7a-tetrahydro-1 H-pyrrolizin-1 -yl ester, [1 S-[1 alpha(Z) ,7(2S*,3R*),7aalpha]]-

71 -36-3 n-Butyl alcohol (I)

75-60-5 Cacodylic acid

13765-19-0 Calcium chromate

10605-21 -7 Carbamic acid, 1 H-benzimidazol-2-yl, methyl ester.

17804-35-2 Carbamic acid, [1-[(butylamino)carbonyl]-1 H-benzimidazol-2- yl]-, methyl ester.

101 -27-9 Carbamic acid, (3-chlorophenyl)-, 4-chloro-2-butynyl ester.

SS-7039 (November 2014) 12 RDA 1693

U238 51-79-6 Carbamic acid, ethyl ester

U178 615-53-2 Carbamic acid, methylnitroso-, ethyl ester

U373 122-42-9 Carbamic acid, phenyl-, 1-methylethyl ester.

U409 23564-05-8 Carbamic acid, [1,2-phenylenebis (iminocarbonothioyl)]bis-, dimethyl ester.

U097 79-44-7 Carbamic chloride, dimethyl-

U114 1111-54-6 Carbamodithioic acid, 1,2-ethanediylbis-, salts & esters

U062 2303-16-4 Carbamothioic acid, bis(1-methylethyl}-, S-(2,3-dichloro-2-propenyl) ester

U389 2303-17-5 Carbamothioic acid, bis(1-methylethyl}-, S-(2,3,3-trichloro-2-propenyl} ester.

U387 52888-80-9 Carbamothioic acid, dipropyl-, S-(phenylmethyl} ester.

U279 63-25-2 Carbary!.

U372 10605-21-7 Carbendazim.

U367 1563-38-8 Carbofuran phenol.

U215 6533-73-9 Carbonic acid, dithallium(1+) salt

U033 353-50-4 Carbonic difluoride

U156 79-22-1 Carbonochloridic acid, methyl ester (1,T)

U033 353-50-4 Carbon oxyfluoride (R,T)

U211 56-23-5 Carbon tetrachloride

U034 75-87-6 Chloral

U035 305-03-3 Chlorambucil

U036 57-74-9 Chlordane, alpha & gamma isomers

U026 494-03-1 Chlornaphazin

U037 108-90-7 Chlorobenzene

U038 510-15-6 Chlorobenzilate

U039 59-50-7 p-Chloro-m-cresol

U042 110-75-8 2-Chloroethyl vinyl ether

U044 67-66-3 Chloroform

U046 107-30-2 Chloromethyl methyl ether

U047 91-58-7 beta-Chloronaphthalene

U048 95-57-8 o-Ch lorophenol

U049 3165-93-3 4-Chloro-o-toluidine, hydrochloride

U032 13765-19-0 Chromic acid H2CrQ4, calcium salt

U050 218-01-9 Chrysene

U051 Creosote

U052 1319-77-3 Cresci (Cresylic acid)

U053 4170-30-3 Croton aldehyde

U055 98-82-8 Cumene (I)

U246 506-68-3 Cyanogen bromide (CN)Br

SS-7039 (November 2014) 13 RDA 1693

U197 106-51-4 2,5-Cyclohexadiene-1,4-dione

U056 110-82-7 Cyclohexane (I)

U129 58-89-9 Cyclohexane, 1,2,3,4,5,6-hexachloro-, (1 alpha,2alpha,3beta,4alpha,5alpha,6beta)-

U057 108-94-1 Cyclohexanone (I)

U130 77.47.4 1,3-Cyclopentadiene, 1,2,3,4,5,5-hexachloro-

U058 50-18-0 Cyclophosphamide

U240 194-75-7 2,4-D, salts & esters

U059 20830-81 -3 Daunomycin

U060 72-54-8 DOD

U061 50-29-3 DDT

U062 2303-16-4 Diallate

U063 53-70-3 Dibenz[ a,h ]anthracene

U064 189-55-9 Dibenzo[ a,i]pyrene

U066 96-12-8 1,2-Dibromo-3-chloropropane

U069 84-74-2 Dibutyl phthalate

U070 95-50-1 o-Dichlorobenzene

U071 541-73-1 m-Dichlorobenzene

U072 106-46-7 p-Dichlorobenzene

U073 91 -94-1 3,3'-Dichlorobenzidine

U074 764-41-0 1,4-Dichloro-2-butene (l,T)

U075 75-71-8 Dichlorodifluoromethane

U078 75-35-4 1, 1-Dichloroethylene

U079 156-60-5 1,2-Dichloroethylene

U025 111 -44-4 Dichloroethyl ether

U027 108-60-1 Dichloroisopropyl ether

U024 111-91 -1 Dichloromethoxy ethane

U081 120-83-2 2,4-Dichlorophenol


U084 542-75-6 1,3-Dichloropropene

U085 1464-53-5 1,2:3,4-Diepoxybutane (l,T)

U395 5952-26-1 Diethylene glycol, dicarbamate.

U108 123-91 -1 1,4-Diethyleneoxide

U028 117-81 -7 Diethylhexyl phthalate

U086 1615-80-1 N,N'-Diethylhydrazine

U087 3288-58-2 0,0-Diethyl S-methyl dithiophosphate

U088 84-66-2 Diethyl phthalate

U089 56-53-1 Diethylstilbesterol

SS-7039 (November 2014) 14 RDA 1693

U090 94-58-6 Dihydrosafrole

U091 119-90-4 3,3'-Dimethoxybenzidine

U092 124-40-3 Dimethylamine (I)

U093 60-11-7 p-Dimethylaminoazobenzene

U094 57-97-6 7, 12-Dimethylbenz[a]anthracene

U095 119-93-7 3,3'-Dimethylbenzidine

U096 80-15-9 alpha,alpha-Dimethylbenzylhydroperoxide (R)

U097 79-44-7 Dimethylcarbamoyl chloride

U098 57-14-7 1, 1-Dimethylhydrazine

U099 540-73-8 1,2-Dimethylhydrazine

U101 105-67-9 2,4-Dimethylphenol

U102 131-11-3 Dimethyl phthalate

U103 77-78-1 Dimethyl sulfate

U105 121-14-2 2,4-Dinitrotoluene


U107 117-84-0 Di-n-octyl phthalate

U108 123-91 -1 1,4-Dioxane

U109 122-66-7 1,2-Diphenylhydrazine

U110 142-84-7 Dipropylamine (I)

U111 621-64-7 Di-n-propylnitrosamine

U041 106-89-8 Epichlorohydrin

U001 75-07-0 Ethanal (I)

U174 55-18-5 Ethanamine, N-ethyl-N-nitroso-

U404 121-44-8 Ethanamine, N,N-diethyl-

U155 91-80-5 1,2-Ethanediamine, N,N-dimethyl-N'-2-pyridinyl-N'-(2-thienylmethyl)-

U067 106-93-4 Ethane, 1,2-dibromo-

U076 75-34-3 Ethane, 1, 1-dichloro-

U077 107-06-2 Ethane, 1,2-dichloro-

U131 67-72-1 Ethane, hexachloro-

U024 111-91-1 Ethane, 1, 1 '-[methylenebis(oxy)]bis[2-chloro-

U117 60-29-7 Ethane, 1, 1 '-oxybis-(1)

U025 111-44-4 Ethane, 1, 1 '-oxybis[2-chloro-

U184 76-01-7 Ethane, pentachloro-

U208 630-20-6 Ethane, 1, 1, 1,2-tetrachloro-

U209 79-34-5 Ethane, 1, 1,2,2-tetrachloro-

U218 62-55-5 Ethanethioamide

U226 71-55-6 Ethane, 1, 1, 1-trichloro-

SS-7039 (November 2014) 15 RDA 1693

U227 79-00-5 Ethane, 1, 1,2-trichloro-

U410 59669-26-0 Ethanimidothioic acid, N,N'- [thiobis[(methylimino)carbonyloxy]]bis-, dimethyl ester

U394 30558-43-1 Ethanimidothioic acid, 2-(dimethylamino)-N-hydroxy-2-oxo-, methyl ester.

U359 110-80-5 Ethanol, 2-ethoxy-

U173 1116-54-7 Ethanol, 2,2'-(nitrosoimino)bis-

U395 5952-26-1 Ethanol, 2,2'-oxybis-, dicarbamate.

U004 98-86-2 Ethanone, 1-phenyl-

U043 75-01 -4 Ethene, chloro-

U042 110-75-8 Ethene, (2-chloroethoxy)-

U078 75-35-4 Ethene, 1, 1-dichloro-

U079 156-60-5 Ethene, 1,2-dichloro-, (E)-

U210 127-18-4 Ethene, tetrachloro-

U228 79-01 -6 Ethene, trichloro-

U112 141-78-6 Ethyl acetate (I)

U113 140-88-5 Ethyl acrylate (I)

U238 51 -79-6 Ethyl carbamate (urethane)

U117 60-29-7 Ethyl ether (1)

U114 1111 -54-6 Ethylenebisdithiocarbamic acid, salts & esters

U067 106-93-4 Ethylene dibromide

U077 107-06-2 Ethylene dichloride

U359 110-80-5 Ethylene glycol monoethyl ether

U115 75-21 -8 Ethylene oxide (1 ,T)

U116 96-45-7 Ethylenethiourea

U076 75-34-3 Ethylidene dichloride

U118 97-63-2 Ethyl methacrylate

U119 62-50-0 Ethyl methanesulfonate

U120 206-44-0 Fluoranthene

U122 50-00-0 Formaldehyde

U123 64-18-6 Formic acid (C,T)

U124 110-00-9 Furan (1)

U125 98-01 -1 2-Furancarboxaldehyde (1)

U147 108-31 -6 2,5-Furandione

U213 109-99-9 Furan, tetrahydro-(1)

U125 98-01 -1 Furfural (1)

U124 110-00-9 Furfuran (I)

U206 18883-66-4 Glucopyranose, 2-deoxy-2-(3-methyl-3-nitrosoureido )-, D-

U206 18883-66-4 D-Glucose, 2-deoxy-2-[[(methylnitrosoamino)- carbonyl]amino]-

SS-7039 (November 2014) 16 RDA 1693

U126 765-34-4 Glycidylaldehyde

U163 70-25-7 Guanidine, N-methyl-N'-nitro-N-nitroso-

U127 118-74-1 Hexachlorobenzene

U128 87-68-3 Hexachlorobutadiene

U130 77-47-4 Hexachlorocyclopentadiene

U131 67-72-1 Hexachloroethane

U132 70-30-4 Hexachlorophene

U243 1888-71 -7 Hexachloropropene

U133 302-01 -2 Hydrazine (R,T)

U086 1615-80-1 Hydrazine, 1,2-diethyl-

U098 57-14-7 Hydrazine, 1, 1-dimethyl-

U099 540-73-8 Hydrazine, 1,2-dimethyl-

U109 122-66-7 Hydrazine, 1,2-diphenyl-

U134 7664-39-3 Hydrofluoric acid (C,T)

U134 7664-39-3 Hydrogen fluoride (C,T)

U135 7783-06-4 Hydrogen sulfide

U135 7783-06-4 Hydrogen sulfide H2S

U096 80-15-9 Hydroperoxide, 1-methyl-1-phenylethyl- (R)

U116 96-45-7 2-lmidazolidinethione

U137 193-39-5 lndeno[1,2,3-cd]pyrene

U190 85-44-9 1,3-lsobenzofurandione

U140 78-83-1 lsobutyl alcohol (l,T)

U141 120-58-1 lsosafrole

U142 143-50-0 Kepone

U143 303-34-4 Lasiocarpine

U144 301 -04-2 Lead acetate

U146 1335-32-6 Lead, bis(acetato-O)tetrahydroxytri-

U145 7446-27-7 Lead phosphate

U146 1335-32-6 Lead subacetate

U129 58-89-9 Lindane

U163 70-25-7 MNNG

U147 108-31 -6 Maleic anhydride

U148 123-33-1 Maleic hydrazide

U149 109-77-3 Malononitrile

U150 148-82-3 Melphalan

U151 7439-97-6 Mercury

U152 126-98-7 Methacrylonitrile (I, T)

SS-7039 (November 2014) 17 RDA 1693

U092 124-40-3 Methanamine, N-methyl- (I)

U029 74-83-9 Methane, bromo-

U045 74-87-3 Methane, chloro- (I , T)

U046 107-30-2 Methane, chloromethoxy-

U068 74-95-3 Methane, dibromo-

U080 75-09-2 Methane, dichloro-

U075 75-71 -8 Methane, dichlorodifluoro-

U138 74-88-4 Methane, iodo-

U119 62-50-0 Methanesulfonic acid, ethyl ester

U211 56-23-5 Methane, tetrachloro-

U153 74-93-1 Methanethiol (I , T)

U225 75-25-2 Methane, tribromo-

U044 67-66-3 Methane, trichloro-

U121 75-69-4 Methane, trichlorofluoro-

U036 57-74-9 4, 7-Methano-1 H-indene, 1,2,4,5,6, 7,8,8-octachloro-2,3,3a,4, 7, 7a-hexahydro-

U154 67-56-1 Methanol (I)

U155 91 -80-5 Methapyrilene

U142 143-50-0 1,3,4-Metheno-2H-cyclobuta[cd]pentalen-2-one, 1, 1 a,3,3a,4,5,5,5a,5b,6-decachlorooctahydro-

U247 72-43-5 Methoxychlor

U154 67-56-1 Methyl alcohol (I)

U029 74-83-9 Methyl bromide

U186 504-60-9 1-Methylbutadiene (1)

U045 74-87-3 Methyl chloride (l ,T)

U156 79-22-1 Methyl chlorocarbonate (l,T)

U226 71 -55-6 Methyl chloroform

U157 56-49-5 3-Methylcholanthrene

U158 101 -14-4 4,4'-Methylenebis(2-chloroaniline)

U068 74-95-3 Methylene bromide

U080 75-09-2 Methylene chloride

U159 78-93-3 Methyl ethyl ketone (MEK) (1,T)

U160 1338-23-4 Methyl ethyl ketone peroxide (R,T)

U138 74-88-4 Methyl iodide

U161 108-10-1 Methyl isobutyl ketone (1)

U162 80-62-6 Methyl methacrylate (l,T)

U161 108-10-1 4-Methyl-2-pentanone (I)

U164 56-04-2 Methylthiouracil

SS-7039 (November 2014) 18 RDA 1693

U010 50-07-7

U059 20830-81-3

U167 134-32-7

U168 91 -59-8

U026 494-03-1

U165 91-20-3

U047 91-58-7

U166 130-15-4

U236 72-57-1

U279 63-25-2

U166 130-15-4

U167 134-32-7

U168 91-59-8

U217 10102-45-1

U169 98-95-3

U170 100-02-7

U171 79-46-9

U172 924-16-3

U173 1116-54-7

U174 55-18-5

U176 759-73-9

U177 684-93-5

U178 615-53-2

U179 100-75-4

U180 930-55-2

U181 99-55-8

U193 1120-71-4

U058 50-18-0

U115 75-21-8

U126 765-34-4

U041 106-89-8

U182 123-63-7

U183 608-93-5

U184 76-01-7

U185 82-68-8

See F027 87-86-5


Mitomycin C

5, 12-Naphthacenedione, 8-acetyl-10-[(3-amino-2,3,6-trideoxy)-alpha-L-lyxohexopyranosyl)oxy]-7,8,9, 1 0-tetrahydro-6,8, 11-trihydroxy-1-methoxy-, (8S-cis)-

1-Naphthalenamine

2-Naphthalenamine

Naphthalenamine, N,N'-bis(2-chloroethyl)

Naphthalene

Naphthalene, 2-chloro-

1,4-Naphthalenedione

2,7-Naphthalenedisulfonic acid, 3,3'-[(3,3'- dimethyl[1, 1 '-biphenyl]-4,4'-diyl)bis(azo)bis[5-amino-4-hydroxy]-, tetrasodium salt

1-Naphthalenol, methylcarbamate.

1,4-Naphthoquinone

alpha-Naphthylamine

beta-Naphthylamine

Nitric acid, thallium(1+) salt

Nitrobenzene (I ,T)

p-Nitrophenol

2-Nitropropane (I,T)

N-Nitrosodi-n-butylamine

N-Nitrosodiethanolamine

N-Nitrosodiethylamine

N-Nitroso-N-ethylurea

N-Nitroso-N-methylurea

N-Nitroso-N-methylurethane

N-Nitrosopiperidine

N-Nitrosopyrrolidine

5-Nitro-o-toluidine

1,2-Oxathiolane, 2,2-dioxide

2H-1,3,2-Oxazaphosphorin-2-amine, N ,N-bis(2-chloroethyl)tetrahydro-, 2-oxide

Oxirane (l ,T)

Oxiranecarboxyaldehyde

Oxirane, (chloromethyl)-

Paraldehyde

Pentachlorobenzene

Pentachloroethane

Pentachloronitrobenzene (PCNB)

Pentachlorophenol

19 RDA 1693

U161 108-10-1 Pentanol, 4-methyl-

U186 504-60-9 1,3-Pentadiene (I)

U187 62-44-2 Phenacetin

U188 108-95-2 Phenol

U048 95-57-8 Phenol, 2-chloro-

U039 59-50-7 Phenol, 4-chloro-3-methyl-

U081 120-83-2 Phenol, 2,4-dichloro-


U089 56-53-1 Phenol, 4,4'-(1,2-diethyl-1,2-ethenediyl)bis-, (E)-

U101 105-67-9 Phenol, 2,4-dimethyl-

U052 1319-77-3 Phenol, methyl-

U132 70-30-4 Phenol, 2,2'-methylenebis[3,4,6-trichloro-

U411 114-26-1 Phenol, 2-(1-methylethoxy)-, methylcarbamate.

U170 100-02-7 Phenol, 4-nitro-

See F027 87-86-5 Phenol, pentachloro-

See F027 58-90-2 Phenol, 2,3,4,6-tetrachloro-

See F027 95-95-4 Phenol, 2,4,5-trichloro-


U150 148-82-3 L-Phenylalanine, 4-[bis(2-chloroethyl)amino]-

U145 7446-27-7 Phosphoric acid, lead(2+) salt (2:3)

U087 3288-58-2 Phosphorodithioic acid, 0,0-diethyl S-methyl ester

U189 1314-80-3 Phosphorus sulfide (R)

U190 85-44-9 Phthalic anhydride

U191 109-06-8 2-Picoline

U179 100-75-4 Piperidine, 1-nitroso-

U192 23950-58-5 Pronamide

U194 107-10-8 1-Propanamine (l,T)

U111 621 -64-7 1-Propanamine, N-nitroso-N-propyl-

U110 142-84-7 1-Propanamine, N-propyl- (1)

U066 96-12-8 Propane, 1,2-dibromo-3-chloro-

U083 78-87-5 Propane, 1,2-dichloro-

U149 109-77-3 Propanedinitrile

U171 79-46-9 Propane, 2-nitro- (l,T)

U027 108-60-1 Propane, 2,2'-oxybis[2-chloro-

U193 1120-71-4 1,3-Propane sultone

See F027 93-72-1 Propanoic acid, 2-(2,4,5-trichlorophenoxy)-

U235 126-72-7 1-Propanol, 2,3-dibromo-, phosphate (3: 1)

SS-7039 (November 2014) 20 RDA 1693

U140 78-83-1 1-Propanol, 2-methyl- (l,T)

U002 67-64-1 2-Propanone (I)

U007 79-06-1 2-Propenamide

U084 542-75-6 1-Propene, 1,3-dichloro-

U243 1888-71-7 1-Propene, 1, 1,2,3,3,3-hexachloro-

U009 107-13-1 2-Propenenitrile

U152 126-98-7 2-Propenenitrile, 2-methyl- (l,T)

U008 79-10-7 2-Propenoic acid (1)

U113 140-88-5 2-Propenoic acid, ethyl ester (I)

U118 97-63-2 2-Propenoic acid, 2-methyl-, ethyl ester

U162 80-62-6 2-Propenoic acid, 2-methyl-, methyl ester (I,T)

U373 122-42-9 Propham.

U411 114-26-1 Propoxur.

U194 107-10-8 n-Propylamine (l,T)

U083 78-87-5 Propylene dichloride

U387 52888-80-9 Prosulfocarb.

U148 123-33-1 3,6-Pyridazinedione, 1,2-dihydro-

U196 110-86-1 Pyridine

U191 109-06-8 Pyridine, 2-methyl-

U237 66-75-1 2,4-(1 H,3H)-Pyrimidinedione, 5-[bis(2- chloroethyl)amino]-

U164 56-04-2 4(1 H)-Pyrimidinone, 2,3-dihydro-6-methyl-2-thioxo-

U180 930-55-2 Pyrrolidine, 1-nitroso-

U200 50-55-5 Reserpine

U201 108-46-3 Resorcinol

U203 94-59-7 Safrole

U204 7783-00-8 Selenious acid

U204 7783-00-8 Selenium dioxide

U205 7488-56-4 Selenium sulfide

U205 7488-56-4 Selenium sulfide SeS2 (R,T)

U015 115-02-6 L-Serine, diazoacetate (ester)

See F027 93-72-1 Silvex (2,4,5-TP)

U206 18883-66-4 Streptozotocin

U103 77-78-1 Sulfuric acid, dimethyl ester

U189 1314-80-3 Sulfur phosphide (R)

See F027 93-76-5 2,4,5-T

U207 95-94-3 1,2,4,5-Tetrachlorobenzene

U208 630-20-6 1, 1, 1,2-Tetrachloroethane

SS-7039 (November 2014) 21 RDA 1693

U209 79-34-5 1, 1,2,2-Tetrachloroethane

U210 127-18-4 Tetrachloroethylene

See F027 58-90-2 2,3,4,6-Tetrachlorophenol

U213 109-99-9 Tetrahydrofuran (I)

U214 563-68-8 Thallium(!) acetate

U215 6533-73-9 Thallium(!) carbonate

U216 7791 -12-0 Thallium(!) chloride

U216 7791 -12-0 Thallium chloride TICI

U217 10102-45-1 Thallium(!) nitrate

U218 62-55-5 Thioacetamide

U410 59669-26-0 Thiodicarb.

U153 74-93-1 Thiomethanol (I,T)

U244 137-26-8 Thioperoxydicarbonic diamide [(H2N)C(S)]2S2, tetramethyl-

U409 23564-05-8 Thiophanate-methyl.

U219 62-56-6 Thiourea

U244 137-26-8 Thiram

U220 108-88-3 Toluene

U221 25376-45-8 Toluenediamine

U223 26471 -62-5 Toluene diisocyanate (R,T)

U328 95-53-4 o-Toluidine

U353 106-49-0 p-T oluidine

U222 636-21 -5 o-T oluidine hydrochloride

U389 2303-17-5 Triallate.

U011 61 -82-5 1 H-1,2,4-Triazol-3-amine

U226 71 -55-6 1, 1, 1-Trichloroethane

U227 79-00-5 1, 1,2-T richloroethane

U228 79-01 -6 T richloroethylene

U121 75-69-4 T richloromonofluoromethane

See F027 95-95-4 2,4,5-T richlorophenol

See F027 88-06-2 2,4,6-T richlorophenol

U404 121-44-8 Triethylamine.

U234 99-35-4 1,3,5-Trinitrobenzene (R,T)

U182 123-63-7 1,3,5-Trioxane, 2,4,6-trimethyl-

U235 126-72-7 Tris(2,3-dibromopropyl) phosphate

U236 72-57-1 Trypan blue

U237 66-75-1 Uracil mustard

U176 759-73-9 Urea, N-ethyl-N-nitroso-

SS-7039 (November 2014) 22 RDA 1693

U177 684-93-5 Urea, N-methyl-N-nitroso-

U043 75-01 -4 Vinyl chloride

U248 181-81 -2 Warfarin, & salts, when present at concentrations of 0.3% or less

U239 1330-20-7 Xylene (I)

U200 50-55-5 Yohimban-16-carboxylic acid, 11, 17-dimethoxy-18-[(3,4,5-trimethoxybenzoyl)oxy]-, methyl ester, (3beta, 16beta, 17alpha, 18beta,20alpha)-

U249 1314-84-7 Zinc phosphide Zn3P2, when present at concentrations of 10% or less

FOOTNOTE: 1CAS Number given for parent compound only.

Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq.

Subparagraph (a) of paragraph (6) of Rule 0400-12-01 -.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following :

(a) Exclusion of comparable fuel and syngas fuel. [40 CFR 261.38)

1. Specifications for excluded fuels.

Wastes that meet the specifications for comparable fuel or syngas fuel under subpart (i) or (ii) of this part, respectively, and the other requirements of this subparagraph, are not solid wastes.

(i) Comparable fuel specifications.

(I) Physical specifications.

I. Heating value. The heating value must exceed 5,000 Btu/lbs. (11,500 J/g).

II. Viscosity. The viscosity must not exceed: 50 cS, as-fired .

(II) Constituent specifications. For compounds listed in Table 1 to this subparagraph, the specification levels and, where non-detect is the specification, minimum required detection limits are: (see Table 1 of this subparagraph).

(ii) Synthesis gas fuel specifications.


Synthesis gas fuel (i.e., syngas fuel) that is generated from hazardous waste must:

(1) Have a minimum Btu value of 100 Btu/Scf;

(11) Contain less than 1 ppmv of total halogen;

(111) Contain less than 300 ppmv of total nitrogen other than diatomic nitrogen (N2);

(IV) Contain less than 200 ppmv of hydrogen sulfide; and

(V) Contain less than 1 ppmv of each hazardous constituent in the target list of appendix VIII constituents in paragraph (5) of this rule.

23 RDA 1693

(iii) Blending to meet the specifications.

(I) Hazardous waste shall not be blended to meet the comparable fuel specification under subpart (i) of this part, except as provided by item (11) of this subpart.

(II) Blending to meet the viscosity specification. A hazardous waste blended to meet the viscosity specification for comparable fuel shall:

I. As generated and prior to any blending, manipulation, or processing, meet the constituent and heating value specifications of subitem (i)(l)I and item (i)(II) of this part;

II. Be blended at a facility that is subject to the applicable requirements of Rules 0400-12-01-.05 and .06, or subparagraph (4)(e) of Rule 0400-12-01-.03; and

Ill. Not violate the dilution prohibition of subpart (vi) of this part.

