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SAMPLE DATA PACKET
u.0. CJ^VIKVJI^WICJ^IAUL. r-K.\-» i c,»-HVJPI rvvziLPi^iCLP Sample Management OfficeP.O. Box 818 - Alexandria, Virginia 22313Phone: 703/557-2490 - FTS/557-2490
SPECIAL ANALYTICAL SERVICEPACKING LIST
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Sample Sample Description Sample Condition on f-Numbers Le., Analysis, Matrix, Concentration Receipt at Lab
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Sampling Date(s)://;-JL-^
Date Shipped:/^-J-^Site Name/Code:
Ship To;£'A/^KcafyA/i^£FA/^A/c^I S . I f f i l LftCi^l^^b ^i>'Sr Louf<, / //^ 63/^i-
Attn:"DR'.|f1fW^FrC.^ / rJT^^
SAS Number^^- /^
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White - SMO Copy, Yellow - Region Copy, Pink - Lab Copy for return to SMO, Gold - Lab Copy
Sample Number,
l ^ lOrganics Analysis Data Sheet
(Page1»
Laboratory Name: £)U^lg^-^^X=^ SnO^ Case No: r$/<^ ••^^JV-7',„- ^^>a^^ Q QC Report No:Lab Sample 10 No:
Sample Mairix: l.l-)\'fff^ ConlractNo: .5AS /^ - S^S ^
Data Release Authorized By: ^.ai^L^lM^- Date Sample Received: ^0-^' - S^
Volatile Compounds
Concentration: Cowy Medium (Circle One)
Dale Extracted/Prepared: ___ _ —- •'••;——
Dale Analyzed: _
Cone/Oil Factor: -pH.
Percent Moisture: INot Decanted)-
CAS '\ ug/lorug/KgNumbar '•s^ (CirckOro)74-87-374-83-97S«-47S-00-37S-09-267 4.17S-1&075-35-*75-34-3156-60.567-66-3107-06-270-93-371-55-656-23-6108-OS-475-27-4
Chloronietham^Bromornethane ^^Vinyl Chloride '\ChloroethaneMethyfent ChlorideAcetoneCarbon Oisuiridc1.1-DichlorOfthene1.1-OichloroethaneTrans-1.2-OichloroetheneChloroform1.2-Oichloraethine2-Butanone -1.1.1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloroniethane
-\
^
CAS ua/torua/KsNumtMf (CireftOif)78-87-5100G1-02-679^)1-6124-48-179-00-S71-43-210061-01-S^10-75-87SSS,-2lOB'-lO^591-78-6 ''127-18-479-34-5108-88-3108-90-7100-41.4100-42-5
1,2-OichloropropaneTrans* 1.3'OichloropropefieTrichloroethweDibromochtoromethane1.1.2'TrichloroethaneBenzenecis-1.3-Oichloropropene2-ChloroethylvinytetherGromoform4-Methvl.2-Penianone^HexanoneTetf ctfloroethene-1,1.2.2^Te|rachloroethaneToluene \Chlorobemene s.Cthytbenzene , ^S^StyrefieToial Xytenes
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11/85
Laboratory Name: £M^ l«5-bPVM(7
Case No: ^^ F
,. _ Organics Analysis Data Sheetr (Page2>
Sorruvolatile Compounds
Concentration: /^mfi Medium (CirdeOne) GPC Cleanup OYe» Ofio
Date Extracted/Prepared: IG/^ / •g(o
Date Analyied: IQ / ! { » /•f,l^
Cone/Oil Factor; ______ULO-Percent Moisture (Decanted)-.
Separatorv Funnel Exiraction OYes
Continuous Liquid • Liquid Extraction QYes
Numlxr (Circl* On*)t08.9S-2111^4-49&-S7-8541-73-1106-46-7100-51-69S-SO-195-48-73963B-32-9106.44-5621-64-767.72-138-95-378.59-188-75-5105-67.965-8501 1 1 - 9 1 - 1120-83-2120-82-191-20-3106-47-887-68.359-50.791-57.677.47-488-06-295-95-491-58-788-74-4131-11-3
208-96-899-03-2
Phenolbis(-2-Chloroethvl)£ther2-Chloraphenol1.3-Oichlorobeiuene1.4-DicnlorobeitteneBeniyl Alconol1.2-Dichlorobenxene2-Meihylphenolbis(2-chloroaopropv1)Ether4-Methvlpheno:N-NiirotO-Oi-n-PropvlamineHexacntoroethJneNhrobenzeneIsophorone2-Niirophenol2. 4-DimethytphenolBeruoic Acidbis(-2-Cl)loroe(rM»v|Me(hin«2.4-Dicnloropnenol1.2.4-TrichloroberueneNaphihJiene4-ChloroanilineHeitachlorobufdiene4-Chloro-3-Me<hY<phenol2 -MeitiYtnaphihJieneHctachlotocycloptnua.eni-2.4.6.Ttichtorophenal2.4. S-TfichlofOphenol2-Chtotontphthaltnt2-NitrwnilineDirntlhyf PhltuUie
ActfUonthyterK3-Nur<Mn4line
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CAS uu/iurug'KgNumixir (Cin:l«0n«
83.32.951.28.510002-7132-64.9121-14-2606-20-284.66.27005-72-3B6-73-7100-01-6534.52-186-30-6101.55-3118.74.117-86-585.01.8120-12.784-74.2206-44012900085-68-791-94-156-55-3117.81-721801-9117-840205-99-220708-9iO.32.8193-39-5>3-70-3
