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Science & Technology Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder and Jacob George 09-28-2011 Presented at the 2011 COMSOL Conference in Boston

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Page 1: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

Science & Technology

Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration

Amit Halder and Jacob George

09-28-2011

Presented at the 2011 COMSOL Conference in Boston

Page 2: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

2 © Corning Incorporated 2011 Science & Technology

Corning Incorporated Founded:

1851

Headquarters:

Corning, New York

Employees:

~ 26,000 worldwide

2010 Sales:

$6.6 Billion

Fortune 500 Rank (2011):

350

• Corning is the world leader in specialty glass and ceramics.

• We create and make keystone components that enable high-technology systems for consumer electronics, mobile emissions control, telecommunications, and life sciences.

• We succeed through sustained investment in R&D, 160 years of materials science and process engineering knowledge, and a distinctive collaborative culture.

Page 3: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

3 © Corning Incorporated 2011 Science & Technology

Corning Market Segments and Additional Operations

• Emerging Display Technology

• Drug Discovery Technology

• New Business Development

• Equity Companies • Cormetech, Inc. • Dow Corning Corp. • Eurokera, S.N.C. • Samsung Corning

Precision Materials Co., LTD (SCP)

• Cell Culture & Bioprocess

• Assay & High-Throughput Screening

• Genomics & Proteomics

• General Laboratory Products

• LCD Glass Substrates

• Glass Substrates for OLED and LTPS-LCD

• Optical Fiber & Cable

• Hardware & Equipment • Fiber optic

connectivity products

• Emissions Control Products • Light-duty gasoline

vehicles • Light-duty and

heavy-duty on-road diesel vehicles

• Heavy-duty non-road diesel vehicles

• Stationary

• Corning® Gorilla® Glass

• Display Optics & Components

• Optical Materials • Semiconductor

materials • Specialty fiber • Polarcor™

• Optics • Aerospace and

Defense • Ophthalmic

Specialty

Materials

Other

Products

& Services

Life

Sciences Telecom

Display

Technology

Environmental

Technologies

Page 4: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

4 © Corning Incorporated 2011 Science & Technology

Corning’s strength is based on a broad portfolio of core technologies…

… and the ability to integrate them.

Core Capabilities

Modeling and

Simulation

Semiconductor

Materials and

Processes

Thin Films

and

Surface

Sciences

Optical Physics

and Network

Technologies

Biochemical

Sciences

Organic

Materials

and

Processes

Inorganic

Materials

and

Processes

Characterization

Sciences and

Services

Network Integration

and Connectivity

Research

Systems Engineering

Research & Development

Page 5: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

5 © Corning Incorporated 2011 Science & Technology

Ideas Major

Opportunities

Research Development Engineering

Customer & Market Understanding

Identify

many high

value ideas

Select highest

value opportunities;

Optimize value proposition

Scale up

for commercial

capacity

Research & Development Pipeline Management

Page 6: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

6 © Corning Incorporated 2011 Science & Technology

Microwave drying is one of the steps in the process Faster and cheaper

Models are critical in analysis and optimization

Microwave drying of ceramic substrates

Mixing Extrusion Drying Firing

Page 7: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

7 © Corning Incorporated 2011 Science & Technology

Ceramic Structure

Heating,

Vaporization,

Transport

How is microwave drying taking place?

Page 8: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

8 © Corning Incorporated 2011 Science & Technology

Equilibrium Moisture & vapor

pressure

Water Pressure driven Capillarity (sat, temp) driven

Vapor Pressure driven Diffusion in air

Air Pressure driven Diffusion in vapor

Energy Convection & Conduction Evaporation Microwave absorption

Transport Model: Porous Media Assumption

Page 9: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

9 © Corning Incorporated 2011 Science & Technology

Modeling Strategy

Microwave dryer and material geometry

Solve Maxwell’s equations

Solve transport model

Governing Equations

Boundary Conditions Input Parameters

Input Parameters Boundary Conditions Initial Conditions

Velocity Equations Concentration Equations Temperature Equation

Update dielectric properties

Page 10: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

10 © Corning Incorporated 2011 Science & Technology

Require a robust model Computationally intensive if all physics included

Reduce the problem to include important physics Experiments Modeling

Micro scale models

Reduced model Robust Scale up easier

Page 11: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

11 © Corning Incorporated 2011 Science & Technology

Conjugate model (half channel + half wall)

Page 12: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

12 © Corning Incorporated 2011 Science & Technology

Multiphase heat and mass transport model: Equations

1

).()(

gw

www

SS

InSt

1

).()(

2

av

vgav

g

g

gvggvgg IxDMMC

SuSt

gegp

g

g

gggggggg uuk

SPuuSuSt

22 )()(.)(

IuSt

gggg

).()(

QITkTnCt

TC efffluidfluidpeffpeff

.,,

gveqv SKI ,

Liquid phase and Gas phase mass

balance

Mass balance of Air and Vapor in the gas phase

Momentum balance of gas phase

Energy balance of mixture

Convection and diffusion equation

Stefan-Maxwell’s multi species diffusion equation

Weakly compressible Navior-Stokes equation

Conduction and convection equation

ww

w

p

wwcap

w

p

ww

w

p

wwcap

w

p

www cDP

kP

kP

kPP

kn

)(

Scalar expressions

Comsol Implementation

Page 13: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

13 © Corning Incorporated 2011 Science & Technology

Results: Transient pressure and mass flux profiles along the wall

Wall in the

conjugate

model Channel in the

conjugate model

Wall

surface

Page 14: Science & Technology · Science & Technology . Microwave drying of cellular ceramic substrates: A conjugate modeling approach to understand surface moisture migration Amit Halder

14 © Corning Incorporated 2011 Science & Technology

Conclusions Micro scale model of one channel and one wall developed

Model is qualitatively validated against experiments

Fundamental understanding of drying phenomenon is enhanced by using conjugate model