(iv) Treatment to meet the comparable fuel specifications.

(I) A hazardous waste may be treated to meet the specifications for comparable fuel set forth in subpart (i) of this part provided the treatment:

I. Destroys or removes the constituents listed in the specification or raises the heating value by removing or destroying hazardous constituents or materials;

II. Is performed at a facility that is subject to the applicable requirements of Rules 0400-12-01 -.05 and .06, or subparagraph (4)(e) of Rule 0400-12-01 -.03; and

Ill. Does not violate the dilution prohibition of subpart (vi) of this part.

(11) Residuals resulting from the treatment of a hazardous waste listed in paragraph (4) of this rule to generate a comparable fuel remain a hazardous waste.

(v) Generation of a syngas fuel.

(1) A syngas fuel can be generated from the processing of hazardous wastes to meet the exclusion specifications of subpart (ii) of this part provided the processing:

I. Destroys or removes the constituents listed in the specification or raises the heating value by removing or destroying constituents or materials;

II. Is performed at a facility that is subject to the applicable requirements of Rules 0400-12-01 -.05 and .06, or subparagraph (4)(e) of Rule 0400-12-01-.03 or is an exempt recycling unit pursuant to part (1 )(f)3 of this rule; and

Ill. Does not violate the dilution prohibition of subpart (vi) of this part.

(II) Residuals resulting from the treatment of a hazardous waste listed in paragraph (4) of this rule to generate a syngas fuel remain a hazardous waste.

(vi) Dilution prohibition.

SS-7039 (November 2014) 24 RDA 1693

No generator, transporter, handler, or owner or operator of a treatment, storage, or disposal facility shall in any way dilute a hazardous waste to meet the specifications of subitem (i)(l)I and item (i)(II) of this part for comparable fuel, or subpart (ii) of this part for syngas.

2. Implementation.

(i) General.

(I) Wastes that meet the specifications provided by part 1 of this subparagraph for comparable fuel or syngas fuel are excluded from the definition of solid waste provided that the conditions under this subparagraph are met. For purposes of this subparagraph, such materials are called excluded fuel; the person claiming and qualifying for the exclusion is called the excluded fuel generator and the person burning the excluded fuel is called the excluded fuel burner.

(11) The person who generates the excluded fuel must claim the exclusion by complying with the conditions of this subparagraph and keeping records necessary to document compliance with those conditions.

(ii) Notices.


(I) Notices to the Commissioner.

I. The generator must submit a one-time notice, except as provided by subitem Ill of this item, to the Commissioner or to the Regional or State RCRA and CAA Directors, in whose jurisdiction the exclusion is being claimed and where the excluded fuel will be burned, certifying compliance with the conditions of the exclusion and providing the following documentation:

A. The name, address, and RCRA ID number of the person/facility claiming the exclusion;

B. The applicable EPA Hazardous Waste Code(s) that would otherwise apply to the excluded fuel;

C. The name and address of the units meeting the requirements of subpart (iii) of this part and part 3 of this subparagraph, that will burn the excluded fuel;

D. An estimate of the average and maximum monthly and annual quantity of material for which an exclusion would be claimed, except as provided by subitem Ill of this item; and

E. The following statement, which shall be signed and submitted by the person claiming the exclusion or his authorized representative:

"Under penalty of criminal and civil prosecution for making or submitting false statements, representations, or omissions, I certify that the requirements of subparagraph (6)(a) of Rule 0400-12-01 -.02 have been met for all comparable fuels identified in this notification. Copies of the records and information required at subpart (6)(a)2(viii) of Rule 0400-12-01 -.02 are available

25 RDA 1693

at the generator's facility. Based on my inquiry of the individuals immediately responsible for obtaining the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."

II. If there is a substantive change in the information provided in the notice required under this subpart, the generator must submit a revised notification.

Ill. Excluded fuel generators must include an estimate of the average and maximum monthly and annual quantity of material for which an exclusion would be claimed only in notices submitted after December 19, 2008 for newly excluded fuel or for revised notices as required by subitem II of this item.

(II) Public notice.

Prior to burning an excluded fuel, the burner must publish in a major newspaper of general circulation local to the site where the fuel will be burned, a notice entitled "Notification of Burning a Fuel Excluded Under the Resource Conservation and Recovery Act" and containing the following information:

I. Name, address, and RCRA ID number of the generating facility(ies);

II. Name and address of the burner and identification of the unit(s) that will burn the excluded fuel;

Ill. A brief, general description of the manufacturing, treatment, or other process generating the excluded fuel;

IV. An estimate of the average and maximum monthly and annual quantity of the excluded fuel to be burned; and

V. Name and mailing address of the Commissioner or the Regional or State Directors to whom the generator submitted a claim for the exclusion.

(iii) Burning.


The exclusion applies only if the fuel is burned in the following units that also shall be subject to Federal/State/local air emission requirements, including all applicable requirements implementing section 112 of the Clean Air Act or the Tennessee Air Quality Act:

(I) Industrial furnaces as defined in subparagraph (2)(a) of Rule 0400-12-01 -.01;

(II) Boilers, as defined in subparagraph (2)(a) of Rule 0400-12-01 -.01, that are further defined as follows:

I. Industrial boilers located on the site of a facility engaged in a manufacturing process where substances are transformed into

26 RDA 1693

new products, including the component parts of products, by mechanical or chemical processes; or

II. Utility boilers used to produce electric power, steam, heated or cooled air, or other gases or fluids for sale;

(Ill) Hazardous waste incinerators subject to regulation under paragraph (15) of Rule 0400-12-01 -.05 or Rule 0400-12-01 -.06 and applicable CM MACT standards or the comparable standard under the Tennessee Air Quality Act.

(IV) Gas turbines used to produce electric power, steam, heated or cooled air, or other gases or fluids for sale.

(iv) Fuel analysis plan for generators.


The generator of an excluded fuel shall develop and follow a written fuel analysis plan which describes the procedures for sampling and analysis of the material to be excluded. The plan shall be followed and retained at the site of the generator claiming the exclusion.

(I) At a minimum, the plan must specify:

I. The parameters for which each excluded fuel will be analyzed and the rationale for the selection of those parameters;

II. The test methods which will be used to test for these parameters;

Ill. The sampling method which will be used to obtain a representative sample of the excluded fuel to be analyzed;

IV. The frequency with which the initial analysis of the excluded fuel will be reviewed or repeated to ensure that the analysis is accurate and up to date; and

V. If process knowledge is used in the determination, any information prepared by the generator in making such determination.

(II) For each analysis, the generator shall document the following:

I. The dates and times that samples were obtained, and the dates the samples were analyzed;

II. The names and qualifications of the person(s) who obtained the samples;

Ill. A description of the temporal and spatial locations of the samples;

IV. The name and address of the laboratory facility at which analyses of the samples were performed;

V. A description of the analytical methods used, including any clean-up and sample preparation methods;

VI. All quantitation limits achieved and all other quality control results for the analysis (including method blanks, duplicate analyses, matrix spikes, etc.), laboratory quality assurance data,

27 RDA 1693

and the description of any deviations from analytical methods written in the plan or from any other activity written in the plan which occurred;

VII. All laboratory results demonstrating whether the exclusion specifications have been met; and

VIII. All laboratory documentation that support the analytical results, unless a contract between the claimant and the laboratory provides for the documentation to be maintained by the laboratory for the period specified in subpart (ix) of this part and also provides for the availability of the documentation to the claimant upon request.

(111) Syngas fuel generators shall submit for approval, prior to performing sampling, analysis, or any management of an excluded syngas fuel, a fuel analysis plan containing the elements of item (I) of this subpart to the Commissioner. The approval of fuel analysis plans must be stated in writing and received by the facility prior to sampling and analysis to demonstrate the exclusion of a syngas. The approval of the fuel analysis plan may contain such provisions and conditions as the Commissioner deems appropriate.

(v) Excluded fuel sampling and analysis .


(I) General.

For wastes for which an exclusion is claimed under the specifications provided by subpart 1 (i) or (ii) of this subparagraph, the generator of the waste must test for all the constituents in appendix VIII in paragraph (5) of this rule, except those that the generator determines, based on testing or knowledge, should not be present in the fuel. The generator is required to document the basis of each determination that a constituent with an applicable specification should not be present. The generator may not determine that any of the following categories of constituents with a specification in Table 1 to this subparagraph should not be present:

I. A constituent that triggered the toxicity characteristic for the constituents that were the basis for listing the hazardous secondary material as a hazardous waste, or constituents for which there is a treatment standard for the waste code in subparagraph (3)(a) of Rule 0400-12-01 -.10;

II. A constituent detected in previous analysis of the waste;

Ill. Constituents introduced into the process that generates the waste; or

IV. Constituents that are byproducts or side reactions to the process that generates the waste.

(Note: Any claim under this subpart must be valid and accurate for all hazardous constituents; a determination not to test for a hazardous constituent will not shield a generator from liability should that constituent later be found in the excluded fuel above the exclusion specifications.)

(II) Use of process knowledge. For each waste for which the comparable fuel or syngas exclusion is claimed where the generator of the excluded fuel is not the original generator of the hazardous waste, the generator of

28 RDA 1693

the excluded fuel may not use process knowledge pursuant to item (I) of this subpart and must test to determine that all of the constituent specifications of subparts 1 (i) and (ii) of this subparagraph, as applicable, have been met.

(111) The excluded fuel generator may use any reliable analytical method to demonstrate that no constituent of concern is present at concentrations above the specification levels. It is the responsibility of the generator to ensure that the sampling and analysis are unbiased, precise, and representative of the excluded fuel. For the fuel to be eligible for exclusion, a generator must demonstrate that:

I. The 95% upper confidence limit of the mean concentration for each constituent of concern is not above the specification level; and

II . The analyses could have detected the presence of the constituent at or below the specification level.

(IV) Nothing in this subpart preempts, overrides or otherwise negates the provision in subparagraph (1)(b) of Rule 0400-12-01 -.03, which requires any person who generates a solid waste to determine if that waste is a hazardous waste.

(V) In an enforcement action, the burden of proof to establish conformance with the exclusion specification shall be on the generator claiming the exclusion.

(VI) The generator must conduct sampling and analysis in accordance with the fuel analysis plan developed under subpart (iv) of this part.

(VII) Viscosity condition for comparable fuel.

I. Excluded comparable fuel that has not been blended to meet the kinematic viscosity specification shall be analyzed as-generated .

II. If hazardous waste is blended to meet the kinematic viscosity specification for comparable fuel, the generator shall:

A. Analyze the hazardous waste as-generated to ensure that it meets the constituent and heating value specifications of subpart 1 (i) of this subparagraph; and

B. After blending, analyze the fuel again to ensure that the blended fuel meets all comparable fuel specifications.

(VIII) Excluded fuel must be re-tested, at a minimum, annually and must be retested after a process change that could change its chemical or physical properties in a manner than may affect conformance with the specifications.

(vi) Reserved

(vii) Speculative accumulation.

Excluded fuel must not be accumulated speculatively, as defined in subpart (1)(b)3(viii) of this rule.

(viii) Operating record.

SS-7039 (November 2014) 29 RDA 1693

The generator must maintain an operating record on site containing the following information:

(I) All information required to be submitted to the implementing authority as part of the notification of the claim :

I. The owner/operator name, address, and the facility Installation ID number of the person claiming the exclusion;

II. For each excluded fuel, the hazardous waste codes that would be applicable if the material were discarded; and

Ill. The certification signed by the person claiming the exclusion or his authorized representative.

(11) A brief description of the process that generated the excluded fuel. If the comparable fuel generator is not the generator of the original hazardous waste, provide a brief description of the process that generated the hazardous waste;

(Ill) The monthly and annual quantities of each fuel claimed to be excluded;

(IV) Documentation for any claim that a constituent is not present in the excluded fuel as required under item (v}(I} of this part;

(V) The results of all analyses and all detection limits achieved as required under subpart (iv) of this part;

(VI) If the comparable fuel was generated through treatment or blending, documentation of compliance with the applicable provisions of subparts 1 (iii) and (iv) of this subparagraph;

(VII) If the excluded fuel is to be shipped off-site, a certification from the burner as required under subpart (x) of this part;

(VIII) The fuel analysis plan and documentation of all sampling and analysis results as required by subpart (iv) of this part; and

(IX) If the generator ships excluded fuel off-site for burning, the generator must retain for each shipment the following information on-site:

I. The name and address of the facility receiving the excluded fuel for burning ;

II. The quantity of excluded fuel shipped and delivered;

Ill. The date of shipment or delivery;

IV. A cross-reference to the record of excluded fuel analysis or other information used to make the determination that the excluded fuel meets the specifications as required under subpart (iv) of this part; and

V. A one-time certification by the burner as required under subpart (x) of this part.

(ix) Records retention.

Records must be maintained for a period of three years.

SS-7039 (November 2014) 30 RDA 1693

(x) Burner certification to the generator.

Prior to submitting a notification to the Commissioner, a generator of excluded fuel who intends to ship the excluded fuel off-site for burning must obtain a onetime written, signed statement from the burner:

(I) Certifying that the excluded fuel will only be burned in an industrial furnace, industrial boiler, utility boiler, or hazardous waste incinerator, as required under subpart (iii) of this part;

(11) Identifying the name and address of the facility that will burn the excluded fuel; and

(Ill) Certifying that the State in which the burner is located is authorized to exclude wastes as excluded fuel under the provisions of this subparagraph.

(xi) Ineligible waste codes.

Wastes that are listed as hazardous waste because of the presence of dioxins or furans , as set out in appendix VII in paragraph (5) of this rule, are not eligible for these exclusions, and any fuel produced from or otherwise containing these wastes remains a hazardous waste subject to the full hazardous waste management requirements.

(xii) Regulatory status of boiler residues.

Burning excluded fuel that was otherwise a hazardous waste listed subparagraphs (4)(b) through (d) of this rule does not subject boiler residues , including bottom ash and emission control residues, to regulation as derived-from hazardous wastes.

(xiii) Residues in containers and tank systems upon cessation of operations.


(1) Liquid and accumulated solid residues that remain in a container or tank system for more than 90 days after the container or tank system ceases to be operated for storage or transport of excluded fuel product are subject to regulation under Rules 0400-12-01- .03 through 0400-12-01 -.10.

(11) Liquid and accumulated solid residues that are removed from a container or tank system after the container or tank system ceases to be operated for storage or transport of excluded fuel product are solid wastes subject to regulation as hazardous waste if the waste exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (e) of this rule or if the fuel were otherwise a hazardous waste listed under subparagaphs (4)(b) through (d) of this rule when the exclusion was claimed.

(Ill) Liquid and accumulated solid residues that are removed from a container or tank system and which do not meet the specifications for exclusion under subpart 1 (i) or (ii) of this subparagraph are solid wastes subject to regulation as hazardous waste if:

I. The waste exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (d) of this rule; or

11 . The fuel were otherwise a hazardous waste listed under subparagraphs (4)(b) through (d) of this rule. The hazardous waste code for the listed waste applies to these liquid and accumulated solid resides .

31 RDA 1693

(xiv) Waiver of RCRA Closure Requirements.

Interim status and permitted storage and combustion units, and generator storage units exempt from the permit requirements under subparagraph (4)(e) of Rule 0400-12-01 -.03, are not subject to the closure requirements of Rules 0400-12-01 -.05 and 0400-12-01-.06 provided that the storage and combustion unit has been used to manage only hazardous waste that is subsequently excluded under the conditions of this subparagraph, and that afterward will be used only to manage fuel excluded under this subparagraph.

(xv) Spills and leaks.

(I) Excluded fuel that is spilled or leaked and that therefore no longer meets the conditions of the exclusion is discarded and must be managed as a hazardous waste if it exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (d) of this rule or if the fuel were otherwise a hazardous waste listed in subparagraphs (4)(b) through (d) of this rule.

(11) For excluded fuel that would have otherwise been a hazardous waste listed in subparagraphs (4)(b) through (d) of this rule and which is spilled or leaked, the hazardous waste code for the listed waste applies to the spilled or leaked material.

(xvi) Nothing in this part preempts, overrides, or otherwise negates the provisions in CERCLA Section 103, which establish reporting obligations for releases of hazardous substances, or the Department of Transportation requirements for hazardous materials in 49 CFR parts 171 through 180.

3. Failure to comply with the conditions of the exclusion.

An excluded fuel loses its exclusion if any person managing the fuel fails to comply with the conditions of the exclusion under this subparagraph, and the material must be managed as hazardous waste from the point of generation. In such situations, EPA or the Commissioner may take enforcement action under RCRA section 3008(a), or the Commissioner may take enforcement action under T.C.A. §§ 68-212-101 et seq.

Table 1: Detection and Detection Limit Values for Comparable Fuel Specification

Total Nitrogen as N Total Halogens as Cl

Chemical Name

Total Organic Halogens as Cl Polychlorinated biphenyls total [Arocolors, total] Cyanide, total Metals: Antimony, total Arsenic, total Barium, total Beryllium, total Cadmium, total Chromium, total Cobalt Lead, total Manganese Mercury, total Nickel, total

SS-7039 (November 2014) 32

GAS No.

NA NA NA 1336-36-3 57-12-5

7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7439-92-1 7439-96-5 7439-97-6 7440-02-0

Concentration limit (mg/kg at 10,000 BTU/lb)

4900 540 (1) ND ND

12 0.23 23 1.2

2.3 4.6 31 1.2 0.25 58

Minimum required

detection limit (mg/kg)

1.4 1

1.2

RDA 1693

Selenium, total 7782-49-2 0.23 Silver, total 7440-22-4 2.3 Thallium, total 7440-28-0 23

Hydrocarbons: Benzo[ a]anthracene 56-55-3 2400 Benzene 71 -43-2 4100 Benzo[b]fluoranthene 205-99-2 2400 Benzo[k]fluoranthene 207-08-9 2400 Benzo[a]pyrene 50-32-8 2400 Chrysene 218-01 -9 2400 Dibenzo[a, h]anthracene 53-70-3 2400 7, 12-Dimethylbenz[a]anthracene 57-97-6 2400 Fluoranthene 206-44-0 2400 lndeno(1 , 2, 3-cd)pyrene 193-39-5 2400 3-Methylcholanthrene 56-49-5 2400 Naphthalene 91 -20-3 3200 Toluene 108-88-3 36000

Oxygenates: Acetophenone 98-86-2 2400 Acrolein 107-02-8 39 Allyl alcohol 107-18-6 30 Bis(2-ethylhexl) phthalate [Di-2-ethylhexyl phthalate] 117-81 -7 2400 Butyl benzyl phthalate 85-68-7 2400 o-Cresol [2-Methyl phenol] 95-48-7 2400 m-Cresol [3-Methyl phenol] 108-39-4 2400 p-Cresol [4-Methyl phenol] 106-44-5 2400 Di-n-butyl phthalate 84-74-2 2400 Diethyl phthalate 84-66-2 2400 2, 4-Dimethylphenol 105-67-9 2400 Dimethyl phthalate 131-11 -3 2400 Di-n-octyl phthalate 117-84-0 2400 Endothall 145-73-3 100 Ethyl methacrylate 97-63-2 39 2-Ethoxyethanol [Ethylene glycol monoethyl ether] 110-80-5 100 lsobutyl alcohol 78-83-1 39 lsosafrole 120-58-1 2400 Methyl ethyl ketone [2-Butanone] 78-93-3 39 Methyl methacrylate 80-62-6 39 1, 4-Naphthoquinone 130-15-4 2400 Phenol 108-95-2 2400 Propargyl alcohol [2-Propyn-1-ol] 107-19-7 30 Safrole 94-59-7 2400

Sulfonated Organics: Carbon disulfide 75-15-0 ND 39 Disulfoton 298-04-4 ND 2400 Ethyl methanesulfonate 62-50-0 ND 2400 Methyl methanesulfonate 66-27-3 ND 2400 Phorate 298-02-2 ND 2400 1, 3-Propane sultone 1120-71 -4 ND 100 Tetraethyldithiopyrophosphate [Sulfotepp] 3689-24-5 ND 2400 Thiophenol [Benzenethiol] 108-98-5 ND 30 0, 0, O-Triethyl phosphorothioate 126-68-1 ND 2400

Nitrogenated Organics: Acetonitrile [Methyl cyanide] 75-05-8 ND 39 2-Acetylaminofluorene [2-AAF] 53-96-3 ND 2400 Acrylonitrile 107-13-1 ND 39

SS-7039 (November 2014) 33 RDA 1693

4-Aminobiphenyl 92-67-1 ND 2400 4-Aminopyridine 504-24-5 ND 100 Aniline 62-53-3 ND 2400 Benzidine 92-87-5 ND 2400 Dibenz[a, j]acridine 224-42-0 ND 2400 0, O-Diethyl O-pyrazinyl Phosphorothioate [Thionazin] 297-97-2 ND 2400 Dimethoate 60-51-5 ND 2400 p-(Dimethylamino) azobenzene (4-dimethylaminoazobenzene] 3,3' -Dimethylbenzidine 60-11-7 ND 2400 a, a-Dimethylphenethylamine 119-93-7 ND 2400

122-09-8 ND 2400 3, 3'-Dimethoxybenzidine 119-90-4 ND 100 1, 3-Dinitrobenzene [m-Dinitrobenzene] 99-65-0 ND 2400 4, 6-Dinitro-o-cresol 534-52-1 ND 2400 2, 4-Dinitrophenol 51-28-5 ND 2400 2, 4-Dinitrotoluene 121-14-2 ND 2400 2, 6-Dinitrotoluene 606-20-2 ND 2400 Dinoseb (2-sec-Butyl-4, 6-dinitrophenol] 88-85-7 ND 2400 Diphenylamine 122-39-4 ND 2400 Ethyl carbamate [Urethane] 51 -79-6 ND 100 Ethylenethiourea (2-lmidazolidinethione) 96-45-7 ND 110 Famphur 52-85-7 ND 2400 Methacrylon it rile 126-98-7 ND 39 Methapyrilene 91-80-5 ND 2400 Methomyl 16752-77-5 ND 57 2-Methyllactonitrile, [Acetone cyanohydrin] 75-86-5 ND 100 Methyl parathion 298-00-0 ND 2400 MNNG (N-Metyl-N-nitroso-N[prime]- nitroguanidine) 70-25-7 ND 110 1-Naphthylamine, [ a-Naphthylamine] 134-32-7 ND 2400 2-Naphthylamine, (~-Naphthylamine] 91-59-8 ND 2400 Nicotine 54-11-5 ND 100 4-Nitroaniline, [p-Nitroaniline] 100-01-6 ND 2400 Nitrobenzene 98-95-3 ND 2400 p-Nitrophenol, [p-Nitrophenol] 100-02-7 ND 2400 5-Nitro-o-toluidine 99-55-8 ND ·2400 N-Nitrosodi-n-butylamine 924-16-3 ND 2400 N-Nitrosodiethylamine 55-18-5 ND 2400 N-Nitrosodiphenylamine, [Diphenylnitrosamine] 86-30-6 ND 2400 N-Nitroso-N-methylethylamine 10595-95-6 ND 2400 N-Nitrosomorpholine 59-89-2 ND 2400 N-Nitrosophiperidine 100-75-4 ND 2400 N-Nitrosopyrrolidine 930-55-2 ND 2400 2-Nitropropane 79-46-9 ND 30 Parathion 56-38-2 ND 2400 Phenacetin 62-44-2 ND 2400 1, 4-Phenylne diamine, [p-Phenylenediamine] 106-50-3 ND 2400 N-Phenylthiourea 103-85-5 ND 57 2-Picoline [alpha-Picoline] 109-06-8 ND 2400 Propylthioracil, (6-Propyl-2-thiouracil] 51-52-5 ND 100 Pyridine 110-86-1 ND 2400 Strychnine 57-24-9 ND 100 Thioacetamide 62-55-5 ND 57 Thiofanox 39196-18-4 ND 100 Thiourea 62-56-6 ND 57 T oluene-2,4-diamine (2,4-Diaminotoluene] 95-80-7 ND 57 Toluene-2, 6-diamine (2, 6-Diaminotoluene] 823-40-5 ND 57 o-T oluidine 95-53-4 ND 2400 p-Toluidine 106-49-0 ND 100 1, 3, 5-Trinitrobenzene, [sym-Trinitobenzene] 99-35-4 ND 2400

SS-7039 (November 2014) 34 RDA 1693

Halogenated Organics: Allyl chloride Aramite Benzal chloride [Dichloromethyl benzene] Benzyl chloride bis(2-Chloroethyl)ether [Dichoroethyl ether] Bromoform [Tribromomethane] Bromomethane [Methyl bromide] 4-Bromophenyl phenyl ether [p-Bromo diphenyl ether] Carbon tetrachloride Chlordane p-Chloroaniline Chlorobenzene Chlorobenzilate p-Chloro-m-cresol 2-Chloroethyl vinyl ether Chloroform Chloromethane [Methyl chloride] 2-Chloronaphthalene [beta-Chloronaphthalene] 2-Chlorophenol [o-Chlorophenol] Chloroprene [2-Chloro-1 , 3-butadiene] 2, 4-D [2, 4-Dichlorophenoxyacetic acid] Diallate 1, 2-Dibromo-3-chloropropane 1, 2-Dichlorobenzene [o-Dichlorobenzene] 1, 3-Dichlorobenzene [m-Dichlorobenzene] 1, 4-Dichlorobenzene [p-Dichlorobenzene] 3, 3[prime]-Dichlorobenzidine Dichlorodifluoromethane [CFC-12] 1, 2-Dichloroethane [Ethylene dichloride] 1, 1-Dichloroethylene [Vinylidene chloride] Dichloromethoxy ethane [Bis(2-chloroethoxy)methane] 2,4-Dichlorophenol 2, 6-Dichlorophenol 1, 2-Dichloropropane [Propylene dichloride] cis-1, 3-Dichloropropylene trans-1, 3-Dichloropropylene 1,3-Dichloro-2propanol Endosulfan I Endosulfan II Endrin Endrin aldehyde Endrin Ketone Epichlorohydrin [1 -Chloro-2, 3-epoxy propane] Ethylidene dichloride [1 , 1-Dichloroethane] 2-Fluoroacetamide Heptachlor Heptachlor epoxide Hexachlorobenzene Hexachloro-1, 3-butadiene [Hexachlorobutadiene] Hexachlorocyclopentadiene Hexachloroethane Hexachlorophene Hexachloropropene [Hexachloropropylene] lsodrin Kepone [Chlordecone] Lindane [gamma-BHC] [gammaHexachlorocyclohexane] Methylene chloride [Dichloromethane] 4, 4' -Methylene-bis(2-chloroaniline) Methyl iodide [lodomethane]

SS-7039 (November 2014) 35

107-05-1 140-57-8 98-87-3 100-44-77 111-44-4 75-25-2 74-83-9 101 -55-3 56-23-5 57-74-9 106-47-8 108-90-7 510-15-6 59-50-7 110-75-8 67-66-3 74-87-3 91 -58-7 95-57-8 1126-99-8 94-75-7 2303-16-4 96-12-8 95-50-1 541-73-1 106-46-7 91 -94-1 75-71 -8 107-06-2 75-35-4 111 -91 -1 120-83-2 87-65-0 78-87-5 10061 -01-5 10061-02-6 96-23-1 959-98-8 33213-65-9 72-20-8 7421-93-4 53494-70-5 106-89-8 75-34-3 640-19-7 76-44-8 1024-57-3 118-74-1 87-68-3 77-47-4 67-72-1 70-30-4 1888-71 -7 465-73-6 143-50-0 58-89-9 75-09-2 101-14-4 74-88-4

ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

39 2400 100 100 2400 39 39 2400 39 14 2400 39 2400 2400 39 39 39 2400 2400 39 7 2400 39 2400 2400 2400 2400 39 39 39 2400 2400 2400 39 39 39 30 1.4 1.4 1.4 1.4 1.4 30 39 100 1.4 2.8 2400 2400 2400 2400 59000 2400 2400 4700 1.4 39 100 39

RDA 1693

Notes:

Pentachlorobenzene Pentachloroethane Pentachloronitrobenzene [PCNB} [Quintobenzene] [Quintozene] Pentachlorophenol Pron amide Silvex [2, 4, 5-Trichlorophenoxypropionic acid} 2, 3, 7, 8-Tetrachlorodibenzo-p-dioxin [2, 3, 7, 8-TCDD] 1, 2, 4, 5-Tetrachlorobenzene 1, 1, 2, 2-Tetrachloroethane T etrachloroethylene [Perchloroethylene] 2, 3, 4, 6-Tetrachlorophenol 1, 2, 4-Trichlorobenzene 1, 1, 1-Trichloroethane [Methyl chloroform] 1, 1,2-T richloroethane [Vinyl trichloride}

Trichloroethylene T richlorofluoromethane [T richloromonofluoromethane} 2, 4, 5-Trichlorophenol 2, 4, 6-Trichlorophenol 1, 2, 3-Trichloropropane Vin I Chloride

608-93-5 76-01 -7 82-68-8 87-86-5 23950-58-5 93-72-1 1746-01 -6 95-94-3 79-34-5 127-18-4 58-90-2 120-82-1 71-55-6 79-00-5 79-01 -6 75-69-4 95-95-4 88-06-2 96-18-4 75-01 -4

ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

2400 39 2400 2400 2400 7.0 30 2400 39 39 2400 2400 39 39 39 39 2400 2400 39 39

NA - Not Applicable. ND - Nondetect. 125 or individual halogenated organics listed below.