191-2<-2
Aceruphth«ne2.4-Oinhrophtftot4-NftrophenolDibenzofuran2,4'Oirutrotoluene2,6-OinitrotolueneDieihylphthatale4-Chtorophenvl-phenyfeiherFitforenf4-Nftroaniline4.6-Oinilro-2-MethytphenolN-NitrosodiphenylamirwOt4-Bromophenvl-phenyleiher•<exach{orobenzene"enHchlorophcnolPhenanthreneAnthracene3J-n-ButyfphthJ t^teFiuoranihenePyreneButYlbcniv<phtha late3. S'-DtChlofobcnztdineBenzo(a(An|hrace"cbi$(2-ElhylhexYlK*"*"al3'cChfysene3<.n-OctY< FhihalaleBenu(b IFfuora mhe neBeruo(k)Fluor« nihene3emo(aK\fen«Endeno(1.2. 3-cdlPvreneDiberufa. h»AmhfaceoeBetuofq. h. J)Pery(ene
5600
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7 85
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<-.„ >...- ^4 q «, F"Organics Analysis Date Sheet
(Page 4)
TorHativaly Idantifiad Compounds
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Dilution Factor; ^dnTiTOutput File: *(S257!:L2Data File; >(»257::E2Na«: 2493F-08Misc; Lit 5996 8600273; 3101-2493F
10
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Cotpound B.T. Scant Area Cone Units q
1) '04 1,4-D1CH-11R06E1CENE B.18 490 143960 40.00 UE/MIPE 942) 2-FL10WHENOL (SURROMTE) 5.33 213 211634 A^-tiMIPE 1004) •D8 WPHTHaflC 11.83 845 347300 40.00 U6/UIPE 1007> •010 MBWHTreC 17.25 1370 183112 40.00 DG/yiPE 1008) 2,4,6-TRIBCTIOPHENOL (SURfil 19.72 1609 14202 t«^4-W>WtE-400
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( Sample Number
^^g^ Organics Analysis Data Sheet
(Pagel)
Case No: ^\Ql-^^S/--Laboratory Name:
Lab Sample 10 No: QC Report No:Contract No:Sample Matrix:
Data Release Authorized By: ^O^&QMJt Q. VlJtM^ Oate Sample Received:
Volatile Compounds
Concentration: <^w/) Medium (Circle Onel
Date Extracted/Prepared:
Oate Analyzed: _
Cone/Oil Factor: -pH-
Percent Moisture: (Not Oecanied) -
GAS \. ug/lorug/KgNumber ''< (CirctoOne)74-87-374-83-976-01.47S-00-375.09-267-C4-175-<&<75-35-476^4-3156^0-567-66-3107-06-278-93-371-55-656-23-5108-05-475-27-4
ChktromethanejfonjOmj lhJncVin»< CMorio*,Chloreelhane \,Methylene Chloride '\Acetone ''Carbon Oisulfrie1.1-Oichlonwthene1.1-OichloroethaneTrans-1,2 ichloroeth«neChlorofomi1.2-Oichloroethtnc2-8utanone1.1.1-TrichloroethaneCarbon TetraehlorideVinyl AcetateBroniodichlorometha ne
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CAS ua/lorug/KgNumlw (Cireto0n«|78-87-510061-02-679-01-6124-4S-179-00-571-43-210061-01-5110-75-87S-2S-2108-10-1S»^78-6127-i»479^34-5 108-88-3108-90-7100.41-4100-42-5
1.2-0*chl4ropropaneTrans-1.3-DtchloropropeneTrichloroetheneOibromochkiFomethanel.l.2-Trichloroethan«Benzenecis-1.3-Oichloroaropene2-OMoroetWwiyfeltw8ronMform4^UlethYl.2.Pentanone244exanoneTelnchloroeihene1.1 . 2.2-Tftnchloroethanetbh(eneChlor henzeneElhvlbenieneStyrene \Total Xytenes \
-
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•.••<" -»t
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11/85
Laboratory N.me: _£N • • • e-ObYNg-
Case No: _________c.^\^Sampta Number
a-4q3F- oqOrganics Analysis Data Sheet
(Page 2)
Smnrvolatile Compounds
Concentration: (Sow) Medium (Circle One) GPC Cleanup OYet Offio
Date Extracted'Prepared: \0/^/'!ita_______ Separatory Funnel Extraction OYes
Date Analyzed: _____10- llg-^^_______ Continuous Uquid - Liquid Extraction GYes
Conc/Dil Factor: ___________S___________
Percent Moisture (Decanted) ______________
Number (Circte On«l108.95.2U1-M-493-57-854t-73-t106-46-7100.51-6- -95-50-195-48.739638-32-9106-44-5621-64.767-72-198-95-37B-S9-188-75-5105-67-965-85-01 1 1 - 9 1 - 1120-83-2120-82-191-20-3106-47-887-68.359-50-791-57-677-47-488-06-295-95-491-58-788-74-41 3 1 - 1 1 . 3208-96-899-09.2
