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sample information an al yzed b ˜˜ : dr . ro ert s p pp s ... · 9 79 2 11. 77 5 11. 92 6 12. 2...

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  • Sample Information An al yzed b ˜˜ : Dr . Ro ert S P pp s ... · 9 79 2 11. 77 5 11. 92 6 12. 2 13 ... 58 96 49 04 8 49. 91 9. 23 3 51 32 2 51 58 2 57 44. 54 7 58 19 0 Sample Information
1
Peak Report TIC R.Time Name Area% 3 0 . 0 l o n e - ) Z ( 3 - x e H 3 8 5 . 8 9.792 Santene 0.84 5 4 . 1 e n e l c y c i r T 5 7 7 . 1 1 4 1 . 0 e n e j u h T - a h p l a 6 2 9 . 1 1 1 0 . 7 1 e n e n i P - a h p l a 2 5 3 . 2 1 4 1 . 0 e n e h c n e F - a h p l a 1 5 1 . 3 1 9 2 . 0 1 e n e h p m a C 5 5 2 . 3 1 3 0 . 0 e n e m y C - o 6 2 4 . 4 1 14.517 Sabinene 0.11 0 7 . 0 1 e n e n i P - a t e b 4 3 8 . 4 1 15.457 Myrcene 1.81 6 1 . 0 e n e r d n a l l e h P - a h p l a 4 2 5 . 6 1 16.680 3-Carene 9.59 8 1 . 0 e n e n i p r e T - a h p l a 3 8 1 . 7 1 0 3 . 0 e n e m y C - p 7 5 6 . 7 1 0 7 . 6 e n e n o m i L 4 7 9 . 7 1 4 6 . 0 e n e r d n a l l e h P - a t e b 4 7 0 . 8 1 5 3 . 0 e l o e n i C - 8 , 1 5 6 1 . 8 1 4 1 . 0 e n e n i p r e T - a m m a g 3 3 8 . 9 1 3 0 . 1 e n e l o n i p r e T 8 4 6 . 1 2 6 0 . 0 e n e m y c - p - o r d y h e D 8 4 9 . 1 2 22.605 Linalool 0.39 4 0 . 0 l o h c n e F - o d n e 5 4 9 . 3 2 7 0 . 0 l a n e l o h p m a C - a h p l a 4 5 4 . 4 2 6 0 . 0 l o e v r a c o n i P - s n a r t 9 1 4 . 5 2 25.853 Camphor 0.08 4 0 . 0 l a l l e n o r t i C 8 0 2 . 6 2 0 3 . 0 l o e n i p r e T - a t e b - s n a r t 7 1 4 . 6 2 5 0 . 0 l o e n r o b o s I 5 9 9 . 6 2 27.584 Borneol 1.43 5 2 . 0 l o - 4 - n e n i p r e T 5 7 1 . 8 2 3 0 . 0 l o - 8 - n e m y C - p 8 7 5 . 8 2 8 8 . 0 l o e n i p r e T - a h p l a 4 7 1 . 9 2 5 2 . 0 e t a t e c a l y h c n e F - o d n e 4 4 7 . 0 3 4 0 . 0 l o l l e n o r t i C 0 3 3 . 1 3 6 0 . 0 e t a t e c a l y n e h t n a s y r h C 4 7 7 . 4 3 2 1 . 0 e t a t e c a l y v r a c o n i P - s n a r t 4 3 0 . 5 3 8 4 . 0 3 e t a t e c a l y n r o B 1 3 3 . 5 3 3 1 . 1 e t a t e c a l y n r o b o s I 0 6 4 . 5 3 35.927 Black Spruce unidentified 0.08 6 0 . 0 e t a t e c a l y v r a c o n i P - s i c 8 1 0 . 6 3 38.478 Black Spruce unidentified 0.06 7 0 . 0 e t a t e c a l y n i p r e T - a h p l a 9 9 3 . 9 3 7 0 . 0 e t a t e c a l y l l e n o r t i C 7 1 6 . 9 3 8 2 . 0 e t a t e c a l y n a r e G 4 7 4 . 1 4 4 0 . 0 e n e m e l E - a t e b 3 2 2 . 2 4 43.489 Junipene 0.10 6 1 . 0 e n e l l y h p o y r a C - a t e b 3 3 1 . 4 4 5 0 . 0 e n e l u m u H - a h p l a 5 8 3 . 6 4 47.588 trans-Cadina-1(6),4-diene 0.07 8 0 . 0 D e n e r c a m r e G 3 6 9 . 7 4 5 1 . 0 e n e l o r u u M - a h p l a 8 4 0 . 9 4 1 2 . 0 e n e n i d a C - a m m a g 9 1 9 . 9 4 7 6 . 0 e n e n i d a C - a t l e d 3 3 2 . 0 5 4 0 . 0 e n e h p r o m A - a h p l a 2 2 3 . 1 5 3 1 . 0 r e m o s i e n e l o b a s i B 2 8 5 . 1 5 7 0 . 0 l o n i d a C - a h p l a - i p e 5 4 4 . 7 5 7 0 . 0 l o n i d a C - a t l e d 7 4 5 . 7 5 5 1 . 0 l o n i d a C - a h p l a 0 9 1 . 8 5 100.00 Chromatogram Spruce Oil, Black, Canada min 7,635,731 10.0 20.0 30.0 40.0 50.0 60.0 TIC 8.583 9.792 11.775 11.926 12.352 13.151 13.255 14.426 14.517 14.834 15.457 16.524 16.680 17.183 17.657 17.974 18.074 18.165 19.833 21.648 21.948 22.605 23.945 24.454 25.419 25.853 26.208 26.417 26.995 27.584 28.175 28.578 29.174 30.744 31.330 34.774 35.034 35.331 35.460 35.927 36.018 38.478 39.399 39.617 41.474 42.223 43.489 44.133 46.385 47.588 47.963 49.048 49.919 50.233 51.322 51.582 57.445 57.547 58.190 Sample Information Analyzed by : Dr. Robert S. Pappas Analyzed : 9/18/2018 2:46:19 AM Sample Type : Essential Oil Sample Name : Spruce Oil, Black, Canada Sample ID : D0B0913E Injection Volume : 0.10 Instrument ID: : GC-3 This report is valid for 1 year from the analyzed date. ©Copyright 2018 by Essential Oil University. All rights reserved. Any publishing, copying, use, dissemination, or distribution of this report, including online, without the express written permission of Essential Oil University is strictly prohibited. Comments: The analysis of this Spruce, Black, Canada batch sample meets the expected chemical profile for authentic essential oil of Picea mariana. No contamination or adulteration was detected