Subparagraph (k) of paragraph (7) of Rule 0400-12-01 -.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste Treatment, Storage, and Disposal Facilities is amended by deleting it in its entirety and substituting instead the following:

(k) Certification of Completion of Post-closure Care [40 CFR 265.120]

No later than 60 days after the completion of the established post-closure care period for each hazardous waste disposal unit, the owner or operator must submit to the Commissioner, by registered mail , a certification that the post-closure care period for the hazardous waste disposal unit was performed in accordance with the specifications in the approved post-closure plan. The certification must be signed by the owner or operator and a qualified Professional Engineer. Documentation supporting the qualified Professional Engineer's certification must be furnished to the Commissioner upon request until he releases the owner or operator from the financial assurance requirements for post-closure care under part (8)(f)3 of this rule.


Part 2 of subparagraph (g) of paragraph (1) of Rule 0400-12-01 -. 10 Land Disposal Restrictions is amended by deleting subpart (iv) in its entirety and substituting instead the following:

(iv) The treatment facility must submit a one-time certification signed by an authorized representative with the initial shipment of waste or treatment residue of a restricted waste to the land disposal facility. The certification must state :


"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification . Based on my inquiry of those individuals immediately responsible for obtaining this information, I believe that it has been maintained and operated properly so as to comply with the treatment standards specified in Rule 0400-12-001 -.10(3)(a) without impermissible dilution of the prohibited waste . I am aware there are significant penalties for submitting a false

36 RDA 1693


certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."

A certification is also necessary for contaminated soil and it must state:

"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification and believe that it has been maintained and operated properly so as to comply with treatment standards specified in Rule 0400-12-01 -.10(3)(j) without impermissible dilution of the prohibited waste. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."

(I) A copy of the certification must be placed in the treatment facility's onsite files. If the waste or treatment residue changes, or the receiving facility changes, a new certification must be sent to the receiving facility, and a copy placed in the file.

(II) Debris excluded from the definition of hazardous waste under Rule 0400-12-01 -.02(1 )(c)6 (i.e., debris treated by an extraction or destruction technology provided by Table 1, subparagraph (3)(f) of this rule, and debris that the Commissioner has determined does not contain hazardous waste), however, is subject to the notification and certification requirements of part 4 of this subparagraph rather than the certification requirements of this subpart.

(111) For wastes with organic constituents having treatment standards expressed as concentration levels, if compliance with the treatment standards is based in whole or in part on the analytical detection limit alternative specified in part (3)(a)4 of this rule, the certification, signed by an authorized representative, must state the following:

"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification. Based on my inquiry of those individuals immediately responsible for obtaining th is information, I believe that the nonwastewater organic constituents have been treated by combustion units as specified in Rule 0400-12-01-.10(3)(c), Table 1. I have been unable to detect the nonwastewater organic constituents, despite having used best good-faith efforts to analyze for such constituents. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."

(IV) For characteristic wastes that are subject to the treatment standards in subparagraph (3)(a) of this rule (other than those expressed as a method of treatment) or subparagraph (3)(j) of this rule and that contain underlying hazardous constituents as defined in part (b)10 of this paragraph; if these wastes are treated on-site to remove the hazardous characteristic; and are then sent off-site for treatment of underlying hazardous constituents, the certification must state the following:

"I certify under penalty of law that the waste has been treated in accordance with the requirements of Rule 0400-12-01-.10(3)(a) or Rule 0400-12-01 -.10(3)(j) to remove the hazardous characteristic. This decharacterized waste contains underlying hazardous constituents that require further treatment to meet treatment standards. I am aware that

37 RDA 1693

there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."

(V) For characteristic wastes that contain underlying hazardous constituents as defined in part (b )10 of this paragraph that are treated on-site to remove the hazardous characteristic and to treat underlying hazardous constituents to levels in subparagraph (3)(i) of this rule Universal Treatment Standards, the certification must state the following:

"I certify under penalty of law that the waste has been treated in accordance with the requirements of Rule 0400-12-01 -.10(3)(a) to remove the hazardous characteristic, and that underlying hazardous constituents, as defined in Rule 0400-12-01 -.10(1)(b)10, have been treated on-site to meet the Rule 0400-12-01 -.10(3)(i) Universal Treatment Standards. I am aware that there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4 ), this declaration is made under penalty of perjury."


Waste code K161 of the Table "Treatment Standards for Hazarous Wastes" following part 10 of subparagraph (a) of paragraph (3) of Rule 0400-12-01 -.10 Land Disposal Restrictions is amended by deleting "137-30-4" in the third column to the right of "Dithiocarbamates (total) 10 " and replacing it with "NA" so that, as amended, the entry for K161 shall read as follows :

K161 Purification solids (including Antimony 7440-36-0 1.9 1.15 mg/L TCLP filtration, evaporation, and centrifugation solids), baghouse dust and floor sweepings from the production of dithiocarbamate acids and their salts.

Arsenic 7440-38-2 1.4 5.0 mg/L TCLP

Carbon disulfide 75-15-0 3.8 4.8 mg/L TCLP

Dithiocarbamates NA 0.028; or 28; or CMBST (total) 10 CMBST,

CHOXD, BIODG orCARBN

Lead 7439-92-1 0.69 0.75 mg/L TCLP

Nickel 7440-02-0 3.98 11.0 mg/L TCLP

Selenium 7782-49-2 0.82 5.7 mg/L TCLP

Authority: T.C.A. §§ 68-212-101 et seq . and 4-5-201 et seq .

SS-7039 (November 2014) 38 RDA 1693

* If a roll -call vote was necessary, the vote by the Agency on these rulemaking hearing rules was as follows:

Board Member Aye No Abstain Absent Signature (if required)

Marty Calloway X (Petroleum Business with at least 15 Underground Storaqe Tanks) Stacey Cothran X (Solid/Hazardous Waste Manaqement Industry) Kenneth L. Donaldson X (Municipal Government) Dr. George Hyfantis, Jr. X (Institution of Hiqher Learninq) Bhag Kanwar X (Single Facility with less than 5 Underground Storage Tanks) Alan M. Leiserson X Environmental Interests Jared L. Lynn X (Manufacturinq experienced with Solid/Hazardous Waste) David Martin X (Workinq in a field related to Aqriculture) Beverly Philpot X (Manufacturing experienced with Underground Storage Tanks/Hazardous Materials) DeAnne Redman X (Petroleum Manaqement Business) Mayor A. Franklin Smith, Ill X (County Government) Mark Williams X (Small Generator of Solid/Hazardous Materials representinq Automotive Interests)

I certify that this is an accurate and complete copy of rulemaking hearing rules, lawfully promulgated and adopted by the Underground Storage Tanks and Solid Waste Disposal Control Board on 06/03/2015, and is in compliance with the provisions of T.C.A. § 4-5-222.

I further certify the following:

Notice of Rulemaking Hearing filed with the Department of State on: 03/16/2015

Rulemaking Hearing(s) Conducted on: (add more dates). 05/19/2015

Date: June 3, 2015

Signature:

Name of Officer: Stacey Cothran

Title of Officer: Board Chair ----------------------

Subscribed and sworn to before me on: --~- c-~----3~,~~- o~l:;;, _______ _ Notary Public Signature: ~ -~ Q; µL-L -----------=---'--------

My commission expires on: _ 3L-=-=Lu....L:..=..c--==---..ad-=--_,_{-+--=ol~·-o--'-J Co _____ _

SS-7039 (November 2014) 39 RDA 1693

Rules of the Underground Storage Tanks and Solid Waste Disposal Control Board Chapter 0400-12-01 Hazardous Waste Management Rule 0400-12-01-.02 Identification and Listing of Hazardous Waste Rule 0400-12-01-.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste

Treatment, Storage, and Disposal Facilities Rule 0400-12-01 -. 10 Land Disposal Restrictions

All rulemaking hearing rules provided for herein have been examined by the Attorney General and Reporter of the State of Tennessee and are approved as to legality pursuant to the provisions of the Administrative Procedures Act, Tennessee Code Annotated, Title 4, Chapter 5.

Department of State Use Only

r· ·· i_ t_

N

:c 0....

.- ,, -. ,- · -· ,._ ,_ .. __ - --

w =, C.C::::CL (._)

w (J)


ery II Attorney General and Reporter

.s-/ .s-/ :J.D 11 I I Date

Filed with the Department of State on: ___ Sc.....+-

1

1 -=t--+-{~11:~ - --------

Effective on : 0 1 ~, l}-, ------=-+--'-0 T+-+-+--iiu.1£- 2-----------

~ Tre Hargett Secretary of State

40 RDA 1693

Public Hearing Comments

One copy of a document containing responses to comments made at the public hearing must accompany the filing pursuant to T.C.A. § 4-5-222 . Agencies shall include only their responses to public hearing comments, which can be summarized. No letters of inquiry from parties questioning the rule will be accepted. When no comments are received at the public hearing, the agency need only draft a memorandum stating such and include it with the Rulemaking Hearing Rule filing. Minutes of the meeting will not be accepted. Transcripts are not acceptable.

There were no comments received during the comment period.

SS-7039 (November 2014) 41 RDA 1693

Regulatory Flexibility Addendum Pursuant to T.C.A. §§ 4-5-401 through 4-5-404, prior to initiating the rule making process as described in T.C.A. § 4-5-202(a)(3) and T.C.A. § 4-5-202(a), all agencies shall conduct a review of whether a proposed rule or rule affects small businesses.

This rulemaking includes the minor changes EPA has identified when reviewing the regulations to supporting continuing authorization. These changes include: (a) correct a typographical error to the process description to K107; {b) for the Waste code K161 of the Table "Treatment Standards for Hazardous Wastes" in Rule 0400-12-01-.10, delete the CAS number "137-30-4" in the third column to the right of "Dithiocarbamates (total) 10" and replacing it with "NA" so that it is consistent with the federal language.

This rulemaking also makes additional housekeeping changes in order for Tennessee's regulations to be consistent with EPA's and surrounding states. These changes include: (a) adding a common chemical name 1,1,1 -Trichloroethane to the U226 list of commercial chemical products (We are adding 1,1,1 -Trichloroethane for the regulated community's convenience but the chemical was already listed as U226 under the names Ethane, 1, 1, 1-trichloro- and Methyl Chloroform and, therefore is not a new listing.); (b) updating the regulatory language regarding the exclusion of comparable fuel and syngas fuel to be equivalent with EPA's language; (c) correcting the introductory statements to Rule 0400-12-01-.10( 1 )(g)2(iv) so that it reads like the federal language; and {d) adding a sentence to the certification statements to reference T.C.A. § 39-16-702(a)(4) as request by the Attorney General's office.

(1) The type or types of small business and an identification and estimate of the number of small businesses subject to the proposed rule that would bear the cost of, or directly benefit from the proposed rule.

There are many small businesses that generate or manage hazardous waste but these amendments will have no measurable impact on any of them.

(2) The projected reporting, recordkeeping, and other administrative costs required for compliance with the proposed rule, including the type of professional skills necessary for preparation of the report or record.

These amendments not add any additional reporting , recordkeeping or administrative cost to the regulated community

(3) A statement of the probable effect on impacted small businesses and consumers.

There will be no measurable impact on small businesses.

(4) A description of any less burdensome, less intrusive or less costly alternative methods of achieving the purpose and objectives of the proposed rule that may exist, and to what extent the alternative means might be less burdensome to small business.

No alternatives are available to achieve the purpose of this rulemaking.

(5) A comparison of the proposed rule with any federal or state counterparts.

This rulemaking make Tennessee's regulations more consistent with the federal regulations and with surrounding states.

(6) Analysis of the effect of the possible exemption of small businesses from all or any part of the requirements contained in the proposed rule.

There is no effect since this rulemaking has no measurable impact on small businesses.

SS-7039 (November 2014) 42 RDA 1693

Impact on Local Governments

Pursuant to T.C.A. §§ 4-5-220 and 4-5-228 "any rule proposed to be promulgated shall state in a simple declarative sentence, without additional comments on the merits of the policy of the rules or regulation , whether the rule or regulation may have a projected impact on local governments." (See Public Chapter Number 1070 (http://state.tn.us/sos/acts/106/pub/pc1070.pdf) of the 2010 Session of the General Assembly)

The Department does not anticipate an impact on local governments.

SS-7039 (November 2014) 43 RDA 1693

Additional Information Required by Joint Government Operations Committee

All agencies, upon filing a rule, must also submit the following pursuant to T.C.A. § 4-5-226(i)(1 ).

(A) A brief summary of the rule and a description of all relevant changes in previous regulations effectuated by such rule;

This rulemaking includes the minor changes EPA has identified when reviewing the regulations to supporting continuing authorization. These changes include: (a) correct a typographical error to the process description to K107; (b) for the Waste code K161 of the Table "Treatment Standards for Hazardous Wastes" in Rule 0400-12-01-.10, delete the CAS number "137-30-4" in the third column to the right of "Dithiocarbamates (total) 10" and replacing it with "NA" so that it is consistent with the federal language.

This rulemaking also makes additional housekeeping changes in order for Tennessee's regulations to be consistent with EPA's and surrounding states. These changes include: (a) adding a common chemical name 1, 1, 1-Trichloroethane to the U226 list of commercial chemical products (We are adding 1, 1, 1-Trichloroethane for the regulated community's convenience but the chemical was already listed as U226 under the names Ethane, 1, 1, 1-trichloro- and Methyl Chloroform and, therefore is not a new listing.); (b) updating the regulatory language regarding the exclusion of comparable fuel and syngas fuel to be equivalent with EPA's language; (c) correcting the introductory statements to Rule 0400-12-01-.10(1 )(g)2(iv) so that it reads like the federal language; and (d) adding a sentence to the certification statements to reference T.C.A. § 39-16-702(a)(4) as request by the Attorney General's office.

(B) A citation to and brief description of any federal law or regulation or any state law or regulation mandating promulgation of such rule or establishing guidelines relevant thereto;

These rules are being promulgated under the authority of T.C.A. §§ 68-212-101 et seq. These amendments will brin the state hazardous waste re ulations more in line with the federal re ulations and surroundin states.

(C) Identification of persons, organizations, corporations or governmental entities most directly affected by this rule, and whether those persons, organizations, corporations or governmental entities urge adoption or rejection of this rule;

Generators, Treatment, Storage and Disposal Facilities of Hazardous Waste are directly affected by this rulemakin and there were no comments received durin the ublic comment eriod .

(D) Identification of any opinions of the attorney general and reporter or any judicial ruling that directly relates to the rule;

I The Department is not aware of any opinions or judicial rulings that directly relate to this rule.

(E) An estimate of the probable increase or decrease in state and local government revenues and expenditures, if any, resulting from the promulgation of this rule, and assumptions and reasoning upon which the estimate is based. An agency shall not state that the fiscal impact is minimal if the fiscal impact is more than two percent (2%) of the agency's annual budget or five hundred thousand dollars ($500,000), whichever is less;

I This rulemaking will not impact state or local government revenues or expenditures.

(F) Identification of the appropriate agency representative or representatives, possessing substantial knowledge and understanding of the rule;

Jackie Okoreeh-Baah Division of Solid Waste Management William R. Snodgrass Tennessee Tower 312 Rosa L. Parks Avenue, 14th Floor Nashville, Tennessee 37243 (615) 532-0825 Jackie.Okoreeh-Baah®tn.aov

SS-7039 (November 2014) 44 RDA 1693

(G) Identification of the appropriate agency representative or representatives who will explain the rule at a scheduled meeting of the committees;

Jenny Howard Deputy General Counsel Office of General Counsel

(H) Office address, telephone number, and email address of the agency representative or representatives who will explain the rule at a scheduled meeting of the committees; and

Office of General Counsel Tennessee Department of Environment and Conservation William R. Snodgrass Tennessee Tower 312 Rosa L. Parks Avenue, 2nd Floor Nashville, Tennessee 37243 (615) 532-8685 Jennv. [email protected]

(I) Any additional information relevant to the rule proposed for continuation that the committee requests.

I The Department is not aware of any additional relevant information.

SS-7039 (November 2014) 45 RDA 1693

Department of State Division of Publications 312 Rosa L. Parks Avenue, 8th Floor Snodgrass/TN Tower Nashville, TN 37243 Phone: 615-741-2650 Email: [email protected]


Sequence Number:

Rule ID(s):

File Date:

Effective Date:

Rulemaking Hearing Rule(s) Filing Form Rulemaking Hearing Rules are rules filed after and as a result of a rulemaking hearing (Tenn. Code Ann. § 4-5-205).

Pursuant to Tenn. Code Ann. § 4-5-229, any new fee or fee increase promulgated by state agency rule shall take effect on July 1, following the expiration of the ninety (90) day period as provided in§ 4-5-207. This section shall not apply to rules that implement new fees or fee increases that are promulgated as emergency rules pursuant to § 4-5-208(a) and to subsequent rules that make permanent such emergency rules, as amended during the rulemaking process. In addition, this section shall not apply to state agencies that did not, during the preceding two (2) fiscal years, collect fees in an amount sufficient to pay the cost of operating the board, commission or entity in accordance with§ 4-29-121 (b} .

Agen~y/Board/Commission: Division:

Contact Person: Address:

Zip: Phone: Email:

Environment and Conservation - --Solid Waste Management Jackie Okoreeh-Baah

- -William R. Snodgrass TN Tower 312 Rosa L. Parks Avenue, 14th Floor Nashville_. Tennessee 37243 (615) §32-0875 [email protected]

Revision Type (check all that apply): X Amendment

New __ Repeal

Rule(s) Revised (ALL chapters and rules contained in filing must be listed here. If needed, copy and paste additional tables to accommodate multiple chapters. Please enter only ONE Rule Number/Rule Title per row)

Chapter Number Chapter Title 0400-12-01 Hazardous Waste Management Rule Number Rule Title 0400-12-01-.02 Identification and Listing of Hazardous Waste 0400-12-01 -.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste

Treatment, Storage, and Disposal Facilities 0400-12-01-.10 Land Disposal Restrictions

SS-7039 (November 2014) RDA 1693

(Place substance of rules and other info here. Statutory authority must be given for each rule change. For information on formatting rules go to http://state.tn.us/sos/rules/1360/1360.htm)

Amendments

Chapter 0400-12-01 Hazardous Waste Management

Part 1 of subparagraph (c) of paragraph (4) of Rule 0400-12-01-.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following:

Industry and Hazardous

Waste Code

Wood preservation:

K001

Inorganic pigments:

K002

K003

K004

K005

K006

KOO?

KOOS

Organic chemicals:

K009

K010

K011

K013

1. The following solid wastes are listed hazardous wastes from specific sources unless they are excluded under subparagraphs (a) and (c) of Rule 0400-12-01-.01(3) and listed in paragraph (5) Appendix IX of this rule.

Hazardous Waste

Bottom sediment sludge from the treatment of wastewaters from wood preserving processes that use creosote and/or pentachlorophenol.

Wastewater treatment sludge from the production of chrome yellow and orange pigments.

Wastewater treatment sludge from the production of molybdate orange pigments.

Wastewater treatment sludge from the production of zinc yellow pigments .

Wastewater treatment sludge from the production of chrome green pigments.

Wastewater treatment sludge from the production of chrome oxide green pigments (anhydrous and hydrated).

Wastewater treatment sludge from the production of iron blue pigments.

Oven residue from the production of chrome oxide green pigments.

Distillation bottoms from the production of acetaldehyde from ethylene.

Distillation side cuts from the production of acetaldehyde from ethylene.

Bottom stream from the wastewater stripper in the production of acrylonitrile.

' Bottom stream from the acetonitrile column in the production of acrylonitrile.

Hazard Code

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(R, T)

(R, T)

SS-7039 (November 2014) 2 RDA 1693

K014

K015

K016

K017

K018

K019

K020

K021

K022

K023

K024

K025

K026

K027

K028

K029

K030

K083

K085

K093

K094

K095

K096

K103

Bottoms from the acetonitrile purification column in the production of acrylonitrile.

Still bottoms from the distillation of benzyl chloride.

Heavy ends or distillation residues from the production of carbon tetrachloride.

Heavy ends (still bottoms) from the purification column in the production of epichlorohydrin.

Heavy ends from the fractionation column in ethyl chloride production.

Heavy ends from the distillation of ethylene dichloride in ethylene dichloride production.

Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer production.

Aqueous spent antimony catalyst waste from fluoromethanes production.

Distillation bottom tars from the production of phenol/acetone from cumene.

Distillation light ends from the production of phthalic anhydride from naphthalene.

Distillation bottoms from the production of phthalic anhydride from naphthalene.

Distillation bottoms from the production of nitrobenzene by the nitration of benzene.

Stripping still tails from the production of methyl ethyl pyridines.

Centrifuge and distillation residues from toluene diisocyanate production.

Spent catalyst from the hydrochlorinator reactor in the production of 1, 1, 1-trichloroethane.

Waste from the product steam stripper in the production of 1, 1, 1-trichloroethane.

Column bottoms or heavy ends from the combined production of trichloroethylene and perchloroethylene.

Distillation bottoms from aniline production.

Distillation or fractionation column bottoms from the production of chlorobenzenes.

Distillation light ends from the production of phthalic anhydride from ortho-xylene.

Distillation bottoms from the production of phthalic anhydride from ortho-xylene.

Distillation bottoms from the production of 1, 1, 1-trichloroethane.

Heavy ends from the heavy ends column from the production of 1, 1, 1-trichloroethane.

Process residues from aniline extraction from the production of aniline.

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(R, T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

K104 Combined wastewater streams generated from nitrobenzene/aniline (T) production.

SS-7039 (November 2014) 3 RDA 1693

K105

K107

K108

K109

K110

K111

K112

K113

K114

K115

K116

K117

K118

K136

K149

K150

K151

Separated aqueous stream from the reactor product washing step in the production of chlorobenzenes.

Column bottoms from product separation from the production of 4-;4 dimethylhydrazine 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

Condensed column overheads from product separation and condensed reactor vent gases from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

Spent filter cartridges from product purification from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

Condensed column overheads from intermediate separation from the production of 1, 1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.

Product washwaters from the production of dinitrotoluene via nitration of toluene.

Reaction by-product water from the drying column in the production of toluenediamine via hydrogenation of dinitrotoluene.

Condensed liquid light ends from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.

Vicinals from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.

Heavy ends from the purification of toluenediamine in the production of toluenediamine via hydrogenation of dinitrotoluene.

Organic condensate from the solvent recovery column in the production of toluene diisocyanate via phosgenation of toluenediamine.

Wastewater from the reactor vent gas scrubber in the production of ethylene dibromide via bromination of ethene.

Spent adsorbent solids from purification of ethylene dibromide in the production of ethylene dibromide via bromination of ethene.

Still bottoms from the purification of ethylene dibromide in the production of ethylene dibromide via bromination of ethene.

Distillation bottoms from the production of alpha- (or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides , and compounds with mixtures of these functional groups, (This waste does not include still bottoms from the distillation of benzyl chloride.).