Phenolbis(-2-CM(XOtlhv»)£lh<r2-Cnlorophenol1.3-DichlOfObenzene1.4-OichlorobenzeneBenlyl Alcohol1. 2-Oichlorobeniene2-Meitivlohenolbis(2-chlon»fOBropYl|Ethcr4-M«hylpheno!N-Nilro*o-Oi-n-PropY**""neHexJchloroethaneNitrodenunfIsophorone2-Nilrophenol2. 4-OimethvlphenolBemoK Acidbisl.2-ChloroettioxY|Meirune2. 4-OichlorophenolI. 2.4-TrjcMofObtn2eneNaphlMlcnc4-ChloroanilineHeK«chloroburd«ene4-Chloro-3-Metnvlphenol2 -M«tnylnJphthJleneKeiuichlorocvclopentadtene2. 4. 6-Tnchloropnenol2. 4. 5-T(ichlwophcnol2-Chl«ron*Dhilulene2-NinunilineOio>elh»l PhtlulneAcenJpri1hy(«ne3-Nnroaniline
1 0 0
1 0 0
1 0 0
1 D 0•son
CAS
13-32-951-28-5100-02-7132-64-9121-14-2606-20-264-66-27005-72.386-73-7100-01-6534-52-186-30-6101-55-3118-74-1>7.86-5
85-01-8120-12-784-74-2206-44-0129-00-0)5-68-791-94-156.55-3117-81 -7218-01.9117-84-0205-99-2207-08-9SO-32-8193-39-5i3-70-3191-24-2
teenaptiihene2.4-Dinhrophenol4-NftfOphenot)iberuofur«n2.4-Oinnrotoluene2.6-DinnfotoluencOleihylphihalale4-ChlOfophenYf-phenytether^uorene4-NrtrMniHne4,6-Dinhro-2-Methyfpherwl
-NitrwodiphcoYlannne ( 1 14.Bro«nophenyt-phenvleihef•te>cachlorobenzene'eniachtorophenotPhinanlhreneAnthracene3i.n.6uly1phlh»(ateFiuofanitienePyrentBulytbeniylphthalale3. 3••D^chlofOt><tn^tdlneBeruo(a»Anihracenet»is(2-ElhYlh<xvl|Ph1h3laTCChrYseneD*-o-OciY« PhthalateBenzo(blFluofa nihe ne8eiuo(klFtuora nthcneBeruo(a|Pyrer»elnd<rw(1.2.3-cd)Pvfen*
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(CJrcl* On*
500
(1H^*w*M be ««o«"l*d *'o«" d'ph»"vl*"ww
<7-85
Organics Analysis Data Sheet(Page 4|
TanOtivoly Idantifiod Compounds
CASNunrtwf
•I^3
<S
K
•r
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13
1A
•IS
16
17
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27
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QUANT REPORT
Operator ID: USERS Quant Rev: 4 Quint TiM;Injected at:
Dilution Factor;Output File: W54: :L2Data File; >ft5254:;E2Hat: 2493F-09Misc: UC 5996 86012740 3101-2495F
G61020 12:30B61016 02:40
1.001)
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t O F i l e : W248;:D3Title; ID F1L£ FOR SAS 3101-2495FLast Calibration: 861020 11:54
Coipound R.T. Scant ftrea Cone Units q
1) "04 1,4-CICH-uROBENZENE 8.17 491 109099 40.00 uS/HIPE 952) 2-FLUOIWlCNa. (SURROGATE) 5.59 241 135952 86.13 U6/MIPE 1004) '06 WWWLENE 11.81 844 246434 41.00 U6/HIPE 1007» «D10 HCDWHTHENE 17.20 1365 129711 40.00 U6/UIPE 1008) 2,4,6-TRIBRDnnPlCNa-(SURR) 19.70 1606 119123 198.19 U6/UIPE 100
11) •D10 PHENflNTHSNE 21.65 1793 389674 40.00 UE/U1PE 101)
• Coipound is ISTD
TOTBL ION CHROMBTOCRBM
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SBHPLE SPECTRUM 1BBCKCROUHD SUBTRflCTED)File >flS2S4 ilWT-MBpk Bb E28B5 1"SUB
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Cttpound No: 8Coipound Hue: 2,4,6-TiIBEOmPHENOL (SUHi)&m Hoiber: 1606ttlcntion Ti«c; 13.70 •in.Orel: 113123Conceirtrttion; 136.13 t6/tlIPEq-»«lut; 1011
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J Sample Number
b^y--Organics Analysis Data Sheet
(Page 1 )
Laboratory Name: £iOU I Q^-bcet^ FnQ-P: Case No:QC Report No:
Contract No: <S7?-S S/0l-^.</^^-
Oate Sample Received:
Lab Sample 10 No: ^ffQS. 7-^/ \J
Sample Matrix:.Data Heleasc Authorized Ry^ f.T,riAi C. • UJ .'HA
Volatile Compounds
Concentraijon: ^Uw/ Medium (Circle One)
Date Extracted/Prepared: ____
Dale Analyzed: ————— ————-
Conc/Dil Factor:
Percent Moisture: (Not Decanted) _
-PH-
ug/lorug/Kg(Circle On«|
74-87-374-83-976-01-47S-00-375-09-267-64-176-16-07S-3S-476-34-31S6-60-567^6-3107.06-278-93-371-55-656-23-5108-05-<75-27-4
QlforoniethaneBrornorhe{haneVinyl CMoriSeChkrocthane \Mtthyteoo Chloride \Acetone ^>Cuban Oisuffid*1.1-DicrilonethefW1,1-OKhloroetnanaTrans-1,2-OKhloroetheneChlorofonn1.2-Oichloroettunt2-eutanone -I, l.l-TrichloroothaneCarbon TetrachlorideVinvl AcetateBrornodichloroniethane
\"'N^
.