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Page 1: Sample Information An al yzed b ˜˜ : Dr . Ro ert S P pp s ... · 9 79 2 11. 77 5 11. 92 6 12. 2 13 ... 58 96 49 04 8 49. 91 9. 23 3 51 32 2 51 58 2 57 44. 54 7 58 19 0 Sample Information

Peak Report TIC R.Time Name Area%

30.0 lone-)Z(3-xeH 385.8 9.792 Santene 0.84

54.1 enelcycirT 577.11 41.0 enejuhT-ahpla 629.11 10.71 eneniP-ahpla 253.21 41.0 enehcneF-ahpla 151.31 92.01 enehpmaC 552.31 30.0 enemyC-o 624.41

14.517 Sabinene 0.11 07.01 eneniP-ateb 438.41

15.457 Myrcene 1.81 61.0 enerdnallehP-ahpla 425.61

16.680 3-Carene 9.59 81.0 enenipreT-ahpla 381.71 03.0 enemyC-p 756.71 07.6 enenomiL 479.71 46.0 enerdnallehP-ateb 470.81 53.0 eloeniC-8,1 561.81 41.0 enenipreT-ammag 338.91 30.1 enelonipreT 846.12 60.0 enemyc-p-ordyheD 849.12

22.605 Linalool 0.39 40.0 lohcneF-odne 549.32 70.0 lanelohpmaC-ahpla 454.42 60.0 loevraconiP-snart 914.52

25.853 Camphor 0.08 40.0 lallenortiC 802.62 03.0 loenipreT-ateb-snart 714.62 50.0 loenrobosI 599.62

27.584 Borneol 1.43 52.0 lo-4-nenipreT 571.82 30.0 lo-8-nemyC-p 875.82 88.0 loenipreT-ahpla 471.92 52.0 etateca lyhcneF-odne 447.03 40.0 lollenortiC 033.13 60.0 etateca lynehtnasyrhC 477.43 21.0 etateca lyvraconiP-snart 430.53 84.03 etateca lynroB 133.53 31.1 etateca lynrobosI 064.53

35.927 Black Spruce unidentified 0.08 60.0 etateca lyvraconiP-sic 810.63

38.478 Black Spruce unidentified 0.06 70.0 etateca lynipreT-ahpla 993.93 70.0 etateca lyllenortiC 716.93 82.0 etateca lynareG 474.14 40.0 enemelE-ateb 322.24

43.489 Junipene 0.10 61.0 enellyhpoyraC-ateb 331.44 50.0 enelumuH-ahpla 583.64

47.588 trans-Cadina-1(6),4-diene 0.07 80.0 D enercamreG 369.74 51.0 eneloruuM-ahpla 840.94 12.0 enenidaC-ammag 919.94 76.0 enenidaC-atled 332.05 40.0 enehpromA-ahpla 223.15 31.0 remosi enelobasiB 285.15 70.0 lonidaC-ahpla-ipe 544.75 70.0 lonidaC-atled 745.75 51.0 lonidaC-ahpla 091.85

100.00

Chromatogram Spruce Oil, Black, Canada

min

7,635,731

10.0 20.0 30.0 40.0 50.0 60.0

TIC

8.58

3

9.79

2 11.7

7511

.926

12.3

5213

.151

13.2

55

14.4

2614

.517

14.8

3415

.457

16.5

2416

.680

17.1

8317

.657

17.9

7418

.074

18.1

65

19.8

33

21.6

4821

.948

22.6

05

23.9

4524

.454

25.4

1925

.853

26.2

0826

.417

26.9

9527

.584

28.1

7528

.578 29

.174

30.7

4431

.330

34.7

7435

.034

35.3

3135

.460

35.9

2736

.018

38.4

7839

.399

39.6

17

41.4

7442

.223

43.4

8944

.133

46.3

85

47.5

8847

.963

49.0

4849

.919 50.2

33

51.3

2251

.582

57.4

4557

.547

58.1

90

Sample Information����Analyzed by : Dr. Robert S. Pappas

����Analyzed : 9/18/2018 2:46:19 AM����Sample Type : Essential Oil����Sample Name : Spruce Oil, Black, Canada

����Sample ID : D0B0913E����Injection Volume : 0.10

����Instrument ID: : GC-3� �� �� �� � This report is valid for 1 year from the analyzed date.

©Copyright 2018 by Essential Oil University. All rights reserved. Any publishing, copying, use, dissemination, or distribution of this report, including online, without the express written permission of Essential Oil University is strictly prohibited.

Comments:

The analysis of this Spruce, Black, Canada batch sample meets theexpected chemical profifile for authentic essential oil ofPicea mariana. No contamination or adulteration wasdetected

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