Organic residuals, excluding spent carbon adsorbent, from the spent chlorine gas and hydrochloric acid recovery processes associated with the production of alpha- (or methyl-) chlorinated toluenes, ringchlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups.

Wastewater treatment sludges, excluding neutralization and biological sludges, generated during the treatment of wastewaters from the production of alpha-(or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional groups.

(T)

(C,T)

(l ,T)

(T)

(T)

(C,T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

SS-7039 (November 2014) 4 RDA 1693

K156

K157

K158

K159

K161

K174

K175

Organic waste (including heavy ends, still bottoms, light ends, spent solvents, filtrates, and decantates) from the production of carbamates and carbamoyl oximes. {This listing does not apply to wastes generated from the manufacture of 3-iodo-2-propynyl nbutylcarbamate.)

Wastewaters (including scrubber waters, condenser waters, washwaters, and separation waters) from the production of carbamates and carbamoyl oximes. {This listing does not apply to wastes generated from the manufacture of 3-iodo-2-propynyl nbutylcarbamate.)

Bag house dusts and filter/separation solids from the production of carbamates and carbamoyl oximes. (This listing does not apply to wastes generated from the manufacture of 3-iodo-2-propynyl nbutylcarbamate. ).

Organics from the treatment of thiocarbamate wastes

Purification solids (including filtration, evaporation, and centrifugation solids), bag house dust and floor sweepings from the production of dithiocarbamate acids and their salts. (This listing does not include K125 or K126.)

Wastewater treatment sludges from the production of ethylene dichloride or vinyl chloride monomer (including sludges that result from commingled ethylene dichloride or vinyl chloride monomer wastewater and other wastewater), unless the sludges meet the following conditions: (i) they are disposed of in a Subtitle C or nonhazardous landfill licensed or permitted by the state or federal government; (ii) they are not otherwise placed on the land prior to final disposal; and (iii) the generator maintains documentation demonstrating that the waste was either disposed of in an on-site landfill or consigned to a transporter or disposal facility that provided a written commitment to dispose of the waste in an off-site landfill. Respondents in any action brought to enforce the requirements of Subtitle C must, upon a showing by the government that the respondent managed wastewater treatment sludges from the production of vinyl chloride monomer or ethylene dichloride, demonstrate that they meet the terms of the exclusion set forth above. In doing so, they must provide appropriate documentation (e.g., contracts between the generator and the landfill owner/operator, invoices documenting delivery of waste to landfill, etc.) that the terms of the exclusion were met.

Wastewater treatment sludges from the production of vinyl chloride monomer using mercuric chloride catalyst in an acetylene-based process.

(T)

{T)

{T)

(T)

(R,T)

(T)

(T)

SS-7039 (November 2014) 5 RDA 1693

K181

Inorganic chemicals:

K071

K073

K106

K176

K177

K178

Pesticides:

K031

K032

K033

K034

K035

Nonwastewaters from the production of dyes and/or pigments (including nonwastewaters commingled at the point of generation with nonwastewaters from other processes) that, at the point of generation, contain mass loadings of any of the constituents identified in part 3 of this subparagraph that are equal to or greater than the corresponding part 3 levels, as determined on a calendar year basis . These wastes will not be hazardous if the nonwastewaters are: (i) disposed in a Subtitle D landfill unit subject to the design criteria in 40 CFR 258.40, (ii) disposed in a Subtitle C landfill unit subject to either Rule 0400-12-01 -.06(14)(b) or Rule 0400-12-01 -.05(14)(b); (iii) disposed in other Subtitle D landfill units that meet the design criteria in 40 CFR 258.40, Rule 0400-12-01 -.06(14)(b), or Rule 0400-12-01 -.05(14)(b); or (iv) treated in a combustion unit that is permitted under Subtitle C, or an onsite combustion unit that is permitted under the Clean Air Act. For the purposes of this listing, dyes and/or pigments production is defined in subpart 2(i) of this subparagraph. Part 4 of this subparagraph describes the process for demonstrating that a facility's nonwastewaters are not K181 . This listing does not apply to wastes that are otherwise identified as hazardous under subparagraphs (b) through (e) of paragraph (3) of this rule and subparagraphs {b} through (d) of paragraph (4) of this rule at the point of generation. Also, the listing does not apply to wastes generated before any annual mass loading limit is met.

Brine purification muds from the mercury cell process in chlorine production, where separately prepurified brine is not used.

Chlorinated hydrocarbon waste from the purification step of the diaphragm cell process using graphite anodes in chlorine production.

Wastewater treatment sludge from the mercury cell process in chlorine production.

Baghouse filters from the production of antimony oxide, including filters from the production of intermediates (e. g., antimony metal or crude antimony oxide} .

Slag from the production of antimony oxide that is speculatively accumulated or disposed, including slag from the production of intermediates (e.g., antimony metal or crude antimony oxide}.

Residues from manufacturing and manufacturing-site storage of ferric chloride from acids formed during the production of titanium dioxide using the chloride-ilmenite process.

By-product salts generated in the production of MSMA and cacodylic acid .

Wastewater treatment sludge from the production of chlordane.

Wastewater and scrub water from the chlorination of cyclopentadiene in the production of chlordane.

Filter solids from the filtration of hexachlorocyclopentadiene in the production of chlordane.

Wastewater treatment sludges generated in the production of creosote.

{T}

(T)

(T}

(T)

(E)

(T)

(T}

(T)

(T)

(T)

(T)

{T}

SS-7039 (November 2014) 6 RDA 1693

K036

K037

K038

K039

K040

K041

K042

K043

K097

K098

K099

K123

K124

K125

K126

K131

K132

Explosives:

K044

K045

K046

K047

Petroleum refining:

K048

K049

KOSO

K051

Still bottoms from toluene reclamation distillation in the production of disulfoton.

Wastewater treatment sludges from the production of disulfoton.

Wastewater from the washing and stripping of phorate production.

Filter cake from the filtration of diethylphosphorodithioic acid in the production of phorate.

Wastewater treatment sludge from the production of phorate.

Wastewater treatment sludge from the production of toxaphene.

Heavy ends or distillation residues from the distillation of tetrachlorobenzene in the production of 2,4,5-T.

2,6-Dichlorophenol waste from the production of 2,4-D.

Vacuum stripper discharge from the chlordane chlorinator in the production of chlordane.

Untreated process wastewater from the production of toxaphene.

Untreated wastewater from the production of 2,4-D.

Process wastewater (including supernates, filtrates, and washwaters) from the production of ethylenebisdithiocarbamic acid and its salt.

Reactor vent scrubber water from the production of ethylenebisdithiocarbamic acid and its salts.

Filtration, evaporation, and centrifugation solids from the production of ethylenebisdithiocarbamic acid and its salts.

Baghouse dust and floor sweepings in milling and packaging operations from the production or formulation of ethylenebisdithiocarbamic acid and its salts.

Wastewater from the reactor and spent sulfuric acid from the acid dryer from the production of methyl bromide.

Spent absorbent and wastewater separator solids from the production of methyl bromide.

Wastewater treatment sludges from the manufacturing and processing of explosives.

Spent carbon from the treatment of wastewater containing explosives.

Wastewater treatment sludges from the manufacturing, formulation and loading of lead-based initiating compounds.

Pink/red water from TNT operations.

Dissolved air flotation (OAF) float from the petroleum refining industry.

Slop oil emulsion solids from the petroleum refining industry.

Heat exchanger bundle cleaning sludge from the petroleum refining industry.

API separator sludge from the petroleum refining industry.

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(T)

(C, T)

(T)

(T)

(C,T)

(T)

(R)

(R)

(T)

(R)

(T)

(T)

(T)

K052 Tank bottoms (leaded) from the petroleum refining industry.

(T)

(T)

RDA 1693 SS-7039 (November 2014) 7

K169

K170

K171

K172

Iron and steel:

K061

K062

Primary aluminum:

K088

Secondary lead:

K069

K100

Veterinary pharmaceuticals:

K084

K101

K102

Ink formulation:

Crude oil storage tank sediment from petroleum refining operations.

Clarified slurry oil tank sediment and/or in-line filter/separation solids from petroleum refining operations.

Spent Hydrotreating catalyst from petroleum refining operations, including guard beds used to desulfurize feeds to other catalytic reactors (this listing does not include inert support media).

Spent Hydrorefining catalyst from petroleum refining operations, including guard beds used to desulfurize feeds to other catalytic reactors (this listing does not include inert support media).

Emission control dust/sludge from the primary production of steel in electric furnaces.

Spent pickle liquor generated by steel finishing operations of facilities within the iron and steel industry (SIC Codes 331 and 332).

Spent potliners from primary aluminum reduction.

Emission control dust/sludge from secondary lead smelting. (Note: This listing is stayed administratively for sludge generated from secondary acid scrubber systems. The stay will remain in effect until further administrative action is taken. If EPA takes further action effecting this stay, EPA will publish a notice of the action in the Federal Register).

Waste leaching solution from acid leaching of emission control dust/sludge from secondary lead smelting.

Wastewater treatment sludges generated during the production of veterinary pharmaceuticals from arsenic or organo-arsenic compounds.

Distillation tar residues from the distillation of aniline-based compounds in the production of veterinary pharmaceuticals from arsenic or organo-arsenic compounds .

Residue from the use of activated carbon for decolorization in the production of veterinary pharmaceuticals from arsenic or organoarsenic compounds.

(T)

(T)

(1,T)

(l,T)

(T)

(C,T)

(T)

(T)

(T)

(T)

(T)

(T)

SS-7039 (November 2014) 8 RDA 1693

K086

Coking:

K060

K087

K141

K142

K143

K144

K145

K147

K148

Solvent washes and sludges, caustic washes and sludges, or water washes and sludges from cleaning tubs and equipment used in the formulation of ink from pigments, driers, soaps, and stabilizers containing chromium and lead.

Ammonia still lime sludge from coking operations.

Decanter tank tar sludge from coking operations.

Process residues from the recovery of coal tar, including, but not limited to, collecting sump residues from the production of coke from coal or the recovery of coke by-products produced from coal. This listing does not include K087 (decanter tank tar sludges from coking operations).

Tar storage tank residues from the production of coke from coal or from the recovery of coke by-products produced from coal.

Process residues from the recovery of light oil, including, but not limited to, those generated in stills, decanters, and wash oil recovery units from the recovery of coke by-products produced from coal.

Wastewater sump residues from light oil refining, including, but not limited to, intercepting or contamination sump sludges from the recovery of coke by-products produced from coal.

Residues from naphthalene collection and recovery operations from the recovery of coke by-products produced from coal.

Tar storage tank residues from coal tar refining.

Residues from coal tar distillation, including but not limited to, still bottoms.

{T)

(T)

{T)

{T)

(T)

{T)

(T)

(T)

(T)

(T)


Part 6 of subparagraph (d) of paragraph (4) of Rule 0400-12-01-.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following:

Hazardous Waste No.

U394

U001

U034

6. The commercial chemical products, manufacturing chemical intermediates, or offspecification commercial chemical products referred to in parts 1 through 4 of this subparagraph, are identified as toxic wastes (T), unless otherwise designated and are subject to the small quantity generator exclusion defined in parts ( 1 )( e) 1 and 7 of this rule.

(Comment: For the convenience of the regulated community, the primary hazardous properties of these materials have been indicated by the letters T (Toxicity), R (Reactivity), I {lgnitability) and C (Corrosivity) . Absence of a letter indicates that the compound is only listed for toxicity.)

These wastes and their corresponding Hazardous Waste Codes are:

Chemical Substance Abstracts No.

30558-43-1 A2213.

75-07-0 Acetaldehyde (I)

75-87-6 Acetaldehyde, trichloro-

SS-7039 (November 2014) 9 RDA 1693

U187 62-44-2

U005 53-96-3

U240 194-75-7

U112 141 -78-6

U144 301 -04-2

U214 563-68-8

see F027 93-76-5

U002 67-64-1

U003 75-05-8

U004 98-86-2

U005 53-96-3

U006 75-36-5

U007 79-06-1

U008 79-10-7

U009 107-13-1

U011 61-82-5

U012 62-53-3

U136 75-60-5

U014 492-80-8

U015 115-02-6

U010 50-07-7

U280 101 -27-9

U278 22781-23-3

U364 22961-82-6

U271 17804-35-2

U157 56-49-5

U016 225-51-4

U017 98-87-3

U192 23950-58-5

U018 56-55-3

U094 57-97-6

U012 62-53-3

U014 492-80-8

U049 3165-93-3

U093 60-11-7

U328 95-53-4


Acetamide, N-(4-ethoxyphenyl)

Acetamide, N-9H-fluoren-2-yl-

Acetic acid, (2,4-dichlorophenoxy)-, salts & esters

Acetic acid, ethyl ester (1)

Acetic acid, lead(2+) salt

Acetic acid, thallium(1+) salt

Acetic acid, (2,4,5-trichlorophenoxy)

Acetone (I)

Acetonitrile (1,T)

Acetophenone

2-Acetylaminofluorene

Acetyl chloride (C,R,T)

Acrylamide

Acrylic acid (I)

Acrylonitrile

Amitrole

Aniline (1,T)

Arsinic acid, dimethyl

Auramine

Azaserine

Azirino[2' ,3':3,4]pyrrolo[ 1,2-a ]indole-4, 7-dione, 6-amino-8-[[ ( aminocarbonyl)oxy]methyl]-1, 1 a,2,8,8a,8b-hexahydro-8a-methoxy-5-methyl-, [1 aS-(1 aalpha, 8beta,8aalpha,8balpha)]-

Barban.

Bendiocarb.

Bendiocarb phenol.

Benomyl.

BenzLi]aceanthrylene, 1,2-dihydro-3-methyl-

Benz[c]acridine

Benzal chloride

Benzamide, 3,5-dichloro-N-(1, 1-dimethyl-2-propynyl)-

Benz[ a ]anthracene

Benz[a]anthracene, 7, 12-dimethyl-

Benzenamine (l,T)

Benzenamine, 4,4'-carbonimidoylbis[N,N-dimethyl-

Benzenamine, 4-chloro-2-methyl-, hydrochloride

Benzenamine, N,N-dimethyl-4-(phenylazo)-

Benzenamine, 2-methyl-

10 RDA 1693

U353 106-49-0 Benzenamine, 4-methyl-

U158 101-14-4 Benzenamine, 4,4'-methylenebis[2-chloro-

U222 636-21-5 Benzenamine, 2-methyl-, hydrochloride

U181 99-55-8 Benzenamine, 2-methyl-5-nitro-

U019 71-43-2 Benzene (l,T)

U038 510-15-6 Benzeneacetic acid, 4-chloro-alpha-(4-chlorophenyl)-alpha-hydroxy-, ethyl ester

U030 101-55-3 Benzene, 1-bromo-4-phenoxy-

U035 305-03-3 Benzenebutanoic acid, 4-[bis(2-chloroethyl)amino]-

U037 108-90-7 Benzene, chloro-

U221 25376-45-8 Benzenediamine, ar-methyl-

U028 117-81-7 1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) ester

U069 84-74-2 1,2-Benzenedicarboxylic acid, dibutyl ester

U088 84-66-2 1,2-Benzenedicarboxylic acid, diethyl ester

U102 131-11-3 1,2-Benzenedicarboxylic acid, dimethyl ester

U107 117-84-0 1,2-Benzenedicarboxylic acid, dioctyl ester




U060 72-54-8 Benzene, 1, 1 '-(2,2-dichloroethylidene)bis[4-chloro-

U017 98-87-3 Benzene, (dichloromethyl)-

U223 26471-62-5 Benzene, 1,3-diisocyanatomethyl- (R,T)

U239 1330-20-7 Benzene, dimethyl- (I)

U201 108-46-3 1,3-Benzenediol

U127 118-74-1 Benzene, hexachloro-

U056 110-82-7 Benzene, hexahydro- (I)

U220 108-88-3 Benzene, methyl-



U055 98-82-8 Benzene, (1-methylethyl)- (I)

U169 98-95-3 Benzene, nitro-

U183 608-93-5 Benzene, pentachloro-

U185 82-68-8 Benzene, pentachloronitro-

U020 98-09-9 Benzenesulfonic acid chloride (C,R)

U020 98-09-9 Benzenesulfonyl chloride (C,R)

U207 95-94-3 Benzene, 1,2,4,5-tetrachloro-

U061 50-29-3 Benzene, 1, 1 '-(2,2,2-trichloroethylidene)bis[4-chloro-

U247 72-43-5 Benzene, 1, 1 '-(2,2,2-trichloroethylidene)bis[4- methoxy-

SS-7039 (November 2014) 11 RDA 1693

U023

U234

U021

U278

U364

U203

U141

U090

U367

U064

U248

U022

U197

U023

U085

U021

U073

U091

U095

U225

U030

U128

U172

U031

U159

U160

U053

U074

U143

U031

U136

U032

U372

U271

U280

98-07-7

99-35-4

92-87-5

22781 -23-3

22961 -82-6

94-59-7

120-58-1

94-58-6

1563-38-8

189-55-9

181 -81 -2

50-32-8

106-51-4

98-07-7

1464-53-5

92-87-5

91 -94-1

119-90-4

119-93-7

75-25-2

101-55-3

87-68-3

924-16-3

71-36-3

78-93-3

1338-23-4

4170-30-3

764-41-0

303-34-4

Benzene, (trichloromethyl)

Benzene, 1,3,5-trinitro

Benzidine

1,3-Benzodioxol-4-ol, 2,2-dimethyl-, methyl carbamate.

1,3-Benzodioxol-4-ol, 2,2-dimethyl-,

1,3-Benzodioxole, 5-(2-propenyl)-

1,3-Benzodioxole, 5-( 1-propenyl)-

1,3-Benzodioxole, 5-propyl-

7-Benzofuranol, 2 ,3-dihydro-2,2-dimethyl

Benzo[rst]pentaphene

2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-oxo-1-phenylbutyl)-, & salts, when present at concentrations of 0.3% or less

Benzo[a]pyrene

p-Benzoquinone

Benzotrichloride (C,R,T)

2,2'-Bioxirane

[1, 1 '-Biphenyl]-4,4'-diamine

[1 , 1 '-Biphenyl]-4,4'-diamine, 3,3'-dichloro

[1, 1 '-Biphenyl]-4,4'-diamine, 3,3'-dimethoxy

[1 , 1 '-Biphenyl]-4,4'-diamine, 3,3'-dimethyl

Bromoform

4-Bromophenyl phenyl ether

1,3-Butadiene, 1, 1,2,3,4,4-hexachloro-

1-Butanamine, N-butyl-N-nitroso-

1-Butanol (I)

2-Butanone (l,T)

2-Butanone peroxide (R,T)

2-Butenal

2-Butene, 1,4-dichloro- (I,T)

2-Butenoic acid, 2-methyl-, 7-[[2,3-dihydroxy- 2-(1 -methoxyethyl)-3-methyl-1-oxobutoxy]methyl]- 2,3,5,7a-tetrahydro-1 H-pyrrolizin-1 -yl ester, [1 S-[1 alpha(Z),7(2S*,3R*),7aalpha]]-

71 -36-3 n-Butyl alcohol (I)

75-60-5 Cacodylic acid

13765-19-0 Calcium chromate

10605-21 -7 Carbamic acid, 1 H-benzimidazol-2-yl, methyl ester.

17804-35-2 Carbamic acid, [1 ·[(butylamino)carbonyl]-1 H-benzimidazol-2- yl]-, methyl ester.

101 -27 -9 Carbamic acid, (3-chlorophenyl)-, 4-chloro-2-butynyl ester.

SS-7039 (November 2014) 12 RDA 1693

U238 51-79-6 Carbamic acid, ethyl ester

U178 615-53-2 Carbamic acid, methylnitroso-, ethyl ester

U373 122-42-9 Carbamic acid, phenyl-, 1-methylethyl ester.

U409 23564-05-8 Carbamic acid, [1,2-phenylenebis (iminocarbonothioyl)]bis-, dimethyl ester.

U097 79-44-7 Carbamic chloride, dimethyl-

U114 1111 -54-6 Carbamodithioic acid, 1,2-ethanediylbis-, salts & esters

U062 2303-16-4 Carbamothioic acid, bis(1 -methylethyl)-, S-(2,3-dichloro-2-propenyl) ester

U389 2303-17-5 Carbamothioic acid, bis( 1-methylethyl)-, S-(2,3,3-trichloro-2-propenyl) ester.

U387 52888-80-9 Carbamothioic acid, dipropyl-, S-(phenylmethyl) ester.

U279 63-25-2 Carbary!.

U372 10605-21 -7 Carbendazim.

U367 1563-38-8 Carbofuran phenol.

U215 6533-73-9 Carbonic acid, dithallium(1+) salt

U033 353-50-4 Carbonic difluoride

U156 79-22-1 Carbonochloridic acid, methyl ester (l,T)

U033 353-50-4 Carbon oxyfluoride (R,T)

U211 56-23-5 Carbon tetrachloride

U034 75-87-6 Chloral

U035 305-03-3 Chlorambucil

U036 57-74-9 Chlordane, alpha & gamma isomers

U026 494-03-1 Chlornaphazin

U037 108-90-7 Chlorobenzene

U038 510-15-6 Chlorobenzilate

U039 59-50-7 p-Chloro-m-cresol

U042 110-75-8 2-Chloroethyl vinyl ether

U044 67-66-3 Chloroform

U046 107-30-2 Chloromethyl methyl ether

U047 91 -58-7 beta-Chloronaphthalene

U048 95-57-8 o-Chlorophenol

U049 3165-93-3 4-Chloro-o-toluidine, hydrochloride

U032 13765-19-0 Chromic acid H2CrQ4, calcium salt

U050 218-01 -9 Chrysene

U051 Creosote

U052 1319-77-3 Cresol (Cresylic acid)

U053 4170-30-3 Crotonaldehyde

U055 98-82-8 Cumene (I)

U246 506-68-3 Cyanogen bromide (CN)Br

SS-7039 (November 2014) 13 RDA 1693

U197 106-51-4 2,5-Cyclohexadiene-1 .4-dione

U056 110-82-7 Cyclohexane (I)

U129 58-89-9 Cyclohexane, 1,2,3.4,5,6-hexachloro-, (1 alpha,2alpha,3beta.4alpha,5alpha,6beta)-

U057 108-94-1 Cyclohexanone (I)

U130 77-47-4 1,3-Cyclopentadiene, 1,2,3.4,5,5-hexachloro-

U058 50-18-0 Cyclophosphamide

U240 194-75-7 2.4-D, salts & esters

U059 20830-81-3 Daunomycin

U060 72-54-8 DOD

U061 50-29-3 DDT

U062 2303-16-4 Diallate

U063 53-70-3 Dibenz[ a,h ]anthracene

U064 189-55-9 Dibenzo[a,i]pyrene

U066 96-12-8 1,2-Dibromo-3-chloropropane

U069 84-74-2 Dibutyl phthalate

U070 95-50-1 o-Dichlorobenzene

U071 541-73-1 m-Dichlorobenzene

U072 106-46-7 p-Dichlorobenzene

U073 91-94-1 3,3'-Dichlorobenzidine

U074 764-41-0 1,4-Dichloro-2-butene (I.T)

U075 75-71-8 Dichlorodifluoromethane

U078 75-35-4 1, 1-Dichloroethylene

U079 156-60-5 1,2-Dichloroethylene

U025 111-44-4 Dichloroethyl ether

U027 108-60-1 Dichloroisopropyl ether

U024 111 -91-1 Dichloromethoxy ethane

U081 120-83-2 2.4-Dichlorophenol


U084 542-75-6 1,3-Dichloropropene

U085 1464-53-5 1,2:3,4-Diepoxybutane (I.T)

U395 5952-26-1 Diethylene glycol, dicarbamate.

U108 123-91-1 1,4-Diethyleneoxide

U028 117-81-7 Diethylhexyl phthalate

U086 1615-80-1 N,N'-Diethylhydrazine

U087 3288-58-2 0,0-Diethyl S-methyl dithiophosphate

U088 84-66-2 Diethyl phthalate

U089 56-53-1 Diethylstilbesterol

SS-7039 (November 2014) 14 RDA 1693

U090 94-58-6 Dihydrosafrole

U091 119-90-4 3,3'-Dimethoxybenzidine

U092 124-40-3 Dimethylamine (I)

U093 60-11 -7 p-Dimethylaminoazobenzene

U094 57-97-6 7, 12-Dimethylbenz[a]anthracene

U095 119-93-7 3,3'-Dimethylbenzidine

U096 80-15-9 alpha,alpha-Dimethylbenzylhydroperoxide (R)

U097 79-44-7 Dimethylcarbamoyl chloride

U098 57-14-7 1, 1-Dimethylhydrazine

U099 540-73-8 1,2-Dimethylhydrazine

U101 105-67-9 2,4-Dimethylphenol

U102 131-11 -3 Dimethyl phthalate

U103 77-78-1 Dimethyl sulfate



U107 117-84-0 Di-n-octyl phthalate

U108 123-91 -1 1,4-Dioxane

U109 122-66-7 1,2-Diphenylhydrazine

U110 142-84-7 Dipropylamine (I)

U111 621 -64-7 Di-n-propylnitrosamine

U041 106-89-8 Epichlorohydrin

U001 75-07-0 Ethanal (1)

U174 55-18-5 Ethanamine, N-ethyl-N-nitroso-

U404 121 -44-8 Ethanamine, N,N-diethyl-

U155 91 -80-5 1,2-Ethanediamine, N,N-dimethyl-N'-2-pyridinyl-N'-(2-thienylmethyl)-

U067 106-93-4 Ethane, 1,2-dibromo-

U076 75-34-3 Ethane, 1, 1-dichloro-

U077 107-06-2 Ethane, 1,2-dichloro-

U131 67-72-1 Ethane, hexachloro-

U024 111-91-1 Ethane, 1, 1 '-[methylenebis(oxy)]bis[2-chloro-

U117 60-29-7 Ethane, 1, 1 '-oxybis-(1)

U025 111-44-4 Ethane, 1, 1 '-oxybis[2-chloro-

U184 76-01 -7 Ethane, pentachloro-

U208 630-20-6 Ethane, 1, 1, 1,2-tetrachloro-

U209 79-34-5 Ethane, 1, 1,2,2-tetrachloro-

U218 62-55-5 Ethanethioamide

U226 71-55-6 Ethane, 1, 1, 1-trichloro-

SS-7039 (November 2014) 15 RDA 1693

U227 79-00-5 Ethane, 1, 1,2-trichloro-

U410 59669-26-0 Ethanimidothioic acid, N,N'- [thiobis[(methylimino)carbonyloxy]]bis-, dimethyl ester

U394 30558-43-1 Ethanimidothioic acid, 2-(dimethylamino)-N-hydroxy-2-oxo-, methyl ester.