0»t» Repon«ng»For »pontng f*wlt» MI CPA. th« loflowingAdifaiional ftqi wlooinoM* —pl-ninB fid«rMwfon of **eh ftog mu« tw •Ephot.
V—«M H ma r««w(t M J yfw «««M«f lhan •r e uJi la (hft d«MetMn l-nd.f«port ttw wlue.
id wn MufyMd to* bw no( «te*«cMd. ftaponthe* bmH lor lh« «ww4* wth Itw U (•.«. 1(U bMWM*trft(MH/**«MiO«1 •OiOA. <ThJ> ta n« nMKCMilV
f "tWynwN tfctoaiMi *imH.» Tfw IOM«*M« chauM rwtf: U-
CAS UB/locua/Kg (••vjNumber (Cird» OrrI .-. .78-87-510061-02-679-01-6124-48-179.00-571.43-2100614)1-5110-75475-25-2108-10-15X^6127-18>479-34.5 108-88-3108-90-7100-41-4100-42-5
1.2-OichloropropaneTrans-1,3-DichloropropeneTrichloroethencObromochlorometnane1.1.2-TrichloroethtneBenzenecjs-1.3-Oichlonipropene2-Chloroe(hv<vinyletherBroinofonn4-Mtthy<-2-Pcntat>on«2^1eKanoneTetrachtoroelheoe4.1.2. 2-TetnchloroelhaneTollxneChlorob«nzeneElhytoemene'Styrene \Total Xylenes \
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Fwml 11/85
Laboratory Name: ,£N'' '<^nnVM&
C.seNo:___SdfL
S«np4« Number
^ISF-IOOrganics Analysis Data Sheet
(Page 2»
Semivolatile Compound*
Concentration: (uy> Medium (Circle One) GPC Cleanup OYet QMo
Date Extracted'Prepared: l0/(p / ^(^
Date Analyzed: lO/l^/-^
Conc/Dil Facior: ______L
Separatory Funnel Extraction QYes
Continuous Liquid • Liquid Extraction QYes
Percent Moisture (Oecanled).
CAS uff/ldma/KgNumtxr (Circl« On* I108-95-2111-44-495-57-8S41-73-1)06-46.7100-S1-695-50-195-48-739638.32-9106-44.5621-64-767.72-198-95-378-59-188-75-5105-67-965-85-01 1 1 . 9 1 . 1120-83.2120-82-191.20-3106-47-887-68-359.50-791-57-677-47-488-OS-Z95.95-491-58-788-74-*131-H-3208-96-899-09-2
Phenolbis(-2-Chloro«hYf|Elhtr2-Chlorophenol1. 3-Dichlorobefucne1. 4-DichlorobenxeneBe iuv< Alcohol1,2-0ich(orobenzene2-Methvfphenolbis(2-chloroisopropYl|Elner4-Methylpheno!N-Nttroso-Oi-n-ProovfJinineHenachloroeirianeNilrobenreneIsoplwow2-Nhrophenol2. 4-DimtthyfphcnolBcruoic Acidb<s(-2.Chlo'otthoxY|Melhane2. 4-Dichloropheno!1 . 2.4-TrichlorobenieneNaphthalene4-ChlofoaoihneHexachlorobutadiene4-Chloro-3-Melhylphenol2.M«lhv1naptithJleneMeKachlOfocYClopeoiadiene2. 4.6-Tnchlorophenol2. 4. 5.Trichlorophenol2-Chloforuphltulene2.Nilroani(ineOuneihvl PhihiHieAcen«phthy1ene3-Nilroamlin«
10 0
-
1 0 o
1 0 0
1 0 00.-1 ^
CASNumb«r13-32-9
51-28-500-02-7
)32-64-9121-14.2606-20-284-66-27005-72-386-73-7100-01-6534-S2-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-444129-00-0B5-68-791-94-156-55-31 1 7 . 8 1 - 7218-01-9117-84-0205-99-2207-08-950-32-8193-39-5S3-70-3191-24-2
AcenJphihene2.4-Oiniiropherwll.Nrtfophenol)ib«fuofuran2.4 •Oinitrotoluene2 6-DmhrotolueneO.«thyfptnhat2t«4-CMorophcnyl-phenvlcther^uorene4-Nitroani(irx-4.6-Oiniiro-2-M«thy1pher.o(
.Nilre$odiphenY<»mine < • )4 -Bromophenvf-phenvlelher^exach^o^obenrencPentachlorophenolPhen«nlhfeneAnthraceneD<-n-BuiylphihalaieFluoranthenePyreneBut-<fbeniYlphlhal<ie3 3'-0ichlorobent«<iifteBentofa AnthracenelMri2-Elhylhc«vl»PhlMla»Chfvsene0<-n-0civ< PhihalateBeruofblFluorxni heneBenzo(k)Fluof«ntheneBeiuo(a)Pvronelodeno(l. 1. 3-cd»PvreneOiberu(a. htAnibraceoe
MI .'1 ot-nB^KB(CuclfOni
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| Smpio Number
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Organics Analysis Data Sheet(Page 4)
Tanlativoly Identifiod Compounds
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M
19
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Ouint Rev: 4 Quant Tine:Injected it:
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Cinpound R.T. Scant Area Cone Unitf q
1) •04 1,4-DIOURuBENZErC 8.22 499 198255 40.00 UE/tlIPE 932) 2-FUX1ROFHENOL (SURROHffE) 5.92 276 211494 73.74 U&tllPE 1004) •M WHTHttBC 11.B1 846 4<i8655 4C.OO UK/WIPE 1007) •OH fICENMWtBC 17.21 1370 231353 40.00 UG/WIPE 1008) 2,4,6-TlilBROMOPHENa. (aDR) 19.68 1610 93979 B7.66 U6/IIIPE 100
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Cenpoand N0: 1 (I5TDICopound Hue: M 1,4-DICHLOEOBEnZEnEScin Ncaber: 499Betention Tl«e; 8.22 «n.ftre.: 199255Concentrttton: 40.1111 U6/UIPEq-ualoe: 93
BTL122
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BTL122
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CoipQand No: 4 (ISTD)ConpoBiiJ Hue: SS NAPHTKRLENEScan Nniber; 848Ectention TiM: 11.81 •inftrcB: 468855Concentration: 40.00 UG/UIPEq-valm: 100
BTU22
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BTL»22
REFERENCE STHNBRRD SPECTRUMF i l t > B 2 i e i 1998 48 PPM STD 1 S c * n 1S86Bpk At> 8SS8 Sl»6 16. B7 mn.
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Data File; >ft5355::GHue: 2433F-10Misc: MC 5396 B60t!741 3101-24S3FQutirt TiM: 861020 12:31Injectfd it: 361016 1)3:28
Coipoand Ho: 10Cotpoiind HMM ; 2)4,5-Trichloropliei«)lScan Hadxr; 11B3Eetention TiM: 15,28 •in,ftren; 1BS1Concenlrttion: .62 U6/HIPEq-ualne; 63
BTll22
Sample Numb«r
L^?^ lOrganics Analysis Data Sheet . '.
(Rage I)
oryName: <^AJ / .JW^ ^n(3 case No: 1^/01-^•3
^<nCQS{^ 0Laborai
Lab Sample ID No:
Sample Malfix: ^<-31'0'£.
Case No:
QC Report No:
Contract No: ^ S ^/^/•- -<^3•/=
Dale Sample Received:Oata Release Authorized By: )fAQt.raOAtA- C. lUtU i
Volatile Compounds
Concentration: ^owV Medium (Circle One)
Dale Extracted/Prepared: _
Dale Analyzed: ——— _
Cone/Oil Factor: ——————————pH .
Percent Moisture: (N01 Oecanied)
CAS ug/lorug/KgNumbw (Cirelt OrM)74-S7-374<3-9~~~~76-01-475-00-375.09-267.64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23^5108-05-475-27-4
ChloromethaneBromo<nethaneVinyKHIorKteCWoroaIhirte^MtthylenaCliloridi'-Aceiorw "-'Carbon Oisuinde1.1-Oiehloroethene1.1-OichloroetturKiTrans-1,2-OichloroethtneChloroform1.2-Oichloroethane2-Butanone1.1.1-TricriloroetrianeCarbon TetnehlorkleVinyl AcetateBromodichloramethane
'--''--
CAS uo/lorua/KgNumber (Cireto OrrI78-87-510061-02-679-01-6114-48-179-00-571-43-210061-01-5110-75-87S-2S.2fea.JO-1591-78 ,127-18-479-34-S108-88-3 -108-90-7100-41-4100-42-5
1.2-DichloropropaneTnins-1.3-OichloropropeneTriehloroelheneObromochlonnnethano1.1.2-TrichloroethaneBerueriecjs-1.3-Oichloropropene2-ChloroethylvinyletherBromolorm4-Met»yl-2-Feritar»ne2-Heianone9<trach(oroelhene1. l7'2>2-TetrachloroethaneToluene '\Chloroberuene'Ethvlbenzene .'s^Styrerx \Toul Xylcnw
'
\,
r ' 3COra0"-I0
; 10 EPA. «*• Mtoiiwr M«M*U •.wMiw f WMd.rilihl f •fteoura^d. Hmnn -r. ih*
V|«<M M ihe nesuft n a vJua «rut«r itut •r •wf M th« ««we*ian 1—1. C Th-llfir«WI ft** *4lu« b—A OOftI r GC/MS. S«H I CW«»P<N» < »wc*dM>10
- IIHMI lor Hu iMiipto wtti •f U (•4, lOUIfciWI
t hmitJ Th« <,»mM. •hwM rw* U*Compound we uuivnd (M but •«M •l«<>c««4. rh* n
fc**e»»*» M •Mimaned wiJuw. Thta (tog «mimMMff • conewHrM*«t («« Hnm..1y .