U359 110-80-5 Ethanol, 2-ethoxy-

U173 1116-54-7 Ethanol, 2,2'-(nitrosoimino)bis-

U395 5952-26-1 Ethanol, 2,2'-oxybis-, dicarbamate.

U004 98-86-2 Ethanone, 1-phenyl-

U043 75-01-4 Ethene, chloro-

U042 110-75-8 Ethene, (2-chloroethoxy)-

U078 75-35-4 Ethene, 1, 1-dichloro-

U079 156-60-5 Ethene, 1,2-dichloro-, (E)-

U210 127-18-4 Ethene, tetrachloro-

U228 79-01-6 Ethene, trichloro-

U112 141-78-6 Ethyl acetate (1)

U113 140-88-5 Ethyl acrylate (I)

U238 51 -79-6 Ethyl carbamate (urethane)

U117 60-29-7 Ethyl ether (I)

U114 1111 -54-6 Ethylenebisdithiocarbamic acid, salts & esters

U067 106-93-4 Ethylene dibromide

U077 107-06-2 Ethylene dichloride

U359 110-80-5 Ethylene glycol monoethyl ether

U115 75-21-8 Ethylene oxide (l,T)

U116 96-45-7 Ethylenethiourea

U076 75-34-3 Ethylidene dichloride

U118 97-63-2 Ethyl methacrylate

U119 62-50-0 Ethyl methanesulfonate

U120 206-44-0 Fluoranthene

U122 50-00-0 Formaldehyde

U123 64-18-6 Formic acid (C,T)

U124 110-00-9 Furan (1)

U125 98-01 -1 2-Furancarboxaldehyde (I)

U147 108-31 -6 2,5-Furandione

U213 109-99-9 Furan, tetrahydro-(1)

U125 98-01-1 Furfural (1)

U124 110-00-9 Furfuran (I)

U206 18883-66-4 Glucopyranose, 2-deoxy-2-(3-methyl-3-nitrosoureido)-, D-

U206 18883-66-4 D-Glucose, 2-deoxy-2-[[(methylnitrosoamino )- carbonyl]amino ]-

SS-7039 (November 2014) 16 RDA 1693

U126 765-34-4 G lycidylaldehyde

U163 70-25-7 Guanidine, N-methyl-N'-nitro-N-nitroso-

U127 118-74-1 Hexachlorobenzene

U128 87-68-3 Hexachlorobutadiene

U130 77-47-4 Hexachlorocyclopentadiene

U131 67-72-1 Hexachloroethane

U132 70-30-4 Hexachlorophene

U243 1888-71 -7 Hexachloropropene

U133 302-01 -2 Hydrazine (R,T)

U086 1615-80-1 Hydrazine, 1,2-diethyl-

U098 57-14-7 Hydrazine, 1, 1-dimethyl-

U099 540-73-8 Hydrazine, 1,2-dimethyl-

U109 122-66-7 Hydrazine, 1,2-diphenyl-

U134 7664-39-3 Hydrofluoric acid (C,T)

U134 7664-39-3 Hydrogen fluoride (C,T)

U135 7783-06-4 Hydrogen sulfide

U135 7783-06-4 Hydrogen sulfide H2S

U096 80-15-9 Hydroperoxide, 1-methyl-1-phenylethyl- (R)

U116 96-45-7 2-lmidazolidinethione

U137 193-39-5 lndeno[1,2,3-cd]pyrene

U190 85-44-9 1,3-lsobenzofurandione

U140 78-83-1 lsobutyl alcohol (l,T)

U141 120-58-1 lsosafrole

U142 143-50-0 Kepone

U143 303-34-4 Lasiocarpine

U144 301-04-2 Lead acetate

U146 1335-32-6 Lead, bis( acetato-O )tetrahydroxytri-

U145 7446-27-7 Lead phosphate

U146 1335-32-6 Lead subacetate

U129 58-89-9 Lindane

U163 70-25-7 MNNG

U147 108-31 -6 Maleic anhydride

U148 123-33-1 Maleic hydrazide

U149 109-77-3 Malononitrile

U150 148-82-3 Melphalan

U151 7439-97-6 Mercury

U152 126-98-7 Methacrylonitrile (I, T)

SS-7039 (November 2014) 17 RDA 1693

U092 124-40-3 Methanamine, N-methyl- (1)

U029 74-83-9 Methane, bromo-

U045 74-87-3 Methane, chloro- (I , T)

U046 107-30-2 Methane, chloromethoxy-

U068 74-95-3 Methane, dibromo-

uo8o 75-09-2 Methane, dichloro-

U075 75-71 -8 Methane, dichlorodifluoro-

U138 74-88-4 Methane, iodo-

U119 62-50-0 Methanesulfonic acid, ethyl ester

U211 56-23-5 Methane, tetrachloro-

U153 74-93-1 Methanethiol (I, T)

U225 75-25-2 Methane, tribromo-

U044 67-66-3 Methane, trichloro-

U121 75-69-4 Methane, trichlorofluoro-

U036 57-74-9 4, 7-Methano-1 H-indene, 1,2,4,5,6, 7,8,8-octachloro-2,3,3a,4, 7, 7a-hexahydro-

U154 67-56-1 Methanol (I)

U155 91-80-5 Methapyrilene

U142 143-50-0 1,3,4-Metheno-2H-cyclobuta[cd]pentalen-2-one, 1, 1 a,3,3a,4,5,5,5a,5b,6-decachlorooctahydro-

U247 72-43-5 Methoxychlor

U154 67-56-1 Methyl alcohol (1)

U029 74-83-9 Methyl bromide

U186 504-60-9 1-Methylbutadiene (I)

U045 74-87-3 Methyl chloride (l,T)

U156 79-22-1 Methyl chlorocarbonate (l,T)

U226 71 -55-6 Methyl chloroform

U157 56-49-5 3-Methylcholanthrene

U158 101-14-4 4,4'-Methylenebis(2-ch loroaniline)

U068 74-95-3 Methylene bromide

uo8o 75-09-2 Methylene chloride

U159 78-93-3 Methyl ethyl ketone (MEK) (l,T)

U160 1338-23-4 Methyl ethyl ketone peroxide (R,T)

U138 74-88-4 Methyl iodide

U161 108-10-1 Methyl isobutyl ketone (I)

U162 80-62-6 Methyl methacrylate (l,T)

U161 108-10-1 4-Methyl-2-pentanone (1)

U164 56-04-2 Methylthiouracil

SS-7039 (November 2014) 18 RDA 1693

U010 50-07-7

U059 20830-81 -3

U167 134-32-7

U168 91-59-8

U026 494-03-1

U165 91-20-3

U047 91-58-7

U166 130-15-4

U236 72-57-1

U279 63-25-2

U166 130-15-4

U167 134-32-7

U168 91-59-8

U217 10102-45-1

U169 98-95-3

U170 100-02-7

U171 79-46-9

U172 924-16-3

U173 1116-54-7

U174 55-18-5

U176 759-73-9

U177 684-93-5

U178 615-53-2

U179 100-75-4

U180 930-55-2

U181 99-55-8

U193 1120-71-4

U058 50-18-0

U115 75-21-8

U126 765-34-4

U041 106-89-8

U182 123-63-7

U183 608-93-5

U184 76-01-7

U185 82-68-8

See F027 87-86-5


Mitomycin C

5, 12-Naphthacenedione, 8-acetyl-10-[(3-amino-2,3,6-trideoxy)-alpha-L-lyxohexopyranosyl)oxy]-7,8,9, 10-tetrahydro-6,8, 11-trihydroxy-1-methoxy-, (8S-cis)-

1-Naphthalenamine

2-Naphthalenamine

Naphthalenamine, N,N'-bis(2-chloroethyl)

Naphthalene

Naphthalene, 2-chloro-

1,4-Naphthalenedione

2,7-Naphthalenedisulfonic acid, 3,3'-[(3,3'- dimethyl[1, 1 '-biphenyl]-4,4'-diyl)bis(azo)bis[5-amino-4-hydroxy]-, tetrasodium salt

1-Naphthalenol, methylcarbamate.

1,4-Naphthoquinone

alpha-Naphthylamine

beta-Naphthylamine

Nitric acid, thallium(1+) salt

Nitrobenzene (l ,T)

p-Nitrophenol

2-Nitropropane (l,T)

N-Nitrosodi-n-butylamine

N-Nitrosodiethanolamine

N-Nitrosodiethylamine

N-Nitroso-N-ethylurea

N-Nitroso-N-methylurea

N-Nitroso-N-methylurethane

N-Nitrosopiperidine

N-Nitrosopyrrolidine

5-Nitro-o-toluidine

1,2-Oxathiolane, 2,2-dioxide

2H-1,3,2-Oxazaphosphorin-2-amine, N,N-bis(2-chloroethyl)tetrahydro-, 2-oxide

Oxirane (l,T)

Oxiranecarboxyaldehyde

Oxirane, (chloromethyl)-

Paraldehyde

Pentachlorobenzene

Pentachloroethane

Pentachloronitrobenzene (PCNB)

Pentachlorophenol

19 RDA 1693

U161 108-10-1 Pentanol, 4-methyl-

U186 504-60-9 1,3-Pentadiene (I)

U187 62-44-2 Phenacetin

U188 108-95-2 Phenol

U048 95-57-8 Phenol, 2-chloro-

U039 59-50-7 Phenol, 4-chloro-3-methyl-



U089 56-53-1 Phenol, 4,4'-(1 ,2-diethyl-1,2-ethenediyl)bis-, (E)-

U101 105-67-9 Phenol, 2,4-dimethyl-

U052 1319-77-3 Phenol, methyl-

U132 70-30-4 Phenol, 2,2'-methylenebis[3,4,6-trichloro-

U411 114-26-1 Phenol, 2-(1-methylethoxy)-, methylcarbamate.

U170 100-02-7 Phenol, 4-nitro-

See F027 87-86-5 Phenol, pentachloro-

See F027 58-90-2 Phenol, 2,3,4,6-tetrachloro-



U150 148-82-3 L-Phenylalanine, 4-[bis(2-chloroethyl)amino]-

U145 7446-27-7 Phosphoric acid, lead(2+) salt (2:3)

U087 3288-58-2 Phosphorodithioic acid, O,O-diethyl S-methyl ester

U189 1314-80-3 Phosphorus sulfide (R)

U190 85-44-9 Phthalic anhydride

U191 109-06-8 2-Picoline

U179 100-75-4 Piperidine, 1-nitroso-

U192 23950-58-5 Pronamide

U194 107-10-8 1-Propanamine (l ,T)

U111 621 -64-7 1-Propanamine, N-nitroso-N-propyl-

U110 142-84-7 1-Propanamine, N-propyl- (1)

U066 96-12-8 Propane, 1,2-dibromo-3-chloro-

U083 78-87-5 Propane, 1,2-dichloro-

U149 109-77-3 Propanedinitrile

U171 79-46-9 Propane, 2-nitro- (l,T)

U027 108-60-1 Propane, 2,2'-oxybis[2-chloro-

U193 1120-71 -4 1,3-Propane sultone

See F027 93-72-1 Propanoic acid, 2-(2,4,5-trichlorophenoxy)-

U235 126-72-7 1-Propanol, 2,3-dibromo-, phosphate (3:1)

SS-7039 (November 2014) 20 RDA 1693

U140 78-83-1 1-Propanol, 2-methyl- (l,T)

U002 67-64-1 2-Propanone (I)

U007 79-06-1 2-Propenamide

U084 542-75-6 1-Propene, 1,3-dichloro-

U243 1888-71-7 1-Propene, 1, 1,2,3,3,3-hexachloro-

U009 107-13-1 2-Propenenitrile

U152 126-98-7 2-Propenenitrile, 2-methyl- (l,T)

U008 79-10-7 2-Propenoic acid (I}

U113 140-88-5 2-Propenoic acid, ethyl ester (I)

U118 97-63-2 2-Propenoic acid, 2-methyl-, ethyl ester

U162 80-62-6 2-Propenoic acid, 2-methyl-, methyl ester (I,T)

U373 122-42-9 Propham.

U411 114-26-1 Propoxur.

U194 107-10-8 n-Propylamine (l,T)

U083 78-87-5 Propylene dichloride

U387 52888-80-9 Prosulfocarb.

U148 123-33-1 3,6-Pyridazinedione, 1,2-dihydro-

U196 110-86-1 Pyridine

U191 109-06-8 Pyridine, 2-methyl-

U237 66-75-1 2,4-(1 H,3H)-Pyrimidinedione, 5-[bis(2- chloroethyl)amino]-

U164 56-04-2 4(1 H)-Pyrimidinone, 2,3-dihydro-6-methyl-2-thioxo-

U180 930-55-2 Pyrrolidine, 1-nitroso-

U200 50-55-5 Reserpine

U201 108-46-3 Resorcinol

U203 94-59-7 Safrole

U204 7783-00-8 Selenious acid

U204 7783-00-8 Selenium dioxide

U205 7488-56-4 Selenium sulfide

U205 7488-56-4 Selenium sulfide SeS2 (R,T)

U015 115-02-6 L-Serine, diazoacetate (ester)

See F027 93-72-1 Silvex (2,4,5-TP)

U206 18883-66-4 Streptozotocin

U103 77-78-1 Sulfuric acid, dimethyl ester

U189 1314-80-3 Sulfur phosphide (R)

See F027 93-76-5 2,4,5-T

U207 95-94-3 1,2,4,5-Tetrachlorobenzene

U208 630-20-6 1, 1, 1,2-Tetrachloroethane

SS-7039 (November 2014) 21 RDA 1693

U209 79.34.5 1, 1,2,2-Tetrachloroethane

U210 127-18-4 Tetrachloroethylene

See F027 58-90-2 2,3,4,6-Tetrachlorophenol

U213 109-99-9 Tetrahydrofuran (I)

U214 563-68-8 Thallium(I) acetate

U215 6533-73-9 Thallium(I) carbonate

U216 7791-12-0 Thallium(I) chloride

U216 7791-12-0 Thallium chloride TICI

U217 10102-45-1 Thallium(I) nitrate

U218 62-55-5 Thioacetamide

U410 59669-26-0 Thiodicarb.

U153 74-93-1 Thiomethanol (l,T)

U244 137-26-8 Thioperoxydicarbonic diamide [(H2N)C(S)]2S2, tetramethyl-

U409 23564-05-8 Thiophanate-methyl.

U219 62-56-6 Thiourea

U244 137-26-8 Thiram

U220 108-88-3 Toluene

U221 25376-45-8 Toluenediamine

U223 26471-62-5 Toluene diisocyanate (R,T)

U328 95.53.4 o-Toluidine

U353 106-49-0 p-Toluidine

U222 636-21-5 o-Toluidine hydrochloride

U389 2303-17-5 Triallate.

U011 61-82-5 1 H-1,2,4-Triazol-3-amine

U226 71-55-6 1, 1, 1-Trichloroethane

U227 79-00-5 1, 1,2-Trichloroethane

U228 79-01-6 Trichloroethylene

U121 75-69-4 Trichloromonofluoromethane

See F027 95.95.4 2,4,5-Trichlorophenol

See F027 88-06-2 2,4,6-Trichlorophenol

U404 121-44-8 Triethylamine.

U234 99.35.4 1,3,5-Trinitrobenzene (R,T)

U182 123-63-7 1,3,5-Trioxane, 2,4,6-trimethyl-

U235 126-72-7 Tris(2,3-dibromopropyl) phosphate

U236 72-57-1 Trypan blue

U237 66-75-1 Uracil mustard

U176 759.73.9 Urea, N-ethyl-N-nitroso-

SS-7039 (November 2014) 22 RDA 1693

U177 684-93-5 Urea, N-methyl-N-nitroso-

U043 75-01 -4 Vinyl chloride

U248 181 -81 -2 Warfarin, & salts, when present at concentrations of 0.3% or less

U239 1330-20-7 Xylene (1)

U200 50-55-5 Yohimban-16-carboxylic acid, 11, 17-dimethoxy-18-[(3,4,5-trimethoxybenzoyl)oxy]-, methyl ester, (3beta, 16beta, 17alpha, 18beta,20alpha)-

U249 1314-84-7 Zinc phosphide Zn3P2, when present at concentrations of 10% or less

FOOTNOTE: 1CAS Number given for parent compound only.

Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq .

Subparagraph (a) of paragraph (6) of Rule 0400-12-01-.02 Identification and Listing of Hazardous Waste is amended by deleting it in its entirety and substituting instead the following:

(a) Comparable/Syngas Fuel Exclusion [40 CFR 261.38]

VVastes that meet the following comparable/syngas fuel requirements are not solid wastes:

1. Comparable fuel specifications

(i) Physical specifications

(I) Heating value. The heating •,ialue must exceed 5,000 BTU/lbs. (11 ,500

(11) Viscosity. The viscosity must not exceed: 50 cs, as fired.

fi" ..... 1)--c ..... o-n .... s .... ti .... tu-e .... n+-t s-p-e-c-if-ic-at .... io .... n-s

Table 1: D Chemical Name

Total Nitrogen as N Total Flalogens as Cl Total Grganic Flalogens as Cl Polychlorinated biphenyls total

[.'\rocolors, total j Cyanide, total Metals;

Antimony, total Arsenic, total Barium, total Beryll ium, total Cadmium, total Chromium, total

-Gooalt


For compounds listed in table 1 to this subparagraph the specification levels and, where non detect is the specification, minimum required detection limits are: (see Table 1 ).

NA 0000 -t-8400 4900 NA +GOO -t-8400 MG NA i-B

1336 36 3 NQ NQ +.4

a-7--+U NQ NQ +.G

7440 36 0 NQ -1--2 7440 38 2 NQ ~ 7440 39 3 NQ 23 7440 41 7 NQ ~

7440 43 9 NQ ~

7440 47 3 NQ ~

7440 48 4 NQ 4-,e

23 RDA 1693

Lead, total -74J9..924 e-7 +8+GG d-1-Manganese 7439 Be a NG ~

- Meroury, total 7439 97 e NG ~

Nickel, total 744Q Q2 Q +00 +MOO w Selenium, total 7782 49 2 NG ~

Silver, total 744Q 22 4 NG ~

Thal lium, total 744Q 28 Q NG ~

Hydrocarbons: Ben:zo[ajanthracene ~ NG ;M.00

Benzene ~ 0000 -1-9600 4400 Ben:zo[bjfluoranthene 2Q§ 99 2 NG ;M.00

Ben:zo[kllluoranthene 2Q7 QB 9 NG ;M.00

Ben:zo[ajpyrene ~ NG ;M.00

Ghrysene 218 Q1 9 NG ;M.00

bliben:zo[a, hjanthracene ~ NG ;M.00

7, 12 rnmethylben:z[aJanthracene e-7-9-7-e NG ;M.00

i;;Iuoranthene 2Qe 44 g NG ;M.00

lndeno(1, 2, 3 cd)pyrene 193 39 5 NG ;M.00

3 Methylcholanthrene ~ NG ;M.00

Naphthalene ~ @)Q +9400 ~ Toluene 1Q8 88 3 e900G +9400 3eQOO

Oxygenates: Acetophenone ~ NG ;M.00

Acrolein 1Q7 Q2 8 NG w ,A,l lyl alcohol 1Q7 1 s e NG ao Bis(2 ethylhexl) phthalate [bli 2 ethylhexyl

phthalateJ 117 81 7 NG ;M.00

Butyl ben:zyl phthalate ~ NG ;M.00

o Gresol [2 Methyl phenoll 9&-48--7 NG ;M.00

m Gresol [3 Methyl phenolJ 1Q8 39 4 NG ;M.00

p Gresol [4 Methyl phenoll 1Q€l 44 5 NG ;M.00

rn n butyl phthalate 84--74-2 NG ;M.00

methyl phthalate ~ NG ;M.00

2, 4 rnmethylphenol 1g5 e7 9 NG ;M.00

rnmethyl phthalate 131 11 3 NG ;M.00

Di n octyl phthalate 117 84 Q NG ;M.00

Endothall 145 73 3 NG -1-QQ

Ethyl methacrylate ~ NG w 2 Ethoxyethanol [Ethylene glycol 11Q 8Q 5 NG -1-QQ

monoethyl etherJ lsobutyl alcohol ~ NG w lsosalrole 12Q 58 1 NG ;M.00

Methyl ethyl ketone [2 ButanoneJ ~ NG w Methyl methacrylate W-62-e NG w 1, 4 Naphthoquinone 13Q 15 4 NG ;M.00

--Pfleool 1Q8 95 2 NG ;M.00

Propargyl alcohol [2 Propyn 1 oil 1 Q7 19 7 NG ao -Salrole 94-W-7 NG ;M.00

Sullonated Organics: Garbon disulfide -7a-1--&-0 NG NG w rnsulloton 298 Q4 4 NG NG ;M.00

Ethyl methanesullonate @-W--0 NG NG ;M.00

Methyl methanesullonate ee-2-7--3 NG NG 24-0Q

Phorate 298 Q2 2 NG NG 24-0Q

1, 3 Propane sultone 112Q 71 4 NG NG -1--00 +etraethyldithiopyrophosphate [SulloteppJ 3e89 24 5 NG NG 24-0Q

Thiophenol [Ben:zenethiolJ 1Q8 98 5 NG NG ao

SS-7039 (November 2014) 24 RDA 1693

0, 0, 0 Triethyl phosphorothioate 126 68 1

Nitro§enatea 0r§anics: Acetonitrile fMethyl cyaniaej ~ Nf} Nf} w 2 Acetylarninofl1:1orene [2 AAF] ~ Nf} Nf} 2400 Acrylonitrile 107 13 1 Nf} Nf} w 4 Arninobiphenyl 92-e-7-4 Nf} Nf} 2400 4 Arninopyriaine 504 24 5 Nf} Nf} 400

---AAilifle ~ Nf} Nf} 2400 Ben2iaine 9U7-a Nf} Nf} 2400 Qiben2[a, jjacriaine 224 42 0 Nf} Nf} 2400 0, 0 Qiethyl 0 pyra2inyl 297 97 2 Nf} Nf} 2400

Phosphorothioate fThiona2in] Qirnethoate 6Q..&1--e Nf} Nf} 2400 p (Qirnethylarnino) a2oben2ene

f 4 airnethyl arninoawbenwne] eG-4-1--7 Nf} Nf} 2400 3,3' Qirnethylben2iaine 119 93 7 Nf} Nf} 2400 u, u Qirnethylphenethylarnine 122 09 8 Nf} Nf} 2400 3, 3' Qirnetho*yben2iaine 119 90 4 Nf} Nf} 400 1, 3 Qinitrobenwne frn Qinitroben2ene] 99-65--0 Nf} Nf} 2400 4, 6 Qinitro o cresol 534 52 1 Nf} Nf} 2400 2, 4 Qinitrophenol ~ Nf} Nf} 2400 2, 4 Qinitrotol1:1ene 121 14 2 Nf} Nf} 2400 2, 6 Qinitrotol1:1ene 606 20 2 Nf} Nf} 2400 rnnoseb [2 sec B1:1tyl 4, 6 ainitrophenol] 88-8e-+ Nf} Nf} 2400 Qiphenylarnine 122 39 4 Nf} Nf} 2400 Ethyl carbarnate f blrethane] a-1--79-e Nf} Nf} 400 Ethylenethiomea (2 lrniaawliainethione) W-4-a-7 Nf} Nf} -t--1-0 Farnph1:1r ~ Nf} Nf} 2400 Methacrylonitrile 126 98 7 Nf} Nf} w Methapyrilene ~ Nf} Nf} 2400 Methornyl -1-e?@-7-7-e Nf} Nf} e7 2 Methyllactonitrile, [Acetone ~ Nf} Nf} 400

cyanohyarin] Methyl parathion 298 00 0 Nf} Nf} 2400 MNNG (~J Metyl N nitroso N' ~ Nf} Nf} -t--1-0

nitro§1:1aniaine) 1 Naphthylarnine, fu Naphthylarnine] 134 32 7 Nf} Nf} 2400 2 Naphthylarnine, f~ Naphthylarnine] 9-1--5-9-8 Nf} Nf} 2400 Nicotine a4-1-1-5 Nf} Nf} 400 4 ~Jitroaniline, fp ~Jitroaniline] 100 01 6 Nf} Nf} 2400 Nitroben2ene ~ Nf} Nf} 2400 p Nitrophenol, fp ~Jitrophenolj 100 02 7 Nf} Nf} 2400 5 Nitro o tol1:1iaine 99-aa-8 Nf} Nf} 2400 N Nitrosoai n b1:1tylarnine 924 16 3 Nf} Nf} 2400 N Nitrosoaiethylarnine ea4U Nf} Nf} 2400 ~J Nitrosoaiphenylarnine, ~ Nf} Nf} 2400

[Qiphenylnitrosarnine] N Nitroso N rnethylethylarnine 10595 95 6 Nf} Nf} 2400 N Nitrosornorpholine ~ Nf} Nf} 2400 N Nitrosophiperiaine 100 75 4 Nf} Nf} 2400 N Nitrosopyrroliaine 930 55 2 Nf} Nf} 2400 2 Nitropropane -7-9-4e-9 Nf} Nf} w Parathion ~ Nf} Nf} 2400 Phenacetin ~ Nf} Nf} 2400 1, 4 Phenylne aiarnine, 106 50 3 Nf} Nf} 2400

fp Phenyleneaiarnine] N Phenylthio1:1rea 103 85 5 Nf} Nf} e7 2 Picoline falpha Picoline] 109 06 8 Nf} Nf} 2400 Propylthioracil , [6 Propyl 2 th io1:1racilj ~ Nf} Nf} 400