cri«Mi« 1^ ttw fw^ « l.m MM llw w«cj|* •MM«iMl ••MI »«(fM-lhf—fLC-c.iaJL KbM«4dfe«w-.clOp«/<«W6MKw*«>w« «4 3 pgi/( - « ew(M«L f^wt — JJ.
& N \ / 1 R-0 PY ( &LJboratory H*
C»»NO: ^^°?
Organics Analysis Date Sheet(Page 2>
Semivolatile Compounds
Concentration: ('S^5 Medium (Circle One) GPC Cleanup OYet tSHio
Dale Extracted'•Prepared: IP/b /"g I?_______ Separatory Funnel Extraction OVes
Dale Analyzed: _____^0 /lb/'6tx?________ Continuous Liquid - Liquid Extraction OYes
Cone/Oil Factor: ______!______________
Percent Moisture (Decanted)-
CAS " ug,i|ijiuui'Kfl"Number (Circl* On*)108-95.2H1-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64.767-72-198-9S-378-59-188-75-5105.67-965-85-01 1 1 . 9 1 . 1120-83-2120-82-191-20-3106-47-887-68-359.50.791.57.677-47-468.06-295-95-491-58-788-74-*1 3 1 - 1 1 - 3208.96.899-09-2
Phenolbis(-2-ChtofOClhvt»Ether2-Chloroctwwl1.3-Oichlorobenzene1,4-0ich(oroberueneBeniYl Alcohol1.2-Oichlorobefuene2-Meihylphenolbis(2-ch(orotsopropvl lEther4.Methy4>henofN- Nitroso-Ot •n-Propy<J mineHe ka chloroethaneNitroberueneIsophorone2-Nitrophenot2. 4-Dimethyl phenoleenzoic Acidb<s<-2-ChforoeihoxY)Meihane2. 4-Otchloroohenol1 . 2. 4-Tr(ch(ofotxmeneNaph|h«1ene4-ChloroanilfneHexachlorobutadiene4 -Chloro-3 - Meihytphenol2-Me1hv1n»phiha<en<He xachlorocyclope nia diene2. 4. 6-TftChlofoohenoI2. 4. 5-TftChlorophenol2 •Chloronxptilhafe ne2-NiiroJnilineDuneihyl PhthalaicAcenaphthylene3'Nilro«niline
'p.i.1 .
Ir 0
i DO
1 0 050 U
n l uui-pe'CAS ugAtLua tsNumbar fCircK Or>«)
83-32.951.28-5100-02-7132-64.9121 -14 -2606-20-234.66-27005-72-386.73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01 -8120-12-784-74.2206-14-0129-00-095-68-791-94.156.55.31 1 7 - 8 1 - 7218-01.9117.84-0205.99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaphihene ) 12.4-Oinhfopheoot4-NitropherwlDibefuofuran2.4-Oinitroiotutne2. 6-OinitrotofueneOielhylphihalale4'Ch)oroph« nyl-phenytetherFiLrOrcnc4-NitroaniIine4.6-0«niiro-2-Meth^ph<nolN-NitrosodiphenyOmtne ( 1 14-Brotnophenyl-phenYleiherHeKachlorobenrenePentachlorophenolPhenanlhreneAnthraceneOi-n-Buiyfphihal.ateFtu0f»nlhenePyreotBuivlbenr^phthalate3. 3"-Dichlofobetwid«neBenzo(a |Anthr»cenebi^-EihylhexYOP^'^a^ieChryseoeDrn-Ociyf PhlhalaleBenzo(b)RuorantheneBeiuo(k(Flu<Ka mh«rteBefUO(«lPv»eneIndent 1 . 2 . 3-cd)Pvfe"eOibenf(a. hIAnthfceoeBeruo(q. h. i)Pery<cnc
600
(1hC«n"ot be —fMffd how diptxrty<**"*rt<
7-85
L«bofa.w N.m<=: JS I ' ' IR-DPV\)€- '_
c.s.No-_a^ai_Organics Analysis Data Sheet
(Page 4)
Tontativflly Idantidod Compounds
CASNumlMf
•l^T
3•«
11
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14
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la20
2122-
23
24
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26
27
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OJWT RETORT
Operator 10: USERS Ouant StV. 4 Quant Tine!Injfcted at:
Di lu t ion Factor:Output Fil«! *W256:;L2Data File; >B5256::E2NaM: 2493F-11Iliac: Lit 5996 86002742 3101-2493F
861020 12:33861016 04:1;
1.000
BTLt23
10 File: »W24B!:D3Ti t l e : 10 FILE FOR SflS 3H1-2493FLast Calibration: 861020 11:54
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8.165.46
11.8017.2119.7021.65
491229845
137016121801
65;0176101
170306144542135674516295
40.0080.3140.0040.00
202.5640.00
Ue/M!PEUGAIIPEU6/mPEDe/wireU64(IFEuG/tlIPE
91100100100100100
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Coipimni No; 1 (ISTII)_ _ CoipoiindntM: D4 1,4-BICHLOBOBENZiNE
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Cnpound No: 2Cnpoand HIM Z-FLUOMPHENOL 0)U!0«flTE)Scan Noiiber: 2:9Eitention Tiw: 5.46 >in.BtBa: 76101Concentration: 80.31 UG/UIFEq-valne; IflO
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Coipoand Ho: 4 (ISTD)dnpoand IbM: M NAPXTHALENEScan tfaliber: 84SBetention TIM: 11.30 *in.Arg<: 171306Concentrttitn: 40.01 IfS/UIPEq-valw: 100
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Dtta File: >a5256:;E2Noe; 2493F-11Hisc; UK 5996 B6GB2742 3101-2433?ijaant Tile: 861020 12:33Injectfd it: B610I6 04:15
COTpoand Ho: 7 (ISTO)COTpoand Hf»: D10 flCDWKTMBffiScu NBber: 1370Bitintion TiM: 17.21 tin.RreB: 114542Concentration; 40.00 U&/UIPEq-valae: 100
BTU23
Fil. >B0457 NVO H1384 ME! LVL Si.An.244eBpk Bb
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Coipoand No: BCupoand NaM: 2,4,6-TlIBIiOHOPKiX)L (SUM)Scan Nmber: 1E12Ketention TIK; 19.70 •in,Area: 135674Conctirtrttion: 202.56 OS/IIIPEq-valae: 100
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CoiMnnd No: 11 (ISTO)Cnpoani Nae: DID PKINfiNTHEBffiScan Nimber: 1801Betention lim: 21.65 •in.fliea: 516295CoTicenttiticin: 40.00 OG/UIPEq-value: 100
BTL123
Laboratory Name: ^JUUl d^^OF. FD^?.
Lab Sample 10 No: ^OQS^^ ^
Sample Matrix: iL>l<p^_______________ Sf^ SIOt-^93 ^Dale Sample Received: ——/0/^/y6Data Release Authored By: JpyXr^Jyft. Uj\A \
Volatile Compounds
Concentralion: <ow) Medium (Circle One)
Dale Extracted/Prepared: .
Dale Analyzed: _
Cone/Oil Factor: -pH-
Organics Analysis Data Sheet(Page!)
f^l<31 --^1^3^
Percent Moisture: (Not Decanted)
'~CAS ug/lorug/KgNumte«< (CircteOrrI74^7-3 •74-83-976-01.475-00-37S09-267-64-17S-IS-07S-3S-475^4-3166-60-567-66-3107-06-278-93-371-55-656-23-5108-05-475-27-4
•Qilonxn«thaneBluntomaihaneViny< ChlorioaChloRMthane ' -MelhyteneChlgride ~ -AcetocwCarbon OitulfKia1.1-Dichkxothene1.1-OicMoroethana^fTrans-1.2-OtChlaroetheneChloroform1.2-OichloroiHhlne2-Butanone -1 . 1 . 1-TrichloroelhaneCartoon Tetrad ilorideVinyl AcetateBromodichlorecnethane
's^\^
'*
CASNumtKf78-87-510061-02-679.0»-6124-48-179-00-571-43-210061-01-S110-75-8^5-25-2108*10-1591-7a-6~s,127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
1.2-0ichloropropan«Trans-1.3-OidiloroprapeneTrichlotOttheneOibnxnochkxoniethane1.1.2.TrichlBn)ethan«Benzenecis-1,3-Dfchloropropene2-ChloroetrrrlvlnyletherBrofoolorrn4-Methyl-2-Pentinon«2-HexanoneTt!racrilon>ethene1,1,''2> -Teirachloroethan«Toluene \ChlorobenieneEthyfbenzene ,' \Sivrene "\Total Xylenes
0
0ug/lorug/Kg
(Circle One)
.
'
'\
fonnl 11/85
Laboratory Name: feN • • >^DV^^_
CaseNo:_^^LiJ-
Organics Analysis Data Sheet(Page 2)
Concentration: /Low) Medium ,_.._.