SS-7039 (November 2014) 25 RDA 1693

Pyridine 110 86 1 ND ND 2400 Strychnine ~ ND ND -1-00 Thioacetamide eUa--a ND ND fH. Thiolanox 39196 18 4 ND ND -1-00 Thiourea 6Ue-6 ND ND fH. Toluene 2,4 diamine [2,4 Qiaminotoluenej g§-00-+ ND ND fH. Toluene 2, 6 diamine [2, 6 ND fH.

rnaminotoluenej 823 40 5 ND NG fH. o Toluidine ~ ND ND 2400 p Toluidine 106 49 0 ND ND -1-00 1, 3, 5 Trinitrobenzene, ~ ND ND 2400

[sym Trinitobenzenej

Halogenated Organics: Allyl chloride 107 05 1 ND ND Jg

Aramite 140 57 8 ND ND 2400 Benzal chloride [Qichloromethyl benzenej ~ ND ND -1-00 Benzyl chloride 100 44 77 ND ND -1-00 bis(2 Chloroethyl)ether [Qichoroethyl 111 44 4 ND ND 2400

etherj Bromolorm [TribromomethaneJ ~ ND ND Jg

Bromomethane [Methyl bromidej -74-83--9 ND ND Jg

4 Bromophenyl phenyl ether [p Brome 101 55 3 ND ND 2400 diphenyl etherj

Carbon tetrachloride ~ ND ND Jg

Chlordane fH.-74-9 ND NG +4 p Chloroaniline 106 47 8 ND ND 2400 Chlorobenzene 108 90 7 ND ND Jg

Chlorobenzilate 510 15 6 ND ND 2400 p Chloro m cresol W--W--7 ND ND 2400 2 Chloroethyl vinyl ether 110 75 8 ND ND Jg

Chloroform e+-ew ND ND Jg

Chloromethane [Methyl chloridej -74-87-3 ND ND Jg

2 Chloronaphthalene ~ ND ND 2400 [beta Chloronaphthalenej

2 Chlorophenol [o Chlorophenolj ~ ND ND 2400 Chloroprene [2 Chloro 1, 3 butadienej 1126 99 8 ND ND Jg

2, 4 g [2, 4 Qichlorophenoxyacetic acidj 94--75-+ ND ND 7-,0

Qiallate 2303 16 4 ND ND 2400 1, 2 Qibromo 3 chloropropane 00--1-U ND ND Jg

1, 2 Qichlorobenzene [o rnchlorobenzenej ~ ND ND 2400 1, 3 Qichlorobenzene 541 73 1 ND ND 2400

[m Qichlorobenzenej 1, 4 Qichlorobenzene [p rnchloroben;rnnej 106 46 7 ND ND 2400 3, 3' Qichlorobenzidine 9-1--944 ND ND 2400 Qichlorodilluoromethane [C~C 12l -7e-7+-8 ND ND Jg

1, 2 Qichloroethane [Ethylene Elichloridej 107 06 2 ND ND Jg

1, 1 Qichloroethylene [Vinylidene ~ ND ND Jg

chlorideJ rnchloromethoxy ethane [Bis(2 chloro

ethoxy)methanej 111 91 1 ND ND 2400 2,4 Qichlorophenol 120 83 2 ND ND 2400 2, 6 Qichlorophenol 8-7-ee-G ND ND 2400 1, 2 Qich loropropane [Propylene +8-8-7-a ND ND Jg

dichloridej sis 1, 3 Qichloropropylene 10061 01 5 ND ND Jg

trans 1, 3 rnchloropropylene 10061 02 6 ND ND Jg

1,3 Qichloro 2propanol 00--23-4 ND ND w Endosullan I 959 98 8 ND ND +.4 Endosullan II 33213659 ND ND +.4

SS-7039 (November 2014) 26 RDA 1693

-eRGfffi ~ NG NG +.4 EREJFiR alEJeRyEle 7421 9d 4 NG NG +.4 ERElFiR KetoRe 5d494 70 5 NG NG +.4

EpiGRIOFORyElFiR [1 CRIOFO 2, d epo~ pFopaReJ 106 89 8 NG NG dG

-ethyliEleRO EliGRIOFiEle ~ NG NG w [1, 1 QicRIOFOOtRaReJ

2 FlumoacetamiEle 640197 NG NG -1-00 HeptaGRIOF -?e-44-8 NG NG +.4 HeptacRIOF epoxiEle 1024 57 d NG NG u HexacRloml3eRzeRe 118 74 1 NG NG 2400 HexaGRIOFO 1, d 13utaElieRO ~ NG NG 2400

[HexacRloml3utaElieReJ HexacRlomcyclopeRtaElieRe -77---47-4 NG NG 2400 HexaGRIOFOetRaRe e-7-72-1- NG NG 2400 HexaGRIOFOpRORO +G-W-4 NG NG WOOG HexacRlompmpeRe 1888717 NG NG 2400

[HexaGRIOFOpropyleReJ --ffiOOAA 465 7d 6 NG NG 2400

KepoRO [CRIOF90GOROJ 14d 50 0 NG NG 4700 biRElaRO [gamma BHCJ [gamma HexacRlorn a8-89-9 NG NG +.4

cycloRexaReJ MetRyleRe GRloFiEle [QicRloFometRaReJ +&-09-2 NG NG w 4, 4' MetRyleRO 13is(2 GRIOFOaRiliRe) 101 14 4 NG NG -1-00 MetRyl ioEliEle [loElometRaReJ ~ NG NG w PeRtaGRIOFOl3CRZORO 608 9d 5 NG NG 2400 PeRtaGRIOFOOtRaRO -76-04-7 NG NG w PeRtaGRIOFORitrnl3eRZORO [PCNBJ ~ NG NG 2400

[QuiRtol3eRZOROJ [QuiRtOZOReJ PeRtaGRIOFOpROROI gJ...86-e NG NG 2400 PFORamiEle 2d950 58 5 NG NG 2400 Sil¥0l< [2, 4, 5 +FiGRIOFOpROROXypFopioRiG aciEll ~ NG NG +.-0 2, d, 7, 8 +etFaGRIOFOElil3eRZO p ElioxiR 1746016 NG NG dG

[2, d, 7, 8 +CQQJ 1, 2, 4, 5 +OtFaGRIOFOl3CRZORO 9a-94-3 NG NG 2400 1, 1, 2, 2 +etFaGRIOFOetRaRe -79-34-a NG NG w +O!FaGRIOFOO!RyleRO [POFGRIOFOO!RyleReJ 127 18 4 NG NG w 2, d, 4, 6 +O!FaGRIOFOpReRol ~ NG NG 2400 1, 2, 4 +FiGRIOFOl3CRZORO 120 82 1 NG NG 2400 1,1,1 +FiGRIOFOO!RaRO [Me!Ryl GRIOFOIOFmJ -7--1---M-e NG NG w 1,1,2 +FiGRIOFOO!RaRO [ViRyl tFiGRIOFiEleJ -79-00-e NG NG w

+FiGRlornetRyleRe -79--0-1---e NG NG w +FiGRlornfluoFOmetRaRO [+FiGRIOFOmORO -?a-69-4 NG NG w

FluoFOme!RaReJ 2, 4, 5 +FiGRIOFOpReRol ~ NG NG 2400 2, 4, 6 +FiGRIOFOpROROI ~ NG NG 2400 1, 2, d +FiGRIOFOpFOpaRe 96--1-8-4 NG NG w ViRyl CRIOFiEle -?e-G-1--4 NG NG w

Nete&:-

NA Net Applicaele. ND Nendetect.

~2a eF individl:lal t:iale§enated 9F€Janics listed eelew.

a Aesence ef PCBs can alse ee demenstrnted ey l:lsin§ appmpFiate scrnenin§ mett:leds, e.€J., imml:lneassay kit feF PCB in eils (Mett:led 4020) eF celeFimetFic analysis foF PCBs in eil (Mett:led 9079).

SS-7039 (November 2014) 27 RDA 1693

1a Some minimum required detection limits are above the total halogen limit of 540 ppm. The detection limits reflect what was achieved during EPA testing and analysis and also analytical complexity associated with measuring all halogen compounds on Appendix VIII at low levels . EPA recognizes that in practice the presence of these compounds will be functionally limited by the molecular weight and the total halogen limit of 540 ppm.

2.

3.

Synthesis gas fuel specifications


(i)

(ii)

(iii)

(iv)

(") •

Have a minimum Btu value of 100 Btu/scf (British thermal unit per standard cubic

Contain less than 1 ppmv of total halogen;

Contain less than 300 ppmv of total nitrogen other than diatomic nitrogen-fN:.~

Contain less than 200 ppmv of hydrogen sulfide; and

Contain less than 1 ppmv of each hazardous constituent in the target list of Appendix VIII constituents of this rule .

Implementation

1/Vaste that meets the comparable or syngas fuel specifications provided by parts 1 or 2 of this subparagraph (these constituent levels must be achieved by the comparable fuel when generated, or as a result of treatment or blending, as provided in subparts 3(iii) or (iv) of this subparagraph) is excluded from the definition of solid 'Naste provided that the fellowing requirements are met:

(i) Notices

For purposes of this subparagraph, the person claiming and qualifying for the exclusion is called the comparable/syngas fuel generator and the person burning the comparable/syngas fuel is called the comparable/syngas burner. The person who generates the comparable fuel or syngas fuel must claim and certify to the exclusion.

(I) Commissioner, Department of Environment and Conservation (Director, Division of Solid Waste Management and Director of Division of Air Pollution Control) .

I.

II.

Ill .

The generator must submit a one time notice to the Commissioner and Directors of Solid VVaste Management and Air Pollution Control, in whose jurisdiction the exclusion is being claimed and where the comparable/syngas fuel will be burned, certifying compliance with the conditions of the exclusion and providing documentation as required by subitem 3(i)(l)III of this &Ubparagraph;

If the generator is a company that generates comparable/syngas fuel at more than one facility, the generator shall specify at which sites the comparable/syngas fuel will be generated;

A comparable/syngas fuel generator's notification to the Commissioner must contain the following items:

[\ Ii.

B.

The name, address, and Installation Identification number of the person/facility claim ing the exclusion ;

The applicable Hazardous Waste Codes for the

SS-7039 (November 2014) 28 RDA 1693

(ii)


(11)

Burning

C.

D.

hazardous waste;

Name and address of the units, meeting the requirements of subpart 3(ii) of this subparagraph, that will burn the comparable/syngas fuel ; and

The following statement is signed and submitted by the person claiming the mwlusion or his authorized representative:

"Under penalty of criminal and civil prosecution for making or submitting false statements, representations, or omissions, I certify tAat the requirements of Rule 0400 12 01 .02(6)(a) have been met for all waste identified in this notification. Copies of the records and information required at Rule 0400 12 01 .02(6)(a)3(x)

, are available at the comparable/syngas fuel generator's facility. Based on my inquiry of the individuals immediately responsible for obtaining the information, the information is, to the best of my knowledge and belief, true, accurate , and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment."

Public notice

Prior to burning an excluded comparable/syngas fuel, the burner must publish in a major newspaper of general circulation local to the site where the fuel will be burned , a notice entitled "Notification of Burning a Comparable/Syngas Fuel Excluded Under the Resource Conservation and Recovery /\ct" containing the following information:

I.

II.

Ill.

IH .. \I

IF ,

Name, address, and Installation Identification number of the generating facility;

Name and address of the unit(s) that will burn the comparable/syngas fuel;

/\ brief, general description of the manufacturing, treatment, or other process generating the comparable/syngas fuel ;

/\n estimate of the average and maximum monthly and annual quantity of the waste claimed to be excluded; and

Name and mailing address of the Commissioner to whom the claim was submitted.

The comparable/syngas fuel exclusion for fuels meeting the requirements of parts 1 or 2 of this subparagraph and subpart (i) of th is part applies only if the fuel is burned in the following units that also shall be subject to Federal/State/local air emission requirements , including all applicab le Clean /\ir /\ct, Maximum Achievable Control Technologies (C/\A M/\CT) requirements:

(I)

(11)

Industrial furnaces as defined in Rule 0400 12 01 .01 (2)(a);

Boi lers, as defined in Rule 04 00 12 01 .01 (2)(a), that are further defined as follows :

29 RDA 1693

(iii)

(iv)


I.

II.

Industrial boilers located on the site of a facility engaged in a manufacturing process where substances are trans-fermea--iR-te new products, including the component parts of products, by mechanical or chemical processes; or

Utility boilers used to produce electric power, steam-, heated or cooled air, or other gases or fluids for sale;

ft4-4---FHl-i-:la1-czo1a r1tdKc10>HUt;-S-v'lv-./afts~te-i n-ttcCrr1i n-tte-tt-ro-at~OfHrs-s UHJb~jtc!<eCb!t,-ltt10~rt1eti-gHlU lnc:1a-ttti OHlnl+-tlUttntl-det,tJr--1RF"itl-U llt,le-;0,1441t01b0f-1t--.2~ 01 .05(15) or Rule 0400 12 01 .06(15) or applicable CA/\ MACT standards .

(IV) Gas turbines used to produce electric power, steam, heated or cooled air, or other gases or fluids for sale .

Blending to meet the viscosity specification

A hazardous waste blended to meet the viscosity specification shall:

(I)

(11)

(111)

As generated and prior to any blending, manipulation, or processing meet the constituent and heating value specifications of item 1 (i)(I) and subpart 1 (ii) of this subparagraph;

Be blended at a facility that is subject to the applicable requirements of Rules 0400 12 01 .05 and .06, or Rule 0400 12 01 .03(4)(e); and

Not violate the dilution prohibition of subpart 3(vi) of this subparagraph .

Treatment to meet the comparable fuel exclusion specifications

(I)

(11)

A hazardous waste may be treated to meet the exclusion specifications of subparts 1 (i) and (ii) of this subparagraph provided the treatment:

I.

II.

Ill.

Destroys or removes the constituent listed in the specification or raises the heating value by removing or destroying hazardous constituents or materials;

Is performed at a facil ity that is subject to the applicable requirements of Rules 04 00 12 01 .05 and .06, or Rule 04 00 12 01 .03(4)(e); and

Does not violate the dilution prohibition of subpart 3(vi) of this subparagraph.

Residuals resulting from the treatment of a hazardous waste listed in paragraph (4) of this rule to generate a comparable fuel remain a hazardous waste .

Generation of a syngas fuel

fl+-- A syngas fuel can be generated from the processing of hazardous wastes to meet the exclusion specifications of part 2 of this subparagraph provided the processing :

I.

II.

Destroys or removes the constituent listed in the specification or raises the heating value by removing or destroying constituents or materials ;

Is performed at a facility that is subject to the applicable

30 RDA 1693

(vi)

(vii)


(11)

Ill.

requirements of Rules 0400 12 01 .05 and .06, or Rule 0400 12 01 .03(4 )(e); or is an exempt recycling unit pursuant to part (1 )(f)3 of this rule; and

Does not violate the dilution prohibition of subpart 3(vi) of this subparagraph.

Residuals resulting from the treatment of a hazardous waste listed in paragraph (4) of this rule to generate a syngas fuel remain a hazardous wast&.

Dilution prohibition for comparable and syngas fuels

No generator, transporter, handler, or owner or operator of a treatment, storage, or disposal facility shall in any way dilute a hazardous waste to meet the exclusion specifications of item 1 (i)(I), subpart 1 (ii) or part 2 of this subparagraph.

Vl/aste analysis plans

The generator of a comparable/syngas fuel shall develop and follow a written waste analysis plan which describes the procedures for sampling and analysis of the hazardous waste to be excluded. The plan shall be followed and retained at the facility excluding the waste.

(I)

(11)

At a minimum, the plan must specify

I.

II.

Ill.

IV.

\I v.

The parameters for which each hazardous waste will be analyzed and the rationale for the selection of those parameters;

The test methods which will be used to test for these parameters;

The sampling method which will be used to obtain a representative sample of the waste to be analyzed;

The frequency with which the initial analysis of the waste will be reviewed or repeated to ensure that the analysis is accurate and up to date; and

If process knowledge is used in the •.vaste determination, any information prepared by the generator in making such determination.

The waste analysis plan shall also contain records of the following:

I.

II .

Il l.

IV.

\I ..

The dates and times waste samples 'Nero obtained, and the dates the samples were analyzed;

The names and qualifications of the person(s) who obtained the samples;

A description of the temporal and spatial locations of the samples;

The name and address of the laboratory facility at which analyses of the samples were performed;

A description of the analytical methods used, including any clean up and sample preparation methods;

31 RDA 1693

(viii)


(111)

VI.

VII.

VIII .

/\II quantitation limits achieved and all other quality coA-tfffi results for the analysis (including method blanks, duplicate analyses, matrix spikes, etc .), laboratory quality assurance data, and description of any deviations from analytical methods written in the plan or from any other activity written in the plan which occurred;

/\II laboratory results demonstrating that the exclusion specifications have been met for the waste; and

/\II laboratory documentation that support the analytical results, unless a contract between the claimant and the laboratory provides for the documentation to be maintained by the laboratory for the period specified in subpart 3(xi) of this subparagraph and also provides for the availability of the documentation to the claimant upon request.

Syngas fuel generators shall submit for approval, prior to performing sampling, analysis, or any management of a syngas fuel as an excluded waste, a waste analysis plan containing the elements of item 3(vii)(I) of this subparagraph to the appropriate regulatory authority. The approval of waste analysis plans must be stated in writing and received by the facility prior to sampling and analysis to demonstrate the exclusion of a syngas. The approval of the waste analysis plan may contain such provisions and conditions as the regulatory authority deems appropriate.

Comparable fuel sampling and analysis

(I)

(II)

General

For each waste for which an exclusion is claimed, the generator of the hazardous waste must test for all the constituents on appendix VIII to this rule, except those that the generator determines, based on testing or knowledge, should not be present in the waste. The generator is required to document the basis of each determination that a constituent should not be present. The generator may not determine that any of the follmving categories of constituents should not be present:

I.

II.

Ill.

IV.

/\ constituent that triggered the toxicity characteristic for the waste constituents that were the basis of the listing of the waste stream, or constituents for which there is a treatment standard for the waste code in Rule 04 00 12 01 .10(3)(a);

/\ constituent detected in previous analysis of the waste;

Constituents introduced into the process that generates the waste; or

Constituents that are byproducts or side reactions to the process that generates the waste.

(Note to subpart 3(viii) : /\ny claim under this subparagraph must be valid and accurate for all hazardous constituents; a determination not to test for a hazardous constituent will not sh ield a generator from liabi lity should that constituent later be found in the waste above the exclusion specifications.)

For each waste for which the exclusion is claimed where the generator of the comparable/syngas fuel is not the original generator of the hazardous waste, the generator of the comparable/syngas fuel may not use process

32 RDA 1693

(ix)

(x)


(111)

knowledge pursuant to item 3(viii)(I) of this subparagraph and must test to determine that all of the constituent specifications of subpart 1 (ii) and ~-ef--this subparagraph have been met.

The comparable/synga-s-fuel generator may use any reliable analytical method to demonstrate that no constituent of concern is present at concentrations above the specification levels. It is the responsibility cif the generator to ensure that the sampling and analysis are unbiased, precise, and representative of the waste. For the waste to be eligible for exclusion, a generator must demonstrate that:

I.

II.

Each constituent of concern is not present in the waste above the specification le1w<el at the 95% upper confidence limit around the mean; and

Tho analysis could have detected the presence of the constituent at or below the specification level at the 95% upper confidence limit around the mean.

(IV) Nothing in this item preempts, overrides or otherwise negates the provision in-Rule 0400 12 01 .03(1 )(b), which requires any person who generates a solid waste to determine if that waste is a hazardous waste.

(V) In an enforcement action, the burden of proof to establish conformance with the exclusion specification shall be on the generator claiming the exclusion .

(VI) The generator must conduct sampling and analysis in accordance with their waste analysis plan developed under subpart 3(vii) of this subparagraph.

(VII) Syngas fuel and comparable fuel that has not been blended in order to meet the kinematic viscosity specifications shall be analyzed-as generated.

fV-111) If a comparable fuel is blended in order to meet the kinematic viscosity specifications, the generator shall:

(IX)

I.

II.

Analyze the fuel as generated to ensure that it meets the constituent and heating value specifications; and

After blending, analyze the fuel again to ensure that the blended fuel continues to meet all comparable/syngas fuel specifications.

Excluded comparable/syngas fuel must be re tested, at a minimum, annually and must be retested after a process change that could change the chemical or physical properties of the waste .

Speculative accumulation

Any persons handling a comparable/syngas fue l are subject to the speculative accumulation test under subpart (1 )(b)3(iv) of this rule.

Records

The generator must maintain records of the following information on site :

(I) All information required to be submitted to the implementing authority as part of the notification of the clai m-;

33 RDA 1693


I.

II.

Ill.

The owner/operator name, address, and facility Installation ID number of the person claiming the exclusion;

The applicable Hazardous Waste Codes for each hazardous waste excluded as a fuel; and

The certification signed by the person claiming the exclusion or his authorized representative.

(11) A brief description of tho process that generated the hazardous waste and process that generated tho excluded fuel, if not tho same;

(111) An estimate of tho average and maximum monthly and annual quantities of each waste claimed to be excluded;

(IV) Documentation for any claim that a constituent is not present in tho hazardous waste as required under item 3(viii)(I) of this subparagraph;

(V) Tho results of all analyses and all detection limits achieved as required under subpart 3(viii) of this subparagraph;

(VI) If tho excluded waste was generated through treatment or blending, documentation as required under subpart 3(iii) or (iv) of this subparagraph;

(VII) If tho waste is to be shipped off site, a certification from tho burner as required under subpart 3(xii) of this subparagraph;

(VIII) A waste analysis plan and tho results of tho sampling and analysis that includes the following:

I.

II .

Ill.

IV.

\I .. VI.

VII .

VIII.

Tho dates and times waste samples wore obtained, and the dates tho samples v,•oro analyzed;

Tho names and qualifications of tho porson(s) who obtained tho samples;

A description of tho temporal and spatial locations of tho samples;

The name and address of tho laboratory facility at which analyses of tho samples were performed;

A description of the analytical methods used, including any clean up and sample preparation methods;

All quantitation limits achieved and all other quality control results for the analysis (including method blanks, duplicate analyses, matrix spikes, etc .), laboratory quality assurance data, and description of any deviations from analytical methods written in the plan or from any other activity written in tho plan which occurred;

All laboratory analytica l results demonstrating that tho exclusion specifications have boon met for tho waste; and

All laboratory documentation that support tho analytical results , unless a contract between tho claimant and tho laboratory provides for tho documentation to be maintained by tho laboratory for the period specified in subpart 3(xi) of this

34 RDA 1693

(a)

(xi)

(xii)

(xiii)

(IX)

subparagraph and also provides for the availability of--tl:le documentation to the claimant upon request; and

If the generator ships comparable/syngas fuel off site for burning, the generator must retain for each shipment the following information on site :

I.

II.

II.

IV.

\I ..

The name and address of the facility receiving the comparable/syngas fuel for burning;

The quantity of comparable/syngas fuel shipped and delivered;

The date of shipment or delivery;

A cross reference to the record of comparable/syngas fuel analysis or other information used to make the determination that the comparable/syngas fuel meets the specifications as required under subpart a(viii) of this subparagraph; and

A one time certification by tho burner as required under subpart a(xii) of this subparagraph.

Records retention

Records must be maintained for the period of three years. A generator must maintain a current ·Naste analysis plan during that throe year period.

Burner certification

Prior to submitting a notification to tho Commissioner, a comparable/syngas fuel generator who intends to ship their fuel off site for burning must obtain a one time written, signed statement from tho burner:

(I)

(11)

(111)

Certifying that tho comparablo/syngas fuel will only be burned in an industrial furnace or boiler, utility boiler, or haz:ardous waste incinerator, as required under subpart a(ii) of this subparagraph;

Identifying tho name and address of tho units that will burn tho comparable/syngas fuel; and

Certifying that the state in which tho burner is located is authoriz:od to exclude wastes as comparablo/syngas fuel under the provisions of this subparagraph .

Ineligible waste codes

VVastes that are listed because of presence of dioxins or furans, as set out in Appendix VII of this rule, are not eligible for this exclusion, and any fuel produced from or otherwise containing these wastes remains a haz:ardous waste subject to full haz:ardous waste management requirements.

Exclusion of comparable fuel and syngas fuel. (40 CFR 261 .381

1. Specifications for excluded fuels .

Wastes that meet the specifications for comparable fuel or syngas fuel under subpart (i) or (ii) of this part, respectively, and the other requirements of th is subparagraph, are not solid wastes .

SS-7039 (November 2014) 35 RDA 1693

(i)

(ii)

(iii)

(iv)


Comparable fuel specifications.

(I)

(11)

Physical specifications.

I. Heating value. The heating value must exceed 5,000 Btu/lbs. (11,500 J/g).

II . Viscosity. The viscosity must not exceed: 50 cS , as-fired.

Constituent specifications. For compounds listed in Table 1 to this subparagraph, the specification levels and, where non-detect is the specification, minimum required detection limits are: (see Table 1 of this subparagraph).

Synthesis gas fuel specifications.


(I)

(II)

( 111)

(IV)

(V)

Have a minimum Btu value of 100 Btu/Scf:

Contain less than 1 ppmv of total halogen:

Contain less than 300 ppmv of total nitrogen other than diatomic nitrogen

Contain less than 200 ppmv of hydrogen sulfide: and

Contain less than 1 ppmv of each hazardous constituent in the target list of appendix VIII constituents in paragraph (5) of this rule .

Blending to meet the specifications.

(I)

( 11)

Hazardous waste shall not be blended to meet the comparable fuel specification under subpart (i) of this part, except as provided by item (11) of this subpart.

Blending to meet the viscosity specification. A hazardous waste blended to meet the viscosity specification for comparable fuel shall :

I.

II.

Ill.

As generated and prior to any blending, manipulation, or processing, meet the constituent and heating value specifications of subitem (i)(l)I and item (i)(II) of this part:

Be blended at a facility that is subject to the applicable requirements of Rules 0400-12-01 -.05 and .06 , or subparagraph (4)(e) of Rule 0400-12-01 -.03: and

Not violate the di lution prohibition of subpart (vi) of th is part.

Treatment to meet the comparable fuel specifications.