Date Extracted'Prepared: i&^ /'81^
Date Analysed: in-Ho -'^fe'
Cone/Oil Factor:
Semivolatile Compounds
(Circle One) GPC Cleanup DYct Otto
Separatoiv Funnel Extraction OYes
Continuous Liquid - Liquid Extraction QYes
Percent Moisture (Decanted)-
CAS * MfM^rayrKyNumb«r (Circl* On*)108-95-21I1.A4-495-57-8541-73-1106.46.7100-51-695-50.195-48-739638-32-9106-44-5621.64-76W2-198-95-376-59.188-75.5105-67-965-85-01 1 1 . 9 1 - 1120.83-2120-82.191-20-3106-47-887-68-359.50.791-57-677-47-488-06-295.95-491-S8-788-74.4131-11.3208-96-899-09-2
Phtnolbis<-2-Chlotoethvl|EthtT2-ChlwoQhtnol1.3-Dichloroben2ene1.4-OichlorobenzeneBenzvt Alcohol1. 2-0ich(orobenzene2-MethrlphenolbH(2<hloroitoorooyllElher4-MeihrtihenolN-Nhroio-Di-n-PropvfamintHeuchlotMlhlneNitrabeiu«n6Isophorone2-Nnrophenol2. 4-OiinethrlphenolBemoic Acidbis(-2-Chloroelhoi;v|Melhane2. 4-Oichlorophenol1.2.4.TrichlofotienzeneNaphthilene4.ChloroanilineHeKachloroburdiene4.Chloro-3-Methvlphenol2 -MttnylnaphihaleneHexachlorocvciopentadiene2.4. 6-Trichlorophenol2.4. S-Trichlorophenol2-Chloro<uphthalene2-NtrunilineOimeihrl PhthiteieAeeiuphthylene3-Nitroaniline
>0 0
\ou
lou
1 0 L»soo
CASNumber13-32-9
S1-28-S00-02-7
132-64-9121-14-2606.20-284-66-27005-72-3B6-73-7100-01-6534.S2-116-30-6101-55-3118-74-187-86-585-01-8120-12.784-74-2206-44.0129-00-085-68.791-94-156-55-3117-81.7218-01-9117-840205-99-2207-08-9iO.32-8193.39.553-70-3191-24-2
Ac*Mphlh<ne2.4-D*nhropheno(4-NhrophenolOibenrofurin2.4-Oinitrotoluen*2,6-OinitrolofueneDi«thv<phttula»4-Chloraphenv(-phenyte<herFfuorene4-Nhroaniline4.6-Oinitro-2-Melhylph«nol»l.tli<r<»<>diphei>Yl«""nt ( 1 14-Br(inKioh<nvt-phenyleirierHemchtorobenienePeniachlwophenolPhenanthreneAnthrfceneDi-n-BulylphlhJialeFluoranthenePyreoeButylbenzY<«'"'""«3. 3"-DichIofObe"»idineBeruo(a)Anthracenet)lt(2•ElhYl^'e«Y^^f'hIt"l'^<ChryseneOi-n-Octyl PtithJiale8*nio(b)fluoranlhene8enio(klFluonn<hene8tnn><a)Pvt«ntIndenod. 2- 3-cdlPY'eneDibeiuli. htAnihraceneBfiuiKg. h. ilPefytene
(Circl* Om
AO U
(1 hCannot be ««ow»l«d horn d>ptMfiyt«m«ne
7--85
SMnpteNii
^^F-1'2-Organics Analysis Data Sheet
(Page4»
TmilBtivoly Identifiod Compounds
CASNumlf
^3.
13
1B
19
TO
5173
23
24
T.
26
27
28
M
30
CompcMM*d Nun*
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Fwm 1. Pan B 7 85
Operator ID: USERS Quant Rev: 4 Quint Tile: 861020 12:28Injected it: 861016 01:53
D i l u t i o n Factor: l.OOOOutput File: 'W253; !L2Data File: >1»253!:E2Flaw: 2493F-12Hue: LHC mi 86012743 ?101-2493F BTLt20
ID File: W24a;:03Tit l e : ID FILE FOR SOS 3101-2493FLast Calibrat ion: 8610211 11:54
Cucimind R.T. Scant Area Cone Units q
1) *D4 1,4-DICrLOHBENZHC 8.23 497 236463 40.00 UG/W1PE 942) 2-FLUOROPHENCL (SURROBffE) 5.97 278 215460 62.9B US/WIPE 1BO4) *08 WiPHTrMLENE 11.84 648 523115 40.00 UE/VIPE 1007) •010 ftCEWlPHT}£NE 17.2a 1368 235(00 40.00 U6/UIPE 1008) 2,4,6-TRIBRtHPrEHX (SURR) 19.6; 1606 28140 25.78 UE/VIPE 100
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CoiponTxi No: 1 (ISTB)Ctrpoand HIM: 04 1,4-DICTLOHIBENZEHEScinteiber: 497Eeteirtion Ti«e; B.23 •in.Arei. 236463Concentration: 40.00 U6/BIPEq-ualne: 94
BTL120
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BTL120
Data File; >fl5!53::E2toe: 2493F-12Hi»c: LHC 5996 86002743 3101-2493FQoant TIM: 861020 12:28Injected at: 861016 01:53
Cfltpoand No: 11 (1STII)Coipoand ItaM: D10 FKENWTHSENESon NDdxr: 1798Beltntion TiM: 21.63 >in.ftrea: 427473Concentration: 40.00 OG/HIPEq-valne: 100
BTL120