(I) A hazardous waste may be treated to meet the specifications for comparable fuel set forth in subpart (i) of this part provided the treatment:

I. Destroys or removes the constituents listed in the specification or raises the heating value by removing or destroying hazardous constituents or materials :

36 RDA 1693

(v)

(vi)

(11)

II .

Ill.

Is performed at a · facility that is subject to the applicable requirements of Rules 0400-12-01 -. 05 and .06, or subparagraph (4)(e) of Rule 0400-12-01 --.03: and

Does not violate the dilution prohibition of subpart (vi) of this part.

Residuals resulting from the treatment of a hazardous waste listed in paragraph (4) of this rule to generate a comparable fuel remain a hazardous waste.

Generation of a syngas fuel.

(I)

(11)

A syngas fuel can be generated from the processing of hazardous wastes to meet the exclusion specifications of subpart (ii) of this part provided the processing :

I.

II.

111.

Destroys or removes the constituents listed in the specification or raises the heating value by removing or destroying constituents or materials:

Is performed at a facility that is subject to the applicable requirements of Rules 0400-12-01 -.05 and .06, or subparagraph (4)(e) of Rule 0400-12-01 -.03 or is an exempt recycling unit pursuant to part (1 )(f)3 of this rule: and

Does not violate the dilution prohibition of subpart (vi) of this part.

Residuals resulting from the treatment of a hazardous waste listed in paragraph (4) of this rule to generate a syngas fuel remain a hazardous waste .

Dilution prohibition.

No generator, transporter, handler, or owner or operator of a treatment, storage, or disposal facility shall in any way dilute a hazardous waste to meet the specifications of subitem (i)(l)I and item (i)(II) of this part for comparable fuel, or subpart (ii) of this part for syngas.

2. Implementation.

(i)

(ii)


General.

(I)

(11)

Notices.

(I)

Wastes that meet the specifications provided by part 1 of this subparagraph for comparable fuel or syngas fuel are excluded from the definition of solid waste provided that the conditions under this subparagraph are met. For purposes of this subparagraph, such materials are called excluded fuel : the person claiming and qualifying for the exclusion is called the excluded fuel generator and the person burning the excluded fuel is called the excluded fuel burner.

The person who generates the excluded fuel must claim the exclusion by complying with the conditions of this subparagraph and keeping records necessary to document compliance with those conditions.

Notices to the Commissioner.

I. The generator must submit a one-time notice, except as provided by subitem Ill of this item, to the Commissioner or to

37 RDA 1693

( 11)


II.

Ill.

the Regional or State RCRA and CAA Directors, in whose jurisdiction the exclusion is being claimed and where the excluded fuel will be burned, certifying compliance with the conditions of the exclusion and providing the following documentation:

A.

B.

C.

D.

E.

The name, address, and RCRA ID number of the person/facility claiming the exclusion:

The applicable EPA Hazardous Waste Code(s) that would otherwise apply to the excluded fuel:

The name and address of the units meeting the requirements of subpart (iii) of this part and part 3 of this subparagraph, that will burn the excluded fuel:

An estimate of the average and maximum monthly and annual quantity of material for which an exclusion would be claimed, except as provided by subitem Ill of this item: and

The following statement, which shall be signed and submitted by the person claiming the exclusion or his authorized representative :

"Under penalty of criminal and civil prosecution for making or submitting false statements, representations, or omissions, I certify that the requirements of subparagraph (6)(a) of Rule 0400-12-01-.02 have been met for all comparable fuels identified in this notification. Copies of the records and information required at subpart (6)(a)2(viii) of Rule 0400-12-01 -.02 are available at the generator's facility. Based on my inquiry of the individuals immediately responsible for obtaining the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. As specified in Tennessee Code Annotated Section 39-16-702(a)(4 ), this declaration is made under penalty of perjury."

If there is a substantive change in the information provided in the notice required under this subpart, the generator must submit a revised notification.

Excluded fuel generators must include an estimate of the average and maximum monthly and annual quantity of material for which an exclusion would be claimed only in notices submitted after December 19, 2008 for newly excluded fuel or for revised notices as required by subitem II of this item.

Public notice.

Prior to burning an excluded fuel, the burner must publish in a major newspaper of general circulation local to the site where the fuel wil l be burned, a notice entitled "Notification of Burning a Fuel Excluded Under the Resource Conservation and Recovery Act" and containing the following information:

38 RDA 1693

(iii)

(iv)


I.

II .

Ill.

IV.

V.

Name, address, and RCRA ID number of the generating facility(ies);

Name and address of the burner and identification of the unit(s) that will burn the excluded fuel ;

A brief, general description of the manufacturing, treatment. or other process generating the excluded fuel ;

An estimate of the average and maximum monthly and annual quantity of the excluded fuel to be burned ; and

Name and mailing address of the Commissioner or the Regional or State Directors to whom the generator submitted a cla im for the exclusion.

Burning.

The exclusion applies only if the fuel is burned in the following units that also shall be subject to Federal/State/local air emission requirements, including all applicable requirements implementing section 112 of the Clean Air Act or the Tennessee Air Quality Act:

(I)

(11)

( 111)

(IV)

Industrial furnaces as defined in subparagraph (2)(a) of Rule 0400-12-01 -.01;

Boilers, as defined in subparagraph (2)(a) of Rule 0400-12-01 -.01, that are further defined as follows:

I.

II.

Industrial boilers located on the site of a facility engaged in a manufacturing process where substances are transformed into new products, including the component parts of products, by mechanical or chemical processes: or

Utility boilers used to produce electric power, steam , heated or cooled air, or other gases or fluids for sale;

Hazardous waste incinerators subject to regulation under paragraph (15) of Rule 0400-12-01 -.05 or Rule 0400-12-01 -. 06 and applicable CM MACT standards or the comparable standard under the Tennessee Air Quality Act.

Gas turbines used to produce electric power, steam, heated or cooled air, or other gases or fluids for sale.

Fuel analysis plan for generators.

The generator of an excluded fuel shall develop and follow a written fuel analysis plan which describes the procedures for sampling and analysis of the material to be excluded. The plan shall be followed and retained at the site of the generator claiming the exclusion.

(I) At a minimum, the plan must specify:

I. The parameters for wh ich each excluded fuel will be analyzed and the rationa le for the selection of those parameters ;

II . The test methods which will be used to test for these parameters ;

39 RDA 1693

(v)


(11)

( 111)

Ill.

IV.

V.

The sampling method which will be used to obtain a representative sample of the excluded fuel to be analyzed;

The frequency with which the initial analysis of the excluded fuel will be reviewed or repeated to ensure that the analysis is accurate and up to date; and

If process knowledge is used in the determination, any information prepared by the generator in making such determination.

For each analysis, the generator shall document the following :

I.

II.

Ill.

IV.

V.

VI.

VII.

VIII .

The dates and times that samples were obtained, and the dates the samples were analyzed;

The names and qualifications of the person(s) who obtained the samples;

A description of the temporal and spatial locations of the samples:

The name and address of the laboratory facility at which analyses of the samples were performed;

A description of the analytical methods used, including any clean-up and sample preparation methods:

All quantitation limits achieved and all other quality control results for the analysis (including method blanks, duplicate analyses, matrix spikes , etc.), laboratory quality assurance data, and the description of any deviations from analytical methods written in the plan or from any other activity written in the plan which occurred:

All laboratory results demonstrating whether the exclusion specifications have been met: and

All laboratory documentation that support the analytical results, unless a contract between the claimant and the laboratory provides for the documentation to be maintained by the laboratory for the period specified in subpart (ix) of this part and also provides for the availability of the documentation to the claimant upon request.

Syngas fuel generators shall submit for approval, prior to performing sampling, analysis, or any management of an excluded syngas fuel, a fuel analysis plan containing the elements of item (I) of this subpart to the Commissioner. The approval of fuel analysis plans must be stated in writing and received by the facility prior to sampling and analysis to demonstrate the exclusion of a syngas. The approval of the fuel analysis plan may contain such provisions and cond itions as the Commissioner deems appropriate.

Excluded fuel sampling and analysis .

(I) General .

For wastes for which an exclusion is claimed under the specifications provided by subpart 1 (i) or (i i) of this subparagraph, the generator of the

40 RDA 1693


waste must test for all the constituents in appendix VIII in paragraph (5) of this rule, except those that the generator determines, based on testing or knowledge, should not be present in the fuel. The generator is required to document the basis of each determination that a constituent with an applicable specification should not be present. The generator may not determine that any of the following categories of constituents with a specification in Table 1 to this subparagraph should not be present:

I.

II.

Ill.

IV.

A constituent that triggered the toxicity characteristic for the constituents that were the basis for listing the hazardous secondary material as a hazardous waste, or constituents for which there is a treatment standard for the waste code in subparagraph (3)(a) of Rule 0400-12-01 -.1 0:

A constituent detected in previous analysis of the waste:

Constituents introduced into the process that generates the waste: or

Constituents that are byproducts or side reactions to the process that generates the waste.

(Note: Any claim under this subpart must be valid and accurate for all hazardous constituents: a determination not to test for a hazardous constituent will not shield a generator from liabi lity should that constituent later be found in the excluded fuel above the exclusion specifications.)

(11)

(111)

(IV)

(V)

Use of process knowledge. For each waste for which the comparable fuel or syngas exclusion is claimed where the generator of the excluded fuel is not the original generator of the hazardous waste, the generator of the excluded fuel may not use process knowledge pursuant to item (I) of this subpart and must test to determine that all of the constituent specifications of subparts 1 (i) and (ii) of this subparagraph, as applicable, have been met.

The excluded fuel generator may use any reliable analytical method to demonstrate that no constituent of concern is present at concentrations above the specification levels. It is the responsibility of the generator to ensure that the sampling and analysis are unbiased, precise, and representative of the excluded fuel. For the fuel to be eligible for exclusion, a generator must demonstrate that:

I.

II.

The 95% upper confidence limit of the mean concentration for each constituent of concern is not above the specification level : and

The analyses could have detected the presence of the constituent at or below the specification level.

Nothing in this subpart preempts, overrides or otherwise negates the provision in subparagraph (1 )(b) of Rule 0400-12-01 -.03, which requires any person who generates a solid waste to determine if that waste is a hazardous waste.

In an enforcement action, the burden of proof to establish conformance with the exclusion specification shall be on the generator claiming the exclusion.

41 RDA 1693

(vi)

(vii)

(viii)


(VI) The generator must conduct sampling and analysis in accordance with the fuel analysis plan developed under subpart (iv) of this part.

(VII) Viscosity condition for comparable fuel.

I.

II.

Excluded comparable fuel that has not been blended to meet the kinematic viscosity specification shall be analyzed as-generated .

If hazardous waste is blended to meet the kinematic viscosity specification for comparable fuel, the generator shall:

A.

B.

Analyze the hazardous waste as-generated to ensure that it meets the constituent and heating value specifications of subpart 1 (i) of this subparagraph; and

After blending, analyze the fuel again to ensure that the blended fuel meets all comparable fuel specifications.

(VIII) Excluded fuel must be re-tested, at a minimum, annually and must be retested after a process change that could change its chemical or physical properties in a manner than may affect conformance with the specifications.

Reserved

Speculative accumulation.

Excluded fuel must not be accumulated speculatively, as defined in subpart (1 )(b)3(viii) of this rule .

Operating record .

The generator must maintain an operating record on site containing the following information:

(I)

(11)

(111)

(IV)

(V)

All information required to be submitted to the implementing authority as part of the notification of the claim:

I.

II.

Ill.

The owner/operator name, address, and the facility Installation ID number of the person claiming the exclusion;

For each excluded fuel, the hazardous waste codes that would be applicable if the material were discarded; and

The certification signed by the person claiming the exclusion or his authorized representative.

A brief description of the process that generated the excluded fuel. If the comparable fuel generator is not the generator of the original hazardous waste, provide a brief description of the process that generated the hazardous waste;

The monthly and annual quantities of each fuel claimed to be excluded ;

Documentation for any claim that a constituent is not present in the excluded fuel as required under item (v)(I) of this part;

The results of all analyses and all detection limits achieved as required under subpart (iv) of this part;

42 RDA 1693

(ix)

(x)

(xi)

(xii)


(VI) If the comparable fuel was generated through treatment or blending, documentation of compliance with the applicable provisions of subparts 1 (iii) and (iv) of th is subparagraph :

(VII) If the excluded fuel is to be shipped off-site. a certification from the burner as required under subpart (x) of this part:

(VIII) The fuel analysis plan and documentation of all sampling and analysis results as required by subpart (iv) of this part: and

(IX) If the generator ships excluded fuel off-site for burning. the generator must retain for each shipment the following information on-site :

I.

II.

Ill .

IV.

V.

The name and address of the facility receiving the excluded fuel for burning:

The quantity of excluded fuel shipped and delivered:

The date of shipment or delivery:

A cross-reference to the record of excluded fuel analysis or other information used to make the determination that the excluded fuel meets the specifications as required under subpart (iv) of this part: and

A one-time certification by the burner as required under subpart . (x) of this part.

Records retention .

Records must be maintained for a period of three years .

Burner certification to the generator.

Prior to submitting a notification to the Commissioner. a generator of excluded fuel who intends to ship the excluded fuel off-site for burning must obtain a onetime written. signed statement from the burner:

(I)

(11)

(111)

Certifying that the excluded fuel will only be burned in an industrial furnace. industrial boiler. utility boiler, or hazardous waste incinerator. as required under subpart (iii) of this part:

Identifying the name and address of the facility that will burn the excluded fuel : and

Certifying that the State in which the burner is located is authorized to exclude wastes as excluded fuel under the provisions of this subparagraph.

Ineligible waste codes .

Wastes that are listed as hazardous waste because of the presence of dioxins or furans . as set out in appendix VII in paragraph (5) of th is rule, are not eligible for these exclusions. and any fuel produced from or otherwise containing these wastes remains a hazardous waste subject to the full hazardous waste management requirements.

Regulatory status of boiler residues .

43 RDA 1693

(xiii)

Burning excluded fuel that was otherwise a hazardous waste listed subparagraphs (4)(b) through (d) of this rule does not subject boiler residues, including bottom ash and emission control residues , to regulation as derived-from hazardous wastes.

Residues in containers and tank systems upon cessation of operations.

(I)

(II)

(111)

Liquid and accumulated solid residues that remain in a container or tank system for more than 90 days after the container or tank system ceases to be operated for storage or transport of excluded fuel product are subject to regulation under Rules 0400-12-01 -.03 through 0400-12-01 -.10.

Liquid and accumulated solid residues that are removed from a container or tank system after the container or tank system ceases to be operated for storage or transport of excluded fuel product are solid wastes subject to regulation as hazardous waste if the waste exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (e) of this rule or if the fuel were otherwise a hazardous waste listed under subparagaphs (4)(b) through (d) of this rule when the exclusion was claimed.

Liquid and accumulated solid residues that are removed from a container or tank system and which do not meet the specifications for exclusion under subpart 1 (i) or (ii) of this subparagraph are solid wastes subject to regulation as hazardous waste if:

I.

II.

The waste exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (d) of this rule: or

The fuel were otherwise a hazardous waste listed under subparagraphs (4)(b) through (d) of this rule. The hazardous waste code for the listed waste applies to these liquid and accumulated solid resides.

(xiv) Waiver of RCRA Closure Requirements .

(xv)

Interim status and permitted storage and combustion units, and generator storage units exempt from the permit requirements under subparagraph (4 )(e) of Rule 0400-12-01 -.03, are not subject to the closure requirements of Rules 0400-12-01 -.05 and 0400-12-01-.06 provided that the storage and combustion unit has been used to manage only hazardous waste that is subsequently excluded under the conditions of this subparagraph, and that afterward will be used only to manage fuel excluded under this subparagraph.

Spills and leaks.

(I)

(II)

Excluded fuel that is spilled or leaked and that therefore no longer meets the conditions of the exclusion is discarded and must be managed as a hazardous waste if it exhibits a characteristic of hazardous waste under subparagraphs (3)(b) through (d) of this rule or if the fuel were otherwise a hazardous waste listed in subparagraphs (4)(b) through (d) of this rule.

For excluded fuel that would have otherwise been a hazardous waste listed in subparagraphs (4)(b) through (d) of this rule and which is spilled or leaked, the hazardous waste code for the listed waste applies to the spilled or leaked material.

(xvi) Nothing in this part preempts, overrides, or otherwise negates the provisions in CERCLA Section 103, which establ ish reporting obligations for releases of

SS-7039 (November 2014) 44 RDA 1693

hazardous substances, or the Department of Transportation requirements for hazardous materials in 49 CFR parts 171 through 180.

3. Fai lure to comply with the conditions of the exclusion.

An excluded fuel loses its exclusion if any person managing the fuel fails to comply with the cond itions of the exclusion under this subparagraph, and the material must be managed as hazardous waste from the point of generation. In such situations, EPA or the Commissioner may take enforcement action under RCRA section 3008(a), or the Commissioner may take enforcement action under T.C.A. §§ 68-212-101 et seq.

Table 1: Detection and Detection Limit Values for Comparable Fuel Specification

Total Nitrogen as N Total Halogens as Cl

Chemical Name

Total Organic Halogens as Cl Polychlorinated biphenyls total (Arocolors, total] Cyanide, total Metals: Antimony, total Arsenic, total Barium, total Beryllium, total Cadmium, total Chromium, total Cobalt Lead, total Manganese Mercury, total Nickel, total Selenium, total Silver, total Thall ium, total

Hydrocarbons: Benzo(alanthracene Benzene Benzo(bjfluoranthene Benzo(kjfluoranthene Benzo(ajpyrene Chrysene Dibenzo(a, hjanthracene 7, 12-Dimethylbenz(a]anthracene Fluoranthene lndeno(1, 2, 3-cd)pyrene 3-Methylcholanthrene Naphthalene Toluene

Oxygenates: Acetophenone Acrolein Allyl alcohol Bis(2-ethylhexl) phthalate (Di-2-ethylhexyl phthalatel Butyl benzyl phthalate o-Cresol (2-Methyl phenol]

SS-7039 (November 2014) 45

GAS No.

NA NA NA 1336-36-3 57-12-5

7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7439-92-1 7439-96-5 7439-97-6 7440-02-0 7782-49-2 7440-22-4 7440-28-0

56-55-3 71-43-2 205-99-2 207-08-9 50-32-8 218-01-9 53-70-3 57-97-6 206-44-0 193-39-5 56-49-5 91-20-3 108-88-3

98-86-2 107-02-8 107-18-6 117-81-7 85-68-7 95-48-7

Concentration limit (mg/kg at 10,000 BTU/lb)

1f 0.23 23 u 2.3 4.6 fil u 0.25 58 0.23 2.3 23

Minimum required

detection limit /ma/ka)

M 1

RDA 1693

m-Cresol (3-Methyl phenol) 108-39-4 2400 p-Cresol (4-Methyl phenol] 106-44-5 2400 Di-n-butyl phthalate 84-74-2 2400 Diethyl phthalate 84-66-2 2400 2, 4-Dimethylphenol 105-67-9 2400 Dimethyl phthalate 131-11 -3 2400 Di-n-octyl phthalate 117-84-0 2400 Endothall 145-73-3 100 Ethyl methacrylate 97-63-2 39 2-Ethoxyethanol (Ethylene glycol monoethyl ether] 110-80-5 100 lsobutyl alcohol 78-83-1 39 lsosafrole 120-58-1 2400 Methyl ethyl ketone [2-Butanone] 78-93-3 39 Methyl methacrylate 80-62-6 39 1, 4-Naphthoguinone 130-15-4 2400 Phenol 108-95-2 2400 Propargyl alcohol (2-Propyn-1-ol] 107-19-7 30 Safrole 94-59-7 2400

Sulfonated Organics: Carbon disulfide 75-15-0 ND 39 Disulfoton 298-04-4 ND 2400 Ethyl methanesulfonate 62-50-0 ND 2400 Methyl methanesulfonate 66-27-3 ND 2400 Phorate 298-02-2 ND 2400 1 , 3-Propane sultone 1120-71 -4 ND 100 Tetraethyldithiopyrophosphate [Sulfotepp] 3689-24-5 ND 2400 Thiophenol [Benzenethioll 108-98-5 ND 30 0, 0, O-Triethyl phosphorothioate 126-68-1 ND 2400

Nitrogenated Organics: Aceton itrile (Methyl cyanide] 75-05-8 ND 39 2-Acetylaminofluorene (2-AAF] 53-96-3 ND 2400 Acrylonitrile 107-13-1 ND 39 4-Aminobiphenyl 92-67-1 ND 2400 4-Aminopyridine 504-24-5 ND 100 An iline 62-53-3 ND 2400 Benzidine 92-87-5 ND 2400 Dibenz(a, jjacridine 224-42-0 ND 2400 0, O-Diethyl O-pyrazinyl Phosphorothioate [Thionazinj 297-97-2 ND 2400 Dimethoate 60-51-5 ND 2400 p-(Dimethylamino) azobenzene (4-dimethylaminoazobenzene] 3,3'-Dimethylbenzidine 60-11 -7 ND 2400 a., a.-Dimethylphenethylamine 119-93-7 ND 2400

122-09-8 ND 2400 3, 3'-Dimethoxybenzidine 119-90-4 ND 100 1, 3-Dinitrobenzene [m-Dinitrobenzene] 99-65-0 ND 2400 4, 6-Dinitro-o-cresol 534-52-1 ND 2400 2, 4-Dinitrophenol 51 -28-5 ND 2400 2, 4-Dinitrotoluene 121 -14-2 ND 2400 2, 6-Dinitrotoluene 606-20-2 ND 2400 Dinoseb [2-sec-Butyl-4, 6-dinitrophenol] 88-85-7 ND 2400 Diphenylamine 122-39-4 ND 2400 Ethyl carbamate (Urethane] 51 -79-6 ND 100 Ethylenethiourea (2-lmidazolidinethione) 96-45-7 ND 11Q Famphur 52-85-7 ND 2400 Methacrylonitrile 126-98-7 ND 39 Methapyrilene 91 -80-5 ND 2400 Methomyl 16752-77-5 ND 57 2-Methyllactonitrile, [Acetone cyanohydrin] 75-86-5 ND 100

SS-7039 (November 2014) 46 RDA 1693

Methyl parathion 298-00-0 ND 2400 MNNG (N-Metyl-N-nitroso-N[prime]- nitroguanidine) 70-25-7 ND 11Q 1-Naphthylamine, [ a.-Naphthylamine] 134-32-7 ND 2400 2-Naphthylamine, m-Naphthylamine] 91 -59-8 ND 2400 Nicotine 54-11 -5 ND 100 4-Nitroaniline, [p-Nitroaniline] 100-01 -6 ND 2400 Nitrobenzene 98-95-3 ND 2400 p-Nitrophenol, [p-Nitrophenol] 100-02-7 ND 2400 5-Nitro-o-toluidine 99-55-8 ND 2400 N-Nitrosodi-n-butylamine 924-16-3 ND 2400 N-Nitrosodiethylamine 55-18-5 ND 2400 N-Nitrosodiphenylamine, [Diphenylnitrosamine] 86-30-6 ND 2400 N-Nitroso-N-methylethylamine 10595-95-6 ND 2400 N-Nitrosomorpholine 59-89-2 ND 2400 N-Nitrosophiperidine 100-75-4 ND 2400 N-Nitrosopyrrolidine 930-55-2 ND 2400 2-Nitropropane 79-46-9 ND 30 Parathion 56-38-2 ND 2400 Phenacetin 62-44-2 ND 2400 1, 4-Phenylne diamine, [p-Phenylenediamine] 106-50-3 ND 2400 N-Phenylthiourea 103-85-5 ND 57 2-Picoline [alpha-Picoline] 109-06-8 ND 2400 Propylthioracil, [6-Propyl-2-thiouracil] 51 -52-5 ND 100 Pyridine 110-86-1 ND 2400 Strychnine 57-24-9 ND 100 Thioacetamide 62-55-5 ND 57 Thiofanox 39196-18-4 ND 100 Thiourea 62-56-6 ND 57 Toluene-2,4-diamine [2,4-Diaminotoluene] 95-80-7 ND 57 Toluene-2, 6-diamine [2, 6-Diaminotoluene] 823-40-5 ND 57 o-Toluidine 95-53-4 ND 2400 p-Toluidine 106-49-0 ND 100 1, 3, 5-Trinitrobenzene, [sym-Trinitobenzene] 99-35-4 ND 2400

Halogenated Organics: Ally! ch loride 107-05-1 ND 39 Aramite 140-57-8 ND 2400 Benzal chloride [Dichloromethyl benzene] 98-87-3 ND 100 Benzyl ch loride 100-44-77 ND 100 bis(2-Chloroethyl)ether [Dichoroethyl ether] 111-44-4 ND 2400 Bromoform [T ribromomethane] 75-25-2 ND 39 Bromomethane [Methyl bromide] 74-83-9 ND 39 4-Bromophenyl phenyl ether [p-Bromo diphenyl ether] 101 -55-3 ND 2400 Carbon tetrachloride 56-23-5 ND 39 Chlordane 57-74-9 ND .11 p-Chloroaniline 106-47-8 ND 2400 Chlorobenzene 108-90-7 ND 39 Chlorobenzilate 510-15-6 ND 2400 p-Chloro-m-cresol 59-50-7 ND 2400 2-Chloroethyl vinyl ether 110-75-8 ND 39 Chloroform 67-66-3 ND 39 Chloromethane [Methyl chloride] 74-87-3 ND 39 2-Chloronaphthalene [beta-Chloronaphthalene] 91-58-7 ND 2400 2-Chlorophenol [o-Chlorophenol] 95-57-8 ND 2400 Chloroprene [2-Chloro-1, 3-butadiene] 1126-99-8 ND 39 2, 4-D [2, 4-Dichlorophenoxyacetic acid] 94-75-7 ND z Diallate 2303-16-4 ND 2400 1, 2-Dibromo-3-ch loropropane 96-12-8 ND 39 1, 2-Dichlorobenzene [o-Dichlorobenzene] 95-50-1 ND 2400 1, 3-Dichlorobenzene [m-Dichlorobenzene] 541-73-1 ND 2400

SS-7039 (November 2014) 47 RDA 1693

1, 4-Dich lorobenzene [p-Dichlorobenzene) 3, 3[prime)-Dichlorobenzidine Dichlorodifluoromethane [CFC-121 1, 2-Dichloroethane [Ethylene dichloride) 1, 1-Dichloroethylene [Vinylidene chloride) Dichloromethoxy ethane [Bis(2-chloroethoxy}methane) 2,4-Dichlorophenol 2, 6-Dichlorophenol 1, 2-Dich loropropane [Propylene dichloride) cis-1, 3-Dichloropropylene trans-1, 3-Dich loropropylene 1,3-Dich loro-2propanol Endosulfan I Endosulfan II Endrin Endrin aldehyde Endrin Ketone Epichlorohydrin [1 -Chloro-2, 3-epoxy propane) Ethylidene dichloride [1, 1-Dichloroethane) 2-Fluoroacetamide Heptachlor Heptachlor epoxide Hexachlorobenzene Hexachloro-1, 3-butadiene [Hexachlorobutadiene) Hexachlorocyclopentadiene Hexachloroethane Hexachlorophene Hexachloropropene [Hexachloropropylene) lsodrin Kepone [Chlordecone) Lindane [gamma-BHC) [gammaHexachlorocyclohexanel Methylene chloride [Dichloromethane) 4, 4'-Methylene-bis(2-chloroaniline) Methyl iodide [lodomethane) Pentachlorobenzene Pentachloroethane Pentachloronitrobenzene [PCNB) [Quintobenzene) [Quintozene) Pentachlorophenol Pron amide Silvex [2, 4, 5-Trichlorophenoxypropionic acid) 2, 3, 7, 8-Tetrachlorodibenzo-p-dioxin [2, 3, 7, 8-TCDD) 1, 2, 4, 5-Tetrachlorobenzene 1, 1, 2, 2-Tetrachloroethane T etrachloroethylene [Perchloroethylene l 2, 3, 4, 6-Tetrachlorophenol 1, 2, 4-Trichlorobenzene 1, 1, 1-Trich loroethane [Methyl chloroform) 1, 1,2-Trichloroethane [Vinyl trichloride) T richloroethylene

Notes:

Trichlorofluoromethane [Trich loromonofluoromethane) 2, 4, 5-Trichlorophenol 2, 4, 6-Trichlorophenol 1, 2, 3-Trich loropropane Vin I Chloride

NA - Not Applicable. ND - Nondetect. 125 or individual halogenated organics listed below.

SS-7039 (November 2014) 48

106-46-7 91-94-1 75-71 -8 107-06-2 75-35-4 111-91-1 120-83-2 87-65-0 78-87-5 10061-01-5 10061-02-6 96-23-1 959-98-8 33213-65-9 72-20-8 7421-93-4 53494-70-5 106-89-8 75-34-3 640-19-7 76-44-8 1024-57-3 118-74-1 87-68-3 77-47-4 67-72-1 70-30-4 1888-71-7 465-73-6 143-50-0 58-89-9 75-09-2 101-14-4 74-88-4 608-93-5 76-01 -7 82-68-8 87-86-5 23950-58-5 93-72-1 1746-01-6 95-94-3 79-34-5 127-18-4 58-90-2 120-82-1 71-55-6 79-00-5 79-01-6 75-69-4 95-95-4 88-06-2 96-18-4 75-01-4

RDA 1693


Subparagraph (k) of paragraph (7) of Rule 0400-12-01-.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste Treatment, Storage, and Disposal Facilities is amended by deleting it in its entirety and substituting instead the following:

(k) Certification of Completion of Post-closure Care [40 CFR 265.120]

No later than 60 days after the completion of the established post-closure care period for each hazardous waste disposal unit, the owner or operator must submit to the Commissioner, by registered mail, a certification that the post-closure care period for the hazardous waste disposal unit was performed in accordance with the specifications in the approved post-closure plan. The certification must be signed by the owner or operator and a qualified Professional Engineer. Documentation supporting the qualified Professional Engineer's certification must be furnished to the Commissioner upon request until he releases the owner or operator from the financial assurance requirements for post-closure care under part (8)(f)3 of this rule.


Part 2 of subparagraph (g) of paragraph (1) of Rule 0400-12-01-.10 Land Disposal Restrictions is amended by deleting subpart (iv) in its entirety and substituting instead the following:

(iv) The treatment facility must submit a one-time certification signed by an authorized representative with the initial shipment of waste or treatment residue of a restricted waste to the land disposal facility. A The certification is also necessary for contaminated soil and it must state:


"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification. Based on my inquiry of those individuals immediately responsible for obtaining this information, I believe that it has been maintained and operated properly so as to comply with the treatment standards specified in Rule 0400-12-001-.10(3)(a) without impermissible dilution of the prohibited waste. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury."

A certification is also necessary for contaminated soil and it must state:

"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification and believe that it has been maintained and operated properly so as to comply with treatment standards specified in Rule 0400-12-01-.10(3)U) without impermissible dilution of the prohibited waste. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702(a)(4), this declaration is made under penalty of perjury. "

(I) A copy of the certification must be placed in the treatment facility's onsite files. If the waste or treatment residue changes, or the receiving facility changes, a new certification must be sent to the receiving facility, and a copy placed in the file.

(11) Debris excluded from the definition of hazardous waste under Rule 0400-12-01-.02(1 )(c)6 (i.e., debris treated by an extraction or destruction technology provided by Table 1, subparagraph (3)(f) of this rule, and debris that the Commissioner has determined does not contain hazardous waste), however, is subject to the notification and certification

49 RDA 1693

requirements of part 4 of this subparagraph rather than the certification requirements of this subpart.

(111) For wastes with organic constituents having treatment standards expressed as concentration levels, if compliance with the treatment standards is based in whole or in part on the analytical detection limit alternative specified in part (3)(a)4 of this rule, the certification , signed by an authorized representative, must state the following:

"I certify under penalty of law that I have personally examined and am familiar with the treatment technology and operation of the treatment process used to support this certification. Based on my inquiry of those individuals immediately responsible for obtaining this information, I believe that the nonwastewater organic constituents have been treated by combustion units as specified in Rule 0400-12-01 -. 10(3)(c), Table 1. I have been unable to detect the nonwastewater organic constituents, despite having used best good-faith efforts to analyze for such constituents. I am aware there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702{a){4), this declaration is made under penalty of perjury. "

(IV) For characteristic wastes that are subject to the treatment standards in subparagraph (3)(a) of this rule (other than those expressed as a method of treatment) or subparagraph (3)U) of this rule and that contain underlying hazardous constituents as defined in part (b)10 of this paragraph; if these wastes are treated on-site to remove the hazardous characteristic; and are then sent off-site for treatment of underlying hazardous constituents, the certification must state the following:

"I certify under penalty of law that the waste has been treated in accordance with the requirements of Rule 0400-12-01 -.10(3)(a) or Rule 0400-12-01 -.10(3)U) to remove the hazardous characteristic. This decharacterized waste contains underlying hazardous constituents that require further treatment to meet treatment standards. I am aware that there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702{a){4), this declaration is made under penalty of perjury."

(V) For characteristic wastes that contain underlying hazardous constituents as defined in part (b )1 O of this paragraph that are treated on-site to remove the hazardous characteristic and to treat underlying hazardous constituents to levels in subparagraph (3)(i) of this rule Universal Treatment Standards, the certification must state the following:

"I certify under penalty of law that the waste has been treated in accordance with the requirements of Rule 0400-12-01-.10(3)(a) to remove the hazardous characteristic, and that underlying hazardous constituents, as defined in Rule 0400-12-01 -. 10(1)(b)10, have been treated on-site to meet the Rule 0400-12-01 -.10(3)(i) Universal Treatment Standards. I am aware that there are significant penalties for submitting a false certification, including the possibility of fine and imprisonment. As specified in Tennessee Code Annotated Section 39-16-702{a){4), this declaration is made under penalty of perjury."

Authority: T.C.A. §§ 68-212-101 et seq. and 4-5-201 et seq .

Waste code K161 of the Table "Treatment Standards for Hazarous Wastes" following part 10 of subparagraph (a) of paragraph (3) of Rule 0400-12-01 -.10 Land Disposal Restrictions is amended by deleting "137-30-4" in the third

SS-7039 (November 2014) 50 RDA 1693

column to the right of "Dithiocarbamates (total) 10 " and replacing it with "NA" so that, as amended, the entry for K161 shall read as follows :

K161 Purification solids (including Antimony 7440-36-0 1.9 1.15 mg/L TCLP filtration, evaporation, and centrifugation solids), baghouse dust and floor sweepings from the production of dithiocarbamate acids and their salts.

Arsenic 7440-38-2 1.4 5.0 mg/L TCLP

Carbon disulfide 75-15-0 3.8 4.8 mg/L TCLP

Dithiocarbamates +37-aG-4-NA 0.028; or 28; or CMBST (total) 10 CMBST,

CHOXD, BIODG orCARBN

Lead 7439-92-1 0.69 0.75 mg/L TCLP

Nickel 7440-02-0 3.98 11 .0 mg/L TCLP

Selenium 7782-49-2 0.82 5. 7 mg/L TCLP


SS-7039 (November 2014) 51 RDA 1693

* If a roll-call vote was necessary, the vote by the Agency on these rulemaking hearing rules was as follows:

Board Member Aye No Abstain Absent Signature (if required)

Marty Calloway X (Petroleum Business with at least 15 Underground Storaqe Tanks) Stacey Cothran X (Solid/Hazardous Waste Management Industry) Kenneth L. Donaldson X (Municipal Government) Dr. George Hyfantis, Jr. X (Institution of Higher Learning) Bhag Kanwar X (Single Facility with less than 5 Underground Storage Tanks) Alan M. Leiserson X Environmental Interests Jared L. Lynn X (Manufacturing experienced with Solid/Hazardous Waste) David Martin X (Working in a field related to Aqriculture) Beverly Philpot X (Manufacturing experienced with Underground Storage Tanks/Hazardous Materials) DeAnne Redman X (Petroleum Manaqement Business) Mayor A. Franklin Smith, Ill X (County Government) Mark Williams X (Small Generator of Solid/Hazardous Materials representinq Automotive Interests)

I certify that this is an accurate and complete copy of rulemaking hearing rules, lawfully promulgated and adopted by the Underground Storage Tanks and Solid Waste Disposal Control Board on 06/03/2015, and is in compliance with the provisions of T.C.A. § 4-5-222.

I further certify the following:

Notice of Rulemaking Hearing filed with the Department of State on: 03/16/2015

Rulemaking Hearing(s) Conducted on: (add more dates). 05/19/2015

Date: June 3, 2015

Signature: _____________________ _

Name of Officer: Stacey Cothran --~-------------------Tit I e of Officer: Board Chair ----------------------

Subscribed and sworn to before me on: ------- -----------Notary Public Signature: ------------------

My commission expires on: _________________ _

SS-7039 (November 2014) 52 RDA 1693

Rules of the Underground Storage Tanks and Solid Waste Disposal Control Board Chapter 0400-12-01 Hazardous Waste Management Rule 0400-12-01 -.02 Identification and Listing of Hazardous Waste Rule 0400-12-01 -.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste

Treatment, Storage, and Disposal Facilities Rule 0400-12-01 -.10 Land Disposal Restrictions

All rulemaking hearing rules provided for herein have been examined by the Attorney General and Reporter of the State of Tennessee and are approved as to legality pursuant to the provisions of the Administrative Procedures Act, Tennessee Code Annotated , Title 4, Chapter 5.


Filed with the Department of State on :

Effective on :

SS-7039 (November 2014) 53

Herbert H. Slatery Ill Attorney General and Reporter

Date

- ------------ --

Tre Hargett Secretary of State

RDA 1693

Public Hearing Comments

One copy of a document containing responses to comments made at the public hearing must accompany the filing pursuant to T.C.A. § 4-5-222. Agencies shall include only their responses to public hearing comments, which can be summarized . No letters of inquiry from parties questioning the rule will be accepted . When no comments are received at the public hearing, the agency need only draft a memorandum stating such and include it with the Rulemaking Hearing Rule filing. Minutes of the meeting will not be accepted. Transcripts are not acceptable.

There were no comments received during the comment period.

SS-7039 (November 2014) 54 RDA 1693

Regulatory Flexibility Addendum Pursuant to T.C.A. §§ 4-5-401 through 4-5-404, prior to initiating the rule making process as described in T.C.A. § 4-5-202(a)(3) and T.C.A. § 4-5-202(a), all agencies shall conduct a review of whether a proposed rule or rule affects small businesses.

This rulemaking includes the minor changes EPA has identified when reviewing the regulations to supporting continuing authorization. These changes include: (a) correct a typographical error to the process description to K107; (b) for the Waste code K161 of the Table "Treatment Standards for Hazardous Wastes" in Rule 0400-12-01-.10, delete the CAS number "137-30-4" in the third column to the right of "Dithiocarbamates (total) 10" and replacing it with "NA" so that it is consistent with the federal language.

This rulemaking also makes additional housekeeping changes in order for Tennessee's regulations to be consistent with EPA's and surrounding states. These changes include: (a) adding a common chemical name 1,1,1-Trichloroethane to the U226 list of commercial chemical products (We are adding 1,1,1-Trichloroethane for the regulated community's convenience but the chemical was already listed as U226 under the names Ethane, 1, 1, 1-trichloro- and Methyl Chloroform and, therefore is not a new listing.); (b) updating the regulatory language regarding the exclusion of comparable fuel and syngas fuel to be equivalent with EPA's language; (c) correcting the introductory statements to Rule 0400-12-01-.10(1)(g)2(iv) so that it reads like the federal language; and (d) adding a sentence to the certification statements to reference T.C.A. § 39-16-702(a)(4) as request by the Attorney General's office.

(1) The type or types of small business and an identification and estimate of the number of small businesses subject to the proposed rule that would bear the cost of, or directly benefit from the proposed rule.

There are many small businesses that generate or manage hazardous waste but these amendments will have no measurable impact on any of them.

(2) The projected reporting, recordkeeping, and other administrative costs required for compliance with the proposed rule, including the type of professional skills necessary for preparation of the report or record.

These amendments not add any additional reporting, recordkeeping or administrative cost to the regulated community

(3) A statement of the probable effect on impacted small businesses and consumers.

There will be no measurable impact on small businesses.

(4) A description of any less burdensome, less intrusive or less costly alternative methods of achieving the purpose and objectives of the proposed rule that may exist, and to what extent the alternative means might be less burdensome to small business.

No alternatives are available to achieve the purpose of this rulemaking.

(5) A comparison of the proposed rule with any federal or state counterparts.

This rulemaking make Tennessee's regulations more consistent with the federal regulations and with surrounding states.

(6) Analysis of the effect of the possible exemption of small businesses from all or any part of the requirements contained in the proposed rule.

There is no effect since this rulemaking has no measurable impact on small businesses.

SS-7039 (November 2014) 55 RDA 1693

Impact on Local Governments

Pursuant to T.C.A. §§ 4-5-220 and 4-5-228 "any rule proposed to be promulgated shall state in a simple declarative sentence, without additional comments on the merits of the policy of the rules or regulation, whether the rule or regulation may have a projected impact on local governments." (See Public Chapter Number 1070 (http://state.tn.us/sos/acts/106/pub/pc1070.pdf} of the 2010 Session of the General Assembly}

The Department does not anticipate an impact on local governments.

SS-7039 (November 2014) 56 RDA 1693

Additional Information Required by Joint Government Operations Committee

All agencies, upon filing a rule, must also submit the following pursuant to T.C.A. § 4-5-226(i)(1 ).

(A) A brief summary of the rule and a description of all relevant changes in previous regulations effectuated by such rule;

This rulemaking includes the minor changes EPA has identified when reviewing the regulations to supporting continuing authorization. These changes include: (a) correct a typographical error to the process description to K107; (b) for the Waste code K161 of the Table "Treatment Standards for Hazardous Wastes" in Rule 0400-12-01-.10, delete the CAS number "137-30-4" in the third column to the right of "Dithiocarbamates (total) 1 O" and replacing it with "NA" so that it is consistent with the federal language.

This rulemaking also makes additional housekeeping changes in order for Tennessee's regulations to be consistent with EPA's and surrounding states. These changes include: (a) adding a common chemical name 1, 1, 1-Trichloroethane to the U226 list of commercial chemical products (We are adding 1, 1, 1-Trichloroethane for the regulated community's convenience but the chemical was already listed as U226 under the names Ethane, 1, 1, 1-trichloro- and Methyl Chloroform and, therefore is not a new listing.); (b) updating the regulatory language regarding the exclusion of comparable fuel and syngas fuel to be equivalent with EPA's language; (c) correcting the introductory statements to Rule 0400-12-01-.10(1 )(g)2(iv) so that it reads like the federal language; and (d) adding a sentence to the certification statements to reference T.C.A. § 39-16-702(a)(4) as request by the Attorney General's office.

(B) A citation to and brief description of any federal law or regulation or any state law or regulation mandating promulgation of such rule or establishing guidelines relevant thereto;

These rules are being promulgated under the authority of T.C.A. §§ 68-212-101 et seq. These amendments will brin the state hazardous waste re ulations more in line with the federal re ulations and surroundin states.

(C) Identification of persons, organizations, corporations or governmental entities most directly affected by this rule, and whether those persons, organizations, corporations or governmental entities urge adoption or rejection of this rule;

Generators, Treatment, Storage and Disposal Facilities of Hazardous Waste are directly affected by this rulemakin and there were no comments received durin the ublic comment eriod.

(D) Identification of any opinions of the attorney general and reporter or any judicial ruling that directly relates to the rule;

I The Department is not aware of any opinions or judicial rulings that directly relate to this rule.

(E) An estimate of the probable increase or decrease in state and local government revenues and expenditures, if any, resulting from the promulgation of this rule, and assumptions and reasoning upon which the estimate is based. An agency shall not state that the fiscal impact is minimal if the fiscal impact is more than two percent (2%) of the agency's annual budget or five hundred thousand dollars ($500,000), whichever is less;

I This rulemaking will not impact state or local government revenues or expenditures.

(F) Identification of the appropriate agency representative or representatives, possessing substantial knowledge and understanding of the rule;

Jackie Okoreeh-Baah Division of Solid Waste Management William R. Snodgrass Tennessee Tower 312 Rosa L. Parks Avenue, 14th Floor Nashville, Tennessee 37243 (615) 532-0825 [email protected]

SS-7039 (November 2014) 57 RDA 1693

(G) Identification of the appropriate agency representative or representatives who will explain the rule at a scheduled meeting of the committees;

Jenny Howard Deputy General Counsel Office of General Counsel

(H) Office address, telephone number, and email address of the agency representative or representatives who will explain the rule at a scheduled meeting of the committees; and

Office of General Counsel Tennessee Department of Environment and Conservation William R. Snodgrass Tennessee Tower 312 Rosa L. Parks Avenue, 2nd Floor Nashville, Tennessee 37243 (615) 532-8685 Jennv. Howardtmtn.aov

(I) Any additional information relevant to the rule proposed for continuation that the committee requests.

I The Department is not aware of any additional relevant information.

SS-7039 (November 2014) 58 RDA 1693

Department of StateDivision of Publications312 Rosa L. Parks Avenue, Bth Floor Snodgrass/TN TowerNashville, TN 37243Phone: 61 5-741 -2650Emaìl: publications. information@tn. gov

Agency/Board/Comm¡ss¡on: Ënvironment and Conservation

Division: Solid Waste Management


Sequence Number:

Rule lD(s).

File Date:

Effective Date:

'7

Filing Form for Stay of Effective Date on Rules,W¡thdrawal of Stay, ând Withdrawal of Rules

Contact Person:

Addiesi:Z|p:

Phone:

Email:

Kasey Washburn

G-'10 War Memorial Building, Nashville, TN

äi+s(615) 741-4140

[email protected]

Type of Action on Rule:

X Stay of Effective Date of Rules

Rule Filing Date: A5/09n7

Rule Original Effective Date: 0B/07n7Length ol Stay (not to exceed 75 days): 75 days

New Ëffective Date of Rule Filing. 10/21/17

Notice of Withdrawal of Stay

Stay Filing Date:

Stay Effective Date:

New Effective Date of Rule Filing:

(mm/dd/vv)

(mm/dd/vv)

furn/dd/vv)

Notice of Withdrawal of Rules

Rule Filing Date

Rule Effective Date

(mm/dd/vv)

(mm/dd/vv)

Rule(s) (ALL chapters and rules contained in filing must be listed here. lf needed, copy and paste additionaltables to accommodate multiple chapters. Please enter only ONE Rule Number/RuleTitle per row)

Chapter Number0400-12-01

Ghapter Title

Rule Number4400-12-01-.02o4oo-rz-or- os

0400-12-01-.1 0

Hazardous Waste ManagementRule Titleldentification and Listing of Haza¡dous Wastelnterim Status Standards for Owners and Operators of Existing Hazardous WasteTreatment, Sto¡age, and Disposal FacilitiesLand Disposal Restrictions

SS-7041 (July 2014) RDA 1693

Date:

Signature:

Name of Officer:

Title of Officer:

0 17

Kasey hburn

Legislative Attorney

lly 0ommission


and sworn to before me on:

Notary Public Signature:

My commission expires on:

?JÐ ?r2t1

slnlætq

Filed with the Department of State on:

Tre HargettSecretary of State

2SS-7041 (Juty 2014) RDA 1693

Department of State Division of Publications


Sequence Number: ~ 0~9~""~1~\ -_\~'1--~--312 Rosa L. Parks Avenue, 8th Floor Snodgrass/TN Tower Nashville, TN 37243 Rule ID(s): -~N~A ___ _ Phone: 615-741-2650 Email : [email protected] File Date: ~ [ ~, ,.._..

Effective Date: 't / 3:j fl

Filing Form for Stay of Effective Date on Rules, Withdrawal of Stay, and Withdrawal of Rules

- - --- - - - - - ·------- -Agency/Board/Commission: Underground Storage Tanks and Solid Waste Disposal Control Board

- - -- -Division: Solid Waste Management

Contact Person: . Jackie Okoreeh-Baah -

Address: William R. Snodgrass TN Tower 312 Rosa L. Parks Avenue, 14th Floor

_ t:-!_a_shvJ lle, Tennesse_e Zip: 37243

Phone: (615) 532-0825 - -- - - - -

Email: Jackie.Okoreeh-Baah@tn .gov

Type of Action on Rule:

X Stay of Effective Date of Rules

Rule Filing Date: 05/09/17 (Seq.# 05-07-17) (Rule ID 6521)

Rule Original Effective Date: 08/07/17 (Stayed by JGOC to 10/21/17)

Length of Stay (not to exceed 75 days): _7_5 __________________ _

New Effective Date of Rule Filing:: 01/03/18 ---------------------

Notice of Withdrawal of Stay

Stay Filing Date: _(._m_m_/i_d_dl_,,_y.,,__y)'-----------------Stay Effective Date: ~(m_m_/i_d_d~1/Y~Y~) _______________ _

New Effective Date of Rule Fi ling : ~(m_m_/i_d_d~1/y~y~) _______________ _

Notice of Withdrawal of Rules

Rule Filing Date: ~(m_m_/i_d_d~1/Y~Y~) _______________ _

Rule Effective Date: (mm/ddlyy) ~--~----------------

Rule(s) (ALL chapters and rules contained in filing must be listed here. If needed, copy and paste additional tables to accommodate multiple chapters. Please enter only ONE Rule Number/RuleTitle per row)

Chapter Number Chapter Title ' 0400-12-01 Hazardous Waste Management

Rule Number Rule Title 0400-12-01-.02 Identification and Listing of Hazardous Waste 0400-12-01-.05 Interim Status Standards for Owners and Operators of Existing Hazardous Waste

Treatment, Storaqe, and Disposal Facilities 0400-12-01-.10 Land Disposal Restrictions

SS-7041 (July 2014) RDA 1693

d,10, H • IIIJJ l1

,,,,, . ""OL L '',,, ..:.\ c., ~ ••• ft • G _,,{'

........... • • e, • '!It - ~~ .... , ...

: : S ,,4,1:: ·.o ~ Date: _SE_e~t_e_m_b.....,e,_r ~6.---, 2_0_1_7 ____________ _ : • r-c- Of: • f1' ~ J \ -: • cfVN.c::-s • : Signature: ' y - o • ~, ...;, Sc::- • - - ----,"''f-"-'--~.~----------------~ y • •vo7:4R ...;f:: • : ::%··. PuE3'-tcY .: . §aame of Officer: _J_e_d_L_._L_,_y_n_n _______________ _

... :,..,t.PO • • • • ..... ~ ,," ··, IV' • • ••• '\<v'~ ,, ',,,, Cou N1'i, \\,,, Title of Officer: ' 11 ,11111111 1\ ----------------------

Chairman

Subscribed and sworn to before me on: - -+-~+''-L--/ ~~----fl---'-//_1_ ---;-- -----..-----~. __ _ Notary Public Signature: - ~( .... __ ~~====-=---cf!_:__• __ {b_..:_~~---=--=------

My commission expires on: ---~-----'---=----'---''----3---,/,__.:>._ a_al_ O ____ _


11'

C , l..Li ,., .,. l-l-.

ro

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Ow (/)

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i.JJ \-

~ u-:1 (n -;;-:

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_.;":(.

c .. --

SS-7041 (July 2014)

Filed with the Department of State on: ____ q-+(_-=1--'-+l l'-'~L.._ ______ _

2

I Tre Hargett Secretary of State

RDA 1693

Tennessee Secretary of State

Tre Hargett

Cody Ryan York Director of Publications

Mr. Wayne Gregory Office of General Counsel Environment and Conservation 312 Rosa L. Parks A venue

Publications Division

3 12 Rosa L. Parks A venue, 8th Floor

Nashville, Tennessee 37243-1102

September 12, 2017

2nd Floor, William R. Snodgrass Tennessee Tower Nashville, TN 37243

Dear Mr. Gregory,

615-253-4564 Cody. [email protected]

The 75-day stay that we have assigned sequence number 09-11-17 has a typographical error in the new effective date. The effective date after the 75 days was miscalculated. The true effective date of these rules will be January 4, 2018.

If you have any questions, please feel free to contact my office at 615-741 -2650.

Cody Ryan York Director of Publications

sos.tn.gov

rulemaking hearing rule(s) filing form...2017/07/05 · pursuant to tenn. code ann. 4-5-229, any...

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